Millipore Milli Q manual 1997
Contents
1. Wait 10 seconds to validate the selection Bring the point of use trigger forward to begin ICLEAN ING 421mn the sanitisation cycle At 400 minutes on the LCD put the trigger EANING 400mn back to its upright position OSE THE VALVE s At the end of the sanitisation cycle the system will automatically go into PRE OPERATE mode Remove the tubing from the point ofuse Remove the adapter fitting Replace the MILLIPAK 40 The Milli Q system is now ready for normal use Milli Q User Manual Page 23 of 34 Replacing the Q Gard Purification Pack figure 4 t 2 3 Note After replacing the Q Gard pack the Milli Q will begin a purge cycle for 5 minutes followed by a TOC rinsing cycle 60 minutes for A10 models Replacing the MILLIPAK 40 Figure 7 1 2 ka 3 4 my w Cleaning the screen filter in the feedwater line Figure 3 2 I 3 4 5 y Mur The final filter MILLIPAK 40 should be changed whenever the product flowrate becomes too low lt 0 5 LPM or whenever the QUANTUM and Q Gard cartridges are replaced The lifetime ofthe MILLIPAK 40 is dependent upon the quality ofthe feedwater and dependent upon the amount of water dispensed through the Milli Q To change the MILLIPAK 40 MUJ Q Ge Bio Syn A10 Put the Milli Q system into STANDBY mode by pressing OPERATE STANDBY for 2 seconds Do not turn off the electrical2. a eate re Er ee Boden K ee ee u Fittings 7 tserte for Water CONNECTION gt ES Sanitisatomn porrptugforcteaning the UF modtie PointofUse Gun with support arm mmm Stieker with serial number tor number and system type A Eocking clip serews i Locking clips m7 How the system works INTRODUCTION Dr ZZ ur Ze ze L eme Pre treated water from EDI Reverse Osmosis distillation or deionisation enters the system and is pumped through u he Q Gard pack for an initial purification step The water is then exposed to UV light at both 185 and 254 wavelengths which oxidises organic compounds and kills bacteria The function ofthe QUANTUM cartridge is to remove trace ions and oxidation by products produced by the action oftheUV light Purified water then passes through an Ultrafiltration UF module The UF module acts as a barrier to colloids particles and organic molecules with a molecular weight greater than 5000 Daltons The contaminants retained by the UF are periodically flushed out ofthe system via tubing to a drain A manual 3 way valve allows you to direct ultrapure water through a final
3. 9 e Press MENU again for 2 seconds 18 2 oum to return to the initial operating mode TOC 3 ppb _ Milli Q User Manual Page 19 of 34 MOI Q Ac Bto SjnA10 Using the keypad continued do KEYPAD ACTION DISPLAY MUI Q MENU function continued Ac a BioSyn A10 Non temperature compensated resistivity display In either PRE OPERATE or PRODUCT mode Press MENU for 2 seconds I OPERATE STAND3Y MEASURE NS Press MENU four times 5 E RV I E E OP T I ON S I ANGUACH HN i 1S1M OPERATE STANDBY MEASURE CLFV NG Press twice on OPERATE STANDBY OPERATBSTANO3Y MEASURE CLEANING The arrow keys allow the choice of a compensated or a non temperature compensated resistivity display y OPERATE STANDBY MEASURE CLEANING eo Press MENU again for 2 seconds to return to the initial operating mode Purging the air out of the Ultrafiltration a Cartridge See Appendix 1 Purging the air from the UF cartridge i Milli Q User Manual Page 20 of 34 Startup of the Milli Q The intermittent recirculation of water inside the Milli Q has allowed the cartridge s to become fully hydrated Before installing the point ofuse filter MILLIPAK 40 dispense about 2 3 litres of water from the system MUIO fie Gr Bio Syn A10 gt Installing the MILLIPAK 40 final filter Figure 7 1 Remove
4. aaron nooo tua Your Milli Q system has a number of operating modes which can be activated via keypad Other modes are automatically activated by the microprocessor These different modes are displayed on the screen and are described below P d _ Standard displays OPERATING MODE ACTION STATUS OF SYSTEM Press the OPERATE The system is in a STANDBY mode While in STANDBY STANDBY button while the this mode system operation is not possible system is OPERATE Automatic recirculation does not occur in this mode mode Press the OPERATE IIn this mode the system will recirculate water for 5 PRE OPERATE STANDBY button while the 4 minutes each hour SV system is in STANDBY mode 5 Automatically occurs from PRE 1 During PRODUCT mode the system displays the OPERATE mode when point of product water resistivity compensated at 25 C 18 2 MQcm use trigger is moved forward This is referred to al PRODUCTION mode W 25 5 18 6 C TEMP 18 6 C TOC 4ppb PROD TIME SETUP COUNTER 9mn gt FAST FLUSH TOC 3 ppb Milli Q User Manual Automatically occurs from PRE OPERATE mode when point of use trigger is moved forward Press the MEASURE keypad button when the system is in PRE OPERATE or PRODUCT mode In PRE OPERATE mode press the MENU button for 2 seconds to view the counter Automatic with Biocel and Synthesis Milli Q systems Occurs automatic
5. the allowed limits during the TOC measurement current temperature If the error persists then contact Millipore Technical Service The water temperature is below 5 C It is necessary that the Temperature too low temperature be above this value The water temperature is above 41 C It is necessary that the Temperature too high water temperature is below this value ha Conductivity too high Conductivity of the sample water exceeded the limit during sampling Overheating The temperature exceeded 60 C during oxidation Ifthe error persists then contact Millipore Technical Service Incomplete oxidation The sample oxidation was not completed in the allotted time If the error persists then contact Millipore Technical Service Low oxidation rate The sample oxidation rate was abnormally low If the error persists contact Millipore Technical Service Ac Gi A 10 DESCRIPTION ERROR Milli Q User Manual Page 29 of 34 APPENDIX 1 Interrupting_the sanitisation cycle UF cartridge Ifa sanitant chemical has been introduced into the Milli Q it is absolutely necessary to let the sanitisation cycle finish in order to completely rinse the sanitant from the system If no sanitant has been introduced then the sanitisation cycle can be cancelled by following these instructions SAN CYCLE I 2 Omn OPERATBSJAN 9V ME ARE CLEANING Vin STANDBY g ES Press
6. CLEANING for 10 seconds I At the end of the sanitisation cycle the Milli Q will go back to its initial mode of operation Purging_trapped air from the UF cartridge In either PRE OPERATE or PRODUCT OPERA US ANO9Y HfASJRE CLEANING Press MENU for 2 seconds OFEfWBSIANDSY MEASURE CLEANING press MENU 5 times Open the point of use valve to begin the air purge cycle Dispense product water from the system to the drain Atthe end ofthe air purge the system will go i back into PRODUCT mode be Close the point of use valve trigger in vertical position 7 Interrupting the A 10 cleaning cycle If an A 10 cleaning cycle has been started from the MENU service mode then it can be cancelled at any time by pressing on the MENU button Milli Q User Manual Page 30 of 34 Q BaSinAlO w I System is not operated for a long time MUI Q Ai BaSnalo Replacing the main electrical power fuse 1 Put the system into STANDBY mode by pressing OPERATE STANDBY for 2 seconds 2 Turn offthe power switch figure 1 G by putting it into the 0 position 3 Unplug the electrical power cord from the wall and from the system 4 Remove the fuse holder figure 1 J 5 Remove the blown fuse and replace it with the spare fuse Note Replace the spare fuse in the holder in the event that it may iced to be used later 6 Replace the fuse holder and plug the power
7. IMPLIED THERE IS NO WARRANTY OF MERCHANTABILITY OR FITNESS FOR A PARTICULAR PURPOSE The warranty provided herein and the data specification and descriptions of Millipore products appearing in Millipore s published catalogues and product literature may not be altered except by express written agreement signed by an officer of Millipore Representations oral or written which are inconsistent with this warranty or such publications are not authorised and ifgiven should not be relied upon vh the event of a breach of the foregoing warranty Millipore s sole obligation shall be to repair or replace at its option any product or part thereof that proves defective in materials or workmanship within the warranty period provided the customer notifies Millipore promptly of any such defect The exclusive remedy provided herein shall not be deemed to have failed of its essential purpose so long as Millipore 1s willing to repair or replace any non conforming Millipore product or part Millipore shall not be liable for consequential damages resulting from economic loss or property damages sustained by a customer from the use of its products However in some states the purchaser may have rights under state law in addition to those provided by this warranty Milli Q User Manual Page 34 of 34 o 4 a 2 In nimm py yyy 7 ES a y 2 2 27
8. cord back in to the system and to the wall Es _Regulating the mobility of the point arm The point ofuse arm can be adjusted in 2 locations This ee is S done by tightening the arm screw s with the 6 sided key figure 2 K Do not overtighten the arm screws This may block movement ofthe arm or damage the arm itself EN Recycling the reject water from the 10 The reject water from the use ofthe A 10 can be recycled to a feed reservoir Contact Millipore Technical Service for more details Keep the Milli Q in PRE OPERATE mode when water is not needed In this mode the Milli Q will operate all cycles to keep the water quality optimum Ifthe Milli Q is to be shut down for a kong time contact Millipore Technical Service for further information Milli Q User Manual Page 31 of 34 PURCHASING INFORMATION Pra eee Te ET FT RE en Voltage Frequency T2 with A10 module Y with Q Gard 0 without A10 module adapter 0 without Q Gard adapter 230 V 50Hz 6 120V 60Hz 7 100 V 50 60 Hz Description 444244444222 R _Q Gard purification pack _Q Gard 1 purification pack 1 _ _______________________ QGAR 000 RI___ _Q Gard 2 purification pack 1 0 00 00 QGAR 000 D2 ___ _ 9 ANTUM __________________________________ _SyMTi
9. filter made up of a 0 22 um membrane MilliPak 40 The final filter removes particles and bacteria greater than 0 22 in size and prevents recontamination ofthe system from the point of use The A 10 TOC monitor takes samples of ultrapure water to determine trace organic levels Samples are taken periodically in PRODUCT mode Milli Q User Manual Page 6 of 34 Mtll Q fe Q Boo SynAl System Schematic ww water flow schematic of a Milli Q system is shown below Only the main components are shown Ld 4 m MIUJ Q Ac BiaSynAlO m E Inlet solenoid valve mE Pump Q Gard Pack selected based upon the type of feedwater QUANTUM ultrapure cartridge N Resistivity cell i a Point ofuse with dispensing valve bs yO MILLIPAK 40 final filter 6 0 Check valve UVlamp Sanitisation port used to introduce chemical sanitants to UF module Ultrafiltration cartridge UF cartridge reject solenoid valve A 10TOC monitor Milli Q User Manual Page 7 of 34 TNNT Specifications Mua Ac 5 Al vw Composition of materials in contact with water n RES Material ieces Material Pack Adapter i Polycarbonate PVDF Q Gard Pack i Fittings PE PA PVDF Inlet solenoid valve Stainless steel i Resistivity cell Stainless steel 316 L QUANTUM cartridge Ultra High density Manifold polyethylene i Tubi
10. power to the system Bring the pack adapter A to its highest position Remove the metal retaining clip F Remove the Q Gard pack from the system Install the new Q Gard pack as described in the INSTALLATION chapter and in STARTUP Make sure that the point ofuse trigger C is in the closed vertical position Remove the venting cap A from the MILLIPAK 40 Unscrew the MILLIPAK 40 from the female thread B on the point ofuse gun Turn it counterclockwise to unscrew it Install the MILLIPAK 40 as described in the INSTALLATION chapter Close the valve on the feedwater line Remove the feedwater tubing C from the fitting F Unscrew the fitting E form the feedwater pipe D and the other fitting F Clean the screen filter G Proceed in the opposite order to reinstall the screen filter Milli Q User Manual Page 24 of 34 MUJ Q Ac Gr BioSynAl Cleaning the A10 Periodically the detection cell in the A 10 needs to be cleaned of any built up residual organic matter Ifthis build up happens then the displayed TOC values could be erratic or higher then previously seen To fix this an autocleaning cycle is needed to oxidise any organic contaminants present in the A 10 detection cell To perform a cleaning cycle ofthe A 10 follow these instructions In PRE OPERATE mode CWRMBSMNOSV MEASURE Ci MMV3 Press MENU for 2 seconds y OPERATBSTANOBY MEASURE GLEANING 5 SERVICE A10 P
11. wall mounting the system install elbow connectors figure 2 baw 4 Connect the feed water tubing C 8 mm OD to inlet FEED 1 H by inserting it firmly in the fitting Verify that the connection is good by pulling several times on the tubing once inserted 5 Connect the other end ofthe feedwater tubing to the reservoir outlet valve Figure 5 System fed from a pressurised source 1 Cut the feed water tubing 8 mm OD Figure 2 D to the desired length lt 2 5 meters 2 Remove the protective plug B from the FEED 1 connection H by pressing on collar A and pulling on the plug 3 The feed water valve or the fitting D should terminate in a 1 2 MNPT fitting The 1 2 FNPT fitting E is screwed on to the fitting D Use the Teflon tape Figure 2 1 which is HE supplied with the unit to ensure a good seal against leaks 4 Connect the tubing C to the fitting F Pull on the tubing afterwards to insure it is secure ha 5 Pressurised feedwater entering the Milli Q system must be regulated between 0 1 Bar 1 5 psi and 0 3 Bar 4 5 psi Installation of a pressure regulator is necessary if the feedwater pressure is over 0 3 5 owe Bar 4 5 psi The regulator should be adjusted while water is dispensed from the system Connection of the reject tubing s figure 3 2 Any Milli Q system with the A 10 TOC or UF option s has have reject tubing on the system The procedure to connect the reject tubing is the s
12. Milli Q User Manual MILLI Q 10 Hc af Academic 77 Gradient y Biocel Synthesis MILLIPORE Page 1 of 34 Operating and Maintenance manual d 10 Academic 7 A Gradienty Biocel Synthesis MILUPORE Milli Q User p NOTICE Information in this document is subject to change without notice and should not be A construed as a commitment by Millipore Corporation Millipore Corporation assumes no responsibility for any errors that may appear in this document This manual is believed to be complete and accurate at the time of publication In no event shall Millipore Corporation be liable for incidental or consequential damages in connection with or arising u from the use of this manual am e ut if Copyright 1997 all rights reserved Millipore Corporation Folder PF 0 Documentation PF 05112 Trademarks Millipore is a registered trademark of Millipore Corporation or an affiliated company RiOs Elix Milli Q Q Gard and Quantum are trademarks of Millipore Corporation i Teflon is a trademark of E I duPont de Nemours amp Co Slo Blo is a trademark of Little Fuse Company All other trademarks are trademarks of their respective manufacturer Milli Q User Manual Page 3 of 34 NOTICE na EH Hp e m A RUE Geddes TABLE OE CONTENT een ss 4 USING OF THE MANUA E a se ea eeu epp e I E M 5 DISTINGUISHING BET
13. POINT OF USE ARM ee ee Bd RECYCLING THE REJECT WATER FROM THE 10 e M Metu 31 SYSTEM IS NOT OPERATED FOR X EONG TIME tt a a e i s tte res us dccem ber eb adt nod TECHNICAL INFORMATION UU UEM 33 TECHNICAL ASSISTANCE te bad etc tta ta ton ates ds ts SD 4 At the end ofthe document FIGURES Milli Q User Manual Page 4 of 34 _ USING OF THE MANUAL This manual describes how to install use and maintain your Milli Q water purification system The use of this equipment is very simple however it is strongly recommended that this manual be read before connecting the system to a source of water or to electrical power A thorough knowledge of your water system not only helps to prevent damage to the system or personal injury but it also helps you to become familiar with all its functions Distinguishing between text specific to one or more Milli O systems The information presented in this manual uses the following notation en The four types ofMilli Q systems and the A 10 TOC option are described in this manual The guide shown on the edge of each page permits you to distinguish between information relevant to all models or to information relevant to a specific model of water system It is important to verify that the column on the edge page corresponding to your model is full before proceeding to study information pertaining to system characteristics oper
14. WEEN TEXT SPECIFIC TO ONE OR MORE MILLI Q 5 8 8 2 022 24 5 INTRODUCTION A HS 6 U GENERALE INFORMATION c ostro en oet ada a a ta peers ond HOWTHE SYSTEM WORKS sun ar era a 6 INSTALLATION onore eese rt eats oly auton re HE nn re ee bes ED EEE TER 10 UNPACKING 10 T INSTALLATION OF THE SYSTEM 2 00 c ie teta ah aah san b din aba RR aA AL UAR Da E LA c ttd uve al MLO OPERATING THE MILLI Q SYSTEM eI nnn ene rere 14 A a ADDITIONAL DISPLAY Se rrinin o ure dpt Hate tbe v ed a Ge E d dete ep peg ete re STARTUP OF THE MIEET Q arte feb dent octo dg uti ath e 22 TIMETABLE FOR ROUTINE MAINTENANCE 000000000 ae I ROUTINE MAINTENANCE u O A ania enna 202 5 JSEROUBPESHOOTING 415 le a ad eine 26 XOUBLESHOOTING MESSAGES rias engere sini LISTOFALARM CODES APRENDO Lee SE 30 INTERRUPTING THE SANITISATION CYCLE OF A UF qii Soiree A opa N 30 amp PURGING TRAPPED AIR FROM THE UF CARTRIDGE le cacao 30 i INTERRUPTING THE 10 CLEANING mm 30 REPLACING THE MAIN ELECTRICAL POWER FUSE nenne 060020 31 REGULATING THE MOBILITY OF THE
15. al operating mode 700 j P it 8DAYS NN Milli Q User Manual Page 18 34 MUI Q Gt Bio S n A10 Use ofKeypad continued KEYPAD 4CTION DISPLAY Cleaning the A10 module Duration 1 hour The A 10 CLEANING mode is used to clean the oxidation chamber of the 10 and is described in detail in the ROUTINE MAINTENANCE section Choosing the display language In either PRE OPERATE or PRODUCT mode Press MENU for 2 seconds 1 OPERATF ISTANDEY nass RU AMSS SERVICE OPT IONS Press MENU four times PS OPERATE STANDBY MF ASURG CLEANING MERI e dn m LANGUAGE tNGL 1 Sil Press the arrow keys to change EN Toe SIT TONS between different languages LANGUAGE SPANIST 22 u en Press MENU again to return to either 18 2MQcm a PRE PRODUCT mode lt ppb Choosing the unit of measurement In either PRE or PRODUCT mode OPERATBSIANDBY MEASURE CLEANING Press MENU for 2 seconds 4 OPERATE STANDBY MEASURE CI ANING OPT IONS Press MENU four times y E t NGL1S5 OPERATE STANDBY MEASURE CLEANING E RV T C E 5 T I ON 5 WA OPERAIEraTANOBY MEASURE CLEANING The arrow keys allow the choice of E RV I CE OPT TONS e e or V Siemens cm as units ROD UNIT 15 ines
16. ally During PRODUCT mode the system can display the product water resistivity non temperature compensated as well as the water temperature The product water temperature is displayed For systems with the A 10 option the product water TOC is also displayed The counter can be used to dispense water from the system for a specific amount of time This time can be selected and changed with the keypad After the counter finishes the system automatically goes into STANDBY mode This is a rinsing of the ultrafiltration module and lasts 30 seconds It does not effect normal use of the system Display of the last TOC measure or oxidation in process Page 14 34 MUI Q Q Bio Syn AlO EXCH CARTRIDGES ET START SANIT tr AIR PURGE EXCHANGE UV LAMP EXCHANGE A10 UV e wat AIOCLEANING 59 ene a Additional displays System maintenance messages DISPLAYED MESSAGE Milli Q User Manual ACTION Occurs automatically See MAINTENANCE chapter for further information Occurs automatically See MAINTENANCE chapter for further information Automatic after installation of ne cartridges gu Occurs automatically Call Millipore Technical Service Occurs automatically Call Millipore Technical Service ES Occurs automatically after installing new purification polisher pack s It also can be started manually See the MAINTENANCE chapter for further i
17. ame as that used for the feed water tubing s s Y i 1 Connect the Ultrafiltration cartridge reject tubing 8 mm OD lt 2 5 m Figured D to the DRAIN 3 I outlet 2 Connect the 10 waste stream tubing 6 mm OD lt 2 5 m Figure 2 E to the OUT 5 J outlet Ifthe Milli Q System is fed by a reservoir the 10 reject water be recycled to the reservoir 4 When starting up the system place the ends ofall reject tubing s to the drain Milli Q Installation Connection of feed water to the system Figure 3 MU1 Q Ac Q Bio Syn Al User Manual Page 11 of 34 Installation of the Q Gard purification pack Figure 4 The Q Gard is only used on Milli Q systems equipped with a pack adapter 1 Raise the pack adapter A to its highest position Remove the two protective plastic inserts B on the pack adapter 2 Remove the two protective inserts on the Q Gard pack C Wet the two O rings with water a 3 Push the Q Gard so that the pack adapter metal rod D goes through the hole at the top of the Q Gard Lift the Q Gard slightly and push the bottom of it into the small opening E on the system At the upper pack adapter push the pack completely in until secure hs 4 Lock the Q Gard in place with the metal locking clip F on the end of the metal guide pin D 5 Bring the adapter cap down to its lowest position G so that 1t covers the top ofthe Q Gard Electrical connec
18. ations MUI Q 4 Gf Bio Syn Al Example FOR COMMON TEXT all the columns are full FOR TEXT SPECIFIC TO A SPECIFIC MODEL Gradient column 2 is full reference figures are located at the back of this manual in foldout sheets ore Dotted portions of drawings represent components or items not delivered with the system Elements shown in light grey represent keypad buttons which are not being referred to in that section of text or not referred to in examples of screen displays Warnings Caution signs are shown throughout this manual to bring items to your attention which present risk or which require delicate manipulations Caution Danger Milli Q User Manual Page 5 of 34 or ral Information The Milli Q system is used as a final water purification stage The feedwater to a Milli Q can be produced by electrodeionisation ELIX Reverse Osmosis RO distillation or deionisation 4 The system produces water of Type 1 quality This is equal to or better than ASTM and NCCLS type water quality standards The principal components ofthe Milli Q system Figure 1 A B 210 pack adapter E D SE QUANTUM atenn 5 Liquid Crystal Display CCD u Er Pa cet TED poa D 7 Power Cord SOCKET m J nr oem ee O
19. e Osmosis RiOs system performance Purified water quality Resistivity 18 2MQ cmat25 C Pyrogens lt 0 02 EU ml TOC Me o5 25 10 ppb 1 5 ppb 2 5 Silicates lt 0 l ppb Heavy metals 0 1 ppb Micro organisms lt 1 cfu ml Particles 0 22 urn Flowrates Product water flowrate Uptol 5 litre minute Up to 10 litre minute Noise level in dB A at 1 metre Test conditions Milli Q system was equipped with a Q Gard purification pack aQUANTUM EX ultrapure cartridge The feedwater to the Milli Q came from a RiOs Reverse Osmosis system TOC levels in the feedwater were lt 50 ppb The quality ofthe Milli Q product water can vary as a function ofthe quality ofthe feedwater Milli Q User Manual Page 9 of 34 INSTALLATION Unpacking The different components supplied with the system are shown in figure 2 and are listed below Milli Q water purification system ha B Electrical power cord C Folder with documents to insert D Tubing 8 mm OD 5 meters length for inlet water connection reject stream for ultrafiltration module E Tubing 6 mm OD 2 5 meters length for A 10 waste stream Tubing used when UF module is sanitised G Fitting 1 4 MNPT hose barb male national pipe thread H Fitting 1 2 FNPT 8 mm OD tubing with screen filter inside D Teflon tape 5 7 Plastic ba
20. e measured temperature needs a short period of time to stabilise If the message persists contact Millipore Technical Service Resistivity lt minimum off scale Resistivity of product water is off scale Let the Milli Q operate for a few minutes to force any air out of the resistivity cell If the message persists Contact Millipore Technical Service Resistivity gt maximum Resistivity of water is off scale Let the Milli Q operate for a measurement is not representative few minutes to force any air out of the resistivity cell If the message persists Contact Millipore Technical Service Contact Millipore Technical Service UV lamp voltage error Contact Millipore Technical Service Defective UV lamp Contact Millipore Technical Service Error with the electronics reference Contact Millipore Technical Service signal problem persists then contact Millipore Technical Service Milli Q User Manual Page 28 of 34 M7 MUI Q t 5 AIO EEPROM saving error If the error persists then contact Millipore Technical Service Error in analogue to digital If the error persists then contact Millipore Technical Service conversion The temperature exceeded acceptable limits during analysis Temperature range error Ifthe error persists contact Millipore Technical Service The resistivity ofthe water in the The correlation between these two measurements has passed A 10 is not accepted at the
21. em is in PRODUCT Ajode but does not produce any or very little water Air is trapped in the final filter Clogged final filter Air is trapped in the UF module Change the cartridge s See the ROUTINE MAINTENANCE chapter The Cartridge s are atthe end of their useful life EXCH CARTRIDGES Put the cartridge s back in place See the ROUTINE MAINTENANCE chapter The cartridge s are either not installed properly or have been removed CARTRIDGE OUT AIR PURGE SYSTEM ERROR Wait for the 5 minute AIR PURGE to finish before using water The cartridges were just replaced These error code numbers are listed later in this manual The error number corresponds to a particular equipment error Press the OPERATE STANDBY button to reinitialise the system Ifthe error persists contact Millipore technical service The Milli Q is connected to a printer A transmission error has occurred between the Milli Q and the printer RS232 ERROR NO FEED WATER OPEN THE VALVE FAST FLUSH SAN CYCLE or CLOSE THE VALVE The Milli Q is connected to a level Fill the reservoir with water before using sensor in the feed reservoir the Milli Q again Follow the displayed instructions and wait for the program to end The Milli Q is operating in a preprogrammed software cycle The limit ofthe UV
22. g containing elbow fittings a Six sided key used to loosen tighten point of use arm Items ordered separately L Q Gard purification pack M QUANTUM ultrapure cartridge N MILLIPAK 40 final filter 0 22 urn for point ofuse gun Checked by Name Signature a Verified by Name Signature Installation of the system The system can either be placed on bench or wall mounted Ifthe system is to be wall mounted ie then it is necessary to first verify that the wall can support the weight of the system Contact AN Millipore Technical Service for further instructions on wall mounting the system Some versions of the Milli Q systems require a drain nearby When a reservoir is used as a feedwater supply locate the system and reservoir close together whenever possible Figure 5 shows the different connections to be made to the system Note The inlet valve pressure regulator and pressure gauge are not supplied with the Milli Q and must be ordered separately Contact Millipore Technical Service for more information a Milli Q User Manual MUtQ A O BiaSynAlO no Date Date Page 10 of 34 System fed from a reservoir 1 Cut the feed water tubing 8 mm OD Figure 2 D to the desired length lt 2 5 meters 2 Remove the protective plug from the FEED 1 connection by pressing on collar A and pulling on the plug 3 For
23. i performance n i OPERATE STANDS MEASURE CIFANINS MRf t e ha OPERATISSTANDBY MEAS RE aEANING MENU 22 Or HWI STANDBY MEASURE CLF W5 1 i OPERATE STANDBY MEAS jRt aEANING MENU P amp OPERATE STANDBY MC amp U CLFASING MENU be i 1 Milli Q User Manual Page 17 of34 mi Q Ac Q BioSyn AIO Use ofKeypad continued KEYPAD ACTION DISPLAY ME function contin Printer OPERATEISTANDBY MIALURE CLEANING In either PRE OPERATE or PRODUCT PROD TIME SETUP 6 Press MENU for at least 2 seconds y OPERATEISTANDBY MEASURE CLEANING Press MENU I OPERATE STANDBY MEASURE CLEANING One press on the MEASURE button starts Qv Y printing 4 OPERATE STANDBY MEASURE CLEANING Press MENU for at least 2 seconds 1 8 display returns back to initial operating mode 3 ppb 2 nc Display the age of the UV lampfs and purification cartridges In either PRE OPERATE or PRODUCT Press MENU for at least 2 seconds x OPERATE STANDBY MEASURE CLEANIKO MENU SERVICE AGE i Press MENU twice E UV LAMP 6SDAYS the age ofthe UV lamp is shown y OPERATE STANDBY MEASURE CLEANING Press OPERATE STANDBY once SERVICE AGE the age of the UV lamp in the AIO TOC mod
24. iX lonex 1 __ 000 IX QUANTUM EX Organex 1 000 EX___ AUANTUM VXJVojatile Or Carbon ftemqyal O pack QTUM 000 VX___ QUANTUM cartridge with non sterileMILLIPAK _ QUANTUM fonex f pack ____________________________ MPK IX QUANTUJ EXJOjgane O pack QTUM MPK EX __ Final Eon gt ns de ee _MILLIPAK 40 final filter sterile 2 pack _______________________ MPGL 045 K2_ _MILLIPAK 40 final filter non sterile 1 pack MPGL 040 01 DRBEHPMON tLe 199 __ Pressure regulator repa ina eM d eese i d 2FMQQgQJPR ___ Pointer ne Nenn mean le we A 0 2 ed PRNT CBLO1___ NW Valljtounting bracket SYSTFIXO1 Necessary if feed pressure gt 0 3 bar 4 5 psi Milli Q User Manual Page 32 of 34 3 I 5 E gt zi 2 w Technical assistance For further information on Millipore products please contact your nearest Millipore subsidiary ADDRESS enn us Milli Q User Manual Page 33 of 34 Warranty Millipore Corporation Millipore warrants the products manufactured by it against defects in materials and workmanship when used in accordance with the applicable instructions for a period of one year from the date of shipment ofthe products MILLIPORE MAKES NO OTHER WARRANTY EXPRESSED OR
25. lamp life has Replace the UV lamp Call Millipore been reached Technical Service EXCHANGE UV LAMP Milli Q User Manual Page 26 of 34 MUI Q 8 80 Syi Al i MUIO 5 fie Gr Bio SynA STATUS PROBLEM CAUSE REMEDY START SANIT A cleaning cycle ofthe UF cartridge Start a cleaning procedure needs to be started See the MAINTENANCE chapter Press OPERATE STANDBY to An error has occurred with the A 10 reinitialise the Milli Q Ifthe error A10 ERROR TOC module persists then contact Millipore Technical Service EXCHANGE A10 UV The limit ofthe UV lamp life has Replace the UV lamp in the A 10 been reached Contact Millipore technical Service The Milli Q has the A 10 inside Let the Milli Q finish the 60 minute A 10 A10 CLEANING The cartridges were just replaced or cleaning cycle The Milli Q can dispense an A 10 cleaning was started from water during this mode the SERVICE MENU Milli Q User Manual Page 27 of 34 1 Ac Bio Syn Al When the ALARM LED is flashing an error code number will be displayed which indicates the nature ofthe problem inside the Milli Q SYSTEM DESCRIPTION ERROR 1 The motor voltage is above its Contact Millipore Technical Service recommended operating value Temperature lt minimum The measured temperature needs a short period of time to stabilise If the message persists contact Millipore Technical Service Temperature gt maximum Th
26. nformation SYSTEM STATUS SERVICE LED blinking The operational lifetime of the purification polisher cartridges has expired SERVICE LED blinking A cleaning of the ultrafiltration module is necessary A 5 minutes air purge of the cartridge is in progress SERVICE LED blinking The operational lifetime of the UV lamp of the Milli Q has expired SERVICE LED blinking The operational lifetime of the UV lamp inside the A10 has expired SERVICE LED blinking A cleaning cycle of the A 10 is in progress Duration is 60 minutes Page 15 of 34 MIUI Q Ac amp Bio SynAlO Alarm displays DISPLAYS CARTRIDGE OUT NO FEED WATER SYSTEM ERROR RS 232 ERROR 110 ERROR NOTE The ALARM LED will blink while the above ALARM messages are displayed on the LCD Milli Q User Manual Gu bla Syn A10 STATUS ofthe SYSTEM The Milli Q has stopped Spann because either the QUANTUM or Q Gard purification pack is loose See the QUANTUM and Q Gard installation section for more information The Milli Q system is connected to a reservoir level sensor and has detected that the reservoir is empty Wait until there is water in the reservoir Indication ofa specific fault or malfunction with an internal component ofthe system See the TROUBLESHOOTING chapter for more information There is a problem with the RS 232 output See the TROUBLESHOOTING chapter for more information Service or mai
27. ng PE Pump head NSF listed and FDA i Three way valve Copolymer of butadiene approved materials and styrene Viton PTFE i O rings EPDM UV lamp and housing Quartz Stainless steel UF housing ABS UF sanitisation port ABS Reject solenoid valve Stainless steel NSF National Sanitation Foundation FDA Food and Drug Administration Electrical specifications Voltage Electrical Frequency power fuse RS 232 Output consumption 230 Volts 120 Volts 230 Volts i d 120 Volts i 2 0 A Slo Blo type RJ 11 connector Dimensions and operating weight with Q Gard and Quantum Height 22 455 mm Length 255 Depth 522000027 855 mm includes the wall mounting points on rear Weight s o 16 0Kg 168 Kg 16 3 Kg 17 1 Kg t 0 6 Kg with A 10 TOC module Environmental Conditions Ambient storage and operating temperature 5 C T 40 C 20 80 without condensation Humidity Milli Q User Manual Page 8 of 34 MUI Q M Q Bo5pAl Hydraulic specifications Feedwater tubing 8 mm outer diameter OD length 3 meters maximum Reject tubing 8 mm and 6 mm OD length 2 5 meters maximum Inlet feedwater pressure Minimum 0 1 bar 1 5 psi Maximum 0 3 bar 4 5 psi Feedwater flowrate gt 15 litre minute LPM Feedwater temperature 5 C to 37 C eedwater quality Millipore recommends using water treated by ELIX Electrodeionisation EDI or Revers
28. ntenance needed for the A10 TOG accessory See the TROUBLESHOOTING chapter for more information Page 16 of 34 Use ofthe Keypad The keypad allows the user to activate the different operating modes or to review information about system ACTION T nd PRE OPERATE Press the OPERATE STANDBY keypad button for at least 2 seconds to switch between these two operating modes STANDBY STANDBY PRE OPERATE PRE OPERATE TOC i MEASURE In PRODUCT or PRE OPERATE mode Press MEASURE to display temperature TEMP 22 6 and last TOC value 3ppb CLEANING The CLEANING function is described in the ROUTINE MAINTENANCE chapter This is for cleaning and sanitising the ultrafiltration module ME TI Programming a dispensing time In PRE OPERATE mode only press MENU for at least 2 seconds j Select or change the COUNTER time by pressing the arrow keys lt 1 lt or gt gt i Press OPERATE STANDBY for at least 2 PREOPERATE seconds to accept the COUNTER time Note Moving the point of use trigger forward will initiate the COUNTER and start to dispense water The system will dispense water from the point ofuse gun for the amount oftime that the COUNTER is set to When the dispensing time is finished COUNT 0 the system will automatically go to STANDBY mode Move the Trigger back to the vertical position to go to PRE OPERATE mode
29. ode by pressing the OPERATE STANDBY button for 2 seconds Do not turn offthe electrical power L 2 Open the front blue door by pulling the 2 latches open figure 4 H 3 Pull out the QUANTUM cartridge 2 4 Install the new QUANTUM cartridge by following the instructions in the INSTALLATION AND STARTUP chapter e Note After replacing the QUANTUM cartridge the system will begin a 5 minute AIR PURGE cycle The Synthesis and A 10 models will also have a TOC rinsing cycle Milli Q User Manual Display EXCHANGE A10 UV See TROUBLESHOOTING Note When the product water flowrate becomes low lt 0 5 1 min change the MILLIPAK 40 final filter If the MILLIPAK 40 has only been in place a short time and becomes clogged then check the quality ofthe MU1 Q Ac Qr BioSyfiAlO Following a message on the LCD Display EXCH CARTRIDGES Replace the expendable cartridges See ROUTINE MAINTENANCE i Display START SANIT Clean the Ultrafiltration module i See ROUTINE MAINTENANCE Display EXCHANGE UV LAMP i Replace the UV lamp See TROUBLESHOOTING f Replace the UV A10 lamp Page 22 of 34 Sanitisation ofthe Ultrafiltration module A regular sanitisation ofthe UF cartridge is necessary to obtain the best water quality and to have the maximum of the UF module The Milli Q system will periodically display every two weeks the message START SANIT to inform you that a sanitisation is neces
30. ress MENU 3 times A10 CLEAN ING 60 Wait 5 seconds to validate the A 10 cycle After 60 mins the system will automatically return to its initial operating mode To interrupt the cleaning cycle OPERATBSTANOBY MEASURE CLEANING Press for 2 seconds to return to the initial operating mode Note It is possible to get water from the point ofuse valve during the A 10 CLEANING mode Page 25 of 34 Milli Q User Manual in TROUBLESHOOTING o AR Troubleshooting messages Whenever the SERVICE LED is blinking a message is displayed on the screen which indicates the nature ofthe service needed REMEDY No electrical power Check the source of power hi The power cord is not plugged into Check the power cord There is no electrical power to the the wall system The system power fuse is defective or blown The feedwater line valve is closed The pump does not work Inlet solenoid valve not opening Feedwater pressure is too low Change the main power fuse See APPENDIX 1 Open the feedwater line valve Contact Millipore Technical Service Contact Millipore Technical Service Verify that the feedwater pressure is at least 0 1 Bar Purge air from the final filter See 4 MAINTENANCE section Replacing the MILLIPAK filter See MAINTENANCE section Replacing the MILLIPAK filter Purge the UF cartridge See Appendix 1 Purging the UF cartridge The Milli Q syst
31. rst time A 5 minute rinsing cycle AIR PURGE occurs automatically whenever new cartridges are installed in the Milli Q System 1 Open the feedwater isolation valve if there is one 2 The system will be waiting to begin the AIR PURGE cycle 3 Start the AIR PURGE by moving the point of use gun trigger down PRODUCT Direct all water from the point ofuse to a drain AIR PURGE 4mn At the end of 5 minutes the system will go into PRODUCT mode Close the point of use valve 5 Ifpossible leave the system in PRE OPERATE mode overnight This P RJE O helps to hydrate the ion exchange resin inside the cartridges 6 In PRE OPERATE mode purge the QUANTUM cartridge of any trapped air by pushing the end of a small screwdriver into the small hole located on the blue door figure 4 K 7 Push the small screwdriver gently into the hole to purge out the trapped i air ner Cleaning the A 10 measurement cell When a Milli Q system is configured as an A 10 model the system starts up by an automatic cleaning ofthe A 10 E analysis cell This cleaning lasts for 1 hour Connection of a printer with the system s RS 232 interface The Milli Q system offers the possibility of sending information to a printer a For further information contact Millipore Technical Service ir m Milli Q User Manual Page 13 of 34 arr ar Se Se Zr rt rra en Modes of operation
32. sary There two choices of sanitisation cycles in the software Cycle 1 This is a short sanitisation maintenance program This allows the UF module to be sanitised at the start ofan evening and throughout that night Cycle 2 This is a longer sanitisation maintenance program This program allows for a more rigorous cleaning ofthe UF module whenever flowrate is diminished from the system or the UF module is severely contaminated A Before starting a sanitisation it is necessary to have more than 25 litres of feedwater available KEYPAD ACTION DISPLAY 4 OPERATE STANDEY MEASURE CIEANINS Put the Milli Q into STANDBY mode by ADE pressing OPERATE STANDBY for 2 gt AA d seconds MEER m Remove the MILLIPAK 40 from the point ofuse figure 6 I Screw the adapter fitting figure 2 onto the point of use Pa Fitthe 12 mm OD tubing figure 2 F onto the end ofthe barb fitting Place the other end of this tubing into a drain or sink 4 Remove the sanitisation port plug from the system Keep it near the system Introduce 3 grams of sodium hydroxide into the sanitisation port 1 a Screw the sanitisation port plug back onto the system Check that it is secure OPERATBSTAMJBr MEASURE CLEANING MENU 2 ANP Press CLEANING for 2 seconds CLEANING 1 Pressing CLEANING again allows the choice o the longer sanitisation cycle i
33. the venting cap A from the MILLIPAK 40 2 Screw the MILLIPAK 40 onto the point ofuse thread B Turn it a maximum of2 3 times 3 Replace the venting cap but do not tighten it onto the MILLIPAK 40 4 Start to purge the MILLIPAK 40 by bringing the point ofuse gun trigger forward 7 5 When all ofthe air is purged from the MILLIPAK 40 by allowing water to run of the vent tighten the venting cap A Nn 6 Close the point ofuse gun trigger C by moving it to the vertical position The system will automatically go into PRE OPERATE mode BL Purpose of the LED on the point of use gun When the point ofuse trigger is brought slightly forward the Milli Q system goes into aRECIRCULATION mode i The green LED will flash when the water quality is not optimal Once the green LED is lit steadily the trigger can be e brought forward to dispense water from the point of use gun Ifthe resistivity is below the setpoint the green LED will blink continuously Milli Q User Manual Page 21 of 34 MAINTENANCE rien nA Gi Every month Annually once a year Note the operating parameters for the Clean the screen filter in the i system as indicated in the back of feedwater line See ROUTINE this manual MAINTENANCE i w lt 1 i i feedwater Routine maintenance Replacing the QUANTUM Ultrapure Cartridge v 1 Put the Milli Q system into STANDBY m
34. tion of system 1 Connect the power cord Figure 2 B to the Milli Q Figure 3 En Connect the other end ofthe power to an earth grounded power source 2 Check that the point of use gun trigger is in the upright position 0 3 Turn the system electrical switch figure 1 by putting it to position I i 4 The serial number is displayed for 10 seconds Note the serial number in the i table below Lol Example RADI ENT VI 00 pep E Wh mus se Type of Milli Q system Note Contact Millipore Technical Service when connecting alowieveltank sensor to the Milli Q system As an A option it is possible to get a NO FEED WATER message when there is water in the reservoir Installation of the QUANTUM Ultrapure Cartridge Figure 4 Note It is important to have the system switched on before installing the Quantum Cartridge 1 Open the blue door on the front of the Milli Q by pressing the 2 latches Ho on the right side of the Zu door to open it 2 Remove the two protective inserts from the QUANTUM cartridge Wet the two rubber O rings on tor the QUANTUM cartridge with water 3 Install the QUANTUM cartridge and push it in as far as it will go 4 Close the door It is necessary to fully snap the latches H shut to hold the QUANTUM cartridge inside Milli Q User Manual Page 12 of 34 WWJQ Ac Gr 8iaSpt Al MIUt Q Ac Gr Bio Syn A10 Rinsing the Milli Q for the fi
35. ule SaaS is shown y OPERATE STANDBY MEASURE CLEANING Pred OPERATE STANDBY 5 ERV E E AG E the age ofthe cartridge s is shown AS Ac G BoSji AtO Use ofKeypad continued CFWATBSANDBY MEASURE CLEANING MENU i either PRE OPERATE or PRODUCT Press MENU for at least 2 seconds 1 OPERATE STANDBY MEASURE CLEANINQ Press MENU I One press on the MEASURE button starts printing 2n OPERATBSTAM8Y MEASURE CLEANING OPERATE STANDBY MEASURE CLEANING Press MENU for at least 2 seconds 1 8 5 2 Q display returns back to initial operating mode 3 ppb Display the age of the UV lamp s and purification cartridges In either PRE OPERATE or PRODUCT Press MENU for at least 2 seconds OPERATEffiTANOBY MEASURE CLEANING y OPERATE STANDBY MEASURE CLEANING MENU Pr MEN er SERVICE AGE Res U twice UV LAMp 6SDAYS the age ofthe UV lamp is shown 1 OPERATE STANDBY MEASURE CLEANING MENU Press OPERATE STANDB Y once 5 ERV I His AGE mn u m the age of the UV lamp in the AIO TOC module Al i gt 8DAYS V is shown L SERVICE AGE OPERATBSTANOBY MEASURE CLEANING Press OPERATE STANDBY the age ofthe cartridge s is shown OPERATE STANDBY MEASURE CLEANING Press MENU for at least 2 seconds 1 8 2 display returns back to initi
Download Pdf Manuals
Related Search