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Electrical Transport Option (ETO) User`s Manual

1. I reported Rorive R T ingie R Drive Leads where Rjeaas is the resistance due to leads and sample contacts Table 3 1 lists the nominal drive impedance for each current range when the drive feedback is disabled 3 2 PPMS ETO User s Manual 1084 700 Rev A1 Quantum Design September 2011 Chapter 3 Section 3 2 Hardware ETO Module and Head RLeads V Drive I sample I sample Vsample Vsample b c Figure 3 3 The equivalent circuit for ETO when drive feedback is disabled The dashed line represents the current source equivalent circuit Table 3 1 ETO current drive output impedance with feedback disabled Current Range Drive Output Impedance 100 mA 100 Q 10 mA 1 kQ 1mA 10kQ 100 uA 100 kQ 10uA 1MQ 1uA 10 MQ 100 nA 100 MQ In most cases the electronics should be run with the drive feedback enabled This will typically yield the most accurate measurement However it may be useful to disabled the feedback if you are measuring an IV curve on a sample with a non linear current voltage characteristic such as a diode With feedback off the IV curve of a diode will contain more points at lower bias currents when the device impedance is large Quantum Design PPMS ETO User s Manual 1084 700 Rev A1 3 3 September 2011 Section 3 2 Chapter 3 ETO Module and Head Hardware 3 2 2 Preamplifiers The ETO head contains a programmable gain amplifier PGA a high gain amplifier HGA
2. cooocccncccooncnoncnonononononoconacanccanccanccnnos 5 5 The immediate mode differential resistance measurement window ceeeee 5 7 List of sequence commands available when ETO is active ooooonoccnnccnocinoncnoncnonaconanos 5 8 The sequence command window for resistance measurements oooccnocccoccnoncnancnnnannss 5 9 The sequence command window for differential resistance measurements 5 10 The sequence command window for IV measurementS ocoonccnnncnnoccnoncnoncnonacnacana ns 5 10 The sequence command window for creating a New Data File eee 5 11 PPMS ETO User s Manual 1084 700 Rev A1 V September 2011 Contents Table of Contents Tables Table 2 1 Table 3 1 Table 3 2 vi A list of hardware components comprising the Electrical Transport Option for a PPMS and b VersaLab Systems isie nepaiso snieni nie as 2 1 ETO current drive output impedance with feedback disabled o ooonconnncnnnnnncnoncn 3 3 Preamp ranges and their associated gains for both 4 wire and 2 wire measurement MOSS it A ada 3 4 PPMS ETO User s Manual 1084 700 Rev A1 Quantum Design September 2011 P R E F A C E Contents and Conventions P 1 Overview The preface contains the following info e Section P 2 discusses the overall scope of the manual e Section P 3 discusses the conventions of the manual e Section P 4 discusses the safety guidelines for this option P 2 Scope of the Manual This manual discusses
3. 0 4 V 1X 10X 10X 130 mV 3X 10X 30X 40 mV 1X 100X 100X 13 mV 1X 300X 300X 4 mV 3X 300X 900X 1 3 mV 1X 3 000X 3 000X 0 4 mV 3X 3 000X 9 000X 130 uV 1X 30 000X 30 000X 40 uV 3X 30 000X 90 000X 2 Wire Mode iene Module Gain Head Gain Total Gain 400 nA 1X 1X 1X 130 nA 3X 1X 3X 40 nA 1X 10X 10X 13 nA 3X 10X 30X 4nA 1X 100X 100X 1 3 nA 3X 100X 300X 3 4 PPMS ETO User s Manual 1084 700 Rev A1 Quantum Design September 2011 Chapter 3 Section 3 4 Hardware Sample Pucks If you are measuring a sample with impedance greater than 10 MQ you will use the HZA and a 2 wire sample mounting configuration In this configuration ETO applies a voltage and measures the current through the sample The preamp range is specified in Amps for these measurements The measurement windows will automatically switch the drop down list to a selection of current ranges when the 2 wire configuration is chosen 3 3 Cables and Jumpers The ETO option includes one 25 pin cable to connect the module to the remotely mounted head one 2 pin cable to power the cooling fans on the head and one 8 pin cable to connect the head to the sample chamber The cable use and routing are shown in Figure 3 4 ETO kits intended for use on PPMSs are shipped with long length module and fan cables ETO kits intended for use on VersaLab systems are shipped with short length cables Both kits use the same sample cable to connect the head to the sample chamber grey Lemo Additional sample cables
4. 4 2 2 Electrical Transport Option Event Log The ETO Event Log window is displayed when ETO is activated This window displays high level hardware and software activity during ETO measurements This log will also display warnings errors and informational messages generated since option activation If you have a problem while a measurement is running entries in the event log can help diagnose the problem 4 3 Electrical Transport Option Data Files All of the data taken by the Electrical Transport Option is stored in a single data file The file name and location can be set on the Data File tab of the ETO Console or within a sequence For more information on changing the data file refer to Section 4 2 1 2 This section contains a list and description of each of the data columns as well as the measurement types that use the different data types Data Type Units Description Resistance dV dI IV Time Stamp Time stamp associated with the x x x row of data Temperature K Sample Temperature X X X Field Oe Magnetic Field se Angle of the sample stage relative paar e Posies deg to the magnetic field Quantum Design PPMS ETO User s Manual 1084 700 Rev A1 4 5 September 2011 Section 4 3 Electrical Transport Option Data Files Chamber Pressure Torr Pressure inside the sample chamber ees Ohms Measure resistance Resistance Std Dev Ohms
5. List of sequence commands available when ETO is active 5 5 1 ETO Resistance Figure 5 6 shows the sequence command window for the resistance measurement This window contains the same controls as the immediate mode window Follow the same steps outlined in Section 5 4 1 to specify the measurement parameters When you are finished press the OK button and the measurement command will appear in the sequence window Since this command allows simultaneous measurements on both channel 1 and 2 it is possible for the two channels to have different measurement times This can be caused by either very different averaging times or by selecting different numbers of points to measure on each channel In this case the sequence will wait for both channels to finish measuring before moving on to the next sequence command 5 8 PPMS ETO User s Manual 1084 700 Rev A1 Quantum Design September 2011 Chapter 5 ETO Measurements AC Resistance Measurement Channel 1 Enable Measurement Excitation Amplitude 10 m Freq 15 vw He Preamp Range av Si C Autorange Sample Wiring LS eS Measurement Configuration Averaging la Number of W Time E Measurements Data Logging Section 5 5 Sequence Measurements Channel 2 Enable Measurement Excitation Amplitude 110 m Freq 1 Y Hz Preamp o C Autorange Range ay Sample Wiring 4 wire M Measurement Configuration Averagin Number of ol Time ms 1 see Meas
6. installation procedure Follow the instructions on the screen to install or remove a new sample The Sample Properties button will launch a separate window to allow you to enter properties of the sample that you would like to store in the data file This information is stored in the data file header For more information regarding the ETO data files refer to Section 4 3 Figure 4 3 shows the Sample Properties window containing the Wiring Sample 1 Info and Sample 2 Info tabs The Wiring tab is used to specify the wiring configuration used on each sample It also lists the types of measurements that can be run with each configuration The two Sample Info tabs allow you to enter sample specific information such as name material and dimensions For more information regarding the wiring configuration refer to Section 5 2 ETO Console Setup Data File Measurement nstallation lead Properties Figure 4 1 Setup tab in the ETO Console window EE Sample Installation Wizard System Status 296 77 K Standby Sealed Instructions Dpen Chamber Cancel Figure 4 2 The Sample Installation Wizard window 4 2 PPMS ETO User s Manual 1084 700 Rev A1 Quantum Design September 2011 Chapter 4 Software Section 4 2 Overview of Electrical Transport Option Software Sample Configuration Witing Sample 1 Info Sample 2 Info Channel 1 Channel 2 Wing Scheme 4 wire Wiring Scheme 2 wie wv Available Meas
7. 2 on the wiring tab Enter any other sample specific information you desire on the two sample tabs This information will be entered into the header section of the data file Switch to the Data File tab to select a new data file for your measurements Press Browse to enter a new file name and location Checking the Create New File Version checkbox will add a numeric suffix to the end of the file name if the file already exists Press the View button to open the data file in MultiVu Note The data file is not created until a measurement is initiated 5 4 Immediate Mode Measurements After the sample puck has been loaded you are ready to take measurements in immediate mode At this point it is a good idea to make a few test measurements in immediate mode to ensure your sample is loaded properly Open up a measurement window to perform the desired test measurements The immediate mode measurement windows are accessible through the Measurement tab in the ETO Console Select a measurement type and press the Launch Measurement button The following sections describe the process of setting up each type of measurement 5 4 1 Taking Resistance Measurements in Immediate Mode The AC Resistance Measurement window contains two identical sets of controls and indicators corresponding to channel and channel 2 Use these blocks to define the measurement parameters and read the measurement results specific to each channel A third section at the bottom of the win
8. and a high impedance amplifier HZA The amplifiers used in a particular measurement are determined both by the measurement type and the range specified in the measurement window Four wire measurements will use the PGA and the HGA when needed while two wire measurements will use the PGA and the HZA at all times The HGA has a typical noise specification of 1 nV Hz giving a noise floor of 10 nQ for a 100 mA excitation The HZA by contrast is a sensitive amp meter and is used to measure impedances above 10 MQ The gain of the preamplifiers is determined in each measurement by selecting the range in the preamp controls The range is typically specified as a voltage This can be interpreted as the maximum sample voltage the system can measure at the chosen range The lower the voltage range the higher the total gain In practice the system can measure up to 110 of the voltage specified by the range If you do not know the impedance of your sample ahead of time you can elect to autorange In this case the system will automatically adjust the range based on the measured signal Selecting autorange will delay the return of data while the system adjusts the gains to find the appropriate range Table 3 2 Preamp ranges and their associated gains for both 4 wire and 2 wire measurement modes 4 Wire Mode TTAR Module Gain Head Gain Total Gain 4V 1X 1X 1X 1 3 V 3X 1X 3X
9. resistivity pucks that mount into the sample chamber Each sample puck has a circuit board around the perimeter with 12 pads organized into three channels Each channel has 4 pads labeled I I V V in the standard 4 wire resistance geometry The circuit board has labels for each pad as well as the channel number corresponding to each group to avoid confusion during sample mounting ETO uses the channel 1 and channel 2 pads There is a space in the center of the puck for physically mounting your sample substrate onto the puck surface For most measurements below room temperature Apeazon N grease is adequate to secure your sample to the puck surface However more exotic mounting methods may be necessary for larger samples The wiring configuration used for each sample depends on the type of sample you are measuring The ETO electronics has a 4 wire standard mode for samples whose resistance is below 10 MQ and a 2 wire high impedance mode for samples whose resistance is 10 MQ up to 5 GQ Both wiring configurations are discussed below along with mounting and wiring examples Since the ETO has two independent sets of measurement electronics it is possible to wire up one sample in standard mode and the other in high impedance mode Note How you wire up your sample determines what electronics you must use You cannot switch back and forth between standard and high impedance modes without physically changing the sample wiring WARNING Do not
10. the operation of the Electrical Transport Option ETO option hardware option software and general use of the option This manual does not provide detailed information about the Versalab system or the MultiVu software application used to operate Versalab This information can be found in the VersaLab User s Manual P 3 Conventions in the Manual File menu Bold text is used to distinguish the names of menus options buttons and panels appearing on the computer screen File gt gt Open The gt gt symbol indicates that you select multiple nested software options lt Enter gt Angle brackets distinguish the names of keys located on the PC keyboard Note Text is set off in this manner to signal supplementary information about the current task the information may primarily apply in special circumstances Quantum Design PPMS ETO User s Manual 1084 700 Rev A1 vii September 2011 Section P 4 Preface Safety Guidelines and Regulatory Information Contents and Conventions This symbol signals specific caution or conditions that could result in system damage bodily harm or loss of life This symbol signals electrical hazards that could result in bodily harm or loss of life Used at all accessible 200 240 V power outlets This symbol signals information on fusing P 4 Safety Guidelines and Regulatory Information Before using this product please read the entire content of this manual and observe all instructions warnings a
11. to configure the leads correctly in order to take full advantage of the instrument s sensitivity The current leads are typically located at the edge of the sample while the voltage leads lie between Figure 1 1 a When current is passed through the sample an electric field is created The voltage leads should be arranged such that they measure a potential drop across a region where the electric field lines are relatively straight This is achieved by placing the voltage leads in line with the current leads or by separating the voltage leads by a distance that is small compared to their distance from the current leads It is also important for a true four terminal measurement that the voltage and current leads do not contact the sample at the same point Otherwise the reported resistance will include the sample contact resistance The lead geometry shown in Figure 1 1 a works well for thin film sample with well defined dimensions Other lead geometries may be used depending on the nature of the sample For instance when measuring a bar shaped sample you may attach the current leads to conductive pads that contact the entire end of the bar and then make voltage leads that 1 2 PPMS ETO User s Manual 1084 700 Rev A1 Quantum Design September 2011 Chapter 1 Section 1 3 Theory of Operation ETO Measure Types contact the sample in a line parallel to those ends You are responsible for determining the best lead arrangement for your needs and for i
12. wire 6 Use the Averaging Time text box to specify the measurement time in seconds 7 Use the Number of Measurements text box to specify the number of resistance points you would like the measurement to include 8 Press the Measure button to start the measurement AC Resistance Measurement Channel 1 Channel 2 Enable Measurement Enable Measurement Excitation Excitation Amplitude 10 m Freq 103 Hz Amplitude 10 m Freq 200 Hz Preamp Preamp Range 1 3 x C Autorange Range 40m v Autorange Sample Sample y Wiring 4 wire x Wiring Measurement Configuration Measurement Configuration Averaging Number of Averaging Number of Time 1 9 Measurements io Time 1 see Measurements 10 Resistance 2nd Harmonic dB Resistance 2nd Harmonic dB Phase Angle 31d Harmonic dB Phase ngle 31d Harmonic dB Temperature Magnetic Field Position deg Save Results to File Figure 5 2 The immediate mode AC Resistance Measurement Window During the measurement the Measure button will read Stop Press this button at any time to end the measurement The measurement results will be displayed at the bottom of the window The Resistance displays the resistance measured in Q The Phase Angle displays the phase angle in degrees between the excitation signal and the measured signal The 2 Harmonic and 3 Harmonic display the amplitude of each harmonic in dB At the very bot
13. 084 700 Rev A1 iii September 2011 Contents Table of Contents CHAPTER 4 SOMA AAA AAA 4 1 NA NO 4 1 4 2 Overview of Electrical Transport Option Software oooncccnncnnonnnoccnonononcnnn nono nono nono ncnn corn nconnccnnacns 4 1 ADA IN A O NO 4 1 421 1 Setup Tab nico lit iii died tido dales load 4 1 421 2 Data File Tab A A A ee ees 4 3 4 2 1 3 Measurement Tab nosene Sa tities lirio llas inca 4 4 4 2 2 Electrical Transport Option Event Log ee cesceseceseceseceseceseeeseeeeeeeaeecaaecnaecaeenaeenaeens 4 5 4 3 Electrical Transport Option Data Files cee ecesccseesesseceseeseeecaeeaeeeeseeesecseeeeeesecaeeaeeeeeeaeeas 4 5 CHAPTER 5 IRA O tobeaceudseesssyes 5 1 A AS E EAT E EE AEA 5 1 5 2 Sample Montin S secreet isesi ti g eea i aa a a 5 1 5 2 1 4 Wire Mounting Configuration esseeesesssesessesresresreerestesstsrrssetstssrentestessestesseeresseeeeestt 5 2 5 2 1 1 Hall Coefficient Mounting Configuration eeeseeeseeeeseseesrssresrrsresresrresrsrrsreesesres 5 2 5 2 2 2 Wire Mounting ConfiguratlON ooooccnoccnonononononoconaconaconncnnncnnn S rui aunean a risanni ia Ee 5 2 3 3 Sample Installation aa 5 2 5 4 Immediate Mode MeasuremMentS cooooccnncccnoncnononannnonononenonnnacnnnnonnnconnnnn nan nc nnnn nc nnnn rra nn annn nc cnn ccnnnss 5 3 5 4 1 Taking Resistance Measurements in Immediate Mode oooocnnccnncccnoccnonnnoncnoncnnonononnnacnonns 5 3 3 42 Current Voltage Curves iii A tia 5 5 5 4 3 Diff
14. PMS DynaCool CAN rack located on the right side of the cryostat The power switch for the CAN rack is located in back Open the CAN rack door and verify that none of the modules installed have power All of the module LEDs should be dark Install the two pieces of Velcro provided with the system on the back panel of the CAN rack between the CAN rack and the cryostat shield These should be in the center of the back panel high enough to ensure the ETO sample cable can reach the grey lemo connector Remove the cover for the second or third module bay from the back and carefully insert the ETO module Finger tighten the two mounting screws to secure the module in place The module should now be flush with the other modules or cover plates Mount the ETO head on the Velcro between the CAN rack and the cryostat with the D shell connector facing the back of the PPMS DynaCool Connect the ETO Module Cable 3101 455 01 and Fan Cable 3101 457 01 between the ETO module and the ETO head Attach the ETO Sample Cable 3101 456 01 between the ETO head and the grey lemo connector Turn on the power to the CAN rack Verify that both the PWR and COP indicator LEDs on the module are green It may take up to 30 seconds for the module to boot and the LEDs to turn green The COP LED will blink green until the option is activated PPMS ETO User s Manual 1084 700 Rev A1 2 3 September 2011 Section 2 2 Chapter 2 Initial Installation of Hardware and Software Instal
15. QuantumDesign el a dl Electrical Transport Option ETO User s Manual Part Number 1084 700 A1 Quantum Design 6325 Lusk Boulevard San Diego CA 92121 USA Technical support 858 481 4400 800 289 6996 Fax 858 481 7410 Second edition of manual completed September 2011 Trademarks All product and company names appearing in this manual are trademarks or registered trademarks of their respective holders U S Patents Foreign Patents c ONTENTS Table of Contents PREFACE Contents and Conventions sesssesoosseesoesooesossoesoossosssessossocssessossocesessoesoossosssesoossossoessoseossse vii PE A O IN vil B 2 Scope ofthe Mantal mesita dla tie o sii vii P 3 Conventionsan the Manta A eee EOE vil P 4 Safety Guidelines and Regulatory Informati0N cooconcnnnnnnncnnncnnnncnnnconnconnconncnnncnnnnnnacrnn cra conan viii CHAPTER 1 Theory OF OperatioN vise asscisessscesessenssssenvavenavevssesseuncoosesusosecnesyeceyusvecesouteycesbexovesesstenscosevecsenshens 1 1 EN o AAA A A E NOA 1 1 1 2 Overview of the Electrical Transport OptiON ooocnoccnoconococoncconnconnconn nono nona nono nonn conocio nnncnnncnnccnnnos 1 1 1 3 Electrical Transport Option Measurement Types oooconoconoccnonncocnconnconncnnncnnncnnncnnn crac cnn conan rancia 1 2 La O CS A OD ne 1 2 13 11 Harmonics Detection n oerien aee aa eee a a aasa a ckecosanstdanea tees TEENE 1 3 EALS MAUL oerien it A ta ae ei Ags 1 3 1 3 2 Curre
16. Select Sample1 Sample 2 AC Excitation N O S Frequency Y Hz ON ov AC Amplitude 10 m C Disable Drive Feedback IV Sweeps a Preamp Gain 4yV v ae Figure 5 3 The immediate mode IV measurement window While the measurement is being performed the Measure button will display Stop Press this at any time to abort the current measurement The status bar at the bottom of the window will display the measurement progress When the status bar is full the IV curve will be available in the data file Quantum Design PPMS ETO User s Manual 1084 700 Rev A1 5 5 September 2011 Section 5 4 Chapter 5 Immediate Mode Measurements ETO Measurements 5 4 3 5 6 Differential Resistance Curves Differential resistance curves like IV curves can only be performed on one channel at a time This measurement applies a small AC excitation and measures the differential resistance at various DC bias points Take the following steps to measure a differential resistance curve in immediate mode 1 2 10 11 12 13 Select the radio button for Sample 1 or Sample 2 to select a channel Select either 4 wire or 2 wire configuration from the Sample Wiring drop down list Select the AC frequency from the Frequency drop down list Use the DC Amplitude text box to specify the maximum value of the DC sweep Use the Steps Quadrant text box to specify the number of DC steps per quadrant of the DC sweep The Step
17. Size will be filled in automatically using the previously entered information If you prefer you can enter the step size and the steps per quadrant will be recalculated Select the DC sweep quadrants by dragging the start and stop cursors around on the sweep graph If the sweep does not start at zero bias select the Ramp to Starting Point check box to ramp the DC bias to the starting value prior to starting the measurement Use the AC Amplitude text box to specify the amplitude of the AC excitation used to measure the differential resistance This value should be less than the DC sweep amplitude Select the Range from the drop down menu Use the Averaging Time text box to specify how long to average each data point Use the Settling Time text box to specify how long in milliseconds to wait after each DC step before beginning each new resistance measurement 100 ms is usually adequate Press the Measure button to begin measuring the curve PPMS ETO User s Manual 1084 700 Rev A1 Quantum Design September 2011 Chapter 5 Section 5 5 ETO Measurements Sequence Measurements dV dl Dialog Selec DC Sweep Sample 1 Sample 2 l 0 q AC Excitation Freq 976 A Hz a Time AC Amplitude 2 m Preamp Range Step Size 5 Sample ac g Steps Quadrant ho Wiring C Ramp to Starting Point Settings Averaging Time pl Settling Time 100 ms an Figure 5 4 The immediate mode differential resistance measuremen
18. The Electrical Transport Option supports three types of measurements e Resistance e IV Curves e Differential Resistance 1 3 1 Resistance The ETO is capable of both four terminal and two terminal resistance measurements In the classic four terminal geometry 4 wire mode two leads pass a current through the sample and two separate leads measure the potential drop across a section of the sample Ideally the voltage leads draw very little or no current The current through the sample and the potential drop across the sample can therefore be known to a high degree of accuracy Ohm s law can then be used to calculate the resistance of the sample for the region between the two voltage leads This geometry eliminates the effects of lead contact resistance from the measurement results The resistance is calculated using Ohm s law V R 1 7 1 where V is the measured potential drop across the sample and is the current through the sample Unlike the AC Transport measurement option available from Quantum Design ETO does not calculate the resistivity Since resistivity relies on sample specific parameters that may not be know or not known accurately at measurement time the option reports the resistance in units of Ohms Resistivity can be calculated as follows oes 2 oar 2 where R is the reported resistance is the voltage lead separation and A is the cross sectional area through which the current is passed It is important
19. The standard deviation of the Ch1 Ch2 resistance Phase Angel Ch1 Ch2 deg ee mA Wave form of the current eres V Wave form of the voltage ae Hz Excitation Frequency uo g s Actual averaging time AC Current wA The peak amplitude of the AC Ch1 Ch2 drive excitation eres mA The DC drive excitation nd di V Magnitude of the voltage aaa V The in phase voltage amplitude Quadrature Voltage V Douro E ase voljage amplitude aaa V The peak voltage of the AC drive DC Voltage y The maximum DC voltage in the Ch1 Ch2 channel e Wench mA Magnitude of the current rena me V The in phase current amplitude Quadrature Current A The out of phase current Ch1 Ch2 AE amplitude 1 Total gain Module gain X head can 90000 gain 29 Harmonic yv The in phase voltage amplitude of the 2 harmonic 23 Harmonic yv The in phase voltage amplitude of the 3 harmonic An encoded integer containing ETO Status Code N information on the current status of the ETO hardware ETO Measurement yv Integer indicating the measurement Mode type for the row of data PPMS ETO User s Manual 1084 700 Rev A1 September 2011 Quantum Design CHAPTER 5 ETO Measurements 5 1 5 2 Introduction This chapter contains the following information e Section 5 2 discusses how to mount samples on the sample pucks e Section 5 3 discusses how to make measurements in immediate mode and in sequence mode Sample Mounting The Electrical Transport Option includes two
20. are necessary when connecting ETO to one of the temperature options available on the PPMS b OA Figure 3 4 Pictures of the ETO option installed onto a a PPMS system b a VersaLab system and c Dynacool system On the PPMS the head is mounted on the dewar using grip tape VersaLab requires the use of the accessory mounting kit 4372 079 3 4 Sample Pucks ETO includes two sample pucks for mounting samples that interface with the VersaLab sample chamber wiring The pucks have a mounted circuit board with labeled contact pads for convenient sample wiring on 3 channels When using ETO only channels 1 and 2 are used Channel 3 may be used with other measurement options or other third party electronics that you hook up to the base system The gold plated contact pads on the puck are useful for either wire bonding or soldering For more information regarding sample wiring refer to Section 5 2 Quantum Design PPMS ETO User s Manual 1084 700 Rev A1 3 5 September 2011 CHAPTER 4 Software 4 1 4 2 4 2 1 Introduction This chapter contains the following information e Section 4 2 presents an overview of the ETO software including the ETO console e Section 4 2 2 discusses the ETO status log e Section 4 3 reviews how to create data files and contains descriptions of each data column contained within the file Overview of Electrical Transport Option Software ETO Console Whenever the Electrical Transport Option is active t
21. dow displays base system information relevant to both channels Figure 5 2 shows the resistance measurement window To make a measurement enable one or both channels set all of the measurement parameters then press the Measure button at the bottom Resistance measurements will run until both channels are finished Make sure to check the Save Results to File checkbox if you want to save the data Measurement results will be displayed in the bottom of the window Take the following steps to run an immediate mode measurement 1 Check the Enable Measurement checkbox corresponding to the channel s you would like to measure 2 Select either 4 wire or 2 wire from the Sample Wiring drop down menu corresponding to the wiring configuration used when the sample was mounted Quantum Design PPMS ETO User s Manual 1084 700 Rev A1 5 3 September 2011 Section 5 4 Chapter 5 Impedance Mode Measurements ETO Measurements 3 Use the Amplitude text box to specify the peak AC amplitude of the sinusoidal excitation applied during the measurement Make sure the excitation is not large enough to damage your sample The Amplitude will have units of mA for 4 wire configurations and in V for 2 wire 4 Select the excitation frequency from the Freq drop down menu 5 Select the Range from the drop down menu or check the Autorange check box if you want the range to be determined for you The Range will have units of volts for 4 wire configurations and amps for 2
22. driver adjusts the applied potential to maintain a constant output current regardless of the sample and lead resistance Figure 3 1 b shows the load lines for the current driver with feedback on As the graph shows the current is independent of the measured voltage across the sample The driver behaves as a current source for potentials up to the 30 V compliance of the source In this mode the current driver has high output impedance This is the default operating mode and is desirable for most measurements and samples When feedback is off the drivers can be represented as a voltage source behind a source resistance Figure 3 3 a shows the equivalent circuit when the feedback is turned off In this case the current passing through the sample is dependent on the sample and lead resistance Figure 3 3 c shows the load lines for the current driver as a function of the measured sample voltage In this configuration the sample current decreases with increasing sample voltage If the sample or lead impedance is comparable or larger than the source impedance the actual current will be significantly lower than the requested current ETO will correct for this discrepancy as best as possible and the corrected current will be reported in the data file The corrected current will be a good approximation of the actual sample current in the limit that Rpeags lt lt Roprive For systems with large lead resistance the current can be manually corrected as follows
23. e AC current response is measured with a current amplifier The DSP is used to filter the AC response and pick out the portion of the response at the same frequency and phase as the drive signal All other components of the signal are filtered out eliminating frequency dependent noise DC offsets and instrument drift The DSP can also calculate harmonic components of the measured signal The current source has a minimum precision of 1 nA and a maximum current of 100 mA It is capable of supplying both DC and AC current with frequencies from 0 1 Hz to 200 Hz The preamplifiers consist of a high gain amplifier a programmable gain amplifier and a high impedance current amplifier These three preamps in conjunction with the current source give the ETO a noise floor of 10 nQ and allow measurement of resistances up to 5 GQ The Electrical Transport option is available on both PPMS and VersaLab systems The ETO software is integrated into the MultiVu software application used to control and monitor the system hardware You may use any MultiVu commands while working with the ETO This software integration allows you to utilize MultiVu sequences to fully automate system operations and run a wide range of measurements without being present in the laboratory Quantum Design PPMS ETO User s Manual 1084 700 Rev A1 1 1 September 2011 Section 1 3 Chapter 1 ETO Measure Types Theory of Operation 1 3 Electrical Transport Option Measurement Types
24. ediate mode the sequence command for IV curves can only perform measurements on one channel at a time To measure both channels requires two sequence commands IV Sequence Select Sample1 Sample 2 AC Excitation Frequency 0 3 Hz AC Amplitude 10 m C Disable Drive Feedback Preamp Gain EN y Sample Wiring Data Logging Waveform Select oy oY ON Ow IV Sweeps 1 v Figure 5 8 The sequence command window for IV measurements 5 10 PPMS ETO User s Manual 1084 700 Rev A1 September 2011 Quantum Design Chapter 5 Section 5 5 ETO Measurements Sequence Measurements 5 5 4 New Data File Figure 5 9 shows the sequence command window to select or create a new data file within a sequence Insert this command whenever you need to switch files such as between measurements of different types Press the Browse button to open the file dialog and select the file Selecting the Create New File Version radio button will create a new file with the name specified or add a numeric suffix if the file already exists Selecting the Append to File radio button will add the data to an existing data file NewDatafileDlg 2default dat Browse default dat File Action Create New File Version Append to File Figure 5 9 The sequence command window for creating a New Data File Quantum Design PPMS ETO User s Manual 1084 700 Rev A1 5 11 September 2011
25. en the file specified in the File Name field provided the file has already been created Quantum Design PPMS ETO User s Manual 1084 700 Rev A1 4 3 September 2011 Section 4 2 Chapter 4 Overview of Electrical Transport Option Software Software ETO Console Setup Data File Measurement Path CAQdY ersal ab Electrical Transports File Name eto_default dat Create new file version Sample Figure 4 4 Data File tab in the ETO Console window 4 2 1 3 MEASUREMENT TAB The Measurement tab is used to open the measurement window for the selected measurement The radio buttons on the right indicate the measurement type selected and the display window gives an example of the type of data that can be collected After you have selected the measurement type press the Launch Measurement button to bring up the immediate mode measurement window While an immediate mode measurement window is active this tab is not active The active measurement window must be closed prior to launching a different measurement window 4 4 PPMS ETO User s Manual 1084 700 Rev A1 Quantum Design September 2011 Chapter 4 Section 4 3 Software Electrical Transport Option Data Files ETO Console Setup Data File Measurement AC Resistance Mode 1 0 Resistance O dvdl OW El ES a goo 3 E e s 0 100 110 Temperature K Launch Measurement Figure 4 5 Measurement tab in the ETO Console window
26. enting the charge of the carriers To measure the Hall potential arrange the voltage leads perpendicular to both the current and field directions Figure 1 2 shows a thin film rectangular sample wired up to detect the Hall potential In this example the magnetic field would be applied normal to the sample surface Using Eq 1 you can rewrite Eq 4 in terms of the resistance R reported by ETO RA R 5 4B Accurately measuring the Hall potential can be difficult To measure the potential difference due only to the Hall potential the voltage leads must be perfectly perpendicular to the bias field If this is not the case the measured potential will include a component due to the longitudinal potential resulting from the sample resistance The magnitude of the longitudinal potential is typically much larger than the Hall potential making even small errors in lead placement problematic Both the Hall potential and the longitudinal potential are proportional to the bias current so the AC filtering technique employed by the ETO does not eliminate this effect V I V l Figure 1 2 Typical lead placement on a rectangular thin film sample for measurement of the Hall potential The magnetic field would be applied normal to the sample surface PPMS ETO User s Manual 1084 700 Rev A1 Quantum Design September 2011 Chapter 1 Section 1 3 Theory of Operation ETO Measure Types 1 3 2 133 Current mA Current Voltage Curv
27. er Verify that the power is off All of the module LEDs should be dark Remove the cover plate for one of the rear high power module bays and carefully insert the module into the bay Gently finger tighten the two mounting screws to secure the module in place The module should now be flush with the other modules or cover plates The ETO head needs to be mounted close to the Grey Lemo connector at the back of the sample chamber Determine the optimal mounting location for the ETO head and place the two pieces of self adhesive grip tape on the PPMS dewar at this location Make sure the head is close enough that the sample cable can easily reach the Grey Lemo without stressing the cable Press the ETO head onto the grip tape to secure it in place Make sure the head is not touching any other dewar components Connect the ETO Module Cable 3101 455 02 and Fan Cable 3101 457 02 between the ETO module and the ETO head PPMS ETO User s Manual 1084 700 Rev A1 September 2011 Quantum Design Chapter 2 Installation 7 Section 2 2 Initial Installation of Hardware and Software Turn on the power to the Model 6000 tower Verify that both the PWR and COP indicator LEDs on the module are green It may take up to 30 seconds for the module to boot and the LEDs to turn green The COP LED will blink green until the option is activiated 2 2 1 2 VERSALAB HARDWARE INSTALLATION Refer to the VersaLab User s Manual for any issues regarding t
28. erential Resistance Curves cccccscccesscecsseceesseceeaeeceeeeecsaeceeaaecseaeeceaeeseaaeceeaeeneneeenaees 5 6 A Sequence Measurement A A 5 7 Sl BETO RESISTAOCE il A ee eo 5 8 A NI NN 5 9 NXS AA OT 5 10 o New Data AA A RT 5 11 iv PPMS ETO User s Manual 1084 700 Rev A1 Quantum Design September 2011 Contents Table of Figures Figures Figure 1 1 Figure 1 2 Figure 1 3 Figure 2 1 Figure 3 1 Figure 3 2 Figure 3 3 Figure 3 4 Figure 4 1 Figure 4 2 Figure 4 3 Figure 4 4 Figure 4 5 Figure 5 1 Figure 5 2 Figure 5 3 Figure 5 4 Figure 5 5 Figure 5 6 Figure 5 7 Figure 5 8 Figure 5 9 Quantum Design Typical lead placement on a rectangular thin film sample for a four wire and b two wire lead geometries versidad rd didas 1 3 Typical lead placement on a rectangular thin film sample for measurement of the Hall potential The magnetic field would be applied normal to the sample surface 1 4 Two graphs showing current and voltage waveforms a and the resulting I V curve b for a diode measured using the ETO oooocccnncccinocacanocononcconnanonnncnnnncananenonnns 1 5 Activate the Electrical Transport Option using the Option Manager dialog box 2 4 Pictures of a the ETO module CM H and b the remotely mounted ETO head Picture of the ETO module front panel showing the CH1 1 measured signal BNC JH 1 CH1 drive signal BNC JH 2 CH2 measured signal BNC JH 3 CH2 dr
29. es The ETO is capable of measuring the current voltage characteristics of any sample or device In this mode the electronics applies a triangular excitation waveform and measures a response waveform These two waveforms are combined to form the current voltage curve for the device under test The triangular excitation waveform always starts and ends at zero bias Figure 1 3 a shows both an excitation waveform and the response waveform for a diode plotted as a function of time The nonlinear device characteristics are clearly visible in the response waveform Figure 1 3 b shows resulting I V curve when the current waveform is plotted as a function of the voltage waveform The ETO software allows you to select the number of quadrants to measure and in what order The resulting curve will contain 256 points per quadrant Both four wire and two wire IV curves can be measured In the four wire case a current excitation waveform is used and a voltage response waveform measured In the two wire case a voltage excitation waveform is used and a current response waveform measured 10 A aBeyon Current mA o ua 10 Time Arb 3 2 1 0 1 b Voltage V Figure 1 3 Two graphs showing current and voltage waveforms a and the resulting I V curve b for a diode measured using the ETO Differential Resistance Curves The ETO is capable of measuring differential resistance as a function of bias current or voltage This is achieved by apply
30. he ETO Console window will be present within the MultiVu window This window can be minimized but will only close when the option is deactivated From the console window you can perform all basic system operations such as sample installation setting up data files and running measurements manually in immediate mode The ETO Console contains a Setup tab Data File tab and a Measurement tab The functionality of each tab is described below 4 2 1 1 SETUP TAB The Setup tab is the default tab for the ETO Console and is displayed when the option is initially activated Figure 4 1 shows the Setup tab within the ETO Console This tab is used to install or remove samples and enter information about the samples that will be entered into the data file The Sample Installation Wizard button will launch a separate window for the wizard when pressed This wizard will guide you through the steps necessary to open the sample chamber to either install or remove a sample Figure 4 2 shows the Sample Installation Wizard window The System Status panel displays the current system status and the Instructions panel displays information and guidance regarding each step of the wizard The wizard does not execute any Quantum Design PPMS ETO User s Manual 1084 700 Rev A1 4 1 September 2011 Section 4 2 Chapter 4 Overview of Electrical Transport Option Software Software commands when started and requires that the user press the Open Chamber button to initiate the
31. he VersaLab system 1 2 Turn off the power to the VersaLab system Open the hood covering the CAN rack and verify that none of the modules already installed have power All of the module LEDs should be dark Install the Accessory Mounting Bracket to the VersaLab frame using the two 6 32 screws washers and nuts provided in the Accessory Mounting Kit Remove the cover plate for the left most module bay as viewed when facing VersaLab Carefully insert the module into the bay Gently finger tighten the two mounting screws to secure the module in place The module should now be flush with the other modules or cover plates Mount the ETO Head to the accessory mounting bracket using the hook and loop fastening tape on both the head and the bracket Be sure to mount the head in the correct orientation Note When installed properly the ETO head should not touch any of the mounting screws and should not interfere with the hood when closed Adjust the location of the head if necessary Connect the ETO Module Cable 3101 455 01 and Fan Cable 3101 457 01 between the ETO module and the ETO head Turn on the power to the VersaLab system Verify that both the PWR and COP indicator LEDs on the module are green It may take up to 30 seconds for the module to boot and the LEDs to turn green The COP LED will blink green until the option is activiated 2 2 1 3 DYNACOOL HARDWARE INSTALLATION 1 Quantum Design Turn off the power to the P
32. ing a small AC excitation on top of a DC offset bias The AC response is measured and used to calculate the differential resistance in the same manner as the standard resistance measurement when no DC bias signal is applied The differential resistance is a direct measure of the first derivative of the IV curve at a given DC bias This type of measurement is very useful for examining small nonlinearities in a given device Quantum Design PPMS ETO User s Manual 1084 700 Rev A1 1 5 September 2011 CHAPTER 2 Installation 2 1 2 2 Introduction This chapter contains the following information e Section 2 2 lists the components of the Electrical Transport Option and describes the procedure for installation on PPMs and VersaLab systems Initial Installation of Hardware and Software This section describes the procedures for the initial installation of the Quantum Design Electrical Transport Option ETO onto the PPMS and VersaLab systems These procedures apply only to the first time you install and use ETO Normal activation and use of the option is covered in Chapter 4 Note If your system came from Quantum Design with ETO already installed you do not need to follow the procedures in this chapter Refer to Chapter 4 for normal operation Table 2 1 lists the components of the Quantum Design Electrical Transport Option Please verify that you have received all the components before you begin the installation process Table 2 1 A
33. ive signal BNC JH 4 the head cable connector JH 5 and the fan cable AMAT A iden svadeseavadanceardadecensadabedanvaies 3 2 The equivalent circuit for ETO when drive feedback is disabled The dashed line represents the current source equivalent circuit 2 ee ee eeeeeereeereeeeeeeeensecnaeenaeens 3 3 Pictures of the ETO option installed onto a a PPMS system b a VersaLab system and c Dynacool system On the PPMS the head is mounted on the dewar using grip tape VersaLab requires the use of the accessory mounting kit 4372 079 3 5 Setup tab in the ETO Console Window ooooonocccoconocononoconoconcconaconccnnn conc nnnanonacrna conan 4 2 The Sample Installation Wizard Window oocoonconnconoccnocnnoonononcnonononoconoconoconccnnncnnnannos 4 2 The Sample Configuration Window oooooccconccooncnoncnonnnonnnnnncnnncnn nono nono noconacnnccnnnannnannos 4 3 Data File Tab in the ETO Console Window oooconcccnocnnocnnocncncncnnonnncnononncconccnnannnannnos 4 4 Measurement Tab in the ETO Console Window ocococcccnocccnonanononononononanacnnnnccnnnccnnnos 4 5 Sample wiring examples a Shows mounted both a 2 wire sample on channel 1 and a 4 wire sample on channel 1 b Shows mounted a 4 wire sample on channel 1 and a 4 wire Hall sample on channel Zo ooooonconnccnicccicacocononaconaconaconncanncnnos 5 2 The immediate mode AC Resistance Measurement Wind W oococonocococcconcconncnnnannss 5 4 The immediate mode IV measurement Window
34. lation 2 2 2 Install the ETO Software Use the following instructions to install the VersaLab Electrical Transport Option software on your PC See the MultiVu User s Manual for MultiVu installation instructions The installation wizard will install all of the option files in the C QDPPMS ETOption C QDVersaLab ETOption or C QDDynacool ETOption directory for PPMS and VersaLab respectively 1 Close all other applications prior to installing the ETO software 2 Double click the ETO Installer msi file to start the installation wizard Follow the instructions on the screen to install the software Note Be sure to select the correct base system type either PPMS or VersaLab when prompted 3 Verify that the ETO software is installed correctly by activating it within the MultiVu software a Open the MultiVu application software b Select Utilities gt gt A ctivate Option c In the Option Manager dialog box select Electrical Transport from the Available Options list and press the Activate button d Electrical Transport will move to the Active Options list inside the Option Manager e The Electrical Transport software will open the ETO Console window and the ETO Event Log window confirming that the software was install correctly Option Manager Available Options Active Options Electrical Transport Activate gt gt Connection Diagrams Close Figure 2 1 Activate the Electrical Transport Optio
35. list of hardware components comprising the Electrical Transport Option for a PPMS b VersaLab and c Dynacool systems a PPMS COMPONENT PART NUMBER ETO Module CM H 4101 451 ETO Head EM QN 4101 455 ETO Module Cable 3101 455 02 ETO Sample Cable 3101 456 01 ETO Fan Cable 3101 457 02 ETO Accessory Kit 4084 710 Quantum Design PPMS ETO User s Manual 1084 700 Rev A1 2 1 September 2011 Section 2 2 Initial Installation of Hardware and Software 2 2 1 2 2 b VERSALAB COMPONENT PART NUMBER ETO Module CM H 4101 451 ETO Head EM QN 4101 455 Accessory Mounting Kit 4372 079 ETO Module Cable 3101 455 01 ETO Sample Cable 3101 456 01 ETO Fan Cable 3101 457 01 ETO Accessory Kit 4084 710 c DYNACOOL COMPONENT PART NUMBER ETO Module CM H 4101 451 ETO Head EM QN 4101 455 ETO Module Cable 3101 455 01 ETO Sample Cable 3101 456 01 ETO Fan Cable 3101 457 01 ETO Accessory Kit 4084 710 Chapter 2 Installation Install the ETO Module 4101 451 and ETO Head 4101 455 Use this section only if the ETO electronics have not been installed on your PPMS or VersaLab system 2 2 1 1 PPMS HARDWARE INSTALLATION Refer to the PPMS User s Manual for any issues regarding the PPMS These installation instructions assume the Model 1000 tower and CAN bus have already been installed and tested 1 2 3 Turn off the power to the Model 1000 CAN tow
36. n using the Option Manager dialog box 2 2 3 Configuring the Electronics The ETO electronics are ready to use out of the box and do not require any calibration files on the PC All of the calibration and configuration information is stored inside the module SROM Contact your customer service representative with any problems associated with the calibration or SROM 2 4 PPMS ETO User s Manual 1084 700 Rev A1 Quantum Design September 2011 C H APTER 3 Hardware 3 1 Introduction This chapter contains the following information e Section 3 2 discusses the operation of the ETO electronics e Section 3 3 discusses the cables and jumpers e Section 3 4 discusses the sample pucks 3 2 ETO Module and Head The Electrical Transport Option electronics consists of the module CM H and the remotely mounted head EM QN The module contains a Digital Signal Processor DSP that performs all AC stimulus response calculations and a secondary processor for post processing and communications The remotely mounted head contains two sets of current drivers and preamplifiers to allow for simultaneous independent resistance measurements on channel 1 and channel 2 Figure 3 1 shows the module and head enclosures b Figure 3 1 Pictures of a the ETO module CM H and b the remotely mounted ETO head EM QN To perform a basic transport measurement an AC drive signal is generated at the requested frequency by the DSP The cu
37. nd cautions These are provided to help you understand how to safely and properly use the Electrical Transport Option ETO Quantum Design Inc disclaims any liability for damage to the system or injury resulting from misuse or improper operation of the system Please contact your Quantum Design representative for any service issues This product is NOT user serviceable by the user viii PPMS ETO User s Manual 1084 700 Rev A1 Quantum Design September 2011 CHAPTER 1 Theory of Operation 1 1 1 2 Introduction This chapter contains the following information e Section 1 2 gives an overview of the Electrical Transport Option e Section 1 3 discusses the different measurements that are possible with ETO Overview of the Electrical Transport Option The Quantum Design Electrical Transport Option ETO enables users to make several different types of transport measurements over a wide range of resistance values and sample types The option contains two separate channels each with their own dedicated electronics to allow simultaneous continuous resistance measurement of two different samples Each channel s electronics consists of a precision current source and voltage preamplifiers coupled to a Digital Signal Processor DSP Measurements are usually made by applying a sinusoidal AC drive current and measuring the AC voltage response However a special 2 wire high resistance mode is available where an AC voltage is applied and th
38. nt Voltage Curves coincida aia 1 5 t33 Differential R sistance CUYOS nad RA 1 5 CHAPTER 2 Iastalla on ala ace dla il iaa 2 1 21 ES A NN 2 1 2 2 Initial Installation of Hardware amp SO tWAT8 ccooooocononoooccnonononononnnnconnnnnononnnnnononnnnnn nn nnconnnnnnnnnnnss 2 1 2 2 1 Install the ETO Module 4101 451 amp ETO Head 4101 455 0oooooocnnnccccocncooonnnonanoconanonns 2 2 2 2 1 1 PPMS Hardware Installation nen neike apiaster inie ia arean ttiie 2 2 2 2 1 2 VersaLab Hardware Installati0N ooooonnnococcnonocnncnononnnonononononononononononnnnonnnnncnnnos 2 3 2 2 1 3 Dynacool Hardware Installati0N ooonnonnnnnnnnnnnonoccnonncnoncnnnccnnocnoconccnnccnnccnnccnnncnnnos 2 3 2 2 2 smstallithe E TO S oft wares cits site ia ii WA de es ES 2 4 22 3 Configuring the Electronics usisne essenin aee a ea thes nEaN RESTS 2 4 CHAPTER 3 PRAT WAL E E icbaectaicedectdaacastiaaeeneuidinsauchatesSeeusisoasscomaipecktinesscoanessuccauiniten 3 1 A A A ER 3 1 3 2 ETO Module Head naniesione a a iets aisle ats eesti 3 1 3 2 0 Current Driver BIECtrOmiCs csds30 cs sesceccaceesesa ibe ck a a stead ehcsecceseaae netos casdanedeebesetdeosaace 3 2 S222 A clesees eote E Liki pees ier bettas hens ele neta RO RE hae rites 3 4 323 Cables Se JUMpers ttre lox e ne ee A ecto ee Unga E E A lot nese owes 3 5 3 4 Sample Pucks s 3s c shiteccieed os hie beeen eee RI ea See ede Blo ete eee 3 5 Quantum Design PPMS ETO User s Manual 1
39. nterpreting the resulting data The Electrical Transport option is also capable of measuring large resistances using a two terminal lead geometry 2 wire mode This mode is typically used for resistances above 10 MQ In 2 wire mode the system applies a voltage across the sample and uses the high impedance amplifier to measure the current passing through the sample The resistance is again calculated using Ohms law Figure 1 1 b shows a sample wired up in the two terminal configuration To achieve the best results the sample should be rectangular or bar shaped with the leads far apart yielding a well defined measurement region where the electric field line density is uniform Lead and contact resistance can usually be ignored in this case as long as they are much less than the sample resistance It V V l I V a b Figure 1 1 Typical lead placement on a rectangular thin film sample for a four wire and b two wire lead geometries 1 3 1 1 HARMONIC DETECTION The second and third harmonics of the measured response are reported in units of dB during a resistance measurement The units of dB are referenced to the voltage of the fandamental response This information can be related to nonlinearities in the sample but is often an indicator of the amount of noise present during a measurement The second and third harmonic contribution is typically less than 50 dB for a good measurement 1 3 1 2 HALL COEFFICIENT While it is not explici
40. rrent driver board in the head receives the drive signal and converts it to a current that is applied to the sample The preamplifier board in the head detects and amplifies the sample response signal and sends it back to the DSP for processing The DSP calculates the in phase and out of phase components of the response signal as well as several harmonic amplitudes Quantum Design PPMS ETO User s Manual 1084 700 Rev A1 3 1 September 2011 Section 3 2 Chapter 3 ETO Module and Head Hardware The module CM H contains four BNC outputs for use in monitoring the drive JH 2 and JH 4 and response signals JH 1 and JH 3 for both channel 1 and 2 The BNC labels are located on the module front panel as shown in Figure 3 2 The drive signal full scale is 10 V For example on the 100 mA range a 50 mA peak excitation current would generate a 5 V peak signal at the BNC The response signal is monitored behind the preamplifiers The response signal measured at the BNC needs to be divided by the total gain to obtain the voltage at the sample Figure 3 2 Picture of the ETO module front panel showing the CH1 1 measured signal BNC JH 1 CH1 drive signal BNC JH 2 CH2 measured signal BNC JH 3 CH2 drive signal BNC JH 4 the head cable connector JH 5 and the fan cable connector JH 6 3 2 1 Current Driver Electronics The current drivers in ETO employ active feedback to approximate an ideal current source When the feedback is on the current
41. t window While the measurement is being performed the Measure button will display Stop Press this at any time to abort the current differential resistance measurement The status bar at the bottom of the window will display the measurement progress When the status bar is full the dV dI curve will be available in the data file 5 5 Sequence Measurements A sequence can be used to run a series of measurements sequentially or to change other system properties while measuring such as temperature or magnetic field Any number of measurement commands or system commands can be run from within a sequence Figure 5 5 shows the list of sequence commands available in MultiVu when ETO is active All ETO specific commands are listed under Measurement Commands gt gt Electrical Transport Note For detailed information about creating and editing sequence files and for a discussion about all standard sequence commands refer to the PPMS or VersaLab User s Manual Quantum Design PPMS ETO User s Manual 1084 700 Rev A1 5 7 September 2011 Section 5 5 Chapter 5 Sequence Measurements ETO Measurements Sequence Commands oe System Commands Beep Call Sequence or Script Chamber Operations Remark Scan Field Scan Temperature Scan Time Sequence Message Set Field Set Temperature Shutdown Wait E Measurement Commands E Electrical Transport ETO dvdl ETO Iv ETO Resistance New Datafile Log Data Sigma Log Data lt gt Figure 5 5
42. ted to the I pad and the V pad as shown in Figure 5 1 a channel 1 It is important that you use the I and V pad or the measured resistance will have the wrong sign or value Hall measurements are not possible in the 2 wire configuration Figure 5 1 Sample wiring examples a Shows mounted both a 2 wire sample on channel 1 and a 4 wire sample on channel 1 b Shows mounted a 4 wire sample on channel 1 and a 4 wire Hall sample on channel 2 53 Sample Installation The sample installation wizard is accessible from the Setup tab on the ETO Console You are encouraged to use this wizard as 1t automates the installation process and leaves the sample chamber in the proper state for temperature cycling Pressing the Sample Installation Wizard 5 2 PPMS ETO User s Manual 1084 700 Rev A1 Quantum Design September 2011 Chapter 5 Section 5 4 ETO Measurements Immediate Mode Measurements button will launch the wizard window shown in Figure 4 2 Follow the instructions on the screen to install your sample When prompted by the wizard install the sample puck using the puck extraction tool For more information on sample installation refer to either the PPMS or Versalab manual Pressing cancel at any time during the wizard will abort the wizard safely Enter sample information after installing the sample puck into the sample chamber Press the Sample Properties button to bring up the dialog window Enter the wiring configuration for sample 1 and
43. tly supported it is possible with proper lead placement to perform 4 wire Hall measurements using the Electrical Transport Option When charged particles move perpendicular to a magnetic field a force is exerted on them perpendicular to both the field and the direction of particle motion The force can be expressed as F qvxB 3 This transverse force can often cause charge carriers to build up on one edge of a sample leading to a potential difference across the sample This potential difference is called the Hall potential Vy The sign of the Hall potential generally indicates the sign of the charge carriers and the Quantum Design PPMS ETO User s Manual 1084 700 Rev A1 1 3 September 2011 Section 1 3 Chapter 1 ETO Measure Types Theory of Operation 1 4 magnitude of the potential is related to the density of charge carriers in the sample The Hall coefficient Ry describes these two properties and is defined as _ Ey V A B UB 4 where Ey is the Hall field j is the current density and B is the magnitude of the magnetic field For a well defined geometry the current density is equal to JA where Z is the current and A is the sample cross sectional area and the Hall field is equal to V Here is the distance between a set of transverse voltage leads used to measure the Hall potential It can be shown that the Ry nq with n representing the number of charge carriers per unit volume in the sample and q repres
44. tom of the window are displayed the Temperature Magnetic Field and Position of the samples inside the sample chamber 5 4 PPMS ETO User s Manual 1084 700 Rev A1 Quantum Design September 2011 Chapter 5 ETO Measurements Section 5 4 Immediate Mode Measurements 5 4 2 Current Voltage Curves Current voltage curves can be taken on only one channel at a time Take the following steps to measure a current voltage curve in immediate mode 1 2 Select the radio button for Sample 1 or Sample 2 to select a channel Select either 4 wire or 2 wire configuration from the Sample Wiring drop down list Select the sweep frequency from the Frequency drop down list Use the AC Amplitude text box to specify the peak amplitude of the sweep The AC Amplitude has the units mA with 4 wire configuration and V in 2 wire Make sure the Disable Drive Feedback box is un checked This feedback should only be disabled if you are measuring a sample with a highly non linear I V characteristic See section XXXX for more details regarding the drive feedback Select the type of excitation waveform desired You have the option of performing a four quadrant sweep or a two quadrant sweep in the positive or negative direction Use the IV Sweeps text box to specify the number of sweeps to average together to create the IV curve Select the Range from the drop down menu Press the Measure button to begin the measurement IV Measurement Select Waveform
45. urements 0 u Figure 5 6 The sequence command window for resistance measurements 5 5 2 ETO dV dI Figure 5 7 shows the sequence command window for differential resistance measurements Follow the same steps outlined in Section 5 4 3 to specify the measurement parameters When you are finished press the OK button and the measurement command will appear in the sequence window As with the immediate mode the sequence command for differential resistance can only perform measurements on one channel at a time To measure both channels requires two sequence commands Quantum Design PPMS ETO User s Manual 1084 700 Rev A1 5 9 September 2011 Section 5 5 Sequence Measurements dV dl Sequence Dialog Select Sample 1 O Sample 2 AC Excitation Frequency 15 w Hz AC Amplitude 2 m Preamp Range Sample Wiring Settings Averaging Time 1 sec Data Logging Chapter 5 ETO Measurements DC Sweep l 0 l Time DC Amplitude 50 Step Size 5 Steps Quadrant 10 Ramp to Starting Point Settling Time 100 ms Figure 5 7 The sequence command window for differential resistance measurements 5 5 3 ETO IV Figure 5 8 shows the sequence command window for the IV curve measurements Follow the same steps outlined in Section 5 4 2 to specify the measurement parameters When you are finished press the OK button and the measurement command will appear in the sequence window As with the imm
46. urements Available Measurements Figure 4 3 The Sample Configuration window 4 2 1 2 DATA FILE TAB The Data File tab is used to specify the data file into which the ETO data is written Pressing the Browse button will bring up a standard Windows file interface that allows you to specify a file name and location on the PC for the data file You can use this window to either select an existing file or create a new file name If a new data file name is selected the data file is not created immediately Instead the file is created when the first data point is written to the file The currently selected target file and its location are displayed in the Path and File Name fields The Create new file version checkbox when checked will add a numeric suffix to the file name displayed if the file already exists If this box is unchecked the option will append to an existing data file The Sample Properties button is also contained in the Data File tab in the event the Setup tab is not used The functionality for this button is identical to that on the Setup tab and you can enter information from either tab The information contained in the Sample Properties window is written to the data file when it is first created New sample information can be entered at any time before a new measurement is taken and the new file is created The View button opens the selected data file and displays the data as a new graph in MultiVu It will always op
47. wire up both channels to the same sample as this may lead to errors in the reported resistance due to stray capacitance Quantum Design PPMS ETO User s Manual 1084 700 Rev A1 5 1 September 2011 Section 5 3 Chapter 5 Sample Installation ETO Measurements 5 2 1 4 Wire Mounting Configuration To make a standard resistance measurement in 4 wire configuration you should mount your sample as shown in Figure 5 1 a for the sampled wired to channel 2 The two current leads should be at the ends of your sample and the two voltage leads should be in line between the current leads Ensure that the polarity of the voltage leads matches that of the current leads or the reported resistance will be negative 5 2 1 1 HALL COEFFICIENT MOUNTING CONFIGURATION ETO can also be used to make Hall measurements Figure 5 1 b shows channel 1 wired for a standard resistance measurement and channel 2 wired for a Hall measurement The wiring arrangement shown yields the proper sign for the Hall coefficient It is important when wiring a Hall sample that the voltage contacts are at the same zero field potential to avoid measuring longitudinal signal This is usually achieved by making sure the voltage contacts are perpendicular to the current contacts ETO does not support 5 wire Hall measurements 5 2 2 2 Wire Mounting Configuration For samples whose resistance exceeds 10 MQ the 2 wire configuration is necessary In this case the sample is connec

Electrical Transport Option (ETO) User`s Manual

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