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DSeries Syringe Pumps Ethernet USB User Manual

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1. oo 66 Outlet Mounting plate SK Pressure transducer cap i dh Le x ab da M rr i z L q va _ B zie H I me a s Valve 2 T X Tee fitting 2 Air tubing ai Actuator to vale m 8 Check valve SE xc 1 4 Air 4 q U upet ey Inlet from H TH TH H TH eservoir 4 3 ACCESSORY DIGITAL 15 DIGITAL DIGITAL ANALOG INPUT GROUND OUTPUT NPUT A B S 0 10V 1234 1 2 3 415 6 7 8 1234 Control Panel Rear QooooooO oo0OO0 O 0O0 O0O0O0 O0 0 O0QO0O00O0 20 0 Wire pair con A B Pump Digital C D Pump Digital p 15 Wir z 15 Wir Wire Pair Output paires Wire Pair Output a Wires A1 A1 15 A1 5 15 A2 A2 15 A2 C6 115 B3 B3 115 B3 D7 115 B4 B4 15 B4 D8 15 Figure 5 5 Air valve installation for 1000D pump D Series Syringe Pumps Section 5 Continuous Flow Introduction Installation amp Operation TOP VIEW 000 000
2. 2 b D i N Po E B d i i P io E 1 i ES ETT 1 is 1 A IN o SS ih 1 A DUT ES a m j p UP e a BaTh FS exs D M Note b This valve system is for use with 65DM 100D 100DX 260D and 500D pumps This air valve will not work with 65D pumps Please consult the factory for options REF LU E amp A 61 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST ONG NO 0 122 227 SHEET 2 OF 2 REV E DATE 03122 PART NUMBER DESCRIPTION 232 4040 00 WINGNUT Lf 0 0 60 1243 529 TUBING 209 0161 1 8 NPT TO 1 8 TUBING MALE CONNECTOR SWAGELOK 69 1243 572 3 WAY VALVE 60 1243 569 TUBING 69 1245 574 AIR ACTUATOR 60 1243 570 TUBING 60 1243 544 TUBING 36 01 44 209 0161 43 1 8 FERRULE SPEEDBITE 72 73 8 209 0095 26 SOLENOID VALVE 2 EE BE HE 2 10 12 15 E ER 18 E 22 25 24 2
3. 60 0823 20 HIE 142 1104 00 FUSE DE 120 0013 00 ER F EDS 1243 234 LOE z 243 243 ER 65DM SYRINGE PUMP 3 J P 1243 ETAINER 65ML 9 963 ID X 813 OD 1243 UP RING 65D PRIMARY S 1248 182 FAR RING 65ML 243 882 PISTON BASE 65ML 1304 01 ROCKER SWITCH DPDT 4 AMP 69 1243 948 FRONT PANE ABEL 65DM DIO A wo no NOTE For current prices and quotations on parts contact Isco Service Department 2 This list is subject to change without notice A 47 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST SHEET 13 OF 13 TELEDYNE ISCO INC REV DESCRIPTION ED PREAMP ASSY CAP SEAL PLUG FW 1 4 20 X 1 4 CUP POINT NOTE For current prices and quotations on parts contact Isco Service Department 2 This list is subject to change without notice A 48 D Series Syringe Pumps Appendix A Replacement Parts A 1 9 Power Circuit Board 141 139 140 GOOD POWER CIRCUIT BOARD REPLACEMENT PARTS 60 1242 348 136
4. 8 26 8 4 Get Status String GG Command 8 26 8 5 Get All Status String G amp Command 8 27 8 6 Get all status strings from four pump operation G amp 2 Command 8 28 8 7 Gradient Download Commands Single pump flow gradient 8 29 8 8 Gradient Download Commands Two pump flow gradient 8 30 8 9 Gradient Upload Commands Single pump flow gradient 8 31 8 10 Gradient Upload Commands Two pump flow gradient 8 32 8 11 Upload Commands Single pump pressure programming 8 33 8 12 Range Serial Commands sse 8 33 9 1 500EHIPx fan filter a tn eee eate peer ex ae CURE RUE E em 9 4 9 2 Accessing the diagnostic menu 9 6 9 3 Analog Input diagnostic screen 9 6 9 4 Optical sensor interrupted by flag bottom sensor shown rear tower cover plate re moved c e ek Gaia s LEONE NER EPA CREME ENSURE 9 7 9 5 Serial connection to a computer 9 8 9 6 Controller case top screws 2 of 4 shown 9 10 9 7 Pump case top screws 2 45 9 10 9 8 Gear train lubrication and motor drive service 9 12 9 9
5. ro System pressure of multi pump pair AB Total volume delivered by multi pump pair AB BAR kPa PSI See NOTE 1 Liters System flow rate of multi pump pair CD System pressure of multi pump pair CD ml min ml hr ul min ul hr See NOTE 2 ATM BAR kPa PSI See NOTE 1 Total volume delivered by multi pump pair CD Liters Analog voltage input on Analog Input 1 of the accessory connector Vo Analog voltage input on Analog Input 2 of the accessory connector Vo Analog voltage input on Analog Input 3 of the accessory connector Vo Analog voltage input on Analog Input 4 of the accessory connector Vo Volume at which Pump A will automatical y switch to refill mode if AUTO REFILL A is ON Volume at which Pump B will automatical y switch to refill mode if AUTO REFILL B is ON Volume at which Pump C will automatical Volume at which Pump D will automatically switch to refill mode if AUTO REFILL D is ON y switch to refill mode if AUTO REFILL C is ON illiliters Volume that Pump A will be refill to if AUTO FILL TO A is ON illiliters Volume that Pump B will be refill to if AUTO FILL TO B is ON illiliters 7 9 D Series Syringe Pumps Section 7 Modbus Configuration Register Table 7 6 Holding Registers Continued
6. DIGITAL INPUT Outlet Pressure transducer 2 Cylinder ek Bea head 2 5 Valve 2 tz Tee fitting 2 Air tubing to valve x Actuator Te Check valve p Inlet from reservoir Wire pair conversion table for A B Pump Pair and C D Pump Pair Control Panel Rear Figure 5 6 Air valve installation for 65D pump 5 12 A B Pump Digital C D Pump Digital Wire Pair Output Wires Wire Pair Output 775 Wires A2 A2 15 A2 C6 15 B3 B3 15 B3 D7 15 B4 B4 15 B4 D8 15 D Series Syringe Pumps Section 5 Continuous Flow Introduction Installation amp Operation 5 4 Continuous Flow Electric valves which provide the best positive valve closure are Electric Valves most commonly used in liquefied gas applications Electric valves require the pump controller to be equipped with the valve driver board The max flow rate for the E1000D dual system will t
7. III DI II II II m m or Eet pt iS OD BR Co row NOTE For current prices and quotations on parts contact Teledyne Isco Service Department 2 This list is subject to change without notice A 3 D Series Syringe Pumps Appendix A Replacement Parts A 1 2 30D Pump A 4 D Series Syringe Pumps Appendix A Replacement Parts 601262101 REPLACEMENT PARTS LIST SHEET 2 OF 3 TELEDYNE ISCO PART m 20 DESCRIPTION 1200 1200 141400 15000 0103290 113370 14299 220622 901610 901640 901640 23361360 HOKE POWER FILTER KT D SUB 9 CONT RK FLSF RVS 24V KB RG CYL 3541D1 00D RG CYL 381D 880D KB RG THR 351047200 INDIVIDUAL ORDER QTY 2 O RING 1 6081D 139 CONN MALE 12 HOSE GLAND F250C 30VM LR F250C 30VM R WV 397 ID 6912444 IVERSAL SENSOR HARNESS 4101304 RKR DPDT CSA 4A KB 411461264 FU 1 6A 250 SB 234 VOLT 41146121 FU 3 2A 250 SB 3AB 100 VOLT amp 117 VOLT 460010119 XDCR PRESS 0 30 000 PSI 60124329 DELRIN PLUG 243348 SLIDE THRUST BEARING 243610 GEAR TRAIN KEY 243816 CYLINDER CAP 65ML 244184 MOTOR ASSEMBLY 01244236 LUBE WHEEL ASSEMBLY 01244323 HARN MN PMP ENCD KB GEAR TRAIN SOAK PAD 30 30D CBA REPLACEMENT KIT XFRMR ASSY 30D 68 WORM GEAR MOD 6 BALL NUT ASSY 21 BA
8. i 9 12 3 Replacement Without Installation Tool 9 12 4 Pump Bearings 30D and 65DM Only D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing 1 Insert tool into ball screw so that the slot on ball screw and tool are lined up then lock with locking pin Rotate the ball screw until the broken halves of shear key are realigned Figure 9 11 Remove the broken shear key halves by gripping them with pliers or vise grips and pulling them out Insert the new shear key into the slot with the gap facing away from the shaft as shown in Figure 9 11 Push the shear key about half way into the worm gear Do not push it all the way in Remove the tool and proceed to the final steps in Section 9 12 5 Follow steps 1 through 5 in section 9 12 1 Insert the cotter pin into the ball screw and screw the cas tle nut onto ball screw with the slot on castle nut outward as shown in Figure 9 11 Use a 4 wrench on the castle nut and rotate the ball screw clockwise until the broken halves of the shear key are realigned Figure 9 11 above CAUTION Never use tools on the ball screw Doing so will render it inop erable and beyond repair 4 5 Remove the castle nut and cotter pin Remove the broken shear key halves by gripping them with pliers or vise grips and pulling them out Insert the new shear key into the slot with the gap facing away
9. 5 17 6 1 Modifier Addition Kit for Two Pumps part 68 1247 079 6 3 6 2 Modifier Addition Components for Continuous Flow System 6 4 7 1 Modbus TCP IP Configuration Options 7 2 7 2 Modbus RTU Configuration 7 2 7 3 Supported Modbus Function 7 3 7 4 Exception Responses 7 3 7 6 8 1 8 2 8 3 8 4 8 5 8 7 9 1 9 3 9 4 B 1 B 2 B 3 B 4 D Series Syringe Pumps Table of Contents i ers e aee Be ep ed a ee aate eA 7 4 Holding Registers eed ep Aa aan nad we ae ed 7 7 External control connector serial pin connections 8 2 USB Interface Pin Connections 8 3 Example of BASIC program to demonstrate conversion of pump commands to DASNET frames 8 8 Example of C program to demonstrate conversion of pump commands to DASNET frames 8 9 Example of a Visual C program to demonstrate conversion of pump commands to DASNET 8 10 Serial Commands onee eee hh 8 20 Error Messages sens wea y dors quee x ERE ea 8 34 Maintenance Kit 9 3 Maintenance Kit Pa
10. B 10 B 5 amp N0 Check Valve u a pes e uA DURCH B 11 B 5 5 To R n or Stop uo 2 ae EE nee the Ree oues B 12 B 5 6 Tips for Running Continuous Flow B 12 B 6 Replacement Parts List eh 14 B 6 1 30D P mp 4 22 Ee en IDEE B 14 B 6 2 30D Air Valve u be treiner nenn EV Es B 17 B 6 3 30D Electric Air Valve B 19 List of Figures 1 1 260D flow rate range Der edo edere a Eee 1 11 1 2 500D flow rate range 1 11 1 3 500 HPx flow rate range 1 12 D Series Syringe Pumps Table of Contents xviii 1 4 1000D flow rate range 1 12 1 5 Pump controller key 1 14 1 6 Pump controller rear panel connectors 1 16 1 7 Pump rear panel connectors 1 17 1 8 Pump front panel controls 1 18 1 9 Syringe pump cylinder cap Attach to pressure transducer connector on back of Pump u a an Be Tea E VER Ee OE Pu 1 20 1 10 Connecting the pump and 1 21 1211 Status Sereen vn nrden veters ee na TRE RE ee reet 1 21 1 12 Menu 1 aches este es sgh BEAR an Bann gate wee RR 1 22 1 13 Three pu
11. REPLACEMENT PARTS LIST SHEET 3 OF 3 TELEDYNE ISCO a ji PART NUMER DESCRIPTION 29 601244221 PSTN ASSY 500 ML NITRONIC 29 601244319 PSTN ASSY 500 ML HASTELLOY 30 601244323 HARN MN PMP ENCD 3l 601244458 TERM BLK INDUCTOR DUAL MOTOR 32 601244459 TERM STRIP ASSY 13 14 2 MOTOR 33 601244460 TERM STRIP ASSY L1 12 2 MOTOR 34 60124446 WIRING ASSY XFRMR DUAL MOTOR 35 601241112 REPLACEMENT KIT POWER CBA 500HPX 36 601244463 ASSY TWO MOTOR DUAL MOTOR PUMP 31 601244465 HARN MOT BRAKE 38 601244466 ASSY FAN COVER BOTTOM 39 601248099 JKT CLG ASSY 500ML KB 40 601248116 B NUT ASSY KB 4 601248111 B SCR ASSY 4 601244469 PREAMP ASSY CYL CAP NITRONIC 4 601244468 PREAMP ASSY CYL CAP HASTELLOY 43 60225413 OTOR BRUSHES PKG 2 44 691243 11 FRONT LABEL 45 69124343 WORM GEAR 46 691243455 CYL CAP SEAL 500D 4 691243560 SPUR GEAR 50T 20P 48 691243563 EXTENDED WORM GEAR 49 691243805 COMBINATION GEAR 50 691243806 GR PIN HLCL DX NOTE For current prices and quotations on parts contact Teledyne Isco Service Department 2 This list is subject to change without notice D Series Syringe Pumps Appendix A Replacement Parts A 1 6 100DM DX and 260D Pumps 260D Z 260HP ANLA Se N FA A 19 D Series Syringe Pumps Appendix A Replacement Parts ITEM NO REPLACEMENT PARTS LIST DWG NO 60 1242 321 SHEET 2 OF 3
12. Initial B Range 00 00 100 0 Gradient Total Flow Rate Units milliliters minute Range 000 0000 Maximum Flow Rate Step Number 01 File 01 99 Step Numbers 02 through 99 LGUL F XX S9 xx IB xx XX FB xx xx D XXXX X srl Gradient Duration Range 0000 1 9999 0 minutes Final B Range 00 00 100 0 Initial B Range 00 00 100 0 Step Number 02 99 File 01 99 Figure 8 10 Gradient Upload Commands Two pump flow gradient 8 32 D Series Syringe Pumps Section 8 Serial Interface LGUL F xxX S XX l XXXXX F xXXXXX D XXXX X Pressure Duration Range 0000 1 9999 0 minutes Final Pressure Range 00010 Maximum Units psi Initial Pressure Range 00010 Maximum Units psi Step Number 01 99 L File 01 99 Figure 8 11 Upload Commands Single pump pressure programming 8 8 4 Range Command The RANGE command provides scaling information for the system parameters For example 6ROO6RANGEA34 may return a string similar to the one shown in Figure 8 12 RO2CP 10000 F 2500000 R 30 00000 V 102 9600 40 Il Js Checksum Max Volume 102 96 Units milliliters Max Refill Rate 30 0 milliliters minute Max Flow Rate 25 milliliters minute Maximum Pressure 10 000 psi Figure 8 12 Range Seria
13. 65HP PUMP REPLACEMENT PARTS LIST MODEL 65D A 26 D Series Syringe Pumps Appendix A Replacement Parts oa c a nm ro lt W a o EX zo Lua uc So Lu lt u ES ao ES a A 27 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST MODEL 65D 65HP PUMP A 28 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST MODEL 65D 65HP PUMP D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST MODEL 65D 65HP PUMP D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST MODEL 65D 65HP PUMP D Series Syringe Pumps Appendix A Replacement Parts 601242498 REPLACEMENT PARTS LIST SHEET 11 OF 13 TELEDYNE ISCO PART NUMBER DESCRIPTION 201 1337 00 BEARING VERIFY PARTS WITH SCO SERVICE DEPT 2 201 0329 00 BEARING CYLINDER 3 69 1243 563 EXTENDED WORM GEAR 4 150 0006 0 BRAKE FAILSAFE REVERSE 24V 25 BORE 5 60 1243 610 GEAR TRAIN KEY 6 69 1243 560 SPUR GEAR 1 69 1243 80 COM
14. Absolute maximum pressure for Pump A ATM BAR kPa PSI See NOTE 1 Absolute maximum flow rate for Pump A ml min ml hr ul min ul hr See NOTE 2 Absolute maximum refill rate for Pump A ml min ml hr ul min ul hr See NOTE 2 Maximum volume for Pump A milliliters 7 10 Absolute maximum pressure for Pump B ATM BAR kPa PSI See NOTE 1 D Series Syringe Pumps Section 7 Modbus Configuration Table 7 6 Holding Registers Continued Register Read Write Type of Registers Description Absolute maximum flow rate for Pump B ml hr ul min ul hr See NOTE 2 Absolute maximum refill rate for Pump B ml min ml hr ul min ul hr See NOTE 2 Maximum volume for Pump B milliliters Absolute maximum pressure for Pump C BAR kPa PSI See NOTE 1 Absolute maximum flow rate for Pump C ml min ml hr ul min ul hr See NOTE 2 Absolute maximum refill rate for Pump C ml min ml hr ul min ul hr See NOTE 2 Maximum volume for Pump C milliliters Absolute maximum pressure for Pump D BAR kPa PSI See NOTE 1 Absolute maximum flow rate for Pump D ml min ml hr ul min ul hr See NOTE 2 Absolute maximum refill rate for Pump D ml min ml hr ul min ul hr See NOTE 2 Maximum volume for Pump D milliliters PUMP TYPE A PUMP TYPE B PUMP TYPE C PU
15. Mounting plate o et ustomer reservoir os 15 15 Lam 15 A UIT 1 e e ius Air supply pdt man mu ur ACCESSORY DIGITAL DIGITAL ANALOG 4 Panhead screws 4 GROUND OUTPUT INPUT B D 0 10V 12 3 456178 1234 Wire pair conversion table for Pump Pair C D Pump Pair A B Pump Digital C D Pump Digital Wire Pair Output LES Wire Pair Output newe A1 Al 15 Al C5 15 A2 A2 15 A2 C6 15 B3 B3 15 B3 D7 15 B4 B4 15 B4 D8 15 Figure 5 4 Air valve installation for 500HPx pumps 5 10 D Series Syringe Pumps Section 5 Continuous Flow Introduction Installation amp Operation
16. Disconnect the power cord and pressure transducer cables and plumbing connections from the pump Wrap the transducer cable around the cylinder cap Using a Allen wrench loosen the lock screw located on the front of the cylinder mounting block about two turns Unscrew the cylinder using either a strap wrench or the clamp and wrench in the Teledyne Isco wrench package 60 1247 130 for 65D and 65DM 60 1247 067 for 100DM 100DX and 260D 68 1247 068 for 500D 60 1247 145 for 500HPx 60 1247 093 for 1000D which will not mar the cylinder s outer surface D Se ries Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing 9 9 1 Piston Seal 9 14 Excludes 30D Accessing the piston seal 9 9 2 Piston Seal Break In Aqueous seals only 5 Once the cylinder has been unscrewed lift it straight up and offthe piston and the push tube N CAUTION Do not tilt the cylinder while removing it Seal damage can result Sometimes dirt or other solids on the seal can cause leakage Removing and cleaning the seal may stop the leak and a new seal may not have to be used However if you remove and inspect the seal and it does not have any obvious crease or you did not find any foreign material on the seal then the seal must be replaced Check the wear ring See Section 9 10 M Note DO NOT use abrasives while cleaning the piston and piston seal area Scratches caused by the use of such abrasives w
17. Attach the 10 2cm pre bent SST tubing from the check valve inlet to the two way valve outlet Connect your tubing from the tee outlet to your equipment Tighten all fittings Tubing for connection to user equipment is not provided Optional 1 16 and 1 8 OD SST tubing may be ordered from Teledyne Isco Table 6 1 contains modifier addition kit components for con necting the outlets of two pumps using a Valco 1 16 tee as a mixer D Series Syringe Pumps Section 6 Table 6 1 Modifier Addition Kit for Two Pumps part 68 1247 079 Modifier Addition Description Part Number Description Part Number Description Part Number Tee union fitting 209 0169 47 18 nut 4 209 0169 27 Check valve cartridge 209 0161 80 OD x 12cm 60 1243 540 x 1 5 60 1243 539 Check valve mixer 60 1243 691 tubing tubing tubing 146 Ferrule 209 0169 34 Valve spacer 2 60 1243 659 Appropriate screws and washers also included 146 Gland nut 209 0169 35 2 way valve 18 209 0098 05 OD 2 Standard check 60 2253 209 Tubing valve inlet 60 1243 658 valve housing 2 Check valve car 60 3864 010 Tubing check valve 60 1243 644 tridge 2 Single check 60 1243 516 Reduction unio
18. of Registers Description Volume that Pump C will be refill to if AUTO FILLTO C is ON milliliters Volume that Pump D will be refill to if AUTO FILL TO D is ON milliliters Percentage of total pump volume that the refilling pump of multi pump pair AB will refill to Percentage of total pump volume that the delivering pump of multi pump pair AB will deliver to Percentage of total pump volume that the refilling pump of multi pump pair CD will refill to Percentage of total pump volume that the delivering pump of multi pump pair CD will deliver to LL MARK A VALID ENTRYS 10 20 30 40 50 60 70 80 90 LL MARK B VALID ENTRYS 10 20 30 40 50 60 70 80 90 LL MARK C POOR FILL MARK D VALID ENTRYS 10 20 30 40 50 60 70 80 90 VALID ENTRYS 10 20 30 40 50 60 70 80 90 Volume being dispensed by Pump A in Dis pense mode milliliters Volume being dispensed by Pump B in Dis pense mode illiliters Volume being dispensed by Pump C in Dis pense mode illiliters Volume being dispensed by Pump D in Dis pense mode illiliters Full scale input range voltage for External mode Volts MIN MOD PRESS Minimum modifier pump pressure ATM BAR kPa PSI See NOTE 1 Value of B for Modifier addition mode C for Continuous Modifier addition mode B FOR MODIFIER OR C FOR CONTIN 000 MODIFIER
19. 4N 64 D F250C 30VM 64 C 30VM 640 F250C 60K PS 6980 R REPL 100 016981 MALE 1 8 TBG 263156 BLOCH PASS VATE 263141 E Ul 263148 ET GASKET SEE E OUTLET AIR VLV N A 263155 E 3 1 CNG 263160 LD GASKET 263171 ENOID MANIFOLD PAINTE 263113 DY PASSIVATED 244496 L MODIFICATION 01263161 LASTIC 59000002 ENCER PLASTIC gt ADP gt wo pro II D PI JRO PO CO oo se OD 1 NOTE For current prices and quotations on parts contact Teledyne sco Service Department This list is subject to change without notice B 18 D Series Syringe Pumps Appendix B Continuous Flow Introduction Installation and Operation for 30D B 6 3 30D Electric Air Valve B 19 D Series Syringe Pumps Appendix B Continuous Flow Introduction Installation and Operation for 30D REPLACEMENT PARTS LIST SHEET 2 OF 2 TELEDYNE ISCO REV PART NUMBER DESCRIPTION 09016402 09016403 01244312 244494 263115 26311 26314 263113 3933010 393306 3934002 03934012 91244348 01263142 09016980 9016981 23050402 1263141 1263148 9016405 D F250C 30VM 50C 30V IC VALVE BODY ASSY VLV MANIFOL
20. The wear ring prevents the piston from direct metal to metal contact with the cylinder wall and should therefore extend at least 0 010 beyond the circumference of the piston lip Check the bottom of the wear ring which rests on the piston lip for extrusion or any unevenness If there is an indentation of 0 0010 or more marking the outline of the piston lip then you should replace the wear ring However if the surface is smooth the wear ring does not need replacing After cylinder seal maintenance or during modifier liquid solvent change the pump cylinder should be flushed to remove possible residue The way in which the cylinder is flushed will depend on your pumping system and whether you are pumping a liquefied gas such as see Section 9 11 1 or a liquid modifier such as methanol see Section 9 11 2 This procedure is used when changing from one gaseous solvent to another 1 Close the valve on the fluid supply tank so that no solvent is supplied to the system 2 Turn the controller ON 3 Run the pump until the cylinder is empty If there was any pressure in the system wait until all the pressure bleeds off 4 Change the solvent tank 5 Close the pump outlet valve 6 Open the valve on the tank to repressurize the system 9 17 D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing 9 11 2 Liquid Solvent Changeover and Flushing To clean the cylinder 9 12
21. flush serial buffer to start again comm close dasnet conversion utility conv_das char in char out unsigned sum char c_ptr c_ptr out point to output out unitnum 0x30 put id first out R add to output if stremp in R if just R add space to string outt out 0x00 else add char to string sprintf out 63 3X 96s strlen in in for sum 0 c ptr c_ptr add all chars together sum c ptr sum 0x100 sum amp OxOFF get check sum sprintf c_ptr 2 2X sum insert into string Note Polling is part of the DASNET definition but is not required and is not shown in this example This code was written in TurboC version 4 5 TurboC is a compiler created by Borland Software Corp Austin TX It is no longer actively sold by Borland International 8 9 D Series Syringe Pumps Section 8 Serial Interface Table 8 5 Example ofa Visual C program to demonstrate conversion ofpump commands to DASNET frames visual C version 10 0 Dasnet cpp Defines the entry point for the console application C C example of DASNET serial control include stdafx h include lt windows h gt include lt stdio h gt include lt conio h gt include lt string h gt void commOpen int port long speed void conv_das char char void dgets char void dputs char void comm_putc
22. 3 12 1 Wire connections 3 18 To specify the volume of the batch delivered press VOLUME C enter the desired volume using the number keys and press ENTER To dispense the batch press RUN The sequence runs once then stops To repeat the sequence press RUN again M Note When the system is in Dispense Mode all gradient modes constant pressure mode and auto refill as well as serial con trol are unavailable until Dispense Mode is turned off The pump can be externally controlled for pressure or flow rate operation with an analog voltage or through the serial interface The serial interface allows you to control the pump operation from an IBM PC or compatible computer that has an RS 232 C serial output The serial interface accepts English command words from the computer like constant pressure refill etc For more information see Section 8 Serial Interface The syringe pump can be controlled externally by analog voltage in either constant flow or constant pressure mode The input range is 0 11 5 volts for all pumps with a resolution of 5000 increments per volt M Note The input range for the 4 20ma option is set to 4 20ma Two wires are required for analog control The analog common or ground wire should be connected to the GND terminal under ANALOG INPUT of the ACCESSORY connector on the con troller rear panel The analog control or input wire should be con nected to terminal 1 under ANALOG INPUT If
23. 3 23 Section 4 Gradient Pumping for Pressure Flow and Concentration Modes 4 1 Introd ction ansehen ae ass Bess eee ade 4 1 4 2 Connecting the 4 2 4 2 1 Inlet Connections setas viera eneen een 4 4 4 2 2 Outlet Connections enen eee 4 5 4 2 3 Dual Gradient System Connections 4 6 4 3 4 4 4 5 4 6 D Series Syringe Pumps Table of Contents Single Pump Gradient Programming 4 8 Dual Pump Concentration Gradient Programming 4 10 Review Revise amp Hold 4 12 Program Conclusion 4 12 Section 5 Continuous Flow Introduction Installation amp Operation 5 1 5 2 5 3 5 4 5 5 5 6 Introduction si sa meer andere ea tan Be 5 1 Continuous Flow Check Valves 5 1 5 2 1 Check Valve Technical 5 2 5 2 2 Dual Check Valve Installation 5 2 5 2 3 Inlet T bing x une ates Re ee quei ais 5 3 Continuous Flow Air 1 5 7 5 3 1 Dual Air Valve Installation 5 7 Continuous Flow Electric 1 5 13 5 4 1 Technical Speci
24. 9600 Baud rate should match controller setting refer to Section 8 2 Data bits 8 Parity None Stop bits 1 Flow control None Run the test again The screen should display Rec whatever is typed from PC Sent Serial Test Press any key to exit Anything typed on the computer keyboard should appear in the top line on the controller display The computer should contin ually display the serial test shown in the second line of the con troller display For some maintenance procedures the case top of the controller or the pump may need to be removed Because interior access is easier with the controller this method of troubleshooting should be used whenever possible 4 NDANGER RISK OF ELECTRIC SHOCK DISCONNECT THE ELECTRIC POWER BEFORE SERVICING ONLY TRAINED SERVICE PERSONNEL MAY REMOVE THE CASE TOP 4 NDANGER RISQUE DE CHOC ELECTRIQUE COUPER L ALIMENTATION AVANT LA R PARATION L USAGER NE DOIT PAS D MONTER L INSTRUMENT OU D RANGER LE M CANISME DEDANS ADRESSER LA REPARATION SEULEMENT AUX TECHNICIENS COMP TENTS Troubleshooting for a number of issues can be done on the con troller main circuit board Remove the four screws holding the case top in place two screws on each side Lift the cover straight up and off D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing j Zen a Figure 9 6 Controller case top screws 2 of 4 shown
25. Depending upon when your pump was manufactured the protective conduit may be directly fastened to the pump or retained with mounting tabs and cable ties If the conduit is fastened directly to the case then it must be removed and the plastic mounting tabs included with the limit sensor assembly package should be installed using the existing screws and screw holes To install the mounting a Remove the screws and the conduit tabs b Then use the same screws and holes to install the mounts Be sure the tab portion of the mount is facing away from the sensors as shown in Figure 9 39 the screw aperture is closest to the sensors If your pump already has the plastic tabs installed cut and discard the plastic cable ties which run through the tabs and hold the conduit 6 Remove the four screws holding the limit sensors and unplug the cable from the power circuit board The replacement limit sensor assembly includes both the upper and lower sensor and the plug M Note There are several additional cable ties along the path from the limit sensors to the power board Two are reusable twist ties and usually 3 others need to be cut to free the limit sensor wires These cable ties must be replaced to prevent the wires from entangling with the worm gear 7 Install the new limit sensor harness and secure the protec tive conduit by running the cable ties through the mounts and tightening Then cut the excess cable tie and discar
26. Pressure transducer v A OEN retainer Transducer seal Cylinder cap seal Piston seal A y N Wear ring Wiper seal Figure 2 18 Inside the pump cylinder wetted materials The standard seals for each pump model satisfy the require ments of most applications including those that use carbon dioxide such as SFE However certain solvents and or conditions require special cylinder seals to facilitate the application Table 2 7 on the following page is provided to help you select the correct seal for your pump and application requirements 2 19 D Series Syringe Pumps Section 2 Fluid System Connections and Accessories Table 2 7 Seal Selection Chart Seal Type Max Seal 65D DM 100DX DM 260D 500D Pressure Description 500HPX GENERAL SFE Black PTFE 202 9096 08 202 9090 75 202 9091 06 202 9091 56 upper seal CARBON graphite filled 202 9990 25 DIOXIDE lower seal 202 9990 23 This is our standard seal It is good for most applications particularly those using organic solvents such as LC SFC and SFE HIGH 0 689 5 Black PTFE graphite fiber 202 9090 76 202 9091 09 202 9093 56 upper seal TEMPERATURE bar reinforced high temperature 202 9990 28 compound lower seal 202 9990 27 This seal is best suited for applications which require temperatures between 50 C and 100 C Its chemical compatibility is similar to that of the general seal LOW 0 13
27. SPRING UP XS PISTON SEAL Ce RETAINER PISTON SEAL 3 SPRING DOWN I i CYLINDER GS RING SA PISTON NA PISTON Each Sipe ve fact Sor q WIPER 39 WIPER SEAL v SEAL SPRING DOWN Si SPRING DOWN zA eo RETAINER ETANER 2 SI RETAINING RETAINING x RING N CD RING N C2 PUSH TUBE ROD A DWG 60 1242 325 REV A PUSH TUBE ROD AN V7 N m 7 FIGURE FIGURE FIGURE THE 1000 amp 2600 PUMPS DO NOT HAVE THESE PARTS BACK UP RING ONLY ON 65D Model 1000D Refer to Replacement Parts Listing 60 1242 347 Figure 9 9 Break in procedure for aqueous seals Drawing does not apply to the 30D M Note For the 30D pump see the 30D Syringe Pump Seal Replace ment instruction sheet included with the seal or piston assem bly kit 9 9 3 Allother piston seals 1 Access the piston seal as previously described 2 Orient a new seal so that the spring in the seal is facing up 3 Slide the seal onto the piston 4 Replace the piston seal retainer 9 9 4 Wiper Seal Although the wiper seal does not normally have to be changed Excludes 30D periodic cleaning is advisable Removal and cleaning 1 Access the cylinder as described previously 2 Locate the piston Figure 9 9 9 15 D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing 9 16 Reinstalling the wiper 3 With the exception
28. Teledyne Isco reserves the right to refuse shipment if no decontamination assurance has been provided prior to shipment Failure to decontaminate a pump may result in legal action taken by state or federal authorities 9 2 M Note It is very important that the shipment be well packed and fully insured Damage claims must be settled between you and the carrier This can delay repair and return of the unit to you D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing 9 2 Maintenance Kits Maintenance kits are available for all pump models for use in many maintenance and servicing tasks Table 9 1 summarizes major kit components Table 9 2 contains part numbers for each kit Table 9 1 Maintenance Kit Contents Piston amp Wiper Seals Replace seals annually at a minimum Replace more often for appli cations involving heavy use or harsh abrasive substances Cylinder Cap Seal Replace when removing installing cap for servicing or periodically if cap is removed more often e g for spooning in highly viscous sub stances Piston seal Wiper seal Control Panel Label Depending on use the most frequently pressed keypad buttons may eventually wear out Port Plug Qt Tubing Connectors en C Fuses Shear Key w Installation Tool ze If the pump motor fails to stop in the event of an overpressure situa Shear key tion the shear key may require replacemen
29. Temperature changes can cause pressure fluctuations For available temperature control options contact Teledyne Isco For correct overpressure response shutdown must be set to ON under PUMP LIMIT options Enter the same refill rate separately for pumps A B C and D The refill rate should always be as high as possible to allow time for refill and repressurization before the next switchover D Series Syringe Pumps Section 6 Modifier Addition 6 1 Overview 6 1 1 Installing the Kit Pumping systems using a modifier usually a solvent may have different configurations depending on the application including Two separate pumps delivering a mixture of super critical fluid and modifier to one or more user provided extractors e A dual pump system in constant pressure mode pumping supercritical fluid with a third pump deliv ering the modifier M Note This is not available for the 30D pump Please contact the factory for details In both configurations the purpose is to dispense a mixture with a programmable v v ratio Modifier concentrations of up to 100 can be programmed Both fluids pass through one way check valves before they meet and are blended in a static mixing tee refer to Figures 6 1 and 6 2 NDANGER Risk of injury The pressure produced could be up to 700 bar Please utilize appropriate tubing and connections as noted M Note The configurations described in this section apply to 65DM 100D
30. nication is provided in Section 7 Modbus Configuration 3 9 D Series Syringe Pumps Section 3 Basic Programming and Operation 3 8 Front Panel Keys 3 10 3 8 1 CONST PRESS and CONST FLOW 3 8 2 PRGM GRAD 3 8 3 HOLD 3 8 4 RECALL 3 8 5 STORE 3 8 6 REFILL 3 8 7 LIMITS In addition to the menu options certain functions and modes are selectable from the front panel keyboard These keys place the system in constant pressure mode or con stant flow mode respectively Information for these operating modes can be found in Section 3 10 This key is used to place the pump system in gradient mode For complete information about gradient programming refer to Section 4 Gradient Pumping for Pressure Flow and Concen tration Modes The HOLD key is used while a gradient is running When HOLD is pressed the program clock freezes and current gradient parameters are maintained To continue the gradient press HOLD or RUN The RECALL key can only be used when the pump s are stopped or when in HOLD mode The RECALL key is used to recall a pre viously programmed gradient When you select this option the controller automatically loads the gradient and switches the pump to program gradient mode 1 Press RECALL and use the number keys to enter the num ber name ofthe gradient you wish to recall Press ENTER 2 If you enter a number of a gradient that does not exist the controller briefly displays the message FILE NUM
31. 500D 68 1247 082 to 65DM 100DM DX 260D 68 1247 078 assembly 60 1247 181 valve 68 1247 126 spacer screws N DANGER RISK OF INJURY THIS EQUIPMENT PRODUCES HAZARDOUS PRESSURES PLEASE UTILIZE APPROPRIATE TUBING AND CONNECTIONS AS NOTED IN THE MANUAL stainless steel tubin screws valve stainless steel tubing L to system reducing union 65DM 100DM DX 260D Figure 2 8 Outlet valve package connection 2 3 3 CO Cylinder For North American gas tank connections the optional con Connection Package nection package is available from Teledyne Isco Table 2 4 CO Cylinder Connection Package 68 1247 043 Part Number Description 209 0161 63 Reducing connector lg to Var 209 0161 16 Va x 2 nipple 209 0161 15 0 830 14 nut 209 0161 17 PTFE washer 209 0161 64 In line filter assembly 2 10 D Series Syringe Pumps Section 2 Fluid System Connections and Accessories PTFE Inline filter Reducing washer Nipple Nut frit assembly connector To coz m To Valve Supply il Figure 2 9 package installation 2 3 4 In Line Filter Package The optional in line filter package should be used when it is important to filter flow exiting the pump This package contains a 0 5 pm filter and 6 tubing This filter is not for use at pressures above 6 000 psi 414 bar Table 2 5 Optional in line
32. 625 In this example the analog voltage range would be 0 0 6 25 volts Pressure If MAX PRESS is set at 510 2 ATM in the LIMITS menu and the desired scale factor is 2 0 volts per 100 ATM do the fol lowing to determine the analog voltage range 2 510 2 x 5 10 204 In this example the analog voltage range would be 0 0 10 204 volts If the controller is equipped with 4 20ma input then the low sig nal is 4ma stop and high signal is 20ma run First select the desired operating mode by pressing CONST PRESS or CONST FLOW D Series Syringe Pumps Section 3 Basic Programming and Operation IU EXE BHO PRESS FLOW n gt CP or CF and selected EXTERNAL pump are displayed j On Off MORE Enter Vmax value Figure 3 13 Button sequence for external control setup 3 13 Remote RUN STOP 3 13 1 Wire Connections The D series syringe pump RUN STOP function can be exter nally controlled by a switch contact closure or TTL input The input voltage is 5 volts and is internally pulled high RUN The input is level sensitive must remain high for RUN or low for STOP and must be high for normal operation of serial RS 232 control To enable the remote RUN STOP feature press MENU gt MORE gt A EXTERNAL 3 DIGITAL A ON Then press RUN or force the RUN STOP pin low to enable the pump Thereafter the RUN STOP pin will control operation first press RUN or force t
33. 9 25 9 13 2 HPx Motor Brush Replacement 9 26 9 14 Calibrations twe sema dw RR RR a a RR Rer 9 35 9 14 1 Pressure Transducer Calibration 9 35 9 14 2 A D Circuit amp 9 35 D Series Syringe Pumps Table of Contents 9 14 3 Limit Sensor Adjustment 9 35 9 14 4 Limit Sensor Calibration Excludes 30D 2 2 2 2a oe Se ae 9 39 9 14 5 30D Limit Sensor Calibration 9 40 9 14 6 Electric Valve Motor Calibration 9 41 Appendix A Replacement Parts 1 Replacement Parts ss ua era acd kenn nee 1 ALT D Series Controller oi oen ci ee ec tan Phe Da Y 2 A 1 2730D Pump latus nee CE PCR e AE A 4 A 1 3 1000D Pump m een er ne een A 8 A 1 4 500D DX Pump u ne Reale ee herr er A 12 A 1 5 500HPx Pump Ra Her A 16 A 1 6 100DM DX and 260D Pumps A 19 A 1 7 65D P mp vr marsen ter edhe GER re a ee eek A 23 A 1 8 65DM eta ee Edw adie eae BR re A 35 A 1 9 Power Circuit Board A 49 A 1 10 Analog Output Circuit Board A 53 A 1 11 Interface Circuit Board A 55 A 1 12 Dual Electric Valve Package A 57 A 1
34. 9 6 2 Pump Case Top Some maintenance and troubleshooting procedures require Removal accessing the pump module interior Remove the four screws holding the case top in place two screws on each side Lift the cover straight up and off M Note For the 30D remove the 6 screws holding the case top in place 3 on each side Figure 9 7 Pump case top screws 2 of 4 shown 9 10 9 7 Test Points 9 7 1 Power Supply Al 9 7 2 Controller D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing The following sections contain tables listing the most commonly used test points and their voltages Refer to the controller sche matic and the pump schematic available online on our Web site N NDANGER RISK OF ELECTRIC SHOCK DISCONNECT THE ELECTRIC POWER BEFORE SERVICING ONLY TRAINED SERVICE PERSONNEL MAY REMOVE THE CASE TOP N N DANGER RISQUE DE CHOC LECTRIQUE COUPER L ALIMENTATION AVANT LA R PARATION L USAGER NE DOIT PAS D MONTER L INSTRUMENT OU D RANGER LE M CANISME DEDANS ADRESSER LA REPARATION SEULEMENT AUX TECHNICIENS COMP TENTS Output voltages of the power supply can be verified The voltages in the pump unit between circuit common TP106 and the fuses or at the test points should be F104 422 VDC to 31 VDC F103 8 1 VDC to 13 VDC F102 22 VDC to 31 VDC TP111 415 VDC 0 6 VDC TP110 15 VDC 0 6 VDC TP109 5 VDC 0 3 VDC The voltage betwee
35. Lincoln NE 68501 USA 800 775 2965 lab instruments 866 298 6174 samplers amp flow meters Sales amp General Information 800 228 4373 USA amp Canada Phone Repair service Fax 402 465 3001 Email February 28 2012 P N 60 1002 040 Rev G IscoService teledyne com ae TELEDYNE ISCO Everywhereyoulook
36. Section 6 Modifier Addition Immediately open the extractant outlet valve s Flow MUST be established through the system at or before the time EQUILIBRATE is displayed To properly equilibrate the pumps they must be delivering fluid 12 Once the message RUNNING is displayed modifier will be delivered at the selected rate Press STOP Close the outlet valves of both pumps Take the pumps out of modifier mode by pressing softkey B under the word MODIFIER The word ON will change to OFF 4 Open the inlet valve of pump B Press REFILL and press B to designate Pump B 6 After pump B has filled press CONST FLOW and set the desired purging flow rate Press RUN and deliver 5 10 ml of modifier back through the inlet valve This ensures that all air is purged from the pump Press STOP B Return to constant pressure mode by pressing D SELECT PUMP and then A Place the pump in modifier mode by pressing softkey B under the words MODIFIER The word OFF will change to ON above MODIFIER Open the outlet valves of both pumps if they are not open 4 Press RUN When A pressure is established the message HOLD PRESS RUN will be displayed 6 Open the extractor inlet valves The message EQUILIBRATE will be displayed on the con troller screen If the controller does not display EQUILI BRATE press RUN While this message is displayed no modifier will be delivered Immediately ope
37. Teledyne Isco Inc REV N DATE 110311 PART NUMBER 60 1244 235 69 1243 576 60 1244 216 60 1243 414 202 9091 06 60 1243 537 60 1243 534 60 1243 348 60 1248 116 69 1243 444 201 69 1244 415 69 1243 431 60 1243 607 201 69 1243 563 113 3250 00 69 1243 560 150 0006 01 201 1337 00 69 1243 800 60 1243 492 141 60 1244 236 DESCRIPTION PREAMPLIFIER CBA ASSY 260ML NITRONIC CYLINDER PISTON ASSY SEAL RETAINER SEAL WEAR RING PISTON BASE THRUST BEARING BALL NUT ASSY CYLINDER SEAL THRUST BEARING INDIVIDUAL ORDER 2 EA UNIVERSAL SENSOR HARNESS WORMGEAR 260D 100DX KEY BEARING SEE NOTE 3 EXTENDED WORM GEAR 260D 100DX CAP 5uF 100VDC GEAR SPUR BRAKE BEARING SEE NOTE 3 COMBINATION GEAR SOAK PAD D SUB SOCKET LUBE WHEEL ASSY 4299 02 0329 00 4001 02 411 0311 51 FUSE I AMP 411 0311 62 FUSE 2 AMP 120 0013 00 60 1244 309 69 1243 465 69 1243 575 60 1244 223 60 1243 468 202 9090 75 Note POWER FILTER 6A TRANSFORMER ASSY CYLINDER CAP SEAL IOOML CYLINDER PISTON ASSY PISTON SEAL RETAINER SEAL For current prices and quotations on parts contact Isco Customer Service Department 2 This list is subject to change without notice 3 Verify the part number with Isco Technical Service Department A 20 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST DWG NO 60 1242 321 SHEET 3 OF 3 Teledyne SER Inc REV N
38. Teledyne Isco One Year Limited Factory Service Warranty This warranty exclusively covers instruments providing a one year covering parts and labor Any instrument that fails during the warranty period due to faulty parts or workmanship will be repaired at the factory at no charge to the customer Teledyne Isco s exclusive liability is limited to repair or replacement of defective instruments Teledyne Isco is not liable for consequential damages Teledyne Isco will pay surface transportation charges both ways within the 48 contiguous United States if the instrument proves to be defective within 30 days of shipment Throughout the remainder of the warranty period the customer will pay to return the instrument to Teledyne Isco and Teledyne Isco will pay surface transportation to return the repaired instrument to the customer Teledyne Isco will not pay air freight or customer s packing and crating charges This warranty does not cover loss damage or defects resulting from transportation between the customer s facility and the repair facility Teledyne Isco limited warranty The warranty for any instrument is the one in effect on date of shipment The warranty period begins on the shipping date unless Teledyne Isco agrees in writing to a different date Excluded from this warranty are normal wear expendable items such as charts ribbon lamps tubing and glassware fittings and wetted parts of valves and damage due to corrosion
39. qu il n y ait aucune fuite de gaz avant d introduire le gaz inflammable au syst me partir d un sys t me temp rature stable et sans aucune fuite de gaz la valeur du flot qui est indiqu par la pompe devrait se stabiliser une valeur moins de 0 01 ml min apr s 15 minutes pendant une extraction statique Important Quand vous utilisez un extracteur Teledyne Isco SFX 2 10 SFX 220 et 3560 soyez absolument certain que le ventilateur du moteur sans brosses fonctionne correctement Quand vous installez l extracteur assurez vous qu il y a un espace vide de 15 centim tres au moins entre le mur et l arri re de l extracteur pour assurer ventilation ad quate Le syst me SFE et les pompes de s rie D utilisent les moteurs de courant continu Ils poss dent des collecteurs et brosses qui produisent des d charges lectriques tincelles entre eux quand les moteurs fonctionnent normalement Ces d charges aussi bien que celles qui sont produites aux contacts des relais pourraient faire exploser un mixture d air et de gaz inflammable De petites modifications aux pompes peuvent les rendre moins dangereuses surtout dans le cas rare d une panne catastrophique du joint d tanch it du piston Cependant il n y a aucune modification qui fera ces pompes l preuve d explosion Enlevez les couvercles de devant et d arri re du cylindre qui sont situ s sur la tour de la pompe Cela permettra au gaz qui s chappe de dissiper plus r
40. receive mode of operation OTHER OPTIONS Sets the fill and refill marks that are used with both con tinuous flow modes Sets the NCV feature On Off See Section 5 6 4 5 6 1 Defining Operation Select Pump This menu allows you to select any pump to display its run screen program and operation data and to make program changes Valve specification To prevent pressure fluctuation at swi tchover you must specify the type of valve package you are using 5 17 D Series Syringe Pumps Section 5 Continuous Flow Introduction Installation amp Operation MORE pe Figure 5 8 Keystrokes to specify valve type M Note VALVE Io Press 3x to return to run screen AIR CHECK VALVES 2 way 3 way ELECTRIC ELECTRIC E PREVIOUS In older controller versions only buttons 1 ACTIVE and 2 PAS SIVE are selectable when specifying the valve type being used Figure 5 8 Active refers to air or electric valves Passive refers to check valves Volume totalizer The total volume delivered is displayed in liters at the top right corner of the screen Refer to the figure below to reset the volume totalizer to zero mu ir TOTAL VOLUME RESET 1 AB Pumps 2 CD Pumps 3 AB amp CD Pumps MORE Figure 5 9 Keystrokes to reset volume totalizer 5 6 2 Constant Flow Mode Menu 2 Once PREVIOUS Press 2x to return to run screen Continuous flow mode is fou
41. time The pump should be stored with methanol or isopropanol at least partially fill the cylinder with either solvent and then run the piston all of the way up when it is not being used The operator can set the maximum pressure limit on the pump controller refer to Section 3 8 7 The pump can be set to stop running if an overpressure condition occurs The shear key is located in the worm gear assembly of the pump Should the maximum pressure circuit fail and excessive pres sures pressures that exceed maximum pressure limits persist in the operation of this pump the torque limiting shear key may become damaged The shear key will yield at pressures slightly above maximum pressure and it will break around 1 5 times the pressure rating 9 12 1 Shear Key D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing In the event of a shear key failure the pump will sound as though it is turning but the piston will not move up the cylinder When this occurs the pump motor will not stop automatically Damage to the pressure transducer and push tube could be pos sible ifthe key failed due to extreme overpressure WARNING The shear key is NOT a safety feature It provides a measure of protection against damage to the equipment Avoid overpressure situations by properly installing and programming the pumping system In applications where overpressure conditions are possible install an appropriate press
42. 1 CLEAR Stops all motors sets flow rate and pressure setpoints to zero CONTIN CONST FLOW CONTIN CONST FLOWCD Puts pump in continuous flow under constant flow mode CONTIN CONST PRESS CONTIN CONST PRESSCD Puts pump in continuous flow under constant pressure mode CONTIN MODIFIER Put pump in continuous modifier addition mode CONST FLOW CONST FLOWB CONST FLOWC CONST FLOWD Put pump in constant flow mode CONST PRESS CONST PRESSB CONST PRESSC CONST PRESSD Put pump in constant pressure mode DELIVER DELIVERCD Set the dual pump mode to deliver fluid when running DIGITAL Returns the status High or Low of the digital outputs Format is digital xxxxxxxx where x is either or L The status order returned corresponds with the outputs 1 8 X no change DIGITAL xxxxxxxx 1 8 8 20 Sets the digital output either High or Low where is either or 1 The order cor responds with the outputs 1 8 D Series Syringe Pumps Section 8 Serial Interface Table 8 6 Serial Commands Continued Command Description DIG CONTROL Returns the status of the digital output control bits as either REMOTE R or INTER NAL I The return message format is DIG CONTROL xxxxxx where x is either R or I R indicates the corresponding bit is controlled remotely and I indicates the corresponding bit is controlled i
43. 13 Single Electric Valve Package A 59 A 1 14 SST Dual Air Valve Package for 100 260D 500D A 61 A 1 15 SST Dual Air Valve Package for 10000 A 63 A 1 16 Single Air Valve Package A 65 A 1 17 Dual Air Valve Package for 500HPx A 67 A 1 18 Dual Check Valve Package for 100 260 500D A 69 A 1 19 Dual Check Valve Package for 1000D A 71 A 1 20 Single Check Valve A 73 Appendix B Continuous Flow Introduction Installation and Opera tion for 30D Bed Introduction cac EEE RT ein ere Del werte hee AS B 1 B 2 Continuous Flow Air Valves B 1 B 2 1 Dual Air Valve Installation B 2 Continuous Flow Electric B 4 B 3 1 Technical Specifications B 4 B 3 2 Dual Electric Valve Installation B 5 B 4 User Supplied Valves ez vr RV ee dee PIA Ri ps B 7 B 5 Continuous Flow B 8 B 5 1 Defining Operation B 9 B 5 2 Constant Flow Mode B 10 B 5 8 Constant Pressure Mode
44. 137X138 1 1 1 5 104 pisaR ss PM 05 POE g 5 8160 SS 124 m C120 117 F101 F102 1 A 49 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT POWER PART LIST DWG NO 60 1242 348 SHEET 2 OF 3 TELEDYNE sco Inc CIRCUIT BOARD REV J DATE 110311 pes PART NUMBER REFERENCE DESIGNATION 110 4568 01 DESCRIPTION CAP 6800uF 25VDC 10 6333 01 C115 CAP 3300uF SOVDC 110 7290 00 CAP 6400uF 150VDC 112 5010 00 C105 CAP 2 2uF 20VDC 112 7510 00 C18 C19 C121 C122 CAP tur 35VDC 270 0000 01 IC HCPL 2232 270 0013 00 IC 4011B 270 0129 03 IC LM2903 270 2002 00 279 0200 07 VR101 IC D469 VR LM7915CT 279 0201 05 VR103 VR LM7815C 279 0605 01 VR102 VR LM317 360 1024 03 K10
45. 3 2 TI p RS232 Cable for computer serial control of two controllers 9 pin to two 25 pin 6 ft 1 8m 68 1020 198 m LJ elie RS232 Extension cable for computer serial con trol of three or more controllers Connects to above cable 25 pin to two 25 pin o df 6 ft 1 8m 68 1020 180 e o KK Transducer Cap assembly for the 30D 65D Transducer cable 6ft 1 8m Figure 1 9 Syringe pump cylinder cap Attach to pressure transducer connector on back of pump N CAUTION The pressure transducer cable length is always 6 feet 1 8m Never attempt to extend the length of this cable 1 20 D Series Syringe Pumps Section 1 Introduction Controller Pump PRESSURE OUTPUT PRESSURE Pressure Transducer TRANSDUCER op conector MAINS 2 7 _ _ LJ 7 Figure 1 10 Connecting the pump and controller N CAUTION Never make any cable connections while the pump is powered ON 1 6 Preliminary Checkout After the electrical connections have been completed follow this brief test of the pump s operation Preliminary checkout of the pump is performed without fluid in the pump If adding a new pump to the controller a hard and soft reset need to be completed See Section 9 4 N CAUTION Always maintain cle
46. 3 Basic Programming and Operation 5V and the preferred output scale is 1 volt per 10 ml min MAX FLOW is set at 50 ml min MAX FLOW cannot exceed the pump specification A controller running one to two pumps can also output cylinder volume on the remaining outputs The volume output range is not adjustable Full scale is equal to one pump stroke P319 Oso 0308 C306 AS e C305 P320 C307 7 U301 TE SI ANALOG OUTPUT 2 5V L NS 5V ANALOG OUTPUT 1 C301 530 E E 5304 5V U302 lov ANALOG OUTPUT 4 o 5V ZN 132137 5V H 25 o AN ANALOG OUTPUT 3 C303 5303 TLN B42 5V Figure 3 15 Output range selection jumpers Table 3 2 Analog Output Options connections to female 25 pin Sub D Pin No Description One or Two Three Pump Pump Function Function Chassis earth Analog common Analog common Analog common Analog common Output 1 Flow Rate A Flow Rate A Output 2 Flow Rate B Flow Rate B Output 3 Volume A Flow Rate C Output 4 Volume B Volume B For additional information about analog output options download technical bulletin TB34Syringe Pump Analog Output Options 3 14 2 Current Loop Output The pump controller can be configu
47. 30D F101 6 25 Amp T DWG 60 1242 302 Figure 1 8 Pump front panel controls Table 1 14 Pump Front Panel Item No on Connector Description Figure 1 8 1 Mains power switch Disconnects power from the pump circuits for setup changes such as connecting the controller 1 mains power is applied to the pump circuitry 0 mains power is removed from the pump circuitry 1 5 Electrical Connections The pump controller may be placed on top of the pump or wherever safety and convenience dictate Power is supplied to the pump controller through the control cable 1 5 1 Cabling D Series Syringe Pumps Section 1 Introduction CAUTION All connections between the pump and controller should be made BEFORE the pump is connected to mains power 1 Connect the pressure transducer cable which originates from the top of the pump cylinder to the nine pin sub D PRESSURE TRANSDUCER connector on the pump rear panel Figure 1 7 Be sure to tighten the thumbscrews Connect the control cable which originates from the first or only pump rear panel to the PUMP A connector on the rear panel of the controller Figure 1 6 and tighten the thumbscrews This cable must be plugged into the PUMP A connector M Note There are four PUMP connectors on the rear of the controller Only the PUMP A connector is wired to supply power to the controller therefore one pum
48. 4 500HP PUMP ONLY DED PUMP P 260HP DED PUMP NOTE This list subject to change without notice A 51 D Series Syringe Pumps Appendix A Replacement Parts This page intentionally blank A 52 D Series Syringe Pumps Appendix A Replacement Parts A 1 10 Analog Output Circuit Board P319 3 308 c306 C305 HA P320 C307 7 U301 2 302 nee C302 m E N 5 HOV C301 5301 sv st U302 5304 5 C304 5V i 332 1771 5V T H302 gun C303 5303 ANALOG OUTPUT CIRCUIT BOARD A 53 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT OC OU DWG NO 60 1242 275 PART LIST y SHEET 2 OF 2 CIRCUI OA REV DATE 92050 IT EN PART NUMBER REFERENCE DESIGNATION DESCRIPTION 301 112 6010 00 C307 C308 CAP 10uF 25VDC 502 141 9002 26 J321 SKT 25 PIN SUB D RA 505 270 1600 27 0501 0302 IC AD7237 NOTE 1 For current prices and quotations on parts contact Isco
49. 4 Selecting Operating Parameters 3 3 Main Menus 3 4 Menu One D Series Syringe Pumps Section 3 Basic Programming and Operation There are four ways to program the system from a menu screen Menu Selection The number keys are used to select from listed menu items Softkey Selection The softkey programming options appear on the fourth line of the screen To either toggle or select an option press the softkey A D directly below that option Keypad Selection The programming keys are located on the left side of the keypad The pump mode limits and refill are all options that may be selected from the keypad Value Selection The number keys are used to enter all numeric values required for pump operation When a numeric value is required a message will blink prompting you to enter an appropriate value There are four main menu screens Access Menu 1 by pressing MENU To move forward and back between Menus 1 2 3 and 4 or to return to the run screen use softkeys A MORE and D PRE VIOUS RETURN Use the number keys to select a menu option Selecting a menu option displays the programming parameters for that option in menu form To exit a menu when multiple pumps are connected press the STORE RECALL CLEAR ENTRY OR MENU key Menu 1 provides programming options for units of measure pump selection refill settings power failure response system reset and display contrast adjustment To save all settings and
50. 7 Connect the DB 25 cable to the controller rear panel elec tric valves connector Figure B 2 B 5 D Series Syringe Pumps Appendix B Continuous Flow Introduction Installation and Operation for 30D 2 2 Inlet Tubing Pl with filter DB 25 Connector to controller electric valve connector Figure B 2 Electric valve installation B 6 D Series Syringe Pumps Appendix B Continuous Flow Introduction Installation and Operation for 30D B 4 User Supplied Valves Users may also choose to supply their own valves The following information is necessary to choose the appropriate valves to work with Teledyne Isco Continuous Flow software Check valves Do not use spring loaded check valves if refilling at atmospheric pressure the pump seals are not designed to draw against a vacuum Powered valves These are electrically triggered from the pump controller and could be air or electrically actuated Digital outputs 1 4 provide signals for control of four two way valves One wire for each valve is connected to its specific connector on the rear of the controller A second wire for each valve connects to ground The signal provided is an open collector which functions as a switch open for closure of the fluid path A switch closure low signals opening of the fluid path Table B 3 shows the relationship between the digital output pump valve loca
51. A Pressure Pump B Digital Inputs 1 8 Pressure Pump C 1 High Units psi 5 0 Low Resolution 0 2 psi ALOG1 ALOGS refer to Table 8 6 Units volts 5000 Resolution 0 2 millivolt Range 7500 to 58035 1 5000V to 11 6070V Figure 8 3 Get Status String Command R049 37510 00128 01017 06981 05743 00421 00442 00449 25046 11111000 CS l Pressure Pump A Pressure Pump B Digital Inputs 1 8 Pressure Pump C 1 High Units psi 5 0 Low Resolution 0 2 psi ALOG1 ALOG6 refer to Table 8 6 Units volts 5000 Resolution 0 2 millivolt Range 7500 to 58035 1 5000V to 11 6070V Figure 8 4 Get Status String GG Command 8 26 D Series Syringe Pumps Section 8 Serial Interface Same as Figure 7 3 30B5 37510 00128 01017 06981 05743 00421 00442 0000005921 0010696698 R R 0027500000 0057744222 R R 1 00449 11111000 0052500000 0016778750 R R 0000005921 37500 00000000 24 Pump B L_ Pump C Control Status Pump A L Local control R Remote control E External control Operation Status Pump A S Pump stopped R Running F Refilling H Hold clock stopped E Equilibrating Volume Pump A Units Liters E9 Resolution 1 nanoliter Flow Rate Pump A Units Liters minute E10 Resolution 0 1 nanoliter minute Problem Status Pum
52. AN VT Burda 3 10 3 8 8 RAPID PRESS er een ere ER nen 3 12 3 8 9 DISP S sera Ite ud ee A Boe tate ier ET 3 13 3 8 10 ACC CTRE onser ae ehe een ORA I gs 8 18 3 8 11 ZERO PRESS en ee V ee le 3 13 3 9 Control of Multiple 3 13 3 9 1 Multi Pump Operation 3 14 3 9 2 Independent Control of up to Four Separate Pumps 3 14 3 10 Operating Modes os 1 0 ne re eee 3 15 3 10 12 Constant Flow poecie Be I ga RR og 3 16 3 10 2 Constant Pressure onee ee eee 3 16 8108 Dispense Mode sa leer a ara ar 3 17 3 11 External Control eee 3 18 3 12 External Control Analog 3 18 3 12 1 Wire connections co 8 18 3 12 2 Preparation inne d e ae aceti eder hati Mois atts 3 19 3 12 3 External Control for 3 19 3 12 4 Calculation Examples 3 20 3 12 5 S t p cse an Na oe OR ned CUR 3 20 3 13 Remote RUN STOP 0 e ccc ehh hn 3 21 3 13 1 Wire Connections ao ce eee eee eens 3 21 3 14 Analog Flow Rate and Volume Output Options 3 22 3 14 1 Voltage Analog Output 3 22 3 14 2 Current Loop
53. D or STOP to stop all pumps PRESS RUN KEY TO ESCAPE PRESS STOP KEY TO STOP ALL PUMP A PUMP B PUMP C PUMP D A B C D Figure 1 14 Four pump stop menu If you encountered any problems during the preliminary checkout please contact the Teledyne Isco Service Department The number is 800 775 2965 or 402 464 0231 M Note In the event of an emergency turn off the controller switch This will cause all pumps to immediately stop 1 23 D Series Syringe Pumps Section 1 Introduction 1 24 D Series Syringe Pumps Section 2 Fluid System Connections and Accessories 2 1 Introduction This section discusses general fluid system connections and the installation of fluid connection accessories temperature and pressure control accessories and optional kits and attachments NDANGER RISK OF INJURY THIS EQUIPMENT PRODUCES HAZARDOUS PRESSURES USE APPROPRIATE TUBING AND CONNECTIONS AS INSTRUCTED M Note When operating at flow rates at or below 500 ul min it is strongly suggested that an insulating cover or temperature control jacket be installed See Sections 2 4 1 and 2 4 2 2 2 Fluid System All D Series pump models connect similarly but with varying Connections port sizes Take care to follow the tips provided to ensure safety and proper operation 2 2 1 Ports There are two ports in the pump standard cylinder cap Either port can serve as the inlet or outlet As shown in Figure 2 1 you may plug on
54. D Series Syringe Pumps Section 1 Introduction Table 1 2 65D Technical Specifications CYLINDER CAPACITY 67 97 ml POWER REQUIREMENTS Mains voltage line cord is a Disconnect Device 100 10 VAC 1 5 A maximum 117 12 VAC 1 5 A maximum 234 23 0 75 A maximum Factory Set LINE FREQUENCY 50 or 60 Hz LINE VOLTAGE NOISE TOLERANCE 1 7 x nominal rms line voltage 10 usecond pulses any phase angle random or repetitive DIMENSIONS PUMP CONTROLLER 27 18cm 27 18cm 46 74 cm 30 48 cm 101 09 cm 13 59 cm Width Depth Height WEIGHT PUMP CONTROLLER 32 8 kg 2 96 kg FLOW RATE RANGE 0 01 ul min to 25 ml min for any pressure up to 1379 bar FLOW RATE ACCURACYP 0 3 maximum 0 25 ul min seal leakage FLOW RATE DISPLAY RESOLUTION 0 01 ul min 1 0 ul min in Constant Pressure Mode ANALOG OUTPUT ACCURACY x 196 of selected range DISPLACEMENT RESOLUTION REFILL TIME REFILL OR DEPRESSURIZATION RATE 2 55 nl step 1 7 minutes 0 01 ul min to 40 ml min at any pressure from 0 to 1379 bar PRESSURE RANGE 0 6895 to 1379 bar PRESSURE ACCURACY 0 1 of full scale at constant temperature PRESSURE REPEATABILITY 0 5 of full scale within 48 hours at constant temperature ZERO PRESSURE DRIFT 0 25 of full scale within 48 hours at constant temperature PRESSURE DISPLAY RESOLUTION AMBIENT TEMPERATURE RANGE 6 895 kPa 5 to 4
55. DATE 110311 4 60 1243 536 WEAR RING S O 60 1248 127 BALL SCREW ASSY 100DM 100DX 46 60 1243 608 100DM 100DX 48 60 1244 220 GEAR LUBRICATION ASSY NOT SHOW O 49 60 2254 132 MOTOR BRUSHES 209 0161 00 52 202 2062 23 O RING 1 609 ID 139 CROSS SECTION 60 1248 117 60 1245 158 0 1245189 60 60 1245 160 61 60 1245 174 64 60 1244 456 260 PREAMPLIFIER ASSEMBLY O AS ser sertu DAA o EE En Eu Eo oL OL For current prices and quotations on parts contact Isco Customer Service Department 2 This list is subject to change without notice 3 Verify the part number with Isco Technical Service Department A 21 D Series Syringe Pumps Appendix A Replacement Parts This page intentionally blank A 22 D Series Syringe Pumps Appendix A Replacement Parts A 1 7 65D Pump Im KJ Lu D On A rem TE NE AN dWNd dHG9 Q69 1300W 1511 SLYVd 1N3N32V 1d 48 A 23 D Series Syringe Pumps Appendix A Replacement Parts oa a o a xo ao zo un ze Ei xu 26 24 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST MODEL 65D 65HP PUMP A 25 D Series Syringe Pumps Appendix A Replacement Parts SEE SECTION A A el Sc
56. DIGITAL OUTPUT BIT2 HIGH 1 DIGITAL OUTPUT BIT 2 LOW 0 DIGITAL OUTPUT BIT 3 HIGH 1 DIGITAL OUTPUT BIT 3 LOW 0 DIGITAL OUTPUT BIT 4 HIGH 1 DIGITAL OUTPUT BIT 4 LOW 0 DIGITAL OUTPUT BIT 5 HIGH 1 DIGITAL OUTPUT BIT 5 LOW 0 DIGITAL OUTPUT BIT 6 HIGH 1 DIGITAL OUTPUT BIT 6 LOW 0 DIGITAL OUTPUT BIT 7 HIGH 1 DIGITAL OUTPUT BIT 7 LOW 3 3 3 5 5 5 5 3 3 3 Sf 5 A ay 3 7 5 D Series Syringe Pumps Section 7 Modbus Configuration Table 7 5 Coils Continued Register Address Type Size Description 71 R W 1 BIT 0 DIGITAL OUTPUT BIT 8 HIGH 1 DIGITAL OUTPUT BIT 8 LOW 0 Disable Dispense Mode A 1 Enable Dispense Mode A Only configure if in Constant Flow Mode 0 Disable Dispense Mode B 1 Enable Dispense Mode B Only configure if in Constant Flow Mode 0 Disable Dispense Mode C 1 Enable Dispense Mode C Only configure if in Constant Flow Mode 0 Disable Dispense Mode D 1 Enable Dispense Mode D Only configure if in Constant Flow Mode RW 1 Reset total volume delivered by multi pump pair AB RW RW RW RW 1 Reset total volume delivered by multi pump pair CD Pressure Units Pressure Units BAR Pressure Units kPa Pressure Units PSI Flow Units ml min Flow Units ml hr Flow Units ul min Flow Units ul hr 0 Overpressure Alarm OFF 1 Overpressure Alarm
57. Filter Package 68 1247 011 Part Number Description 60 1243 231 1 5 m stainless steel tubing 146 OD x 0 020 ID 60 1243 232 0 3 m stainless steel tubing 146 OD x 0 020 ID 209 9012 17 In line solvent filter with replacement frit 0 5 micron filter 209 0094 07 Zero volume 46 valve nut 209 0094 08 Zero volume 146 valve ferrule Installation 1 Attach the reducing adapter from the pump accessory package to the pump outlet using the nut and ferrule pro vided Or connect to the reducing union of the outlet valve package 2 Attach the 1 5 m length of tubing to the reducing adapter Cut to the desired length 3 Then attach the in line filter to the end of the tubing The flow direction is indicated on the filter body 4 Connect the remaining 0 3 m length of tubing between the in line filter and the receiving device Cut to the desired length 0 3 m Tubing Length 4 In line Filter 1 5 m Tubing Length Figure 2 10 In line filter package D Series Syringe Pumps Section 2 Fluid System Connections and Accessories 2 4 Temperature and Pressure Controls 2 4 1 Cylinder Insulating Cover Notches for tubing Side Latches Notch for cable Some applications such as those with very low flows may require additional measures to maintain steady rates The optional insulating cover can reduce flow noise due to tem perature fluctuations and improve pump perfo
58. Flow and Concentration Modes 4 6 4 2 3 Dual Gradient System Connections Connection of the dual gradient system requires two refill valve kits and the gradient mixer package as discussed in the intro duction on Page 4 1 The Dual Gradient System is not available for the 30D pump Please contact the factory for details The static mixer has an internal volume of 3 1 pl and pressure rating of 413 7 bar and is supplied with PEEK Fingertight III fittings for connection to the 1 16 tubing in the kit M Note The static mixer can be replaced by a user supplied dynamic mixer Solvents are fed from each pump through the in line filters and check valves and into the static mixer where they are mixed and fed into your system apparatus Kit components and connections are shown in Figures 4 3 and 4 4 1 Connect the 10 cm length of 146 stainless steel tubing to the center port outlet of the mixer using the PEEK fit tings provided 2 Connect the other end of the tubing to the Valco valve at the port marked pump using a Valco nut and fer rule 3 Connect the two in line filters oriented with flow toward the check valves indicated by the arrow on the housing one filter to each piece of 46 stainless steel tubing outlet from each pump 4 Using the PEEK fittings connect the 45 7 cm lengths of stainless steel tubing to each inlet port on the mixer Connect the other ends to the outlet fittings
59. Flow Introduction Installation and Operation for 30D 601262101 REPLACEMENT PARTS LIST SHEET 3 OF 3 TELEDYNE ISCO PART NUMER DESCRIPTION 601263131 SHEAR KEY 30D 601264082 ASSY 30D PRESS AMP 6012670 COOLING JACKET ASSY 30D 602254132 OTOR BRUSHES PKG 2 605363068 DUAL MALE F250C ADPTR KB E E 69124356 SPUR GEAR 243563 EXTENDED WORM GEAR 24380 COMBINATION GEAR 243802 PINION GEAR 264154 REPLACEMENT TERMINAL STRIP ASSY 244413 TRANSDUCER CABLE ASSEMBLY 263096 LABEL FRNT PNL 30D PMP 62990 BRG NDL 1 37510 2 0630D 629902 BRG NDL 1 2501D 1 9380D 629951 BRG NDL 1 37510 2 0630D 629952 WSHR BRG NDL 1 25010 1 9380D 200104 SCR SET 1 4 20X1 4 232609100 NUT HEX 1 2 20 601243201 PAN DRIP 601263145 SQUARE AMPLIFIER BOX COVER 209016405 PLUG F250C 60K PSI NOTE For current prices and quotations on parts contact Teledyne Isco Service Department 2 This list is subject to change without notice B 16 D Series Syringe Pumps Appendix B Continuous Flow Introduction Installation and Operation for 30D B 6 2 30D Air Valve B 17 D Series Syringe Pumps Appendix B Continuous Flow Introduction Installation and Operation for 30D REPLACEMENT PARTS LIST SHEET 2 OF 2 TELEDYNE ISCO REV B PART NUMBER DESCRIPTION DD 504 062 ID 099 D CNTRL VLV 3 PORT
60. Installation amp Operation 5 14 5 4 2 Dual Electric Valve Installation Plumbing connections Electrical connections To install the electric valve package refer to Figure 5 7 on the following page 1 Position the valve bases 1 3 cm apart 2 Use the plugs to stopper the ports that will not be con nected NDANGER RISK OF INJURY THE PRESSURE PRODUCED COULD BE 700 BAR PLEASE UTILIZE APPROPRIATE TUBING AND CONNECTIONS NOTED IN THE MANUAL 3 Loosely attach the tubing lengths from the valve assembly to the pumps 4 Allow the bracket to hang vertically and place the straps around the pressure transducer caps Tighten the wing nuts 5 Install the four bracket panhead screws on the bottom of the bracket 6 Tighten the tubing nuts 7 Connect the inlet tube to the supply reservoir Connect the outlet tee to your apparatus 8 Connect the DB 25 cable to the controller rear panel SFX 220 VALVES connector Figure 5 7 D Series Syringe Pumps Section 5 Continuous Flow Introduction Installation amp Operation OVERHEAD VIEW Y 6 32 HEXNUT 60 1242 343 REV C io SPACER BLOCK ar WINGNUT 6 32 HEXNUT STRAP MOUNT STRAP OPTIONAL REDUCING FITTING FOR 1 16 TUBING M 1 8 NUT AND FERRULE FOR
61. July 22 1991 edition of Chemical and Engineering News is reprinted with permission from Professor Robert E Sievers and his colleagues at the University of Colorado at Boulder Even though they were not performing supercritical fluid extraction it details the problems their lab experienced using nitrous oxide under simi lar conditions We add our support for their suggestion to use only carbon dioxide or other less hazardous fluids for supercritical fluid extraction ERING CHEMICAL uS LETTERS 29 69 Num 4991 goa 17138 UN 25 234 N 0009 F ion ethano EMICAL SA so ide ex los jt eth super ical uid ni x s 500 m e pump ome posted Sa extract uld TR others N with pol mixture ick wave OF P ol oF bh jon ap rous oxide s ethan ne hm onat ed V xractio nie odifiers 9 AU ove be ce in the dca ig cted for SUP ee catalyst su Ben nol 3 ihe ot c n be we n par a nr ion natt enc cal ni us the fu xplosi0 samples we e t ed super 9 tetraeth le or ous OX when e er et nol z thy orate the critic n c po d oxide A ate 0 07 ud This Lim pau en hosilid 00 ps ld d entis ylort 0 07 5 aa mn cm v pu pers of di we ture WS PS sees st Pr Because lof E other e5 m exp at 4 mate us may ju carb substitut evers Annen mix ur ANE ee gous sol Robert fc t ee sor 0 n plode
62. Keystrokes to set up constant flow B 10 B 6 Keystrokes to set up constant pressure B 10 B 7 Keystrokes to set up No Check 1 B 11 B 8 Keystrokes to Run or Stop the pumps B 12 List of Tables 1 1 30D Technical Specifications 1 2 1 2 65D Technical Specifications 1 3 1 3 65DM Technical Specifications 1 4 1 4 100DM Technical Specifications 1 5 1 5 100DX Technical 1 6 1 6 260D Technical Specifications 1 7 1 7 500D Technical Specifications 1 8 1 8 500HPx Technical 1 9 1 9 1000D Technical Specifications 1 10 1 10 Pump Controller Front Panel Label 1 14 1 11 Pump Controller Key Functions 1 15 1 12 Pump Controller Rear Panel Connectors 1 16 1 13 Pump Rear Panel Connectors 1 17 1 14 Pump Front Panel ie oense eeen nere 1 18 2 1 D Ser
63. MULTPUMPLLB MULTPUMPLLB PANEL VI PANEL VI README DOC README DOC SERIALIO LLB SERIALIO LLB Once the system is properly connected turn the pump con troller s and computer on Then use the following procedure to place your controller s in serial control mode Press MENU gt MORE A and select SERIAL 1 Factory controller default settings are baud rate 9600 and unit ID 6 To restore defaults press MENU then SYSTEM RESET 5 Resetting a system erases all programs and user settings 1 Press MENU gt MORE A gt 1 Serial Option to enter the serial option setup screen 2 Select the communication baud rate between 300 and 115 2K by pressing NEXT BAUD A until you reach the desired baud rate M Note All units in the network must be set to the SAME baud rate 8 5 D Series Syringe Pumps Section 8 Serial Interface 8 7 User written Software 8 6 8 6 3 Verify Operation 8 7 1 DASNET 3 Select an identification number for each controller up to seven by pressing NEXT ID B until you reach the desired number M Note Multiple controllers in a network must each have a different ID number If several units are being configured place a label on the rear of each instrument listing the ID number and baud rate This will help identify the controller in the future and prevent assigning the same ID number to two controllers or assigning an incorrect baud rate To verify network operation open a t
64. Name Teledyne Isco Manufacturers Address 4700 Superior Lincoln Nebraska 68504 USA Mailing Address P O Box 82531 Lincoln NE 68501 Equipment Type Environment Laboratory Equipment for Light Industrial Commercial Environments Trade Name Model No Series D Series Controller Pump Controller Yearoflssue 2014 Standards to which Conformity is Declared EN 61326 1 2006 EMC Requirements for Electrical Equipment for Measurement Control and Laboratory Use EN 61010 1 2010 Safety Requirements for Electrical Equipment for Measurement Control and Laboratory Use Standard Description Severity Applied Performance Criteria EN61000 4 2 Electrostatic Discharge Level 2 4kV contact discharge A 2009 Level 3 8kV air discharge A EN61000 4 3 Radiated RF Immunity 80 MHz to 2 7GHz 8096 AM at 1kHz A 2010 Level 1 10 V m EN61000 4 4 Electrical Fast Transient on Mains Level 2 2kV on AC lines A 2010 and I O EN61000 4 5 Surge on AC Lines 2kV common mode 1KV differential mode A 2005 EN61000 4 6 Conducted RF on AC Mains and 150 kHz to 80 MHz 3V rms 8096 modulated A 2008 I O A EN61000 4 11 Voltage Dips Short Interruptions 0 5 cycle each polarity 100 2004 EN61000 3 2 AC Harmonic Flicker Pass 2009 3 3 2008 CISPR11 RF Emissions Radiated below 1 Group 1 Class A Industrial Scientific and Pass EN 55011 2009 GHz and Conducted AC Mains Medical Equipment I the undersigned hereby declare that the design of the eq
65. ON 0 Overpressure Display OFF 1 Overpressure Display ON 0 Overpressure Shutdown OFF 1 Overpressure Shutdown ON 0 Underpressure Alarm OFF 1 Underpressure Alarm ON 0 Underpressure Display OFF 1 Underpressure Display ON 0 Underpressure Shutdown OFF 1 Underpressure Shutdown ON 0 Overflow Alarm OFF 1 Overflow Alarm ON 0 Overflow Display OFF 1 Overflow Display ON 0 Overflow Shutdown OFF 1 Overflow Display ON 0 Underflow Alarm OFF 1 Underflow Alarm ON 0 Underflow Display OFF 1 Underflow Display ON 0 Underflow Shutdown OFF 1 Underflow Shutdown ON 0 Poor Fill Alarm A OFF 1 Poor Fill Alarm A ON 0 Poor Fill Alarm B OFF 1 Poor Fill Alarm B ON 0 Poor Fill Alarm 1 Poor Fill Alarm C ON 0 Poor Fill Alarm D OFF 1 Poor Fill Alarm D ON 1 Stop all motor and reset flow rate and pressure set points to default 0 Transducer of Pump A not connected 1 Transducer of Pump A connected 0 Pump A not at upper flag limit 1 Pump A at upper Flag Limit Empty 0 Pump A not at lower flag limit 1 Pump A at lower flag limit Full 1 Pump A is overpressure 1 Pump A is underpressure 7 6 D Series Syringe Pumps Section 7 Modbus Configuration Table 7 5 Coils Continued Register Address Type Description 1 Motor failure Pump A 0 Transducer of Pump B not connected 1 Transducer of Pump B connected 0 Pump B not at upper
66. Overpressure 9 18 Conditions 7 Cycle the pump between REFILL and RUN a few times opening and closing the appropriate valves at the proper time to purge any remaining gas from the pump Use about 10 20 mls per stroke to purge This procedure is typically used for modifier systems when changing from one liquid solvent to another If high ionic strength aqueous reagent solutions are allowed to remain in the pump solid residues may be formed which will scratch the seals and the polished inner surface of the cylinder of the pump These scratches allow leakage which decreases flow rate 1 Press CONST FLOW RUN You will be asked to designate which pump if more than one is present 2 Press a softkey to run the desired pump 3 Run the pump until the message CYLINDER EMPTY is displayed 4 Place the pump inlet line in a flask containing a compati ble solvent or a detergent solution 5 Press REFILL You will be asked to designate the pump to refill if more than one is present Press a softkey to refill the pump 6 Fill the pump and repeat this procedure several times 7 Place the pump inlet line in a flask containing distilled water or appropriate solvent Fill the pump once more and then run it until empty You are now ready to fill the pump with the new liquid solvent M Note Do not leave buffer solutions which contain dissolved salts or corrosive buffers in the cylinder overnight or for long periods of
67. RG CYL 3541DI 00D KB RG CYL 381D 880D KB RG THR 351DX720D INDIVIDUAL ORDER QTY 2 RING 1 6091D 139 MALE 12 HOSE LAND F250C 30VM LR F250C 30VM R WV 397 ID 691244415 IVERSAL SENSOR HARNESS 410130401 RKR DPDT CSA 4A KB 411461264 FU 1 6A 250 SB 234 VOLT 41146121 FU 3 2A 250 SB 3AB 100 VOLT amp 117 VOLT 460010119 DCR PRESS 0 30 000 PSI 60124329 ELRIN PLUG 01243348 LIDE THRUST BEARING 243610 EAR TRAIN KEY 243816 CYLINDER CAP 65ML 244184 MOTOR ASSEMBLY WITH ENCODER AND GEAR 244236 LUBE WHEEL ASSEMBLY 244323 HARN MN PMP ENCD KB 243981 GEAR TRAIN SOAK PAD 249130 30D CBA REPLACEMENT KIT 244493 XFRMR 551 30D 245168 WORM GEAR MOD 248116 BALL NUT ASSY 248121 BALL SCREW ASSY 249128 RPLCMNT KIT 30D PISTON ASSY 249129 RPLCMNT KIT 30D PISTON SEAL 263098 CYLINDER CAP SEAL 30ML 263144 PUSH ROD 30ML 263109 CYLINDER 30ML o JOT 4 so Po c ae 05 en mie CO o FO JO Go IND gt DP DP DP mn mn HM DP DM In M For current prices and quotations on parts contact Teledyne Isco Service Department his list is subject to change without notice B 15 D Series Syringe Pumps Appendix B Continuous
68. See Figure 1 2 FLOW RATE ACCURACYP 0 5 maximum 1 0 ul min seal leakage FLOW RATE DISPLAY RESOLUTION 1 0 ul min ANALOG OUTPUT ACCURACY x 196 of selected range DISPLACEMENT RESOLUTION REFILL TIME REFILL OR DEPRESSURIZATION RATE 31 71 nl step 2 5 minutes 1 0 ul min to 204 ml min at any pressure from 0 to 258 6 bar PRESSURE RANGE 0 6895 to 258 6 bar PRESSURE ACCURACY 0 5 of full scale at constant temperature PRESSURE REPEATABILITY 0 5 of full scale within 48 hours at constant temperature ZERO PRESSURE DRIFT 0 25 of full scale within 48 hours at constant temperature PRESSURE DISPLAY RESOLUTION AMBIENT TEMPERATURE RANGE 6 895 kPa 5 to 40 C TEMPERATURE DRIFT 0 15 of full scale C HUMIDITY 95 maximum DEAD HEADSPACE VOLUME 4 00 0 020 ml POLLUTION DEGREE INSTALLATION CATEGORY MAXIMUM ALTITUDE Underwriters Laboratories UL has certified all D Series Pumps with the exception of the 100 VAC versions Using water at 137 9 bar and a temperature controlled environment at 30 C The analog output is an optional accessory Pressure repeatability specification is based upon re zeroing pressure transducer every 48 hours Refer to sub section ZERO PRESS in Section 3 of the manual for re zeroing procedure e Volume in and above the piston seal head clearance at automatic shutoff and inlet and ou
69. Service Department 800 228 4250 2 This list subject to change without notice A 54 D Series Syringe Pumps Appendix A Replacement Parts A 1 11 Interface Circuit Board 222 08 DM 208 K201 K202 K203 5 CR202 K204 K205 cr206 K206 ge ee K oaos iir Lett D p u201 v nne TP203 T204 25 Ll ci TP202 U202 c202 5 PH R204 5 205 CR208 R203 P219 _ TT N cus 0202 R202 1 1 19212 1 203 Urt us pair L um CR214 S 25 CD an Ar TP201 7 Om CR216 TP206 R206 R208 R209 R21 van 0205 U206 l TP207 208 eO Ow 15V C205 3 J v Oren Lo 2 4j F Oro S203 206 7 CR215 R217 R219 N U204 230 LILI CR217 P218 wo C208 4 207 R220 0 20 TTT 202 18 MOA 96969 9 INTERFACE CIRCUIT BOARD A 55 D Series
70. Si vous utilisez cet instrument d une maniere autre que celles qui sont specifi es dans ce manuel la protection fournie par l instrument peut tre affaiblie cela augmentera votre risque de blessure AVIS Les liquides qui sont analys s dans cet instrument peuvent tre canc rig nes hasards biologiques inflammables ou radioactifs Si vous devez utiliser ces liquides hasardeux il est tr s recommand que vous le faites l int rieur d un environnement isol concu pour tels liquides Cet environnement isol devrait tre construit selon les r glements f d raux provinciaux et locaux aussi que le plan de votre organisation qui concerne l v nement d un accident avec les mati res hasardeuses En tout cas utilisez toujours l instrumentation d Isco avec prudence et sens commun D Series Syringe Pumps Warnings Cautions and Notices Commonly Ordered Replacement Parts for the D Series Syringe Pumps Description Part Number Cylinder Seals General 30D Seal Assembly 0 2068 bar 60 1249 128 30D Piston Assembly 0 2068 bar 60 1249 129 65D 0 1379 bar 202 9096 08 65DM 0 689 5 bar 202 9096 08 100DX DM 0 689 5 bar 202 9090 75 260D 0 517 1 bar 202 9091 06 500D 0 258 6 bar 202 9091 56 500HPx 0 344 7 bar 202 9091 56 1000D 0 137 8 bar upper seal 202 9990 25 1000D 0 137 8 bar lower seal 202 9990 23 For more information on seals refer to Table 2 7 65D 30D Inlet Outlet fittings l4 F250C Gland 209 0164 02 ba F250C C
71. Table 5 3 Continuous Flow Check Valve Package for 1000D part 68 1247 128 Part Number Description 004 7302 251 SST tubing 250 x 035 60 1243 893 Valve to pump tubing 209 0163 36 Male connector 1 4 tube OD to 1 4 NPT 209 0164 06 Check Valve w 1 4 tube connections 209 0168 15 Tee union 1 4 tube OD 60 1243 936 2 x 2 SST tubing elbow 5 6 D Series Syringe Pumps Section 5 Continuous Flow Introduction Installation amp Operation 5 3 Continuous Flow Air Air valves generally open and close faster and are less prone to Valves error and component wear making them suitable for industrial use and other applications where the system will be constantly running however they require a user supplied pressurized air source of 80 to 115 psi 5 5 to 7 9 bar Air Valve Package Numbers A1000D 68 1247 104 A500D 68 1247 061 A500HPx 60 5364 343 A65DM 2600 A100DM A100DX 68 1247 058 A65D 68 1247 129 Table 5 4 Continuous Flow Technical Specifications Air Valves Pressure fluctuation at switchover 5 psi 0 35 bar at system backpressures from 100 psi 6 9 bar to the single pump maximum Higher fluctuation occurs at pressures below 100 psi Minimum 50 76 psi 3 5 bar Maximum system backpressure The single pump maximum Valves rated to 10 000 psi 689 5 bar Air supply source pressure 80 to 115 psi 5 5 to 7 9 bar Maximum flow rate ml min Liquids 65 of the single pump A100
72. Temperature and Pressure 1 2 12 2 4 1 Cylinder Insulating 2 12 2 4 2 Temperature Control Jacket 2 13 2 4 8 Back Pressure Regulation 2 18 2 5 Seal Options 2 2 0 nu ee oe ted uo dne ar cA a vede 2 19 Section 3 Basic Programming and Operation 3 1 Introduction etd ER a afoot AES 3 1 3 2 General Controller 3 1 3 2 1 Rates Units and Limits 3 1 3 2 2 Programming Screens 3 1 39 23 Run Screens an ille ie wann er nn rer ea AES 3 2 3 2 4 Selecting Operating 3 3 3 3 an gazon acterend ires ne daten ee gen 3 3 3 4 One sins jean Ss OE at ehe ge ES 8 8 3 4 1 Flow and or Pressure Units of Measure 3 3 3 4 2 Pump Selection if multiple pumps 2222 eee en 8 4 UA Gs di 3 4 3 4 4 Power Failure STOP 3 5 xiii D Series Syringe Pumps Table of Contents xiv 3 4 5 System Reset Restore Default Settings 3 5 3 4 6 Display Contrast
73. This page intentionally blank D Series Syringe Pumps Appendix A Replacement Parts 7 Appendix A Replacement Parts A 1 3 1000D Pump D Series Syringe Pumps OO OO A 3 qunm AL 527 e ON ET IN S en NN IR In 8 52 te I en LA AN 7 N Bi Em Si 4 N re 79 27 1000DX 1000 8 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST DWG NO 60 1242 347 SHEET 2 OF 3 PART NUMBER DESCRIPTION REV H DATE 073109 1 160 1244 334 PREAMP ASSY NITRONIC PREAMP ASSY HASTELLOY CONNECTOR 1 4 TO 1 4 NPT 316 STAINLESS STEEL 4 209 0168 09 PIPE PLUG 1 4 NPT 316 STAINLESS STEEL 1000mI PISTON ASSY NITRONIC 6 60 1243 172 1000mI SEAL RETAINER NITRONIC UPPER SEAL 8 60 1243 776 WEAR RING 9 160 1243 803 PISTON BODY NITRONIC 10 202 9990 23 LOWER SEAL 11 60 1243 721 PISTON BASE NITRONIC 69 1243 779 1000ml CYLINDER CAP SEAL 1000mI CYLINDER NITRONIC 1000mI CYLINDER HASTELLOY 1000mI PISTON ASSY HASTELLOY 16 60 1243 792 1000ml SEAL RETAINER HASTELLOY PISTON BODY HASTELLOY 19 209 0169 35 GLAND NUT 1 16 ID FERRULE 1 16 ID FERRULE 1 8 ID CABLE TIE TEFZEL RIGHT WASH TUBE LEFT WASH TUBE THRUST BEARING 60 1248 116 BALL NUT ASSY BALL SCREW ASSY THRUST BEARING INDIVIDUAL ORDER 2 EA UNIVERSAL SEN
74. be placed under inde pendent control as you must run it to return 5 10 ml of modifier back through the valve to be sure that the cylinder is free of air To properly equilibrate the pumps they must be delivering fluid When preparing your system for modifier operation if you are connecting pump A to a CO tank you will need to use the stainless steel tubing P N 60 1243 391 and appropriate connecting fittings If you do not have these fittings a cyl inder connection package P N 68 1247 043 may be ordered from Teledyne Isco Once the pressure has been zeroed and the pumps are filled you are ready to set up your modifier addition parameters You will need to place the pumps in modifier mode set the pressure limits under the limits option on the main menu and designate the percent of modifier found under pump on the run screen to be added If your modifier boils at 3 5 bar at room temperature you may want to increase the minimum pressure for pump B to prevent vapor the default minimum pressure is 3 5 bar Before operation in modifier mode zero and fill the pumps under independent control constant pressure mode Once the pumps are ready place them in modifier mode Press MENU gt MORE A gt MULTI PUMP 4 and select CONTIN MODIFIER 5 6 2 1 Mininum Modifier Pressure Setting D Series Syringe Pumps Section 6 Modifier Addition The default setting for the minimum modifier pump pressure is 50PS
75. cable Temperature control jacket assembly A Outlet tubing not supplied EU y Cylinder Inlet connector Cooling Jacket lock port 10 32 set screw k z Inlet tubing i not supplied O ring Cylinder housing Front cover Cylinder lock A 1 4 20 set screw Cover screw ax SC Figure 2 16 Temperature control jacket installation Reassembling the pump Refer to Figure 2 16 for the following steps 1 Lower the cylinder cooling jacket assembly over the piston and push rod assembly 2 17 D Series Syringe Pumps Section 2 Fluid System Connections and Accessories M Note To avoid seal damage ensure that the cylinder is aligned straight with the piston before lowering 2 Screw the assembly into the cylinder housing until the cyl inder is snug against the piston and no longer turns Unscrew the cylinder a minimum of a turn Line the inlet and outlet cylinder cap ports up as before Turn the cooling jacket ports to the desired location and lock the cooling jacket to the cylinder by tightening the set Screw 5 Lock the cylinder by tightening the lock screw Replace the front cover and adjust both covers so they are flush with the cylinder housing 7 Reinstall tubing 8 Reconnect the pump pressure transducer cable 2 4 3 Back Pressure The back pressure regulator option from Teledyne Isco reduces Regulation fl
76. char int comm_getc void BOOL GetCTS void char unitnum HANDLE hCom DCB dcbSerialParams int tmain int argc TCHAR argv console appication int commport long speed char in 512 out 512 printf Starting Program printf Enter Unit ID scanf_s d amp unitnum printf Enter Comm port scanf_s d amp commport printf Enter Baud Rate scanf_s ld amp speed fflush stdin clear stdin buffer commOpen commport speed while 1 _cputs n rString Q TO Quit gt gt gt gets_s in 200 _strupr_s in convert to upper case if in O Q break conv_das in out _cputs Dasnet Output gt gt gt puts out printf nWriting to serial port dputs out _strset_s out 256 0 dgets out printf Dasnet Response gt gt s n out 8 10 D Series Syringe Pumps Section 8 Serial Interface Table 8 5 Example ofa Visual C program to demonstrate conversion of pump commands to DASNET frames Continued CloseHandle hCom printf Comm intr released n void conv das char in char out unsigned sum char c_ptr c_ptr out out unitnum 0x30 put id first out R if stremp in R out r out 0x00 else sprintf_s out 255 3 3X 96s strlen in in for sum 0 c ptr c_ptr sum c ptr sum 0x100 sum amp OxOFF get check sum sprintf_s c_ptr 255 2 2X sum void dgets ch
77. constant pressure B 10 D Series Syringe Pumps Appendix B Continuous Flow Introduction Installation and Operation for 30D B 5 4 No Check Valve To limit fluid backflow from the pump to the supply reservoir one of two approaches is generally used Either a check valve is installed in the supply line or the NO CHECK VALVE NCV software feature is enabled on the controller The No CHECK VALVE NCV feature controls the opening of the inlet valves such that just prior to refill the pump is depres surized to a user specified value pressure point or until a user specified time out period time point This reduces pressure in the cylinder before the inlet valve is opened The NCV software feature is disabled by default however if no check valve is installed on the supply line it is recommended that this feature is enabled gt 1 Contin Const Flow 2 Contin Const Press V MORE OTHER OPTIONS MULTI PUMP NCV 1 AB Pumps 1 Pressure Point 2 CD Pumps 2 Time Point 3 Function NCV Figure B 7 Keystrokes to set up No Check Valve B 11 D Series Syringe Pumps Appendix B Continuous Flow Introduction Installation and Operation for 30D B 5 5 To Run or Stop This menu setting allows the operator to run or stop both pairs of pumps simultaneous PREVIOUS Press 3x to return to run screen B MULTI PUMP Four PUMP Run SToP Figure B 8 Keystrokes to Run or Stop the pumps M
78. cooling facilitates filling with fluids such as liquid The jacket can also be used with a circulating temperature controlled bath to keep the fluid inside the pump at a constant temperature This may be necessary when operating at very low flow rates below 500 nl min where temperature fluctuation can cause flow variations 2 13 D Series Syringe Pumps Section 2 Fluid System Connections and Accessories Table 2 6 Packages and Parts Item Description Part Number Temperature control jacket packages for 65D 65DM 100DM 100DX 2600 68 1247 047 30D 68 1267 001 500D 500HPx 68 1247 057 500SP 68 1247 115 1000D 60 5364 199 Temperature control jacket assembly 65DM 100DM 100DX 260D 60 1248 053 30D 60 1268 020 500D 500HPx 60 1248 099 1000D 60 1248 183 Key 3 socket 490 0031 54 Inlet outlet connector 2 209 0161 00 Installation procedure 60 1242 183 O ring 2 100DM 100DX 260D 202 2062 23 30D 65D 65HP 500D 202 2062 11 500HPx 1000D 202 2062 35 M Note Removing the pump For the 30D pump remove the cylinder cap assembly ONLY cylinder for 30D Do not remove the cylinder from the cylinder block 1 Run the pump until the control display shows CYLINDER EMPTY 2 Remove the fluid fittings from the sides ofthe pump cap Figure 2 13 Transducer Connector gt e Fluid Fittings I E Figure 2 13 Fluid fittings 2 14 D Series Syringe Pumps Section 2 Fluid System Conn
79. cross contamination or difficulties with incompatible fluids In comparison to other D Series pumps those with external transducers have a greater dead volume space due to transducer and tubing differences This dead volume space increases the possibility of residual liquid being held in the pump Also the external transducer may retain residual liquid Dead volumes are listed in the specification tables found in Section 1 To flush the pump remove the transducer and its tubing from the top ofthe pump N CAUTION Never immerse the transducer in solvent Using nitrogen blow out any liquid that remains inside the cyl inder transducer port and tubing WARNING Liquids expelled by compressed gasses may cause injury Wear eye protection Certain liquids also may require other personal protective equipment Refer to the applicable Material Safety Data Sheet MSDS for more information The optional accessories discussed in this section are used to make fluid connections from the pump s to another apparatus When making fluid connections that use ferrules be sure to use the ferrules provided in the kit Push the tubing completely into the connector and finger tighten Then tighten with a wrench to clamp the ferrules onto the tubing The optional manual refill kit provides a high pressure two way valve that connects to the pump inlet to a fluid reservoir The kit contains all tubing and hardware necessary for valve instal
80. feed and drain the wash gland as shown in Figure 2 5 on the following page A small pump can be used to deliver the wash fluid through one of the two tubes to rinse the cylinder and seals The second tube drains the wash fluid to waste If the system is configured to recirculate the wash fluid ensure that you change the wash fluid at regular intervals Select a wash fluid that will best flush the cylinder of any residue left by the pumped fluid yet will not damage the seals 2 5 D Series Syringe Pumps Section 2 Fluid System Connections and Accessories N CAUTION The pressure in the wash gland and line should NEVER exceed the system pressure or the wash pressure limit as labeled on the pump Units with a wash pressure limit label can be damaged if the pressure is exceeded M Note If the primary pump seal fails the pressure of the delivery fluid will be exerted on the secondary wash gland seal During operation the wash gland outlet should always be uncapped and routed for either recirculation or drainage Detailed information about pumping salt solutions and brines is available in technical bulletin TB04 Pumping Salt Solutions and Brines Drip tray outlet 5 4 1 8 Wash Gland Tubes Wash gland tubes ND 1 8 Tubing N Splash pan outlet N S Outlet Fluid Inlet Fluid LO User supplied Figure 2 5 Drain tube installat
81. from the shaft as shown in Figure 9 11 Push the shear key about 1 2 way into the worm gear Do not push it all the way in For 65DM pumps proceed to the next section For all other pump models proceed to the final steps in Section 9 12 5 Follow the step by step instructions in Section 9 12 2 Replacement Using Installation Tool or in Section 9 12 3 Replacement Without Installation Tool Then proceed with the instructions in this section The 30D and 65DM pumps have an outer bearing set not included in the other pumps The set includes two thrust washers and one thrust bearing see Figure 9 12 9 21 D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing Figure 9 12 30D and 65DM Bearing set Note that the 30D and 65DM spacer is shaped differently from that of the other pumps and must be properly oriented during reinstallation Figure 9 13 When performing shear key replacement on the 30D and 65DM pumps use care to keep the bearings in position with the bearing between the two washers while installing the spacer Proceed to the final steps in Section 9 12 5 Ball screw KA Inner bearing set not accessed Worm gear Outer bearing set Shear key Figure 9 13 80D and 65DM Shear key replacement 9 12 5 Completion of Shear 1 Slide the spacer onto the ball screw The spacer will push Key Replacement the shear key into proper position Install the castle nut on the b
82. front panel except that pump remains under remote serial control UNITSA Enter the desired flow or pressure units after the equal sign Acceptable values are BAR KPA PSI ML MIN ML HR UL MIN UL HR Sets all pumps Return the volume remaining in cylinder in ml Format is XXX XXXX ml VOLTOT Returns the total volume delivered when using continuous flow or modifier VOLTOTCD VOL RESET Will reset the volume total to zero VOL RESETCD Zeros the pressure sensor offset ZERODIFF1 Zeros the pressure sensor offset for the respective analog input ZERODIFF2 ZERODIFF3 NOTE 1 The analog input range is 1 5 to 11 6 volts There is NO conversion of the returned number The number returned 0 to 65535 decimal will have an offset of 7500 added to the number 7500 0 volts and a scale of 5000 for every 1 volt for example number 7500 volts 32500 7500 5000 5000 vols NOTE 2 The only pump B commands accepted in continuous pumping mode or modifier addition mode are B FLOWB LIMITSB PRESSB REFILLB REFILLB STATUSB VOLB 8 8 1 Get Status Command The G and G amp serial commands retrieve information from the pump controller Each command returns a text string which can be read as shown in Figures 8 3 and 8 5 8 25 D Series Syringe Pumps Section 8 Serial Interface R046 237510 00128 01017 06981 05743 00421 00442 00449 11111000 CS l Pressure Pump
83. gas to quickly dissipate away from the pump cyl inder area and to reduce the amount entering the motor compartment e Seal the syringe pump motor compartment with tape and purge it with a con tinuous flow of nitrogen N gas This will also reduce the possibility of accu mulating an explosive mixture around the motor and relays For further information telephone Teledyne Isco at 800 775 2965 or fax 402 465 3085 to consult the Teledyne Isco Service Department USE THE Teledyne Isco SFE SYSTEM AND SYRINGE PUMPS IN THESE POTENTIALLY HAZARDOUS APPLICATIONS AT YOUR OWN RISK 5 97 D Series Syringe Pumps Warnings Cautions and Notices AVERTISSEMENT D EXPLOSION AVERTISSEMENT Les pompes de Serie D Teledyne Isco et l extracteur SFX 2 10 SFX 220 et SFX 3560 ne sont pas l preuve d explosion Remarque de s ret concernant l usage d un fluide inflammable avec les pompes seringue d Isco S rie D et le systeme SFX Le syst me SFX et pompes seringue Teledyne Isco doivent tre plac es l int rieur d une hotte chimique fonctionnelle quand vous utilisez thane ou tout autre gaz inflammable Assurez vous que toute la tuyauterie SFE est compl tement scell e avec aucune fuite de gaz en ex cutant une preuve de fuite en utilisant du Cette m thode est d taill e la partie 2 du man uel de la pompe S rie D et la partie 2 du manuel SFX 2 10 SFX 220 et 3560 Il faut absolument
84. gee alge ere 9 11 9 7 2 Controller ic nr eek ere er E qu xe pre Roe RR 9 11 9 8 Gubrication ass ern MENOR ART he PAIN 9 12 9 81 Ball N t ouo ue e es orn M abe see d Ug e es 9 12 9 9 Seal Cleaning and 1 9 13 9 9 1 Piston Seal Excludes 30D seg Room als Rache e eae 9 14 9 9 2 Piston Seal Break In Aqueous seals 9 14 9 9 3 All other piston seals senen eee ee 9 15 9 9 4 Wiper Seal Excludes 30D ene eee eee 9 15 9 10 Wear Ring Cleaning and Replacement 9 17 9 11 Flushing the 9 17 9 11 1 Gas Solvent Changeover 9 17 9 11 2 Liquid Solvent Changeover and Flushing 9 18 9 12 Overpressure Conditions 9 18 9 12 1 Shear Key 2 hfe vie eo teen SEDI cr 9 19 9 12 2 Replacement Using Installation 9 20 9 12 3 Replacement Without Installation Tool 9 21 9 12 4 Pump Bearings 30D and 65DM 9 21 9 12 5 Completion of Shear Key Replacement 9 22 9 13 Motor Br ushes re waer ma E S E SC Be gated 9 23 9 13 1 Motor Brush Disassembly
85. it will be polled again If after three attempts at polling it does not reply it will be dropped from the polling rotation When the instrument does respond the polling rotation does not advance until an error free transfer has occurred The frame format for data transfers from the network controller is as follows destination acknowledgement message source length message checksum CR e The destination is the 1 digit unit identification number of the instrument to receive the message Examples Hexadecimal Format Using MODULO D Series Syringe Pumps Section 8 Serial Interface Acknowledgment is one character to indicate the success of the previous transmission There are three possibilities 1 E means error resend the message immediately E is sent by the network controller only Other units signify errors by not replying causing the controller to resend the message 2 B means busy resend message at next poll 3 R signifies previous message was received Message source is the unit ID of the unit that origi nated the message If there is no message this location is a space 20H Length is the length of the message in 2 digit hexadecimal format Maximum length is 256 with 256 being represented by a 00 This field is eliminated if there are no messages Message field is the area where the actual information is located The maximum length is 256 characters long Checksum is also a 2 digit hex
86. lation Kit components and connections are shown in Figure 2 7 1 To attach the two way valve to the pump housing use the valve spacer block and screws provided a For the 500D pump screw the male adapter into the inlet port of the pump 2 Connect the pre bent stainless steel tubing from the valve to the pump inlet Use the nut and ferrule to connect the tubing at the inlet and the valve fittings to connect the tub ing at the valve 3 Connect the PTFE refill tubing with the filter to the port of the two way valve using the nuts and ferrules supplied nut ferrule to pre bent 7 system SST tubing PTFE tubing stainless steel tubing filter Figure 2 7 Refill hit installation 2 3 2 Manual Outlet Valve Kit Kit installation D Series Syringe Pumps Section 2 Fluid System Connections and Accessories M Note spacer block valve When connecting to pressurized sources in supercritical fluid applications use the stainless steel tubing without a filter An in line filter is contained in the connection package refer to Section 2 3 3 Table 2 2 Manual Refill Kits Pump Model Part Number 1000D 68 1247 117 500D 68 1247 083 65DM 100DM DX 260D 68 1247 077 60 1247 180 65D 68 1247 127 NDANGER RISK OF INJURY THIS EQUIPMENT PRODUCES HAZARDOUS PRESSURES PLEASE UTILIZE APPROPRIATE TUBING AND CONNECTIONS AS NOTED IN THE MANUAL The optional manual
87. limits LOCAL Returns the instrument to local control Front panel control is enabled and all motors are stopped if control was previously remote MAXFLOWA MAXFLOWB MAXFLOWC MAXFLOWD Enter to designate the maximum flow rate setpoint MAXFLOWA MAXFLOWB MAXFLOWC MAXFLOWD Returns the maximum flow rate setpoint MAXPRESSA MAXPRESSB MAXPRESSC MAXPRESSD 8 22 Enter to designate the maximum pressure setpoint D Series Syringe Pumps Section 8 Serial Interface Table 8 6 Serial Commands Continued Command Description MAXPRESSA MAXPRESSB MAXPRESSC MAXPRESSD Returns the maximum pressure setpoint MFLOWA MFLOWB MFLOWC MFLOWD Enter to designate the maximum flow limit in constant pressure mode MFLOWA MFLOWB MFLOWC MFLOWD Returns the maximum flow limit setpoint MINFLOWA MINFLOWB MINFLOWC MINFLOWD MINFLOWA MINFLOWB MINFLOWC MINFLOWD MINPRESSA MINPRESSB MINPRESSC MINPRESSD Enter to designate the minimum flow rate setpoint Returns the minimum flow rate setpoint Returns the minimum pressure setpoint MINPRESSA MINPRESSB MINPRESSC MINPRESSD Returns the minimum pressure setpoint MODE MODE A P B P C P D P A B C D refer to the pump connection P Constance Pressure F Constant Flow R Refill PG Pressure Gradient F1 Flow Gradient 1 Pump F2 Concentrated Gradient 2 Pump CF Con
88. min for any pressure up to 689 bar 0 3 of setpoint maximum 0 25 l min seal leakage FLOW RATE DISPLAY RESOLUTION 0 01 ul min 1 0 ul min in Constant Pressure Mode ANALOG OUTPUT ACCURACY x 196 of selected range DISPLACEMENT RESOLUTION 2 55 nl step REFILL TIME 1 7 minutes REFILL OR DEPRESSURIZATION RATE PRESSURE RANGE PRESSURE ACCURACY 0 01 ul min to 40 ml min at any pressure from 0 to 689 bar 0 6895 to 689 bar 0 5 of full scale at constant temperature x 0 196 FS optional PRESSURE REPEATABILITY 0 5 of full scale within 48 hours at constant temperature ZERO PRESSURE DRIFT 0 25 of full scale within 48 hours at constant temperature PRESSURE DISPLAY RESOLUTION AMBIENT TEMPERATURE RANGE 6 895 kPa 5 to 40 C TEMPERATURE DRIFT 0 12 of full scale C HUMIDITY 95 maximum DEAD HEADSPACE VOLUME 1 30 0 020 ml POLLUTION DEGREE INSTALLATION CATEGORY MAXIMUM ALTITUDE Underwriters Laboratories UL has certified all D Series Pumps with the exception of the 100 VAC versions Using water at 137 9 bar and a temperature controlled environment at 30 C The analog output is an optional accessory Pressure repeatability specification is based upon re zeroing pressure transducer every 48 hours Refer to sub section ZERO PRESS in Section 3 of the manual for re zeroing procedure e Volume in and above the piston seal hea
89. misuse accident or lack of proper maintenance This warranty does not cover products not sold under the Teledyne Isco trademark or for which any other warranty is specifically stated No item may be returned for warranty service without a return authorization number issued by Teledyne Isco This warranty is expressly in lieu of all other warranties and obligations and Teledyne Isco specifically disclaims any warranty of merchantability or fitness for a particular purpose The warrantor is Teledyne Isco 4700 Superior Lincoln NE 68504 U S A This warranty applies to the USA and countries where Teledyne Isco does not have an authorized dealer Customers in countries outside the USA where Teledyne Isco has an authorized dealer should contact their Teledyne Isco dealer for warranty service Before returning any instrument for repair please call fax or e mail the Teledyne Isco Service Department for instructions Many problems can often be diagnosed and corrected over the phone or by e mail without returning the instrument to the factory Instruments needing factory repair should be packed carefully and shipped to the attention of the service department Small non fragile items can be sent by insured parcel post PLEASE BE SURE TO ENCLOSE A NOTE EXPLAINING THE PROBLEM Shipping Address Teledyne Isco Attention Repair Service 4700 Superior Street Lincoln NE 68504 USA Mailing Address Teledyne Isco PO Box 82531
90. no aparelho ou ferimentos parao operador necessario que o utilizador tenha um conhecimento completo da lingua inglesa e dos respectivos termos t cnicos ou seja treinado por uma pessoa que tenha esse conhecimento antes de operar com este aparelho Tia Tnv anoduyn BAaBns Tov opyavov N yprnotn ELVAL o XPNOTNG va yvaop da tny ayyuka yAoooa Ka oc OX TIKOUG t VIKOUG N VA EKTOL EDTEL ATO OTOLO EXEL TPOVHOLUEVOG EPYAOTEL GTO OPYAVO ALTO gt gt gt gt gt gt C Figyelmeztet s k sz l k meghib sod s nak valamint a kezel s r l s nek megel z se rdek ben a felhaszn l nak felt tlen l rtenie kell az angol nyelvet ezen bel l a m szaki kifejez seket vagy pedig a haszn latba v telt megel z en a k sz l k kezel s ben m r gyakarlott szem ly ltal t rt n betanit s sz ks ges D Series Syringe Pumps Warnings Caution
91. of the 500D which has wrench flats use a spanner wrench with an 1 8 pin of appropriate size or the proper tool from the Isco wrench package in the round hole on the side of the piston Teledyne Isco has piston wrench tools which are also included in the wrench packages for each model of pump Refer to Table 9 3 on the following page Table 9 3 Piston Wrench Tools Pump Model Part Number Piston wrench tool 69 1243 905 Wrench package 60 1247 130 Refer to the 30D Seal Replace ment Instruction included in the seal replacement kit Wrench package 60 1249 132 100DM 100DX Piston wrench tool 69 1243 888 Wrench package 60 1247 067 260D Piston wrench tool 69 1243 889 Wrench package 60 1247 067 500D Piston wrench tool 69 1243 890 Wrench package 60 1247 068 500HPx 1000D Piston wrench tool 69 1243 788 Wrench package 60 1247 093 4 Use the tool to twist the piston loose then unscrew it by hand Remove the retaining ring 500D only and wiper retainer then lift off the wiper seal Being careful not to scratch any sealing surfaces gently break free any solids from the seal and piston Rinse all the solids away with distilled water Install the piston seal onto the retainer with the spring ori ented towards the retainer Install the wiper seal onto the piston base with the spring facing down M Note In the Model 1000D pump and the 500D with wash gland option the wiper seal
92. outlet valve kit provides manual control of the pump outlet port by connecting a shutoff valve between the pump and the rest of the system 1 Attach the two way valve using the spacer block and pan head screws a For the 500D pump screw the male adapter into the pump outlet Connect the pre bent length of stainless steel tubing to the outlet port on the pump using the nut and ferrule Connect the other end to the top port on the valve using the valve fitting M Note For the 500D this piece of tubing should be cut to the proper length for connection to your system Due to the wide variety of applications for this model fittings to connect the tubing to your system are not provided in the kit D Series Syringe Pumps Section 2 Fluid System Connections and Accessories M Note When nuts are torqued to the cylinder cap ports the pressure reading may be affected If the pressure no longer reads zero release the pressure in the cylinder and press ZERO PRESS 3 Use the valve fittings to attach stainless steel tubing to the top port ofthe two way valve a For models 65DM 100DM DX and 260D connect the reducing union to the other end of this tubing 4 Connect the stainless steel tubing between the valve s bot tom port and your apparatus Cut to the desired length Table 2 3 Manual Outlet Valve Kits Pump Model Part Number nutferrule Y male adapter 500D A stainless steel tubing 1000D 68 1247 118
93. pumps are stopped 2 Close the pump B outlet valve and open the pump B inlet valve 3 Press REFILL Press softkey B to designate that pump B is the active pump the pump being refilled Pump B will fill with modifier 4 After pump B has filled press run and deliver 5 10 ml of modifier back through the inlet valve to ensure all air is purged from the pump before pressing stop 5 Close the inlet valve M Note When using the pumps with liquefied make sure you pur chase CO in a dip tube CO tank 1 Place the pumps in independent control constant pres sure mode as detailed above 2 Be sure the pumps are stopped 3 Close the pump A outlet valve before opening the tank sup ply valve and pump A inlet valve 4 Press REFILL Press softkey A to designate that pump A is the active pump the pump being refilled Pump A will fill with pressurized fluid 5 After pump A has refilled wait 15 seconds before closing the tank supply valve and pump A inlet valve Pump A delivers supercritical fluid while pump B meters mod ifier Both fluids pass through one way check valves before they meet and are blended together in a mixing tee Modifier concen trations of up to 100 percent v v are programmable via the con troller If higher concentrations are needed put the modifier in pump A to be delivered as the primary fluid Both pumps operate in constant pressure mode and will flow up to their maximum rate
94. return to the main menu press RETURN D UNITS 4 POWER FAILURE STOP SELECT PUMP 5 SYSTEM RESET REFILL 6 DISPLAY CONTRAST MORE RETURN Figure 3 1 Menu 1 program selections 3 4 1 Flow and or Pressure Units of Measure Figure 3 2 Units menu Displayed units are user selectable by selecting menu 1 item 1 PRESSURE UNITS FLOW UNITS 1 ATM 3 PSI 5 mL MIN 7 uL MIN 2 BAR 4 kPA 6 mL HR 8 uL HR PREVIOUS A B C D 3 3 D Series Syringe Pumps Section 3 Basic Programming and Operation 3 4 3 4 2 Pump Selection if multiple pumps 3 4 3 Refill To set auto refill volume To set refill rate Disable Enable auto refill Use numbers 1 4 to select the pressure units ATM BAR PSI kPa The units selected will be displayed on the first line after PRESSURE UNITS Use numbers 5 8 mL MIN mL HR uL MIN uL HR to set the flow rate units The selected units will be displayed on the first line after FLOW UNITS If multiple pumps are connected to a single controller the SELECT PUMP option selects the pump A B C or D whose current state and settings appear on the display The letter of the current pump will appear in lower case in the upper left corner of the run screen When multiple pumps are connected the UNITS selected for one pump will apply to all of the pumps The refill option allows you to set the refill rate or set the pump to automatically refill when a certain volume i
95. set point for Pump D in Constant Pressure mode Pa PSI See 7 7 D Series Syringe Pumps Section 7 Modbus Configuration Table 7 6 Holding Registers Continued of Register Registers Description Pressure set point for multi pump pair AB in Continuous Flow Constant Pressure mode ATM BAR kPa PSI See NOTE 1 Pressure set point for multi pump pair CD in Continuous Flow Constant Pressure mode ATM BAR kPa PSI See NOTE 1 Flow rate set point for Pump A in Constant ow mode min ml hr ul min ul hr See NOTE 2 ow rate set point for Pump B in Constant ow hoile min ml hr ul min ul hr See NOTE 2 F F F Flow rate set point for Pump C in Constant Flow mode F F F C ml min ml hr ul min ul hr See NOTE 2 ow rate set point for Pump D in Constant eh ml hr ul min ul hr See NOTE 2 ow rate set point for multi pump pair AB in ontinuous Flow Constant Flow mode min ml hr ul min ul hr See NOTE 2 Flow rate set point for multi pump pair CD in Continuous Flow Constant Flow mode ml min ml hr l min uhr See NOTE 2 ml hr ul min ul hr See NOTE 2 ml hr ul min ul hr See NOTE 2 ml hr ul min ul hr See NOTE 2 Refill flow rate for Pump D ml hr ul min ul hr See NOTE 2 Maximum pressure set point for Pump A ATM BAR kPa PSI See NOTE 1 Maximum pressure set point for Pump
96. such that the implied length is incorrect Does NOT mean data value is outside the expectation of the controller Illegal Data Value 7 3 D Series Syringe Pumps Section 7 Modbus Configuration Table 7 5 Coils Register Address i Description 0 Stop Pump A 1 Run Pump A 0 Stop Pump B 1 Run Pump B 0 Stop Pump C 1 Run Pump C 0 Stop Pump D 1 Run Pump D Link Run Stop operation of multi pump pair AB amp multi pump pair CD 0 Disable 1 Enable 0 Stop Pump A if in Refill 1 Run Pump A in Refill 0 Stop Pump B if in Refill 1 Run Pump B in Refill 0 Stop Pump C if in Refill 1 Run Pump C in Refill 0 Stop Pump D if in Refill 1 Run Pump D in Refill Pump A in Constant Pressure mode wl rm Pump B in Constant Pressure mode 1 Pump C in Constant Pressure mode Pump D in Constant Pressure mode Pump A in Constant Flow mode 2 3 4 015 Pump B in Constant Flow mode 016 Pump C in Constant Flow mode 1 Pump A amp Pump B in MEDIEN mode 1 Pump A amp Pump B in Continuous Flow Constant Pressure mode 1 Pump A amp Pump B in Modifier addition mode 1 Pump A amp Pump B amp Pump C in Continuous Modifier addition mode co 1 Pump C amp Pump D in Independent mode 1 Pump C amp Pump D in Continuous Flow Constant Flow mode 1 Pump C amp Pump D i
97. the system a Fill both pumps completely by pressing REFILL and selecting each pump to fill b Route the outlet to waste or reservoir and press RUN Press STOP when fluid comes out of the outlet c Open the valves to atmosphere by pressing ACC CTRL then selecting each valve to open d Zero the pressure in each pump by pressing ZERO PRESS and selecting each pump to zero e Connect the outlet tubing and fill each pump once more 3 Reset total volume see Figure 5 9 5 21 D Series Syringe Pumps Section 5 Continuous Flow Introduction Installation amp Operation 5 22 Liquefied Gases Checklist 1 Equilibration When the pumps begin running the system will go through an equilibration phase during which both pumps Open the valves to atmosphere by pressing ACC CTRL then selecting each valve to open Zero the pressure in each pump by pressing ZERO PRESS and selecting each pump to zero Fill both pumps completely by pressing REFILL and select ing each pump to fill Pressurize both pumps by pressing RAPID PRESS Maximum flow rate and target pressure value will be displayed Press D to continue pressurization Reset total volume see Figure 5 9 must be full and delivering fluid Additional guidelines Please become familiar with the fol lowing guidelines Pressure limits for continuous constant flow mode are set by the limits of pump A for the A B pair and pump C for the C D pair
98. the three stant equipment ote profes jan surrounding in Cof qam Research to i Qo ado one eat ty of Color peddin doing a gr university and much often mixed such others of nitroV umes larger V vii D Series Syringe Pumps Warnings Cautions and Notices viii CAUTION Avoid spills Liquids associated with this instrument may be classified as carcinogenic biohazardous flammable or radioactive Should these liquids be used itis highly recommended that this application be accomplished in an isolated environment designed for these types of materials in accordance with federal state and local regulatory laws and in compliance with your organization s chemical hygiene plan in the event of a spill In all cases when using Teledyne Isco instrumentation prudence and common sense must be used WARNING Pinch point This symbol warns you that your fingers or hands will sustain serious injury if you place them between the moving parts of the mechanism near this symbol WARNING Avoid hazardous practices If you use this instrument in any way not specified in this manual the protection provided by the instrument may be impaired this will increase your risk of injury CAUTION Liquids associated with this instrument may be classified as carcinogenic biohazardous flammable or radioactive Should these liquids be used it is highly recommended that this application be accomplish
99. the worm and worm gear Do not substitute 9 8 1 Ball Nut The ball screw which drives the ball nut must be kept lubricated with Never seez 1 Remove the case top as detailed in section 9 6 and front cover to gain access to all parts requiring lubrication 9 12 9 9 Seal Cleaning and Replacement D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing 2 3 To lubricate the ball nut run the pump until the ball nut reaches its maximum height Apply two beads of lubricant on opposite sides ofthe ball screw down its entire length The precision thrust bearing at the base of the ball screw refer to Figure 9 8 is factory lubricated and should not need re greasing Before cleaning or replacing the piston or wiper seals the cyl inder must first be emptied M Note 30D has its own set of seal replacement instructions which are included in the seal replacement kit The following instructions do not apply to the 30D The 30D uses a special tool including in the kit that is necessary for the seal replacement N CAUTION Handle with care Never let surfaces of seals piston or cylin der come into contact with abrasives or fingernails Tools required 14 and ls Allen wrenches 2 Phillips screwdriver Wrench set from maintenance kit Never Seez lubricant from accessory package Run the pump until empty CFa 0 000mL MIN OPSI 0 CYLINDER EMPTY 204 000mL MIN FLOWRATE
100. two locat ing pins install the three screws and three flat washers to hold motor in place and tighten the screws Figure 9 23 At this time verify that the small flat support plate is still in place under the motor assembly and is aligned with the holes in the motor mounts Figure 9 25 Lay the pump on its side and align the flat support plate with the two holes in the bottom of the case then install the two screws with two lock washers into the bottom of the motor plate and tighten screws Figure 9 20 top mid dle screws While the pump is still on its side align the circuit board assembly so the three mounting holes in the bottom of the case line up with the three mounting holes on the circuit board assembly and install the three screws with three lock washers but do not tighten at this time Figure 9 20 Set the pump upright and check the following Check that there are no pinched wires under the circuit board assembly Check that the ferrite beads are not pinched between the motors and the fan Check that the ferrite beads are not pinched between the motor plate and the bearing plate 9 33 D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing Make are not pinched in these areas Figure 9 35 Motor plate and bearing plate 8 Figure 9 36 Installing the deflector shield 10 11 12 9 34 sure the ferrite beads Once it has been determined that al
101. uninter rupted it has a logic 0 Therefore Top 0 Bottom 1 Cylinder is full Top 1 Bottom 0 Cylinder is empty Top 1 Bottom 1 Illegal state An illegal state can indicate failure of one or both sensors The controller display will toggle immediately between CYLINDER FULL and CYLINDER EMPTY when you press REFILL or RUN the pump will not run Flag Sensor Figure 9 4 Optical sensor interrupted by flag bottom sensor shown rear tower cover plate removed Select the pump to be tested A B or C TRAVEL LIMIT SENSE AND MOTOR POSITION Upper limit 0 Lower limit 0 Tach counter Up 100 Down 100 Exit Press UP 100 A or DOWN 100 B to move the piston up or down 100 counts The tach counter value will increase or decrease by 100 counts accordingly When the ball nut assembly reaches the top or bottom of the tower the corresponding limit will change from 0 to 1 If the cylinder was refilled using the REFILL button 9 7 D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing it may require multiple presses of the UP 100 softkey before the Lower Limit indicator changes to 0 When the Lower Limit indi cator is 1 pressing the DOWN 100 softkey will have no effect Ifthe rear tower cover plate is removed to expose the sensors as shown above in Figure 9 4 you can simply interrupt the sensors with a slip of paper rather than using the flag If eithe
102. voltage Complete instructions for this feature are provided in Sections 3 12 through 3 12 5 One controller can control up to four pumps at once either together or independent of each other Complete information about using the MULTI PUMP feature is pro vided in Section 3 9 and Section 5 6 This option resets the total volume display of multi pump pair AB or multi pump pair CD to zero when operating in continuous flow or modifier mode 1 AB PUMPS 2 CDPUMPS 3 AB AND CD PUMPS 3 5 6 Valve Electric Vale Check Valve Figure 3 6 Types of valves D Series Syringe Pumps Section Basic Programming and Operation This feature identifies the type of valves passive active air active ball air or electric being used for the flow operation Valves are set to active by default If active valve active ball valve or electric is selected the controller will match the pressure more closely before switching delivery pumps If active ball valve is selected the controller will have a timed delay after valve open closure before switching delivery pumps This delay is to accommodate the slower opening closing ball valves The number for the selected valve type will be blinking Press 1 2 3 or 4 to select the correct valve type The 30D pump has manual valve kits part number 60 1247 180 and 60 1247 181 Air Valve Ball Valve 3 7 D Series Syringe Pumps Section 3 Basic Progr
103. zero release all pressure inside the pump then press ZERO PRESSURE on the front panel of the controller to readjust The tubing must be cut squarely to prevent possible problems Square ends are easier to insert through the ferrule and will decrease dead volume Electrochemically machined steel tubing should be used throughout the plumbing system Electrochemically machined tubing has flat burr free ends and is free of cutting residues This tubing is available pre cut through many chromatographic supply distributors in assorted lengths A less desirable alternative is to purchase a tubing cutter designed to handle steel tubing For quick fixes the tubing may also be cut by hand D Series Syringe Pumps Section 2 Fluid System Connections and Accessories N CAUTION Wear goggles to perform the following procedure Tools required Fine jewelers file goggles and two pairs of pliers 1 Using the jewelers file score the tubing around its entire circumference 2 Secure the tubing with pliers on either side of the score line with approximately 1 5mm between each pair of pliers and the score line Do not squeeze the tubing too tightly as this will flatten or deform its exterior 3 Bend the tubing back and forth to crack it at the score line 4 It may be necessary to deburr the outer tubing ends with the file Make sure the tubing ends are clean and the inner bore is clear before installing the cut tube M Note It i
104. zip folder Extract the sub folder named Remote Pump 8 7 D Series Syringe Pumps Section 8 Serial Interface Table 8 3 Example of BASIC program to demonstrate conversion of pump commands to DASNET frames 1 CLS Z PRINT INPUT ALL ENTRIES IN CAPITAL LETTERS 5 INPUT INPUT UNIT ID gt gt UNITNUM GET UNIT NUMBER 30 REM OPEN COM PORT SET FOR COM2 EDIT TO COMI IF NEED 40 OPEN COM2 1200 N 8 1 ASC FOR RANDOM AS 2 50 PRINT INPUT ENTER STRING HIT TO EXIT gt gt I GET OUTPUT STRING FROM USER 65 IF I THEN GOTO 50 BLANK INPUT THEN GO BACK 70 IF I THEN GOTO 200 Q INPUT THEN QUIT 80 GOSUB 10000 CONVERT STRING TO DASNET FORMAT 90 GOSUB 20000 OUT DASNET STRING TO COM 2 120 PRINT DASNET FORMATTED CMD gt gt O OUTPUT FORMATTED CMD TO USER 124 PRINT PRINT gt gt gt gt PRESS CTRL C IF NO RESPONSE FROM PUMP lt lt lt lt 125 LINE INPUT 2 Z GET RESPONSE FROM PUMP CR ENDS STRING 127 PRINT DASNET RESPONSE gt gt Z PRINT RESPONSE 1287 CLEAR BUFFER 130 GOTO 50 GO BACK 200 CLOSE 2 CLOSE COM2 210 SYSTEM END PROGRAM AND EXIT TO DOS 10000 REM this SUBROUTINE will convert a string I into a string O 10005 REM in DASNET protocol 10015 REM UNITNUM UNIT NUMBER OF PUMP 10020 REM AFTER THE STRING IS SENT TO PUMP A CR IS REQUIRED TO TERMINATE MESSAGE 10030 REM VAR USED 0 1 IL Y LLSUM CSUM UNITNUM 10100 O CHR ASC 0 UNITNUM PU
105. 0 C TEMPERATURE DRIFT 0 015 of full scale C HUMIDITY 95 maximum DEAD HEADSPACE VOLUME 1 30 0 020 ml POLLUTION DEGREE INSTALLATION CATEGORY MAXIMUM ALTITUDE Underwriters Laboratories UL has certified all D Series Pumps with the exception of the 100 VAC versions Using water at 137 9 bar and a temperature controlled environment at 30 C The analog output is an optional accessory Pressure repeatability specification is based upon re zeroing pressure transducer every 48 hours Refer to sub section ZERO PRESS in Section 3 of the manual for re zeroing procedure e Volume in and above the piston seal head clearance at automatic shutoff and inlet and outlet ports to the fittings 1 3 D Series Syringe Pumps Section 1 Introduction Table 1 3 65DM Technical Specifications CYLINDER CAPACITY 67 97 ml POWER REQUIREMENTS Mains voltage line cord is a Disconnect Device 100 10 VAC 1 5 A maximum 117 12 VAC 1 5 A maximum 234 x 23 VAC 0 75 A maximum eactory Set LINE FREQUENCY 50 or 60 Hz LINE VOLTAGE NOISE TOLERANCE 1 7 x nominal rms line voltage 10 usecond pulses any phase angle random or repetitive DIMENSIONS PUMP CONTROLLER 27 18 cm 27 18 cm 45 0 cm 30 48 cm 103 0 cm 13 59 cm Width Depth Height WEIGHT PUMP CONTROLLER 33 2 kg 2 96 kg FLOW RATE RANGE FLOW RATE ACCURACY 0 01 pl min to 30 ml
106. 00 4 2 Electrostatic Discharge Level 2 4kV contact discharge A 2009 Level 3 8kV air discharge A EN61000 4 3 Radiated RF Immunity 80 MHz to 2 7GHz 8096 AM at 1kHz A 2010 Level 1 10 V m EN61000 4 4 Electrical Fast Transient on Mains Level 2 2kV on AC lines A 2010 and I O EN61000 4 5 Surge on AC Lines 2kV common mode 1KV differential mode A 2005 EN61000 4 6 Conducted RF on AC Mains and 150 kHz to 80 MHz 3V rms 8096 modulated A 2008 VO EN61000 4 11 Voltage Dips Short Interruptions 0 5 cycle each polarity 100 A 2004 EN61000 3 2 AC Harmonic Flicker Pass 2009 3 3 2008 CISPR11 RF Emissions Radiated below 1 Group 1 Class A Industrial Scientific and Pass EN 55011 2009 GHz and Conducted AC Mains Medical Equipment I the undersigned hereby declare that the design of the equipment specified above conforms to the above Directive s and Standards as of February 13 2015 Vikas V Padhye Ph D Executive Vice President Teledyne Isco 4700 Superior Street Lincoln Nebraska 68504 Phone 402 464 0231 Fax 402 464 0318 60 1262 111 Rev A TELEDYNE ISCO Everywhereyoulook Pi mUB SERE VI SUISSES Name and amount of Hazardous Substances or Elements in the product HET X BE ER Hazardous Substances or Elements Component Name Fre TMB 219 14 Pb Hg Cd Cr VD PBB
107. 00D pump 5 6 5 3 Air valve installation for 65DM 100DM DX 260D and 500D pumps 5 9 5 4 Air valve installation for 500HPx pumps 5 10 5 5 Air valve installation for 1000D pump 5 11 5 6 Air valve installation for 65D pump 5 12 5 7 Electric valve installation 5 15 5 8 Keystrokes to specify valve type 5 18 5 9 Keystrokes to reset volume 5 18 D Series Syringe Pumps Table of Contents 5 10 Keystrokes to set up constant flow 5 19 5 11 Keystrokes to set up constant pressure 5 19 5 12 Keystrokes to set up No Check Valve 5 20 5 13 Keystrokes to Run or Stop the 5 21 6 1 Modifier addition kit installation Two pump configuration 6 2 6 2 Modifier addition kit installation continuous flow 6 3 6 3 Minimum modifier pressure screen 6 7 7 1 RS 485 Connection stii eene eee een hmm n 7 1 8 1 Serial network connection example Single connection 8 4 8 2 Serial network connection example Dual 8 4 8 3 Get Status String
108. 020 198 Figure 8 2 Serial network connection example Dual connection 8 4 3 Three or More UNIT 2 1200 BAUD EJ Tuus B mm RS 232 C MP CI A PUMP SS If additional instruments are to be connected in series use the Controllers Compiler daisy chain cable 68 1020 180 This cable is attached to the required remaining connector on the Y cable Figure 8 2 and then to the RS 232 C connectors on the rear panels of the additional con trollers 8 4 8 5 Serial Control Check List 8 6 Controller Setup 8 6 1 Restore Defaults if desired 8 6 2 Change Defaults D Series Syringe Pumps Section 8 Serial Interface In order to build and operate a custom program for Isco syringe pumps you must have the following 1 Ao a pm 8 Sample program Isco LabView toolkit LabView Compiler purchased separately Connection cable s 1 controller cable 480 7996 00 2 controllers cable 68 1020 198 3 to 7 controllers cables 68 1020 198 and 68 1020 180 Source code serial commands in computer language for DASNET conversion DASNET serial driver The toolkit comes with directories for two different versions of LabView Copy the zip files onto your computer The files within each directory are as follows labview8 5 labview5 8 2 CONTROL LLB CONTROL LLB DASNET DLL DASNET DLL DATA LLB DATA LLB ISCO1 LLB ISCO1 LLB ISCO2 LLB ISCO2 LLB ISCO3 LLB ISCO3 LLB
109. 0D 265 2 maximum rate A500HPx 265 2 A500D 132 6 A260D 69 55 A100DX 32 50 A100DM 16 25 A65DM 19 50 A65D 16 25 Liquefied gases 45 of the single pump maximum rate Cylinder cooling jack ets should be used to obtain this rate Temperature range 0 to 40 C Wetted materials in valve packages Air valves Hastelloy PEEK and PTFE Check valves SS316 sapphire ruby PEEK PTFE Tubing and fittings SS316 gold 5 3 1 Dual Air Valve To install the air valve package refer to Figure 5 3 5 5 or 5 6 Installation depending on your pump model 1 Position the valve bases 1 3 cm apart 2 Use the plugs to stopper the ports which will not be con nected 5 7 D Series Syringe Pumps Section 5 Continuous Flow Introduction Installation amp Operation Plumbing connections NDANGER RISK OF INJURY THE PRESSURE PRODUCED COULD BE 700 BAR PLEASE UTILIZE APPROPRIATE TUBING AND CONNECTIONS NOTED IN THE MANUAL 3 Loosely attach the tubing lengths from the valve assembly to the pumps 4 Allow the bracket to hang vertically place the straps around the pressure transducer caps Tighten the wing nuts 5 Install the four panhead screws on bottom of the bracket 6 Tighten the tubing nuts 7 Connect the inlet tube to the supply reservoir Connect the outlet tee to your apparatus D Series Syringe Pumps Section 5 Continuous Flow Introduction Installation amp Operation Optional reducing Optional reducin
110. 1 8 1 A INLET 2 A OUTLET 3 B INLET 4 B OUTLET 5 C INLET 6 C OUTLET 7 D INLET 8 D OUTLET to toggle the desired valve open or closed Numbers 1 8 represent digital output terminals 1 8 respectively To exit press PREVIOUS D The ZERO PRESSURE key will correct pressure sensor drift Before pressing ZERO PRESS the pump should have port fit tings installed and be depressurized 1 2 Press ZERO PRESS The display will show the current pressure and ask if you want to zero the pressure Press A B C or D to zero the desired pump or If the pump is not depressurized press DO_NOT D to exit the zero pressure operation If four pumps are connected press the STORE RECALL OR CLEAR ENTRY key When using multiple pumps there are four multi pump oper ating modes of delivery and one independent mode Continuous flow in constant flow mode Continuous flow in constant pressure mode Modifier addition in constant pressure mode Modifier addition in continuous flow constant pressure mode Independent mode 3 13 D Series Syringe Pumps Section 3 Basic Programming and Operation M Note The 30D pump cannot be used in multiple pump modes Please contact the factory for details 3 9 1 Multi Pump Operation A D Series continuous flow pumping system in constant flow mode will consist of two syringe pumps and a valve package all regulated by one controller Installation and operating instruc tions for this sy
111. 1 K102 RLY SPDT 24VDC 10A 400 0151 01 CR104 CR105 CR106 CR108 400 0154 01 113 114 MUR1515 DIO 1N5401 400 0914 00 101 DIO 1N914 400 2152 22 102 CR103 CR107 DIO 1N5242B 401 0008 00 109 KBU8D 401 0150 00 110 CRI CR112 CR115 402 0237 00 0105 0105 DIO 1N5060 XSTR 2N3702 402 0237 01 ano Qt XSTR 2N3704 402 0640 00 0106 0108 XSTR IRF641 402 0964 00 0107 0109 XSTR IRF9641 402 1000 50 Q101 0102 0104 XSTR TIP50 411 0311 42 FUSE 75A T 411 0311 56 FUSE 1 5 T 411 0312 70 FUSE 4A T 411 0322 75 FUSE 5A FAST BLO 65HP amp 500HP PUMP ONLY NOTE This list subject to change without notice A 50 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT DWG NO 60 1242 348 PART LIST POWER SHEET 3 OF 3 TELEDYNE sco Inc CIRCUIT BOARD REV J DATE 110311 ju PART NUMBER REFERENCE DESIGNATION DESCRIPTION 409 9006 00 WSHR NYL DF137A 409 9005 03 INSUL SLCON T0220 279 0601 04 U105 U106 IC H74A1 400 2152 08 CR116 CR117 DIO 1N5234B 402 9270 00 Q112 0115 XSTR 2N7000 270 0474 01 0107 IC 74HC14 170 1000 15 Y101 XTAL 56 531 1 8432 MHz 12 6010 00 C135 C138 CAP 10UF 25V TANT 60 1245 151 U108 CODED PUMP ID CHIP 60 1245 152 U108 CODED PUMP ID CHIP 100DM DED PUMP ID CHIP 100DX P P P 65D 65HP DED PUMP ID CHIP 260D DED PUMP ID CHIP 500D DED PUMP ID CHIP 1000D SPST X
112. 10 LIMITS CURRENT PUMP 1 MAX PRESS 3 MAX FLOW 2 MIN PRESS 4 MINFLOW PUMP A 5 FLOW LIMIT PREVIOUS A B C D Figure 3 9 Limits menu MAX PRESS PSI SET PRESS VALUE ON ON OFF DISPLAY ALARM SHUTDOWN PREVIOUS A B C D Figure 3 10 Limits setpoint Max Press menu M Note These features are discussed later in this section under Limits Programming Options 2 Press the number 1 key to set the value A message will blink on the right side of the screen prompting you to enter the selected limit 3 Enter the desired limit setpoint using the number keys 4 Press ENTER to save the value The pump can be set to shut off or not at this limit condition by pressing softkey C under shutdown This will toggle this option to ON 5 To exit the limit menu press the softkey D PREVIOUS If four pumps are connected press STORE RECALL or CLEAR ENTRY to exit the limits menu 6 Once all the limits have been set press softkey D PREVI OUS to return to the main menu Limits programming In addition to setting the upper and lower limits the pump also options allows the user to specify whether they want the alarm message displayed an alarm to sound when the limit is reached the pump to shut down when the limit is reached D Series Syringe Pumps Section 3 Basic Programming and Operation 3 12 Flow rate limit for pressure control 3 8 8 RAPID PRESS These features are set using the soft
113. 100 260D 65DM PUMP OR MALE CONNECTOR FOR 500D PUMP 1 8 NUT 1 8 FERRULE PRESSURE TRANSDUCER CAP TUBING TO VALVE ASSEMBLY PRESWAGED PUMP CONNECTION TUBING MOUNTING PLATE PUMP STRAP m 1 OF 2 e ol 9 e SYRINGE PUMP HEAD g y e mo ELECTRIC VALVE mc 4 EACH DL INLET TEE 4 EACH 5 CUSTOMER RESERVOIR 4 J DB 25 CONNECTOR TO CONTROLLER EXTRACTOR connector CONTROLLER dE 1 REAR PANEL oo EXTRACTOR CEES I ACCESSORY Irt ANALOG OUTPUT DIGITAL 445 DIGITAL DIGITAL EE GROUND OUTPUT esso V BRACKET PANHEAD ald SCREWS 9509090950909 Gore FRONT VIEW AR Figure 5 7 Electric valve installation 5 15 D Series Syringe Pumps Section 5 Continuous Flow Introduction Installation amp Operation 5 5 User Supplied Valves 5 16 Users may also choose to supply their own valves The following information is necessary to choose the appropriate valves to work with Teledyne Isco Continuous Flow software Check valves Do not use spring loaded check valves if refilling at atmospheric pressure the pump seals are not designed to draw
114. 1247 067 for 100DM 100DX an d 260D P N 68 1247 068 for 500D P N 60 1247 093 for 1000D or 60 1247 130 for 65D and 65DM which will not mar the cylinder s outer surface a For the 30D the cylinder cap is removed and the pump is run to its extreme The clearance between the piston top surface and the top of the cylinder needs to be adjusted to 025 050 0 6 1 3 mm with the cylinder cap seal removed 9 Center the pump bottom limit sensor with respect to the mounting screws and tighten them 10 Raise the top limit sensor to the extent of the slots and tighten the upper screw Now the new limit sensors MUST be calibrated as explained in the following section 9 38 9 14 4 Limit Sensor Calibration Excludes 30D D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing Once the new limit sensor assembly is installed the sensors must be calibrated Before calibrating the limit sensors be sure the cylinder is unscrewed several turns Follow steps 8 10 in the previous section 9 14 3 Use the following procedure to calibrate the limit sensors 1 Connect the pressure cable and power cord and turn the controller ON 2 Press REFILL and enter the maximum rate 10 11 12 13 14 15 16 17 18 19 20 21 22 23 Press STOP when the interrupter flag is approximately l4 from the full lower sensor Press A FLOW RATE and use t
115. 16 TUBING REMOVE 1 8 HEX NUT AND FERRULE Figure 5 1 Check valve package installation 65DM 100D 265D 500D pumps 5 4 Table 5 2 Continuous Flow Check Valve Package for Qty D Series Syringe Pumps Section 5 Continuous Flow Introduction Installation amp Operation 100D 260D 500D part 68 1247 059 Part Number Description loose 209 0169 41 18 ferrule 3 loose 209 0169 27 nut 2 209 0168 05 1g pipe plug 209 0166 80 Vg plug assembly 60 2253 240 Check valve housing analytical standard inlet 60 3864 010 Check valve cartridge 60 1243 519 6 4 cm x 6 4cm tubing 2 4 4 4 2 60 1243 518 6 4 cm tubing 1 60 1243 391 60 1243 557 1 5 m 0 125 tubing 1 5 m 0 085 ID PTFE tubing 60 1243 517 Double check valve housing 209 0161 01 0 12 male connector 209 0161 36 Tee union for 16 OD tubing 209 0169 42 Reducing tubing connector le to Ae 60 2258 019 209 0169 81 209 0169 80 Nut assembly Male nut for 18 tubing 10 u replacement filter 5 5 D Series Syringe Pumps Section 5 Continuous Flow Introduction Installation amp Operation Outlet Tee u 1 4 1000D on N Connector 2 Check Valve 1 4 Conn 4 fx M ud Plug Inlet Tee e 9 C Figure 5 2 Check valve package installation 1000D pump
116. 2 8 kg 2 96 kg FLOW RATE RANGE 0 01 ul min to 50 ml min for any pressure up to 689 5 bar FLOW RATE ACCURACY 0 396 maximum 0 25 ul min seal leakage FLOW RATE DISPLAY RESOLUTION 0 01 ul min 1 0 ul min in Constant Pressure Mode ANALOG OUTPUT ACCURACY x 196 of selected range DISPLACEMENT RESOLUTION 9 65 nl step REFILL TIME 1 72 minutes REFILL OR DEPRESSURIZATION RATE 0 01 ul min to 60 ml min at any pressure from 0 to 689 5 bar PRESSURE RANGE 0 6895 to 689 5 bar PRESSURE ACCURACY 0 5 of full scale at constant temperature PRESSURE REPEATABILITY 0 5 of full scale within 48 hours at constant temperature ZERO PRESSURE DRIFT 0 25 of full scale within 48 hours at constant temperature PRESSURE DISPLAY RESOLUTION 6 895 kPa AMBIENT TEMPERATURE RANGE 5 to 40 C TEMPERATURE DRIFT 0 0 1276 of full scale C HUMIDITY 95 maximum DEAD HEADSPACE VOLUME 1 30 0 020 ml POLLUTION DEGREE INSTALLATION CATEGORY MAXIMUM ALTITUDE Underwriters Laboratories UL has certified all D Series Pumps with the exception of the 100 VAC versions Using water at 137 9 bar and a temperature controlled environment at 30 C The analog output is an optional accessory Pressure repeatability specification is based upon re zeroing pressure transducer every 48 hours Refer to sub section ZERO PRESS in Section 3 of the manual for re zeroing procedure e Volume in and above the piston
117. 222 R 2500000000 0035681623 L 1000000000 0016778750 L N Transducer disconnected Pump B Pump C Pump D 44no0000000 18000 p000000000 2500000000 21000 0000000000 T Multipump Pair CD Check sum Volume total continuous flow or modifer mode multi pump pair AB Units Liters E6 System pressure multi pump pair AB displays Pump for other modes Units psi 5 Resolution 0 2 psi System flowrate multi pump pair AB displays Pump A for other modes Units Liters minute E10 Resolution 0 1 nanoliter minute G amp 2 Command Figure 8 6 Get all status strings from four pump operation 8 28 D Series Syringe Pumps Section 8 Serial Interface 8 8 2 Gradient Download This command downloads a step from the D Series pump to the Command PC This command will respond with PROBLEM INVALID COMMAND if the file or step does not exist If the file and step is valid the controller will respond as shown in Figures 8 7 and 8 8 8 8 3 Gradient Upload These commands upload a step from the PC to the D Series Commands pump This command will respond with PROBLEM INVALID COMMAND if the file or step does not exist If the file and step is valid the controller will respond as shown in Figures 8 9 and 8 10 Figure 8 11 shows an example of a pressure programming upload command Gradient upload commands must follow the format shown in the figures below Where necessary leading and trailin
118. 40 to 408 409 8 ml min flow rate x 4 985 Figure 1 3 500 HPx flow rate range 1000D Flow Rate Range 425 408 og o 3 Flow Rate ml min 0 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Pressure bar 137 9 Flow Rate ml min Max Pressure bar 0 001 to 340 137 9 340 to 408 409 8 ml min flow rate x 1 9756 Figure 1 4 1000D flow rate range 1 3 Unpacking Teledyne Isco Customer Service Dept PO Box 82531 Lincoln NE 68501 USA Phone 800 228 4373 402 464 0231 FAX 402 465 3022 E mail Iscolnfo teledyne com D Series Syringe Pumps Section 1 Introduction After removing the pump controller and accessories from the shipping carton examine them for signs of shipping damage Be sure no internal parts have shaken loose in transit If there is any shipping damage file a claim with the delivering carrier immediately Compare the contents of the boxes with the enclosed packing slip If there are shortages contact Teledyne Isco immediately D Series Syringe Pumps Section 1 Introduction 1 4 Controls and Indicators STANDBY CONST ACC press LIMITS 11 The pump controller regulates all pumping functions It is designed to sit on top of the pump base but may be located else where according to safety and convenience Programming and setup are pe
119. 43514 AIR ACTUATOR 601243892 EE TO CHEC E SST TUBING 209016966 4 OD TUBI SWAGELOK 209016369 4 SST BAC FERRULE SWAGELOK 209016368 4 SST FRO FERRULE SWAGELOK 209016406 CHECK VALVE INGS SWAGELOK 601248184 NLET FILTE Y OO MD ony m wo ro NOTE For current prices and quotations on parts contact Isco Service Department 2 This list is subject to change without notice A 64 D Series Syringe Pumps Appendix A Replacement Parts A 1 16 Single Air Valve Package Im IM M gt H e E IDE is o d Tees Oo r N a u 85 2 x N 2 ze PI SE s i Ts 8 I T d ae 18 REF o Pd UV REF I 1 IN A Is vg van oe e DWG 60 1242 334 Jm m A 65 D Series Syringe Pumps Appendix A Replacement Part
120. 5 26 7 10 11 12 13 14 15 16 17 18 19 20 21 22 23 4 25 26 27 N NOTE 1 This list is subject to change without notice A 62 D Series Syringe Pumps Appendix A Replacement Parts A 1 15 SST Dual Air Valve Package for 1000D REPLACEMENT PARTS LIST 10000 SST AIR VALVE PACKAGE A 63 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST SHEET 2 OF 2 TELEDYNE ISCO INC REV PART NUMBER DESCRIPTION oO 09016382 4 OD SST TUBING TEE W FITTINGS VALCO 9016384 4 OD SS UBING FERRULE VALCO 09016383 4 OD TUBING NUT VALCO 124389 TEE TO VALVE STAINLESS STEE BING 09016369 4 OD HS UBING FERRULE 209016568 4 OD GLAND NUT SPEEDB 601243893 VALVE TO PUMP STAINLESS STEEL TU 209016336 4 NPT TO 1 4 TUBING SST 691243518 3 WAY HASTELLOY VALVE W FITTINGS 209009326 SOLENOID VALVE 209016172 8 OD TUBE FITTING 209016173 8 NPT IO 1 4 OD TUBE FITTING oO c DI ony HI ro 6912
121. 6 Tubing cutting by hand 2 2 pre cut 2 2 U Unpacking 1 18 Vv Valve designating as passive active or electric 3 7 user supplied 5 16 B 7 NOTICE Disregard the following Declaration of Conformity and Radio Interference Statement if your instrument does not have a CE label on its rear panel Radio Interference Statement FCC This equipment has been tested and found to comply with the limits for a class A digital device pursuant to Part 15 of the FCC Rules These limits are designed to provide reasonable protection against harmful interference when the equipment is operated in a commercial environment This equip ment generates uses and can radiate radio frequency energy and if not installed and used in accordance with the instruction manual may cause harmful interference to radio communications Operation of this equipment in a residential area is likely to cause harmful interference in which the user will be required to correct the interference at his own expense Canada This ISM apparatus meets all requirements of the Canadian Interference Causing Equipment Regulations Ce g n rateur de fr quence radio ISM respecte toutes les exigences du R glement sur le materiel brouilleur du Canada DECLARATION OF CONFORMITY ISM A Application of Council Directive 2004 108 The EMC Directive 2006 95 EEC The Low Voltage Directive 2012 19 EU WEEE Directive Manufacturer s
122. 61 00 MALE HOSE CONNECTOR 60 1248 099 COOLING JACKET ASSY 500ML 202 2062 1 O RING 2 109 ID 139 CROSS SECTION CONFIGURATION 2 NOT INTERCHANGEABLE WITH CONFIGURATION PARTS 60 1244 444 MOTOR MOUNT ASSEMBLY 60 1245 161 CBA SYRINGE PUMP DRIVE UNITS 5000 60 1245 176 CBA MOTOR DRIVE FOR 500HP ONLY 60 1244 323 MAIN HARNESS Note For current prices and quotations on parts contact Isco Customer Service Department 2 This list is subject to change without notice 3 Verify the part number with Isco Technical Service Department A o gt A 14 This page intentionally blank D Series Syringe Pumps Appendix A Replacement Parts A 15 D Series Syringe Pumps Appendix A Replacement Parts A 1 5 500HPx Pump A 16 D Series Syringe Pumps Appendix A Replacement Parts 601242968 REPLACEMENT PARTS LIST TELEDYNE ISCO PART NUMER DESCRIPTION 1200007 1200012 1411001 1500006 DCTR 330 UH 11 0 2 1032900 0 FLTR 10 PWR UB D SOCKET RK FLSF RVS 24V RG CYL 3541D1 00D 11331 RG CYL 381D 880D 1429902 RG THR 351DX720D 220621 O RING ZED 2139 2909156 SEAL 1 5631DX1 810D 9001137 RING RING EXT 1 37 6100 CONN MALE 12 HOSE 6583 FIG TUBE 3 8 OD X 3 8 MALE NPT 656 FIG TUBE 3 8 OD X 3 8 MALE NPT 6813 LUG PIPE 3 8 NPT NITRONIC 6914 G PIPE 3 8 NPT HASTELLOY 3600 HR WV 397 ID 00384 SR OP
123. 7 9 Black PTFE graphite filled 202 9092 75 202 9092 06 202 9092 56 N A PRESSURE bar single point contact This seal may provide better sealing at lower pressure Its chemical compatibility is similar to that of the general seal AQUEOUS 0 689 5 White translucent ultra high 202 9090 77 202 9094 06 202 9094 56 N A bar molecular weight polyethyl ene This seal has better wetting properties making it a good choice for aqueous solutions It is also the best choice for electrochemical detection Note This seal requires a special break in procedure before installation See Section 9 9 2 AMMONIA NH3 0 275 8 White virgin PTFE 202 9090 78 202 9091 07 202 9091 57 upper seal NITRIC ACID bar 202 9990 26 lower seal 202 9990 24 This is the only seal recommended for ammonia M Note Call the factory for seal availability for the 30D pump 2 20 D Series Syringe Pumps Section 3 Basic Programming and Operation 3 1 Introduction 3 2 General Controller Information 3 2 1 Rates Units and Limits 3 2 2 Programming Screens This section will familiarize you with the D Series pump con troller and describe operating the pump under each of the various modes constant flow constant pressure dispense and refill Pump setup and operation is regulated by the D Series controller Operating parameters are entered via the keypad on the front pane
124. 9 X2 e REPLACEMENT PARTS LIST DUAL CHECK VALVE PKG 1000D A 71 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST SHEET 2 OF 2 TELEDYNE ISCO INC PART NUMBER DESCRIPTION 63 36 11 4 NPT TO 1 4 TBG SST MALE CONN 64 06 CHECK VALVE W FITTINGS SWAGELOK 68 15 1 4 SST TBG TEE W FITTING SWAGELOK 63 68 1 4 SST FRONT IBG FERRULE SWAGELOK 63 69 1 4 SST BACK TBG FERRULE SWAGELOK 69 66 11 4 OD TUBING NUT SWAGELOK NOTE For current prices and quotations on parts contact Isco Service Department 2 This list is subject to change without notice A 72 A 1 20 Single Check Valve Package ce GM 3 v PD EC Dx e Wo Sad Q 4 I 06 CY REPLACEMENT PARTS LIST DOUBLE CHECK VALVE PACKAGE D Series Syringe Pumps Appendix A Replacement Parts 66 dd A 73 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST soma Isco Inc REV C DATE 03122 ITEM NO PART NUMBER DESCRIPTION 1 209 0169 27 NUT 2 209 0169 41 FERRULE 3 209 0169 42 TUBING REDUCER CONNECTOR 4 60 2253 240 CV HOUSING INLET ANALYTICAL STANDARD INERT 5 60 3864 010
125. 9 Pump Maintenance Troubleshooting and Servicing 24 Install the covers 9 14 5 30D Limit Sensor The following steps are for the 30D limit sensor calibration Calibration 1 Disconnect the mains power and the transducer cable from the cylinder cap 2 Remove the cylinder cap and the cylinder cap seal 3 Reattach the transducer cable to the cylinder cap and set out ofthe way 4 Attach a controller to the pump and reconnect the mains power Turn the pump and controller on Turn off AUTO REFILL if it is turned on Press REFILL and enter the maximum flow rate AR Ct Press STOP when the interrupter flag is about 1 4 6mm from the lower sensor 9 Press A FLOW RATE and use the number keys to change the refill flow rate to 10 mL min Press the ENTER key 10 Press REFILL When the lower limit sensor is interrupted the motor will stop 11 Press CONST FLOW 12 Press A FLOW RATE and select MAX 13 Loosen the lower screw on the upper limit sensor about one turn Do not remove the screw 14 Press RUN 15 Press STOP when the volume counter in the upper right hand corner of the LCD reads 005 00 mL or less 16 Press A FLOW RATE and enter 5 mL min 17 Press RUN 18 When the counter changes from 000 01 to 000 00 press STOP 19 Lower the upper limit sensor to the point where the flag just interrupts the sensor CYLINDER EMPTY will flash on the screen 20 Tighten the upper
126. 91 00 ee 6299 02 ae lt ADP on gt co gt ESS UNIVERSAL SENSOR FD HEX NUT 1 2 20 STEE ER I 174 G 11 174 ER 1 3 8 Ds SIE m CL ro 9 9 EAR ST R GE OD M MO PO PO MD HD MD 114 Sa m EO gt Qo R i ER PIN 125 X T5 LONG SST OR STL 60 ER ASSY 60 1244 236 E WHEEL ASSY 60 1243 492 PA 141 4001 02 SUB For current prices and quotations on parts contact Isco Service Department This list is subject to change without notice A 46 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST SHEET 12 OF 13 TELEDYNE ISCO INC REV PART NUMBER DESCRIPTION 007 01 CHOKE 330UH AMP 60 1244 323 Al ESS 0 11 3500 20 PANEL MOUNT BANANA JACK 143 400 1 0 BINDING POST RED 143 8 0 BINDING POST BLACK 69 1244 4 TERMINAL STRIP ASSY 60 1244 184 OTOR ASSY 60 2254 132 OTOR BRUSHES PKG OF 2 60 1245 169 OT DRIVE CBA MOD 65DM 4 0311 62 FUSE 2 AMP FOR J00 117V UNITS ELD R
127. A Replacement Parts REPLACEMENT PARTS LIST NO 0120 02 SHEET 2 OF 3 Teledyne 5 0 REV N DATE 073109 60 1243 185 60 1248 116 60 1248 117 BALL SCREW ASSY 201 4299 02 THRUST BEARING INDIVIDUAL ORDER 2 EA 7 69 1244 415 UNIVERSAL SENSOR HARNESS 69 1243 431 WORM GEAR 9 9 1 60 1243 654 0 1243 607 SHEAR KEY FOR 500HP ONLY 0 No 6 201 0329 00 BEARING SEE NOTE 3 AT BOTTOM OF PAGE 69 1243 563 EXTENDED WORM GEAR 113 3250 00 5uF 100VDC 69 1243 560 SPUR GEAR 150 0006 0 BRAKE 201 1337 00 BEARING SEE NOTE 3 AT BOTTOM OF PAGE TES MEI HEN 4 De 8 n ES 10 M 16 18 EH 19 me e For current prices and quotations on parts contact Isco Customer Service Department 2 This list is subject to change without notice 3 Verify the port number with Isco Technical Service Department A 13 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST OWS NO 88 2422 SHEET 3 OF 3 leledyns WECO mes REV N DATE 073109 PART NUMBER DESCRIPTION H CONFIGURAT on 1 PARTS NOT INTERCHANGEABLE WITH CONFIGURATION 2 PARTES 141 4001 02 60 1244 193 411 0311 51 FUSE T 40 60 1244 220 GEAR LUBRICATION ASSY NOT SHOWN 4i 60 2254 132 MOTOR BRUSHES S 69 1243 717 24T 24P PINION GEAR 45 69 1243 718 COMBINATION GEAR 209 01
128. ATE ACCURACY 0 5 maximum 1 5 ul min seal leakage FLOW RATE DISPLAY RESOLUTION 1 0 ul min ANALOG OUTPUT ACCURACY DISPLACEMENT RESOLUTION REFILL TIME x 196 of selected range 25 38 nl step 2 5 minutes REFILL OR DEPRESSURIZATION RATE 1 0 ul min to 408 ml min at any pressure from 0 to 137 9 bar PRESSURE RANGE 0 6895 to 137 9 bar PRESSURE ACCURACY 0 5 of full scale at constant temperature PRESSURE REPEATABILITY ZERO PRESSURE DRIFT PRESSURE DISPLAY RESOLUTION 0 5 of full scale within 48 hours at constant temperature 0 25 of full scale within 48 hours at constant temperature 6 895 kPa AMBIENT TEMPERATURE RANGE 5 to 40 C TEMPERATURE DRIFT 0 12 of full scale C HUMIDITY 95 maximum DEAD HEADSPACE VOLUME 11 0 0 7 ml POLLUTION DEGREE INSTALLATION CATEGORY MAXIMUM ALTITUDE Underwriters Laboratories UL has certified all D Series Pumps with the exception of the 100 VAC versions A team lift is recommended when moving this instrument Using water at 137 9 bar and a temperature controlled environment at 30 C The analog output is an optional accessory Pressure repeatability specification is based upon re zeroing pressure transducer every 48 hours Refer to sub section ZERO PRESS in Section 3 of the manual for re zeroing procedure f Volume in and above the piston seal head clearance at automatic shutoff and inlet and o
129. B ATM BAR kPa PSI See Refill flow rate for Pump A Refill flow rate for Pump B Refill flow rate for Pump C m m m m Maximum pressure set point for Pump C ATM BAR kPa PSI See Maximum pressure set point for Pump D ATM BAR kPa PSI See NOTE 1 Minimum pressure set point for Pump A ATM BAR kPa PSI See NOTE 1 Minimum pressure set point for Pump B ATM BAR kPa PSI See NOTE 1 Minimum pressure set point for Pump C ATM BAR kPa PSI See NOTE 1 Minimum pressure set point for Pump D ATM BAR kPa PSI See NOTE 1 min ml hr ul min ul hr See NOTE 2 min ml hr ul min ul hr See NOTE 2 l min ml hr ul min ul hr See NOTE 2 min ml hr ul min ul hr See NOTE 2 ml hr ul min ul hr See NOTE 2 ml hr l min ul hr See NOTE 2 min ml hr ul min ul hr See NOTE 2 ml hr ul min ul hr See NOTE 2 Maximum flow rate set point for Pump A Maximum flow rate set point for Pump B Maximum flow rate set point for Pump C Maximum flow rate set point for Pump D Minimum flow rate set point for Pump A Minimum flow rate set point for Pump B Minimum flow rate set point for Pump C MH MO ro m m m m m m m m Minimum flow rate set point for Pump D Maximum flow limit in Co
130. B840WI 24 13040 W RKR DPDT CSA 4A INDIVIDUAL ORDER 2 EACH elo AP Cn S Co pro me NITRONIC HASTELLOY PF IPS P TS Dd IS o m TS U md lt jr gt 31274 6 25A 250 SB 111 VOLT qu 46121 3 2 250 SB 234 VOLT gt 91212 beat 250 SB 100 VOLT OO S ADP IW J JP PO c perl 243185 DBI on ov R WIPER 500 L KB 24329 LRN KB 243348 SL DE THRUST B G 244236 WHL LUBE ASSY 243454 RT SEAL 5 TRONIC eo 243159 RT SEA ASTELLOY 243535 BASE TRONIC 243198 BASE L 3 PSTN 5 PSTN 5 ASTELLOY 243538 R WE R 500 243511 CYL INDER 50 IC eo 243151 Gul INDER 50 LLOY 243601 SHEAR KEY 243610 KEY GRTN 99 9 99 mn an mn an YM DD eo 243981 GEAR TRAIN SOAK PAD or current rices and quotations on parts contact Teledyne Isco Service Department is list is subject to change without notice D Series Syringe Pumps Appendix A Replacement Parts 601242968
131. BALL ACTIVE AIR 30D ELECTRIC PREVIOUS Press 3x to return VALVE to run screen Figure B 3 Keystrokes to specify valve type Volume totalizer The total volume delivered is displayed in liters at the top right corner of the screen Refer to the figure below to reset the volume totalizer to zero 1 AB Pumps gt 2 CD Pumps 3 AB amp CD Pumps TOTAL VOLUME RESET 5 8 PREVIOUS Press 2x to return to MORE run screen Figure B 4 Keystrokes to reset volume totalizer B 9 D Series Syringe Pumps Appendix B Continuous Flow Introduction Installation and Operation for 30D B 5 2 Constant Flow Mode Continuous flow mode is found under the multi pump options on Menu 2 Once you have accessed the multi pump options you may select Constant Flow mode or Constant Pressure mode mewu EB CONTIN CONST FLOW 4 1 will blink Fi 5 PREVIOUS Starts Press 3x to operation returnto run MULTI PUMP screen 1 AB Pumps 2 CD Pumps Figure B 5 Keystrokes to set up constant flow B 5 3 Constant Pressure Continuous flow mode is found under the multi pump options on Mode Menu 2 Once you have accessed the multi pump options you may select Constant Flow mode or Constant Pressure mode ES gt V CONTIN CONST PRESS 2 will blink E PREVIOUS ED Press 3x to Starts meee return to run operation screen 1 AB Pumps 2 CD Pumps Figure B 6 Keystrokes to set up
132. BER DOES NOT EXIST It then assumes you will be creating a new gradient under that number and displays the program gradient run screen The STORE key is operational in the programmed gradient mode It is used to save the program gradient parameters and exit the programming parameter entry mode The REFILL key manually places the pump in refill mode The controller allows the user to set the minimum and maximum flow rate limits the minimum and maximum pressure limits and the maximum rate the pump will run while controlling the pressure in constant pressure mode When using a single controller to operate multiple pumps you need to select the appropriate pump before setting any pump parameters The available pumps will be displayed above the softkeys These selections corre spond with the connector that the pump control cable is plugged into on the rear panel of the pump controller To select a pump press the softkey under the pump desig nation The top line of the screen will indicate the currently selected pump The maximum and minium limits you set cannot exceed the pump specifications D Series Syringe Pumps Section 3 Basic Programming and Operation To set the limits 1 Press LIMITS To display the Limits menu enter the num ber of the limit you wish to program One of five limit set point menus will appear MAX PRESS MIN PRESS MAX FLOW MIN FLOW or FLOW LIMIT The MAX PRESS limit setpoint menu is shown in Figure 3
133. BINATION GEAR 8 201 4299 02 THRUST BALL BEARING INDIVIDUAL ORDER 2 9 60 1243 624 BEARING RETAINING RING 0 60 1248 121_ LDA SCREW ASSY 60 1243 348 SLIDE THRUST BEARING 2 60 1248 116 IBA UT ASSY 3 69 1244 415 HARNESS UNIVERSAL SENSOR 4 232 6091 00 SLOTTED HEX NUT 1 2 20 STEE 5 201 6299 52 THRUST WASHER 1 4 6 201 6299 02 THRUST BEARING L 4 1 201 6299 5 THRUST WASHER 1 3 8 8 2990 THRUST BEARING 1 3 8 9 60 1245 168 WORM GEAR MOD 20 60 1243 949 ISHEAR KEY 2 236 0008 12 COTTER PIN 2125 X 73 LONG SST OR SIL 22 60 1244 309 TRANSFORMER ASSY 23 60 1244 23 32 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST SHEET 12 OF 13 TELEDYNE ISCO REV UMBER DESCRIPTION 323 MA ESS 07 01 CHOKE 330UH II AMP 0 20 PANEL MOUNT BANANA JACK 1 00 BINDING POST RED 08 00 BINDING POST BLACK I4 4 TERMINAL STRIP ASSY 14 184 ASSY een OTOR BRUSHES PKG OF 2 245 7169 OTOR DRIVE CBA MOD 65DM 0311 62 FUSE 2 FOR 100 117V UNITS 0823 2 DRIP SHIELD 2 1104 FUSE HOLDER ER FILTE TROGE TROGE P PA D D DER 65DM SYRINGE PUMP RETAINER 65ML SEAL 563 ID X 813 OD B W UP RING 65D PRIMARY SEAL 24 243 880 PISTON BA
134. Break in procedure for aqueous seals Drawing does not apply to the 30D 9 15 9 10 Accessing the shear 9 20 9 11 Shear key amp 9 20 9 12 30D and 65DM Bearing set 9 22 9 13 30D and 65DM Shear key replacement 9 22 9 14 D Series motor brush replacement 9 24 9 15 Location of motor brushes 9 24 9 16 Length of a new motor brush 1 1 9 24 9 17 Inserting new motor brush 9 25 9 18 For 30D a cable tie holds the wires together 9 25 9 19 Remove screws and washers then the plate 9 26 9 20 Remove the five screws from the bottom of the pump 9 26 9 21 two pin connector 9 27 9 22 Encoder ssh degli ate lende hed atd ae a 9 27 9 23 Location of screws and washers holding the motor in place 9 28 9 24 Motor assembly enen ene 9 28 9 25 Support plate ilie boda ara en ana aa Soe 9 29 9 26 Position of wires connected to the 58 9 29 9 27 Wire connections c un vaer DEVO Ee ER N USATE 9 29 9 28 Set screws holding the t
135. CHECK VALVE CARTRIDGE 6 60 1243 517 DOUBLE CV HOUSING 7 60 2258 019 NUT ASSY 8 209 0169 81 TUBING NUT 9 209 0169 80 FILTER ANALYTICAL STANDARD INERT 10 209 0169 00 NUT 11 209 0169 10 FRONT FERRULE 12 209 0169 11 BACK FERRULE Note 1 For current prices and quotations on parts contact Isco Service Department 800 228 4250 2 This list is subject to change without notice A 74 D Series Syringe Pumps Appendix A Replacement Parts A 75 D Series Syringe Pumps Appendix A Replacement Parts A 76 D Series Syringe Pumps Appendix Continuous Flow Introduction Instal lation and Operation for 30D B 1 Introduction B 2 Continuous Flow Air Valves Air Valve Package Number AD Series continuous flow pumping system consists of two syringe pumps and a valve accessory package regulated by one controller This system allows you to continuously deliver liq uefied gas or liquid under constant flow or constant pressure mode Continuous flow can be used in either of two modes continuous constant pressure or continuous constant flow Both of these modes assume positive displacement of the piston Before programming continuous flow appropriate valves must be connected the pumps must contain fluid and there must be back pressure for operation Air valves generally open and close faster and are less prone to error and component wear making them suitable for industrial use and other applications where
136. D MONTER L INSTRUMENT OU D RANGER LE M CANISME DEDANS ADRESSER LA REPARATION SEULEMENT AUX TECHNICIENS COMP TENTS M Note For HPx pumps please refer to Section 9 13 2 for the motor brush replacement procedure The bottom brush is accessed through an opening in the bottom of the pump module ka N D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing Quick Disconnect Motor Brush Retainer one of two Figure 9 14 D Series motor brush replacement M Note Parts for Configuration 1 and Configuration 2 are not inter changeable Figure 9 15 Location of motor brushes A new brush is 1 1 cm long Brushes should be replaced before they reach 0 4 cm Figure 9 16 Length of a new motor brush 1 1 cm 9 24 D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing 1 Unscrew the brush retainer from the motor using a straight edge screwdriver 2 Pull the brush out of the slot and measure its length Ifit is nearing 0 4 cm replace both brushes M Note Alternatively the entire motor can also be replaced For lon ger lived optimal performance replace the motor when the brushes wear down 9 13 1 Motor Brush 1 Remove the wire lead by pulling on the spade connector Disassembly 2 Unscrew the brush retainer from the motor using a straight edge screwdriver 3 Pull the old brush out of the slot 4 Connect the new brush to the wire lead 5 Ins
137. D PASSIVATED OD X 2 17 TUBE DER LONG E VLV ODY PASSIVATED ER SHORT CPLG 2 00 OT KB OT ASSY W CPLR BA SENSOR 4 OD X 3 18 TUBE EPLACEMENT FILTER 10 MICRON LE NUT FOR 1 8 TUBING FLON TUBING 125 OD X 062 ID LET NUT LET GASKET LUG F250C 60K P lt ADP BR wo gt HSE OZ OMI TTE ODO T 2 6 6 6 6 6 6 6 6 6 6 6 6 2 2 0 6 6 2 lt gt ADP m wo Ile 3 NOTE 1 For current prices ond quotations on parts contact Teledyne Isco Service Department 2 This list is subject to change without notice B 20 D Series Syringe Pumps Index D Series Syringe Pumps Index A Acc key 3 13 Accessories analog output option 3 22 back pressure regulation 2 18 cylinder connection package 2 9 cooling heating jacket 2 13 cylinder insulating cover 2 12 in line filter package 2 11 manual control 3 13 outlet valve package 2 9 refill kit 2 8 Air valve package 5 7 B 1 Alarms pressure limits 3 11 Analog output option 3 22 Automatic refill 3 4 B Back pressure regulation 2 18 Baud rate 3 6 c Check valve package 5 1 B 1 cylinder connection package 2 9 Commands serial 8 20 Constant flow mode 3 16 Constant pressure mod
138. D Series Pumps Installation and Operation Guide 236 TELEDYNE ISCO Everywhereyoulook Part 69 1243 969 of Assembly 60 1243 998 Copyright 2013 All rights reserved Teledyne Isco Rev C October 2015 Foreword This instruction manual is designed to help you gain a thorough understanding of the operation of the equipment Teledyne Isco recommends that you read this manual completely before placing the equipment in service Although Teledyne Isco designs reliability into all equipment there is always the possibility of a malfunction This manual may help in diagnosing and repairing the malfunction If a problem persists call or e mail Teledyne Isco technical support for assistance Simple difficulties can often be diagnosed over the phone For faster service please have your serial number ready If it is necessary to return the equipment to the factory for service please follow the shipping instructions provided by technical support including the use of the Return Merchandise Authorization RMA specified Be sure to include a note describing the malfunction This will aid in the prompt repair and return of the equipment Teledyne Isco welcomes suggestions that would improve the information presented in this manual or enhance the operation of the equipment itself Teledyne Isco is continually improving its products and reserves the right to change product specifications replacement parts schematics and instructions with
139. DSPACE VOLUME 0 15 of full scale C 95 maximum 10 45 0 65 ml POLLUTION DEGREE INSTALLATION CATEGORY MAXIMUM ALTITUDE Underwriters Laboratories UL has certified all D Series Pumps with the exception of the 100 VAC versions A team lift is recommended when moving this instrument Using water at 137 9 bar and a temperature controlled environment at 30 C The analog output is an optional accessory Pressure repeatability specification is based upon re zeroing pressure transducer every 48 hours Refer to sub section ZERO PRESS in Section 3 of the manual for re zeroing procedure f Volume in and above the piston seal head clearance at automatic shutoff and inlet and outlet ports to the fittings 1 9 D Series Syringe Pumps Section 1 Introduction Table 1 9 1000D Technical Specifications CYLINDER CAPACITY POWER REQUIREMENTS Mains voltage line cord is a Disconnect Device 1015 0 ml 100 10 VAC 1 5 A maximum 117 12 VAC 1 5 A maximum 234 23 0 75 A maximum Factory Set LINE FREQUENCY 50 or 60 Hz LINE VOLTAGE NOISE TOLERANCE 1 7 x nominal rms line voltage 10 usecond pulses any phase angle random or repetitive DIMENSIONS PUMP 27 18 cm 46 74 cm 102 36 cm CONTROLLER 27 18 cm 30 48 cm 13 59 cm Width Depth Height WEIGHT PUMP 38 5 kg CONTROLLER 2 96 kg FLOW RATE RANGE See Figure 1 4 FLOW R
140. FLOW or CONSTANT PRESSURE STOP Stops the drive motor ENTER Enters selected values to memory NUMBER KEYS These keys are used to make menu selections and enter values when setting parameters M Note A more in depth explanation of the keypad is provided in Section 3 Basic Programming and Operation under Section 3 8 Front Panel Keys D Series Syringe Pumps Section 1 Introduction Figure 1 6 Pump controller rear panel connectors No on Figure 1 6 Table 1 12 Pump Controller Rear Panel Connectors Connector Description PUMP D This connector is only used during multiple pump operation The control cable from the rear panel of the fourth pump is attached to this connector PUMP C This connector is only used during multiple pump operation The control cable from the rear panel of the third pump is attached to this connector PUMP B This connector is only used during multiple pump operation The control cable from the rear panel of the second pump is attached to this connector PUMP A This plug connects the control cable from the pump rear panel This connec tion should be secured with the thumbscrews IMPORTANT The pump A connector is the only input power connector on the rear panel of the controller During single pump operation the pump must be attached to this connector to supply power to the controller N WARNING Do not connect or disconnect t
141. H 53H 54H 4FH 50H Step 2 FED1H 100H 22FH Step 3 D1H FED1H amp offH Step 4 Convert D1H to ASCII Hex and put at end of message Step 5 Put a CR ODH at the end of message for end of frame Step 1 559 82 51 48 52 83 84 79 80 Step 2 303 256 559 Step 3 209 303 amp 255 Step 4 Convert 209 into ASCII Hex and put at end of message Step 5 Put a CR 13 at the end of message for end of frame The carriage return CR signifies end of frame The format for frames sent from the unit to the network con troller is as follows acknowledgement message destination length message checksum CR D Series Syringe Pumps Section 8 Serial Interface All the parameters are as previously described except message destination Message destination is the 1 digit identification number of the unit that the message is sent to An example of a typical data exchange is summarized below For illustration we will assume the network consists of a computer serving as a combination network controller and master There will be one slave unit a Model 260D pump Details on the pump message format are in section 8 8 The computer will be unit 0 and the pump will be unit 6 Network Controller and Master Unit 0 CR 1R 5D CR M Note A CR must start the network The controller is checking for the presence of unit 1 but will get no response in 200 ms
142. I This can be changed to a value appropriate for the type of modifier being used If there is no need to change minimum pressure press PRE VIOUS D three times to return to the main menu The screen will display the words PRESSURE MODIFIER To change the minimum pressure Press MIN MOD PRESS B IF YOUR MODIFIER BOILS AT ROOM TEMP ENTER THE MINIMUM PRESS TO PREVENT VAPOR 50PSI MIN PRESS PREVIOUS Figure 6 3 Minimum modifier pressure screen 6 2 2 Modifier Concentration To select the limits Select MIN PRESS B ENTER MIN PRES will flash Type the desired pressure value and then press ENTER Press PREVIOUS D four times to return to the main menu The screen will display the words PRESSURE MODIFIER To set the modifier concentration press PUMP C or PUMP B or C Use the numeric keys to enter the desired percentage of modifier and press ENTER to save the value 1 Once modifier mode has been selected the desired pres sure limits must be set Select number 2 LIMITS from the main menu 2 The pump for which the limits are being set will be shown on the top left of the display LIMITS PUMP A If it is any pump other than pump press A LIMITS PUMP A will then be displayed 3 Press number 1 to select LIMITS and then 1 again to set the MAX pressure limits Enter the desired maximum pressure using the numeric keypad and press ENTER to store the value Then press D PREVIOUS to return to the limit
143. ID HANDLE VALUE hCom printf nComm d port not available port Sleep 2000 lexit 1 Sleep 1000 return else printf nComm d port available port dcbSerialParams DCBlength sizeof dcbSerialParams if GetCommState hCom amp dcbSerialParams error getting state printf Error getting Comm Port state 8 12 D Series Syringe Pumps Section 8 Serial Interface Table 8 5 Example ofa Visual C program to demonstrate conversion of pump commands to DASNET frames Continued Sleep 2000 exit 1 switch speed case 19200 dcbSerialParams BaudRate CBR_ 19200 break case 38400 dcbSerialParams BaudRate CBR_ 38400 break case 57600 dcbSerialParams BaudRate CBR_57600 break case 115200 dcbSerialParams BaudRate CBR_115200 break default case 9600 dcbSerialParams BaudRate CBR_9600 break dcbSerialParams ByteSize 8 dcbSerialParams StopBits ONESTOPBIT dcbSerialParams Parity NOPARITY if SetCommState hCom amp dcbSerialParams error setting serial port state printf Setting Comm port state failed Sleep 2000 exit 1 timeouts COMMTIMEOUTS timeouts 0 timeouts ReadIntervalTimeout 100 timeouts ReadTotalTimeoutConstant 100 timeouts ReadTotalTimeoutMultiplier 100 timeouts WriteTotalTimeoutConstant 50 timeouts WriteTotalTimeoutMultiplier 10 if SetCommTimeouts hCom amp timeouts error occureed Inform user printf Setting Comm port timeouts f
144. ING Use proper tools to hold the cylinder while installing the cylinder cap Installing the cap without holding the cylinder can damage the pump 36 Torque the cylinder cap to 50 ft lbs 68 N m 37 Reattach the transducer cable 9 14 6 Electric Valve Motor If a motor is replaced on the electric valve assembly it must be Calibration calibrated before use in order to obtain optimum closure force Remove the top covers from both the controller and the electric valve assembly WARNING The instrument must be powered on during this procedure use extreme caution while servicing 1 Note the voltage value written on the side ofthe newly installed motor D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing Calibration Voltage Value Figure 9 40 Electric valve motor voltage 2 Inside the controller attach the leads of a voltmeter across resistor R204 on the electric valve interface board 3 Press ACC CTRL ES gt PRGM GRAD En 4 Press the number key that corresponds with the new motor This opens the valve 5 Press the corresponding number key again to close the valve the motor will continue to apply torque to the valve for approximately 30 seconds 6 On the electric valve assembly CBA adjust the correspond ing potentiometer to the voltage printed on the side of the motor refer to Figure 9 41 M Note This procedure must be done during the 30 seconds that the motor i
145. ION L USAGER NE DOIT PAS D MONTER L INSTRUMENT OU D RANGER LE M CANISME DEDANS ADRESSER LA REPARATION SEULEMENT AUX TECHNICIENS COMP TENTS N WARNING Earth ground bonding conductor Do not remove or disconnect Mise la terre Ne pas enlever ni d connecter A N WARNING Line voltage is present inside this unit at all times regardless of switch settings If internal adjustments or repairs are necessary the line cords must be disconnected to remove possible shock hazard before opening the case The following sections contain maintenance and repair proce dures which you can do yourself or have done by a technician at your site To view the schematic drawings referred to in this section first find the serial number for your unit Then go to our Web site at www isco com In the left column under Service amp Support click Schematics D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing 9 1 1 Service Department 9 1 2 How to Ship Returns Enter your serial number in the field provided and click Get Schematics If you need assistance or don t see the correct sche matic for your specific unit contact our service department Ifyou have a question about a procedure need parts information or need some help call or email the Teledyne Isco Service department In your message be sure to include all the details about your instrument and the nature of the error Call the Servic
146. L F xx S xx IBS xx xx FBS xx xx D XXXX X L Gradient Duration Final B Range 0000 1 9999 0 minutes Range 00 00 100 0 Initial B ge Range 00 00 100 0 Step Number 02 99 File 01 99 Figure 8 8 Gradient Download Commands Two pump flow gradient 8 30 D Series Syringe Pumps Section 8 Serial Interface Step Number 01 LGUL F xx S 01 FL xxx XXXX I amp xx xx F xx XXx D XXXX X Gradient Duration Range 0000 1 9999 0 minutes Final Gradient Percentage Range 00 00 100 0 Initial Gradient Percentage Range 00 00 100 0 Gradient Total Flow Rate Units milliliters minute Range 000 0000 Maximum Flow Rate Step Number 01 File 01 99 Step Numbers 02 through 99 LGUL F xx S xx I xXX XX F xx Xx D XXXX X EL pps E Ep Gradient Duration Range 0000 1 9999 0 minutes Final Gradient Percentage Range 00 00 100 0 Initial Gradient Percentage Range 00 00 100 0 Step Number 02 99 File 01 99 Figure 8 9 Gradient Upload Commands Single pump flow gradient 8 31 D Series Syringe Pumps Section 8 Serial Interface Step Number 01 LGUL F xx S 01 FL xxx Xxxxx IB xx xx FB xx Xxx D XXXX X l Gradient Duration Range 0000 1 9999 0 minutes Final B Range 00 00 100 0
147. LL SCREW ASSY 28 RPLCMNT 300 PISTON ASSY 29 RPLCMNT KIT 30D PISTON SEAL 263098 CYLINDER CAP SEAL 30ML 263144 PUSH ROD 30ML 263105 CYLINDER 30ML gt CN lt gt oo YI S FCT JS co nmno on Io Jw PO OJ J ADP cn JO Jew Po oO o o o o o o o o 9o o o o o o o o gt Io For curren rices and quotations on parts contact Teledyne Isco Service Department his list is subject to change without notice 5 D Series Syringe Pumps Appendix A Replacement Parts 60126210 REPLACEMENT PARTS LIST TELEDYNE ISCO PART NUMER DESCRIPTION 601263131 SHEAR KEY 30D 601264082 ASSY 30D PRESS AMP 601261010 COOLING JACKET ASSY 30D 60225413 OTOR BRUSHES PKG 2 A 605363068 DUA LE F250C ADPTR KB 691243560 SP 691243563 EXTENDED WORM GEAR 691243800 CO ATION GEAR 691243802 P GEAR 691264154 RE EMENT TERMINAL STRIP ASSY 691244413 TR UCER CABLE ASSEMBLY 691263096 LABEL FRNT PNL 30D PMP NOTE 1 For current prices ond quotations on parts contact Teledyne Isco Service Department 2 This list is subject to change without notice
148. M 100DX 260D 500D and 1000D pumps that use Valco or SSI fittings The 65D pump can be configured and operated in a similar manner However due to the higher operating pressure and the AE F250C fittings the 65D requires hardware that is not listed in this section Call the factory for details to configure a 65D pump for this type of operation The mixing tee union fitting check valves and SST tubing are pre assembled The only connections you have to make are to the pump outlet ports and outlet tubing from the tee to your appa ratus tubing not provided 6 k D Series Syringe Pumps Section 6 Modifier Addition M Note Tighten fittings just enough to hold tubing in place Final tight ening will be done after all tubing and fittings are connected The following installation steps refer to Figure 6 1 independent pumps or Figure 6 2 continuous flow system The PTFE tubing part 023 0504 02 and filter part 209 9012 10 from the syringe pump refill kit should be con nected to the inlet valve of pump B Two Independent Pumps Refill kit Figure 6 1 Modifier addition kit installation Two pump configuration 6 2 Modifier Addition Kit A Mixing Tee Reduction Union CV w Seal Refill kit x Attach a 2 way valve to each pump housing using the spacer block and screws Attach the pump outlet tubing two way valve assembly to each pump outlet
149. MP TYPE D SOFTWARE MAJOR REV SOFTWARE MINOR REV D D D D D D D D D D D D D D 50 RO ro SOFTWARE MICRO REV M Note Pressure and flow rate based on user selected units D Series Syringe Pumps Section 7 Modbus Configuration 7 12 D Series Syringe Pumps Section 8 Serial Interface 8 1 Overview The Teledyne Isco D Series pump can be remotely controlled by a computer through a built in RS 232 C serial or USB interface This function is supported by the Teledyne Isco LabView toolkit You can write your own custom program to control Isco syringe pumps using any format such as BASIC or C This section provides the syntax and responses for serial commands Sim plified examples of programs are also provided It is possible for you to write custom programs capable of controlling up to 7 con trollers from a single computer each with up to 4 connected pumps Writing programs for serial control requires substantial knowledge of the software language used so Isco does not provide support for developing your own programs The toolkit is a sample program capable of running one controller and one to three pumps Its primary purpose is to provide an example to help the programmer start constructing custom pro grams for individual pump systems and applications To mod
150. NITS In the Units menu select the desired units to display for pres sure For example press 3 to select PSI for the pressure units In the Units menu select the desired units to display for flow For example press 5 to select ML MIN for the flow units The first line of the display will show the selected units 8 Press PREVIOUS D to return to Menu 1 10 11 Press RETURN D to exit Menu 1 Press CONST FLOW to set the pump mode to constant flow CFa will be displayed in the upper left corner of the screen Press FLOW RATE The words ENTER FLOW RATE should flash on the display Use the numeric keys to enter a flow rate of 10 ml min and press ENTER M Note If you make an error press CLEAR ENTRY to delete it 12 13 Press RUN Observe the flow rate displayed on the first line After a few moments the setpoint and flow rate display should match Once the setpoint and flow rate match press STOP a If three or fewer pumps are connected you will be prompted to press A to stop pump A B to stop pump B C to stop pump C or D to stop all pumps D Series Syringe Pumps Section 1 Introduction PRESS RUN KEY TO ESCAPE PRESS ALL PUMP OR STOP KEY TO STOP ALL PUMP A PUMP B PUMP C ALL PUMP A B C D Figure 1 13 Three pump stop menu b If four pumps are connected to the controller you will be prompted to press A to stop pump A B to stop pump B C to stop pump C D to stop pump
151. Note Before pressing RUN ensure that ON CONT FLOW is displayed on the screen and that the set flow rate pressure is correct Always verify the valve settings before running a program If a controller is reset or moved to a different power source it will revert back to default settings Active B 5 6 Tips for Running Liquids Checklist Continuous Flow 1 Degas liquids if appropriate 2 Purge air from the system a Fill both pumps completely by pressing REFILL and selecting each pump to fill b Route the outlet to waste or reservoir and press RUN Press STOP when fluid comes out of the outlet c Open the valves to atmosphere by pressing ACC CTRL then selecting each valve to open d Zero the pressure in each pump by pressing ZERO PRESS and selecting each pump to zero e Connect the outlet tubing and fill each pump once more 3 Reset total volume see Figure B 4 B 12 D Series Syringe Pumps Appendix B Continuous Flow Introduction Installation and Operation for 30D Liquefied Gases Checklist 1 Open the valves to atmosphere by pressing ACC CTRL then selecting each valve to open 2 Zero the pressure in each pump by pressing ZERO PRESS and selecting each pump to zero 3 Fillboth pumps completely by pressing REFILL and select ing each pump to fill 4 Pressurize both pumps by pressing RAPID PRESS Maximum flow rate and target pressure value will be displayed Press D to continue pressurization 5 R
152. PBDE AX PER X Circuit Boards X E EJ BEREIT X LCD Display X Capacitor B X Wiring p Z X O Internal Cables p X O External Cables rns EERE X Line Cord RER X X Transformer E ARER 5 2 Front Panel Label MEE X BE BAL X X DC Motor FHRFFEFEYYARTANEMKEE Name and amount of Hazardous Substances or Elements in the product GENE RMA R EE EST MENEN E ER ES DL e O Represent the concentration of the hazardous substance in this component s any homogeneous pieces is lower than the ST standard limitation X GRUB S EU S ESTERI IIA RISE HST ENEN KEER EINER RESEN ER PI RAR ET XE SUR X Represent the concentration of the hazardous substance in this component s at least one homogeneous piece is higher than the ST standard limitation Manufacturer may give technical reasons to the X marks IRE AA The Environmentally Friendly Use Period EFUP was determined through experience Er B RAS TO CE XR B EH BUEN EF 207 1622007 MEN SFRRKRKAD A A HA BA A SS The date of Manufacture is in code within the serial number The first three numbers are the year of manufacture 207 is year 2007 followed by a letter for the month A is January B is February and so on
153. PRESSURE 00000 MAINS 60 1242 306 Figure 1 7 Pump rear panel connectors Item No on Figure 1 7 Table 1 13 Pump Rear Panel Connectors Connector Description 1 Pressure outputs Two red binding post banana jacks providing pressure output voltages Left Jack Right Jack VDC psi VDC psi 1 0 V 2000 psi 0 1 V 2000 psi 1 0 V 3000 psi 0 1 V 3000 psi 1 0 V 1000 psi 0 1 V 1000 psi Pump 65D 30D All others Ground A black binding post banana jack providing a connection to circuit common Pressure transducer The pressure transducer cable must be plugged in for the pump to operate Control cable This cable connects the pump to the controller Mains IEC power connector with EMI filter D Series Syringe Pumps Section 1 Introduction External Fuses Limits pump current drawn from main power supply Replace with same type T time delay fuses 1 2 0 Amp for 100 117 volt operation 2 1 0 Amp for 234 volt operation For 500HPx Pumps 1 7 5 Amp for 100 volt operation 1 6 25 Amp for 117 volt operation 2 8 2 Amp for 234 volt operation For 30D Pumps 1 3 2 Amp for 100 117 volt operation 2 1 6 Amp for 234 volt operation To remove rotate cap counterclockwise Chassis ground Ground point for high static installations Internal fuses not F101 4 0 Amp T replaceable by the F102 F104 1 5 Amp T operator F103 0 75 Amp For 500HPX
154. Pumps Section 3 Basic Programming and Operation Unless otherwise specified the pump will refill to full cylinder capacity To specify a smaller refill volume press 2 and enter the desired volume Press 5 to toggle this feature off or on for each pump The system can also be programmed to refill a pump based on an external analog input voltage with a range of O to 11 5 volts Information about this feature is provided in Section 3 12 3 This feature allows you to set the activity of the pump in the event of a power failure Press 4 to toggle this feature between STOP to remain stopped after power is restored or CONT to automatically resume after power is restored M Note In a multiple pump system this action is applied to all con nected pumps To restore default program settings press 5 To continue with the reset press CONTINUE to cancel the reset press DO NOT D CAUTION Resetting the system erases all programs and user settings This is a basic reset For information about performing a hard reset refer to Section 9 4 2 From the menu you can adjust the screen brightness for your light conditions and viewing angle Use softkeys B DOWN or C UP to reduce or increase the brightness Menu 2 provides programming options for serial communication pump status external control multiple pump operation volume reset and valve control To save all settings and return to the main menu pre
155. R 100D 260D VALVE PKG 60 1245 741 UBING 1 8 OD 1 4X3 4 FOR 100D 260D VALVE PKG 2 3 3 6 8 9 10 11 2 13 15 16 7 18 60 1248 157 209 0169 80 7 NUT ASSY 7 M 19 60 1243 557 TUBING TEFLON 085 ID 60 INCHES LONG 20 209 0169 81 ALE NUT 1 8 TUBING LTER 10 MICRO 22 60 1244 3512 AIN HARNESS 25 69 1244 348 24 69 1243 827 ENSOR CIRCUIT BOARD ASSY UBING 1 8 OD 1 4 X 1 9 FOR 1000D VALVE PKG 4 NOTE 1 This list is subject to change without notice A 58 D Series Syringe Pumps Appendix A Replacement Parts A 1 13 Single Electric Valve Package dogz aool was9 00001 0005 Z1 aoool aoos t dogz aool wase o1 0001 0005 009 0001 0689 REPLACEMENT PARTS LIST SINGLE ELECTRIC VALVE PACKAGE A 59 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST ONG NO 0 1242 87 SHEET 2 OF 2 REV B DATE 110311 PART NUMBER DESCRIPTION 60 3934 002 MOTOR CIRCUIT BOARD ASSY 2 60 3934 012 MOTOR ASSY W COUPLER 3 209 0169 44 GLAND NUT 1 8 TUBING SSI 4 60 1243 737 TEE 1 8 TUBING INCLUDES ITEMS 3 amp 5 5 209 0163 53 FERRULE 1 8 ID HASTELLOY SSI 6 8 9 60 1243 827 TUBING 1 8 OD 1 4 X 1 9 60 1244 313 VALVE ASSY 1 8 TUBING INCLUDES ITEMS 3
156. S 0 D rit A 39 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARIS LIST 69DM SYRINGE PUMP A 40 D Series Syringe Pumps Appendix A Replacement Parts D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARIS LIST 65DM SYRINGE PUMP A 42 D Series Syringe Pumps Appendix A Replacement Parts 65DM SYRINGE PUMP REPLACEMENT PARTS LIST A 43 D Series Syringe Pumps Appendix A Replacement Parts 000 1 31998 Y Y NOILDIS Y Y NOLIO3S m2 REPLACEMENT PARIS LIST 65DM SYRINGE PUMP A 44 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST 65DM SYRINGE PUMP A 45 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST SHEET 11 OF 13 TELEDYNE ISCO INC REV PART NUMBER DESCRIPTION 201 133 00 BEARING VERIFY PARTS WITH ISCO SERVICE DEPT 201 0329 00 FARING CYLINDER 69 1243 363 EXTENDED WORM GEAR 150 0006 01 FAILSAFE REVERSE 24V 25 BORE 60 1243 610 RAIN KEY 69 1243 56 EAR 69 1243 800 BINATION GEAR 201 4299 0 UST BALL BEARING 35MM ID X 72MM OD 1243 624 FARING RETAINING RING 1248 127 SCREW ASSY 1243 348 E THRUST BEARING 1248 116 UT ASSY 1244 4 5 60
157. SE 65ML 7304 01 ROCKER SWITCH DPDT 4 AMP 69 1243 948 FRONT PANEL LABEL 65DM EAR RING 65ML Cc del Ge oO gt For current prices and quotations on parts contact Teledyne Isco Service Department his list is subject to change without notice A 33 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST SHEET 13 OF 13 TELEDYNE ISCO REV PART NUMBER DESCRIPTION 60 1244 235 CALIBRATED PREAMP ASSY 69 1243 465 INDER CAP SEAL 60 1243 29 ELRIN PLUG 23 2001 04 EL SCREW 4 20 X 1 4 CUP POINT NOTE For current prices and quotations on parts contact Teledyne Isco Service Department 2 This list is subject to change without notice A 34 D Series Syringe Pumps Appendix A Replacement Parts A 1 8 65DM REPLACEMENT PARTS LIST 65DM SYRINGE PUMP A 35 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARIS LIST 65DM SYRINGE PUMP A 36 Syringe Pumps Appendix A Replacement Parts D Series A 37 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARIS LIST 65DM SYRINGE PUMP D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARIS LIST 65DM SYRINGE PUMP lt SLAY N by M
158. SOR HARNESS WORM GEAR KEY EXTENDED WORM GEAR BEARING NOTE I This list is subject to change without notice A 9 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST DWG NO 60 1242 347 SHEET 3 OF 3 REV H DATE 073109 PART NUMBER DESCRIPTION 411 0311 62 FUSE 2 AMP 35 411 0311 51 FUSE AMP 39 SUB D SOCKET 42 410 1304 01 43 60 1245 162 POWER DRIVE CBA DIGITALLY ENCODED 1000D CAPACITOR 5 f 100VDC 46 60 1244 184 MOTOR ASSY FOR 10000 PUMP 48 69 1243 800 COMBINATION GEAR FOR 10000 PUMP 49 69 1243 805 COMBINATION GEAR FOR 10000 PUMP amp 55 60 1248 183 COOLING JACKET ASSY 10000 MALE HOSE CONNECTOR T 202 2062 35 O RING 3 109 ID 139 CROSS SECTION o NOTE I This list is subject to change without notice A 10 D Series Syringe Pumps Appendix A Replacement Parts This page intentionally blank A 11 D Series Syringe Pumps Appendix A Replacement Parts A 1 4 500D DX Pump A 12 500D DX HP DWG 60 1242 322 REV CONFIGURATION 2 NOTES THESE PARTS COMPOSE CONFIGURATION 1 AND ARE NOT INTERCHANGEABLE WITH CONFIGURATION 2 PARTS ESE PARTS COMPOSE CONFIGURATION 2 AND ARE NOT INTERCHANGEABLE WITH CONFIGURATION 1 PARTS D Series Syringe Pumps Appendix
159. Syringe Pumps Appendix A Replacement Parts REPLACEMENT L L 2 PART LIST T R F B nn B Isco Inc R C U B D REV A DATE 99100 d PART NUMBER REFERENCE DESIGNATION DESCRIPTION 201 112 6010 00 C201 C208 CAP 10uF 25VDC 202 141 9002 27 J216 SKT 25 PIN D SUB RTANG 203 270 0803 01 U201 U204 C 2803 204 270 1300 37 U206 C 82C55A 2 205 270 1500 40 0205 051286 206 270 0105 24 U202 C LM324 207 279 0205 07 U203 C VREF 336 2 5V 208 365 5012 00 K201 K202 K203 K204 K205 RLY DPDT 12VDC K206 K207 209 379 5027 50 R213 R216 RES 9 X 2 7K 210 379 5027 51 R203 RES 8 X 2 7K 211 400 0720 00 U207 C SP720 212 400 0151 01 CR212 CR213 DIO MUR1520 213 400 2022 00 CR208 CR215 DIO ZENER 22V 1N4748A 214 400 2152 08 CR214 CR217 DIO ZENER 6 2V 1N5234B 215 400 2152 11 CR207 DIO ZENER 4 7V 1N5230B 216 401 0150 00 CR201 CR202 CR203 CR204 CR205 DIO 1N5060 CR206 CR210 CR216 217 402 9270 00 Q202 XSTR 2N7000 218 110 6310 00 C210 CAP 100uF 50VDC 219 112 5005 00 C211 CAP 1 0uF 20VDC 220 150 0004 00 D5201 LED MV5753 RED 221 400 2152 22 CR211 DIO ZENER 12V 1N5242B 222 60 0854 042 1201 1202 INDUCTOR ASSY NOTE 1 For current prices and quotations on parts contact Isco Service Department 800 228 4250 2 This list subject
160. T UNIT ID FIRST IN OUTPUT STRING 10110 IL LEN IS LENGTH OF INPUT STRING 10115 REM IF INPUT IS JUST ADD SPACE AND JMP BY CHAR 10120 IF I THEN I I 10180 10130 O O ADD R TO OUTPUT STRING 10140 Y HEXS IL OF CHAR IN INPUT STRING IN HEX 10150 IF IL lt 16 THEN Y 00 Y PAD OUT CHAR IN STRING IF NEED 10160 IF IL gt 16 THEN Y 0 Y MORE THAN 16 THEN ONLY ONE PAD 10170 O 0 Y ADD CHAR TO OUTPUT STRING 10180 O O I ADD INPUT STRING TO OUTPUT STRING 10190 IL LEN O SUM GET NEW LENGTH AND CLEAR SUM OUT 10200 FOR LI 1 TO IL TO ADD ALL ASCII FOR SUM 10210 SUM SUM 0 LI 1 GET THE ASCII OF LI ASCII CHAR 10220 NEXT LI 10230 REM THIS FINDS THE CHECKSUM 10235 REM THE IS FIRST SUBTRACTED FROM 256 10236 REM THEN ANDED WITH 255 TO AND OFF EXTRA BITS 10240 CSUM 256 SUM AND 255 GET CHECK SUM 10245 IF CSUM lt 16 THEN O O 0 PAD OUT CSUM IF NEED 10250 O O HEX CSUM PUT AT END OF OUTPUT STRING 10270 RETURN DONE RETURN 20000 REM THIS SUBROUTINE SENDS O TO THE COM PORT 20010 PRINT 2 CR SEND CR TO COM PORT 20020 PRINT 2 O SEND O TO COM PORT 20030 PRINT 2 CR SEND CR TO COM PORT 20040 RETURN DONE Note Polling is part of the DASNET definition but is not required and is not shown in this example If this program is run on a PC as is the comm
161. TURE RANGE 6 895 kPa 5 to 40 C TEMPERATURE DRIFT 0 15 of full scale C HUMIDITY 95 maximum DEAD HEADSPACE VOLUME 2 10 0 020 ml POLLUTION DEGREE INSTALLATION CATEGORY MAXIMUM ALTITUDE Underwriters Laboratories UL has certified all D Series Pumps with the exception of the 100 VAC versions Using water at 137 9 bar and a temperature controlled environment at 30 C The analog output is an optional accessory Pressure repeatability specification is based upon re zeroing pressure transducer every 48 hours Refer to sub section ZERO PRESS in Section 3 of the manual for re zeroing procedure e Volume in and above the piston seal head clearance at automatic shutoff and inlet and outlet ports to the fittings 1 7 D Series Syringe Pumps Section 1 Introduction Table 1 7 500D Technical Specifications CYLINDER CAPACITY 507 38 ml POWER REQUIREMENTS Mains voltage line cord is a Disconnect Device 100 10 VAC 1 5 A maximum 117 12 VAC 1 5 A maximum 234 23 0 75 A maximum Factory Set LINE FREQUENCY 50 or 60 Hz LINE VOLTAGE NOISE TOLERANCE 1 7 x nominal rms line voltage 10 usecond pulses any phase angle random or repetitive DIMENSIONS PUMP CONTROLLER 27 18 cm 27 18 cm 46 74 cm 30 48 cm 102 36 cm 13 59 cm Width Depth Height WEIGHT PUMP CONTROLLER 33 25 kg 2 96 kg FLOW RATE RANGE
162. To set up this option use the following procedure 1 Press MENU 3 14 3 10 Operating Modes D Series Syringe Pumps Section 3 Basic Programming and Operation 2 Press softkey A MORE 3 Press number 4 MULTI PUMP The multi pump menu will appear 4 Press number 1 for pumps A or B press number 2 for pumps C or D 5 Press number 4 INDEPENDENT The controller will set the pumps to Independent mode Number 4 will blink indicating that INDEPENDENT mode is selected 6 Select the HOLD PRESS or NORMAL mode of operation Press softkey A to toggle between the two modes HOLD PRESS In constant pressure mode after the pump is empty if the outlet pressure rises past the set point the pump will restart and run the system to the set point pressure NORMAL This feature shuts the system down if a pump runs empty in constant pressure mode Once the pumps have been set to this mode they will operate independently from one another Each pump will operate at its defined limit and rate Independent mode is the default setting for the pump When you select a command such as STOP or REFILL the display will prompt you to designate which pump to stop or refill Only the designated pump will stop the other pumps will continue to run M Note In an emergency situation toggling the On Standby switch will cause all pumps to immediately stop 7 Return to the run screen by pressing D three times Then press D SELECT PUMP Th
163. a total of up to 200 steps One program can contain from 1 to 200 steps When operating in gradient mode any connected pumps not used for gradient are inoperable 1 To access the gradient programming menus press PRGM GRAD select PRESSURE 2 or FLOW 3 and CONTINUE C The home screen will appear with either PG Pressure Gradient or FG Flow Gradient in the upper left corner PGa 0 000mL MIN 2 5 013 28mL STOPPED REE 00 00 00 MIN FINAL PSI PROGRAM EDIT REVIEW OPTION 2 Press PROGRAM A 3 At the prompt enter a file number between 1 and 99 This is the file name of your program and can be the name of a new program you are creating or a stored program you want to edit or run Press ENTER M Note If a selected stored program is in a different mode than that of the controller selected in Step 1 a brief notification will appear displaying the controller s mode and the file s mode If you attempt to run the program without changing the mode of either it or the controller the program will not run and the same message will be displayed 4 To enter the flow rate for this program either press FLOWRATE A and use the number keys and Enter or for maximum possible flow simply press MAX C ENTER FLOWRATE 0 00000 XX 00000 FLOWRATE PREVIOUS MAX 5 To proceed to the programming screen press STEP FWD B The programming screen will appear with the file number and step number at the to
164. ad 8 29 8 8 4 Range Command 8 33 8 8 5 Error Messages 8 34 Section 9 Pump Maintenance Troubleshooting and Servicing 9 T Introduction ane eten e Re AER GR Gba URL Moe ae 9 1 9 1 1 Service Department ee eeen 9 2 9 1 2 How to Ship Returns 2 259 en 9 2 9 2 Maintenance aan oenen nn Bte Ee Hae eC SE WE odes 9 3 9 3 General Cleaning E Red e Rd 9 4 9 4 Resetting the System eee 9 4 9 4 1 Basic Reset i645 nea Br near nen 9 4 9 4 2 Hard Reset tt oe oa eR an este he ee No WEE 9 4 9 5 Diagnostic Menu cuore eL a ae ER de a ee S een 9 6 9 5 1 LOD TEST Iu re ia ex ec er us 9 6 9 52 ANALOG INPUTS sete dit ROV RURSUS PIE ea 9 6 95 3 KEYPAD TEST gt ossen god eC Re Ra e er CT ee RO GS 9 7 9 5 4 MOTOR CONTROL LIMITS nnee eeen 9 7 9 5 5 SERIAL TEST Tosti a IRAN as RC dta est eae 9 8 9 6 Removing the Case 9 9 9 6 1 Controller Case Top Removal 9 9 9 6 2 Pump Case Top 1 9 10 9 1 Test Points Snore bake ee eR V UE marl NEA eA 9 11 9 7 I Power Supply AT ara anr aten ea EEG ER Whee
165. adecimal number This number when added to all the previous characters in the message excluding control characters will result in a sum If there are no errors the result of modulo 256 division of this sum should be 0 Frame is R304STOPD1 CR R 3 0 4 S TD P 52H 33H 30H 34H 53H 54H 4FH 50H D1H 300H 300H MODULO 256 00 It is important to note that all characters are converted to the ASCII equivalent and added except for the checksum The two characters ofthe checksum are converted to hexadecimal numbers and concatenated to form a single two digit number This number is then converted to its ASCII equivalent and added to the end of the message Step 1 22FH 52H 33H 30H 34H 53H 54H 4FH 50H Step 2 2FH 22FH 100H 2R2FH 100H 22FH Modulo 200H 2 Step 3 D1H 100H 2FH Step 4 Convert D1H to ASCII Hex and put at end of message Step 5 Put a CR 0DH at the end of message for end of frame 8 15 D Series Syringe Pumps Section 8 Serial Interface 8 16 Decimal Format Using MODULO Hexadecimal Format Using NO MODULO Decimal Format Using NO MODULO Step 1 559 82 51 48 52 83 84 79 80 2947 256 559 Modulo 512 47 Step 2 472559 256 Step 3 209 256 47 Step 4 Convert 209 to ASCI Hex and put at end of message Step 5 Put a CR 13 at the end of message for end of frame Step 1 22FH 52H 33
166. against a vacuum The balls in Teledyne Isco check valves are closed by gravity Powered valves These are electrically triggered from the pump controller and could be air or electrically actuated Digital outputs 1 4 provide signals for control of four two way valves One wire for each valve is connected to its specific connector on the rear of the controller A second wire for each valve connects to ground The signal provided is an open collector which functions as a switch open for closure of the fluid path A switch closure low signals opening of the fluid path Table 5 6 shows the relationship between the digital output pump valve location and the fluid path status for the ACCESS CTRL connections Refer to the accessory control connections on the rear panel of the pump controller Table 5 6 Accessory Control Digital Outputs Digital Pump Valve Fluid Path Status Output Location 1 A Inlet open or closed Outlet open or closed Inlet open or closed Outlet open or closed Outlet open or closed Inlet open or closed 2 3 4 5 Inlet open or closed 6 7 8 Outlet open or closed Alternate connections can be made to drive low power 12 15 V relays or electric valves Assume two wires per relay or valve The first wire is connected to the appropriate digital output on the back of the pump controller The second wire can be con nected to the 15 V connector to supply a max
167. ailed Sleep 2000 exit 1 printf nComm intr installed int comm getc DWORD dwBytesRead 0 8 13 D Series Syringe Pumps Section 8 Serial Interface 8 14 Table 8 5 Example ofa Visual C program to demonstrate conversion of pump commands to DASNET frames Continued char buf 2 buf 0 0 get char if there if ReadFile hCom buf 1 amp dwBytesRead NULL error occurred Report to user return buf 0 void comm_putc char outchar DWORD dwBytesRead 0 char out 2 out 0 outchar if WriteFile hCom out 1 amp dwBytesRead NULL error occurred Report to user There are three types of operation within the network network controller master and slave A computer typically serves as the network controller It supervises all data flow on the network It also polls each unit which initiates data transfer and commands The network controller typically a PC should not be confused with the pump controller The network controller is used in addition to the pump controller The slave unit simply responds to commands accordingly The D Series pump functions as a slave unit These functions may be combined in one unit i e a computer can function as both a network controller and a master All data transfers are in a frame format When the network con troller polls an instrument it will start to respond within 200 ms If it does not reply
168. all screw If the shear key isn t completely in the slot the spacer will position it properly as the castle nut is tightened 2 Tighten the castle nut a For the 30D and 65DM torque to 200 in Ibs 23 N m Do not exceed this limit or damage to the bearings will occur 9 22 9 13 Motor Brushes D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing b For all other models torque to 250 in Ibs 28 N m 3 Loosen the nut until it can be turned by hand Tighten the nut finger tight 4 Torque the castle nut to 100 in Ibs 5 Insert the cotter pin through the castle nut and ball screw Ifthe holes do not line up loosen the castle nut slightly until any set of holes allow the cotter pin to be inserted N CAUTION Do not loosen the nut more than 30 beyond the torqued pos tion to align the holes 6 Reinstall the access cover If the pump does not run properly one possible cause is worn brushes Inspect the motor brushes every two years of operation or every 6 000 piston strokes whichever comes first Both brushes wear at approximately the same rate therefore only the top brush which is more easily accessible need be inspected AN DANGER RISK OF ELECTRIC SHOCK DISCONNECT THE ELECTRIC POWER BEFORE SERVICING ONLY TRAINED SERVICE PERSONNEL MAY REMOVE THE CASE TOP N NDANGER RISQUE DE CHOC ELECTRIQUE COUPER L ALIMENTATION AVANT LA R PARATION L USAGER NE DOIT PAS
169. am that you wish to enter the pressure The words ENTER PRES SURE will flash on the screen 3 Use the number keys to enter the desired pressure M Note If you make an error press CLEAR ENTRY to delete one char acter at a time 4 Press ENTER once the desired pressure is displayed 5 Press RUN to initiate pump operation 3 10 3 Dispense Mode For applications such as reactant feed and batch delivery where a specified volume is pumped Dispense Mode is available with Teledyne Isco syringe pumps Dispense mode flow rate begins at zero ramps up to level out at the programmed flow rate then ramps back down to zero deliv ering a precise specified volume The slope rate and run time are dependent upon the pump model being used Start Stop Specified Flow ramp up ramp down Figure 3 11 Depiction of dispense mode sequence M Note For time controlled delivery you must run the pump in stan dard gradient mode as described in Section 4 In order to access Dispense Mode control the pump must be in Constant Flow mode Press CONST FLOW to enter this mode Toggle Dispense Mode off or on by pressing DISP Note that pressing the DISP key while in Constant Pressure mode has no effect To adjust the flow rate press FLOWRATE A enter the desired rate using the number keys and press ENTER 3 17 D Series Syringe Pumps Section 3 Basic Programming and Operation 3 11 External Control 3 12 External Control Analog
170. amming and Operation 3 6 Menu Three Menu 3 provides programming options for poor fills diagnostics pressure calibration alternative pressure inputs pressure control setting and pressure setpoint tolerance To save all settings and return to the main menu press PRE VIOUS RETURN D 1 POOR FILL ALARM 4 DIFF MODES 2 DIAGNOSTIC MENU 5 PRESS INTEGRAL 3 PRESS CALIBRATION 6 PRESS DEADBAND PREVIOUS Figure 3 7 Menu 3 program selections 3 6 1 Poor Fill Alarm 3 6 2 Diagnostic Menu 3 6 3 Pressure Calibration In constant pressure mode this feature allows you to set a fill point as a percentage of pump volume If this volume percentage is not reached after a refill and re pressurization the system issues an alarm and stops the pump This selection displays an additional menu containing testing options for the system Refer to Section 9 5 for a complete expla nation of how to use the diagnostic menu This is a stored psi value to ensure optimal operation of the pressure transducer On most pumps this value known as the midpoint adjustment can be found on a tag on the transducer cable shown below The midpoint adjustment value is individual to each pump and is stored within the controller software Therefore this value must be re entered if the controller or pump is switched con troller is reset or if a pump is plugged into a different port on the controller This calibration feature is not applicabl
171. amp 5 COUPLING SHIELD 60 3933 010 SPIDER 10 209 0169 10 FRONT FERRULE 1 8 ID FOR 500D VALVE PKG O 1 209 0169 11 BACK FERRULE 1 8 ID FOR 500D VALVE PKG 12 209 0170 04 FITTING NUT 1 8 TUBING FOR 500D VALVE PKG 5 4 13 60 1243 742 TUBING 1 8 OD 1 4 X 2 2 FOR 5000 VALVE PKG 15 209 0163 60 FERRULE 1 8 ID FOR 100D 260D VALVE PKG TUBING 1 8 OD 1 4X3 4 FOR 100D 260D VALVE PKG 18 60 1248 157 NUT ASSY 19 60 1245 557 TUBING TEFLON 085 ID 60 INCHES LONG T 21 209 0169 80 FILTER 10 MICRON 22 60 1244 312 MAIN HARNESS 23 69 1244 548 SENSOR CIRCUIT BOARD ASSY NOTE 1 This list is subject to change without notice A 60 D Series Syringe Pumps Appendix A Replacement Parts A 1 14 SST Dual Air Valve Package for 100 260D 500D 65DM 100DM DX 260D amp 500D AIR VALVE PACKAGE Or AIR VALVE PACKAGE REPLACEMENT PARTS LIST ram I Ne 5 x pU c
172. ands entered at the keypad will be output on serial port 2 This code was written in QBa sic version 4 5 QBasic is an integrated BASIC language interpreter created by Microsoft Corp Redmond WA included in MSDOS version 5 0 and later and in Windows 95 98 NT 3 x and NT4 8 8 D Series Syringe Pumps Section 8 Serial Interface Table 8 4 Example ofC program to demonstrate conversion of pump commands to DASNET frames include lt stdio h gt include lt conio h gt include b comm c edit to path needed a C example of DASNET serial control int conv_das unsigned char in 256 out 256 buf 256 char unitnum main unsigned port int speed cputs ENTER UNIT ID get parms scanf d amp unitnum cputs ENTER COM PORT scanf 96d amp port cputs ENTER BAUD RATE scanf d amp speed comm_open port speed open comm port in 0 50 cputs ALL ENTRIES IN CAPS n r while 1 cputs n rENTER STRING Q TO QUIT gt gt gt cgets in if in 2 Q break conv_das amp in 2 out convert string cputs nDASNET FORMATTED OUTPUT gt gt gt puts out output converted string comm_putc 0x0d send CR to serial port dput out output converted string to serial port comm_putc 0x0d end with a CR dgets buf get response cputs nDASNET RESPONSE gt gt gt puts buf output response comm_flush
173. apidement loin de la pompe et r duira aussi la quantit de gaz qui entre dans le compartiment du moteur Scellez le compartiment du moteur de la pompe avec un ruban adh sif et circulez un flot con tinu d azote N l int rieur du compartiment Cela r duira aussi la possibilit d accumuler une mixture explosive autour du moteur et relais se trouvent la premiere possibilit des tincelles lectriques Pour l information suppl mentaire t l phonez gratuitement 800 775 2965 ou t l copiez 402 465 3085 pour consulter le d partement de service technique UTILISEZ LE SYSTEME SFE ET LES POMPES SERINGUE TELEDYNE ISCO DANS TELLES APPLICATIONS POTENTIELLEMENT HASARDEUSES A VOS RISQUES ET PERILS vi D Series Syringe Pumps Warnings Cautions and Notices WARNING PLEASE READ At the request of our Supercritical Fluid Extraction laboratory staff we want our customers to be aware of the potential hazards involved with supercritical fluid extraction Oxidizing gases such as nitrous oxide in contact with organic matrices or flammable modifiers can detonate under certain conditions Likewise flammable fluids such as methane under high pressure conditions can present a hazard With concern for the safety of our customers we have designed our extractors to be as safe as possible However we do not recommend the use of our instrument with potentially explosive reactions The letter below which appeared in the
174. ar buffer char ptr DWORD dwBytesRead 0 ptr buffer while 1 char buf 2 get char if there if ReadFile hCom buf 1 amp dwBytesRead NULL lerror occurred Report to user buffer buf 0 if buffer 0x0d amp amp ptr buffer ll dwBytesRead 0 buffer 0 break void dputs char out int n DWORD dwBytesRead 0 D Series Syringe Pumps Section 8 Serial Interface Table 8 5 Example ofa Visual C program to demonstrate conversion of pump commands to DASNET frames Continued int count 0 n strlen out start of packet if WriteFile hCom v 1 amp dwBytesRead NULL error occurred Report to user data if WriteFile hCom out n amp dwBytesRead NULL error occurred Report to user end of packet if WriteFile hCom v 1 amp dwBytesRead NULL error occurred Report to user void commOpen int port long speed TCHAR szComPort 20 if port lt 10 wsprintf szComPort _T COM d port else wsprintf szComPort _T COM d port hCom CreateFile szComPort GENERIC_READIGENERIC_WRITE desired access should be read amp write 0 COM port must be opened in non sharing mode NULL don t care about the security OPEN EXISTING IMPORTANT must use OPEN EXISTING for a COM port 0 usually overlapped but non overlapped for existance test NULL always NULL for a general purpose COM port if INVAL
175. arance behind the pump such that the MAINS power cord can be unplugged at any time 1 Before connecting the line cord make sure the voltage rat ing on the serial tag matches your outlet s voltage Plug in the line cord Turn the pump power switch ON Turn the controller ON STANDBY switch ON 2 The display will briefly show the software revision on the first line the pump model s connected to the controller PUMP CONTROLLER ISCO INC REV ____ PUMP MODEL CD Jun 16 2011 SERIAL CHANNEL X UNIT ID 6 Baud 9600 Figure 1 11 Status Screen D Series Syringe Pumps Section 1 Introduction Figure 1 12 Menu 1 1 22 3 4 Check the upper left corner of the controller screen The current pump mode will appear in a two letter abbrevia tion e g CF for constant flow This will be followed by a lowercase letter indicating the current pump e g a indi cates that pump A is the current pump The current pump is the one for which parameters are being set a If a pump other than pump A is currently selected In the lower right corner of the screen directly over softkey D are the words SELECT PUMP Press MENU gt 2 gt A to select pump A The display will automatically switch to the run screen showing a in the upper left corner Press MENU to display Menu 1 1 UNITS 4 POWER FAILURE STOP 2 SELECT PUMP 5 SYSTEM RESET 3 REFILL 6 DISPLAY CONTRAST MORE RETURN 5 Press 1 for U
176. ate the two pumps manually for initial setup i e refill and purging of air If the Teledyne Isco air valve package is used the air valves are switched through ACCESS CTRL When air valves are used lights on the air valve actuator indicate which valves are open The 30D will not work in Receive Mode Table B 4 Key functions in the Multi pump Mode Display Option Description NORMAL Uses a finer slower pres sure match control when switching from one pump to the other Uses a coarser faster pressure match control when switching from one pump to the other NORMAL PRESS Uses pressure matching when switching from one pump to the other LOW PRESS Uses no pressure matching when switching from one pump to the other DELIVER Sets the pump into the delivery mode of operation OTHER OPTIONS Sets the fill and refill marks that are used with both con tinuous flow modes Sets the NCV feature On Off See Section B 5 4 B 8 D Series Syringe Pumps Appendix B Continuous Flow Introduction Installation and Operation for 30D B 5 1 Defining Operation Select Pump This menu allows you to select any pump to display its run screen program and operation data and to make program changes Valve specification To prevent pressure fluctuation at swi tchover you must specify the type of valve package you are using or or gt AIR PASSIVE CHECK VALVES MORE 2 way ACTIVE
177. because there is no unit 1 Network Controller and Master Unit 0 IR 5D CR Still no response Network Controller and Master Unit 0 1R 5D CR Still no response so unit 1 will be dropped from the poll Network Controller and Master Unit 0 2R 5C CR Checks for unit 2 but will get no response in 200 ms because there is no unit 2 Network Controller and Master Unit 0 2R 5C CR Still no response Network Controller and Master Unit 0 2R 5C CR Still no response so unit 2 will be dropped from the poll In this way units 3 5 will be checked and dropped from the poll Network Controller and Master Unit 0 6R 58 CR Check for presence of unit 6 Unit 6 R 8E CR Unit 6 responds Network Controller and Master Unit 0 TR 57 CR Since unit 7 does not exist it will be dropped from the polling scheme Network Controller and Master Unit 0 6ROO8IDENTIFY 84 CR The master verifies the fact that unit 6 is a Model D In 8 17 D Series Syringe Pumps Section 8 Serial Interface 8 18 this example the master and the network controller are a single unit Ifthey were separate units the master would send the inquiry to the network controller then the network controller would send the message to the slave unit the next time it is polled The slave would respond with the message to the network controller The next time the master is polled the message would be relayed The same sequence would occur with all messages Sin
178. cap with wrenches Removing the pump Refer to Figure 2 16 on the next page for the following steps cylinder 1 Empty the cylinder Be sure the piston is left fully extended 2 Turn the pump s mains power switch OFF or disconnect the power cord 3 Remove the pump front cover by loosening the four cover screws two on each side ofthe pump 4 Using a Allen wrench loosen the lock screw located on the front of the cylinder mounting block 5 Disconnect the transducer cable from the pump and remove the inlet and outlet tubing 6 Unscrew the cylinder from the cylinder housing It may be necessary to use a tubing strap wrench or the Isco wrench package to unscrew the cylinder without marring its outer surface 7 Lift the cylinder off the piston and push rod Installation 1 Install the O rings in the grooves of the cooling jacket 2 Lubricate the O rings with soapy water or a light oil to ease assembly of the cooling jacket onto the cylinder 3 Slide the cooling jacket onto the cylinder using a twisting motion M Note It is important that the cooling jacket be installed with the lock ing set screw away from the cylinder cap 2 16 D Series Syringe Pumps Section 2 Fluid System Connections and Accessories N CAUTION Be careful not to damage the O rings when pushing them over the threads of the cylinder Cylinder cap 0 ring Outlet connector Pressure port transducer
179. ce the master and the network controller are combined in this example the relaying of messages is not necessary Unit 6 RO27SERIES 1240 02__ Model ___D PUMP REV __XX CR The pump responds with identity and software revision letter In this example 02__ would be 021 Model D would be 260D REV __ signifies the software revision XX would be replaced by the correct checksum which is B4 Network Controller and Master Unit 1 6RO06REMOTEI6 CR This places the pump in the remote mode Unit 6 8E CR The pump acknowledges that it accepted the command Network Controller and Master Unit 1 6RO0ACONST FLOWFS CR This puts the pump into constant flow rate mode Unit 6 8E CR The pump verifies that it received the message Network Controller and Master Unit 1 6RO09FLOW 1 00AB CR This sets the pump s flow rate to 1 00 ml per minute Unit 6 R 8bE CR The pump verifies that it received the message Network Controller and Master Unit 1 6R 58 CR Polls the pump Unit 1 8bE CR Pump responds Network Controller and Master Unit 1 6RO03RUNFO CR The pump is started Unit 1 8E CR The pump responds D Series Syringe Pumps Section 8 Serial Interface The system is now running and the network controller continues the polling scheme If the controller gives an improper command the units will respond with a problem message indicating the type of error The format of the message is given in section 8 8 of this manual an
180. chnical bulletin TB02 Constant Pressure Pump Operation for Receive Mode available on the Teledyne Isco web site In any syringe pump continuous flow system a flow irregularity occurs at the time of switchover from one pump module to the other This flow irregularity can be measured as a pressure fluc tuation Teledyne Isco pressure fluctuation at switchover is 0 35 bar at system backpressures from 6 9 bar to the single pump maximum Before programming continuous flow appropriate valves must be connected the pumps must contain fluid and there must be backpressure for operation Continuous flow is not available with the 30D pump Please contact the factory for details 5 2 Continuous Flow The following section describes the installation procedure for Check Valves continuous flow check valves M Note Due to the higher operating pressure and special fittings the model 65D pump requires hardware that is not listed in this section Call the factory for details to configure a 65D pump for this type of operation The check valve package connects two D Series syringe pumps allowing continuous flow operation The tees check valves and connecting tubing come assembled so that you can quickly and easily install this package in your system For additional conve nience the two lengths of pump connection tubing come with the 5 1 D Series Syringe Pumps Section 5 Continuous Flow Introduction Installation amp Operation fitti
181. computer has and the number of controllers you wish to connect Network communications are initiated by your computer To connect one controller use a null modem cable available from Teledyne Isco part 480 7996 00 to connect the 9 pin serial output port of the computer to the RS 232 C port on the rear of the controller as shown in Figure 8 1 8 3 D Series Syringe Pumps Section 8 Serial Interface CONTROL COMPUTER rn RS 232 C gt Ls Null Modem Cable part 480 7996 00 Figure 8 1 Serial network connection example Single connection D SERIE CONTROL S N LER Ss RS 232 C PUMP A 17 G um ju SYRINGE PUMP With this configuration your sample program is capable of Constant flow Constant pressure Gradient 8 4 2 Two Controllers Compiler required M Note In order for the network to operate properly all instruments connected to the network must be turned on even if they are not being used To connect two controllers in the network use the Y cable 68 1020 198 as shown in Figure 8 2 C PUMP C PUMP D SERIES CONTROLLER CONTROL COMPUTER UNIT n 1200 BAUD D SERIES CONTROLLER cy T IT 1 RS 232 C m PUMP erm 68 1
182. d M Note Be sure the circuit board connector is mated pin for pin with the jack 9 36 DWG 60 1242 217 REV A D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing SCREW UPPER LIMIT SENSOR CYLINDER LOCK SCREW LOCATED ON OPPOSITE SIDE OF PUMP Be LOWER LIMIT SENSOR POWER p CIRCUIT BOARD pump AH 9 BACK e PANEL o C tL E H CJ cy Figure 9 38 Limit sensor replacement UPPER LIMIT SENSOR amp LOWER di LIMIT d SENSOR dim 2 2 g PLASTIC MOUNT INSTALLED PLASTIC CONDUIT MOUNT I SCREW HOLE am _ CONDUIT CONDUIT SHOWN SCREWED DIRECTLY TO CASE SS CABLE RETAINER RETAINING TAB INSTALL Figure 9 39 Installing the plastic mounts PLASTIC CONDUIT MOUNT USING EXISTING SCREW HOLE AND SCREW 9 37 D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing 8 Not 30D Be sure that the cylinder is unscrewed several turns If you need to use a wrench we recommend a strap wrench or wrenches in the Teledyne Isco wrench package P N 68
183. d clearance at automatic shutoff and inlet and outlet ports to the fittings 1 4 D Series Syringe Pumps Section 1 Introduction Table 1 4 100DM Technical Specifications CYLINDER CAPACITY 102 93 ml POWER REQUIREMENTS Mains voltage line cord is a Disconnect Device 100 10 VAC 1 5 A maximum 117 12 VAC 1 5 A maximum 234 23 0 75 A maximum Factory Set LINE FREQUENCY 50 or 60 Hz LINE VOLTAGE NOISE TOLERANCE 1 7 x nominal rms line voltage 10 usecond pulses any phase angle random or repetitive DIMENSIONS PUMP CONTROLLER 27 18cm 27 18cm 46 74 cm 30 48 cm 101 09 cm 13 59 cm Width Depth Height WEIGHT PUMP CONTROLLER 32 8 kg 2 96 kg FLOW RATE RANGE 0 01 ul min to 25 ml min for any pressure up to 689 5 bar FLOW RATE ACCURACY 0 396 maximum 0 25 ul min seal leakage FLOW RATE DISPLAY RESOLUTION 0 01 ul min 1 0 ul min in Constant Pressure Mode ANALOG OUTPUT ACCURACY x 196 of selected range DISPLACEMENT RESOLUTION REFILL TIME REFILL OR DEPRESSURIZATION RATE 4 825 nl step 3 5 minutes 0 01 ul min to 30 ml min at any pressure from 0 to 689 5 bar PRESSURE RANGE 0 6895 to 689 5 bar PRESSURE ACCURACY 0 5 of full scale at constant temperature PRESSURE REPEATABILITY 0 5 of full scale within 48 hours at constant temperature ZERO PRESSURE DRIFT 0 25 of full scale within 48 hou
184. d specifies the commands used for this instrument It is important to follow this format Spaces are ignored anywhere within the message field Commands must be in uppercase letters The network definition allows multiple commands in a message field when delimited by semicolons but the D Series controller is limited to single commands It will respond with a PROBLEM INVALID COMMAND message 8 19 D Series Syringe Pumps Section 8 Serial Interface 8 8 Serial Commands for the D Series Pump Table 8 6 is a list of the serial commands recognized by the pump These commands are the message part of the DASNET protocol The operand always follows the equals sign The REMOTE command must be sent once before any command that changes the operation of the pump will be accepted When setting a value the serial command will always be fol lowed by an equal sign Table 8 6 Serial Commands Command Description Enter for percentage of modifier Status of the analog voltage input on pin 21 P6 See NOTE 1 Status of the analog voltage input on analog input of the accessory connector See NOTE 1 Status of the analog voltage input on analog input 2 of the accessory connector See NOTE 1 Status of the analog voltage on analog input 1 of the accessory connector See NOTE 1 Status of the analog voltage input for Press D See NOTE 1 Status of the analog voltage on analog input 4 of the accessory connector See NOTE
185. ducer can also be read via the ALOGx serial commands RANGEA Provides scaling information for the system parameters See 8 8 4 for more informa RANGEB tion about this serial command RANGEC RANGED RAPIDA Activates the automatic rapid pressurization cycle constant flow mode only RAPIDB RAPIDC RAPIDD RECEIVE Set the dual pump mode to receive fluid when running RECEIVECD REFILL Move cylinder to bottom at preset refill rate REFILLB REFILLC REFILLD REFILL Enter to designate refill rate REFILLB REFILLC REFILLD REMOTE Disables controller front panel control and enables all serial commands Stops all motors if control was previously local RLIMITA Returns the refill flow rate limit RLIMITB RLIMITC RLIMITD RSVP Pump responds with READY message RSVPB RSVPC RSVPD RUN Same as front panel Initiates pumping RUNB RUNC RUND RUNALL SETFLOWA Returns the flow rate setpoint SETFLOWB SETFLOWC SETFLOWD 8 24 D Series Syringe Pumps Section 8 Serial Interface Table 8 6 Serial Commands Continued Command Description SETPRESSA Returns the pressure setpoint SETPRESSB SETPRESSC SETPRESSD STATUSA Returns with status of pump May be any combination of responses listed below STATUSB STATUSC STATUSD STATUS STOP PROBLEM OVER PRESSURE RUN UNDER PRESSURE REFILL CYLINDER FULL HOLD CYLINDER EMPTY EQUIL MOTOR FAILURE LOCAL REMOTE EXTERNAL Same as
186. e 3 16 Contact Service Department 9 2 Continuous flow 5 1 air valves 5 7 B 1 check valves 5 1 B 1 electric valves 5 13 B 4 operation 5 17 B 8 software 5 16 B 7 specifications 5 2 5 7 5 13 B 2 B 4 Controller front panel label 1 14 keypad 3 10 rear panel connectors 1 16 Cooling heating jacket 2 13 Cutting tubing 2 2 D DASNET protocol 8 6 Displays setting the contrast 3 5 Drain tube 2 5 E Electric valve package 5 13 B 4 Electrical connections 1 18 analog control 3 18 controller 1 16 pump 1 17 Error messages serial command 8 34 External control 3 18 analog 3 6 DASNET 8 6 pinout 8 2 remote run stop 3 21 serial commands 8 20 serial error messages 8 34 serial interface 7 1 8 1 F Flow rate limit 3 12 H Help key 3 13 ID numbers 3 6 In line filter accessory package 2 11 K Keypad acc ctrl 3 13 help 3 13 hold 3 10 limits 3 10 multi pump mode 3 14 5 17 B 8 rapid press 3 12 recall 3 10 store 3 10 zero press 3 13 L Liquid connections drain tube 2 5 M Main menu 3 3 units 3 3 Maintenance 9 1 calibration 9 35 flushing the cylinder 9 17 Index 1 D Series Syringe Pumps Index Index 2 general cleaning 9 18 lubrication 9 12 motor brush replacement 9 23 power supply voltages 9 11 removing the case top 9 9 replacement parts A 2 A 56 seal cleaning and replacement 9 13 shear key 9 19 solvent changeover 9 17 Teledyne Isco S
187. e Department before returning the unit for factory repair Often a problem can be solved in the field with just a little extra help Contact us at Toll free 800 775 2965 Outside USA Canada and Mexico 402 464 0231 Email IscoService teledyne com In the rare event that an instrument must be returned for main tenance the following measures must be taken to ensure a proper return Teledyne Isco Technical Service 800 775 2965 must be contacted prior to shipment to obtain a clean return form The applicable MSDS paperwork of the last substance ran must be received by Technical Service The syringe pump must be shipped with the cylinders removed from the pumps and any residue completely rinsed with methanol or water Wrap the unit in heavy paper or a plastic bag If the original box is not available put the wrapped unit in a strong cardboard box at least six inches longer in each basic dimension than the unit Fill the box equally around the unit with resilient packing material Sealit with strapping tape and ship it to the address on the warranty The warranty at the end of the manual also describes the conditions under which Teledyne Isco will pay surface shipping costs NOTICE Do not return the pump without contacting the Teledyne Isco Technical Service Do not return the pump without first providing written guarantee that it has been decontaminated of hazardous or potentially lethal materials
188. e aq ure aback beige ond 1 1 1 3 Unpacking a 4 eel ds en EISE a ees 1 13 1 4 Controls and Indicators ane eee en 1 14 1 5 Electrical Connections 1 18 15 1 Cabling Asen ci ses aren dar ander ee an hebt Darf 1 19 1 6 Preliminary Checkout eee een 1 21 Section 2 Fluid System Connections and Accessories 2 l Introduction SE ES E Ve I CE ARTE ra ae 2 1 2 2 Fluid System Connections 2 1 2 2 1 POTS aan PH d ERU D ES REUS P S 2 1 2 2 2 Installation Tips 2 2 ee EEE 2 2 2 2 3 Tubing Requirements 2 2 2 2 4 Accessory Packages oan en eee 2 3 2 2 5 Installing the 1 16 Fittings 260D 65DM and 100DM DX only 2 4 2 2 6 Draining Overflow eene 2 5 2 2 7 Cylinder Washing Wash Gland 2 5 2 2 8 Cylinder Washing Nitrogen 2 7 2 2 9 Flushing Pumps with External Transducers 2 8 2 3 Fluid Connection 1 2 8 2 3 1 Manual Refill Kit eee 2 8 2 3 2 Manual Outlet Valve 2 9 2 3 8 Cylinder Connection Package 2 10 2 3 4 In Line Filter 2 11 2 4
189. e display will show each pump s information and allow you to select any pump for program ming changes The pump has three delivery modes and one refill mode When using a single controller to operate multiple pumps inde pendently you need to select the appropriate pump run screen before selecting a mode To select the appropriate pump press SELECT PUMP D and an intermediate screen will be shown Press the softkey for the appropriate pump the run screen for that pump will appear Constant Flow Refer to Section 3 10 1 This mode is used when the flow rate must remain constant during the pumping operation Constant Pressure Refer to Section 3 10 2 D Series Syringe Pumps Section 3 Basic Programming and Operation 3 10 1 Constant Flow 3 10 2 Constant Pressure 3 16 The constant pressure mode is used when the application of fixed pressure throughout the pumping operation is required The pump will maintain the desired pressure by positive or negative displacement of the piston Programmed Gradient Refer to Section 4 In the programmed gradient mode the pump can provide the fol lowing types of gradient Two pump concentration gradient on pumps A and B e Single pump linear pressure gradients on pump A e Single pump flow programs on pump A Dispense For applications requiring delivery of a specific volume Refer to Section 3 10 3 Refill Refer to Section 3 4 3 You can set the refill rate and change it when in ref
190. e port and use a single port as both the inlet and outlet Standard port information e 1000 NPT e 500D 16 NPT 65DM 100DM DX 260D l Valco e 65D 30D l4 F250C 500HPx 28 NPT M Note Custom caps are available with different port configurations and sizing Contact the factory for details D Series Syringe Pumps Section 2 Fluid System Connections and Accessories Pressure Transducer gt Nut amp Collar a Tubing to valve Pressure transducer cap Nut amp Ferrule Nut Tubing to valve Plug Figure 2 1 Liquid system plumbing connections 30D on 2 2 Left 2 2 2 Installation Tips 2 2 3 Tubing Requirements Purchased cut tubing Cutting the tubing Be sure to keep the tubing as straight as possible at the end as this will make it easier to install the ferrules Be sure to cut the ends of the tubing squarely Do not leave burrs on the ends of the tubing When installing ferrules on the tubing be sure the tubing extends beyond the ferrule to allow for proper crimping Ifthe connection leaks retighten fittings Push the tubing completely into the port before tight ening the nut When connections are made to the cylinder cap the pressure reading may be affected If the pressure no longer reads
191. e to the HPx or 30D pump models Standard calibration for the transducer is a two point adjustment at zero and maximum pressure The midpoint adjustment number is the difference between the pressure at half maximum as read by a pressure gauge with a precision of 0 25 accuracy and the syringe pump transducer output Figure 3 8 Location of transducer midpoint value 3 8 3 6 4 Diff Modes 3 6 5 Press Integral 3 6 6 Pressure Deadband 3 7 Menu Four 3 7 1 Modbus Options D Series Syringe Pumps Section 3 Basic Programming and Operation Press CALA CALB CALC or CALD to select the correct pump enter the calibration number and press ENTER This feature allows the use of other analog inputs for pressure input to the pump The standard pressure transducer MUST be connected to pump in order for this feature to work Press 1 OFF to turn off this feature Press 2 0 to 50 ANLGI to use a 5 volt 50 psi transducer on ANALOG INPUT 1 of the ACCESSORY connector Press 3 Custom ANLGI to use 5 volt custom pressure transducer on ANALOG INPUT 1 of the ACCESSORY connector Press 4 500 ANLG2 to use a 5 volt 500 psi pressure transducer on ANALOG INPUT 2 of the ACCESSORY connector Press 5 5000 ANLG3 to use a 5 volt 5000 psi transducer on ANALOG INPUT 3 of the ACCESSORY connector The pressure control algorithm can be adjusted by turning OFF the integral compensation This may be desirable at very low flow rates or du
192. eatures are being pro grammed For complete information about programming menus refer to Sections 3 3 through 3 7 3 1 D Series Syringe Pumps Section 3 Basic Programming and Operation 3 2 3 Run Screens The run screen appears once a program has been loaded and the pump is running The run screen which is determined by your program selections displays current information about pump operation The fol lowing sections explain the display line by line Line One No matter what mode you are in the first line ofthe run screen is always the same Active Pump Actual Pressure PGa 000 mL MIN PSI XXX XX ml L_ Current Mode Volume Remaining Actual Flow Rate Line Two The second line varies slightly depending on the operating mode A file or step will only be displayed when oper ating in the gradient mode Elapsed Time STOPPED FILE STEP 000 00 00 Step of program running or Status loaded file number Line Three Line three varies depending on the mode the rate and units are set by the user so these will vary depending on your programming requirements The ending time will always be displayed on this line Ending Time Current Pressure PS MIN FINAL PSI 00 00 00 Final Pressure Rate Line Four Line four varies depending on the mode The options presented on this line are softkey selectable i e you use the softkeys A D located under the screen to choose the option 3 2 3 2
193. ections 3 3 3 2 Units MENU PE 3 3 3 3 Menu 2 program selections 3 5 3 4 Serial option menu venen 3 6 3 5 Total volume reset oaeen eee eee eee eeen 3 6 3 6 Types of valves naan ee x px a Denn a 3 7 3 7 Menu 3 program selections 3 8 3 8 Location of transducer midpoint value 3 8 3 9 Limits menu uoo qu epe eR ew ne que ni ae 3 11 3 10 Limits setpoint Max Press menu 3 11 3 11 Depiction of dispense mode sequence 3 17 3 12 External control for refill 3 20 3 13 Button sequence for external control setup 3 21 3 14 Analog voltage output connection rear panel 3 22 3 15 Output range selection jumpers 3 23 4 1 Pump inlet connections 4 4 4 2 Pump outlet connections 4 5 4 3 Dual gradient system connections Inlet valves A amp are from refill valve kits 4 7 4 4 Dual gradient connections Detail 4 7 5 1 Check valve package installation 65DM 100D 265D 500D pumps 5 4 5 2 Check valve package installation 10
194. ections and Accessories 3 Run the pump until the display shows CYLINDER FULL M Note This will fill the pump with air to prevent spills later 4 Toggle the STANDBY switch on the controller turning off the controller display 5 Toggle the POWER switch on the pump to turn off the pump 6 Unplug the pump from the MAINS power 7 Disconnect the transducer connector from the top of the transducer Figure 2 13 and position the cable out of the way 8 Place the two parts of the CYLINDER HOLDER part of Wrench Kit 60 1249 132 onto the pump cylinder just below the threads for the cylinder cap approximately 1 4 6 mm below the cylinder cap Figure 2 14 Cylinder holder Hex wrench Figure 2 14 Secure screws with the 1 4 hex wrench M Note If your pump has a cooling jacket installed assemble the CYLINDER HOLDER below the cooling jacket 9 Install the 5 16 18 X 1 Cap Screws supplied with the Wrench Kit to hold the two parts of the CYLINDER HOLDER in place Figure 2 14 10 Tighten the cap screws referred to in step 9 above with the hex wrench supplied with the Wrench Kit as shown in Figure 2 14 securing the CYLINDER HOLDER to the pump cylinder 11 Using the two wrenches supplied with the Wrench Kit remove the cylinder cap assembly Figure 2 15 2 15 D Series Syringe Pumps Section 2 Fluid System Connections and Accessories Cap assembly Wrenches Figure 2 15 Removing the cylinder
195. ed in an isolated environment designed for these types of materials in accordance with federal state and local regulatory laws and in compliance with your company s chemical hygiene plan in the event of a spill In all cases when using Teledyne Isco instrumentation prudence and common sense must be used B gt WARNING Team lift To reduce the risk of injury do not attempt to lift this instrument independently It is highly recommended that a team be used when lifting this instrument gt D Series Syringe Pumps Warnings Cautions and Notices AVIS viter de r pandre Les liquides qui sont pomp s dans cet instrument peuvent tre canc rigenes hasards biologiques inflammables ou radioactifs Si vous devez utiliser ces liquides hasardeux il est tr s recommand que vous le faites l int rieur d un environnement isol concu pour tels liquides Cet environnement isol devrait tre construit selon les reglements f d raux provinciaux et locaux aussi que le plan de votre organisation qui concerne l v nement d un accident avec les matieres hasardeuses En tout cas utilisez toujours l instrumentation d Isco avec prudence et sens commun gt gt gt ATTENTION Risque de pincement Ce symbole vous avertit que les mains ou les doigts recevront une blessure s rieuse si vous les mettez entre les l ments en mouvement du m canisme pr s de ce symbole ATTENTION viter les usages hasardeux
196. een ea ran 7 2 7 1 3 Modbus Configuration Options 7 2 Section 8 Serial Interface 8 1 8 2 8 8 8 4 8 5 8 6 Overview anne hassen bao asi kun 8 1 Network Control and 8 2 USB Interface 22622 aerden e e Re eR Roe ea abe 8 3 Cabling for Serial 1 8 3 84 1 One Controller RADIIS e ae eee et 8 3 8 4 2 Two Controllers Compiler required 8 4 8 4 3 Three or More Controllers Compiler required 8 4 Serial Control Check 1 8 8 5 Controller Setup ten Zon ceo nee eb Pe ie ele e 8 5 8 6 1 Restore Defaults if desired 8 5 8 6 2 Change Defaults en ee eee 8 5 8 6 8 Verify Operation seo secure dieo een 8 6 XV D Series Syringe Pumps Table of Contents xvi 8 7 User written Software 8 6 8 7 1 DASNET tronen eden nente RARUS ag na nee gan ende PU MSS 8 6 8 7 2 Universal Driver from Teledyne Isco 8 7 8 8 Serial Commands for the D Series Pump 8 20 8 8 1 Get Status Command 8 25 8 8 2 Gradient Download Command 8 29 8 8 8 Gradient Uplo
197. en Advertencias y Precauciones Esta se al alerta sobre la presencia de alto voltaje en el interior del producto Esta se al le advierte sobre la importancia de las instrucciones del manual que acompanan a este producto D Series Syringe Pumps Warnings Cautions and Notices To prevent damaging the instrument or injuring yourself it is absolutely necessary that you understand everything in English above all technical terms before operating the instrument Otherwise it is necessary for you to receive complete instruction from someone qualified who understands both the instrument and English very well Um eine Besch digung des Ger tes oder eine Gef hrdung des Anwenders zu vermeiden ist es notwendig da dieser vollstandig die englische Sprache und die technischen Bezeichnungen beherrscht Oder der Anwender mu von einer Person einge bt werden die bereits vorher dieses Ger t bedienst hat Pour emp cher dommage l instrument ou blesser vous m me il faut absolument que vous compreniez tout en anglais surtout les termes techniques avant d actionner l instrument Autrement il faut que vous receviez l instruction parfaite d une personne tr s comp tente qui comprend bien les deux l instrument et anglais Para prevenir cualquier dano en el instrumento o en el operador es necesario que el usuario comprenda perfectamente el lenguaje ingl s y las t rminos t cnicos intr nsecos o bien ser f
198. end to have a lower percentage flow rate due to port size restrictions with a maximum flow rate equal to that of the E500D system see Table 5 5 Electric Valve Package Numbers E1000D 68 1247 109 E500D 68 1247 091 E65DM E260D E100DM E100DX 68 1247 090 M Note Electric valves are not available for the 65D and 500HPx pumps Please consult the factory for options Electrical valves can only be used with pumps A B 5 4 1 Technical Dual system maximum flow rates under optimal conditions are Specifications approximately 65 of the max flow rate for each pump model Table 5 5 Continuous Flow Technical Specifications Electric Valves Pressure fluctuation at switchover 0 35 bar at system backpressures from 6 9 bar to the single pump maximum Higher fluctuation occurs at pressures below 6 9 bar Minimum 3 5 bar Maximum system backpressure The single pump maximum Valves rated to 689 5 bar Maximum flow rate ml min Liquids 6596 of the single pump E1000D 132 6 maximum rate E500D 132 6 excluding E1000 systems E260D 69 55 E100DX 32 50 E100DM 16 25 E65DM 19 50 Liquefied gases 4596 of the single pump maximum rate Cylinder cooling jack ets should be used to obtain this rate Temperature range 0 to 40 C Wetted materials in valve packages Check valves SS316 sapphire ruby PEEK PTFE Tubing and fittings SS316 gold 5 13 D Series Syringe Pumps Section 5 Continuous Flow Introduction
199. erminal emulator program on your computer such as HyperTerminal and establish con nection with the controller M Note If you will be using multiple controllers daisy chained to a sin gle serial port you must connect and test each controller one at a time 1 Press MENU gt MORE A gt MORE A and select DIAGNOSTIC MENU 2 2 Select SERIAL TEST 6 The SENT value displayed will increment indefinitely until you exit the test by pressing any key This same value should appear on your computer screen If it does not verify that you are using the correct serial port on the computer and that the communi cation cables are properly connected and in working order When designing software to control the D Series pumps you must follow the DASNET communications protocol This protocol allows a number of instruments to be controlled from a single RS 232 C serial port Up to seven D Series controllers may share a single serial data channel with each controller only accepting commands that are meant for it Each pump controller can then control up to four pumps each Figure 8 1 shows a simple system where the PC is connected to the serial port on the rear panel of the pump controller shown sitting on top of the pump module The pump control cable is attached to the pump A connector on the rear panel of the controller DASNET converts your direct serial commands into a form rec ognizable to our instruments Using a computer language
200. ert the new brush into the slot needlenose pliers rec ommended 6 Push the spring down into the slot in the motor You may need to use the edge of the screwdriver to gently press the metal tabs on the spring down into the slot Reinstall the brush retainer tightening it with the screw driver do not overtighten Figure 9 17 Inserting new motor brush Cable Tie Figure 9 18 For 30D a cable tie holds the wires together 9 25 D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing 9 13 2 HPx Motor Brush This section goes through the various steps needed to replace the Replacement HPx motor brush The following tools are required e 2 Phillips screwdriver e Flat blade screwdriver 64 hex wrench M Note Completely read these instructions before proceeding Disassembly of Motor 1 Remove the two screws and flat washers that hold the Brush deflector shield in place then remove the plate Figure 9 19 Screws and washers Figure 9 19 Remove screws and washers then the plate 2 Lay the pump on its side and remove five screws and lock washers on the bottom of the pump that secure the circuit board mounting plate and the motor mounting plate to the bottom of the case Figure 9 20 Figure 9 20 Remove the five screws from the bottom of the pump 3 Return pump to an upright position 9 26 D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Serv
201. ervice 9 2 torque limiter 9 18 wear ring 9 17 Master network 8 9 Menus display contrast 3 5 main menu 3 3 power failure 3 5 pump status 3 6 refill 3 4 serial options 3 6 total volume reset 3 6 Modes of operation 3 15 Monitoring flow rate 3 22 Multi pump 3 6 key functions 3 14 5 17 B 8 N Network 8 9 Noise reduction 2 12 Operating modes 3 15 Operational test 1 21 Outlet valve accessory package 2 9 Parts A 2 A 56 Power failure actions 3 5 Preliminary checkout 1 21 Pressure drift 3 13 limits setting 3 10 rapid pressurization 3 12 Pump front panel 1 18 rear panel connectors 1 17 status 3 6 R Refill kit 2 8 Refill rate setting 3 4 Remote run stop 3 21 Repairs 9 2 Replacement parts A 2 A 56 Returning equipment 9 2 S Safety 1 i 1 ix Seals break in procedure 9 14 cleaning and replacement 9 13 Serial control cabling 8 20 commands 8 20 error messages 8 34 examples 8 15 set up 8 34 Serial options 3 6 Service Department 9 2 Slave network 8 9 Software continuous flow 5 16 B 7 DASNET 8 6 example BASIC 8 8 example C 8 9 user written 8 6 Solvent changeover 9 17 Specifications 1 2 1 3 1 4 1 10 Supercritical fluid extraction 6 1 modifier addition 6 6 preparation for modifier 6 4 refilling the pumps 6 8 System preliminary checkout 1 21 T Technical specifications 1 2 1 3 1 4 1 10 Total volume reset 3
202. eset total volume see Figure B 4 Equilibration When the pumps begin running the system will go through an equilibration phase during which both pumps must be full and delivering fluid Additional guidelines Please become familiar with the fol lowing guidelines Pressure limits for continuous constant flow mode are set by the limits of pump A for the A B pair and pump C for the C D pair Temperature changes can cause pressure fluctuations For available temperature control options contact Teledyne Isco For correct overpressure response shutdown must be set to ON under PUMP LIMIT options Enter the same refill rate separately for pumps A B C and D The refill rate should always be as high as possible to allow time for refill and repressurization before the next switchover B 13 List B 6 1 30D Pump Appendix B Continuous Flow Introduction Installation and Operation for 30D D Series Syringe Pumps B 6 Replacement Parts EU 0000 a gt 3 NV FU _ D 4 Q V lt XQ A B 14 D Series Syringe Pumps Appendix B Continuous Flow Introduction Installation and Operation for 30D 601262101 REPLACEMENT PARTS LIST SHEET 2 OF 3 TELEDYNE ISCO PART NUMER DESCRIPTION 120000701 120001300 141400102 15000060 201032900 133100 42990 02206223 09016100 09016402 9016403 233613600 HOKE POWER FILTER KT D SUB 9 CONT RK FLSF RVS 24V KB
203. ew 14 Grasp the connector on one of the orange wires and wiggle the connector to loosen the brush then gently pull the brush out of the motor Once out disconnect wire from brush Repeat this process for the second orange wire 9 31 D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing Figure 9 32 Loosen the connector 15 Connect the bottom orange wire to the new brush and insert the new brush into the motor using the connector as leverage to guide brush into the motor Hold the connector so the brush is fully engaged into the motor Figure 9 33 then reinstall the set screw that holds brush in place Repeat this process for the top orange wire Figure 9 33 New brush reinstalled set screw replaced Reassembly of Motor 1 Install the small support plate on the bottom of the blue Brush motor mounts so the adhesive side is against the rubber mounts Figure 9 25 2 Carefully slide the motor assembly back into the case so the motor gears mesh with the brown gear in the bearing plate and the motor plate fits over the two locating pins It may be necessary to spin the motor gears to get the teeth to align with the brown gear Do not force the gears to fit or damage to the gear teeth may occur 9 32 Figure 9 34 Location of locating pins D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing Locating Pin Once the motor plate is located properly over the
204. fications 5 13 5 4 2 Dual Electric Valve Installation 5 14 User Supplied Valves ann sa nase SR 5 16 Continuous Flow 5 17 5 6 1 Defining Operation 5 17 5 6 2 Constant Flow Mode E 5 18 5 6 3 Constant Pressure Mode 5 19 5 6 4 No Check Valve 0 eee ee 5 20 5 6 5 To R n Or Stops SSD en er Bee ee ne ea ER 5 21 5 6 6 Tips for Running Continuous 5 21 Section 6 Modifier Addition 6 1 6 2 6 3 Overview ve ee S e te es ba c eb heek e 6 1 6 1 1 Installing the Kat anne en IR ee see 6 1 6 1 2 Modifier Mode Setup 6 4 6 1 3 Two Pump 6 5 Programming veis ade ve wan EE EEUU E Ce WERE RE 6 6 6 2 1 Mininum Modifier Pressure Setting 6 7 6 2 2 Modifier Concentration 6 7 TESTEN RS TE Td 6 8 Section 7 Modbus Configuration 7 1 Overview nei eet eid Ket a CAE E TEE 7 1 TAA Modbus RU ii 2 oere man a ar a a Eu E ni 7 1 71 1 2 Modbus TCP IP p osios enc ner eer w
205. file number between 1 and 99 This is the file name of your program and can be the name of a new program you are creating or a stored program you want to edit or run Press ENTER M Note If a selected stored program is in a different mode than that of the controller selected in Step 1 a brief notification will appear displaying the controller s mode and the file s mode If you attempt to run the program without changing the mode of either it or the controller the program will not run and the same message will be displayed 4 To enter the flow rate for this program either press FLOWRATE A and use the number keys and Enter or for maximum possible flow simply press MAX C D Series Syringe Pumps Section 4 Gradient Pumping for Pressure Flow and Concentration Modes ENTER FLOWRATE 0 00000 XX 00000 V FLOWRATE PREVIOUS MAX 5 To proceed to the programming screen press STEP FWD B The programming screen will appear with the file number and step number at the top of the screen FGa FILE 1 STEP 1 STORE TO EXIT 1 INIT96 3 0 00 MIN 2 FIN 4 DURATION 1 0MIN INSERT DELETE 6 To set the initial pressure or flow for this step press INIT 1 to activate this parameter Use the number keys to enter the desired value then press ENTER to save it 7 To set the final pressure or flow for this step press FINAL 2 to activate this parameter User the number keys to enter the desired va
206. flag limit 1 Pump B at upper Flag Limit Empty 0 Pump B not at lower flag limit 1 Pump B at lower flag limit Full 1 Pump B is overpressure 1 Pump B is underpressure 1 Motor failure Pump B 0 Transducer of Pump C not connected 1 Transducer of Pump C connected 0 Pump not at upper flag limit 1 Pump C at upper Flag Limit Empty 0 Pump C not at lower flag limit 1 Pump C at lower flag limit Full 1 Pump C is overpressure 1 Pump C is underpressure 1 Motor failure Pump C 0 Transducer of Pump D not connected 1 Transducer of Pump D connected 0 Pump D not at upper flag limit 1 Pump D at upper Flag Limit Empty 0 Pump D not at lower flag limit 1 Pump D at lower flag limit Full 1 Pump D is overpressure 1 Pump D is underpressure 1 Motor failure Pump D 1 POOR FILL A ERROR 1 POOR FILL B ERROR 1 POOR FILL C ERROR 1 POOR FILL D ERROR 1 VALVE ERROR DIGITAL IN 1 DIGITAL IN 2 DIGITAL IN 3 DIGITAL IN 4 gt gt gt D D D D D D D D D D D D D D D D D D D D gt Table 7 6 Holding Registers of Registers Register Description Pressure set point for Pump A in Constant Pressure mode Pa PSI See Pressure set point for Pump B in Constant Pressure mode Pa PSI See Pressure set point for Pump C in Constant Pressure mode Pa PSI See Pressure
207. g fitting for Ine fitting for Ine Outlet Outlet Vg nut and ferrule Vg nut and ferrule 100 260D or male 0 18 100 2600 male 8 18 T 7 connector 5000 9 Pre swaged pum Nie Pre swaged pi pr connection tubin connection tubin Strap d Q 1 of 2 Inlet tee Inlet tee 2 total 2 total Check valve Check valve Inlet cus tomer omer Actuator Actuator To controll Red wj To controlle Red wires Mh n cin m Bracket pan Front Vi head Bracketpan Front View head ACCE DIGITAL GROUND SQRY IGITAL UT PUT INPUT A B C D G 0 10V 1 213 4156178011234 Ogg DIGITAL INPUT ALOG 15 1234 OOo Control Panel Rear Wire pair conversion table for A B Pump Pair and C D Pump Pair A B Pum Digital D Pum Digital 2 Wire Pair On aie Pair Al Al 15 Al C5 15 A2 A2 15 A2 C6 15 B3 B3 15 B3 D7 15 B4 B4 15 B4 D8 15 Figure 5 3 Air valve installation for 65DM 100DM DX 260D and 500D pumps 5 9 D Series Syringe Pumps Section 5 Continuous Flow Introduction Installation amp Operation Outlet a Pre swaged 3 8 male connector tubing
208. g zeros must be included so that the numerical values are represented properly Also note that the single pump gradient commands include spaces in the command string Step Number 01 LGDL F xx S 01 FL xxx Xxxxx I xx xx F xXx Xxx D XXXX X Gradient Duration Range 0000 1 9999 0 minutes Final Gradient Percentage Range 00 00 100 0 Initial Gradient Percentage Range 00 00 100 0 Gradient Total Flow Rate Units milliliters minute Range 000 0000 Maximum Flow Rate Step Number 01 File 01 99 Step Numbers 02 through 99 LGDL F xx S xx I xx XX F XX XX D XXXX X Gradient Duration Range 0000 1 9999 0 minutes Final Gradient Percentage Range 00 00 100 0 Initial Gradient Percentage Range 00 00 100 0 Step Number 02 99 File 01 99 Figure 8 7 Gradient Download Commands Single pump flow gradient 8 29 D Series Syringe Pumps Section 8 Serial Interface Step Number 01 LGUL F xx S 01 FL xxx xxxx IB xx xxX FBS xx xxX D XxxX X i L Gradient Duration Range 0000 1 9999 0 minutes Final B get Range 00 00 100 0 L Initial B Range 00 00 100 0 Gradient Total Flow Rate Units milliliters minute Range 000 0000 Maximum Flow Rate Step Number 01 File 01 99 Step Numbers 02 through 99 LGU
209. guration Options tem Vae Description 300 1200 2400 4800 9600 Communication Speed Default 19200 38400 57600 115200 19200 Slave ID 1 247 Device address Default 1 Baud Rate 7 2 D Series Syringe Pumps Section 7 Modbus Configuration Table 7 2 Modbus RTU Configuration Options Even 1 Stop Bit Odd 1 Stop Bit None 1 Stop Bit None 2 Stop Bit Communication parameters Default Even 1 Stop Bit Word order for 32 bit integers and IEEE 754 floating point Word Order Big Endian Little Endian numbers Big Endian AB CD Little Endian CD AB Default Big Endian Time to transmit single charac Min Baud Rate ter t1 Used to calculate inter Character Time dependent frame and inter character Max 999ms space t1 5 13 5 50 m sec default Table 7 3 Supported Modbus Function Codes Function Code Description 01 Read Discrete Output Coils 03 Read Analog Output Holding Registers Write Single Discrete Output Coil Write Multiple Discrete Output Coils Write Multiple Analog Output Holding Regis ters Table 7 4 Exception Responses Exception Code Name Description Function code received is Illegal Function not supported Data address received is Illegal Data Address not an allowable address A value contained in the query data field is not an allowable value for the addressed location This may indicate a fault in the structure of the remainder of a complex request
210. gure 2 3 for components and fittings for the 30D 65D Slotted collet Gland Ta La Valve or Collet grips tubing fitting body here for anti vibratio Collar AE TJ P i Line contact sealing Figure 2 3 30D 65DFitting 2 4 2 2 6 Draining Overflow Figure 2 4 Drain tube installation 2 2 7 Cylinder Washing Wash Gland D Series Syringe Pumps Section 2 Fluid System Connections and Accessories The drip tray outlet on the pump cylinder provides a means of draining fluid from seal leakage Use the ID flexible tubing included with the accessory package to divert the leakage away from the pump To install the drain tube push one end of the tubing over the end of the drip tray outlet as shown in Figure 2 4 The 1000D has two drain tube outlets one for the drip tray and one for the splash pan located at the bottom of the pump see Figure 2 5 The 1000D also includes a wash gland as a stan dard feature see the following section for details The wash gland tubes can also be used as lines for draining away fluid Drip tray outlet A thin film of liquid wets the inside of the cylinder each time the piston travels up the cylinder The lowest flow rates are con ducive to the most abrasive or corrosive pumping environments as the deposited film remains on the inside of the cylinder wall for the longest time The Model 1000D syringe pump is equipped for cylinder washing with two 1 8 tubes on the back to
211. he RUN STOP pin low to enable the pump Thereafter the RUN STOP pin will control operation Pressing STOP on the front panel will override the RUN STOP pin Two wires are required for external RUN STOP control The digital common or ground wire should be connected to one of the four DIGITAL GROUND terminals of the ACCESSORY con nector on the controller rear panel The control wire should be connected to terminal 1 under DIGITAL INPUT If an electri cally isolated relay is used one relay terminal should be con nected to digital ground and the other to terminal 1 under DIGITAL INPUT 3 21 D Series Syringe Pumps Section 3 Basic Programming and Operation 3 14 Analog Flow Rate and Volume Output Options 3 14 1 Voltage Analog Output Iftwo pumps are used with the controller the second control wire should be connected to terminal 2 under DIGITAL INPUT Ifthree pumps are used with the controller the third control wire should be connected to terminal 3 under DIGITAL INPUT If four pumps are used with the controller the fourth control wire should be connected to terminal 4 under DIGITAL INPUT For the 4 20ma option the negative current wire is connected to DIGITAL GROUND and the positive should be connected to DIGITAL INPUT The analog output option provides for analog monitoring of the syringe pump flow rate If two or less pump modules are con nected to the controller pump volume delivered can also be mon itored via a
212. he control cable when the pump is con nected to the mains voltage ACCESSORY These terminals allow connection of input and output signals such as analog controls and external RUN STOP RS 232 RS 485 This serial port connector may be used with an RS 232 or RS 485 cable to place the pump under remote control Refer to Section 8 for RS 232 and Section 7 for RS 485 pin connections USB ETHERNET Optional circuit provides USB and Ethernet functionality Refer to Section 8 for USB pin connections and Section 7 for Ethernet pin connections 4 20mA OUTPUT ANALOG OUTPUT ELECTRIC VALVES 12 CH OUTPUT D Series Syringe Pumps Section 1 Introduction Optional circuit provides 4 20mA current loop output and additional digital inputs and outputs Optional circuit provides flow rate and volume outputs See Section 3 9 Optional circuit provides motor drive for valve operation Additional circuit provides flow rate pressure and volume outputs DIGITAL 1 02 ANALOG OUTPUT Optional circuit provides additional digital inputs and outputs Optional circuit provides flow rate and volume outputs See Section 3 9 SERIAL TAG This tag indicates the serial number of the instrument CHASSIS GROUND Ground point for high static or remote controller installations a Connectors based on installed optional circuit board configuration doo 6 PRESSURE OUTPUT TRANSDUCER
213. he number key to set 10 ml min Press the ENTER key Press REFILL After the lower limit sensor is interrupted the motor will stop Press CONST FLOW Press A FLOW RATE and select MAX Press RUN Press STOP when the volume counter in the upper right hand corner of the LCD reads 005 00 ml or less Press A FLOW RATE and enter 5 ml min Press RUN Press STOP when the counter reads 000 30 or less Press A FLOW RATE and enter 1 ml min Press RUN When the counter counts from 000 01 to 000 00 press STOP Lower the upper limit sensor to the point where the flag just interrupts the sensor CYLINDER EMPTY will flash on the screen Tighten the top upper limit mounting screw Turn the controller to STANDBY and disconnect the pres sure cable Screw the cylinder into the cylinder mounting block until the cylinder bottoms firmly against the stop ring in the cyl inder mounting block the cylinder will no longer turn Do not overtighten Unscrew the cylinder a minimum of turn then line up the inlet and outlet ports as you had them before Do not unscrew the cylinder more than one full turn from the stop position Lock the cylinder by tightening the locking screw Connect the pressure cable and power cord and turn the controller ON Press REFILL Wait until you have access to the second upper limit sensor mounting screw and tighten it 9 39 D Series Syringe Pumps Section
214. his is the same value entered when setting LIMITS as described in Section 3 of your user manual for MAX PRESS or MAX FLOW V Volts per unit of flow or pressure U Incremental unit of flow or pressure Vmax Maximum input voltage M Note For the 4 20ma input option The maximum flow or pressure sets the limit at 20ma No other formula applies The refill option allows you to set the refill rate or set the pump to automatically refill when a certain volume is reached From Menu 2 the system can be programmed to automatically refill a pump based on an external analog signal with a range of 0 to 11 5 volts To access this feature press MENU gt MORE A gt EXTERNAL 3 D Series Syringe Pumps Section 3 Basic Programming and Operation FULL SCALE INPUT RANGE XX XXX VOLTS OFF OFF SETRANGE EXTERNAL REFILL PREVIOUS Figure 3 12 External control for refill menu 3 12 4 Calculation Examples 3 12 5 Setup 3 20 To set the full scale value maximum 11 5 volts press SET RANGE A enter the desired value and press ENTER To place the pump under external control press EXTERNAL B The feature will turn from OFF to ON To SET the external control for refill press REFILL C The feature will turn from OFF to ON Flow Rate If MAX FLOW is set at 25 ml min in the LIMITS menu and the desired scale factor is 5 0 volts per 20 ml min do the fol lowing to determine the analog voltage range 35 25x 3
215. hnical Specifica tions Electric Valves Pressure fluctuation at 3 44 bar at system back pressures from 6 9 switch over bar to the single pump maximum Higher fluctuation occurs at pressures below 6 9 bar Minimum 3 5 bar Maximum system back The single pump maximum Valves rated to pressure 2068 bar Maximum flow rate ml min Liquids 65 of the single pump maximum rate excluding E1000 systems Liquefied gases 45 of the single pump maximum rate Cyl inder cooling jackets should be used to obtain this rate Temperature range 5 to 40 C Wetted materials in valve package Tubing and fittings SS316 gold B 4 D Series Syringe Pumps Appendix B Continuous Flow Introduction Installation and Operation for 30D B 3 2 Dual Electric Valve To install the electric valve package refer to Figure B 2 on the Installation following page 1 Position the valve bases 1 3 cm apart 2 Use the plugs to stopper the ports that will not be con nected NDANGER RISK OF INJURY THE PRESSURE PRODUCED COULD BE 2068 BAR PLEASE UTILIZE APPROPRIATE TUBING AND CONNECTIONS NOTED IN THE MANUAL 3 Loosely attach the tubing lengths from the valve assembly to the pumps 4 Install the four bracket panhead screws on the bottom of the bracket Plumbing connections 5 Tighten the tubing nuts 6 Connect the inlet tube to the supply reservoir Connect the outlet tee to your apparatus Electrical connections
216. icing 4 Unplug the two pin connector Figure 9 21 Figure 9 21two pin connector 5 Unplug connector from the encoder by carefully pulling down on the connector Figure 9 22 Encoder 9 27 D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing 6 Remove the three screws and three flat washers that hold the motor plate onto the bearing plate Two of the screws are on top and the third screw is down below the fan Fig ure 9 23 Figure 9 23 Location of screws and washers holding the motor in place 7 Slide the motor assembly straight back until the motor gears clear the bearing plate then lift the motor assembly completely out of the case Figure 9 24 Motor assembly 8 The small support plate on the bottom of the mounting plate is adhered with doubled sided tape Remove the sup port plate and set aside for now It will be reused when the motor assembly is reinstalled into the case Figure 9 25 9 28 D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing Figure 9 25 Support plate M Note Make a note of the position of the two orange and two black wires connected to the motors Marking them Top and Bot tom may help keep them straight during assembly Figure 9 26 Position of wires connected to the motors 9 The wire connections from the motors to the terminal strips are shown in Figure 9 27 Orange Orange Top B
217. ies Syringe Pump Accessory Packages 2 3 2 2 Manual Refill Kits eee ehm 2 9 2 3 Manual Outlet Valve Kits eenen eee eee 2 10 2 4 Cylinder Connection Package 68 1247 043 2 10 2 5 Optional in line Filter Package 68 1247 011 2 11 2 6 Packages and Parts au tonen ee ae OE D 2 14 2 7 Seal Selection Chart oee eee eee ee 2 20 3 1 Key functions in the Multi pump Mode 3 14 3 2 Analog Output Options connections to female 25 pin Sub D 3 23 3 3 Analog Output Signal Sub D Pins for 4 20mA 3 24 3 4 Analog Output Signal Sub D Pins for 0 10 VDC 3 25 4 1 Manual Refill Valve Kits neee eee eee 4 1 4 2 Manual Outlet Valve Kits eenen eee een eens 4 2 423 Swaging Detail s raini was etn a beak ea pi 4 2 5 1 Continuous Flow Technical Specifications Check Valves 5 2 5 2 Continuous Flow Check Valve Package for 100D 260D 500D part 68 1247 059 5 5 5 3 Continuous Flow Check Valve Package for 1000D part 68 1247 128 5 6 5 4 Continuous Flow Technical Specifications Air Valves 5 7 5 5 Continuous Flow Technical Specifications Electric Valves 5 13 5 6 Accessory Control Digital Outputs 5 16 5 7 Key functions in the Multi pump Mode
218. ify the program in any way you must have the complete LabView Compiler available from LabView s manufacturer National Instruments Corporation www ni com Tel 800 531 5066 Fax 512 683 8411 11500 N Mopac Expwy Austin TX 78759 3504 This section ofthe manual provides detailed information about Cable Connections for Serial Control Setting up the Controller s for Serial Control DASNET Protocol Serial Commands 8 1 D Series Syringe Pumps Section 8 Serial Interface 8 2 Network Control and Network communications are always initiated by the network Communication controller which is typically a computer Messages from the instruments are in response to messages from the network con troller All information on the network is transmitted as groups of ASCI characters called frames The message frames contain the origin of the message the destination of the message and a checksum to verify the validity of the message Each instrument is provided with a method of selecting unit identification numbers and a baud rate For proper operation each instrument must be set to a unique unit identification number see Section It is also important that each unit s baud rate is set to the same speed Possible baud rates are 1200 and 19200 Other baud rates of 300 1200 2400 4800 9600 19200 38400 57600 and 115200 are supported by the D Series pumps but are not part of the Teledyne Isco defined communications standard Electrica
219. ill cause leaking If either the cylinder or seal has been scratched it must be replaced to maintain flow rate specifica tions M Note If your pump uses polyethylene piston seals be sure to follow the special instruction below for this type of seal 1 Unscrew the piston seal retainer Figure 9 9 from the pis ton and remove the seal from it Notice that the spring imbedded in the seal is facing up or is on the top side of the seal 2 Clean both the piston seal retainer and the cylinder thor oughly Make sure all parts which come in contact with the seal are free of dirt and other solids 3 Once the seal and cylinder surfaces have been cleaned rinse both parts with isopropyl alcohol The break in procedure is intended only for the UHMWPE aqueous piston seal to prevent the spring from bowing out its shape 1 Assemble the piston assembly per Figure 9 9A Be sure to install the top seal on the piston with the spring facing down 2 Slide the cylinder over the piston assembly per Figure 9 9B and allow it to sit for 15 minutes This breaks in the seal for the steps that follow 3 Remove the cylinder 4 Reassemble the top seal with the spring facing up per Figure 9 9C D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing 5 Install the cylinder over the piston assembly again and screw onto the mounting block 6 Leak test the pump PISTON SEAL CJ RETAINER PISTON SEAL
220. ill mode To set constant flow operation use the following procedure 1 Press CONST FLOW CFa will be displayed in the upper left corner of the screen This denotes that you will be defining constant flow parameters for pump A If you wish to define parameters for pump B C or D press softkey D select pump and then press softkey A B C or D to select pump B C or D respectively M Note If the main menu is displayed you must press D under CONST FLOW 2 Press A to change the flow rate The words ENTER FLOW RATE will flash on the screen 3 Use the number keys to enter the desired flow rate M Note If you make an error press CLEAR ENTRY to delete one char acter at a time 4 Press ENTER once the desired flow rate is displayed 5 Press RUN to begin pump operation Programming a constant pressure operation only requires a few keystrokes Use the following procedure 1 Press CONST PRESS CPa will be displayed in the upper left corner of the screen This denotes that you will be defining constant pressure parameters for pump A If you D Series Syringe Pumps Section 3 Basic Programming and Operation wish to define parameters for pump B C or D press soft key D select pump and then press softkey A B C or D to select pump A B C or D respectively M Note If the main menu is displayed you must press softkey D under RETURN before pressing CONST PRESS 2 Press the A softkey to indicate to the progr
221. imum of 200 mA for switching of relays or valves Observe correct polarity if the valve or relay is polarized D Series Syringe Pumps Section 5 Continuous Flow Introduction Installation amp Operation 5 6 Continuous Flow Once your valve package has been properly installed and you Mode have ensured that fluid connections are leak free the system is ready for operation Teledyne Isco convention is to name the pumps pump A and pump B reading from left to right Before running in continuous flow mode become familiar with independent mode which allows the controller to operate two pumps independently and simultaneously You must operate the two pumps manually for initial setup i e refill and purging of air If the Teledyne Isco air valve package is used the air valves are switched through ACCESS CTRL When air valves are used lights on the air valve actuator indicate which valves are open Table 5 7 Key functions in the Multi pump Mode Key Display Option Description NORMAL Uses a finer slower pres sure match control when switching from one pump to the other Uses a coarser faster pressure match control when switching from one pump to the other NORMAL PRESS Uses pressure matching when switching from one pump to the other LOW PRESS Uses no pressure matching when switching from one pump to the other DELIVER Sets the pump into the delivery mode of operation RECEIVE Sets the pump into the
222. ion and wash gland connection 2 6 D Series Syringe Pumps Section 2 Fluid System Connections and Accessories M Note Wash gland options are available for the 500D syringe pump with 116 wash tubes Contact Teledyne Isco for more informa tion 2 2 8 Cylinder Washing All pumps that do not have a wash gland are equipped with a Nitrogen Purge purge connector tube near the top of the pump body The purge connector enables the pump cylinder beneath the piston to be purged with nitrogen which can increase useful cylinder life by flushing residue from the system Figure 2 6 shows a typical con nection to the purge tube on the back of the pump To purge with nitrogen 1 Attach gas supply by slipping the plastic tube over the purge connector as shown below 2 Regulate the nitrogen supply to slightly above atmospheric pressure PISTON PLASTIC TUBE d CYLINDER lu PURGE NNECTOR SLIP PLASTIC TUBE OVER PURGE CONNECTOR Close up view of nitrogen purge tube N3908LIN gt Figure 2 6 Purge connector installation 2 7 D Series Syringe Pumps Section 2 Fluid System Connections and Accessories 2 2 9 Flushing Pumps with External Transducers 2 3 Fluid Connection 2 8 Accessories 2 3 1 Manual Refill Kit Kit installation When changing pumped liquids in the Model 65D 30D or other models with external transducers flush the pump to prevent
223. is installed with the spring facing up Place the piston base onto the push tube 4 Install the piston seal retainer onto the piston base Replace the cylinder over the piston and push tube assem bly and screw it into the cylinder mounting block The cyl inder should be screwed into the cylinder mounting block until the cylinder bottoms firmly against the stop ring in 9 10 Wear Ring Cleaning and Replacement 9 11 Flushing the Cylinder 9 11 1 Gas Solvent Changeover D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing the cylinder mounting block the cylinder will no longer turn Do not overtighten 6 Unscrew the cylinder until the inlet and outlet ports are lined up as you had them before Do not unscrew the cylin der more than one full turn from the stop position 7 Lock the cylinder by tightening the locking screw on the front of the cylinder mounting block to 30 in lbs 3 4 N m Reinstall covers Although the wear ring does not routinely need to be replaced occasionally it becomes worn or damaged depending on how the pump has been used Teledyne Isco recommends that when replacing the seal or cleaning the piston check the wear ring for any signs of deterioration 1 Follow the instructions in section 9 9 Seal Cleaning and Replacement to access the cylinder 2 Remove the piston seal retainer and slide off the seal The wear ring should then slide easily up and off the piston
224. keys A C which toggle the feature on and off M Note The Max Press maximum pressure display on and alarm on options cannot be disabled Display When a limit has been exceeded this feature causes the display to automatically flash an OVER or UNDER LIMIT message To turn off this function press softkey A once to toggle to OFF DISPLAY Alarm When a limit has been exceeded this feature causes the pump to automatically beep a warning To turn off this function press softkey B once to toggle to OFF ALARM Shutdown When a limit has been exceeded this feature causes the pump to shut down To turn off this function press softkey C once to toggle to ON SHUTDOWN When the pump is controlling pressure CONSTANT PRESSURE MODE the flow rate is not user controlled and may range up to the maximum flow ofthe pump In some cases it is desired to limit the rate of pumping during system pressur ization This can be done by selecting limit 5 FLOW LIMIT The FLOW LIMIT value is used as the upper range of flow rate during pressure control This limit is not the same as the MAX FLOW limit which is a threshold above when the pump is stopped or an alarm is activated as selected by the operator To save your changes and return to the main menu press softkey D PREVIOUS This option is available when operating in the constant flow mode and in the two pump concentration gradient mode It allows rapid pressurization to a s
225. l Commands 8 33 D Series Syringe Pumps Section 8 Serial Interface 8 34 8 8 5 Error Messages If an error occurs in a message one of the following responses will be sent The format of an error message is PROBLEM Refer to Table 8 7 Table 8 7 Error Messages Error Description PROBLEM LOCAL MODE The pump was sent a command before being placed in remote mode See Section 8 8 PROBLEM INVALID COMMAND The command sent was not recog nized by the pump PROBLEM INVALID OPERAND The operand character s following the sign is missing or is incorrect e g the number was too large PROBLEM PUMP RUNNING PROBLEM OVERPRESSURE PROBLEM UNDERPRESSURE The command sent is only valid when the pump is stopped Sent in response to a high or low pressure limit condition PROBLEM CYLINDER EMPTY PROBLEM CYLINDER FULL PROBLEM NO PUMP Sent when the pump cylinder is empty Sent when the pump cylinder is full Sent when the pump is not present PROBLEM WRONG PUMP MODE Sent when the pump is in the incor rect mode for the command D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing 9 1 Introduction JN NDANGER RISK OF ELECTRIC SHOCK DISCONNECT THE ELECTRIC POWER BEFORE SERVICING ONLY TRAINED SERVICE PERSONNEL MAY REMOVE THE CASE TOP N N DANGER RISQUE DE CHOC LECTRIQUE COUPER L ALIMENTATION AVANT LA R PARAT
226. l of the controller Operating selections are displayed as menu items on the controller screen or are associated with a ded icated key on the controller keypad Operating modes such as CONST FLOW CONST PRESS DISP and REFILL all have such dedicated keys WARNING UL Underwriter Laboratories has certified the D Series Controller and Pumps on the basis that explosive chemicals or chemicals that could become explosive under pressure are NOT used The instruments are not explosion proof Use extreme caution when pumping hazardous fluids The following information is intended to familiarize you with controller operation Once you have become familiar with the keypad and the main menu you will find it easy to direct the pumping operations required for your applications If you make an incorrect entry press CLEAR ENTRY to delete your last keystroke If you have entered a programming mode but do not wish to make any changes press ENTER to keep the current setting or press softkey D to return to the previous screen To allow pump operation to be tailored to your application both the pressure and flow rate units may be set by the user refer to Section 3 4 1 The pump also allows user programmed refill as well as pumping rates refer to Section 3 4 3 The system protection limits may also be set by the user refer to Section 3 8 77 The programming screens are divided into separate menus These menus are accessed when different f
227. l standards are RS 232 C connector pin usage is out lined in Table 8 1 Characters consist of 1 start bit 8 data bits low order first with 8 bit always set to zero and 1 stop bit There is no parity bit used All characters will be printable ASCII characters Control characters 0 1FH are ignored except for car riage return 0DH The serial unit number and baud rate can be changed from the default values through the MENU key Select SERIAL under the menu and adjust the values using the softkeys WARNING Connecting devices to energized circuits may cause personal injury or property damage Power must be removed from the pump before connecting external devices Table 8 1 External control connector serial pin connections Name Use CHASSIS GROUND _ Used to connect to the shield of the interconnect cable RECEIVE Serial interface data input Standard RS 232 C signal levels TRANSMIT Serial interface data output Standard RS 232 C signal levels REQUEST TO SEND RTS chain RS 232 C input is buff ered and connected to pin 21 CLEAR TO SEND CTS buffered RS 232 C output of pin 25 input 11 VDC DATA SET READY is held on COMMON Signal common for all signals 11 VDC DATA CARRIER DETECT is held on 8 2 8 3 USB Interface 8 4 Cabling for Serial Control 8 4 1 One Controller D Series Syringe Pumps Section 8 Serial Interface 5 VDC Test Voltage 11 VDC Negative te
228. l wires are clear of being pinched lay the pump back on its side and fully tighten the three screws to secure the circuit board assem bly to the case Figure 9 20 Set the pump upright and install the deflector shield so the tab lies flat against the bearing block then install the two screws and two flat washers Deflector shield should rest flat against the bearing block Plug in the connector to the encoder being careful not to bend any pins Figure 9 22 Carefully plug in the 2 pin connector for the motor assem bly then secure the wires within the nylon twist tie attached to the bottom of the case Figure 9 21 Check that the capacitor right above the motor shaft is not in contact with the motor shaft If the capacitor is rubbing D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing on the shaft carefully pry up on the capacitor until it no longer makes contact No contact allowed between the capacitor and the motor shaft Figure 9 37 Capacitor and motor shaft 9 14 Calibrations It should not be necessary to readjust the instrument unless repairs have been made on the electronic circuitry or the con troller cable length has been changed 9 14 1 Pressure Transducer Calibration M Note Please contact the factory if your pressure transducer requires recalibration 9 14 2 A D Circuit This adjustment is done in the controller unit Adjustment 1 With the controller operating and pump
229. limit upper mounting screw 21 Press REFILL on the controller to lower the piston until the lower screw in the upper limit sensor is exposed and then tighten the upper limit screw 22 Press RUN 28 The pump will stop when the upper limit sensor is inter rupted 24 Lay a straight edge across the top of the cylinder and mea sure the clearance between the piston and the top of the cylinder 9 40 D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing 35 If the clearance is not between 0 025 and 0 050 0 6 1 3 mm loosen the screw holding the interrupter and move the interrupter SLIGHTLY Repeat steps 22 25 Set both the REFILL and FLOW RATE to MAX Press REFILL and allow the pump to interrupt the lower sensor The pump will stop Press RUN and allow the pump to interrupt the upper sen sor The pump will stop Lay a straight edge across the top of the cylinder and mea sure the clearance If the clearance is not within range repeat steps 22 30 Turn off the pump and controller Disconnect the mains power Detach the cable from the transducer Install a cylinder cap seal If the cylinder cap seal is being reused inspect the seal for cracks damage or excessive deformation slight flaring of the top edge is acceptable Apply a small amount of Never Seez lubricant to the first few threads of the cylinder Install the cylinder cap WARN
230. lly need to refill the pumps The system must be stopped while the pumps are refilling Pump A the CO pump may be refilled simply by designating the pump to be refilled and then pressing REFILL refer to instructions below Pump B the modifier pump may also be refilled in this manner However if you wish to ensure that air is purged from pump B it must be placed under independent control before refilling Once under independent control the pump will run until 5 10 ml of modifier are delivered back to the source see refilling pump B below Press STOP Close the outlet valves of both pumps Press REFILL and press A to designate pump A Ne As soon as the pump pressure drops below the known tank pressure open the tank supply valve and the pump A inlet valve 5 After pump A has refilled the message CYLINDER FULL will be displayed on the controller front panel Wait 15 seconds before closing the tank supply valve and the pump inlet valve 6 Open the outlet valves of both pumps 7 Press RUN 8 When A pressure is established the message HOLD PRESS RUN will be displayed 9 Open the extractor inlet valves 10 The message EQUILIBRATE will be displayed on the con troller screen Ifthe controller does not display EQUILI BRATE press RUN While this message is displayed no modifier will be delivered To refill pump B the modifier pump To start modifier 11 D Series Syringe Pumps
231. lowing sections Section 1 Introduction Section 2 Fluid System Connections and Accessories Section 8 Basic Programming and Operation Section 4 Gradient Pumping for Pressure Flow and Concen tration Modes Section 5 Continuous Flow Introduction Installation amp Oper ation Section 6 Modifier Addition Section 7 Modbus Configuration Section 8 Serial Interface Section 9 Pump Maintenance Troubleshooting and Servicing Appendix A Replacement Parts The technical specifications for the D Series Syringe Pumps are detailed in Tables 1 2 through 1 9 M Note Underwriters Laboratories UL has certified all Series D Pumps with the exception of the 100 VAC versions 1 1 D Series Syringe Pumps Section 1 Introduction Table 1 1 CYLINDER CAPACITY 30D Technical Specifications 30 42 ml POWER REQUIREMENTS Mains voltage line cord is a Disconnect Device 100 10 VAC 2 8 A maximum 117 12 VAC 2 4 A maximum 234 23 1 2 A maximum Factory Set LINE FREQUENCY 50 or 60 Hz LINE VOLTAGE NOISE TOLERANCE 1 7 x nominal rms line voltage 10 usecond pulses any phase angle random or repetitive DIMENSIONS PUMP CONTROLLER 27 18 cm 27 18 cm 46 74 cm 30 48 cm 100 cm 13 59 cm Width Depth Height WEIGHT PUMP CONTROLLER 36 4 kg 2 96 kg FLOW RATE RANGE FLOW RATE ACCURACY 0 01 ul min to 22 ml min for any pressure up to 2068 bar x 0 596 above 69 bar and above 0 25
232. lue then press ENTER to save it 8 Set either the desired RATE 3 of change or DURATION 4 in minutes Once one value has been set and saved the other will automatically appear M Note DURATION in minutes can have a resolution of 0 1 with a maximum of 9 999 minutes per step 9 Ifyou want to add another step to the file program press INSERT C 10 The step number will increase by one and the default ini tial value will be the final value entered for the previous step Edit as desired 11 When programming is complete press the STORE key to save the file and return to the home screen 12 To start the program press RUN two times M Note When a gradient run is started digital output 8 of the controller ACCESSORY connector will toggle from high to low open to closed for one second D Series Syringe Pumps Section 4 Gradient Pumping for Pressure Flow and Concentration Modes 4 5 Review Revise amp Hold Options 4 6 Program Conclusion 4 12 The flow rates and ramp rate for Pump A in each step will be in direct opposite proportion to the values set for Pump B INIT B FIN B and RATE Note that an entire gradient program can be removed only by deleting each of its steps one at a time as discussed in the next section 4 5 Review Revise amp Hold Options When the last remaining step is deleted the entire file is removed While in the programming menu you can also Delete To delete the curre
233. lumn represents the four analog input terminals on the rear panel of the controller For any terminal shorted to ground the value should read a steady zero XX XXXX ACC1 XX XXXX B XX XXXX ACC2 XX XXXX XX XXXX ACC3 XX XXXX D XX XXXX ACC4 XX XXXX MORE ACCESSORY DIGITAL DIGITAL OUTPUT DIGITAL INPUT GROUND A B D 1234 12 3 4 5 6 7 8 T Figure 9 3 Analog Input diagnostic screen Press EXIT D to return to the diagnostic menu 9 6 D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing 9 5 3 KEYPAD TEST The screen will briefly display the name of each key pressed Press EXIT D to return to the diagnostic menu 9 5 4 MOTOR Tests the digital position controls CONTROL LIMITS From the Limits menu you can set minimum and maximum flow rate limits and pressure limits as well as the maximum flow rate in constant pressure mode High and low limits cannot exceed pump specifications The pump stays within these limits by means of a flag that moves up and down with the ball nut assembly and two optical sensors at the top and bottom of the tower side plate When a sensor is interrupted it has a logic 1 when it is
234. ml min maximum 1 0 ul min seal leakage FLOW RATE DISPLAY RESOLUTION 0 01 ul min 1 0 ul min in Constant Pressure Mode ANALOG OUTPUT ACCURACY DISPLACEMENT RESOLUTION 0 2 4 20 mA output 0 5 voltage output using the 12 channel output option 1 825 nl step REFILL TIME 1 05 minutes REFILL OR DEPRESSURIZATION RATE 0 01 ul min to 29 ml min at any pressure from 0 to 2068 bar PRESSURE RANGE 0 6895 to 2068 4 bar PRESSURE ACCURACY 0 2 of full scale at constant temperature PRESSURE REPEATABILITY ZERO PRESSURE DRIFT 0 05 of full scale within 48 hours at constant temperature 0 05 of full scale within 48 hours at constant temperature PRESSURE DISPLAY RESOLUTION 6 895 kPa AMBIENT TEMPERATURE RANGE 5 to 40 C TEMPERATURE DRIFT 0 015 of full scale C HUMIDITY 95 maximum DEAD HEADSPACE VOLUME 0 88 0 02 ml POLLUTION DEGREE INSTALLATION CATEGORY MAXIMUM ALTITUDE Using water at constant pressure and constant temperature above 69 bar and above 0 25 ml min b The analog output is an optional accessory Pressure repeatability specification is based on zeroing the pressure transducer before measurement Refer to sub section ZERO PRESS in Section 3 of the manual for re zeroing procedure d Volume in and above the piston seal head clearance at automatic shutoff and inlet and outlet ports to the fittings 1 2
235. mp stop menu 1 23 1 14 Four pump stop menu 1 23 2 1 Liquid system plumbing connections 30D on Left 2 2 2 2 1 16 Tubing adapter for 30D 65D pumps 2 4 223 30D 65DEitting Spe ree EE ir lene Roa Pleas idi 2 4 2 4 Drain tube installation enen cee 2 5 2 5 Drain tube installation and wash gland 2 6 2 6 Purge connector installation 2 7 2 7 Refill kit installation enen eneen eee eee 2 9 2 8 Outlet valve package connection 2 10 2 9 package installation nen eee neces 2 11 2 10 In line filter package 2 senen ene 2 11 2 11 Cylinder insulation 2 12 2 12 System with temperature control jacket installed 2 13 2 13 Fluid fittings sate era a a ea 2 14 2 14 Secure screws with the 1 4 hex wrench 2 15 2 15 Removing the cylinder cap with wrenches 2 16 2 16 Temperature control jacket installation 2 17 2 17 Back pressure 2 18 2 18 Inside the pump cylinder wetted materials 2 19 3 1 Menu 1 program sel
236. n 209 0162 10 valve housing le Ferrule zero 209 0169 41 x 2 57 SST 60 1243 570 tubing Continuous Flow System Modifier Addition Kit To user supplied Electric Valve z device package co 5 i Mixing tee SN 5 6 d a C 0 0 E E i el e ed 5 Inlet rf s T M Note Valve pkg 2 Way Valve The modifier pump is a single pump when its cylinder is empty the system stops The cylinder must be manually refilled before the system can run again Figure 6 2 Modifier addition kit installation continuous flow Refill Kit Solvent modifier 6 3 D Series Syringe Pumps Section 6 Modifier Addition Table 6 2 contains modifier addition components for connecting to a continuous flow system Table 6 2 Modifier Addition Components for Continuous Flow System Description Part Number Tee union fitting 146 209 0169 47 Check valve cartridge 60 3864 010 Single check valve housing 60 1243 516 Tubing check valve 60 1243 644 2 way valve 16 OD 209 0098 05 60 1243 658 Reduction union 18 to 16 209 0162 10 Tubing valve inlet Valve spacer 60 1243 659 146 OD x 12 cm tubing 60 1243 540 x 2 57 SST tubing 60 1243 570 Check valve cartridge Vg 209 0161 80 Check valve mixer tubing 60 1243 691 6 1 2 Modifier Mode Se
237. n Continuous Flow Constant Pressure mode 0 Multi pump pair AB in Delivery mode 1 Multi pump pair AB in Receive mode 0 Multi pump pair AB in Low Press operation 1 Multi pump pair AB in Normal Press operation 0 Use Fast coarser pressure match control for multi pump pair AB 1 Use Normal finer pressure match control for multi pump pair AB 0 Multi pump pair CD in Delivery mode 1 Multi pump pair CD in Receive mode 0 Multi pump pair CD in Low Press operation 1 Put multi pump pair CD in Normal Press opera tion 0 Use Fast coarser pressure match control for multi pump pair CD 1 Use Normal finer pressure match control for multi pump pair CD 1 Activates the automatic rapid pressurization cycle Constant Flow mode only for Pump A 1 Activates the automatic rapid pressurization cycle Constant Flow mode only for Pump B 1 Activates the automatic rapid pressurization cycle Constant Flow mode only for Pump C 1 Activates the automatic rapid pressurization cycle Constant Flow mode only for Pump D 1 Pump A is Equilibrating 1 Pump B is Equilibrating 7 4 D Series Syringe Pumps Section 7 Modbus Configuration Table 7 5 Coils Continued Register Address Type Description 1 Pump C is Equilibrating 1 Pump D is Equilibrating 1 Pump A is in Hold clock stopped 1 Pump B is in Hold clock stopped 1 Pump C is in Hold clock stopped 1 Pump D i
238. n motor common TP101 and VM TP105 should be 60 to 90 V See section 4 The voltages in the controller unit between circuit common TP16 TP5 TP6 and the test points should be TP32 5 VDC 0 002 VDC TP12 8 1 VDC to 13 VDC TP43 15 VDC 0 6 VDC TP44 15 VDC 0 6 VDC TP20 43 8 VDC 0 0 VDC TP9 2 5 VDC 0 0 VDC TP7 15 VDC 0 0 VDC M Note These voltages are displayed during the Analog Input routine in the Diagnostics section of the firmware Section 9 5 2 D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing 9 8 Lubrication The pump is a precision engineered instrument that must be lubricated every two years or every 6 000 strokes whichever comes first to ensure proper service life The pump has an easy to access lube wheel that keeps the main gears lubricated during operation See Figure 9 8 configuration 1 or 2 depending on your pump motor type For your conve nience a lubrication kit containing Never seez and DUOLEC 1608 lubricants is included in your pump accessory package 7 A f Z ond ear unseen Configuration 1 Figure 9 8 Gear train lubrication and motor drive service Worm Worm Gear The worm and worm gear are lubricated by a lubrication wheel Apply DUOLEC 1608 directly to the wheel until it is saturated The wheel may also be directly lubricated by trickling oil into the wheel while the pump is running M Note Use only DUOLEC 1608 lubrication on
239. n the extractant outlet valve s M Note Flow MUST be established through the system at or before the time EQUILIBRATE is displayed To properly equilibrate the pumps they must be delivering fluid 9 Once the message RUNNING is displayed modifier will be delivered at the selected rate 6 9 D Series Syringe Pumps Section 6 Modifier Addition 6 10 D Series Syringe Pumps Section 7 Modbus Configuration 7 1 Overview 7 1 1 Modbus RTU Figure 7 1 RS 485 Connection Modbus is a simple command response mechanism to read from and write to specific memory locations called registers A register is a holding place for a piece of digital information within the equipment For more information on Modbus please refer to the following documents which can be found on the www modbus org website Modbus Application Protocol Vol 1 and Modbus Over Serial Line Vol 1 and Modbus Messaging on TCP IP The Isco D Series Syringe pump controller supports the Modbus RTU and Modbus TCP IP protocols The Modbus RTU protocol implementation uses a 2 wire RS 485 connection The RS 485 connections are located on the DB25 connector labeled RS 232 RS 485 We recommend connecting the ground reference wire as shown in Figure 7 1 The matching connection is a D Subminiature 25 pin standard plug such as an AMP part 747912 2 from an electronic parts supplier N WARNING Connecting devices to energized circuits may cause personal injury or propert
240. nalog output These outputs are often used with analog based plant or process monitoring equipment Output voltage for pressure is located on the back panel of the pump module via standard banana jacks The output connection is the female 25 pin Sub D connector located on the rear panel of the controller under 4 20mA Output DIGITAL I O This output can also be 4 20 mA OUTPUT ANALOG OUTOUT ACCESSORY ELECTRIC VALVES 12 CH OUTPUT 4 20mA OUTPUT DIGITAL DIGITAL DIGITAL ANALOG INPUT GROUND OUTPUT INPUT G N D Spes USB ETHERNET MOM SSO OSS OOS SS OS l 25 pin cable EEE 1234 12 3 415 6178 1234 Controller rear panel RS 232 RS 485 Figure 3 14 Analog voltage output connection rear panel 3 22 Voltage analog outputs are pre installed at the factory This option has a total of four outputs for monitoring flow rate with selectable ranges from 0 to 5 to 5V and 0 to 10V The default range at installation is 0 to 10V Each output can be set to a different range The top of the selected range is the same maximum value entered for MAX FLOW when setting LIMITS as described in Section 3 8 7 of this manual For example if the output range is D Series Syringe Pumps Section
241. nd under the multi pump options on you have accessed the multi pump options you may select Constant Flow mode or Constant Pressure mode 5 18 a MORE MULTI PUMP 1 CONTIN CONST FLOW 1 will blink PREVIOUS Press 3x to returnto run screen 1 AB Pumps 2 CD Pumps Figure 5 10 Keystrokes to set up constant flow 5 6 3 Constant Pressure Mode D Series Syringe Pumps Section 5 Continuous Flow Introduction Installation amp Operation Starts operation Continuous flow mode is found under the multi pump options on Menu 2 Once you have accessed the multi pump options you may select Constant Flow mode or Constant Pressure mode EM ES MULTI PUMP 1 AB Pumps 2 CD Pumps Figure 5 11 Keystrokes to set up constant pressure re CONTIN CONST PRESS 2 will blink PREVIOUS Press 3x to return to run screen Starts operation 5 19 D Series Syringe Pumps Section 5 Continuous Flow Introduction Installation amp Operation 5 6 4 No Check Valve To limit fluid backflow from the pump to the supply reservoir one of two approaches is generally used Either a check valve is installed in the supply line or the NO CHECK VALVE NCV software feature is enabled on the controller The No CHECK VALVE NCV feature controls the opening of the inlet valves such that just prior to refill the pump is depres surized to a use
242. ngs already attached The only connections you have to make are between the pump tubing and the double check valve housings and between the outlet and inlet tubing and the tees 5 2 1 Check Valve Technical Dual system maximum flow rates under optimal conditions are Specifications approximately 65 of the max flow rate for each pump model Table 5 1 Continuous Flow Technical Specifications Check Valves Pressure fluctuation at switchover 0 35 bar at system backpressures from 6 9 bar to the single pump maximum Higher fluctuation occurs at pressures below 6 9 bar 3 5 bar Maximum system backpressure The single pump maximum Valves rated to 689 5 bar Maximum flow rate ml min Liquids 6596 of the single pump C1000D 265 2 maximum rate C500D 132 6 C260D 69 55 C100DX 32 50 C100DM 16 25 C65DM 19 50 Liquefied gases 4596 of the single pump maximum rate Cylinder cooling jack ets should be used to obtain this rate Temperature range 0 to 40 C Wetted materials in valve packages Check valves SS316 sapphire ruby PEEK PTFE Tubing and fittings SS316 gold 5 2 2 Dual Check Valve Check valve installation refers to Figure 5 1 or 5 2 depending on Installation your pump model M Note Tighten fittings just enough to hold tubing in place Final tight ening will be done after all the tubing and fittings are in place 1 Move the pumps so that the pump bases are about 1 3 cm apart 2 Use the plugs to sto
243. ns on parts contact Teledyne Isco Service Department 2 This list is subject to change without notice A 68 D Series Syringe Pumps Appendix A Replacement Parts A 1 18 Dual Check Valve Package for 100 260 500D SEEN zer ch 3 gt N 5 3 Jj Of d Ed DE 4 Fa iL ear Cote EGE ESS ELSE d L 0 Bm U RPL CONTINUOUS FLOW CHECK VALVE A 69 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST NO 80 1242 239 SHEET 2 Or 2 Isco Inc REV D DATE 110311 PART NUMBER DESCRIPTION 209 0169 27 NUT 209 0169 41 FERRULE 209 0168 00 PIPE PLUG 209 0166 80 PLUG 1 8 SST HP 60 2255 240 CHECK VALVE HOUSING 60 3864 010 CHECK VALVE CARTRIDGE 60 1243 517 DOUBLE CHECK VALVE HOUSING 209 0161 01 MALE CONNECTOR 209 0161 56 1 8 UNION TEE TUBING REDUCER CONNECTOR 60 2258 019 ASSEMBLY 209 0169 81 TUBING NUT 1 For current prices and quotations on parts contact Isco Service Department 800 228 4250 2 This list is subject to change without notice A 70 D Series Syringe Pumps Appendix A Replacement Parts A 1 19 Dual Check Valve Package for 1000D XE XE Dr 9 xe E 0 5
244. nstant Pressure mode for Pump A ml hr ul min ul hr See NOTE 2 Maximum flow limit in Constant Pressure mode for Pump B min ml hr ul min ul hr See NOTE 2 Maximum flow limit in Constant Pressure mode for Pump C min ml hr ul min ul hr See NOTE 2 7 8 Register D Series Syringe Pumps Section 7 Modbus Configuration Table 7 6 Holding Registers Continued of Registers Description Maximum flow limit in Constant Pressure mode for Pump D min ml hr ul min ul hr See NOTE 2 Actual pressure of Pump A ATM BAR kPa PSI See NOTE 1 Actual flow rate of Pump A min ml hr ul min ul hr See NOTE 2 Volume remaining in Pump A milliliters Actual pressure of Pump B ATM BAR kPa PSI See NOTE 1 Actual flow rate of Pump B min ml hr ul min ul hr See NOTE 2 Volume remaining in Pump B Actual pressure of Pump C illiliters ATM BAR kPa PSI See NOTE 1 Actual flow rate of Pump C ml min ml hr ul min ul hr See NOTE 2 Volume remaining in Pump C milliliters Actual pressure of Pump D Actual flow rate of Pump D BAR kPa PSI See NOTE 1 min ml hr ul min ul hr See NOTE 2 Volume remaining in Pump D System flow rate of multi pump pair AB milliliters ml min ml hr ul min ul hr See NOTE 2 PIP
245. nt pressure Puts pump in constant pressure mode CONST FLOW Constant flow Puts pump in constant flow rate mode STORE Stores the current program in nonvolatile memory and exits program ming mode LIMITS Displays and allows changes to the maximum and minimum pressure and flow rate limits RAPID PRESS Rapid pressure Allows rapid pressurization to the stable pressure point and then switches automatically to constant flow Available in constant flow mode only NOTE This feature is automatic i e RAPID PRESS is pressed only once and the user does not enter a pressure although entering a target pressure may speed equilibration RECALL Replaces the current program with one recalled from nonvolatile memory ACC CTRL Accessory control Manually operates accessories such as valves ZERO PRESS CLEAR ENTRY MENU Zero pressure Sets pressure display to zero Active only from 750 to 750 psi Clear the last digit entered from the numeric key Accesses software to set operational modes units and other optional parameters DISP Activates dispense mode refer to Section 3 10 3 HOLD Freezes the program clock The unit will continue at the current gradient parameters REFILL Turns on pump drive motor to move piston downward at a rate previously programmed RUN Turns on pump drive motor to move piston upward in a previously pro grammed mode such as CONSTANT
246. nt step press DELETE D A deleted step cannot be recovered Used repeatedly this command can be used to delete an entire file Review To review existing program steps press STEP BACK A or STEP FWD B Add New To add a new step between two existing steps nav igate through the program to the step just before your addition Press INSERT C and program the new step Note that the initial value of the next step will default to the final value of the new step and may need to be edited if a dif ferent initial value is needed While Running A gradient program can be reviewed or edited while it is running Simply press EDIT B or REVIEW C to begin If a new step duration is shorter than the elapsed time for that step the program will proceed to the next step If the total flow rate is changed the program will immediately start using the new rate To return to the run screen press RETURN D Hold You can hold a running gradient in its current state while retrieving a different program file to run in its place Press Hold and then Recall to access the new program This feature is used mainly in applications where it is necessary to keep the system pressurized during method changes External Start When a gradient program is in Hold mode a momentary low on digital input 2 of the controller ACCESSORY connector will start the program When a gradient program reaches the end there are four selectable actions the sys
247. nternally by pump software The status order returned corresponds with the outputs 1 8 97 DIG CONTROL command Sets the digital output control bits to either internal or remote where x is either R 1 8 for REMOTE or I for INTERNAL CONTROL R indicates the corresponding bit will be controlled remotely through the serial port I indicates the corresponding bit will be controlled internally by pump software The order corresponds with the out puts 1 8 DISPENSEA Returns the dispense volume for Dispense mode DISPENSEB DISPENSEC DISPENSED DISPENSEA Sets the dispense volume for Dispense mode Format is XXX XXX ml Leading and DISPENSEB trailing zeros are not required Can only be changed when pump is stopped DISPENSEC DISPENSED FLOW Returns the delivering pump s flow rate in continuous pumping mode and modifier FLOWCD addition mode In INDEPENDENT mode FLOW returns the pump A flow rate and FLOWCD returns the pump C flow rate FLOWA Returns the actual flow rate of the pump FLOWB FLOWC FLOWD FLOW Returns the actual flow rate of the pump Enter for a flow rate setpoint constant FLOWB flow mode Format is XXX XXXXXXX ml min Only 5 figures are significant Leading FLOWC and trailing zeros are not required Gets pump information G returns a text string that contains current pressure ana log input and digital input information G amp is the Get All c
248. of the check valve assemblies 5 Connect the two check valve inlets to the outlets of the in line filters with the 12 7 cm lengths of tubing 6 Press the check valves into the clips on the stand as shown below oriented with flow in the upward direction indi cated by the arrow on the housing D Series Syringe Pumps Section 4 Gradient Pumping for Pressure Flow and Concentration Modes OUTLET 1 8 OD X 0 069 ID SST TUBING OUTLET e from INLET refill kit VALVE A from refill kit 1 8 OD X 0 085 ID PTFE TUBING FILL RESERVOIR 10u FILTER MIXER CHECK VALVES 1 16 OD X 0 020 ID SST TUBING INLINE VALVE STAND FILTER Figure 4 3 Dual gradient system connections Inlet valves A amp C are from refill valve kits Close up of mixer assembly Close up of C214W valve stand VALCO VALVE Close up of in line filter 1 16 OD X 0 005 X 10CM SS TUBING P N 60 1243 445 UPCHURCH MIXER P N 209 0166 09 1 16 OD X 0 020 ID BIN Figure 4 4 Dual gradient connections Detail 4 7 D Series Syringe Pumps Section 4 Gradient Pumping for Pressure Flow and Concentration Modes 4 3 Single Pump Gradient A single pump gradient program is based on either pressure or Programming flow and controlled by either time duration in minutes or rate of change units per minute The controller s memory can contain
249. ollar 209 0164 03 14 F250C Plug 209 0164 05 65DM Inlet Outlet fittings Valco 18 Nut 209 0169 27 18 Ferrule 209 0169 41 le Plug 209 0166 80 bs 116 Tubing Reducer 209 0169 42 100DX DM and 260D Inlet Outlet fittings Valco 48 Nut 209 0169 27 18 Ferrule 209 0094 07 le Plug 209 0166 80 lg 116 Tubing Reducer 209 0169 42 500D Inlet Outlet fittings lg Tubing Connector to 48 NPT 209 0161 01 lg NPT Plug 209 0168 00 lg Me Tubing Reducer 209 0162 00 500 HPx Inlet outlet fittings 3g Tubing Connector to 8 NPT 209 016 100 38 NPT Plug 209 016 813 D Series Syringe Pumps Warnings Cautions and Notices Commonly Ordered Replacement Parts for the D Series Syringe Pumps Description Part Number 1000D Inlet Outlet fittings l4 NPT Plug 209 0168 09 Va NPT Connector to 4 tubing 209 1063 36 Stainless Steel Tubing 116 OD x 0 020 ID 004 7300 21 lg OD x 0 069 ID 004 7302 22 xi D Series Syringe Pumps Warnings Cautions and Notices NOTICE If you have ordered one of the following custom pumps from Teledyne Isco technical specifications for tubing and fittings listed in this manual do not apply to your system Contact the factory for details about your custom pump Models 65HP 260HP 500HP 500HV 500SP xii D Series Syringe Pumps Table of Contents Section 1 Introduction 1 1 About This Manual 0 0 cece een tne ene Ene 1 1 1 2 Specifications ana ob Gee ek
250. ommand This returns the same information as G plus flow rates units operation status and more For four pump operation ise the G amp 2 commands Refer to 8 8 1 for a complete description of this serial command IDENTIFY Pump responds SERIES 1240 0__ MODEL D PUMP REV__ For each pump REV is the internal pump program software revision For example if the controller was attached to two 100DMs the message would read SERIES 1240 024 MODEL 100DM PUMP SERIES 1240 024 MODEL 100DM REV__ The series number is the original catalog number for the pump type It may not match the production series number on the pump serial label SERIES 1240 024 MODEL 100DM PUMP SERIES 1240 027 MODEL 100DX PUMP SERIES 1240 021 MODEL 260D PUMP SERIES 1240 025 MODEL 500D PUMP SERIES 1240 103 MODEL 500HPx PUMP SERIES 1240 052 MODEL 1000D PUMP SERIES 1240 063 MODEL 65D PUMP SERIES 1240 096 MODEL 65DM PUMP SERIES 1240 819 MODEL 30D PUMP 8 21 D Series Syringe Pumps Section 8 Serial Interface Table 8 6 Serial Commands Continued Command Description INDEPENDENT INDEPENDENTCD Put pumps in Independent mode IPUMPA 1 IPUMPA 0 IPUMPB 1 IPUMPB 0 IPUMPC 1 IPUMPC O IPUMPD 1 IPUMPD 0 Turns the pressure integral control On and Off for the pump indicated 1 0 OFF LGE F XX A 0X Action to perform when gradient program reaches the end The pump needs to be in local mode only File F 01 99 Acti
251. on A 00 Hold final value 01 Stop after final step 02 Return to initial value and hold 03 Return to initial value and repeat program Start Gradient Command This starts a gradient program same as the RUN key This command will check to see if there is a gradient running and respond with RUNNING if there is The pump needs to be in local mode only LGSL F xx Select Gradient File Command This selects a gradient file to be run This command will reset the controller to the saved file gradient type If the selected gradient file does not exist the controller will respond with PROBLEM INVALID OPERAND The pump needs to be in local mode only LGST Stop Gradient Command This stops a gradient program The pump needs to be in local mode only LGDL F xx S xx Gradient Step Download command This downloads a step from the pump to the PC This command will respond with PROBLEM INVALID OPERAND if the file or step does not exist The controller will respond with step information if the command is valid Refer to 8 8 2 for complete information on Gradient step download com mands The pump needs to be in local mode only LGUL F xx S xx Gradient Step Upload command This transfers a step from the PC to the controller Refer to 8 8 3 for complete information on Gradient step download commands The pump needs to be in local mode only LIMITS LIMITSB LIMITSC LIMITSD Returns the pressure and flow rate
252. oosely attach the tubing lengths from the valve assembly to the pumps 4 Install the four panhead screws on bottom of the bracket 5 Tighten the tubing nuts 6 Connect the inlet tube to the supply reservoir Connect the outlet tee to your apparatus Outlet Tee D 9 y n 9 H j AED TT c 9 n Inlet Tee e N e an ER Inlet Filter N Air Inlet Tubing Figure B 1 Air valve installation for 30D pump D Series Syringe Pumps Appendix B Continuous Flow Introduction Installation and Operation for 30D Wire Pair Conversion Table for A B Pump Pair A B Pum Digital Wire Pair Dd Wires Al Al 15 A2 A2 15 B3 B3 15 B4 B4 15 B 3 D Series Syringe Pumps Appendix B Continuous Flow Introduction Installation and Operation for 30D B 3 Continuous Flow Electric valves which provide the best positive valve closure are Electric Valves most commonly used in liquefied gas applications Electric valves require the pump controller to be equipped with the valve driver board Electric Valve Package Number E30D 62 1247 113 M Note Electrical valves can only be used with pumps A and B B 3 1 Technical Dual system maximum flow rates under optimal conditions are Specifications approximately 65 of the max flow rate for each pump model Table B 2 Continuous Flow Tec
253. ormado por una persona que haya trabajado ya previamente con este instrumento For a forhindre skade p instrumentet eller operatoren er det nodvendig at brukeren har full forst else for det engelske sprak og tekniske uttrykk Ellers ma brukeren fa opplzring av en person som kan engelsk for instrumentet tas i bruk F r att f rhindra skade p instrumentet eller operat ren r det n tv ndigt att anv ndaren har fullst ndiga kunskaper i det engelska spr ket och dess tekniska termer eller utbildas av en person som tidigare brukat instrumentet gt gt gt gt gt gt gt For at undg skade produktet eller brugeren er det nodvendigt at brugeren til fulde forst r det engelske sprog for at forst den tekniske formulering i den engelske manual modsat fald skal brugeren modtage trzening inden apparatet tages drift D Series Syringe Pumps Warnings Cautions and Notices Laitteelle tai k ytt j lle aiheutuvien vahinkojen v ltt miseksi on t rke ett k ytt j hallitsee englannin kielen ja englantilaiset tekniset termit tai on saanut k ytt opastuksen englantia osaavalta henkil lt Per evitare danni allo strum nto od incidenti all operatore necessario che l utilizzatore abbia una completa conoscensza della lingua inglese oppure che venga istruita da una persona che abbia utilizzato precedentemente questo strumento Para impedir qualquer dano
254. ottom Motor Black Bottom Motor Black Top Motor Figure 9 27 Wire connections 9 29 D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing 10 Leaving the wires connected to the terminals use a flat blade screwdriver and remove the set screws holding the two Negative brushes black wires into the motors Set Screws Figure 9 28 Set screws holding the two negative brushes 11 Grasp the connector on one of the black wires and wiggle the connector to loosen the brush Gently pull the brush out of the motor Once out disconnect wire from brush con tact Repeat this process for the second black wire being sure not to get the wires mixed up Figure 9 29 Wires disconnected from brush contact 9 30 D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing 12 Connect the bottom black wire to the new brush and insert the new brush into the motor using the connector as lever age to guide brush into the motor Hold the connector so the brush is fully engaged into the motor Figure 9 30 then reinstall the set screw that holds brush in place Repeat this process for the top black wire Figure 9 30 Connector connected to the brush Figure 9 31 Removing the set screws 13 Leaving the wires connected to the terminals use a flat blade screwdriver and remove the set screws holding the two Positve brushes orange wires into the motors Set Scr
255. out notice Contact Information Customer Service Phone 800 228 4373 USA Canada Mexico 402 464 0231 Outside North America Fax 402 465 3022 Email IscoCSR G teledyne com Technical Support Phone Toll Free 866 298 6174 Samplers Flow Meters and Multi parameter Probes Toll Free 800 775 2965 Syringe Pumps and Liquid Chromatography Email IscoService teledyne com or Iscoeps teledyne com Return equipment to 4700 Superior Street Lincoln NE 68504 1398 Other Correspondence Mail to P O Box 82531 Lincoln NE 68501 2531 Email IscoInfo teledyne com D Series Syringe Pumps Warnings Cautions and Notices Warnings and Cautions The lightning flash and arrowhead within the triangle is a warning sign alerting you to dangerous voltage inside the product The exclamation point within the triangle is a warning sign alerting you to important instructions in this manual Symboles de S curit Ce symbole signale la pr sence d un danger d lectrocution Ce symbole signale l existence d instructions importantes relatives au produit dans ce manuel D Series Syringe Pumps Warnings Cautions and Notices Warnungen und Vorsichtshinweise Der gepfeilte Blitz im Dreieck ist ein Warnzeichen das Sie vor gef hrlichen Spannungen im Inneren des Produkts warnt Das Ausrufezeichen in Dreieck ist ein Warnzeichen das Sie darauf aufmerksam macht da wichtige Anleitungen zu diesem Handbuch geh r
256. ow noise and improves pump performance at pressures less than 3 5 bar Two back pressure regulators are available 7 bar part 209 9012 22 5 bar part 209 9012 21 Fittings to connect the tubing to the regulators are supplied NDANGER RISK OF INJURY THIS EQUIPMENT PRODUCES HAZARDOUS PRESSURES PLEASE UTILIZE APPROPRIATE TUBING AND CONNECTIONS AS NOTED IN THE MANUAL Installation 1 Figure 2 17 Back pressure regulator 2 18 Note the arrow on the regulator indicating the fluid direction Connect your tubing between the pump outlet and the reg ulator using the supplied fittings D Series Syringe Pumps Section 2 Fluid System Connections and Accessories 2 5 Seal Options The pump contains four seals and a wear ring Transducer seal The transducer seal is gold plated to press into minute gaps between the surfaces of the transducer flange and the shelf of the cylinder cap The 30D and 65D do not have transducer seals Cylinder cap seal The cylinder cap seal maintains the pressure within the cylinder Piston seal The piston seal maintains the pressure within the cylinder Wear ring The wear ring supports the seal against movement within the cylinder and keeps the piston centered in the cylinder bore Wiper seal The wiper seal cleans the inside of the cylinder In the model 1000D pump the wiper seal faces the same direction as the piston seal to prevent leakage of the wash gland fluid
257. p A No problem E Empty cylinder B Cylinder at bottom O Over pressure U Under pressure M Motor failure N Pump transduce disconnected Checksum Volume total Continuous flow or modifier mode Units Liters E6 System pressure multi pump displays Pump A for other modes Units psi 5 Resolution 0 2 psi System flow rate multi pump displays Pump A for other modes Units Liters minute E10 Resolution 0 1 nanoliter minute Figure 8 5 Get All Status String G amp Command 8 27 D Series Syringe Pumps Section 8 Serial Interface Lr Flow Rate Pump A Units Liters minute E10 Resolution 0 1nanoliter minute Volume Pump A Units Liters E9 Resolution 1nanoliter Operation Status Pump A S Pump Stopped R Running Refilling H Holding E Equilibrating T Control Status Pump A L Local Control Pressure Pump A R Remote Control Pressure Pump B ALOG1 ALOG6 refer to Table 8 5 E External Control Pressure Pump C Units volts 5000 Problem Status Pump A Pressure Pump D Resolution 0 2 millivolt No problem Units psi 5 Range 7500 to 58035 E Em i i Empty cylinder Resolution 0 2psi 1 5000v to 11 6070v B Cylinder at botto FE 4 74 1 41 rar Over pressure RO F 18000 33036 21000 79500 0 2105 2245 4845 500 27067 4000000000 0010696698 L U Under pressure M Motor failure 0200000000 0057744
258. p must be attached to this con nector Check the serial number tag to make sure the voltage rat ing of the pump is correct Connect the line cord to the MAINS connector on the back of the pump For all systems connect the control cable of the pump module Pump A for multiple pump systems to the connector labeled PUMP A on the rear panel of the controller Subsequent pumps in multiple pump systems can be connected to controller connectors PuMP B PUMP C and PUMP D The transducer cable refer to Figures 1 9 and 1 10 must be plugged into the PRESSURE TRANSDUCER connector on the rear panel of the pump module for the pump to operate Cable part numbers and lengths are listed in the following chart USB and TCP IP use cable package 60 1247 168 Pump controller connect cable see Figure 1 10 7 ft 2 1m attached to Pump module transducer cable see Figure 1 9 4 ft 1 2m pump 30D 65D Pump module transducer cable L 45ft 1 4 m 69 1244 413 1 19 D Series Syringe Pumps Section 1 Introduction Hazloc pumps 10 ft 3m 68 1020 505 Extension cable for pump controller connect 50 ft 15 24m 68 1020 506 9 D Series Pumps 2 only 10 ft 3m 68 1020 210 50 ft 15 2m 68 1020 214 RS232 Cable for computer serial control of a sin gle controller 9 pin to 25 pin 6 ft 1 8m 480 7996 00 nj DT
259. p ofthe screen 4 8 D Series Syringe Pumps Section 4 Gradient Pumping for Pressure Flow and Concentration Modes N PGa FILE 1 STEP 1 STORE TO EXIT 1 INIT OPSI 3 RATE 0 00PSI MIN 2 FINAL OPSI 4 DURATION 1 0MIN INSERT DELETE or b FGa FILE 1 STEP 1 STORE TO EXIT 1 INIT 3 RATE 0 00 2 FIN 4 DURATION 1 0MIN INSERT DELETE 6 To set the initial pressure or flow for this step press INIT 1 to activate this parameter Use the number keys to enter the desired value then press ENTER to save it To set the final pressure or flow for this step press FINAL 2 to activate this parameter User the number keys to enter the desired value then press ENTER to save it Set either the desired RATE 3 of change or DURATION 4 in minutes Once one value has been set and saved the other will automatically appear M Note DURATION in minutes can have a resolution of 0 1 with a maximum of 9 999 minutes per step If you want to add another step to the file program press INSERT C The step number will increase by one and the default ini tial value will be the final value entered for the previous step Edit as desired When programming is complete press the STORE key to save the file and return to the home screen To start the program press RUN two times M Note When a gradient run is started digital output 8 of the controller ACCESSORY connector will
260. pecific volume at a set flow rate or pressure or a two pump flow concentration All Teledyne Isco syringe pump models can be used in gradient mode The model 65D requires special hardware for this Call the factory for complete information You can program the controller to increase or decrease pressure or flow during different steps within a single program by entering a specific value at the beginning and end of each step NDANGER RISK OF INJURY THE PRESSURE PRODUCED COULD BE 700 BAR PLEASE UTILIZE APPROPRIATE TUBING AND CONNECTIONS NOTED IN THE MANUAL Tools and Parts for Single Pump System Open end wrenches Ya 556 746 3 8 Manual Refill Valve Kit see Table 4 1 Manual Outlet Valve Kit see Table 4 2 Tools and Parts for Dual Pump System Open end wrenches lu Sag Ag Ye Manual Refill Valve Kit see Table 4 1 two kits required Gradient Mixer Package part 68 1247 080 Table 4 1 Manual Refill Valve Kits Pump Model Part Number 1000D 68 1247 117 500D 68 1247 083 65DM 100DM DX 260D 68 1247 077 65D 68 1247 127 30D 60 1247 180 4 1 D Series Syringe Pumps Section 4 Gradient Pumping for Pressure Flow and Concentration Modes 4 2 Connecting the 4 2 System Table 4 2 Manual Outlet Valve Kits Pump Model Part Number 1000D 68 1247 118 500D 68 1247 082 65DM 100DM DX 260D 68 1247 078 65D 68 1247 126 30D The syringe pump has two
261. ports at the top of the cylinder One port is used as the inlet for filling the pump and the other as the outlet either port may be used as inlet or outlet Inlet and outlet connections to each pump must be made identically Standard plumbing connections vary between pump models See Table 4 3 for standard port information When making fluid connections that use ferrules be sure to use the ferrules supplied for that pump by Teledyne Isco Push the tubing completely into the connector and finger tighten Then 60 1247 181 tighten with a wrench to clamp the ferrules onto the tubing Table 4 3 Swaging Detail 1 g Valco FERRULE NUT 5 16 24 a IH 1 2 TURN PAST FINGER TIGHT 18 NPT FRONT FERRULE NUT 5 16 24 al 3 4 TURN PAST BACK FERRULE FINGER TIGHT 1 4 NPT FRONT FERRULE NUT 7 16 20 1 1 4 TURN PAST di BACK FERRULE 77 FINGER TIGHT 1 4 F250C M Note LULLAK N GLAND NUT 2 Pump models 2600 100DM DX and 65DM have direct con nection as shown in Figures 4 1 and 4 2 on the following page Valve kits for other models include male adapter fittings D Series Syringe Pumps Section 4 Gradient Pumping for Pressure Flow and Concentration Modes A gradient pumping system includes high pressure two way valves that connect the
262. pper the ports which will not be con nected to the continuous flow package NDANGER RISK OF INJURY THE PRESSURE PRODUCED COULD BE 700 BAR PLEASE UTILIZE APPROPRIATE TUBING AND CONNECTIONS NOTED IN THE MANUAL 3 Attach the connectors appropriate to your pump to the 6 4 cm unbent stainless steel tubing lengths and use the 5 2 5 2 3 Inlet Tubing D Series Syringe Pumps Section 5 Continuous Flow Introduction Installation amp Operation 18 nuts and ferrules to attach to the double check valve housings Attach the inlet tubing assembly The tubing you use depends upon whether or not your source is pressurized a Pressurized Reservoir Connect the 18 x 1 5 m stainless steel tubing to the bottom of the inlet tee using high pressure valve fit tings M Note The filter and PTFE tubing are not used b Nonpressurized Reservoir Connect the l amp x 1 5 m PTFE tubing to the bottom of each inlet check valve using the ferrule and nut with support spring provided in the package Attach the tub ing to the filter connector and then connect the filter M Note The stainless steel tubing is not used 5 Once the contents of the continuous flow package are totally assembled attach the connectors appropriate for your pump on one side of the assembly to a port Then sup porting the tee valve assembly attach the other connector to the port of the second pump Attach the outlet fittings to the top of the uppe
263. pump inlets to fluid reservoirs and the pump outlets to the gradient mixer dual pump system or other apparatus single pump system Each refill kit and outlet valve Two Way package contains one two way valve the gra Valve part dient package contains two The kits contain 209 0098 05 all tubing and hardware necessary for valve installation Following installation the tubing connections must be tested for leaks before any program is run Ifa leak is found tighten the connection slightly Ifthe leak persists swage the connection again with a new ferrule Refer to Technical Bulletin TB05 Field Verification Procedures at http www isco com sp_applications techbulletins for leak test procedures 4 3 D Series Syringe Pumps Section 4 Gradient Pumping for Pressure Flow and Concentration Modes Figure 4 1 Pump inlet connections 4 2 1 Inlet Connections 4 4 Kit components and connections are shown in Figure 4 1 1 Mount the inlet valve on the pump housing with the spacer block and screws provided 2 Connect the pre bent SST tubing from one port of the valve to the pump inlet Use the nut and ferrule to connect the tubing at the inlet and the valve fittings to connect the tub ing at the valve 3 Connect the PTFE refill tubing with the filter to the other port of the valve using the nuts and ferrules supplied M Note When connecting to pressurized sources in supercritical fluid applications use the stainless
264. r sensor fails the sensor harness must be replaced Press EXIT D to return to the diagnostic menu 9 5 5 SERIAL TEST Tests the serial channel First confirm operation of the internal port On the RS 232 C port on the rear of the controller short pins 2 and 3 and then run the test The screen should display Rec Serial Test Sent Serial Test Press any key to exit The four digits in the REC line should match the four digits in the SENT line with a very slight delay If the unit passes the internal port test next perform the I O test Use a null modem cable available from Teledyne Isco part 480 7996 00 to connect the 9 pin serial output port of a com puter to the RS 232 C port as shown on the following page M Note Avoid using a USB converter cable test results have not been shown to be dependable D SERIES IN ue n CONTROLLERS CONTROL COMPUTER 9 RS 232 C 7 RS 232 C a T 17 C A Null Modem Cable SYRINGE PUMP part 480 7996 00 Figure 9 5 Serial connection to a computer 9 8 9 6 Removing the Case Top 9 6 1 Controller Case Top Removal D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing Open a terminal emulator program such as HyperTerminal Hilgraeve Inc Monroe The factory default port settings are BPS
265. r specified value pressure point or until a user specified time out period time point This reduces pressure in the cylinder before the inlet valve is opened The NCV software feature is disabled by default however if no check valve is installed on the supply line it is recommended that this feature is enabled A check valve is not provided for Ball Valve Packages It is rec ommended to turn ON the NCV feature before operating the valves 1 Contin Const Flow 2 Contin Const Press MORE OTHER OPTIONS MULTI PUMP NCV 1 AB Pumps 1 Pressure Point 2 CD Pumps 2 Time Point 3 Function NCV Figure 5 12 Keystrokes to set up No Check Valve 5 20 D Series Syringe Pumps Section 5 Continuous Flow Introduction Installation amp Operation 5 6 5 To Run or Stop This menu setting allows the operator to run or stop both pairs of pumps simultaneous PREVIOUS Press 3x to return to run screen MULTI PUMP Four PUMP Run SToP Figure 5 13 Keystrokes to Run or Stop the pumps M Note Before pressing RUN ensure that ON CONT FLOW is displayed on the screen and that the set flow rate pressure is correct Always verify the valve settings before running a program If a controller is reset or moved to a different power source it will revert back to default settings Active 5 6 6 Tips for Running Liquids Checklist Continuous Flow 1 Degas liquids if appropriate 2 Purge air from
266. r tee Fit tings for 18 tubing as well as an optional reducing fitting for 146 tubing are provided Use the fittings appropriate for your tubing size 7 Tighten all fittings There are two types of inlet tubing provided with this kit The stainless steel tubing is to be used for a pressurized inlet source the PTFE tubing may be used if the source is not pressurized NDANGER RISK OF INJURY THE PRESSURE PRODUCED COULD BE 700 BAR PLEASE UTILIZE APPROPRIATE TUBING AND CONNECTIONS NOTED IN THE MANUAL M Note The fittings for connection to pressurized source are not pro vided A CO cylinder connection package P N 68 1247 043 is available Refer to section 2A 3 2 of the Instruction Manual 5 3 D Series Syringe Pumps Section 5 Continuous Flow Introduction Installation amp Operation 10 2600 ul 65DM PUMP OUTLET g REDUCING FITTING Y FOR 1 16 TUBING OUTLET TEE N PUMP 65DM 100DM DX 260D 8 CONNECTOR lt EACH E FACTORY CONNECTED SML 100 260D _ 65DM PUMP m EN nn rP PLUG ra ll FILTER ASSEMBLY a 7200 PUMP PLUG ep INLET LOW PRESSURE 500D CONNECTOR ASSEMBLY P 2 EACH ee STEEL FILTER ASSEMBLY INLET HIGH PRESSURE INLET LOW PRESSURE N TO USE 500D CONNECTOR DISCONNECT AT HEX NUT INDICATED TO USE FILTER ASSEMBLY DISCONNECT AT HEX NUT INDICATED FOR 1 8 TUBING JA USE 1
267. red to provide a 4 20 mA current loop output The 4 20mA analog output board is pre installed at the factory but can also be purchased in an upgrade kit The board initially contains three output cards for flow rate pressure and volume for Pump A Additional cards can 3 23 D Series Syringe Pumps Section 3 Basic Programming and Operation be purchased to output data for one or two more pumps Refer to Table 3 3 for connections for the 4 20mA and 0 10v 12 channel outputs Connections to the controller DB 25 are the same as shown in figure 3 14 Refer to Table 3 3 and Table 3 4 for cable connections to your equipment Table 3 3 Analog Output Signal Sub D Pins for 4 20mA Pin Channel Data Type Pump 4 Pump A Flow Rate 1 Pump A Flow Rate Signal Return 5 2 Pump A Pressure Signal Return 6 3 Pump A Volume Remaining 3 Pump A Volume Remaining Signal Return 1 4 Pump B Flow Rate 4 Pump B Flow Rate Signal Return 8 5 Pump B Pressure 5 Pump B Pressure Signal Return 9 6 Pump B Volume Remaining 6 Pump B Volume Remaining Signal Return 20 1 Pump C Flow Rate 1 Pump C Flow Rate Signal Return 21 Pump C Pressure 8 Pump C Pressure Signal Return 22 9 Pump C Volume Remaining 8 Pump C Volume Remaining Signal Return 23 10 Pump D Flow Rate 10 Pump D Flow Rate Signal Return 24 fi Pump D Pre
268. ressed all corrected offsets will be lost To perform a basic reset press MENU SYSTEM RESET 5 CON TINUE A To perform a hard reset 1 Turn the controller switch to STANDBY 2 Press and hold CLEAR ENTRY 3 While still holding CLEAR ENTRY turn the controller switch to ON Continue holding down CLEAR ENTRY for one second D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing 4 Release the CLEAR ENTRY key and turn the controller switch back to STANDBY 5 Turn the controller switch back to ON and perform the Basic Reset as described above 9 5 D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing 9 5 Diagnostic Menu The syringe pump controller can run a number of system tests that are initialized using the keypad MORE MORE 2 DIAGNOSTIC MENU 1 LCDTEST 4 KEYPADTEST 2 ANALOGINPUTS 5 MOTOR CONTROL LIMITS 3 A DCAL 6 SERIALTEST MORE PREVIOUS Figure 9 2 Accessing the diagnostic menu 9 5 1 LCD TEST Cycles all segments of the display through all displayed char acters To stop the test press any key 9 5 2 ANALOG INPUTS Displays the values of all analog inputs in volts In the left column with all connected pumps at zero pressure the pressure readings should be near zero After the initial reading pressurize the pump and then observe the test screen once more to verify that the value for that pump has increased The right co
269. rformed using the keypad on the front panel The controller front panel is shown in Figure 1 5 and described in Table 1 10 Table 1 11 explains the key functions The rear panel of the pump controller contains several input and output connectors explained in Table 1 12 and shown in Figure 1 6 The only operational control on the pump itself is the power switch shown in Figure 1 8 The rear panel has several con nectors described in Table 1 13 and shown in Figure 1 7 REFILL CONST RAPID ZERO FLOW PRESS PRESS Figure 1 5 Pump controller key functions Item No on Figure 1 5 Table 1 10 Connector Pump Controller Front Panel Label Description On Standby switch Turns instrument off and on Does not disconnect power Programming keypad Used to program controller Softkeys Labeled A B C and D used to select menu items displayed directly above them Liquid crystal display 40 Characters x 4 line ON STANDBY D Series Syringe Pumps Section 1 Introduction Table 1 11 Pump Controller Key Functions Description Two position toggle switch turns controller on and activates drive motor to maintain position Standby disables the drive motor and halts the controlling processor A C D Softkeys used to select displayed options PRGM GRAD Program gradient Puts pump in gradient mode and accesses the soft key driven gradient programming CONST PRESS Consta
270. ring static tests Under these conditions pressure control may be more stable with integral compensation off If the pressure integral compensation is off there will be a pressure error proportional to the delivery flow rate For this reason the pressure integral is normally turned on for anything but very low flow rates This feature is ON by default Press 1 2 3 or 4 for the associated pump A B C or D to toggle the feature OFF This feature prevents pump pressure hunting when delivering at low flow rates 0 12 ml min for the 30D pump or 0 25 ml min for other models When this function is ON the pump pressure may exceed the set point by up to 3 psi without the piston backing up to reduce the pressure If the pump pressure exceeds the set point by more than 3 psi the motor will reverse the piston until the 3 psi dead band maximum is reached No dead band is allowed if the flow rate is above 0 25 ml min 0 12ml min for 30D pump or when the pressure error is neg ative pressure below the set point If the 3 psi positive pressure error is not acceptable at low flow rate toggle the dead band feature OFF by pressing 1 2 3 or 4 for the associated pump B C or D This feature is ON by default Beginning with Rev 1 05 firmware the Modbus RTU communi cations protocol is supported Rev 2 0 or higher firmware sup ports Modbus TCP communications protocol Complete information about using Modbus RTU and Modbus TCP commu
271. rmance at flow rates under 500 pl min The insulating cover is not available for Models 500HPx and 30D Part numbers e Insulating cover for 65D 60 5364 267 e Insulating cover for 65DM 100DM DX and 260D 68 1247 081 e Insulating cover for 500D 68 1247 085 The cover consists of two pieces that fit over the cylinder as shown in Figure 2 11 Figure 2 11 Cylinder insulation cover 2 12 D Series Syringe Pumps Section 2 Fluid System Connections and Accessories Notches in the cover provide openings for the inlet and outlet tubing and for the cable to the pressure transducer Installation 1 Install the back cover 2 Route the cable around tubing through the appropriate tabs 3 Install the front cover and secure the side latches 2 4 2 Temperature Control The optional cylinder temperature jacket assists in maintaining Jacket cylinder temperatures 30 to 100 C by circulating liquids such as water or water ethylene glycol solution through the 14 upper and lower hose connectors CO connection kit 2 co I 2 1 NP d Sr 1 5 E A L a 1 D 2 1 Au 1 N 33 1 a io 5 TI ct ic B Extruder 13 Circulating Reactor 1 bath Rock Core 1 Etc 1 1 LI 1 1 I 5 1h loe Figure 2 12 System with temperature control jacket installed The jacket is very useful for SFC applications where cylinder
272. rs at constant temperature PRESSURE DISPLAY RESOLUTION AMBIENT TEMPERATURE RANGE 6 895 kPa 5 to 40 C TEMPERATURE DRIFT 0 0 12 of full scale C HUMIDITY 95 maximum DEAD HEADSPACE VOLUME 1 30 0 020 ml POLLUTION DEGREE INSTALLATION CATEGORY MAXIMUM ALTITUDE NOTES Underwriters Laboratories UL has certified all D Series Pumps with the exception of the 100 VAC versions Using water at 137 9 bar and a temperature controlled environment at 30 C The analog output is an optional accessory Pressure repeatability specification is based upon re zeroing pressure transducer every 48 hours Refer to sub section ZERO PRESS in Section 3 of the manual for re zeroing procedure e Volume in and above the piston seal head clearance at automatic shutoff and inlet and outlet ports to the fittings 1 5 D Series Syringe Pumps Section 1 Introduction Table 1 5 100DX Technical Specifications CYLINDER CAPACITY 102 93 ml POWER REQUIREMENTS 100 x 10 VAC 1 5 A maximum 117 12 VAC 1 5 A maximum Fractory Set 234 23 VAC 0 75 A maximum Mains voltage line cord is a Disconnect Device LINE FREQUENCY 50 or 60 Hz LINE VOLTAGE NOISE TOLERANCE 1 7 x nominal rms line voltage 10 usecond pulses any phase angle random or repetitive DIMENSIONS PUMP CONTROLLER Width 27 18 cm 27 18 cm Depth 46 74 cm 30 48 cm Height 101 09 cm 13 59 cm WEIGHT PUMP CONTROLLER 3
273. rt Numbers 9 4 Piston Wrench Tools oee ee eee eee een 9 16 Replacement Shear Keys 9 19 Continuous Flow Technical Specifications Air Valves B 2 Continuous Flow Technical Specifications Electric Valves B 4 Accessory Control Digital Outputs B 7 Key functions in the Multi pump Mode B 8 xxi D Series Syringe Pumps Table of Contents xxii D Series Syringe Pumps Section 1 Introduction 1 1 About This Manual 1 2 Specifications The 65DM 100DM 100DX 260D and 500D pumps have le standard Valco ports Pipe thread fittings of 14 diameter are used for the 1000 38 diameter for the 500HPx and We diameter for the 500D The 65D and 30D use AE F250C high pressure fittings Because of these differences the packages tubing and options for different models have different part numbers Additionally these pumps are typically used for dif ferent applications therefore optional kits and accessories may differ The installation procedures for the different D Series pump models have been combined where applicable and separated where necessary for your convenience Optional system configurations may require additional kits and or software These additional options are described in their respective sections This manual contains the fol
274. s REPLACEMENT PARTS LIST NO 60 1242 334 SHEET 2 OF 2 REV B DATE 03122 ee PART NUMBER DESCRIPTION ST 209 0169 41 1 8 TUBING FERRULE ZERO VOLUME ALD s 60 1203 525 Mene o 209 0161 01 V 8 1 8 TUBING MALE CONNECTOR SWAGELOK 10 69 1243 572 3 WAY VALVE 15 60 1243 516 SINGLE CHECK VALVE HOUSING 20 209 0169 81 1 8 OD TUBING NUT UPCHURCH 209 0161 73 1 4 OD TUBE FITTING 209 0093 26 SOLENOID VALVE NOTE 1 This list is subject to change without notice A 66 D Series Syringe Pumps Appendix A Replacement Parts A 1 17 Dual Air Valve Package for 500HPx IN zz m TS il 67 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST SHEET 2 OF 2 TELEDYNE ISCO REV PART NUMBER DESCRIPTION 09404 2 WAY BALL VALVE 6998 MALE ELBOW CONNECTOR 12 TUBING 631 3 8 FRONT TUBING FERRULE 631 3 8 BACK TUBING FERRULE 650 S097 90166 3 8 TUBE FITTING NUT 53632 INTERMEDIATE TUBE 33032 LOWER CROSSOVER T 5363212 UPPER CROSSOVER T 605363213 PUMP TUBE 691243514 AIR ACTUATOR 023050403 1 8 AIR LINE TUBING OoO o o no no no mno no nmo 2 3 4 5 6 9 S 0 2 NOTE For current prices ond quotatio
275. s and Notices EXPLOSION WARNING WARNING Teledyne Isco D Series Pumps SFX 2 10 and SFX 220 Extractors are NOT EXPLOSION PROOF Teledyne Isco SFX System and D Series Syringe Pump Safety Note when using a flammable fluid The Teledyne Isco SFX system and syringe pumps must be placed within a prop erly operating vent hood fume cupboard when using ethane or any other flamma ble gas Ensure that all SFE tubing connections are completely free of any gas leaks by performing the leak test using CO detailed in Section 2 of the D Series pump manual Section 5 of the SFX 2 10 manual and Section 6 of the SFX 2 10 220 and SFX 3560 manual There must absolutely be NO gas leaks present before introducing the flammable gas In a temperature stable leak free system the flow rate as registered by the pump should settle to a value below 0 01 ml min after 15 minutes during a static extraction Important When using a Teledyne Isco extractor either SFX 2 10 SFX 220 SFX 3560 be absolutely sure the built in venting fan a brushless motor is operating properly The Teledyne Isco D Series Syringe Pumps and the SFX units use brush type drive motors Minor modifications to the pumps may render them safer especially in the rare event of catastrophic piston seal failure However these modifications will not make these pumps explosion proof e Remove the front and back cylinder covers located on the ball screw tower This will allow any escaped
276. s applying torque and the valve is in its closed position The valve may have to be opened and closed more than once to complete this procedure 9 42 D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing Figure 9 41 Electric valve motor adjustment 9 43 D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing 9 44 D Series Syringe Pumps Appendix A Replacement Parts A 1 Replacement Parts Replacement parts are called out in the following illustrations Refer to the call out in the adjacent table to determine the part number for the item Replacement parts can be purchased by contacting Teledyne Isco s Customer Service Department Teledyne Isco Customer Service Department P O Box 82531 Lincoln NE 68501 USA Phone 800 228 4373 402 464 0231 FAX 402 465 3022 E mail Iscolnfo teledyne com A 1 D Series Syringe Pumps Appendix A Replacement Parts A 1 1 D Series Controller 2 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST SHEET 2 OF 2 TELEDYNE ISCO REV UMBER DESCRIPTION 14 230 CABLE ASSEMBLY 23 CABLE ASSEMBLY 232 CABLE ASSEMBLY 1 410 DISPLAY ASSEMBLY 12477 SWITCH ASSEMBLY IS CABLE ASSEMBL 211 FRONT LABE ND MOUNTING PLATE 17 173 REPLACEME CBA CONTROLLER I 114 REPLACEME CBA 4 20 CONTROLLER 17 185 REPLACEME CONTROLLER 30D
277. s in Hold clock stopped 1 Pump A amp Pump B in Concentration Gradient 1 Pump A in Pressure Gradient 1 Pump A in Flow Gradient 1 Controller in Local Operation 1 Controller in Remote Operation 1 Controller in External Operation 1 External Refill control enabled 1 Zero pressure sensor offset for Pump A 1 Zero pressure sensor offset for Pump B 1 Zero pressure sensor offset for Pump C 1 Zero pressure sensor offset for Pump D 0 Pressure Integrator for Pump A OFF 1 Pressure Integrator for Pump A ON 0 Pressure Integrator for Pump B OFF 1 Pressure Integrator for Pump B ON 0 Pressure Integrator for Pump C OFF 1 Pressure Integrator for Pump C ON 0 Pressure Integrator for Pump D OFF 1 Pressure Integrator for Pump D ON 0 Pressure Deadband for Pump A OFF 1 Pressure Deadband for Pump A ON 0 Pressure Deadband for Pump B OFF 1 Pressure Deadband for Pump B ON 0 Pressure Deadband for Pump C OFF 1 Pressure Deadband for Pump C ON 0 Pressure Deadband for Pump D OFF 1 Pressure Deadband for Pump D ON 0 AUTO REFILL A OFF 1 AUTO REFILL A ON 0 AUTO REFILLB OFF 1 AUTO REFILL B ON 0 AUTO REFILL C OFF 1 AUTO REFILL C ON 0 AUTO REFILL D OFF 1 AUTO REFILL D ON 0 AUTO FILL A OFF 1 AUTO FILL A ON 0 AUTO FILL B OFF 1 AUTO FILL B ON 0 AUTO FILL C OFF 1 AUTO FILL C ON 0 AUTO FILLD OFF 1 AUTO FILL D ON 0 DIGITAL OUTPUT BIT 1 HIGH 1 DIGITAL OUTPUT BIT 1 LOW 0
278. s menu 4 If you need to change the minimum pressure limit press 2 MIN Enter the desired minimum pressure using the numeric keypad and press ENTER to store the value 5 Press D PREVIOUS to return to the Limits menu 6 Continue pressing D to return to the run screen 7 MODIFIER ON will be displayed above softkey B and 96 PUMP will be displayed above softkey C To designate the desired modifier concentration press C Then use the numeric keys to enter the desired percentage of modifier Press ENTER to save the desired value 6 7 D Series Syringe Pumps Section 6 Modifier Addition 6 3 Refilling To refill the COs pump 6 8 8 Open the outlet valves of both pumps if they are not open 9 Press RUN 10 When the pressure for Pump A is established the message HOLD PRESS RUN will be displayed 11 Open the extractor inlet valves 12 The message EQUILIBRATE will be displayed on the controller screen If the controller does not display EQUILIBRATE press RUN While this message is dis played no modifier will be delivered 13 Immediately open the extractant outlet valve s Flow MUST be established through the system at or before the time EQUILIBRATE is displayed To properly equilibrate the pumps they must be delivering fluid 14 Once the message RUNNING is displayed modifier will be delivered at the selected rate Once your modifier addition system is running you will occa siona
279. s not running press MENU MORE MORE 2 3 to display the A D Cali bration screen 2 Adjust R109 REF to obtain a voltage of 2 5000 VDC 0 0001 at TP18 REF with respect to TP28 A GND 3 Connect a jumper between TP25 ANLG2 and TP28 A GND 4 Connect a jumper between TP21 ANLG1 and TP18 REF 5 Adjust R86 GAIN until the GAIN display reads 2 5000 0 0001 6 Adjust R10 OFFSET until the OFFSET display reads 0 0000 0 0001 7 Repeat steps 5 and 6 until both readings are within 0 0001 8 Remove the jumpers 9 14 3 Limit Sensor In the event that the limit sensors must be replaced on the pump Adjustment use the following procedure 9 35 D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing 1 Disconnect the instrument from mains power 2 Disconnect the pressure transducer cable from the pump and remove the tubing from the inlet and outlet ports 3 Loosen the four cover screws and remove the front and rear covers ofthe pump 4 The cylinder must be unscrewed several turns to avoid accidentally bottoming the piston out during calibration of the limit sensor Therefore loosen the cylinder lock screw The lock screw is located in the front side of the cylinder mounting block and is a 14 20 setscrew 5 The limit sensor assembly includes two limit sensors the wire harness and connector and a conduit which protects the wires running between the sensors Figure 9 38
280. s often impossible to remove a burr that blocks the inner bore 2 2 4 Accessory Packages The accessory packages for all pumps contain fittings that allow you to attach tubing to the pump refer to Figure 2 1 as well as appropriately sized cylinder seals Note that the tubing is not included Installation 1 Slide first the nut and then the ferrule over the tubing 2 Push the tubing all the way into the port 3 Hold the tubing in place and tighten the nut Table 2 1 D Series Syringe Pump Accessory Packages 1000D 60 1249 103 500D HPx 60 1249 016 65D 60 1249 024 30D 60 1249 131 260D 60 1249 012 100DM DX 60 1249 015 65DM 60 1249 028 2 3 D Series Syringe Pumps Section 2 Fluid System Connections and Accessories 2 2 5 Installing the 1 16 Refer to Figure 2 1 Fittings 260D 65DM 1 Loosen the l46 nut on the adapter until it is held by a few and 100DM DX only tienda 2 Insert the adapter into the port and finger tighten the fit tings Retighten the nut until it is also finger tight Tighten the 48 nut with a wrench to crimp the ferrule Insert the 16 tubing through the 46 nut until it stops Tighten the 146 nut ig Nut IH 9 HE i Ferrule he Ferrule hg Tubing o B Figure 2 2 Egg Tubing adapter for 30D 65D pumps M Note It is recommended that after tightening the fittings be removed and examined F250 Fitting Connection Refer to Fi
281. s reached Press MENU gt REFILL 3 The auto refill menu will appear If more than one pump is connected to the controller pump B pump C and pump D will be displayed on the fourth line To select a pump press the softkey under the pump designation Press 1 to set the volume for pump A The units to the right of the symbol will blink indicating that you should enter a volume Use the number keys to enter an appropriate value and then press ENTER 1 Press to set the refill rate for the designated pump The refill rate can also be changed from the main screen while the pump is refilling 2 A message will blink on the screen prompting you to enter the selected refill rate 3 Enter the desired rate with the number keys press ENTER 4 To save and exit the refill menu press D PREVIOUS The first line will display OFF or ON indicating whether or not this feature is enabled for pump A or the currently selected pump Press 4 to toggle this feature off or on for each pump Auto refill can be set independently for each pump If AUTO REFILL is ON the pump will automatically switch to refill mode when the volume reaches the auto refill mark After refilling pumping will resume in the programmed mode The ACCESSORY outputs which drive powered valves will switch in sequence 3 4 4 Power Failure STOP 3 4 5 System Reset Restore Default Settings 3 4 6 Display Contrast 3 5 Menu Two D Series Syringe
282. seal head clearance at automatic shutoff and inlet and outlet ports to the fittings 1 6 D Series Syringe Pumps Section 1 Introduction Table 1 6 260D Technical Specifications CYLINDER CAPACITY 266 05 ml POWER REQUIREMENTS Mains voltage line cord is a Disconnect Device 100 10 VAC 1 5 A maximum 117 12 VAC 1 5 A maximum 234 x 23 VAC 0 75 A maximum Factory Set LINE FREQUENCY 50 or 60 Hz LINE VOLTAGE NOISE TOLERANCE 1 7 x nominal rms line voltage 10 usecond pulses any phase angle random or repetitive DIMENSIONS PUMP CONTROLLER 27 18 cm 27 18 cm 46 74 cm 30 48 cm 101 09 cm 13 59 cm Width Depth Height WEIGHT PUMP CONTROLLER 32 8 kg 2 96 kg FLOW RATE RANGE See Figure 1 1 FLOW RATE ACCURACYP 0 5 maximum 0 50 ul min seal leakage FLOW RATE DISPLAY RESOLUTION 1 0 ul min ANALOG OUTPUT ACCURACY x 196 of selected range DISPLACEMENT RESOLUTION REFILL TIME REFILL OR DEPRESSURIZATION RATE 16 63 nl step 2 5 minutes 1 0 ul min to 107 ml min at any pressure from 0 to 517 1 bar PRESSURE RANGE 0 6895 to 517 1 bar PRESSURE ACCURACY 0 5 of full scale at constant temperature PRESSURE REPEATABILITY 0 5 of full scale within 48 hours at constant temperature ZERO PRESSURE DRIFT 0 25 of full scale within 48 hours at constant temperature PRESSURE DISPLAY RESOLUTION AMBIENT TEMPERA
283. ss PRE VIOUS RETURN D 1 SERIAL OPTION 4 MULTI PUMP 2 STATUS 5 TOTAL VOL RESET 3 EXTERNAL 6 VALVE MORE PREVIOUS Figure 3 3 Menu 2 program selections 3 5 D Series Syringe Pumps Section 3 Basic Programming and Operation 3 5 1 Serial Option Figure 3 4 Serial option menu 3 5 2 Pump Status 3 5 3 External Control 3 5 4 Multiple Pumps 3 5 5 Total Volume Reset Figure 3 5 Total volume reset 3 6 The serial option menu allows you to set the baud rate and the unit identification number BAUD RATE 1200 UNIT ID 6 NEXT BAUD NEXT ID PREVIOUS A B C D Use softkey A NEXT BAUD to scroll through the available baud rates These are 300 1200 2400 4800 9600 19 2K 38 4K 57 6K and 115 2K Use softkey B NEXT ID to scroll through the available ID numbers These are 1 7 Six is the default as this is the unit identifier for the Teledyne Isco LabView software For a complete discussion of serial control refer to Section 8 in this manual This option displays the controller software revision and model of connected pump s The first line displays the revision of the software Lines 2 3 and 4 display the type of pump connected to the A B C and D pump connectors respectively This screen is also momentarily displayed automatically each time the pump controller is switched on The pump pressure or flow rate operation can be controlled externally with an analog
284. ssure 11 Pump D Pressure Signal Return 25 12 Pump D Volume Remaining 12 Pump D Volume Remaining Signal Return 3 24 D Series Syringe Pumps Section 3 Basic Programming and Operation Table 3 4 Analog Output Signal Sub D Pins for 0 10 VDC Pin Channel Data Type Pump 1 Pump A Flow Rate 4 Pump A Flow Rate Signal Return 2 5 Pump A Pressure Signal Return 3 3 Pump A Volume Remaining 6 Pump A Volume Remaining Signal Return 4 4 Pump B Flow Rate 1 Pump B Flow Rate Signal Return 5 5 Pump B Pressure 8 Pump B Pressure Signal Return 6 6 Pump Volume Remaining 9 Pump B Volume Remaining Signal Return 1 1 Pump C Flow Rate 20 Pump C Flow Rate Signal Return 8 Pump C Pressure 21 Pump Pressure Signal Return 9 9 Pump C Volume Remaining 22 Pump C Volume Remaining Signal Return 10 10 Pump D Flow Rate 23 Pump D Flow Rate Signal Return 11 ii Pump D Pressure 24 Pump D Pressure Signal Return 12 Pump D Volume Remaining 25 Pump D Volume Remaining Signal Return 3 25 D Series Syringe Pumps Section 3 Basic Programming and Operation 3 26 D Series Syringe Pumps Section 4 Gradient Pumping for Pressure Flow and Concentration Modes 4 1 Introduction Gradient pumping is used in applications requiring time con trolled or rate controlled delivery of a s
285. st voltage TRANSMIT CHAIN Serial data from next unit RECEIVE CHAIN Serial data to next unit RTS CHAIN RTS buffered RS 232 C output of pin 4 input CTS CHAIN CTS chain RS 232 C input is buffered and connected to pin 5 NOTE Only pins 2 3 amp 7 are required for serial interface to one controller The Isco D Series syringe pump controller may include an optional USB interface The USB connections are located on the pump controller rear panel labeled USB Ethernet The connector pin usage is outlined in Table 8 2 Use optional cable PN 60 1244 487 to connect the USB to the 25 pin connector labeled USB Ethernet The drivers for the USB can be down loaded from http www isco com support updates asp N WARNING Connecting devices to energized circuits may cause personal injury or property damage Power must be removed from the pump before connecting external devices Table 8 2 USB Interface Pin Connections The cabling scheme for your system will depend on the number of instruments you need to control The computer is always con nected from the serial port to the serial port s of the D Series controller s it is controlling Each controller is connected to its pumps in the normal fashion i e the pump control cables are attached to the pump A B and C connectors on the rear panel of the pump controller The cable you select to connect to your network will depend on the type of serial port your
286. steel tubing without a filter An in line filter is contained in the CO connection package refer to technical bulletin TBO8 CO Applications and Technical Notes at http www isco com sp_applications techbulletins nut ferrule pre bent 7 SST tubing spacer block PTFE tubing or stainless steel tubing valve filter D Series Syringe Pumps Section 4 Gradient Pumping for Pressure Flow and Concentration Modes 4 2 2 Outlet Connections Figure 4 2 Pump outlet connections Kit components and connections are shown in Figure 4 2 1 Mount the two way outlet valve on the side ofthe pump housing opposite the refill valve with the spacer block and screws provided 2 Connect the pre bent SST tubing between one port ofthe valve and the pump outlet Use the nut and ferrule to con nect the tubing at the outlet and the valve fittings to con nect the tubing at the valve 3 Connect the 5 1 cm length of l tubing to the other port of the valve using the valve fittings 4 Connect the l side of the reducing union to the tubing 5 Connect the side of the reducing union to the 1 5 m length of tubing This tubing may be cut to an appro priate length 1 8 NUT 1 8 FERRULE FROM REFILL KIT ASSEMBLY pre bent SST tubing spacer block SST tubing 2 way valve REDUCING UNION VAGE TUBING APPARATUS 4 5 D Series Syringe Pumps Section 4 Gradient Pumping for Pressure
287. stem are provided in Section 5 A pump modifier system includes two D Series syringe pumps regulated by one controller and outlet check valves to prevent system back flow into the pump To connect the system you will need a modifier addition kit Consult with the factory when con figuring 65D pumps as a modifier system Installation and oper ating instructions for this system are provided in Section 6 In these modes the softkeys toggle between the options described in Table 3 1 Table 3 1 Key functions in the Multi pump Mode Display Option Description NORMAL Uses a finer slower pres sure match control when switching from one pump to the other Uses a coarser faster pressure match control when switching from one pump to the other NORMAL PRESS Uses pressure matching when switching from one pump to the other LOW PRESS Uses no pressure matching when switching from one pump to the other DELIVER Sets the pump into the delivery mode of operation RECEIVE Sets the pump into the receive mode of operation MIN MAX POINTS Sets the fill and refill marks that are used with both con tinuous flow modes Sets the NCV feature On Off See Section 5 6 4 3 9 2 Independent Control A D Series syringe pump controller can run four syringe pumps ofup to Four Separate independently of each other in either constant pressure constant Pumps flow mode dispense mode or any combination of the three
288. such as C or BASIC serial commands can be entered converted and then sent to your instrument 8 7 2 Universal Driver from Teledyne Isco D Series Syringe Pumps Section 8 Serial Interface Table 8 3 is an example BASIC language program which per forms the required portion of the DASNET serial protocol Table 8 4 is an example of a C language program which does the same Both of these programs including a DASNET serial driver written in Visual C are available on CD ROM P N ECR 60 1245 096 in the sleeve at the back of the printed manual For a console C example refer to Table 8 4 The Universal Driver from Teledyne Isco is a serial software driver that can translate commands for a variety of compilers When you are creating programs for D Series syringe pumps the driver converts serial commands to DASNET communications protocol sends them to the serial port and waits for a serial response On our website Detailed information about the Universal Driver is provided in Isco Technical Bulletin TB19 Universal Driver Software Tool LabView operation is discussed in detail in Isco Technical Bul letin TBO6 Basic Operation of LabView Toolkit A copy of the driver can be found on the CD included in the back of your D Series pump user manual It can also be downloaded from http www isco com products appnotes asp PL 105 Open the Software Utilities folder and select Universal D Series Pump driver to download the utility to a
289. t lS Shear key for 65DM Installation tool Wrench Package Various wrenches for use with most common part replacements _ Motor Brush Set Inspect the motor brushes every two years of operation or every 6 000 piston strokes whichever comes first inspect the top brush which is easier to access Other option replace entire motor Cable Ties amp Mounts Zero Volume Nut amp Ferrule 100D 260D Universal Sensor Harness 100D 260D 500D 9 3 D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing 9 3 General Cleaning Figure 9 1 500HPx fan filter 9 4 Resetting the System 9 4 1 Basic Reset 9 4 2 Hard Reset 9 4 Table 9 2 Maintenance Kit Part Numbers Kit 60 1247 060 60 1247 072 60 1247 144 60 1247 073 60 1247 074 60 1247 094 60 1247 087 60 1249 127 For general cleaning of the instrument s front panel or enclosure use a mild detergent in water or isopropyl alcohol on a sponge which is mostly squeezed out The 500HPx contains an inlet fan to cool the motors Teledyne Isco recommends inspecting and cleaning if necessary the inlet fan filter on the 500HPx every six months This action completely deletes user programmed settings erasing all programs and returning the controller to factory default settings Record your program settings and parameters before performing a reset operation If ZERO PRESS has been p
290. table pressure point and then switches automatically to the constant flow setpoint This is helpful when you are operating at a low flow rate but wish to rapidly pressurize a solvent 1 Press CONST FLOW to put the pump in constant flow mode or enter a two pump concentration gradient 2 Press RAPID PRESS 3 8 9 DISP 3 8 10 ACC CTRL 3 8 11 ZERO PRESS 3 9 Control of Multiple Pumps 3 6 D Series Syringe Pumps Section 3 Basic Programming and Operation The controller will display maximum flow rate and target pressure setting If these values are correct press D to con tinue rapid pressurization If you know approximately what the pressure will be when the system is stable enter this value as a target pressure Press A and enter the desired pressure value This should shorten the time required to stabilize the system pressure If you would like to limit the maximum flow rate during the rapid pressurization phase press B and enter the desired flow rate limit Press D to continue rapid pressurization The DISP key activates Dispense Mode for applications such as reactant feed and batch delivery where a specified volume is pumped Refer to Section 3 10 3 for programming steps The ACC CONTROL key will allow you to manually operate accessories such as valves via the Digital Output terminals on the back of the controller 1 2 3 Press ACC CTRL From the accessory control menu use the number keys
291. tem can then perform Hold the final value example below e Stop after the final step Return to the initial value and hold it Return to the initial value and repeat the program While the system is in gradient mode these options can be edited at any point before or after gradient programming and while a gradient is running To access the options menu from the home screen press OPTIONS D D Series Syringe Pumps Section 4 Gradient Pumping for Pressure Flow and Concentration Modes GRADIENT ACTION HOLD FINAL VALUE NEXT_ACTION PREVIOUS To scroll through the four options press NEXT_ACTION A When you have reached the desired option press PREVIOUS D to save and exit 4 13 D Series Syringe Pumps Section 4 Gradient Pumping for Pressure Flow and Concentration Modes 4 14 D Series Syringe Pumps Section 5 Continuous Flow Introduction Installation amp Operation 5 1 Introduction AD Series continuous flow pumping system consists of two syringe pumps and a valve accessory package regulated by one controller This system allows you to continuously deliver liq uefied gas or liquid under constant flow or constant pressure mode Continuous flow can be used in either of two modes continuous constant pressure or continuous constant flow Both of these modes assume positive displacement of the piston with the exception of continuous Receive Mode for detailed information about Receive Mode refer to te
292. the system will be constantly running however they require a user supplied pressurized air source of 80 to 115 psi 5 5 to 7 9 bar M Note Air valves can only be used with pumps A and B B 1 D Series Syringe Pumps Appendix B Continuous Flow Introduction Installation and Operation for 30D B 2 B 2 1 Dual Air Valve Installation Plumbing connections Table B 1 Continuous Flow Technical Specifications Air Pressure fluctuation at switch over Valves 34 5 bar at system backpressures from 500 psi 34 5 bar to the single pump maximum Minimum 50 76 psi 3 5 bar The single pump maximum Valves rated to 30 000 psi 2068 bar Air supply source pressure 80 to 115 psi 5 5 to 7 9 bar Maximum flow rate ml min Liquids 65 of the single pump maxi mum rate Liquefied gases 45 of the single pump maximum rate Cylinder cooling jackets should be used to obtain this rate Temperature range Wetted materials in 0 to 40 C valve packages Hastelloy PEEK and PTFE SS316 gold To install the air valve package refer to Figure 5 3 5 5 or B 1 depending on your pump model 1 Position the valve bases 1 3 cm apart 2 Use the plugs to stopper the ports which will not be con nected RISK OF NDANGER INJURY THE PRESSURE PRODUCED COULD BE 2068 BAR PLEASE UTILIZE APPROP RIATE TUBING AND CONNECTIONS NOTED IN THE MANUAL 3 L
293. tinuous Constant Flow CP Continuous Constant Pressure MO Modifier Mode 2 Pump MM Modifier Mode 3 Pump MODIFIER Put pumps in modifier addition mode PRESS PRESSB PRESSC PRESSD Enter to designate pressure setpoint constant pressure mode PRESS PRESSCD Returns the delivering pump pressure in continuous pumping mode and modifier addition mode In INDEPENDENT mode PRESS returns the pump A pressure and PRESSCD returns the pump C pressure PRESSA PRESSB PRESSC PRESSD Returns the actual pressure of the pump 8 23 D Series Syringe Pumps Section 8 Serial Interface Table 8 6 Serial Commands Continued Command Description PRESSCNTRLDIFF1 Sets the pressure control input to Analog input 1 with a pressure range of 50 psi PRESSCNTRLDIFF1 XXXXX Sets the pressure control input to Analog input 1 and sets the pressure range The range is 1 to 5000 the units are psi with a value of 5000 representing 5000 psi at 5 volts PRESSCNTRLDIFF2 Sets the pressure control input to Analog input 2 with a pressure range of 500 psi at 5 volts PRESSCNTRLDIFF3 Sets the pressure control input to Analog input 2 with a pressure range of 5000 psi at 5 volts PRESSCNTRLNORM Sets the pressure control input to the standard input PRESSDIFF XXXXX Differential pressure setpoint PSI 10 0 to 50 000 maximum 0 to 5000 psi PRESSDIFF Reads the differential pressure value PSI 10 The trans
294. tion and the fluid path status for the ACCESS CTRL connections Refer to the accessory control connections on the rear panel of the pump controller Table B 3 Accessory Control Digital Outputs Digital Pump Valve Fluid Path Status Output Location 1 A Inlet open or closed Outlet open or closed Inlet open or closed Outlet open or closed Inlet open or closed Outlet open or closed Inlet open or closed Outlet open or closed Alternate connections can be made to drive low power 12 15 V relays or electric valves Assume two wires per relay or valve The first wire is connected to the appropriate digital output on the back of the pump controller The second wire can be con nected to the 15 V connector to supply a maximum of 200 mA for switching of relays or valves Observe correct polarity if the valve or relay is polarized B 7 D Series Syringe Pumps Appendix B Continuous Flow Introduction Installation and Operation for 30D B 5 Continuous Flow Once your valve package has been properly installed and you Mode have ensured that fluid connections are leak free the system is ready for operation Teledyne Isco convention is to name the pumps pump A and pump B reading from left to right Before running in continuous flow mode become familiar with independent mode which allows the controller to operate two pumps independently and simultaneously You must oper
295. tlet ports to the fittings 1 8 D Series Syringe Pumps Section 1 Introduction Table 1 8 500HPx Technical Specifications CYLINDER CAPACITY 507 38 ml POWER REQUIREMENTS Mains voltage line cord is a Disconnect Device 100 10 VAC 5A maximum 117 12 VAC 5A maximum 234 23 2 5A maximum Factory Set LINE FREQUENCY 50 or 60 Hz LINE VOLTAGE NOISE TOLERANCE 1 7 x nominal rms line voltage 10 usecond pulses any phase angle random or repetitive DIMENSIONS PUMP CONTROLLER 27 18cm 27 18 cm 46 74 cm 30 48 cm 102 36 cm 13 59 cm Width Depth Height WEIGHT PUMP CONTROLLER 42 64 kg 2 96 kg FLOW RATE RANGE See Figure 1 3 FLOW RATE ACCURACY FLOW RATE DISPLAY RESOLUTION ANALOG OUTPUT ACCURACY x 0 596 maximum 1 0 ul min seal leakage 1 0 ul min x 196 of selected range DISPLACEMENT RESOLUTION 25 36 nl step REFILL TIME 1 25 minutes REFILL OR DEPRESSURIZATION RATE 1 0 ul min to 408 ml min at any pressure from 0 to 344 7 bar PRESSURE RANGE PRESSURE ACCURACY PRESSURE REPEATABILITY 0 6895 to 344 7 bar 0 5 of full scale at constant temperature 0 5 of full scale within 48 hours at constant temperature ZERO PRESSURE DRIFT 0 25 of full scale within 48 hours at constant temperature PRESSURE DISPLAY RESOLUTION 6 895 kPa AMBIENT TEMPERATURE RANGE 5 to 40 C TEMPERATURE DRIFT HUMIDITY DEAD HEA
296. to change without notice A 56 D Series Syringe Pumps Appendix A Replacement Parts A 1 12 Dual Electric Valve Package REPLACEMENT PARTS LIST ELECTRIC VALVE PACKAGE 0001 RZ Y x u x ES C o o7 2 N o Q Ass 9 x so SS 5 oa o o 9 3 a a 57 D Series Syringe Pumps Appendix A Replacement Parts REPLACEMENT PARTS LIST NO 60 1242 337 SHEET 2 2 REV DATE 110311 N PART NUMBER DESCRIPTION 1 60 3934 002 MOTOR CIRCUIT BOARD ASSY 60 1243 012 MOTOR ASSY W COUPLER 209 0169 44 60 1243 737 GLAND NUT 1 8 TUBING SSI TEE 1 8 TUBING INCLUDES ITEMS 3 amp 5 209 0163 53 1243 740 FERRULE 1 8 ID HASTELLOY SSI TUBING 1 8 OD 1 6 X 1 6 244 313 VALVE ASSY 1 8 TUBING INCLUDES ITEMS 3 amp 5 60 3933 061 COUPLING SHIELD 60 3933 010 SPIDER 209 0169 10 209 0169 11 FRONT FERRULE 1 8 ID FOR 500D 1000D VALVE PKG BACK FERRULE 1 8 ID FOR 500D 1000D VALVE PKG 209 0170 04 FITTING NUT 1 8 TBG FOR 500D 1000D VALVE PKG 0 1243 742 1 TUBING 1 8 OD 1 4 X 2 2 FOR 500D VALVE PKG 209 0169 27 6 60 1243 746 TUBING 1 8 OD 2 6 LONG 209 0163 60 FERRULE 1 8 ID FOR 100D 260D VALVE PKG UT 1 8 TUBING FO
297. to maintain the set pressure When mod ifier addition mode is selected and RUN is pressed pump A pressure is ramped at its maximum flow rate to the set pressure while pump B waits at a lower pressure 3 5 bar Pump B minimum pressure can be increased if the modifier boils at room temperature and 3 5 bar 6 5 D Series Syringe Pumps Section 6 Modifier Addition 6 2 Programming 6 6 Once pump A has reached the set pressure the controller will enter a hold mode and wait for a pressure drop The start of EQUILIBRATION is signaled by opening the extractor inlet or pressing RUN Flow must then be started through the system by opening all valves The modifier pump will not equilibrate properly without flow Pump B pressure is then slowly ramped upward until its check valve is detected as open At this point the controller exits EQUILIBRATION mode and displays the message RUNNING When RUNNING is displayed the controller monitors pump A piston movement and calculates the pump B piston movement required to deliver the correct ratio of modifier If pump A cannot maintain the set pressure as when the extraction cartridges are initially filling or pump A is refilling the controller reverts to EQUILIBRATION and pump B pressure is dropped below that of pump A to avoid delivery of incorrect modifier concentrations Once the pump A set pressure is reestablished the system will re equilibrate When pump B needs refilling it must first
298. toggle from high to low open to closed for one second Note that an entire gradient program can be removed only by deleting each of its steps one at a time as discussed in Section 4 5 Review Revise amp Hold Options When the last remaining step is deleted the entire file is removed D Series Syringe Pumps Section 4 Gradient Pumping for Pressure Flow and Concentration Modes 4 4 Dual Pump Concentration Gradient Programming 4 10 Two pump concentration gradients enable proportionate use of two different fluids that combine at the mixer refer to Figures 4 3 and 4 4 This type of pumping uses flow mode FG only A single pump gradient program is based on either pressure or flow and con trolled by either time duration in minutes or rate of change units per minute The Dual Pump Concentration Gradient is not available for the 30D pump Please contact the factory for details The controller s memory can contain a total of up to 200 steps One program can contain from 1 to 200 steps When operating in gradient mode any connected pumps not used for gradient are inoperable 1 To access the gradient programming menus press PRGM GRAD then DUAL SYSTEM GRADIENT 1 and CONTINUE C The home screen will appear with FG Flow Gradient in the upper left corner FGa 0 000mL MIN 2PSI 013 28mL STOPPED 00 00 00 FINAL B PROGRAM EDIT REVIEW OPTION 2 Press PROGRAM A 3 At the prompt enter a
299. tup When first setting up a system for modifier mode the pumps should be zeroed and filled To accomplish this the pumps should first be placed under independent control constant pressure mode M Note Once the modifier system is operating the system does not need to be zeroed before refilling If the pumps are running press the STOP key once Press MENU gt MORE A Press 4 MULTI PUMP to display the multi pump menu Press 4 INDEPENDENT to designate that the pumps be operated under independent control The number 4 will blink indicating that Independent Mode has been selected Press D PREVIOUS twice to return to the main menu 6 Press CONST PRESS a p To zero the pumps 1 Place the pumps in independent control constant pres sure mode as detailed above 2 Be sure the pumps are stopped 3 Disconnect the inlet tubing from the inlet valve of pump A 4 Select 2 pump independent control constant pressure mode Refer to Section 5 6 Continuous Flow Mode 6 4 To fill pump B with modifier To fill pump A with supercritical fluid helium head space tank 6 1 3 Two Pump Operation D Series Syringe Pumps Section 6 Modifier Addition Open the inlet valves of each pump Run both pumps empty Zero the pressure on each pump OID MN Reconnect the pump A inlet tubing to the inlet valve 1 Place the pumps in independent control constant pres sure mode as previously explained Be sure the
300. two pumps are used with the controller the second analog control or input wire should be connected to terminal 2 under ANALOG INPUT If three pumps are used with the controller the third analog control or input wire should be connected to ter minal 3 under ANALOG INPUT If four pumps are used with the controller the fourth analog control or input wire should be connected to terminal 4 under ANALOG INPUT When using one of the multi pump operation modes only the ANALOG INPUT terminal 1 needs to be connected to control the A B pump pair and ANALOG INPUT terminal 3 needs to be con nected to control the C D pair For the 4 20ma input option the negative output wire connects to DIGITAL GROUND The positive output wire connects to ANALOG INPUT 1 4 3 12 2 Preparation 3 12 3 External Control for Refill D Series Syringe Pumps Section 3 Basic Programming and Operation Before programming the controller to accept the analog signal you must know the maximum flow rate constant flow or the maximum pressure constant pressure M Note The high and low limits you enter cannot exceed the pump specifications Normal input 10V M Note For the 4 20ma input option the negative output wire con nects to DIGITAL GROUND The positive output wire connects to ANALOG INPUT 1 4 To determine the analog voltage range use the formula explained below FSx 9 Vmax where FS Maximum flow rate or Maximum pressure Full Scale T
301. u nce leen dE an 3 5 3 5 Menu Two eue ue b duae DEMOS EAM dh Din en Y doe eus 3 5 9 5 1 Serial Option sen SYS ae ne ELS Lx Mibi dee de 3 6 3 5 2 Pump Stat s Los crues eru e aro EN A UR A a don 3 6 3 5 3 External Control sary oneen eae i n aE ata atte e ERE E EEG 3 6 9 5 4 Multiple Pumps renten ec re Pe ete E Des 3 6 3 5 5 Total Volume Reset 3 6 3 5 6 Valve rans dt teed eat eR ete eu eget Re ee ge wa ones 3 7 3 6 Menu Three aes a e ee a Sot ec eee sn 3 8 3 6 1 Poor Fill Alarm oa enne Bar sangen 3 8 3 6 2 Diagnostic Menu eenen eee 3 8 3 6 3 Pressure Calibration 3 8 3 6 4 Diff Modes cg Hew 2 00 ex cue ou ea een En 3 9 3 6 5 Press Integral una ers irn ink ie 3 9 3 6 6 Pressure Deadband 3 9 3 4 Menu HOUR ss eters mear attendeerde a a hs adage boden 8 9 3 7 1 Modbus Options enen Na hrs 8 9 3 8 Eront Panel K6ys iure Ln LER o exe pex en ne ra 3 10 3 8 1 CONST PRESS and CONST FLOW 3 10 382 PREM GRAD cu olie een e acetate po a Gok e eR ERE 3 10 3 8 8 HOED an eis Wer EL TE ende 3 10 3 84 RECALL i e soera we deere ner ar 3 10 3 8 9 STORE srate wetn HEERE Due Ret EE neh 3 10 3 8 6 REFILL vs sonen Rer ER E a na AA RE 3 10 3 8 7 LIMITS 3 ees sr aa
302. uipment specified above conforms to the above Directive s and Standards as of September 09 2014 Vikas V Padhye Ph D Executive Vice President of Sales and Marketing and Product Line General Manager Teledyne Isco TELEDYNE ISCO 4700 Superior Street j Lincoln Nebraska 68504 Everywhereyoulook Phone 402 464 0231 Fax 402 464 0318 60 1262 110 Rev _ DECLARATION OF CONFORMITY ISM1 A Application of Council Directive Manufacturer s Name Manufacturer s Address Equipment Type Environment Trade Name Model No Year of Issue Standards to which Conformity is Declared 2004 108 EEC The EMC Directive 2006 95 EEC The Low Voltage Directive 2012 19 EU WEEE Directive Teledyne Isco 4700 Superior Lincoln Nebraska 68504 USA Mailing Address P O Box 82531 Lincoln NE 68501 Laboratory Equipment for Light Industrial Commercial Environments Syringe Pumps 65D 65DX 65DM 65DXX 65HP 100DM 100DX 100DX2 100DX4 260D 260HP 260SP 260DX 260DXX 500D 500DO 500HV 500SP 500DX 500DXX 500HP 500HPX 1000D 1000DO 1000HV 1000DX 1000DXX 2015 EN 61326 1 2006 EMC Requirements for Electrical Equipment for Measurement Control and Laboratory Use EN 61010 1 2010 Safety Requirements for Electrical Equipment for Measurement Control and Laboratory Use Standard Description Severity Applied Performance Criteria EN610
303. ure relief safety device in your apparatus Table 9 4 below provides part numbers for each pump model replacement shear key Table 9 4 Replacement Shear Keys Pump Model Part Number 1000D 500HP 260D 65D 60 1243 607 500HPx 500D 60 1243 654 100DM DX 60 1243 608 65DM 60 1243 949 30D 60 1263 131 1 Place the pump on its side and remove the four panhead screws that attach the access plate to the case bottom as shown in Figure 9 10 2 Remove the cotter pin that passes through the castle nut and ball screw 3 Use a 34 wrench to remove the castle nut shown below 4 Remove the spacer 5 The two broken halves of the shear key should be protrud ing from the brass worm gear and the ball screw M Note The 30D or 65DM pumps have a bearing set not included in the other pumps In addition to following the other steps in this section when performing shear key replacement on a 30D or 65DM pumps ensure that the bearing set is properly rein stalled as described in Section 9 12 4 9 19 D Series Syringe Pumps Section 9 Pump Maintenance Troubleshooting and Servicing Spacer Ball Screw 9 Access Plate gt Cotter Pin Castle Nut gap gap Shear Key gt J Cl shear key for shear key for all 65DM other models Figure 9 11 Shear key replacement 9 12 2 Replacement Using A shear key installation tool part 60 1248 135 is available Installation Tool from Teledyne Isco 9 20
304. utlet ports to the fittings aop D Series Syringe Pumps Section 1 Introduction 260D Flow Rate Range 107 100 4 80 70 60 50 40 Flow Rate ml min 30 20 0 25 50 75 100 125 150 175 200 225 250 275 300 325 350 375 400 425 450 475 500 525 Pressure bar 517 1 Flow Rate ml min Max Pressure bar 0 001 to 90 517 1 90 to 107 107 23 ml min flow rate x 30 Figure 1 1 260D flow rate range 500D Flow Rate Range 204 200 180 1 S 160 140 120 100 80 60 Flow Rate ml min 40 0 20 40 60 80 100 120 140 160 180 200 220 240 Pressure bar 258 6 Flow Rate ml min Max Pressure bar 0 001 to 170 258 6 170 to 204 204 9 ml min flow rate x 7 4 Figure 1 2 500D flow rate range D Series Syringe Pumps Section 1 Introduction 500 HPx Flow Rate Range 425 4 400 4 375 4 350 4 325 4 300 4 275 4 250 4 225 4 200 4 175 4 150 4 125 4 100 4 754 50 25 408 3 gt Flow Rate ml min 0 25 50 75 100 125 150 175 200 225 250 275 300 325 350 375 Pressure bar 344 7 Flow Rate ml min Max Pressure bar 0 001 to 340 344 7 3
305. wo negative brushes 9 30 9 29 Wires disconnected from brush contact 9 30 9 30 Connector connected to the brush 9 31 9 31 Removing the set screws 9 31 9 32 Loosen the connector 9 32 9 33 New brush reinstalled set screw replaced 9 32 9 34 Location of locating pins 9 33 9 35 Motor plate and bearing plate 9 34 9 36 Installing the deflector shield 9 34 9 37 Capacitor and motor shaft 9 35 9 38 Limit sensor replacement 9 37 xix D Series Syringe Pumps Table of Contents xx 9 39 Installing the plastic 9 37 9 40 Electric valve motor voltage 9 42 9 41 Electric valve motor adjustment 9 43 B 1 Air valve installation for 30D pump B 3 B 2 Electric valve installation B 6 B 3 Keystrokes to specify valve type B 9 B 4 Keystrokes to reset volume totalizer B 9 B 5
306. y damage Power must be removed from the pump before connecting external devices DIGITAL VO ACCESSORY DIGITAL DIGITAL DIGITAL ANALOG INPUT GROUND OUTPUT INPUT 0 10V 1234 G N D ooooooOo00o0 o0o0 o0000o0 o0 o0 o00000 0 RS 232 RS 486 Pin on DB2S shell RS 485 2 Wire 18 DATA 11 DATA 7 GND 7 1 D Series Syringe Pumps Section 7 Modbus Configuration 7 1 2 Modbus TCP IP The modbus TCP IP protocol implementation uses an ethernet connection The ethernet connections are located on the optional DB25 connector labeled USB Ethernet Use optional cable PN 60 1244 488 and coupler PN 14 9905 200 to connect to your Ethernet Pin on DB 25 Casing Ethernet Transmit Transmit Receive Receive Vgnd Vgnd 7 1 8 Modbus Configuration To access the Modbus configuration settings press Options gt Modbus Options 1 Modbus RTU 2 Modbus TCP MORE Y MORE Item Description IP Address Internet protocol address of device Default 192 168 1 200 Subnet Mask Subnet mask Default 255 255 255 0 Gateway Gateway Default 0 0 0 0 Port TCP port Default 502 Table 7 2 Modbus RTU Confi

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