Jerome® Hydrogen Sulfide Functional Test Module User`s
Contents
1. If the barbed desiccant fill cap is being used be sure it is not capped and any connected gas source or external desiccator is properly set up e Attach the line cord to the Functional Test Module Plug it into an 110VAC source and turn ON the power switch located on the side of the FTM e Allow the FTM to warm up and stabilize before proceeding Do not remove the cap from the tubing adapter The scrubbed exhaust gas is vented out the exhaust port at the rear of the module e After the warm up period verify that the FTM s pump lamp is flickering rapidly and that the heater lamp is blinking slowly or intermittently If either lamp is continuously off or on the unit may not be operating correctly Temperatures below 10 C or above 30 C may cause this The air source desiccator fill cap or exhaust port on the back of the unit may be plugged 700 0095 E Page 8 of 13 Remove the red vacuum cap and insert the tubing adaptor into the Jerome Analyzer s intake as shown If using a 631 X tighten the intake tube nut to ensure an airtight seal Verify that the Jerome 631 X or J605 is either in Auto range mode or an appropriate manually selected range for the gas level being produced by the FTM Refer to the 631 X or J605 Operation Manuals for additional information Take and record 10 analyzer samples as follows Press SAMPLE on the Jerome 631 X analyzer On the J605 press ENTER START or press the sample butt2. BACK TO THE FACTORY FOR RECALIBRATION NOTE IT IS UNLAWFUL TO SHIP THE FTM BY COMMON CARRIER WITH THE H2S PERMEATION TUBE INSTALLED THE PERMEATION TUBE IS CLASSIFIED AS HAZARDOUS CARGO IF THERE ARE ANY QUESTIONS OR YOU NEED ASSISTANCE CALL AZI CUSTOMER SERVICE TOLL FREE AT 800 528 7411 NOTE REFER TO THE JEROME 631 X OR JEROME J605 OPERATION MANUALS FOR SPECIFICS ON THE OPERATION OF THE HYDROGEN SULFIDE ANALYZERS 700 0095 E Page 3 of 13 INTRODUCTION A hydrogen sulfide gas sample of known concentration is generated from the Functional Test Module FTM and introduced into the Jerome 631 X or J605 Hydrogen Sulfide Gas analyzer If the H2S level shown on the instrument s display falls within the expected range you may be confident that your analyzer is functioning properly Refer to the Jerome 631 X or Jerome J605 Operation Manuals for specifics on the operation of the hydrogen sulfide analyzers Passing a known flow of clean dry air at a fixed temperature over an H2S permeation tube generates the sample gas concentration The flow rate and temperature are factory set to provide a measured concentration of H2S gas e Approximately 250 ppb 0 250 ppm 20 for FTM model Z2600 0918 e Approximately 30 ppb 0 030 ppm 20 for FTM model 22600 0930 Depending on the frequency of use the FTM s H2S permeation tube should last anywhere from three 3 months to two 2 years The permeation tube may be nearing exha
3. reduce the concentration and reduce the reading The FTM has feet on three of its sides The FTM can be oriented on whichever set of feet is best for your situation and application Performance is not affected by the orientation 700 0095 E Page 4 of 13 COMPONENT LOCATION amp IDENTIFICATION The major components of the FTM are identified in the diagram below Desiccant Fill Cap lt gt Pump cycle lamp Desiccant Viewing Window Heater cycle lamp JEROME wg romemona Permeation M AA chamber se cover plate Power switch and line cord receptacle P r Sample gas outlet There is also a male luer exhaust port on the back of the module not pictured MODULE SETUP H2S PERMEATION TUBE INSTALLATION e Inafume hood or well ventilated area remove the eight screws from the permeation chamber cover plate Remove cover plate with gasket from the module and remove the centering plate from the chamber e Unscrew the metal cap from the permeation tube shipping cylinder and slide out the plastic tube The plastic tube contains the permeation tube assembly and several bags of absorbent material e Remove the permeation tube assembly from the plastic tube and install it with the small end up in the center hole of the permeation chamber between the two filters as shown Be sure to save the shipping materials e Reinstall the centering plate and make sure all three cylinders are positioned in the cent
4. ARIZONA INSTRUMENT LLC Arizona Instrument LLC USER MANUAL FUNCTIONAL TEST MODULE H2S FTM 22600 0918 LOW LEVEL H2S FTM 22600 0930 April 2014 ARIZONA INSTRUMENT LLC 3375 N Delaware Street Chandler AZ 85225 USA 800 528 7411 602 470 1414 f 602 281 1745 www azic com Email General azi azic com International intl azic com Customer Service support azic com 3375 N Delaware St Chandler AZ 85225 800 528 7411 sales azic com www azic com MADE IN THE USA AZI P N 700 0095 E Last update April 2014 Z2600 0918 H S Functional Test Module Z2600 0930 Low Level H2S Functional Test Module Operation Manual PROPRIETARY RIGHTS NOTICE This manual contains valuable information and material developed by Arizona Instrument LLC for use with the Jerome instruments No part of this manual can be reproduced or transmitted in any form or by any means electronic mechanical or otherwise without the express written permission of Arizona Instrument LLC This includes photocopying and recording or in connection with any information storage or retrieval system ALL RIGHTS RESERVED Copyright 2000 2014 Arizona Instrument LLC Tygon is a registered trademark of Saint Gobain Performance Plastics Corporation 700 0095 E Page 2 of 13 TABLE OF CONTENTS INTRODUC TION ere tenter Ce rarr earn en neers Pree ean ee ree re Snr e reer teen e 4 COMPONENT LOCATION amp IDENTIFICATION ccccccscscictsscceccdt
5. D COPYRIGHT PROTECTION Jerome Arizona Instrument AZI and the stylized AZI are all registered trademarks of Arizona Instrument LLC All specifications subject to change without notice Copyright 2000 2014 Arizona Instrument LLC All Rights Reserved Tygon is a registered trademark of Saint Gobain Performance Plastics Corporation Arizona Instrument LLC Jerome H S Functional Test Module Operation Manual Part Number 700 0095 If you have any questions regarding the operation of this instrument please call our toll free number 800 528 7411 Internationally call 602 470 1414 or fax 480 804 0656 Arizona Instrument LLC 3375 N Delaware Street Chandler AZ 85225 USA http www azic com email support azic com 700 0095 E Page 12 of 13 FTM TEST FORM FTM TEST FORM DATE WARM UP START TIME PUMP READY flickering rapidly Y N discard discard discard discard discard MEAN PPM MEAN PPM MEAN PPM average of samples 6 10 average of samples 6 10 average of samples 6 10 FTM 930 FTM 918 FTM 930 FTM 918 FTM 930 FTM 918 024 to 036ppm 200 to 300ppm 024 to 036ppm 200 to 300ppm 024 to 036ppm 200 to 300ppm 24 to 36 ppb 24 to 36 ppb 24 to 36 ppb PASS FAIL PASS FAIL PASS FAIL TECHNICIAN 700 0095 E Page 13 of 13
6. ERMEATION TUBE REMOVAL CAUTION A SMALL AMOUNT OF H2S MAY BE RELEASED DURING THIS PROCEDURE THEREFORE THE REMOVAL OF THE PERMEATION TUBE MUST BE PERFORMED IN A WELL VENTILATED AREA OR DIRECTLY UNDER AN EXHAUST HOOD NOTE IT IS UNLAWFUL TO SHIP THE FTM BY COMMON CARRIER WITH THE H2S PERMEATION TUBE INSTALLED IF THERE ARE ANY QUESTIONS OR YOU NEED ASSISTANCE CALL AZI CUSTOMER SERVICE TOLL FREE AT 800 528 7411 Remove the eight screws and washers from the permeation chamber cover plate Remove the centering plate filters and permeation tube as needed e Ensure the permeation tube is placed in the original container and return it with the FTM to Arizona Instrument for calibration At the factory the perm tube will be reinstalled in your module for calibration The FTM must be calibrated with the perm tube and filters in place The perm tube and filters cannot be replaced in the field 700 0095 E Page 6 of 13 ACCESSORIES amp MAINTENANCE PARTS e The FTM includes the following parts Item Name Item Part Number FTM Z2600 0918 or Low Level FTM Z2600 0930 Perm Tube Assembly Perm Tube Housing 1400 3196 0 63 Diameter Fritware 2600 3054 0 250 ppm Perm Tube 1300 1025 or 0 030 ppm Perm Tube 1300 1040 This FTM Operation Manual 700 0095 The perm tube and internal filters can last up to two years depending on usage and both must be replaced at the factory The parts in the Accessory Kit listed below are field replaceable by t
7. ESS WARRANTIES GRANTED ABOVE SHALL EXTEND DIRECTLY TO BUYER AND NOT TO BUYER S CUSTOMERS AGENTS OR REPRESENTATIVES AND EXCEPT FOR WARRANTY OF TITLE IS IN LIEU OF ALL OTHER WARRANTIES WHETHER EXPRESSED OR IMPLIED INCLUDING ANY IMPLIED WARRANTIES OF FITNESS FOR A PARTICULAR PURPOSE AND MERCHANTABILITY SUCH OTHER WARRANTIES BEING SPECIFICALLY DISCLAIMED BY SELLER IN NO EVENT SHALL EITHER PARTY S LIABILITY FOR ANY BREACH OR ALLEGED BREACH OF THIS AGREEMENT EXCEED THE TOTAL EXTENDED PRICE OR PRICES SHOWN ON UNFILLED ORDERS NOR SHALL EITHER PARTY BE LIABLE FOR ANY SPECIAL INCIDENTAL OR CONSEQUENTIAL DAMAGES RESULTING FROM BREACH OR ALLEGED BREACH Notwithstanding the foregoing if any product covered by order s placed hereunder is designated as developmental prototype or experimental no warranty whatsoever except a warranty of title to component materials will be applicable thereto and buyer shall indemnify seller for any claims for liability asserted seller in connection therewith Medical Applications Seller s products are not designed for use in medical appliances devices or systems where malfunction of buyer s product can result in personal injury Buyer s customers using or selling buyer s products for use in medical applications do so at their own risk and agree to fully indemnify buyer The foregoing state the entire liability of seller in connection with products supplied hereunder 700 0095 E Page 11 of 13 TRADEMARK AN
8. dule Remove the tube from the instrument s intake and cap the output tube adaptor or the sample gas outlet if the Tygon tube is removed using the vacuum cap Unspent desiccant may be preserved by using the barbed desiccator fill cap and capping the barb 700 0095 E Page 9 of 13 The desiccant can be regenerated in an oven 200 C 400 F until the desiccant returns to its blue color Store the FTM in a dry well ventilated area away from sources of ignition heat and oxidizing agents CALIBRATION Arizona Instrument recommends annual factory calibration of the FTM Please contact AZI s Customer Service department at 800 528 7411 or 602 470 1414 or by e mail at support azic com for more information Visit AZI s web site at www azic com to request a Return Materials Authorization number and for a list of calibration prices Pre shipping reminders e Remove the permeation tube assembly from the FTM prior to shipping e Package the permeation tube assembly back in the original plastic tube and metal shipping container e Return the permeation tube in the metal shipping cylinder along with the FTM when returning the FTM for factory calibration or repair 700 0095 E Page 10 of 13 WARRANTY Seller warrants to buyer that products delivered pursuant to this Agreement shall at the time of delivery and for a period of one 1 year thereafter the Internal Battery Pack where applicable is warranted for a period o
9. ering plate holes as shown before reinstalling the cover plate 700 0095 E Page 5 of 13 Install two guide pins diagonally across from each other in each end of the permeation chamber Thread the pins in finger tight Make sure the gasket is aligned properly over the screws on the cover plate then position the cover plate with gasket back on the unit using the guide pins for alignment and with the sample gas outlet facing the front of the unit as shown in the large overview picture on the previous page Start the six screws in the plate s remaining screw holes THREADING them in only slightly Remove the two guide pins using the 5 64 Allen wrench Start the two remaining screws in the same holes PROGRESSIVELY tighten all eight screws evenly from the middle positions to the ends After tightening all eight screws start again from the middle positions and ensure all eight screws are tight FLOW SYSTEM CHECK Connect the unit to 110 VAC line power and turn the unit on Cover the hole in the desiccant fill cap with a finger or cap The PUMP light should be on continuously and the sound of the pump may get louder Cover the exhaust port on the back of the module with a finger or cap The PUMP light should be on continuously and the sound of the pump may get louder The flow system is operating properly if the PUMP light remained on Turn the module off and disconnect it from the 110 VAC power P
10. f ninety 90 days only be free from defects in material or workmanship and shall conform to seller s specifications or such other specifications as seller has agreed to in writing Seller s obligations with respect to claims under this warranty shall be limited at seller s option either to the replacement of defective or non conforming product or to an appropriate credit for the purchase price thereof subject to the provisions of seller s Warranty Policy as amended from time to time said Policy being incorporated herein by reference Return products under warranty claims will be shipped to seller s plant by buyer at buyer s expense and shall be accompanied by a statement of the reason for the return and an approved Return Material Authorization Number issued by seller Buyer remains responsible for payment for products not accepted for warranty adjustment and freight and handling costs associated therewith Notwithstanding the foregoing no warranty shall be enforceable in the event that product has been subjected to environmental or stress testing by buyer or any third party without written approval of seller prior to such testing Further no warranty shall be enforceable if the alleged defect is found to have occurred as a result of misuse neglect improper installation repair alteration accident or improper return handling procedure by buyer Discontinued product is warranted only for a credit or replacement at seller s option THE EXPR
11. he user e The following parts are included with the FTM Accessory Kit AZI Y2600 0920 Item Name Item Part Number 1 8 x 3 16 Reducer 1300 0031 These four items are Tubing Adaptor 1400 3010 pre assembled into the 1 of 1 8 Tygon tubing 345 0050 Tubing Assembly at 1 of 3 16 Tygon tubing 2500 3010 Me tacID Barbed Desiccant Fill cap 2600 3010 1 Lb Desiccant 2600 3055 2 Guide pins 2800 2044 115 VAC Line Cord 6000 4003 5 64 Allen wrench 2300 0003 e The following spare parts are also available Item Name Item Part Number 1 Amp Fuse 5100 1012 one spare fuse is included in the line cord receptacle Centering Plate 300 0968 Vacuum Cap Red PS 366 To order any of the above parts return the FTM for factory calibration or for permeation tube or filter replacement call AZI Customer Service at 800 528 7411 or 602 470 1414 Note The desiccant chamber in the Functional Test Module is quite small and is not suitable for extended operating periods in areas of high humidity The Barbed Desiccant Fill cap included with the Accessory Kit may be useful in extremely humid environments To use remove the standard desiccant fill cap from the FTM and replace it with the barbed version Larger external desiccators or bottled clean dry air at 0 PSI may be connected to the module using the barbed desiccant fill cap This is not typically necessary and in most applications the standard desiccant and fill cap are adequate Operating the Funct
12. ional Test Module with depleted or no desiccant will not damage the FTM or the Jerome Analyzer but may cause erratic test results 700 0095 E Page 7 of 13 FUNCTIONAL TEST PROCEDURE CAUTION PERFORM THIS TEST IN A WELL VENTILATED AREA AT NORMAL ROOM TEMPERATURE NOTE THE LOW LEVEL FUNCTIONAL TEST MODULE 22600 0930 REQUIRES 6 HOURS FOR WARM UP AND STABILIZATION FOR BEST RESULTS ALLOW THE FTM TO WARM UP AND STABILIZE OVERNIGHT ALWAYS KEEP THE TUBE ADAPTOR OR SAMPLE GAS OUTLET CAPPED WHEN THE FTM IS WARMING UP OR NOT IN USE THE STANDARD LEVEL FTM 22600 0918 ONLY REQUIRES ONE HOUR OF WARM UP NOTE DO NOT STORE OR OPERATE THE FUNCTIONAL TEST MODULE AT TEMPERATURES EXCEEDING 120 F OR 49 C e Perform a Sensor Regeneration on the Jerome 631 X or J605 Refer to the Jerome Analyzer s operator s manual for the procedure e Inawell vented area remove the red vacuum cap from the sample gas outlet of the FTM and firmly attach the open end of the tubing assembly to the sample gas outlet Place the red vacuum cap on the exposed end of the tubing adaptor at the other end of the tubing assembly USE CAUTION A small amount of H2S will escape Tubing Assembly e Remove the desiccant fill cap and the foam plug Do not remove the fritware rigid white disk at the bottom of the tube Remove any spent desiccant that has turned from blue to pink Refill with fresh indicating type desiccant Replace the foam plug and the cap
13. on at the end of the handle When the concentration reading appears record it wait 30 seconds then take another sample Repeat this until a total of 10 samples have been taken and recorded The last page of this manual can be printed out and used to record the data Disregard the first 5 samples and average the last 5 ACCEPTABLE AVERAGE VALUE RANGES H2S FTM 22600 0918 0 200 TO 0 300 ppm H2S 0 024 TO 0 036 ppm HS 24 TO 36 ppb H2S Low Level H2S FTM Z2600 0930 Ifthe average is within the acceptable range the Jerome Analyzer is functioning properly Ifthe average is NOT within the acceptable range consider the following troubleshooting questions make any necessary corrections and try again Were the functional test procedures followed exactly Is either the source or exhaust port plugged Did the FTM warm up and stabilize for the recommended time period Are all connections tight and proper Does your permeation tube need replacement How long has it been in use and for how many hours Can you check the FTM H2S output with another instrument Is it within range Do you suspect that your Jerome Analyzer may be malfunctioning or is out of calibration Has it been calibrated at the factory in the last year e Call AZI Customer Service Toll Free 800 528 7411 if you need help with any of the above or if you need to return your FTM or Jerome Analyzer for repair Uuuu y Turn off the Functional Test Mo
14. snesticssicnccineiicecieteatcicier 5 MODULE SE coe err ae aea erry meee ee eee eee ne 5 H2S PERMEATION TUBE INSTALLATION vvcssocctnccteritonsrcuticetncalsnasenticabeclnetoadtoatnens 5 FLOW SYSTEM CHECK epee renner Rem enn areemer aeruee mre aE EE 6 PERMEATION TUBE REM VA aati deseatacntussidaiidetisduiasdatiuesdataitiiastdatadaiindaesisuanbenddeanddiies 6 ACCESSORIES amp MAINTENANCE PARTS 1 0 0 ecceeeeeeeeeseeeeeeeenneeeeeeenaneeeeeeenaeeeeeeeeaeeees 7 FUNCTIONAL TEST PROCEDURE siietscnredinssstacsduectasideorbaesianctaaiiasrdentesstesbiaaenntioudenel 8 CALIBRA TION csecsen i ARE EA E AR AR RE 10 WARRANT Y oceciisicisiririsidiodreciisieri ini iii isi diid e d i diada ddila 11 FIM TESIT ac cance a a aN a E 13 An up to date electronic copy of this manual can be found on the AZI website at http www azic com IMPORTANT INSTRUCTIONS READ THIS FIRST CAUTION THE UNIT MUST BE UNPLUGGED IF THE PERMEATION CHAMBER COVER PLATE IS REMOVED FOR ANY REASON THE SOURCE OF H2S WILL BE INSTALLED UNDER THIS COVER PLATE AND WILL NEED TO BE REPLACED AT THE FACTORY WHEN DEPLETED A WELL VENTILATED AREA PREFERABLY A FUME HOOD SHOULD BE USED WHEN REMOVING THE COVER PLATE REMOVING THE PERMEATION TUBE OR FILTERS AND CLOSING THE COVER PLATE NOTE DO NOT STORE OR OPERATE THE FUNCTIONAL TEST MODULE FTM AT TEMPERATURES EXCEEDING 120 F OR 49 C NOTE PLEASE SAVE ALL PACKAGING MATERIAL H2S SHIPPING CYLINDER ETC TO REPACKAGE UNIT FOR SHIPMENT
15. ustion when the Jerome analyzer reads an output of less than 20 of the expected concentration Use of the FTM can be beneficial to e Verify that the Jerome Analyzer is operating e Verify that the Jerome Analyzer is reading correctly if unexpected readings are encountered during sampling operations e Comply with a company s routine maintenance requirements Sampling the H2S output of the FTM does not calibrate the Jerome 631 X or J605 The Jerome Analyzer can only be calibrated using a sophisticated NIST traceable calibration system at the factory or an authorized calibration laboratory Although the calibration interval depends on the amount of use and your quality specifications the recommended factory calibration interval is one year Several factors can affect the test results obtained from the H2S FTM used with the Jerome Analyzer Operator technique and environmental factors are the most important e Operator technique factors include The amount of wait time allowed after sensor regeneration film heat The frequency and number of samples taken and The placement of the equipment where extremes in temperature and airflow will occur e Environmental factors gt Some variation in H2S concentrations will occur with changes in temperature altitude and barometric pressure even though the instrument is automatically compensated for changes in ambient temperature and pressure Other gases may combine with H2S to
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