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Hydrolab DS5X, DS5, and MS5 Water Quality Multiprobes

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1. En Sensor Description Cat No o o Chloropyll a 007284 T Rhodamine WT 007285 NL D f a Blue green Algae 007293 2 4 4 DS5 Sensor Options Sensor Description Cat No Hach LDO Sensor 007455 Clark Cell Dissolved Oxygen Conductivity 004467 Clark Cell Dissolved Oxygen 004470 Conductivity with pH Return 004468 Total Dissolved Gas 004469 pH and ORP with Integrated Reference 004454 pH with Integrated Reference 004446 Low lonic Strength Reference 004445 pH 004461 pH and ORP 004462 Chloride 004496 Nitrate 004494 Ammonium Ammonia 004492 Standard Reference 004463 Circulator 007245 4 beam Turbidity DS5 only 004524 Standard Turbidity DS5 only 004466 Self cleaning Turbidity 007140 uu 1 e Chlorophyll a 007202 Rhodamine WT 007204 d fff 12 2 4 1 DS5 Sensor Options continued General Information Sensor Description Cat No i IL Blue green Algae 007291 13 Visit us at www hachenvironmental com Section 3 Installation DANGER Only qualified personnel should conduct the tasks described in this section of the manual 3 1 Unpacking the Instrument Remove the multiprobe from its shipping carton and inspect it for any visible damage Contact Customer Service at 1 800 949 3766 if any items are missing or damaged
2. Range 0 to 50 mg L EE EE Resolution 0 01 mg L ORP Range 999 to 999 mV Accuracy 20 mV Resolution 1mV Depth Vented Level Range Oto 10m Accuracy t0 01m Resolution 0 001 m Depth 0 25 m Range 0to 25m Accuracy 0 05 m Resolution 0 01 m Depth 0 100 m Range O to 100m Accuracy 0 05 m Resolution 0 01 m Depth 0 200 m Range 0 to 200 m Accuracy t0 1m Resolution 0 1m Hach LDO Sensor Range 0 30 mg L Accuracy 0 01 mg L for 0 8 mg L 0 02 mg L for greater than 8 mg L Resolution 0 01 or 0 1 mg L Salinity Range 0 to 70 ppt Accuracy t 0 2 ppt Resolution 1mV 4 beam Turbidity DS5 Only Range 0 to 1000 NTU Accuracy 5 of reading 1 NTU Resolution 0 1 NTU 100 NTU 1NTU 2 100 NTU Specifications Self cleaning Turbidity Range 0 to 3000 NTU Accuracy 1 up to 100 NTU 3 up to 100 400 NTU 5 from 400 3000 NTU Resolution 0 1 up to 400 NTU 1 0 400 3000 NTU Ammonium Ammonia Range 0 to 100 mg L N Accuracy Greater of 5 of reading or 2 mg L N typical Resolution 0 01 mg L N Nitrate Range 0 to 100 mg L N Accuracy Greater of 5 of reading or 2 mg L N typical Resolution 0 01 mg L N Chloride Range 0 5 to 18 000 mg L Accuracy Greater of 5 of reading or 2 mg L typical Resolution 0 0001 units Total Dissolved Gas Range 400 to 1300 mmHg Accu
3. Communication Port Scan Scan for sondes at all COM ports Scan at COM parts in list fi 2 5 Port Numbers must be separated by semi colons Use to specify a range of port numbers Example 1 3 8 12 PC Baudrate fi 9200 Use automatic Baudrate Scan w Use Extended Timeout 15 s Port Preferred Units Temperature Celsius m Depth meter Y Battery vot Y Log Files Log File Format Spreadsheet M Format Options Date Order County specific zl Digits for Y ear 5 sl Date Separator County specific zl Time Separator County specific zl Radix County specific zl DK Cancel Troubleshooting using Terminal Mode Check the PC and terminal emulation or communication software e Start the communications software before connecting the instrument e Verify that the PC is on and that communication software is running e Verify that the correct communication port was selected COM 1 2 3 4 e Verify that the terminal was set to ANSI terminal emulation and that the correct baud rate 19200 eight bits no parity and one stop bit 19200 8 N 1 was selected e If using a 100 meter or longer cable with the Surveyor make sure the terminal baud rate is set to 9600 and the Sonde baud rate is 9600 55 Troubleshooting Check the power cables and connections e Verify that the PC and multiprobe are prop
4. 1 Allen Screw 4 Battery Clip 2 Housing 5 Lithium Battery 3 Retaining Screw 41 Maintenance Figure 18 leue LI L E Pes M Replacing the Lithium Battery on the MS5 SV TOHCAH S a a g LIII a 1 Allen Screw 4 Retaining Screw 2 Housing 5 Battery Clip 3 Sonde Body 6 Lithium Battery 6 3 Storage and Care Recommendations 6 3 1 Mulitprobe and Sensor Storage Fill the DS storage cup or MS cup with one inch of clean tap water and screw the cup on the multiprobe To prevent sensors from freezing store the multiprobe where freezing will not occur Remove batteries for long term storage 8 size C alkaline batteries for the DS5 or DS5X or 8 size AA alkaline batteries for the MS5 Do not remove the lithium battery which powers the mulitprobe internal clock Store equipment in a carrying case Cat No 011780 or a large plastic container with a circular piece of foam rubber for shock protection Lay the cable in coils of at least 15 cm 6 in diameter at the bottom of the plastic container 6 3 2 Electrical Cable Care 42 Protect all non waterproof cables i e all cables except the waterproof underwater cable from any water source during operation in the field Keep connectors dry at all times Properly lubricate the sealing surface of all u
5. ssssseseeeeeeennennnenns 27 4 3 3 1 Creating Log Files e ct e petet ett eee tere tb teet n e en DE A okie 27 4 3 3 2 Downloading Log Fios EE 28 Section 5 E Un EE 29 5 1 Deployment Considerations nene tierce tee eege n tete it o aaa Hee Ga eee co i E 20 29 Hell Pressure Extremes uite Re UID E hh Dem 29 571 2 Temperature Extremes ss nce ete det dete ee Eee ie ie Eee odere tk e ee steier be 29 Sro Data Transmission Lines iie tih ET 29 5 1 4 Minimum Depth Requirements eseeeeesesesesessseeseeneeee EAEE een EKAA EENES YENA PENAN en trn iS nnne nene cinese 29 5 2 Deployment in Open Waters sssssssssssssssseseseeeneeennen ener enne EEAS sen rene inns sin ret eterni ntis etre nennen nenene 30 5 2 1 Minimum Clearance Requirements nennen nnns nnne enr sin nrt sentes en nennen 30 5 2 2 Long term Deployment in Open Waters enne nn trennen senten 30 5 2 2 1 Anchoring the DS5 or DS5X using the Support Bail 31 5 2 2 2 Anchoring the MS5 using the Balkt eene 32 5 2 2 3 Anchoring the MS5 using the Mooring Fixture sssssssseseeeenennee enne 32 Table of Contents 5 2 3 Short term Deployment in Open Waters nennen nnne nnns entere nnns nnne 33 5 2 4 Minimum Flow Heouremenmts A 35 5 2 5 Non submersible Deployment sss nennen sienne innen nnne 35 Section 6 Maintenance EMMMM 37 6 1 Multiprobe and Accessory Maimtenanmce cece eee enne cette ene ee sete ae ee sete nenere
6. 2 Enter the barometric units mmHg using Hydras 3 LT or a Surveyor 3 Enter the D O units in mg L using Hydras 3 LT or a Surveyor Note If there is a change in barometric pressure after calibration for instance if barometric pressure drops as you move the calibrated Transmitter to a higher elevation for deployment the readings for D O Saturation will not be correct You must enter a new barometric pressure However the readings for D O mg L will be correct regardless of changes in barometric pressure Operation 4 2 7 Pressure Sensor Calibration Note The density of water varies with specific conductance Pressure readings are corrected for specific conductance 1 Remove water from the calibration cup 2 Point sensors down 3 Enter zero for the standard using Hydras 3 LT or a Surveyor 4 2 8 pH ORP Calibration 1 Pour the pH or ORP standard to within a centimeter of the top of the cup 2 Enter the units for pH or ORP using Hydras 3 LT or a Surveyor Note pH is a two point or three point calibration A pH standard between 6 8 and 7 2 is treated as the zero and all other values are treated as the slope First calibrate zero then calibrate slope After the sensors have been properly maintained the sensors can be calibrated Always allow sufficient time for thermal stabilization of the standards To reduce the time for stabilization try to keep all calibration standards and equipment stored at the sam
7. Once the Sonde has been placed in TTY mode it will no longer communicate with Hydras3LT except in terminal mode The Sonde will retain its current baud rate Any ANSI terminal emulator may be used to communicate with the Sonde at 8 data bits No Parity and 1 stop bit External Communications B 6 1 TTY Menu and Commands The TTY menu is accessed by first pressing the spacebar or sending an ASCII space character The multiprobe will finish any line in progress and then start a new line by sending lt cr gt lt lf gt followed by the menu lt cr gt lt lf gt HM lt sp gt The multiprobe will echo the user entry if it is listed in the menu otherwise an ASCII BEL character is sent An ASCII escape character will abort the menu after displaying a cancel message Responding with a will produce a verbose version of the menu lt cr gt lt lf gt Main Menu lt cr gt lt lf gt H eader lt cr gt lt lf gt M easure lt cr gt lt lf gt Q uit TTY Mode lt cr gt lt lf gt Please enter your choice lt sp gt A H eader Responding with an H will show a header identifying the data fields with name and units In addition the instrument ID is displayed HM lt sp gt H lt cr gt lt lf gt lt cr gt lt lf gt Instrument Id lt cr gt lt lf gt lt cr gt lt lf gt lt sp gt lt sp gt Time lt sp gt lt sp gt lt sp gt Temp lt sp gt lt sp gt lbatt lt cr gt lt lf gt HHMMSS lt sp gt lt sp gt lt sp gt lt sp gt lt sp gt C lt sp gt
8. c1 1 2813 x 10 11 c 2 2129 x 10 9 cg 1 4771 x 10 7 c4 4 6475 x 10 6 Cg 5 6170 x 10 5 cg 8 7699 x 10 4 c 6 1736 x 102 cg 1 9524 e StdMth will remove any temperature compensation so the readings are equivalent to conductivity f T 1 e Custom will provide a compensation function that the user can define according to the following function f T aT bT cT dT4 eT fT gT h Select the Set Range 1 Auto 2 High 3 Mid or 4 Low e Auto default allows the multiprobe to automatically select the most appropriate range to measure conductivity The multiprobe will dynamically change the range based on the current measurement conditions over 0 100 mS cm The resolution of the displayed data will also change to accommodate the current range in use e High Mid and Low force the multiprobe to measure conductivity using a fixed range If low range is selected the readings will indicate an over ranged condition for values above 1 5 mS cm The Mid range will over range at 15 mS cm These choices also force the displayed readings to a fixed point or constant resolution format primarily only needed for certain SDI 12 data loggers Otherwise it is best to always select the Auto choice as this gives the best accuracy and performance for the conductivity sensor Select the computation method for salinity 1 2311 or 2 StdMth e 2311 default salinity is computed using an algorithm adapted from the
9. Operation 4 2 2 Calibrating the Sensors Using Hydras 3 LT For more information on Hydras 3 LT refer to the Quick Start Guide Cat No 6234289 or press the F1 key while Hydras 3 LT is active 1 Attach the power and data cable to the Sonde Attach the 9 pin connector to a PC 2 Start Hydras 3 LT Wait for the software to scan for connected Sondes Highlight the multiprobe and press OPERATE SONDE Note If the Sonde appears to be connected and the software does not recognize the Sonde connection remove and replace the connector cable and press RE SCAN FOR SONDE Repeat until Hydras 3 LT recognizes the Sonde 3 Click on the Calibration Tab and click on the parameter to be calibrated 4 Enter the calibration values and click CALIBRATE Ey Hydrolab COM 1 of x System Online Monitoring Log Files Parameter Setup Calibration Settings Software BP mmHg pH Units ORP mv Dep200 meters Turbidity NTUs i SpCond yS cm Res kO cm Zelle TDS g DO Sat Current Value 4 8 mS cm Temp 24 78 C 10 31 2003 2 52 28 PM gt SpCond mS cm Enter SpCond standard mS cm Calibrate 2 52 28 PM E 23 Operation 4 2 3 Calibration Preparation The following is a general outline of the steps required to calibrate all the sensors e Select a calibration standard whose value is near the field samples e Clean and prepare the sensors e To ensure accuracy o
10. The network devices may operate without the signal ground connection but may not be reliable Some RS485 applications require impedance termination because of fast data rates or long cables The most popular termination involves installing a V2 watt resistor across the receiver at each end of the network See the RS485 interface user manual for termination requirements on the PC being used Alternatively the preferred network may be AC terminated by placing a 0 01 uF capacitor in series with the terminating resistor The capacitor appears as a short circuit during signal transitions but appears as an open circuit to any DC loop current This will reduce the power supply current required to operate the network and still provide the proper terminating impedance Do not add a terminating resistor to every receiver in the network For networks with more than about four nodes the transmitters will be unable to drive the cable Only terminate both ends of the main cable B 4 Modbus Interface 60 The multiprobe is configured to respond to Modbus function 3 Read Holding Registers in RTU mode through the RS232 or RS485 communications port at 19200 baud 8 data bits Even Parity and 1 stop bit 19200 8 E 1 All data values are returned in IEEE Floating Point Format 4 bytes Each data value is returned in two 16 bit words with the low word being transmitted first Within each word the high byte is transmitted first Each byte is transmitted
11. 1 External Power 3 RS232 TXD 5 RS485 or SDI 12 DATA 2 Ground 4 RS232 RXD 6 RS485 or SDI 12 RETURN Figure 22 Wiring Diagram for Cable 015xxx 6 Pin Marine to DB 9 6 Pin Marine DB 9 4 Brown External Power 4 2 Red Ground Return 6 Orange RS 232 TXD SS 3 5 o 4 4 Yellow RS 232 RXD 3 8l o o l3 5 Green RS 485 or SDI Data 2 7 l2 Female 6 Blue or Black RS 485 or SDI Return 8 6 o oli 9 Female Figure 23 Wiring Diagram for Cable 013510 DB 9 to External Data Device xd External Power Connector Na DNA NE End View Female qub cB DB9 J J vM 4 External Power Brown efo 2 1 6 7 NC 7o 5 Ground Red 8 o o l4 3 RS 232 TXD Yellow ol o ale 2 RS 232 RXD Green 8 RS 485 or SDI Data Orange Male 9 RS 485 or SDI Return Blue or Black Table 5 Wiring Connections for External Device Cable 013510 Wire Color RS232 RS485 SDI 12 Brown 12VCD IN 12VDC IN 12VCD IN Red Shield Ground Ground Ground Green RS232 RX Yellow RS232 TX Orange RS485 SDI DATA Blue or Black RS485 SDI RETURN 59 External Communications B 3 RS485 Interface Series 5 Multiprobes are compatible with RS485 interfaces RS485 is a standard that specifies a particular method to transmit and receive digital signals This standard is maintained by the Electronic Industries Association in a document titled Standard for Electrical Characteristics of Generators and Receivers for U
12. Communications Data values that are too large to fit in the constant width field are modified so that the numeric digits are displayed as for example The sign and decimal point are preserved C Q uit Responding with a Q or q will reset the multiprobe to full terminal mode and can then be connected to Hydras 3 LT B 6 2 Data Display If the TTY menu is not used a line of data is periodically displayed on the next available line If the screen is full the lines are scrolled All data lines are terminated with lt cr gt lt lf gt and have the same formatting as the M easure command described above 66 Appendix C Using HyperTerminal C 1 HyperTerminal Setup 1 After starting Windows click on the Start button 2 Select Programs gt Accessories gt Communications gt Hyperterminal 3 Enter a name and choose an icon for the application and click OK 4 Select the COM port and click OK Set the communication in a 19200 8 N Xon Xoff format 5 Configure HyperTerminal so the functions arrows and Ctrl keys act as terminal keys not window keys Select the ANSI terminal emulation File gt Properties gt Settings 6 Use Table 9 to communicate with or recover information from the multiprobe Table 9 HyperTeminal Commands Follow the Path Help Help Topics Index HyperTerminal To Displays the on line help utility File Properties Phone number Configure Maximum speed File Properties Ph
13. and connecting the multiprobe to the computer please check the following items Troubleshooting Hydras 3LT If Hydras 3LT does not automatically detect the Sonde when launched Press the RE SCAN FOR SONDES button BER File Help Connected Sondes Pot Sonde sd Operate Sonde Terminal Mode Log Files Pot LlogFie Less Download Selected Files Delete files in sonde after reading If communication is still not established after several attempts try the following 1 Verify that the instrument is powered on and functioning 2 Check power cables and connections Verify that your PC and multiprobe are properly connected to the wall outlet or external battery if used 3 Verify that the input voltage to the multiprobe is between 7V and 18V 4 lf your multiprobe is equipped with an internal battery pack check the batteries polarity and voltages 53 Troubleshooting Verify the Hydras 3 LT Communication Settings 1 Select File gt Options from the Hydras 3 LT Connection Screen C ini xi Bile Heb Download Selected Files Delete files in sonde after reading 2 Ifthe Sondes PC baud rate and COM port are known disable the COM Port and baud rate auto scans and set Hydras3LT to use the known values 54 Troubleshooting 3 In addition the connection timeout may be extended from 10 to 15 seconds which will allow time for additional retries Graphic DataSonde
14. buoyancy of fish eggs and other organisms Transducer Any device or element which converts an input signal into an output signal of a different form ex doorbell microphone The depth or vented level transducer Turbidity The measure of the clarity of a liquid by using colorimetric scales It is also the expression of the optical property that causes a light to be scattered and absorbed rather than transmitted in straight lines through a sample Turbidity is the opposite of clarity ITM A measure of the opacity or translucence of water The main objective is to determine the scattering of light by particles of a body of water and report that scattering in some unit of measurement usually nephelometric turbidity units or NTU based on a primary turbidity standard called formazin Turbidity is caused by plankton both animal and plant clay suspended clay silt etc Although these substances impart color color resulting from turbidity is referred to as apparent color and should not be confused with true color resulting from dissolved substances Apparent color can also result from overshading by vegetation or substrate bottom material color Vented depth ITM The multiprobe transducer measuring depth from 0 to 10 meters See Depth Zero ITM A system s zero is an anchor point set either temporarily by calibration or permanently by design This point can easily be established either electronically or by using laboratory s
15. generates highly reproducible potentials used for pH ORP and ammonium measurements and polarographic analyses e g silver silver chloride electrode Resistivity Resistivity is the electrical resistance offered by a material to the flow of current times the cross sectional area of current flow and per unit length of current path It is the reciprocal of conductivity and is also known as electrical resistivity and specific resistance Resistance declines as ion content increases Response time The time required for a system to react by a prescribed amount to a step change in some variable The extent of the response must be stated as in to 95 of total change or to within 0 1 mg I of the final reading example for D O Salinity Salinity is the measure of the total quantity of dissolved salts in water Salinity refers to the ionic strength of natural waters Salinity and salt concentration are the only terms that can be used when referring to the relative concentration of certain salts in bays estuaries and oceans SDI 12 SDI 12 is a standard used to interface data recorders with microprocessor based sensors SDI 12 stands for serial digital interface at 1200 baud SDI 12 is intended for applications with the following requirements battery powered operation with minimal current drain low system cost use of a single data recorder with multiple sensors on one cable and up to 200 feet of cable between a sensor and a data re
16. lt sp gt Volts lt cr gt lt lf gt The first line is free field text up to 20 characters in length The next line is skipped and the data names are printed The names are right justified with leading spaces inserted to produce a constant width field Most fields are 6 characters wide however fields can also be 5 7 or 8 characters wide The name fields are always separated with a space Any name may appear in any field depending on how the user configured the data display in ANSI mode The next line shows the corresponding units for the data fields The units are right justified text with leading spaces inserted to produce a constant width field equal to the name field The name fields are always separated with a space B M easure Responding with an M will force the multiprobe to send one line of data without waiting for the next data display interval This is useful for synchronizing data acquisition software with the multiprobe data output The data values are right justified to fill a constant width field of 5 6 7 or 8 characters HM lt sp gt M lt cr gt lt lf gt 231302 lt sp gt lt sp gt 24 59 lt sp gt lt sp gt lt sp gt 12 0 lt cr gt lt lf gt Data values may also be appended with a special character or Data values without an appended character will always have a space separator however the appended character may be the only separator between values a space separator is not guaranteed 65 External
17. power puissance of the hydrogen ion H activity pH is a major factor affecting the availability of nutrients to plants and animals It controls in part the concentration of many biochemically active substances dissolved in water and it affects the efficiency of hemoglobin in the blood of vertebrates e g fish and invertebrates e g shrimp as well as the toxicity of pollutants Probe A small tube containing the sensing elements of electronic equipment The probe is an essential part of the water quality monitoring system since it obtains measurements and data which can be stored analyzed and eventually transferred to a computer Probe assembly See Assembly Profiling Electrical exploration wherein the transmitter and receiver are moved in unison across a structure to obtain a profile of mutual impedance between transmitter and receiver lateral search In water quality this term is used as the contrary of unattended monitoring An operator connects the multiprobe to a computer equipped with a communications software Then he lowers the multiprobe in the water and receives measurements from the instrument The data is displayed on the computer screen The multiprobe can be lowered to different locations along the sample area in order to study the nature of the water based on several points of reference Glossary amp Abbreviations Quinhydrone CgH4O5 C6H4 OH 2 green water soluble powder Quinhydrone is used to cali
18. the specific conductance sensor with a small non abrasive brush or cotton swab Use soap to remove grease oil or biological growth Rinse with water 6 7 ORP Sensor Maintenance If the platinum band or stud of the ORP sensor gets dirty and or discolored polish it with a clean cloth and a very mild abrasive such as toothpaste or use a fine polishing strip Rinse with water Soak the sensor overnight in tap water to allow the platinum surface to restabilize 6 8 pH Electrode Maintenance If the pH sensor is coated with oil sediment or biological growth clean the glass with a very clean soft wet non scratching cloth or cotton ball with mild soap Rinse with tap water If the pH sensor becomes dehydrated soak for 24 hours in a pH 4 buffer solution 44 Maintenance 6 8 1 Standard Reference Electrode i 09 Cc e 1 Gently pull the entire 2 Discard the old 3 Drop two KCl salt pellets 4 Refill the sleeve to the reference sleeve away electrolyte from the Cat No 005376HY into top with reference from the Transmitter reference sleeve the reference sleeve electrolyte Note The porous Teflon Reference Junction is the most important part of the pH and ORP performance Make sure it is clean and passes electrolyte readily If not replace it with the spare provided in the maintenance kit Replacement Reference Junctions are Cat No 000548HY V Note When seating the reference sleeve trapped air and excess elec
19. vinegar into the pressure sensor port with a syringe and soak overnight 2 Soap or rubbing alcohol may be used to remove grease oil or biological material Rinse with water Do not use any objects to poke the sensor or the transducer membrane will rupture 6 11 Other Sensor Maintenance Refer to the sensor specific instruction sheet for more information 46 Section 7 Replacement Parts and Accessories Replacement Parts Description Catalog Number 110 VAC Power Adapter 220 VAC Power Adapter 110 VAC External Battery Pack w Charger 220 VAC External Battery Pack w Charger Battery Adapter Battery Plug Cable 5 meter Cable 10 meter Cable 15 meter Cable 25 meter Cable 30 meter Cable 50 meter Cable 75 meter Cable 100 meter Cable 150 meter Cable 200 meter Cable Reel Carrying Case Calibration Cable Calibration Stand Hydras 3 LT Software CD Kit Cigarette Lighter Adapter Conductivity Standard 0 1 mS cm 1 L Conductivity Standard 1 413 mS cm 1 L Conductivity Standard 12 856 mS cm 1 L Conductivity Standard 47 6 mS cm 1 L Conductivity Standard 0 5 mS cm 1 L DS5 DS5X Bail Kit DS5 DS5X Flow Cell DS5 DS5X Pipe Kit DS5 DS5X Basic Maintenance Kit DS5 DS5X Storage Cup Large DS5 DS5X Storage Cup Cap Large Clark Cell Dissolved Oxygen Maintenance Kit pH Maintenance Kit DS5 DS5X Weighted Sensor Guard Large D O Electrolyte 59 mL D O Membrane Pack D O Memb
20. 16 87437 Kempten Germany Telephone 49 0 831 5617 0 Fax 49 0 831 5617 209 Section 10 Limited Warranty Hach Company warrants the Hydrolab Series 5 Sondes to the original purchaser against any defects that are due to faulty material or workmanship for a period of two years from date of shipment unless otherwise noted In the event that a defect is discovered during the warranty period Hach Company agrees that at its option it will repair or replace the defective product or refund the purchase price excluding original shipping and handling charges Any product repaired or replaced under this warranty will be warranted only for the remainder of the original product warranty period This warranty does not apply to consumable products such as chemical reagents or consumable components of a product such as but not limited to lamps and tubing Contact Hach Company or your distributor to initiate warranty support Products may not be returned without authorization from Hach Company Limitations This warranty does not cover e Damage caused by acts of God natural disaster labor unrest acts of war declared or undeclared terrorism civil strife or acts of any governmental jurisdiction e Damage caused by misuse neglect accident or improper application or installation Damage caused by any repair or attempted repair not authorized by Hach Company e Any product not used in accordance with the instructions furnished by Hach Com
21. CAUTION When loosening removable parts from a multiprobe always point those parts away from your body and other people In extreme conditions excess pressure may build up inside any underwater housing causing the caps sensors or other removable parts to disengage with force which may cause serious injury The Sondes use Hydras 3 LT or a Surveyor to set up parameters and calibrate the sensors Figure 6 Operations Setup Calibration Cable Power Adapter DataSonde 4 s or MiniSonde Windows 98 NT 2000 XP 4 1 Parameter Setup 4 1 1 Using the Surveyor for Parameter Setup For more information on the Surveyor refer to the User Manual Cat No 00719618 1 Attach the power and data cable to the Sonde Attach the 9 pin connector to the Surveyor 2 Turn on the Surveyor Wait approximately 10 seconds for initialization 3 Press SETUP CAL Press SETUP Press SONDE 4 Highlight Parameters and press SELECT 5 Use the ARROW keys to highlight the appropriate parameter and press SELECT 6 Highlight the appropriate function and press SELECT A configuration screen will be displayed Depending on the application use the ARROW keys to change the function press SELECT and DONE to finish 19 Operation 4 1 2 Using Hydras 3 LT for Parameter Setup For more information on Hydras 3 LT refer to the Quick Start Guide Cat No 6234289 or press the F1 key while Hydras 3 LT is active 1 Attach the p
22. CAUTION Indicates a potentially hazardous situation that may result in minor or moderate injury Important Note Information that requires special emphasis Note Information that supplements main points in the text 2 1 2 Precautionary Labels Read all labels and tags attached to the instrument Personal injury or damage to the instrument could occur if not observed This symbol when noted on the instrument references the instruction manual for operation and or safety information This symbol when noted on a product enclosure or barrier indicates that a risk of electrical shock and or electrocution exists and indicates that only individuals qualified to work with hazardous voltages should open the enclosure or remove the barrier This symbol when noted on the product identifies the location of a fuse or current limiting device This symbol when noted on the product indicates that the marked item can be hot and should not be touched without care This symbol when noted on the product indicates the presence of devices sensitive to Electro static Discharge and indicates that care must be taken to prevent damage to them This symbol when noted on the product identifies a risk of chemical harm and indicates that only individuals qualified and trained to work with chemicals should handle chemicals or perform maintenance on chemical delivery systems associated with the equipment This symbol when noted on the
23. Mode aXSS1 aXSS1 lt crlf gt Circulator On aXSS0 aXSS0 lt crlf gt Circulator Off 1 The a used in the SDI 12 commands is the SDI 12 address The Transmitter s factory default SDI 12 address is 0 B 2 Connection to an External Device The Series 5 Multiprobe can communicate with an external device using an RS232 RS485 or SDI 12 interface The RS232 interface is always available The Series 5 Multiprobe must be programmed for communication via an RS485 or SDI 12 interface Two cables are available for external communication a 6 pin marine to DB 9 cable Cat No 015xxx and a DB 9 to external device cable Cat No 013510 for SDI 12 or RS485 interfaces Figure 20 Wiring diagrams for these cables are shown in Figure 22 and Figure 23 Wiring for the 6 pin Sonde connector is shown in Figure 21 Wiring to the external device is detailed in Table 5 Figure 20 Communication Cables for the DS5 DS5X and MS5 Water Quality Sondes a gg T EE w Wu ei 1 Cable 6 pin marine to DB 9 Cat No 015XXX 4 Label wire connections 2 Connection to DS5 DS5X or MS5 5 Connections to external device 3 Cable for SDI 12 RS485 Cat No 013510 6 Connection to power 58 External Communications Figure 21 Wiring for 6 Pin Marine Connector on Multiprobe Male
24. Most Significant Bit first For example the floating point value 1 56 OX3FC7AE14 would be transmitted as OxAE 0x14 Ox3F OxC7 External Communications All available data parameters are stored in Holding Registers within the multiprobe which start counting at 40001 They are addressed in the Modbus message structure with addresses starting at 0 Modbus function 03 is used to request one or more holding register values from the multiprobe Each Holding Register is 16 bits 2 bytes in size therefore two Holding Registers 4 bytes are required to represent a single floating point value Only one slave device can be addressed in a single query The query structure is detailed in Table 6 A complete register list can be found at www hachenvironmental com Table 6 Function 03 Query Structure Byte Value Description 1 1 247 Slave device address 2 3 Function code 3 0 255 Starting address high byte 4 0 255 Starting address low byte 5 0 255 Number of registers high byte 6 0 255 Number of registers low byte 7 0 255 CRC high byte 8 0 255 CRC low byte After processing the query the multiprobe will return the 16 bit Holding Register values that were requested The Holding registers will be transmitted as High Byte first followed by the Low Byte The Modbus response starts with the multiprobe address and the function code 03 The next byte is the number of data bytes that follow This value is two time
25. Note It is normal for a small amount of solution to be in the cup 3 2 Instrument Assembly There are many ways to connect a multiprobe to a display or a personal computer DANGER An electrical shock hazard can exist in a wet or outdoor environment if the multiprobe is powered via the external 115 VAC power supply The safest and preferred method of powering this equipment in wet or outdoor environments is with battery or solar power with a combined voltage not to exceed 15 volts If it is necessary to power the multiprobe with the 115 VAC power supply in a wet or outdoor environment a Ground Fault Interrupt GFI circuit is required The installation of the GFI device must be done by a licensed electrician 1 Remove all protective plugs and keep them in a safe place they will be used again for moving and storage 2 Connectthe calibration cable Cat No 013470 or detachable cable 015XXX to the multiprobe The connectors are keyed for proper assembly Align the bigger pin on the multiprobe male connector to the indicator dots on the female cable connector Do not rotate the cable or force or twist the pins into the connectors to prevent damage to the connector pins 3 Power the instrument by connecting the power receptacle from the calibration cable and external power adapter to an approved battery or power supply see Figure 4 on page 16 4 Connect the other end of the calibration cable detachable cable fixed cable or ext
26. United States Geological Survey Water Supply Paper 2311 titled Specific Conductance Theoretical Considerations and Application to Analytical Quality Control This salinity function is only defined from salinities in the 30 to 40 ppt range mild concentrations and dilutions of sea water This salinity function uses specific conductance values C in mS cm compensated Salinity c4C 4 coC3 c4C c4C C5 where c4 5 9950 x 1078 Goes 2 3120 x 1075 c4 3 4346 x 10 3 c4 5 3532 x 10 1 Ge 1 5494 x 1072 e StdMth salinity will be computed using the Practical Salinity Scale 1978 This algorithm is defined for salinities ranging from 2 to 42 ppt and uses conductivity values corrected to 15 C regardless of the compensation function selected for specific conductance This algorithm is described in section 2520B of Standard Methods for the Examination of Water and Wastewater 18th edition 21 Operation 4 1 4 Clark Cell Dissolved Oxygen Parameter Setup For dissolved oxygen set the following functions using Hydras 3 LT or the Surveyor Enable or Disable Salinity Compensation 4 1 5 pH Parameter Setup For pH set the following functions using Hydras 3 LT or the Surveyor Select either 2 or 3 calibration points 4 1 6 Other Parameter Setup Refer to the sensor specific instruction sheet for more information 4 2 Calibration Sensors are checked for calibration before they leave the factory however calibrati
27. a m to 5 00 p m MST Monday through Friday 800 949 3766 By Fax 970 461 3921 By Mail Hach Environmental P O Box 389 Loveland Colorado 80539 0389 U S A Ordering information by e mail sales hachenvironmental com Ordering Information Required e Account number if available e Billing address e Your name and phone number e Shipping address e Purchase order number e Catalog number e Brief description or model number e Quantity International Customers Hach Environmental maintains a worldwide network of dealers and distributors To locate the representative nearest you send an e mail to sales hachenvironmental com or contact Hach Environmental Loveland Colorado U S A Telephone 970 669 3050 Fax 970 669 2932 Technical and Customer Service U S A only Hach Environmental Technical and Customer Service Department personnel are eager to answer questions about our products and their use Call 1 800 949 3766 or e mail techsupport hachenvironmental com 49 Section 9 50 Repair Service Authorization must be obtained from Hach Company before sending any items for repair Please contact the Hach Service Center serving your location In the United States and Outside Europe Hach Company Hach Environmental Product Repair North Dock 5600 Lindbergh Drive Loveland CO 80539 0389 Telephone 800 227 4224 ext 2080 Fax 970 461 3924 In Europe OTT Messtechnik GMBH amp Co KG Ludwigstrasse
28. a mechanism machine or similar device Probe Assembly The unit containing the component parts of a sensor e g D O component consisting of the D O sensor which is made up of 2 electrodes the cathode and the anode Chloride CI A common anion present in both fresh and sea water It is essentially non toxic and is present in all living cells Conductivity Conductivity is inversely related to the resistance of a solution Conductivity is the ratio of the electric current density to the electric field in a material also known as electrical conductivity In limnology conductivity is a measure of the ability of water to pass an electrical current Compensation of this measurement to 25 C constitutes specific conductance This parameter indicates the amount of dissolved substances salts Salts and their concentration dictate osmoregulatory salt balancing functions in plants and animals The ionic strength of water also regulates the toxicity of many substances See Specific conductance Data collection platform or DCP Hardware system and system software used with a computer program to collect data at one or more locations Depth The vertical distance between the water surface and another level for a multiprobe 0 10 0 25 0 100 or 0 200 meters See Vented depth Derating The reduction of the rating of a device to improve reliability or to predict operation at higher or lower ambient temperatures Dissolved ox
29. and calibrated Ensure the readings displayed are accurate e g for Depth meters feet or psi Table 2 Multiprobe Software Symbols Symbol Description Data Out of Sensor Range User Service Required or Data Outside Calibrated Range but Still within Sensor Range Parameter is Not Calibrated a Temperature Compensation Error Non Temperature Parameter Compensation Error 56 Appendix B External Communications B 1 SDI 12 Interface SDI 12 is an industry originated serial digital interface bus designed to allow an operator to connect a wide variety of sensors meteorological hydrological water quality etc to a single SDI 12 datalogger with a single cable bus The multiprobe is compatible with SDI 12 V1 2 A copy of the specification can be found at www sdi 12 org The optional SDI 12 Interface Adapter Cable is required to operate the multiprobe with an SDI 12 Datalogger Note All three wires one ground must be connected for correct SDI 12 operation A label on the SDI 12 Interface Adapter Cable shows the pinout in Figure 19 1 2 3 Connect the data cable to the SDI 12 Interface Adapter Cable connector Disconnect power from the multiprobe Connect the bare wires at the end of the SDI 12 Interface Adapter Cable to the appropriate connections on the SDI 12 datalogger Follow the label on the SDI 12 Interface Adapter Figure 19 SDI 12 Cable Yellow Or
30. ange Red Oo 1 61 6 l2 7 0 o 13 8 o glo It o J5 Male Brown Table 3 SDI 12 Pinouts Pin Number Wire Color SDI 12 Function 4 Brown 12 VDC 5 Red Ground 8 Orange SDI 12 Data 9 Yellow SDI 12 Return 1 Wire color is valid only for this cable Cat No 007139 Use of other cables or cable modifications may result in instrument damage Consult the SDI 12 datalogger manual for information on how to connect the SDI 12 Interface Adapter Note SDI 12 parameters can be setup through Hydras 3 LT 57 External Communications Table 4 is asummary of the SDI 12 user commands supported by the multiprobe For more details on correct use consult the SDI 12 V1 2 specification Table 4 SDI 12 Commands Command Response Description a a lt crif gt Address Acknowledge Identify all aXXHydrolab YYYYYYZZZZserialnumber XX SDI 12 Support Version lt crif gt YYYYYY Instrument ID ZZZZ Software Version aAb b lt crlf gt Change address from a to b aM adddn lt crlf gt Measure n values in ddd seconds aDx aSvalueSvalue lt crlf gt Report Data aRx aSvalueSvalue lt crlf gt Report Continuous Data aC adddnn lt crif gt Concurrent Measure nn values in ddd seconds aXxC aXC lt crlf gt Initiate a cleaning cycle in units equipped with a wiper ax1 aX1 lt crif gt Enable Continuous Mode aX0 aX0O lt crif gt Disable Continuous
31. available for the DS5 DS5X and MS5 See Replacement Parts and Accessories on page 47 6 1 Multiprobe and Accessory Maintenance 6 1 1 Cleaning the Multiprobe Housing Clean the outside of the multiprobe housing using a clean brush soap and water Always use the DS storage cup or the MS cup filled with one inch of tap water to protect the sensors from damage and especially from drying out whenever the multiprobe is not deployed Do not expose equipment to extreme temperatures below 1 C 34 F or above 50 C 122 F Always rinse the multiprobe with clean tap water soon after returning from deployment 6 1 2 Dryer Maintenance Important Note Do not submerge the dryer in water The in line vented level dryer is a part of the cable and penetrator assembly if the Sonde has the vented depth sensor 0 10 meters The GORE TEX patch round patch on dryer allows gases to come into the dryer and is splash proof but not submersible Any water leaks inside the dryer can block the tube which goes into the multiprobe If water leaks are detected contact Technical Support The dryer contains desiccant bag s white bag to keep condensation from forming inside the vented tube which goes from the dryer to the multiprobe If moisture is detected inside the dryer replace the bags Figure 14 To replace the desiccant bag s 1 Unscrew both dryer nuts and unscrew the dryer cap 2 Inspect the indicator strip If the stripe is
32. brate redox sensors The quinhydrone s redox potential is dependent on the pH of the solution Reading The indication shown by an instrument Redox potential Oxidation reduction potential or ORP Eh Voltage measured at an inert electrode immersed in a reversible oxidation reduction system measurement of the state of oxidation of the system The redox potential measures the tendency of electrons to flow either toward or away from a noble metal electrode A substance gains electrons in a reduction reaction and loses electrons in an oxidation reaction ORP varies from substance to substance and oxidation reduction reactions occur simultaneously hence the determination of the potential rather than of a discrete or qualitative value Oxidation and reduction are in a constant state of flux continuously seeking equilibrium Applications for ORP measurement include but are not limited to the following monitoring oxidation of cyanide and chromate wastes e g metal plating bleaching pulp e g paper manufacturing manufacture of bleach e g monitoring chlorination water pollution e g acid mine drainage and monitoring ozone treatment e g water disinfection ORP data has been used to understand more about how substances in sediments affect the water quality at the bottom of lakes reservoirs and ponds Reduction A reaction that increases the electron content of a substance Reference electrode A nonpolarizable electrode that
33. cm Catalog Number 003078HY Hydrolab DS5X DS5 and MS5 Water Quality Multiprobes USER MANUAL February 2006 Edition 3 Hach Company 2006 All rights reserved Printed in U S A jk dk Visit us at www hachenvironmental com Table of Contents Section 1 Specifications unser ediscere deel a dua ee ee 5 Section 2 General Information ee ceeeeeeeeeeeee ae eeceeee ee aaeeeeeaeeeceaeeeeeaaeeecaeeeseaaeeeseeeeesaaesseaeeeseaeeeseaeeeeed 9 2 Safety Information nic tere ed Ettore ft tava de bei ra et o e adag Pear seo P ese ee aed 9 2 1 1 Use of Hazard Information eicere OL Receta e e HE Ro Den ee de ede Pepe d Ee Dna dex 9 251 2 Precautionary Eabels 1 2 tratan ic eser eee OE cre Pe Pe pd CO Re Cb adsense 9 2 2 DS85 DS5X Multiprob6e co t eR Pk RR Ra eek tue e Bae duke gena ated Eege ra eae ere a Ra ua e ae Ra e pe aetas 10 2 3 MSS Olli etu eh desinet tete edet ebat ac fe pea te 10 2 4 Sensor Get NEE 11 2 44 DS5 Sensotr Opto NS corteo he Eat geet Biet gde E eu eene vales b va cec ela ed re testable 12 Sections Installation e ees eO tad d oe adem tea RE cte ftatu 15 CSR e auer VER Eau EE 15 3 Instrument Assembly s inpet e rap esencial nx a eto E E puces kara tav e cust a co T rcu ER EE REDE EE Re 15 E H ee 16 Section Henr M 19 4 1 Parameter e EE 19 4 1 1 Using the Surveyor for Parameter Getup eene 19 4 1 2 Using Hydras 3 LT for Parameter Getup eene
34. corder Sensor The generic name for a device that senses either the absolute value or a change in a physical quantity such as temperature pressure flow rate or pH and converts that change into a useful input signal for an information gathering system Service loop A loop in a wire or cable to reduce the load on the wire or cable Slope Slope is the operation applied to the system s response once the zero has been set Slope is a measure of the sensitivity of a sensor Slope scales the sensor s output to the correct units Also see Zero 71 Glossary amp Abbreviations 72 Specific conductance conductivity at 25 C The ratio of the electric current density to the electric field in a material The ability of a fluid to conduct electricity Specific conductance is the inverse of electrical resistivity corrected at 25 C since fluids conduct more at higher temperatures Spot checking The collection of data using readings at irregular intervals Temperature A measure of heat present in water Aside from dissolved oxygen temperature is considered the single most important parameter Knowledge of water temperature is essential to the measurement of dissolved oxygen conductivity salinity pH alkalinity biological biochemical oxygen needed to meet the metabolic needs of aerobic requiring D O organisms and virtually every other water quality parameter Temperature controls metabolism utilization of inorganic and
35. d The Modem Adapter has a connector labeled modem that connects to the RS232 connection of the modem The other connector labeled multiprobe on the Modem Adapter connects to the multiprobe using a Interface cable and Underwater cable or a Calibration cable A 25 to 9 pin adapter is also required for the cables The Modem Adapter does not require a power supply however the multiprobe and the modem will require power Usually commercial modems are supplied with a wall cube power supply that converts ac mains voltage to 9 12 volts DC Most modem can use the multiprobe power supply by making a cable with the corrector connector for the modem power input The modem Modem Adapter power supply and associate cabling are not water proof and should be installed in a water tight enclosure If AC power is used then a GFI ground fault interrupt device should be installed in the ac wiring to prevent electrocution Program the modem as follows Table 7 Field Modem Commands Command Function AT amp C1 Enable carrier detection AT amp D3 Enable DTR detection AT amp K4 Enable XON XOFF handshaking AT amp QO No error correction or buffering AT amp SO Force continuous DSR AT CO Disable data compression ATSO 1 Answer on first ring AT amp WO Save current settings 1 The modem will automatically use this setup every time it is powered on Office Modem Installation The office modem is connected to the computer
36. dark blue the bag does not need replacement If the stripe is light pink or purple remove discard and replace the old bag 3 Reassemble the dryer 37 Maintenance Figure 14 Dryer Maintenance 1 Dryer Nuts 2 3 Desiccate Packet 2 Dryer Cap 4 Gore tex Patch 6 1 3 FreshFlow Miniature Sample Circulator Maintenance e 1 If the circulator is clogged with twigs or other small debris clean the impeller with some tap water using a soft bristle brush Use a pair of plastic tweezers to help remove debris Rinse with tap water 2 If there is excessive build up on the impeller remove the retaining screw to clean the build up After cleaning the impeller and before inserting the retaining screw apply a very small amount of Loctite 242 threadlock or equivalent on the tip of the screw Do not overtighten 6 2 AN Battery Replacement If the multiprobe is equipped with an internal battery pack the following batteries are customer replaceable The Sondes are also equipped with a customer replaceable Lithium clock battery e 8 size C alkaline batteries for the DS5 and DS5X e 8 size AA alkaline batteries for the MS5 Important Note To keep internal components dry avoid replacing batteries near a water source Important Note If water leaks into the multiprobe battery compartment remove the batteries pour the water out and thoroughly dry the compartment with a towel 6 2 1 A DS5 a
37. des of a sensor membrane At the isopotential points there is a zero potential across the membrane The observed potential of the sensor may not be zero due to the differences in reference electrodes Milliohm mQ Unit of resistance not conductivity or conductance MilliSiemens mS millimho m Units of electrical conductance Millimho m See MilliSiemens Molar concentration Molar solution Aqueous solution that contains one mole unit gram molecular weight of solute in one liter of water For example KCI potassium chloride molar concentration Multiprobe The combination of several sensors electrodes or probe assemblies into a complete stand alone piece of equipment which simultaneously measures several parameters for profiling spot checking or logging readings and data A multiprobe is a multi parameter instrument Nitrate NO3 Nitrate is the most oxidized form of nitrogen and is the primary form of biologically available nitrogen present in aerobic environments Nitrate is a less toxic form of nitrogen than ammonia and is readily assimilated by plants and bacteria Oxidation reduction potential or ORP See Redox potential Parameter A quantity which is constant under a given set of conditions but may be different under other conditions pH Describes the hydrogen ion activity of a system pH 0 7 acid solution pH 7 neutral pH 7 14 alkaline or basic solution The p in pH stands for
38. e temperature before parameter calibration Always use fresh standard and do not tamper with standards 4 2 9 Other Sensor Calibrations Refer to the sensor specific instruction sheet for more information 4 3 Using the DS5 MS5 for Short Term Deployments 4 3 1 Gathering Data Using the Surveyor Refer to the Surveyor Manual Cat No 003070 4 3 2 Gathering Data Using a PC and Hydras 3 LT For online monitoring and real time monitoring information refer to the Hydras 3 LT Quick Start Guide Cat No 6234289 4 3 3 Using the DS5 DS5X MS5 for Unattended Monitoring 4 3 3 1 Creating Log Files Note A log file must be created and then enabled before data can be collected 1 Connect the Data Cable to a computer and to the Sonde 2 Start Hydras 3 LT The software will automatically scan for Sondes All detected Sondes are displayed in the Connected Sondes list in the Main window displayed below If a Sonde is not found reattach the data cable and press RE SCAN FOR SONDES Retry until the Sonde s are found 3 Click on the Log Files tab 4 Click the CREATE button 27 Operation 10 Enter the name for the new log file The empty log file is now created Enter the start and end time of the logging the logging interval the sensor warm up time before logging and how long before logging the circulator will be turned on and if audio signals will be used while logging Select the parameters in the Parameter in S
39. eries must be installed in the correct orientation or serious injury and instrument damage may occur DANGER Do not mix depleted and fresh batteries together or serious injury and instrument damage may occur 1 Set the multiprobe horizontally on the work surface to prevent water leaking into the mulitprobe battery compartment 39 Maintenance 2 Unscrew the battery sleeve Slide the battery sleeve off of the Sonde 3 Discard the old batteries Insert the new batteries observing polarity markings located on the inside label Failure to install the batteries in the correct orientation may cause serious injury and instrument damage 4 Secure the new batteries with the top and bottom rubber bands Figure 16 b Coat the battery sleeve O rings sparingly with silicone grease 6 Screw the battery sleeve back on the Sonde Do not overtighten or instrument damage will occur 7 Discard batteries according to local regulations Figure 16 MS5 Battery Replacement __ _ a S o 1 Remove the Battery Sleeve 4 Bottom Retaining Rubberband 2 Remove depleted AA Batteries 5 Proper Battery Placement 3 Top Retaining Rubberband 6 Replace the Battery Sleeve 6 2 3 Lithium Battery Replacement The typical replacement period for the lithium battery is once every two years The lithium battery powers the real time clock that provides accurate time readings du
40. erly connected to the wall power outlet or external battery is used e Verify that the input voltage to the multiprobe is between 10 and 15 volts e Verify that the battery pack is installed correctly if applicable Check the battery polarity and voltages Check the internal components e Make sure all internal connections are securely seated e Check for the presence of water in the unit If damp or wet dry out thoroughly with a lint free cloth or towel or let it sit out opened in a dry room overnight Determine where the leak occurred and repair appropriately Notify Technical Support for help on preventing further leaks If these checks do not reveal the problem try to substitute other instruments cables and terminals to determine the failing component Troubleshooting Sensor Issues The following list is not an extensive account of the problems encountered If the following solutions do not reveal the problem try to substitute other sensors to determine the failing component Table 1 Sensor Troubleshooting Problem Solution D O readings are too low to calibrate and or pH and or Redox are very high or very low Check the value of the sample solution Ensure the sensors are properly maintained D O readings seem wrong Ensure the D O sensor has been properly maintained and calibrated Conductivity Temperature and or Depth readings seem wrong Ensure the sensors are properly maintained
41. ernal power adapter to the computer serial port 5 Start the communications program Hydras 3 LT 6 The software will automatically scan for Sondes All detected Sondes are displayed in the Connected Sondes list in the Main window displayed below If a Sonde is not found reattach the data cable and press RE SCAN FOR SONDES Retry until the Sonde s are found 15 Installation 3 3 Power Options A logging multiprobe can be powered by several sources e The DS5 and DS5X have an optional internal battery pack IBP holding 8 size C alkaline batteries e The MS5 has an optional internal battery pack holding 8 size AA alkaline batteries e Both multiprobes can use the external battery pack EBP e Both multiprobes can use either of the following power supplies the 110 VAC 12 VDC power adapter or the 220 VAC 12 VDC power adapter e Both multiprobes can use a customer supplied 12 volt deep cycle battery with appropriate amp hour capacity connected via the battery adapter or a cable with a 4 pin female metal shell connector e Both multiprobes can be powered using a Surveyor Datalogging Display which is equipped as a standard with a 7 2V 3 5 Ah NIMH rechargeable battery Note Multiprobes configured with the Self cleaning Turbidity and one or more fluorescence sensors Chlorophyll a Rhodamine WT Blue green Algae require either an internal battery pack or an external power source other than the Surveyor Figure 4 Power Op
42. f calibration discard used calibration standards appropriately Do not reuse calibration standards i l L ed S 1 Remove Sensor Guard 2 Attach the 3 Unscrew and remove 4 Fill the Calibration Cup Calibration Cup the cap from the half full with deionized Calibration Cup water 5 Place the Cap on the 6 Shake the Sonde to 7 In asimilar manner 8 Complete the Calibration Cup make sure each sensor rinse the sensors twice calibration is free from with a small portion of contaminants that might the calibration standard alter the calibration each time discarding the standard Repeat rinse several times 24 Operation 4 2 4 Temperature Sensor Calibration The temperature sensor is factory set and does not require recalibration 4 2 5 Specific Conductance Calibration Note TDS measurements are based on specific conductance and a user defined scale factor The factory default scale is 0 64 g L mS cm This procedure calibrates TDS raw Conductivity and Salinity Specific conductance requires a two point calibration Calibrate the sensor to zero and then to the slope buffer 1 Pour the specific conductance standard to within a centimeter of the top of the Calibration Cup 2 Make sure there are no bubbles in the measurement cell of the specific conductance sensor 3 Enter the SpCond standard
43. fixture which screws onto the mulitprobe bulkhead connector and provides an eyelet for rope or wire when no cable is used during deployment Figure 10 MS5 Mooring Fixture mm mm MI e 1 Mooring fixture used with rope or chain 2 Mooring fixture used with eye bolt 32 Deployment 5 2 3 Short term Deployment in Open Waters Figure 11 Generally short term deployment implies hand held operation Important Note Do not pull Sonde from a moving boat or instrument damage may occur and voids the instrument warranty Do not lower the mulitprobe into the water without screwing on the weighted sensor guard Secure the underwater cable prior to deployment Do not place the instrument where the cable might be severed or damage by boat propellers or any moving parts on a monitoring system Protect all cables from abrasion unnecessary tension repetitive flexure or bending over sharp radii boat gunwale or a bridge railing Do not bend or run the cable over the sheave or pulleys with less than 3 inch radius or 6 inches in diameter Use the V shaped support bail to lift and lower the multiprobe if so equipped This ensures that the weight of the mulitprobe is suspended from the bail If the multiprobe is equipped with a locking sleeve instead of a support bail make sure the locking sleeve or the MSS mooring fixture are properly screwed on the multiprobe 6 pin marine bulkhead connector before depl
44. for mS cm or uS cm using Hydras 3 LT software or a Surveyor 4 2 6 Clark Cell Dissolved Oxygen Sensor Calibration Dissolved oxygen calibrations can be performed using water saturated air or using a water sample with a known dissolved oxygen concentration Note Dissolved oxygen can also be calibrated in a well stirred bucket of temperature stable air saturated water This situation resembles the actual field measurement conditions but is more difficult to accomplish reliably 4 2 6 1 Water Saturated Air Dissolved Oxygen Calibration CAUTION The saturated air method is valid only for the Clark Cell dissolved oxygen sensor If calibrating the Hach LDO sensor refer to the Hach LDO Instruction Sheet Cat No 00745589 Note Calibration of D O Saturation also calibrates D O mg L 1 Fill the Calibration Cup with deionized or tap water specific conductance less than 0 5 mS cm until the water is just below the membrane O ring Do not allow water to contact the membrane or the O ring 2 Carefully remove any water droplets from the membrane with the corner of a tissue 3 Turn the black cap upside down concave upward and lay it over the top of the Calibration Cup This stops the exchange of air and allows the local environment to equilibrate Wait for the reading to stabilize 4 Determine the true barometric pressure for entry as the calibration standard Barometric pressure information can be obtained from a local weather stat
45. ide position and avoid areas with deposits of sand gravel or silt during heavy rainfall Avoid deploying in location where ice will form around the sensors or Sonde Figure 7 Securing the Multiprope to a Structure SS SSG DOOC04 oogooooO0 Ooopoooo 30 Deployment When securing the multiprobe to a structure carefully place straps such as web belts and large plastic Ty wraps on both ends of the mulitiprobe housing Figure 7 Do not use clamps to secure the multiprobe to a structure Also secure the cable in the same manner to protect it from floating debris navigation and vandalism Always make sure the weighted sensor guard is installed to protect the sensors and provide additional sinking weight to the multiprobe Calibration stability is dependent on the environmental conditions in which the sonde is deployed For example a D O sensor on a DS5 or MS5 may become fouled if deployed in a warm shallow biologically active lake However deployment length can be increased by a factor of 5 by using a DS5X which periodically cleans the fouling from the sensors On the other hand the same sonde deployed in a clean water environment or a sonde configured with sensors impervious to fouling i e Temperature Conductivity can be left unattended for months without the need to recalibrate Optimal deployment time for a specific environmen
46. ines When adding a transmission cable to the multiprobe the cable must be large enough to carry the operating current and transfer data without distortion For up to a total of 305 m 1000 ft of cable three 26 AWG wires are suitable for data transmission but two 18 AWG must be used for the power wires Alternatively smaller power wires can be used if the power supply is placed closer to the multiprobe A cable extension kit is available for above ground applications Replacement Parts and Accessories on page 47 5 1 4 Minimum Depth Requirements Sensors must be immersed The Standard Turbidity Sensor minimum deployment depth is 1 meter 29 Deployment 5 2 Deployment in Open Waters 5 2 1 Minimum Clearance Requirements Two inches of clearance is required from the longest probe and two inches around if a Turbidity sensor is supplied 5 2 2 Long term Deployment in Open Waters Important Note The use of pipe clamps to secure the Sonde can cause serious instrument damage When using the multiprobe in open water place the multiprobe where it will not get damaged For example to protect the multiprobe from being hit by floating debris in moderate to high flow levels anchor the multiprobe to the downstream side of a bridge piling Figure 7 The protection kit can also be used to protect the multiprobe In a recreational lake deployment use a marking buoy that will not attract vandalism Place the multiprobe in an upright or on s
47. ing the presence of an ANSI terminal You will not be able to access a Series 5 Multiprobe if logging event is currently active This can be avoided by setting the interval to no less than 2 minutes to allow enough time to call the modem between logging events a logging event occurring during a call will not cause a problem 63 External Communications B 6 TTY Mode 64 The sonde is equipped with a TTY Communication Mode which enables the Sonde to send an ASCII string of characters representing selected parameter values once per second Parameters and Parameter Order may be selected using the Define SDI Parameter Order button in the SDI section of the Settings Tab To enter TTY Mode 1 Press ENTER in the TTY Mode section of the Settings Tab 2 Press YES to verify the entry in mode E HYDROLAB COM 1 lal x System Online Monitoring Log Files Parameter Setup Calibration Settings Software Communication Baudrate MODBUS H 19200 Address 1 SDI Enabled Address fo Delay 20 Seconds Enable Continuous Mode Define SD Parameter Order Save Settings x Log Files 9 Are you sure that you want to enter TTY mode Files K This will close the sonde window Lest Space then Q TTY Mode gt Terminal Mode 4 Files 30 sec TTY Mode Date format MMDDYY D w Use Date Time delimiter Options 1 16 03 PM Z
48. ion or airport or the Surveyor if equipped with BP Some facilities calibrate BP at sea level an elevation correction will need to be made 25 Operation Local Barometric Pressure BP in mmHG can be estimated using BP 760 2 5 Ag 100 or BP 760 2 5 A 30 5 where BP Barometric Pressure at altitude BP Barometric Pressure at sea level Ag Altitude in feet Am Altitude in meters If using the local weather bureau BP remember these numbers are corrected to sea level To calculate the uncorrected atmospheric pressure BP use on the following equations BP BP 2 5 Aq 100 or BP BP 2 5 A 30 5 where BP Barometric Pressure at altitude BP Barometric Pressure at sea level Aq Altitude in feet Am Altitude in meters Local barometric pressure in mbar BPmbar can be converted to local barometric pressure in mmHG BPmmHg using BPmmHG 0 75 x BPmbar 5 Enter the barometric pressure in millimeters of Mercury mmHg at the site using Hydras 3 LT software or a Surveyor 4 2 6 2 Known Concentration Dissolved Oxygen Calibration 26 Note Calibration of D O mg L also calibrates D O 6 Saturation 1 Immerse the sensor in a water bath for which the D O concentration in mg L is known for instance by Winkler titration This calibration method is more difficult to perform than the saturated air method but can yield a higher accuracy if the known D O concentration is highly accurate
49. l a rhodamine WT conductivity depth dissolved 10 General Information oxygen nitrate ORP pH temperature total dissolved gas turbidity and blue green algae Figure 3 MS5 Multiprobe 5 44 5 mm 1 75 inches H us a NS 7 La 724 mm 28 5 inches 1 Calibration Cap 4 Housing 2 Calibration Cup 5 Battery Compartment optional 3 Locking Screw 6 Connector 2 4 Sensor Options MS5 Sensor Options Sensor Description Cat No Hach LDO Sensor 007455 Clark Cell Dissolved Oxygen Conductivity 004467 Clark Cell Dissolved Oxygen 004470 Conductivity with pH Return 004468 Total Dissolved Gas 004469 pH and ORP with Integrated Reference 004454 pH with Integrated Reference 004446 Low lonic Strength Reference 004445 pH 004461 pH and ORP 004462 Chloride 004496 D Nitrate 004494 Ammonium Ammonia 004492 Standard Reference 004463 Circulator 007245 Self cleaning Turbidity 007280 Standard Turbidity 004466 11 General Information MS5 Sensor Options
50. n conjunction with the sensor For use without a circulator use a flow rate of more than 4 liters per minute A 12 inch hose is required for the MS flow cell anda 34 inch hose for the DS flow cell Filter debris from the feed line if necessary If possible invert the multiprobe so that bubbles will float away from the sensors and out the port on the bottom of the flow cell 35 Deployment Figure 13 Flow Cells HYDROLAB bd HYDROLAB HYDROLAB 1 ex 1 DS flow cell 4 Sample flow IN 2 MS flow cell with standard turbidity sensor 5 Sample flow OUT 3 MS flow cell Section 6 Maintenance DANGER Only qualified personnel should conduct the maintenance tasks described in this section of the manual To ensure continued and reliable operation of the water quality monitoring system we recommend scheduling a thorough and regular maintenance program To determine the appropriate maintenance intervals required for a deployment site periodically conduct a visual inspection of the equipment and sensors compare the pre and post calibration results and monitor the sensor response time A contaminated worn out or damaged sensor will not produce reliable readings It is recommended to service all sensors and allow them to equilibrate in tap water overnight before calibration Maintenance kits are
51. n nennen e enne enne enn 37 6 1 1 Cleaning the Multiprobe Housing ccceccceeceeeeeeeeeeeeeeeeeeeeecaaeeeseaeesaaeeeseaeeeseaeeesseeeesesaeeeseaeeeseaeeeteneeeees 37 6 1 2 Dryer Maintenance iii coe eee dele te dete ele ex e den ee dne o ee de e ene eee ae ee aua 37 6 1 3 FreshFlow Miniature Sample Circulator Maintenance 38 6 2 Battery Replacement ninoi o een e pene reed pee repe eno ee uta e dd 38 6 2 1 DS5 and DS5X Battery Replacement enne nnne etnies inneren 38 6 2 2 MS5 Battery Replacement senes nee aai iiaiai iiei 39 6 2 3 Lithium Battery Replacement erener ertainei kaaien aaup ie Teea nennen nennen innen nennen RAe FAKER Aera ieee 40 6 3 Storage and Care Hecommendatons eene nener nnns innen nennen nns 42 6 3 1 M litprobe and Serisor StOrage u ii iet neni ce Ee Eee tee PEE HUE REL De PER eve d 42 6 3 2 Electrical Cable Gare oit entrer a Ce RERO e R ERR EIL a ce REFER HE ED IRR See ches 42 6 4 Sensor Maitena NCE cede e tnnt ha i ica tcd i e e dcc EE dtt e ce o aede Ma dee 43 6 5 Clark Cell Dissolved Oxygen Maintenance eene nennen nent enne sentes nensis nrnn nennen 43 6 6 Specific Conductance Salinity and TDS Maintenance 44 6 7 ORP Sensor Maintenance 44 6 8 pH Electrode Maintenance si ir rt ettet en i p ob d lui ette Pese o E AT HS ET Ru A 44 6 8 1 Standard Reference Electrode esses esent nennen nnnnet nene nnns enne 45 6 8 2 pH Integrated SeriSOt ec c deed gare Fonero neg dg t E
52. nd DS5X Battery Replacement 38 DANGER If the thumbscrew is difficult to remove there may be pressure built up inside the housing To avoid serious injury use extreme caution when loosening the battery cap thumbscrew DANGER Batteries must be installed in the correct orientation or serious injury and instrument damage may occur Do not mix depleted and fresh batteries together or serious injury and instrument damage may occur Figure 15 Maintenance Use only high quality non rechargeable batteries in the DS5 or DS5X multiprobe Refer to Figure 15 and the following directions for DS5 and DS5X battery replacement 1 Set the multiprobe horizontally on the work surface to prevent water leaking into the mulitprobe battery compartment Unscrew the battery cap thumbscrew counterclockwise Pull the cap out of its housing and slide the old batteries out Discard the old batteries Insert the new batteries observing polarity markings located on the inside label Failure to install the batteries in the correct orientation may cause serious injury and instrument damage Coat the battery cap O rings sparingly with silicone grease Insert the cap back into the multiprobe housing Tighten the thumbscew clockwise Finger tighten only DS5 and DS5X Battery Replacement ip i j 1 Battery Cap 2 Battery Cap Screw 6 2 2 A MS5 Battery Replacement DANGER Batt
53. nderwater connectors using silicone grease Use protective plugs when the connectors for underwater and calibration cables are not connected to any instrument Keep all cables clean dry and stored neatly coiled in a large plastic container Do not coil cables any tighter than 6 inches in diameter or cable will be damaged Maintenance Do not knot the cables or use clips to mark a certain depth Do not place the instrument where the cable might be severed or damaged by boat propellers or other moving parts Protect all cables from abrasion unnecessary tension repetitive flexure or bending over sharp radii e g the side of a boat or of a bridge Do not bend or run the cable over the sheave or pulleys with less than a 6 inch diameter If cables are long use a battery powered or hand cranked reel with electrical slip rings to lower and raise the instrument Also a lighter reel without slip rings for shorter cables can be used A last option is to mount the reel horizontally with the instrument and battery installed in the hub Use the V shaped support bail to lift and lower the multiprobe Do not apply more than 5 kilograms 10 Ib of sinking weight to the multiprobe This can increase the possibility of cable breakage due to stress on the attachment points If more weight is needed use a wire line to support the instrument by its bail 6 4 Sensor Maintenance Important Note If a sensor is not in use insert an opti
54. nnne nennen nennen nnne en nens 20 4 1 3 Specific Conductance Parameter Setup ener nnne enne 20 4 1 4 Clark Cell Dissolved Oxygen Parameter Geiup nennen nnns nens 22 4 15 DHiRarameter Set p EE 22 4 4 6 Other Parameter Setup i c eoe c te a eode ee Tata a s opu ve Ed oes 22 Seele Le EE 22 4 2 1 Calibrating the Sensors Using the Surveyor seen nennen nennen nens 22 4 2 2 Calibrating the Sensors Using Hydras 21T nennen nnns nens 23 4 2 3 Calibration Preparation note red pater Gee DA ae deen 24 4 2 4 Temperature Sensor Calibration enne nennen nnn nenen nnne nnns 25 4 2 5 Specific Conductance Calibration essent nnn nnne 25 4 2 6 Clark Cell Dissolved Oxygen Sensor Calibration ssssssssseeeeenenenneen nnne 25 4 2 6 1 Water Saturated Air Dissolved Oxygen Calibration ss ssssseesseeeseneeeneesirnestnestrnsnnnntnnnnnnssrnesrnns 25 4 2 6 2 Known Concentration Dissolved Oxygen Calibration 26 4 2 7 Pressure Sensor Caltration esent nnnr senten sd nnns nennen rennes ensis nennen 27 4 2 9 pE ORP Galibration EE 27 4 2 9 Other Sensor Calibrations eerste eg ee decre s stu eee dau ve dre dd tu ae ee dne e 27 4 3 Using the DS5 MS5 for Short Term Deployments eee nennen nnne nennen snnt nens 27 4 3 1 Gathering Data Using the Gumvevor nennen enne nennen nes en terrens nnn enne 27 4 3 2 Gathering Data Using a PC and Hydras 3 UI 27 4 3 3 Using the DS5 DS5X MS5 for Unattended Monitoring
55. ns nrner et nes inni en nnns nennen rne 67 Gal HyperTerminal Setup 1 erede ee ane ENNEN ue ed ea 67 Appendix D Glossary amp Abbreviatons eene nennen en nensi nennen enn sn nnne 69 Section 1 Specifications Specifications are subject to change without notice DS5 and DS5X Transmitter Outer Diameter Length 8 9 cm 3 5 in 58 4 cm 23 in Weight typical configuration 3 35 kg 7 4 Ib Maximum Depth 225m Operating Temperature 5 to 50 C Battery Supply optional 8 C batteries Computer Interface RS232 SDI 12 RS485 Memory optional 120 000 measurements MS5 Transmitter Outer Diameter 4 4 cm 1 75 in 53 3 cm 21 in Length 74 9 cm 29 5 in with battery pack Weight typical Configuration x is S with battery pack Maximum Depth 225m Operating Temperature b5 to 50 C Battery Supply optional 8 AA batteries Computer Interface RS232 SDI 12 RS485 Memory optional 120 000 measurements Temperature Sensor Range 5 to 50 C Accuracy t 0 10 C Resolution 0 01 C Specific Conductance Sensor Range 0 to 100 mS cm Accuracy 196 of reading 0 001 mS cm Resolution 0 0001 units pH Sensor Range 0 to 14 units Accuracy t 0 2 units Resolution 0 01 units Specifications Clark Cell Dissolved Oxygen Sensor
56. on needs to be specific for a site and application Check the calibration prior to the first use Calibrate the sensors when Fouling has occurred or is noticeable site specific Parameter measurements do not match those of a known calibrated standard Adding or removing certain components for different applications e g the circulator or when replacing components e g the Teflon junction of the pH reference electrode Some system components are affected by time usage and the environment To ensure instrument accuracy it is recommended to perform routine tests of the system under standard conditions The multiprobe can be calibrated in the field or at a facility Equipment checks and adjustment made before going to the field tend to be more precise than those made under field conditions 4 2 1 Calibrating the Sensors Using the Surveyor For more information on the Surveyor refer to the User Manual Cat No 00719618 1 22 Attach the power and data cable to the Sonde Attach the 9 pin connector to the Surveyor Turn on the Surveyor Wait approximately 10 seconds for initialization Press SETUP CAL Press CALIBRATION Press SONDE Use the ARROW keys to highlight the appropriate parameter and press SELECT Highlight the function to program and press SELECT A calibration screen will be displayed Depending on the application use the ARROW keys to change the function press SELECT and DONE to finish the calibration
57. onal sensor expansion port plug in the vacant expansion port to prevent any contamination or damage during maintenance operation or storage 6 5 Clark Cell Dissolved Oxygen Maintenance Dissolved oxygen sensor maintenance is required when the membrane covering the cell becomes wrinkled bubbled torn dirty fouled or otherwise damaged 1 Remove the O ring securing 2 Refill with fresh D O 3 Make sure there areno 4 Hold one end of a new the D O membrane electrolyte until there is bubbles in the membrane against the Remove the old membrane a perceptible meniscus electrolyte body of the D O sensor Shake out the old electrolyte of electrolyte rising with your thumb and with and rinse with fresh D O above the entire a smooth firm motion electrolyte electrode surface of stretch the other end of the sensor the membrane over the sensor surface and hold it in place with your index finger 43 Maintenance F P 5 Secure the membrane with 6 Trim away the excess 7 Proper membrane 8 Let the sensor soak a the O ring Make sure there membrane extending assembly minimum of 4 hours are no wrinkles in the below the O ring 90 relaxed Ideally membrane or bubbles in the the sensor should soak electrolyte for 24 hours Note Readings may initially drift if calibrated before the membrane is fully relaxed 6 6 Specific Conductance Salinity and TDS Maintenance Clean the oval measurement cell on
58. onde list and click the ADD button to place them into the Parameters in log file list Change the order of the parameters using the ARROW buttons Click UPDATE SETTING to send the configuration to the Sonde Click ENABLE to start collecting data Click DISABLE to stop collecting data during logging A fully completed logging run will automatically disable at the end of the run Click DOWNLOAD to download and display the log file Select Printable or Spreadsheet format Note To delete a log file select the log file in the Log File drop down menu and click the DELETE button 4 3 3 2 Downloading Log Files 28 After a log file is created in the Log Files tab the files can be downloaded by checking the appropriate Log File box and clicking DOWNLOAD SELECTED FILES Multiple files can be downloaded at once The downloaded log files are stored in the LogFiles subdirectory of the HYDRAS 3 LT directory on the hard drive Section 5 Deployment 5 1 Deployment Considerations 5 1 1 Pressure Extremes Note The multiprobe maximum immersion depth is 225 meters 738 feet Note The ion specific sensors Nitrate Ammonia and Chloride maximum deployment depth is 15 meters Important Note The 0 10 meter vented depth sensor should be protected from depths over 15 meters 49 feet by installing the seal screw provided in the basic maintenance kit in the face of the multiprobe sensor cap Likewise the 0 25 depth sensor sh
59. one number Configure Connection Access and select the modem transfer speed e g 19200 bps Access and select the connection settings e g N 8 1 Transfer Capture Text Enable a capture file to log the data currently received to a disk or to a hard drive You will be prompted for a file name and a path File Capture to printer Turn the printer on Transfer Send file Upload a file and choose the transfer protocol e g Xmodem You will be prompted for a file name and a path Transfer Receive File Download a file and choose the transfer protocol e g Xmodem You will be prompted for a file name and a path File Open To view a file or find a saved file in the HyperTerminal folder 67 Visit us at www hachenvironmental com Appendix D Glossary amp Abbreviations Ammonia NH3 A colorless gaseous alkaline compound which is soluble in water It has a characteristic pungent odor and is used as a fertilizer In water and soil ammonia is present primarily as NH4 ions and is readily assimilated by plants during nutrition Ammonium NH4 Ammonium is a form of ammonia by the addition of a hydrogen ion H to an ammonia molecule NH3 Ammonia is converted to ammonium as the pH of a solution drops Ammonium is less harmful to aquatic life than ammonia Below a pH of 7 3 more than 99 of the total ammonia is present as ammonium Assembly A unit containing the component parts of
60. organic matter for life processes of aquatic animals and plants Temperature is largely responsible for biochemical reactions and is one of the most important cues for beginning and ending of spawning migration and many other phenomena Titration A method of analyzing the composition of a solution by adding known amounts of standardized solution until a given reaction color change precipitation or conductivity change is produced Winkler titration in calibration A wet chemical method for estimating the D O in water Tolerance Refers to the maximum difference between the true value of a parameter and the actual operator acceptable reading Usually used as a synonym for accuracy Total dissolved gas TDG The amount of gaseous compounds dissolved in a liquid Total dissolved solids TDS The amount of materials in a body of water that are dissolved or too small to be filtered These solids include ions which are important to the internal water balance in aquatic organisms The amount of substances calculated in Kg l dissolved in one liter of water A measure primarily of alkaline earth metals and their salts dissolved or in very fine suspension It provides information regarding the potential buffering capacity of water water hardness and the potential lethality of toxins The concentration of dissolved solids affects osmoregulation salt balancing and is often a cue for migration and spawning TDS concentration affects the
61. ould be protected from depths over 35 meters 164 feet by installing the same seal screw However the 100 and 200 meter depth sensors do not require installation of the seal screw The mulitprobe may be equipped with one of the following depth options 0 10 meters 33 feet 0 to 25 0 to 100 and 0 to 200 meters 82 328 and 656 feet The first option is used to detect water level changes that are automatically compensated for barometric pressure changes Applications include tidal waters rivers stream lakes reservoirs and groundwater The vented level option must have a fixed cable with a vent tube The second third and fourth options are usually used to determine the depth in the water column at which the other parameter readings are made 5 1 2 Temperature Extremes The multiprobe storage temperature range is 1 to 50 C 34 to 122 F non freezing when going or coming back from a deployment site or when storing the multiprobe The mulitprobe operating temperature range is 5 to 50 C 23 to 122 F non freezing Exposing the multiprobe to temperatures outside this range may result in mechanical damage or faulty electronic performance To prevent sensors from freezing store the multiprobe where freezing will not occur To prevent the sensors from dehydrating fill the DS storage cup or MS cup with one inch of clean tap water Always rinse the multiprobe with clean tap water after deployment 5 1 3 Data Transmission L
62. ower and data cable to the Sonde Attach the 9 pin connector to a PC 2 Start Hydras 3 LT Wait for the software to scan for connected Sondes Highlight the multiprobe and press OPERATE SONDE Note If the Sonde appears to be connected and the software does not recognize the Sonde connection remove and replace the connector cable and press RE SCAN FOR SONDE Repeat until Hydras 3 LT recognizes the Sonde 3 Click on the Parameter Setup tab and select the parameter tab to be configured 4 Enter the appropriate values and press SAVE SETTINGS Ey Hydrolab COM 1 lel Ea System Online Monitoring Log Files Parameter Setup Calibration Settings Software SpCond mS cm Sal ppt DO mg pH Units Turbidity NTUs Cond Temp Comp Set Range 1 Auto 12 46 55 PM E 4 1 3 Specific Conductance Parameter Setup For specific conductance set the following functions using Hydras 3 LT or the Surveyor e Select the specific conductance function Fresh Salt StdMth None or Custom e Fresh default is based on the manufacturer s freshwater temperature compensation This function is derived from 20 Operation 0 01N KCI f T c4T5 CoT4 CgTS c4T CsT Ce where C47 1 4326 x 10 9 co 6 0716 x 10 8 c3 1 0665 x 10 5 Ges 5 3091 x 1072 cg 1 8199 e Salt is based on the manufacturer s saltwater compensation f T cT CoT6 Gel c4T4 Gel Gel c T t Cg where
63. oyment Extra weight up to 5 kg 10 Ib maximum can be attached to the Sonde Figure 11 If more weight is needed use a wire line to support the instrument by its bail if so equipped Use a battery powered or hand cranked reel with electrical slip rings to lower and raise the instrument if the cables are very long A lighter reel without slip rings for shorter cables can also be used Figure 12 If sufficient deck space permits mount the reel horizontally with the instrument and a battery installed in the hub Figure 12 The manufacturer s cable reel can also be used to store up to 150 m 490 ft of underwater cable the reel must be ordered with the initial underwater cable purchase In deep deployments currents in conjunction with the sensor guard can put extreme strains on the cabling Using the Weighted Sensor Guard C 2 aS DS S e EAE 8l MS 5 J 1 DS5 Sensor Guard 3 MS5 Sensor Guard 2 DS5 4 MS5 33 Deployment Open Water Deployment Figure 12 MM i D T mj Il mmm 34 Deployment 5 2 4 Minimum Flow Requirements When deploying the multiprobe in waters flowing at less than one foot per second 0 333 mps a circulato
64. pany Freight charges to return merchandise to Hach Company e Freight charges on expedited or express shipment of warranted parts or product Travel fees associated with on site warranty repair This warranty contains the sole express warranty made by Hach Company in connection with its products All implied warranties including without limitation the warranties of merchantability and fitness for a particular purpose are expressly disclaimed Some states within the United States do not allow the disclaimer of implied warranties and if this is true in your state the above limitation may not apply to you This warranty gives you specific rights and you may also have other rights that vary from state to state This warranty constitutes the final complete and exclusive statement of warranty terms and no person is authorized to make any other warranties or representations on behalf of Hach Company Limitation of Remedies The remedies of repair replacement or refund of purchase price as stated above are the exclusive remedies for the breach of this warranty On the basis of strict liability or under any other legal theory in no event shall Hach Company be liable for any incidental or consequential damages of any kind for breach of warranty or negligence 51 Visit us at www hachenvironmental com Appendix A Troubleshooting Troubleshooting Communications If the first screen does not appear after booting up the communications software
65. product indicates the need for protective eye wear De PP Ply E This symbol when noted on the product identifies the location of the connection for Protective Earth ground General Information 2 2 DS5 DS5X Multiprobe The DS5 and DS5X are designed for in situ and flow through applications and can measure up to 15 parameters simultaneously The DS5 and DS5X have seven configurable ports that can include up to ten of the following sensors ambient light ammonia chloride chlorophyll a rhodamine WT conductivity depth dissolved oxygen nitrate ORP pH temperature total dissolved gas turbidity and blue green algae Figure 1 DS5 Multiprobe a SZ CN mes La 571 mm 22 5 inches 2 88 mm 3 45 inches 1 Calibration Cup 5 Bulkhead Connector 2 Storage Cup 6 Battery Compartment optional 3 Locking Screw 7 Bail Attachment 4 Housing Figure 2 DS5X Multiprobe CEN aa Y 571 mm 22 5 inches 2 88 mm A 3 45 inches 1 Calibration Cup 5 Bulkhead Connector 2 Storage Cup 6 Battery Compartment optional 3 Locking Screw 7 Bail Attachment 4 Housing 2 3 MS5 Multiprobe The MS5 is a portable instrument used for long term monitoring or profiling applications The MS5 has four configurable ports that can include a combination of the following sensors ammonia chloride chlorophyl
66. quet eto d dv Eege wees 46 6 9 Temperature Sensor Maintenance esee nennen nennen nnr entretenir intret snnt ens 46 6 10 Pressure Sensor Maintenance nennen tenente sen trt tents ESSEE Ense EESE nnns entrent 46 6 11 Other Sensor Maintenance eene nnneeen nens neret retinens ss teni set nns sensit retinens internen 46 Section 7 Replacement Parts and Accessories eene nter ens 47 Section 8 How to Order 49 Section 9 Repair Service oe aeu ade ded dida e e edet rie TR ned Pone ee opa ge PR ed ege s 50 Section 10 Limited Warranty sssssssssssssssssssseseeeee nennen nnne en nen ener nnn en ren sd dre sinn ren sensi n nenr enn ns 51 Appendix A Troubleshooting iine nudes niii sees cesck pasar de naro i dk sns cr dk pa sace u de Rd ae i 4kR nnd EENEG 53 Appendix B External Communications cece eee eaeeeeeeee eene sn nnnen en res inni sen rens nennen 57 Bal SDI T2 Interface eH Eee Mee ee Lad e p lit dac PO RE id bep febr oa deer 57 B 2 Connection to an External Device eene nnne enne s nn nrns inneren inneren 58 IRCH 60 B 4 Modbus Inteiface idiot e onere EE ee eebe eet dae er E cv ete 60 B 5 Using a Modem with Multiprobes AAA 62 Be TIY MOS endete imma he P ote die eoe gr eec eb depu ete deu sepa o deo RE FERRE c de Done 64 B 6 1 TTY Menu and Comnmands 1 2 tete dte dee Bea ariel Gee de cae e or deu Eu ea 65 B 6 2 Data DIsplay regret rH m ees eit Pedigree e iim eter 66 Appendix C Using Hvperterminal eene nnne nn
67. r option may be used for additional flow in order to achieve reliable Clark Cell dissolved oxygen sensor readings The circulator is activated via Hydras 3 LT software or the Surveyor Turning the circulator on or off will help during profiling and logging D O with a Clark Cell Sensor depending on the flow rate of the water at the site If insufficient flow rate is noticeable turn the circulator on Turn the circulator off to extend battery life when data is not needed for an extended period of time Turn the circulator on when logging data in unattended mode and need to have sufficient flow for accurate measurements note that this will reduce multiprobe battery life When the multiprobe is powered it takes time to warm up The warm up time refers to the time a sensor will be ready to record accurate data Warm up time will vary according to the sensors being used and field conditions e g temperature 5 2 5 Non submersible Deployment DANGER Do not let the flow cell pressure exceed 15 psig Higher pressure can burst the flow cell possibly causing serious bodily injury to oneself and or others For process or pump through situations attach the low pressure flow cell to the mulitprobe This configuration allows studying the water without submerging the multiprobe The flow cell replaces the DS storage cup or MS cup Figure 13 When measuring D O with a Clark Cell Sensor inside a flow cell the manufacturer recommends using a circulator i
68. racy 0 1 of span Resolution 1 0 mmHg Ambient Light Range 0 to 10 000 umol st m 2 Accuracy 5 of reading or 1 umol s71 m 2 Resolution 1 umol el m 2 Chlorophyll a Range 0 to 500 ug L 0 to 50 ug L O to 5 ug L Accuracy 3 for signal level equivalents of 1 ppb Rhodamine WT dye Resolution 0 01 ug L Rhodamine WT Range 0 to 1000 ppb 0 to 100 ppb 0 to 10 ppb Accuracy 3 for signal level equivalents of 1 ppb Rhodamine WT dye Resolution 0 01 ppb Blue green Algae Range 100 to 2 000 000 cells mL 100 to 200 000 cells mL 100 to 20 000 cells mL Accuracy 3 for signal level equivalents of 1 ppb Rhodamine WT dye Resolution 0 01 cells mL Visit us at www hachenvironmental com Section 2 General Information 2 1 Safety Information Please read this entire manual before unpacking setting up or operating this instrument Pay particular attention to all danger and caution statements Failure to do so could result in serious injury to the operator or damage to the equipment Do not use or install this equipment in any manner other than that which is specified in this manual 2 1 1 Use of Hazard Information If multiple hazards exist this manual will use the signal word Danger Caution Note corresponding to the greatest hazard DANGER Indicates a potentially or imminently hazardous situation which if not avoided could result in death or serious injury
69. rane O ring External Power Adapter Cable Macintosh Adapter Cable MS5 Bail Kit 013450 013460HY 011050 012480 011530HY 004164HY 015005HY 015010 015015HY 015025 015030 015050HY 015075HY 015100 015150 015200 013730 011780 013470 013910 6234200 013210 013610HY 013620HY 013640HY 013650HY 013770HY 013850HY 014120 013540 014680HY 003608 003609HY 013430HY 013410HY 014110HY 000537HY 002589HY 000498HY 013170HY 013740 013950HY 47 Replacement Parts and Accessories Replacement Parts Description Catalog Number MS5 Flow Cell 013520HY MS5 Flow Cell for use with turbidity sensor 014610 MS5 Basic Maintenance Kit 013280 MS5 Weighted Sensor Guard black extended 013760 MS5 Weighted Sensor Guard black standard 013330 MS5 Weighted Sensor Guard white extended 014910 MS5 Weighted Sensor Guard white standard 014920 MS5 Mooring Fixture 013530 MS5 Pipe Kit 013550 MS5 Storage Cup Cap O ring 002811 MS5 Storage Cup 003306 MS5 Storage Cup extended 003395HY MS5 Weighted Sensor Guard 014130 Modem Adapter 012650 pH Reference Electrolyte 100 mL 005308HY Potassium Chloride Pellets 99 KCl 20 pellets 005376HY Profiler Data Analysis Software 013350 Retaining Band 005363 SDI 12 and RS485 Adapter Cable 013510 SDI 12 and RS232 Adapter Cable 013790 Small Teflon Junction 002770HY Thumbscrew for Battery Plug 003301 48 Section 8 How to Order U S A Customers By Telephone 6 30
70. ring datalogging Refer to Figure 17 and Figure 18 and the following instructions for proper lithium battery replacement 1 Remove the Allen screws with the Allen wrench to remove the multiprobe sensor cap To help remove the Sonde sensor cap insert the screwdriver head into the notches on the mulitprobe housing at the bottom of the sensor cap 40 Figure 17 10 11 12 13 Maintenance Remove the Sonde body then slide the sleeve off of the Sonde Avoid damage to the circuit board Carefully remove the foil shield Detach the 10 pin connector ribbon cable Remove the retaining screw next to the battery clip Figure 17 and Figure 18 Push the battery out of the battery clip using a small screwdriver Insert the new battery Panasonic reference CR 2032 or equivalent with the positive sign facing up Replace and tighten the retaining screw Reattach the 10 pin connector and replace the foil shield Apply silicone grease to the sensor cap O rings Carefully insert the circuit board and sensor cap assembly Tighten the Allen screws Do not overtighten Reset the time and date after replacing the lithium battery Then enter the time of the location and press ENTER Discard batteries according to local regulations Replacing the Lithium Battery on the DS5 or DS5X HYDROLAB fiV TOHCAH
71. s the number of registers returned The two byte CRC is appended at the end Example The multiprobe stores pH information at holding registers 40007 and 40008 These registers are addressed as 0x0006 and 0x0007 The following sequence of bytes request pH from a multiprobe with slave address 1 pH Query Example Byte 11 Byte 22 Byte 33 Byte 43 Byte 54 Byte 64 Byte 75 Byte 85 0x01 0x03 0x00 0x06 0x00 0x02 0x24 Ox0A 1 Slave Address 2 Command 3 Read Holding Register 3 Address of the first Holding Register to read 0x0006 4 Number of Holding Registers to Read 2 registers 4 bytes 5 CRC Response Byte 11 Byte 22 Byte 33 Byte 44 Byte 54 Byte 64 Byte 74 Byte 85 Byte 95 0x01 0x03 0x04 OxA8 0xC9 0x41 0x06 OxBA Ox3F 1 Slave Address 2 Command 3 Read Holding Register 3 Number of Data Bytes 4 bytes 2 registers 4 pH 5 CRC Result The data is sent Low Word First High Byte First therefore the IEEE Floating Point Formatted value representing the pH is 0x4106A8C9 8 416 Units 61 External Communications B 5 Using a Modem with Multiprobes 62 Field Modem All multiprobes require a modem adapter to enable communications with a commercial telephone modem The modem adapter provides the necessary handshaking and connections to allow a modem to properly answer the incoming call and power down the multiprobe when the call is terminate
72. se in Balanced Digital Multipoint Systems RS485 involves sending an inverted or out of phase copy of the signal simultaneously on a second wire This is called a balanced transmission Any outside electrical noise adds coherently to both signal copies The receiver electrically subtracts the two signals to reproduce the original signal The advantage in the subtraction is that only the intended signal gets reproduced since they are out of phase The in phase noise on the two wires are also subtracted from each other to produce a net zero noise component in the reproduced signal This noise immunity allows the RS485 interface to transmit digital signals at faster rates over longer distances than the RS232 SDI 12 interface The RS232 SDI 12 interface does not use balanced transmission and is therefore susceptible to noise interference which limits the transmission distance and speed Connections RS485 can use two wires to both transmit and receive data A common software protocol must be shared between devices to prevent data collisions on the wires RS485 also allows for multiple transmitters and receivers to be easily connected together Be sure to connect the signal grounds of all devices on the network together The connection can be made using a conductor in the transmission cable or each device can be connected to a good earth ground This connection keeps the common mode voltage the voltage which the signal must overcome to be reproduced low
73. serial port using a standard RS232 connection Program the modem as follows Table 8 Office Modem Commands Command Function ATW1 Report connection speed amp protocol AT amp C1 Enable carrier detection AT amp K4 Enable XON XOFF handshaking AT amp QO No error correction or buffering AT CO Disable data compression AT amp WO Save current settings 1 The modem will automatically use this setup every time it is powered on External Communications The computer will need a terminal emulation program to communicate with the remote multiprobe Setup the program to provide ANSI terminal emulation 19200 baud no parity 8 data bits and 1 stop bit for Series 5 Multiprobes Setup the software to provide a direct connection to the COM port connected to the modem Operating the Modem Check if the modem is communicating with PC by typing AT and pressing ENTER The modem should respond with OK To access a remote site from the office type ATD followed by the phone number for example ATD 15122558841 Add the proper prefixes to the phone number such as 9 for PBX office systems or 1 for long distance Press ENTER The modem should starting dialing the number and negotiating the connection Series 5 Mulitprobes may require as long as 15 seconds to show the startup screen If the startup screen is not displayed send a Break by typing ALT B Telephone noise and delay may prevent the Series 5 Multiprobe from properly determin
74. t can be determined by making periodic measurements of sensitive parameters with another instrument 5 2 2 1 Anchoring the DS5 or DS5X using the Support Bail Figure 8 1 Run a rope or chain through the bail if the Sonde is equipped with a support bail 2 Fixthe bail into the two eyebolts on the top of the Sonde by first loosening the lock nuts and turning the eyebolt 90 and then back so that the bail can be looped through 3 Securely tighten the lock nut on each eyebolt If the mulitprobe is not equipped with internal batteries it may not have a bail but can be secured using the locking sleeve DS5 Support Bail Installation 1 Turn the eye bolts to the positions shown 4 Rotate the eye bolt around the bail as shown 2 Hook the bail into the eye bolt as shown 5 Finish rotating the eye bolts until the bail cannot 3 Rotate the bail into the other eye bolt as shown be removed 31 Deployment 5 2 2 2 Anchoring the MS5 using the Bail Kit Figure 9 MS5 Support Bail Installation 1 Turn the eye bolts to the positions shown 4 Rotate the eye bolt around the bail as shown 2 Hook the bail into the eye bolt as shown 5 Finish rotating the eye bolts until the bail cannot 3 Rotate the bail into the other eye bolt as shown be removed 5 2 2 3 Anchoring the MS5 using the Mooring Fixture A MS5 equipped with an internal battery pack requires the MS5 mooring
75. tandards Also see Slope Glossary amp Abbreviations Abbreviations AgCl Silver Chloride MS MiniSonde Ah Ampere hour mS cm MilliSiemens per centimeter AWG American wire gauge mV Millivolt BDR Basic data recorder nm Nanometer BP Battery pack barometric pressure PA Probe Assembly cc Calibration cable PCB Printed circuit board C Degrees Celsius centigrade ppt Part per thousand CSV Comma separated value psu Practical salinity unit DS DataSonde psiag Pound per square inch absolute EPA External battery pack psig Pound per square inch gage F Degrees Fahrenheit RBP Rechargeable battery pack GFI Ground fault interrupt device RGA Returned good authorization IBP Internal battery pack SDI Serial digital interference IC Interface cable STDREF Standard reference electrode K ic ue dE Or KEMA Un OE ADONIS CIRCLTR FreshFlow miniature sample circulator KCI Potassium chloride SVR Surveyor lorL Liter WSG Weighted sensor guard mmHG Hd E Bacal eng 4PF 4 pin female connector mil A unit of length equal to 0 001 inch 4PM 4 pin male connector M KCI molar potassium chloride 6PF 6 pin female connector um Micrometer 6PM 6 pin male connector m Millimho milliSiemens mS 9PF 9 pin connector uS cm SURE per centimeter micromho 9PM 9 pin male connector m Meter 1 meter 3 281 ft 73 Visit us at www hachenvironmental com
76. tions 5 m ep 110 VAC 12 VDC Power Adapter Cat No 013450 9 Gig MM l 220 VAC 12 VDC Power Adapter Cat No 013460 BR D Cigarette Lighter Adapter Cat No 013210 aui OOOO DIE External Battery Pack 110 VAC 12 VDC Cat No 011050 220 VAC 12 VDC Cat No 012480 Feo Am ala Rd Battery Adapter Cat No 011530HY D Refer to Assembly Options Use the correct power cord with the IEC 320 connector To prevent damage use a regulated 12 VDC adapter An unregulated 12 VDC adapter may exceed the instrument voltage limit rating 16 Figure 5 Assembly Options Surveyor Installation Windows 98 NT 2000 XP E External Power Adapter Cable Cat No 013170HY Calibration Cable Cat No 013470 Detachable Cable Cat No 015XXX External Power Adapter Cable Fixed Cable Cat No 013170HY Detachable Cable Cat No 13470HY SDI 12 or RS485 Adapter Cat No 013510 Requires installation of IBP in multiprobe unless a Surveyor4 is used Detachable Cable Cat No 015XXX lt x EE DS SX Ce m HYDROLAB H BS D ms Refer to Power Options F 17 Visit us at www hachenvironmental com Section A Operation
77. trolyte are purged This purging flushes and cleans the porous Teflon Reference Junction 5 With the Transmitter 6 Turn the Transmitter so sensors pointed down that the sensors point up push the full reference and push the sleeve the sleeve back onto its rest of the way onto its mount until the sleeve mount Rinse with tap has just covered the water O ring located on the mount just behind the silver electrode 45 Maintenance 6 8 2 pH Integrated Sensor ED amp of 1 Remove the plastic 2 Use the supplied 3 Remove the Teflon 4 Replace the blue O ring soaking cap Save the screwdriver to loosen Reference Junction located below the Teflon cap for reuse the Teflon and discard if dirty or Reference Junction if it Reference Junction clogged is damaged or loose e i A amp alm T ee 5 Drop two KCI salt pellets 6 Inject the pH reference 7T Refill the reference 8 Use the supplied Cat No 00537HY into electrolyte into the opening with electrolyte screwdriver to install the reference opening supplied plastic syringe the new Teflon Reference Junction Cat No 002770HY 6 9 Temperature Sensor Maintenance Use soap or rubbing alcohol to remove grease oil or biological growth and rinse with water Do not use any objects to poke the sensor or the transducer membrane will rupture 6 10 Pressure Sensor Maintenance 1 If calcium deposits are forming in the port squirt
78. ygen or D O A measure of the amount of oxygen present in water and available for respiration The concentration of D O is controlled by many factors including consumption by aerobic requiring D O organisms bacteria fish amphibians and invertebrates consumption by plants algae vascular plants particularly during dark hours and water temperature water flow and depth Drift The long term lack of repeatability caused by fouling of the sensor shifts in the calibration of the system or slowly failing sensors Dump To copy the contents of all or part of a storage usually from an internal storage device to an external storage device Eh See Redox potential Electrode An electric conductor which either measures the potential of a solution pH reference redox and ammonium electrodes or forces electric current into or out of a solution D O and conductivity electrodes Emery cloth An abrasive cloth or paper with an adherent layer of emery powder used to polish and clean metal No 400 or finer is recommended 69 Glossary amp Abbreviations 70 Hysteresis error The maximum separation due to hysteresis between upscale and downscale going indications of a measured value A difference in parameter readings which occurs due to a variation in the conditions under which the sensor approached the readings See Response time Isopotential point The point at which the ion activity is the same on both si

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