SCILOGEX RE100-Pro Rotary Evaporator manual
Contents
1. 6 Faults Instruments can t be power ON Check whether the power line is unplugged Check whether the fuse is broken or loose Fault in power on self test Switch OFF the unit then switch ON and reset the instruments to factory default setting not contact If manufacturer supplier these faults are resolved please 7 Maintenance and Cleaning Proper maintenance can keep instruments working properly and lengthen its lifetime Do not spray cleanser into the instrument when cleaning Unplug the power line when cleaning Only use recommended cleansers Dyes Isopropyl alcohol Construction materials Water containing tenside Isopropyl alcohol Cosmetics Water containing tenside Isopropyl alcohol Foodstuffs Water containing tenside Fuels Water containing tenside Before using other method for cleaning or decontamination the user must ascertain with the manufacturer that this method will not harm the instrument Wear the proper protective gloves during cleaning of the instrument A Rotary Evaporator Note Electronic device can not clean with cleanser If you require maintenance service must be cleaned the instrument in advance to avoid pollution of hazardous substances and to send back into original packing If the instrument will not use for a long time please switch off and place in a dry clean room temperature and stable location Rotary Evaporator 8 Associated Regulations Stan2. Motor 4 n Rotary Evaporator d Evaporating flask Receiving flask _ Heating bath a Operation panel Figure 1 Heating bath connector Power supply Figure 2 USB Rotary Evaporator Items Descriptions LED power Push the key and then rotate control knob Speed key to set the rated speed in th from 20 Lice Likio kaj Speed o set the rated speed in the range from to 280 Push the key and then rotate control knob Temperature LCD display k mm to set the rated temperature in the range ey tainly from room temperature to 180 C Push the key and then rotate control knob i metoj t t th ted ti in th f 1 o set the rated time in the range from Speed key ON ike to 999 min Temperature key Control knob Timer key Push the key and then rotate control knob Int key to set the interval for right left running in Figure 3 the range from 1 to 999s Clockwise rotate to increase program values Rotate anti clockwise to decrease program Control knob values POETO Press the knob switch ON OFF the unit Press the key the lift goes up Release the Lift up key key the lift stops and remains in that Figure 4 position Lift down key Press the key the lift goes down Release LCD display LED power Power switch 4 2 Display Speed symbol lo oH H H RPM Pte k Rotate the key the lift stops and remains in that position LCD displays the real working state P
3. bottles or an effective extraction system Evacuated glass vessels must not be heated on one side the evaporating flask must rotate during the heating phase The glassware is designed for operation under a vacuum of up to 10 mbar The equipment must be evacuated prior to heating see chapter Commissioning The equipment must only be aired again after cooling When carrying out vacuum distillation uncondensed vapours must be condensed out or safely dissipated If there is a risk that the distillation residue could disintegrate in the presence of oxygen only inert gas must be admitted for stress relief CAUTION Avoid peroxide formation Organic peroxides can accumulate in distillation and exhaust residues and explode while decomposing Keep liquids that tend to form organic peroxides away from light in particular from UV rays and check them prior to distillation and exhaust for the presence of peroxides Any existing peroxides must be eliminated Many organic compounds are prone to the formation of peroxides e g dekalin diethyl ether dioxane tetrahydrofuran as well as unsaturated hydrocarbons such as tetralin diene cumene and aldehydes ketones and solutions of these substances DANGER OF BURNING The heating bath tempering medium evaporator piston and glass assembly can become hot during operation and remain so for a long time afterwards Let the components cool off before continuing work with the device ATTENTION Avoi
4. d delayed boiling Never heat the evaporating flask in the heating bath without switching on the rotary drive Sudden foaming or exhaust gases indicate that flask content is beginning to decompose Switch off heating immediately Use the lifting Rotary Evaporator mechanism to lift the evaporator piston out of the heating bath Evacuate the danger zone and warn those in the surrounding area When the device is switched off or the power supply disconnected the internal safety lift removes the evaporator piston from the heating bath CAUTION Never operate the device when the evaporator piston is rotating and the lift is raised Always lower the evaporator piston into the heating bath first before starting the rotation drive Otherwise hot tempering medium may be sprayed out Set the speed of the drive so no tempering medium is sprayed out as a result of the evaporator piston rotating in the heating bath If necessary reduce the speed Do not touch rotating parts during operation Imbalance may result in uncontrolled resonance behaviour of the device or assembly Glass apparatus may be damaged or destroyed In the event of unbalance or unusual noises switch off the appliance immediately or reduce the speed The appliance does not start up again automatically following a cut in the power supply The device is only disconnected from the power Rotary Evaporator supply network if the device power switch is off or the 2 Proper Use plu
5. dards and Construction in accordance with the following safety standards EN 61010 1 UL 3101 1 CAN CSA C22 2 1010 1 EN 61010 2 10 Construction in accordance with the following EMC standards EN 61326 1 Associated EU guidelines EMC guidelines 89 336 EWG Instrument guidelines 73 023 EWG Changes or modifications not expressly approved by the party responsible for compliance could void the user s authority to operate the equipment NOTE This equipment has been tested and found to comply with the limits for a Class A digital device pursuant to Part 15 of the FCC Rules These limits are designed to provide reasonable protection against harmful interference when the equipment is operated in a commercial environment This equipment generates uses and can radiate radio frequency energy and if not installed and used in accordance with the instruction manual may cause harmful interference to radio communications Operation of this equipment in a residential area is likely to cause harmful interference in which case the user will be required to correct the interference at his own expense 9 Specifications Items Voltage VAC Frequency Hz Power W Motor Speed Range rpm Speed Display Temperature Range C Heat Control Accuracy C Temperature Display Heat Output W Lift Stroke mm Timer min Overall Dimensions DxWxH mm Weight kg Permissible Ambient Temperature C Speci
6. denser g Figure 12 and Figure 13 Figure 13 Load the cap nut h and locking spring i to Installing the vertical glassware condenser locking condenser in turn device Figure 14 Tighten the cap nut hand screwed h Start the 11 Figure 14 12 Rotary Evaporator Connecting tubes Figure 15 Vacuum tube Cooling water Cooling water Figure 15 5 2 Operation e Make sure the required operating voltage and power supply voltage match Ensure the socket must be properly grounded e Plug in the power cable ensure the power is on and begin initializing e Press Lift up Lift down key the lift goes up down Rotary Evaporator Release Lift up Lift down key the lift stops e Push the speed key and then rotate control knob to set the rated speed e Push the temperature key and then rotate control knob to set the rated temperature Push the timer key and then rotate control knob to set the rated time Deactivate the timer by setting the target value to 0 e Press the Int key and then rotate control knob to set the rated interval value Deactivate the interval by setting the target value to 0 Press the control knob switch ON If these operations above are normal the device is ready to operate If not the device may be damaged during transportation please contact manufacturer supplier for technical support Warning Forbid to transfer the flask when the instrument working 13
7. dous substances or under water Only process media that will not react dangerously to the extra energy produced through processing This also applies to any extra energy produced in other ways e g through light irradiation Tasks with the device must only be performed when operation is monitored Operation with excess pressure is not permitted for cooling water pressure see Technical Data Do not cover the ventilation slots of the device in order to ensure adequate cooling of the drive There may be electrostatic discharges between the medium and the drive which could pose a direct danger The appliance is not suitable for manual operation Safe operation is only guaranteed with the accessories described in the Accessories chapter Refer to the operating instructions for the accessories e g vacuum pump Only use the device under an all side closed exhaust or a compa rable protective device Adapt the quantity and the type of distilland to the size of the distillation equipment The cooler must work properly Monitor the coolant flow rate at the cooler outlet The glass equipment must always be ventilated when working under normal pressure e g open outlet at cooler in order to prevent a pressure build up Please note that dangerous concentrations of gases vapours or particulate matter can escape through the outlet at the cooler Take appropriate action to avoid this risk for example downstream cold traps gas wash
8. fications 100 240 50 60 1400 External rotor brushless motor 20 280 LCD RT 180 1 LCD 1300 Motor 150 1 999 465x457x583 15 5 40 Rotary Evaporator Permissible Relative Humidity 80 Protection Class acc To DIN IP20 EN60529 USB Yes Table 4 SCILOGEX LLC 500 Four Rod Road Suite 122 Berlin CT 06037 USA Tel 1 860 828 5289 Fax 1 860 828 5389 E mail info scilogex com Http www scilogex com
9. g is pulled out The socket for the mains cord must be easily The instrument is designed for distilling in schools laboratories or factories Together with the accessories accessible The voltage stated on the type plate must correspond recommended by manufacturer the device is suitable for to the mains voltage quick and gentle distillation of liquids evaporation of solutions and suspensions Socket must be earthed protective ground contact P P Removable parts must be refitted to the appliance to crystallisation synthesis or cleaning of fine chemicals prevent the infiltration of foreign objects liquids etc drying of powder and granulate material Protect the appliance and accessories from bumps and aecyeling of solvents impacts The appliance may only be opened by experts This device is not suitable for using in residential areas or other constraints mentioned in Chapter 1 3 Inspection 3 1 Receiving Inspection Unpack the equipment carefully and check for any damages which may have arisen during transport Please contact manufacturer supplier for technical support Note If there is any apparent damage to the system please do not plug it into the power line 3 2 Listing of Items The package includes the following items Items Qty Main unit 1 Heating bath 1 Power cable 1 Glassware vertical 1 User Manual 1 Table 1 4 Control and Display 4 1 Control elements Condenser
10. l info scilogex com Http www scilogex com Please provide the customer care representative with the following information e Serial number on the rear panel Certification Description of problem i e hardware or software e Methods and procedures adopted to resolve the problems e Your contact information Warranty This instrument is warranted to be free from defects in materials and workmanship under normal use and service for a period of 24 months from the date of invoice The watranty is extended only to the original purchaser It shall not apply to any product or parts which have been damaged on account of improper installation improper connections misuse accident or abnormal conditions of operation For claims under the warranty please contact your local supplier You may also send the instrument directly to manufacturer enclosing the invoice copy and by giving reasons for the claim 1 Safety Instructions Read the operating instructions in full before starting up and follow the safety instructions Keep the operating instructions in a place where they can be accessed by everyone Ensure that only trained staff work with the appliance Follow the safety instructions guidelines occupational health and safety and accident prevention regulations When working under a vacuum in particular Wear your personal protective equipment in accordance with the hazard category of the medium to be processed O
11. n lock Figure 7 Hold the lift with your hand on the height position and remove the thumb screw on the back of the appliance a Once the transportation lock has been removed the lift moves slowly to its upper end position The distance is 150mm Connect the device to the power supply using power cable b Connect the heating bath to the device c Figure 7 Remove the clamping device for the angle setting of the rotation drive on the right side of the lift by rotating the knurled screw d counter clockwise Set the drive at an angle of approx 30 Figure 8 Then secure the rotation drive from being accidentally turned by tightening the knurled screw in a clockwise direction Figure 8 Open the locking device on the drive head by turning it 60 counter clockwise e Figure 9 Feed the steam pipe in until it stops 10 Rotary Evaporator Then lock the locking device by turning it clockwise by 60 e The plastic screw nut f helps loosen tight fitting piston ground in connections Figure 9 Hold the tight fitting evaporator piston and counter clockwise e and then turn the plastic screw nut f until the evaporator piston neck Figure 9 Note Prior to commissioning hand tighten the plastic screw nut f left aligned e Installing condenser seal Figure 10 and Figure 11 Rotary Evaporator device at 200 rpm for 2 min Then tighten the cap Figure 11 eik e Installing con
12. nN Prem MR Rotary Evaporator User Manual RE100 Pro LCD Digital Rotary Evaporator Please read the User Manual carefully before use and follow all operating and safety instructions www scilogex com SCILOGEX Contents PrefdCe zis o reen 1 SOIVICE EE 1 W ATAUN serpeto o at o 1 l Safety Instructions issie srsti nereiks 2 2a Proper Uses suoni toe A eee AA o Rul 5 3 Inspection ie Ree RERO RD 6 3 1 Receiving Inspection esee 6 82 Tasting of Items ierit rere 6 4 Control and Display see 6 4 1 Control elements svc 1 n tte rts 6 42 DISplay entere novo e tete tid 8 5 Installation and Operation sees 9 5 T Installation sists iere there rettet 9 5 2 OperatiOn tene Rei Rs 12 Gs Faults iiit et et er tee 13 7 Maintenance and Cleaning sess 14 8 Associated Standards and Regulations 15 9 Specifications o ten meer 16 Rotary Evaporator Preface Welcome to the Rotary Evaporator User Manual Users should read this Manual carefully follow the instructions and procedures and be aware of all the cautions when using this instrument Service When help needed you can always contact the Service Department of manufacturer for technical support in the following ways SCILOGEX LLC 500 Four Rod Road Suite 122 Berlin CT 06037 USA Tel 1 860 828 5289 Fax 1 860 828 5389 E mai
13. ower ON LED power flash When the unit running LED power is lit Power ON or OFF Table 2 Speed display area tii Remote control External probe Sn is Temp 4 Temperature 0 e Timer Timer display TE area Timer Int a niena display min sec area Liu J Interval Figure 5 Speed display area Speed symbol Temperature display area Rotary Evaporator Descriptions Display in case of remote control Display when using external probe Display when the rotating function is switched ON Display when the heating function is switched ON Display when timer function is switched ON Display when Int function is switched ON When setting value and flashed The setting setting speed displaying the value does not flash until real speed reaches the set point Display when the rotating function is switched ON When setting temperature displaying the setting value When the heating function is switched ON displaying the real Ro tary Evaporator value Temperature Display when the heating function is symbol switched ON When setting timer displaying the rated Timerdisplay time When the timer function is area switched ON displaying remaining time Interval display area 3 5 1 Displaying the Int target value Table 3 Installation and Operation Installation Adjustable base Figure 6 Figure 6 CAUTION Loosen transportatio
14. therwise there is a risk of splashing liquids body parts hair clothing and jewellery getting caught injury as a result of glass breakage CAUTION Inhalation of or contact with media such as poisonous liquids gases spray mist vapours dusts or biological and microbiological materials can be hazardous to user Set up the device in a spacious area on an even stable clean non slip dry and fireproof surface Rotary Evaporator Ensure that there is sufficient space above the device as the glass assembly may exceed the height of the device Prior to each use always check the device accessories and especially the glass parts for damage Do not use damaged components Ensure that the glass assembly is tension free Danger of cracking as a result of stress due to incorrect assembly external mechanical hazards local temperature peaks Ensure that the stand does not start to move due to vibrations respectively unbelance Beware of hazards due to flammable materials combustible media with a low boiling temperature glass breakage CAUTION Only process and heat up media that has a flash point higher than the adjusted safe temperature limit of the heating bath that has been set The safe temperature limit of the heating bath must always be set to at least 25 C lower than the fire point of the media used Rotary Evaporator Do not operate the appliance in explosive atmospheres with hazar
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