Apollo 9000 User Manual, Errata B
Contents
1. Add new sentence Wipe o ring down with a lint free wiper to remove excess grease to step 6b add 9 Continued Page 3 of 12 Apollo 9000 Errata B Section Page 2 9 Page 2 24 Page 4 of 12 Reference Delete all text in 2 9 and replace with Description Fresh catalyst background might be too high for most applications Before initial Apollo 9000 operation and each time the catalyst is replaced the catalyst conditioning procedure must be performed To condition the combustion tube catalyst 1 Make sure DI water vessel contains a minimum 1 liter supply 2 Set the combustion furnace temperature to 900 C Press and hold the Set button on the Temperature Controller and then press the Up arrow button until the display reads 900 C Release both buttons and wait until the furnace reaches 900 C Run the TOC Talk Cleaning Procedure Method as a sample for 10 replicates overnight in repetitive sampling mode every 5 minutes the minimum time allowed The next day exit the repetitive sampling procedure return the combustion furnace temperature to 680 C and run DI water as a TOC Sample For applications measuring 1 ppmC samples or less the raw data for this sample should be Less than 30000 area counts for the standard Apollo 9000 Less than 375000 area counts for the Apollo 9000 HS If your results do not approximate these values and you are running samples higher than 1ppmcC it may be2. 26 Delete the third and fourth sentences ns Delete step 7 Increment subsequent steps Diagrams Mode Diagrams p ii See second to last page of this erratum for current Ready Mode diagram Ready Mode p iii Update to current design TOC w ASM Needle Sparge p iv Update to current design TOC w IC Sparger Sparge p v Update to current design A p vi Update to current design s ee Wiring Diagram p vii See last page of this erratum for current Wiring diagram a e Page 10 of 12 Apollo 9000 Errata B Section Page Reference Description Spare Parts Entire section Remove Delete entire spare parts section in all subsequent user manual revisions A current parts list will be included separately in the unit kit box Please note Furnace Area and Remove following part s 14 773 1 068 14 7620 079 100 425 following changes Supplies Change part 14 7604 080 to 14 8072 080 and modify description to Injection block top half Modify description of 14 7698 000 to Injection port assembly for Apollo 9000 Remove 14 7605 080 14 7606 080 and 14 7641 043 Plumbing Area Remove 14 7631 150 Entire Index Remove References to the air cylinder Clippard 3 way valve Air Cylinder under the Combustion Furnace Injection slider and Injection slider under injection port slider sliding valve and under Valves valve 6 Appendix Page A 3 Daily Maintenance Add Inspect and clean syringe if appropriate
3. Checks Weekly Add Clean Syringe Reference Errata page 9 of 11 under Cleaning Maintenance Syringe on how to remove and clean syringe Checks Page 11 of 12
4. 12 Section Page New 5 4 Sample Blanks Reference Add new subtopic Run Recirculating TOC and TC Blanks Apollo 9000 Errata B Description If the DI water contribution to your standards is significant to your analysis you may want to run a recirculating blank method The blanking procedure for TC and TOC analysis will recycle DI water through the furnace and then sample from the water trap to determine the sample blank value Make sure to set the number of replicates to at least 6 when running a sample blanking procedure The results for blank methods are in raw data counts and the last 3 replicates are averaged as the sample blank IMPORTANT The raw data value for the sample blank should be less than the raw data for your DI water run as a TOC sample If it is not Tekmar Dohrmann recommends rerunning the sample blank or manually setting the sample blank To run a sample blank select the appropriate sample blank type under the Sample setup screen Table 5 4 2 outlines the correct blank setups for the default TOC and TC methods TOC TC Sample Method ID Blank Sample ID Blank Method ID TOC TC 0 20ppmC Blank TOC_TC Rng 1 Blank TOC_TC Rng 1 TOC TC 1 400ppmC Blank TOC_TC Rng 1 Blank TOC_TC 1 400ppmC TOC TC 10 750ppmC Blank TOC_TC Rng 2 Blank TOC_TC Rng 2 TOC TC 100 4000ppmC Blank TOC_TC Rng 3 Blank TOC_TC Rng 3 TOC TC 1000 25000ppmC Blank TOC_TC Rng 3 Blank TOC_TC Rng 3 When TOC_TC Blank Range 1 is chosen T
5. OC_TC 0 20ppmC will automatically be set as the Method ID Make sure to change this to TOC_TC 1 400 ppmc Table 5 4 2 TOC TC Sample Blanks Continued Page 7 of 12 Apollo 9000 Errata B Section Page New 5 4 Sample Blanks Page 8 of 12 Reference Add new subtopic Run an IC Blank Description The blanking procedure for IC analysis will measure the background of the DI water and acid used in an IC measurement to determine the sample blank value Make sure to set the number of replicates to at least 6 when running a sample blanking procedure The results for blank methods are in raw data counts and the last 3 replicates are averaged as the sample blank IMPORTANT The raw data value for the sample blank should be less than the raw data for your DI water run as an IC sample If it is not Tekmar Dohrmann recommends rerunning the sample blank or manually setting the sample blank To run a sample blank simply choose the appropriate sample blank type under the sample setup screen Table 5 4 3 outlines the correct blank setups for the default IC methods IC Sample Method ID Blank Sample ID Blank Method ID IC 0 20ppmC Blank IC Rng 1 Blank IC Rng 1 IC 1 400ppmC Blank IC Rng 1 Blank IC 1 400ppmC IC 10 750ppmC Blank IC Rng 2 Blank IC Rng 2 IC 100 4000ppmC Blank IC Rng 3 Blank IC Rng 3 When IC Blank Range 1 is chosen IC 0 20ppmC will automatically be set as the Method ID Make sure to change this to IC 1 400 ppm
6. T kmar DouRMANN Errata B Apollo 9000 User Manual 14 9000 074 May 24 2000 Overview Table of Contents G9 2 16 cal Leena aoe ern nn TTD ne nC OE TRO ERO 3 Errata for the Tekmar Dohrmann Apollo 9000 User Manual Rev A Part Number 14 9000 074 Version ae ea eee eee een eu nee eens 3 05 21 99 This information is near the bottom on the copyright page which backs the title page ETN US icc seats etre occ saica sted acdesteccatst a eatesiercasd a qatcterapieeeaeseieaees 5 NaDa EE 5 The Apollo 9000 User Manual and online help files a you received do not contain information about the Gl pyc 9 lt 1 che ere ee eC ee a teeter ane Rane hee enone 6 latest enhancements made to the instrument and software We will send you the revised user manual Chapter O aA EEAO A E OA 9 and online help files as soon as possible and DIAQKAINS aeaaee A RRE ORR 10 apologize for any inconveniences you may experience Spare Parts P A T T A A E 11 Please refer to the errata for the latest technical Index PEE AE E A E A A E O E E ETA EEA A 1 1 BOSC e o a a aie Appendix aaa A 11 technical assistance or have any questions regarding documentation please do not hesitate to contact the Tekmar Dohrmann Customer Support Center at 800 874 2004 or 513 247 7000 Thank you for your understanding The Tekmar Dohrmann Apollo 9000 Team Apollo 9000 Errata B Apollo 9000 Errata B created on May 24 2000 Section Page Reference Description Chap
7. acceptable to run standards and samples However if you are running gt 1ppmC samples then repeat the conditioning procedure to lower the raw data for your DI water and background NOTE Some users may not have DI water clean enough to meet these guidelines If you are running samples gt 1 ppmC your results may be acceptable If results are not acceptable then Tekmar Dohrmann recommends using an improved DI water source Apollo 9000 Errata B Section Page Reference Description Chapter 3 3 2 Figu re 32 update D TOC Talk Apollo 9000 HS i a Setup Run Results Help Page 3 3 ua Instrument Setup Status s screen to Operator Name USER4 x System i Preferences C Ready Sample Standby Max Integration Time min 4 0 Gas Flow Rates cc min Stabilize Baseline Time sec 30 To Furnace J Outlier Deletions 1 amp Print data report after each sample set Auto Shutdown w furnace off a Options 0 8mm Particulate Kit Installed Halt System If Out of Calibration Over Range l Autosampler Sparge Option Set instrument preferences Figure 3 2 Instrument Setup Status Screen Page 3 4 Update all 0 8 mm Particulate Kit Installed references to Particulate Kit Installed to Stabilize Baseline The recommended time is 15 seconds Time sec change last sentence text to 3 3 Change Gas Input 200cc min Page 3 6 Permeation Dryer flow to Change Gas Input Valve 7 ASM Sp
8. arge Valve 4 to Delete second to last bullet point in second column Entire chapter Replace all range 0 20 1 400 Chapter 4 references of 0 100 with Page 5 of 12 Apollo 9000 Errata B Section Page Reference Description Chapter 5 5 2 Figure 5 2 1 Update Instrument Setup Status screen to show 0 8 mm particulate option Page 5 3 and 15 second Baseline Stabilization time Page 5 4 Figure 5 2 4 Update Analysis Setup screen to show Method ID TOC 0 20ppmC Page 5 6 Figure 5 3 1 Update Instrument Setup Status screen to show 0 8 mm particulate option and 15 second Baseline Stabilization time Add new Section 5 4 Sample Blanks Add new subtopic Tekmar Dohrmann recommends setting the blank value to the raw data Manually Set the value of your DI water run as a sample To set this up go to the sample Sample Blank blanks review screen in the Results menu and enter the correct raw data value into for all three blank columns for the desired range of analysis Press OK to accept the changes Table 5 4 1 outlines the blank ranges as they correlate to the standard methods Sample Method ID Blank Type TOC TC 0 20ppmC TOC_TC Rng 1 TOC TC 1 400ppmC TOC_TC Rng 1 TOC TC 10 750ppmc TOC_TC Rng 2 TOC TC 100 4000ppmC TOC_TC Rng 3 TOC TC 1000 25000ppmC TOC_TC Rng 3 IC 0 20ppmC IC Range 1 IC 1 400ppmC IC Range 1 IC 10 750ppmC IC Range 2 IC 100 4000ppmC IC Range 3 Table 5 4 1 Blank Ranges Continued Page 6 of
9. cC Table 5 4 3 IC Sample Blanks Apollo 9000 Errata B Section Page Reference Description Chapter 6 6 1 Page 6 3 Correct misspelling in fourth paragraph of first column change text to pinch Add seventh bullet Inspect and clean syringe if appropriate to Daily Maintenance Checks text to read Add third bulletto Clean syringe see section 6 2 8 Weekly Maintenance Checks text to read Add procedure for Add following section on how to remove and clean syringe Cleaning Syringe Cleaning Syringe Copy from section 6 2 8 Syringe on page 6 11 but add after step 7 8 Pull plunger out of syringe Clean both plunger face and syringe with DI water until both are free of debris Modify and increment previous step 8 to 9 Reinstall the syringe making sure the Teflon washer is still in the 8 port valve Increment and add subsequent steps for installing the syringe 6 2 4 Delete entire Increment subsequent s and delete all references to Combustion Furnace pp 6 6 7 section Air Cylinder in Table of Contents and Index 6 2 5 Renumber 86 2 5 Increment subsequent s to 6 2 4 Page 6 7 Change text in Remove the 1 16 sample line entering the top of the injection port step 3 to Page 6 8 Delete steps Increment subsequent steps 4 5 12 and 14 Change text in Reattach the 1 16 sample line to the top of the injection port Make sure step 15 to fitting is hand tight but d
10. o not overtighten Delete step 16 Increment subsequent steps Step 17 Delete last sentence Delete steps 18 Increment subsequent steps and 19 Change text in Reinstall right cover to the instrument step 20 to Continued Page 9 of 12 Apollo 9000 Errata B Section Page Reference Description 6 2 6 Delete entire Increment subsequent 8s Page 6 9 section 6 2 8 Change section Replace Clean Syringe Page 6 11 title text to Copy from section 6 2 8 Syringe on page 6 11 but add after step 7 8 Pull plunger out of syringe Clean both plunger face and syringe with DI water until both are free of debris Modify and increment previous step 8 to 9 Reinstall the syringe making sure the Teflon washer is still in the 8 port valve Increment and add subsequent steps for installing the syringe 6 2 16 Figures 6 2 16 2 3 Update images to show new injection port Page 6 19 Page 6 20 Delete step 2a Place a loosely wadded tuft approximately 1 2 thick of quartz Replace step 2 text wool through the top of the combustion tube to just above the with narrow opening To prevent catalyst from dropping through the quartz wool gently pack the top of the quartz wool so that there is no space between the perimeter of the quartz wool and the glassware Page 6 21 a enn 4and Increment subsequent steps Page 6 25 Change reference to section X X in the second sentence to section 6 2 1 Page 6
11. ter 1 1 3 Figure 1 4 6 Replace with new drawing new injection port design does not have a slider Page 1 10 valve Replace last two The injection port provides the interface for the sample line and the paragraphs in furnace carrier gas into the combustion furnace The sample line enters second column from the top of the injection port and the carrier gas enters from the right with of the injection port Chapter 2 2 4 Replace last For most connections allow 3mm 1 8 of tubing to extend past the end of Page 2 8 sentence instep 2 the ferrule For 8 port valve fittings make sure tubing is flush with the end of second column of the ferrule with Page 2 11 Remove text from 1 2 Tygon step 2 of second column 2 5 Delete step 2a Place a loosely wadded tuft approximately 1 2 thick of quartz Page 2 13 replace step 2 text wool through the top of the combustion tube to just above the with narrow opening To prevent catalyst from dropping through the quartz wool gently pack the top of the quartz wool so that there is no space between the perimeter of the quartz wool and the glassware Add new step Add 0 5 quartz wool on top of catalyst The added quartz wool will between steps 3 protect and add life to the catalyst and 4 Page 2 14 Figure 2 5 4 Replace with new image new injection port design does not have a slider valve Page 2 15 Figure 2 5 5 Replace with new image new injection port design does not have a slider valve
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