SOP Site Report D - National Atmospheric Deposition Program
Contents
1. calibration mass of the new instrument The calibration mass can be found in the calibration summary labeled HgAmt Separate values are required for both the A and B cartridges Swap 1130 Pump Module New Serial Number If a second 1130 Pump Module is available and is installed record the serial number of the replacement unit Swap 1130 Sampling Head New Serial Number If the 1130 sampling head exterior box is replaced record the serial number of the replacement unit Swap 1135 sampling Head New Serial Number If the 1135 sampling head exterior box is replaced record the serial number of the replacement unit Remarks Block 5 Enter any additional comments or explanation regarding the quarterly maintenance activities in this block Please be concise and clear 5 Remarks AMNet SOP Site Report D Annual As Needed Maintenance 2011 05 Version 1 4 Appendix AMNet SOP Site Report D Annual As Needed Maintenance 2011 05 Version 1 4 For offce use only g Se National Atmospheric Deposition Program Atmospheric Mercury Network AMNet Site Report D 3 Date YYYY MM DD a ee e 4 Service Options Checklist Task Period impacted 1600 itime 24 h Comments Actions Doi 2 87 607 00660 Dog Gol cartridges changed New serial number 004 2 587 teflon vwahes repeced 0035 2 7 cuvette cleaned 2 87 cuvette repisced por 2 87 pumpserviced DCE 1130 Heated boot e prod pos 1130 case heater re2. AMNet SOP Site Report D Annual As Needed Maintenance 2011 05 Version 1 4 NADP AMNet Standard Operating Procedure Site Report D Annual As Needed Maintenance amp s National Atmospheric Deposition Program AMNet SOP Site Report D Annual As Needed Maintenance 2011 05 Version 1 4 For information about the National Atmospheric Deposition Program NADP contact NADP Program Office Illinois State Water Survey University of Illinois at Urbana Champaign 2204 Griffith Drive Champaign Illinois 61820 7495 URL http nadp isws illinois edu e mail nadp isws illinois edu phone 217 333 7871 AMNet SOP Site Report D Annual As Needed Maintenance 2011 05 Version 1 4 AIRMoN AMNet AMoN CAMD CAMNET CASTNET CVAFS DFU DQO GEM GOM Hg LPM LST MDE MDN MSDS NADP NIST NOAA NOS NIN OSHA PBM 5 PO QA QAAG QC QR RF RGM RPF SOP SQL TGM UHP U S EPA USGS Abbreviations Atmospheric Integrated Research Monitoring Network Atmospheric Mercury Network Ammonia Monitoring Network Clean Air Markets Division Canadian Atmospheric Mercury Network Clean Air Status and Trends Network Cold Vapor Atomic Fluorescence Spectroscopy Dry Filter Unit Data Quality Objectives Gaseous Elemental Mercury expressed in ng m Gaseous Oxidized Mercury expressed in pg m Mercury the element hydrargyrum Liters per Minute Local Standard Time Mercury Deposition Event Mercury Deposition Networ
3. g guide Additional information is available in the user manuals for the instrumentation the instrument Technical Notes and from the AMNet site liaison AMNet SOP Site Report D Annual As Needed Maintenance 2011 05 Version 1 4 Field Activities Table 1 Annual As Needed Equipment Maintenance Field Activities Reset or replace 2537 lamp Install new matched pair of gold cartridges Maintenance required Clean or replace 2537 Teflon valves Clean or replace cuvette Service or repair the 2537 pump New UV lamp 2537 pump brushes and diaphragm New matched pair of gold cartridges 2537 V2 and V3 valves Reagent grade water Laboratory grade methanol Clean non talc gloves Adjustable wrench Flat head screwdriver Phillips screwdriver Pliers Allen wrenches Consumables required Tools required Completing the Report Site Block 1 Enter the site name and the site ID Site names are chosen during the site selection and installation process The site ID is a four character code that is assigned by the NADP Program Office Operator Block 2 Enter the name and initials of the person that performed the maintenance and to whom questions should directed if there are questions about the report Three initials should be used if possible 2 Operator Initials AMNet SOP Site Report D Annual As Needed Maintenance 2011 05 Version 1 4 Date Block 3 Enter the date the maintenance was performed
4. gm Refer to Tekran Tech Note TN2537 004 Pump Brushes Replacement Procedure Model 2537 for the proper procedure The model 2537B cannot be serviced It should be replaced at the time of failure Refer to Tekran Tech Note TN2537 006 Pump Replacement Procedure Model 2537 for the proper procedure 1130 Heater Boot Replaced If the 1130 elutriator heater does not reach the proper operating temperature the heater may need to be replaced 1130 Case Heater Replaced If the 1130 case heater is at ambient temperature when in operation it needs to be replaced 1135 Case Heater Replaced If the 1135 case heater is at ambient temperature when in operation it needs to be replaced Heated sample line rinsed If high blanks are observed and other troubleshooting techniques have been exhausted the sample line may need to be cleaned To clean elevate one end of the line and flush the line with reagent grade water Follow with a methanol rinse and dry with zero air AMNet SOP Site Report D Annual As Needed Maintenance 2011 05 Version 1 4 Independent Survey Performed An independent site survey should be performed at least once every 2 years The AMNet Site Liaison will contact the site to schedule the site survey Swap 2537 New Serial Number If a second 2537 is available and is installed record the serial number of the replacement unit Verify that the scale factors are set properly Swap 2537 New Cal Amount pg Record the
5. k Material Safety and Data Sheets National Atmospheric Deposition Program National Institute of Standards and Technology National Oceanic and Atmospheric Administration Network Operations Subcommittee National Trends Network Office Safety and Health Administration Particle Bound Mercury less than 2 5 um in diameter expressed in pg m NADP Program Office Quality Assurance Quality Assurance Advisory Group Quality Control Quality Rating Response Factor Reactive Gaseous Mercury Regenerable Particulate Filter Standard Operating Procedure Structured Query Language Total Gaseous Mercury Ultra High Purity United States Environmental Protection Agency United States Geological Survey AMNet SOP Site Report D Annual As Needed Maintenance 2011 05 Version 1 4 Introduction Maintenance activities are required annually for each site in the NADP Atmospheric Mercury Network AMNet Near the end of each calendar year the operator should complete the maintenance activities described in this Standard Operating Procedure SOP document Site Report D Annual As Needed Maintenance Depending on conditions at the site e g relative humidity line voltage some maintenance activities may be required more frequently In such instances the maintenance activities should be completed on an as needed basis The activities described in this SOP exam the ambient mercury monitoring system and ensure that the instrument is free from ty
6. on If you are unable to adjust the lamp and achieve satisfactory operating condition replace the lamp according to the Tekran user manual and Tech Note TN 2537 13 Gold Cartridges Changed If either the SPAN or ambient GEM values deviate by more than 15 between the A and B cartridges the gold cartridges may need to be replaced Refer to Tekran 2537 user manual for proper gold cartridge replacement procedure Starting in 2009 Tekran identifies the gold cartridges with serial numbers Record the serial numbers of the new gold cartridge on the form 2537 Teflon Valves Cleaned If channel specific cartridge differences are observed valves V2 and V3 valves may need to be cleaned Remove valves and back flush with reagent grade water and methanol Dry replace and retest 2537 Teflon Valves Replaced If cleaning the 2537 Teflon valves does not correct the problem the valves may need to be replaced AMNet recommends annual replacement of the 2537 V2 and V3 valves When replacing the valves do not over tighten the PFA tubing nuts 2537 Cuvette Cleaned Refer to Section 10 10 Cuvette Cleaning of the Tekran 2537 user manual for the proper procedure 2537 Cuvette Replaced If cleaning the cuvette does not correct the problem the cuvette may need to be replaced Refer to the Tekran 2537 user manual for the proper procedure 2537 Pump Serviced The model 2537A pump can be serviced Servicing the pump includes replacing the brushes and diaphra
7. or the date the maintenance was started if maintenance extends multiple days Enter the date in the form YY YY MM DD where YYYY is the 4 digit year MM is the numeric designation for the month and DD is the day of the month 13 Date YYYY MM DD Service Options Checklist Block 4 Tasks listed at the top of the Report require confirmation that specific tasks were completed Tasks listed at the bottom of the Report require the reporting of measured values When a component is replaced the serial number of the new component should be recorded feel 4 Service Options Checklist Task Done Period Impacted local time 24 hr Comments ues Gee eee ee 25999 SSI een number on asore 00 A EE ee EE E eea O S 90999 oor asrnmosevews _ _ one 199099090909 O __ 10094099900 __ S om 49590999 _ _ on racasmewenses __ _ oi 99999000 _ a Comments Arion E 0 __ Swap 1130 Pump Module New Serial Number Swap 1130 Sampling Head New Serial D16 Number Swap 1135 Sampling Head New Serial D17 Number AMNet SOP Site Report D Annual As Needed Maintenance 2011 05 Version 1 4 2537 Lamp Adjusted or Changed If lamp voltage exceeds 12 5V the lamp indicator light on the 2537 front panel will illuminate Adjust lamp voltage according to Tekran user manual and Tech Note TN 2537 13 Lamp Driver Modification Kit Installati
8. pical mechanical and operational faults The SOP and its associated report identify the components that require maintenance the consumables required as part of the maintenance and the tools necessary to perform the maintenance A copy of the annual as needed maintenance report is included in the Appendix to this document The activities associated with the annual as needed maintenance require no in lab preparation The Report requires confirmation that specific tasks were completed and the reporting of specific measurements An X in the Done column indicates the task was performed The date and time of the period impacted by each task should be indicated in the report Users are encouraged to use the electronic version of the Report The completed report should be named using the naming scheme RSSSSYYYYMM xls where R is the report type e g A B C or D refer to title of the corresponding SOP SSSS is the 4 charater site ID YYYY is the 4 digit year and MM is the 2 digit designation for the month For example DVT99200912 xls is the annual as needed maintenance report that was completed in December 2009 for VT99 A copy of the report should be submitted to the NADP Program Office upon completion of the maintenance activities The information contained in the report and in all other reports is used when validating the data It is important that all reports are submitted in a timely manner This SOP is not intended to be a troubleshootin
9. piced D10 1135case heater repeced D11 Heated sample Ine rire ed D12 Independents urvey pe formed pig Swap 287A New Seria Number Did Swap 287A New Cal Hg amount 1061 Di5 Swap 1130 Pump Mod ule New Serial Number Dis Swap 1130 Sampling Head New Seris Number Swap 1135 Sampling Head New SerelNumber 5 Remarks Please upload the completed form to http nadp isws illinois edu upload amn Problems Contact Mark Olson at 608 335 4232 10
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