The miVac Modular Concentrator Series
Contents
1. The miVac Modular Concentrator Series User Manual Part number 04 5057 Issue 2 6 September 2012 rc es SQ Contents Ta dg ere To OM NER 2 ETT a AEEA S AOA AA APANE E IEEE 4 Warnings and cautions 0 cccccseeeeeeeeeeeeees 4 Precautions varen 4 Combustible solvents rrrrrrrrnnnrnrennrnnnnnvenn 5 Electrical earthing cccccseeeeeceeeeeeseeeeeeeaees 5 Strong AGIOS sanne seemeidnnddk spe 5 Limitations Of USe rrarrrnnnrrrrannerrannennnnrnnnnnene 5 Ga EE EEE EE 6 Duo concentrator rrrarrrnnnnenvnnnrvnnnnennnnnnnnnnene 6 Quattro Concentrator 6 SpeedTrap mnvvannvvnnrvnnnevnnnevnnnnnnnrnnnnrnnnnennnne 7 Duo Quattro PUMP cccccceeceeeeeeeeeeeeees 7 Super high VACUUM PUMDP cccceeeseeeeeeeeeees 8 Pressure controller cccccececseeeeeeeeeeeeeeeees 8 Lyo OPTION rerrnnnnvvrnnnnonnnnnnrnnnnnnrennnnnnennnnsnennnnn 9 DNA concentrator rrnnrnnnnnornnnnrrnnnnennnnrnnnnnr 10 ROOTS seedet aner ecenesestiaoesebeesaecacs 10 Vapour trap rrrrnnnrvvrnnnnvvnnnnnrvvnnnnrennnnenennnnnn 11 CCESSOFIGS rrrrannnnnanrernnnrnnnnnrnnannennassennnnsnnnn 12 Basic Operation ennxrnnnnennnnnrnnnnennnnennnnnennn 13 OL EL NE NN 13 Opening the lid rrrnnrrrnrrrnnnnnnnnronnnrrnnnnnnnnre 14 Standby mode sirrinin nisani ninen 14 OOS EE 15 LCD SEE eee 16 Getting started rrrrnrrrrrrrnnnnnrnrvrnrrrnnnnnnnnre 17 Selecting a method rrr2. The evaporator should not be discarded in your regular disposal stream Contact your Representative or Genevac for proper disposal instructions Within the EU it is Genevac s responsibility under the WEEE directive to provide for the recycling of Genevac products ad All rights reserved Genevac Ltd 2012
3. Patents miVac products are protected by the following patents and patent applications 1153278 FR 52 04 5057 Issue 2 6 September 2012 User Manual miVac Modular Concentrator Series Amendment control Issue Reason for change Date Issued 2 1 Revise layout includes many changes from previous issue 4 Feb 11 2 2 Expand Pre heat instructions and add section in Troubleshooting Expand instructions for setting chamber temperature and heat time Remove list of 07 Mar 11 rotors Revise electrical specifications Add entrapment safety warning to Opening the Lid Add recommended service interval 2 3 Referred to DNA concentrator in place of DNA flow of energy in place of 23 Mar 11 heat flow solvent being condensed in place of solvent being concentrated 2 4 Add troubleshooting rotor slipping Standardised conventions across all 05 Mar 12 manuals Move Standby mode before Controls Changed Check before use to Recommended practice Update DNA image Add instruction to replace pump catch pot with vapour trap Add recommended Method and SpeedTrap Mode to Acceptable Solvents table 2 5 Add SpeedTrap jar seal maintenance Add SVP specifications update 27 Jul 12 dimension and weight specifications Add Lid seal maintenance Amend environment specification pollution degree 2 Add spindle friction washer replacement instructions 2 6 Update MST seal kit part number and Spindle friction washer part number 5 Sep 12 04 5057 Issue
4. seal leaks Check for damage dirt Clean if required Hoses Check for leaks Check for blockages Check connections Control valve if fitted not opening Check connected to concentrator pump outlet Check vapour flow direction Condenser jar not sealed Remove jar and check seal for damage debris Replace seal see Maintenance Pump inefficient Run system without samples for five minutes Repeat three times then reload samples Exhaust silencer muffler blocked Replace exhaust silencer muffler SpeedTrap jar seal leaking See Maintenance SpeedTrap jar seal Condenser jar full Empty jar Pump needs servicing Contact your distributor Excessive concentration times Poor vacuum See Maintenance SpeedTrap not operating correctly See SpeedTrap Insufficient chamber heat Adjust Heat time Excessive solvent in pump SpeedTrap not operating correctly See SpeedTrap Incorrect run settings 04 5057 Issue 2 6 September 2012 Select run settings suitable for your solvent 47 miVac Modular Concentrator Series User Manual Other troubleshooting continued Symptom Cause Corrective action miVac pump runs Connected directly to mains Connect to concentrator using continuously power interconnecting lead Excessive sample Solvent vapour exhausting in to Check connections odour lab Check pump system exhaust ducted
5. similar type of plates e Do not exceed the maximum safe loading weight of 0 6 kg per swing for Duo swing rotors and 1 1 kg per swing for Quattro swing rotors Final checks e Make sure tubes vials are located correctly in the rotor e For swing rotors rotate a swing rotor by hand after loading to check that all plates are correctly located before starting a run and before re starting an interrupted run 04 5057 Issue 2 6 September 2012 31 miVac Modular Concentrator Series User Manual Method Guide Pre programmed methods The concentrator has three pre programmed methods during the evaporation process air is vented into the evaporation chamber to optimise evaporation conditions for the solvent The amount of venting is determined by the method selected Method Venting rate When to use H20 Low For water only OH High For alcohols and alcohol mixtures No venting For all other solvents The OH and H20 methods also turn the pump off periodically to aid the flow of energy into the samples For Duo and Quattro concentrators the H20 method is optimised for aluminium rotors This method is recommended when evaporating more than a few tubes of water however full vacuum may be faster if there are just a few tubes For DNA systems use the H2O method when evaporating water or solvents with similar boiling points Alternatively the performance of any miVac modular system can be enhanced with the addition of a pressu
6. the system when it is operating in auto mode The auto or manual LED flashes to indicate the system is stopping four longer beeps sound when the rotor is about to stop The time remains on the LCD screen until the lid is opened 04 5057 Issue 2 6 September 2012 19 miVac Modular Concentrator Series User Manual Advanced Operation Method parameters can be adjusted at any time including when the concentrator is operating To adjust a method parameter Turn the SELECT control brackets appear around different areas of the LCD display Press the SELECT control the brackets begin to flash Turn the SELECT control the selected value increments up or down Press the SELECT control the new value is entered Note If the SELECT control is not pressed the displayed value is automatically entered after 30 seconds Method choice There are three methods to choose from e H20 for water only e OH for alcohols and alcohol mixtures Eo ene for all other solvents For further information refer to Method Guide 20 04 5057 Issue 2 6 September 2012 User Manual miVac Modular Concentrator Series Setting chamber temperature The chamber temperature can be controlled from 30 C to 80 C by 1 C increments If the temperature is set below 30 C the display shows C and the chamber heater is turned off Once the new value is selected the display reverts back to showing the current chamber temperature in t
7. to suitable fume extraction point No SpeedTrap LED No mains supply Check SpeedTrap mains power illumination supply lead Excessive boiling of Warm solvent Stop run and empty jar solvent in SpeedTrap restart run jar No solvent in Excessive vacuum Check vacuum appropriate to SpeedTrap jar application Incorrect run type Select suitable run type Poor cooling Allow SpeedTrap to cool for 30 minutes with no concentration then Restart run Check LED status Check air flow ensure vents are clear from obstruction Poor solvent recovery Excessive vacuum Check vacuum appropriate to application Incorrect run type select suitable run type Poor cooling Allow SpeedTrap to cool for 30 minutes with no concentration then restart run Check LED status Check air flow ensure vents are clear from obstruction 48 04 5057 Issue 2 6 September 2012 User Manual Technical Data Specifications DNA concentrator Max rotor speed 1465 rom Sample acceleration 250G Drive system Permanent magnet electronic Dimensions w x dx h 360 x 602 x 300 mm Catch pot Add 141 mm to width Weight 41 5 kg Duo Concentrator Max rotor speed 1465 rom Max sample acceleration 250 G Drive system Permanent magnet electronic Dimensions wxd xh 360 x 424 x 300 mm Weight 21 kg Quatro concentrator Max rotor speed 1130 rom Max sample acceleration 250 G Drive system Permanent magnet electronic Dimensions wxdxh 480 x 594 x 300 mm Weight 35 kg
8. 057 Issue 2 6 September 2012 User Manual miVac Modular Concentrator Series Other troubleshooting Symptom Cause Corrective action Display blank No power Check power supply lead Lid will not open difficult to open Dirty lid seal Clean lid and seal External control valve if fitted wrong way round Rotor will not spin double beep Lid not fully closed Open and close lid Check lid seal fully seated Check for obstructions Rotor jammed Check for freedom of rotor Rotor will not stop Rotor spindle greasy or slippery rotor continues to spin after spindle stops Clean degrease rotor and spindle Fit spindle friction washer or replace if defective Excessive vibration noise Rotor imbalanced Check and rebalance rotor Rotor slipping Clean degrease rotor and spindle fit spindle friction washer Missing exhaust silencer muffler Replace exhaust silencer muffler Uneven work surface Take corrective action Chamber fails to reach programmed temperature Heat time not set or insufficient Adjust Solvent splashes condensation inside vacuum chamber SpeedTrap not operating correctly See SpeedTrap Poor vacuum See Maintenance Overfull plates See Loading Samples Concentrator vacuum chamber too cold Pre heat before use Vacuum problems Pump not running Check connections mains power supply Lid
9. 057 Issue 2 6 September 2012 User Manual miVac Modular Concentrator Series Basic Operation Power up The Duo DNA or Quattro concentrator powers up as soon as It is connected to mains power All segments of the LCD screen temporarily switch on and illuminate to test they are functioning correctly i CO TOTAL HEAT a m GE I am ED a am iC PNL Co ODD lig When the display reverts to showing the current settings the system is ready to be used Hon TOTAL EIH H l There is a power switch on the back of the SpeedTrap which allows it to be switched off while it remains connected to mains power Power switch The vacuum pump remains in standby mode until the system is started refer to Starting the concentrator 04 5057 Issue 2 6 September 2012 13 miVac Modular Concentrator Series User Manual Opening the lid The concentrator lid is automatically locked when the rotor spins and only unlocks when it is safe to open To open manually lift the front edge of the lid Warning Risk of hand entrapment Secure the lid in the upright position before placing hands near the concentrator Standby mode When the system is idle powered up but not operating press the STOP E button to enter standby mode Press any button to restart the system 14 04 5057 Issue 2 6 September 2012 User Manual miVac Modular Concentrator Series Controls On the front panel there are four push buttons a r
10. 2 6 September 2012 53 mi Vac Genevac Limited The Sovereign Centre Farthing Road Ipswich IP1 5AP United Kingdom Sales and Service Hotlines Service 44 0 1473 243000 Sales 44 0 1473 240000 Fax 44 0 1473 461176 Email service genevac co uk salesinfo qgenevac co uk applications genevac com Web site http www genevac com Genevac Inc SP Industries 815 State Route 208 Gardiner NY 12525 United States of America Sales and Service Hotline 1 845 267 2211 Fax 1 845 267 2212 Email salesinfo genevacusa com Service spscientific com Useful Information Read these instructions before operating the miVac pressure controller and keep them near the system for easy reference Your attention is drawn in particular to the Safety section These instructions are correct at time of going to press and may be subject to change without notice Some of the features and software functions described within this user manual may not apply to equipment manufactured before this manual s publication date this includes systems that have been upgraded No part of these instructions may be reproduced in any form or be processed duplicated or distributed by electronic or optical means without the written permission of Genevac Limited If you need to contact Genevac for assistance use either the telephone or fax Hotlines shown Please have the instrument serial number at hand Alternatively email or visit our web site
11. 57 Issue 2 6 September 2012 User Manual miVac Modular Concentrator Series Lyo option Using the cooling vents on side of the SpeedTrap as mounting holes and fit the lyo option isolation valve bracket to the SpeedTrap Note Different sized screws are supplied to allow the bracket to be fitted to either side of the SpeedTrap Using a length piece of vacuum pipe connect the concentrator to the isolation valve Using another length of vacuum pipe connect the other side of the isolation valve to the SpeedTrap vacuum inlet Fit the isolation valve to the bracket as shown Connect the remaining vacuum pipe between the SpeedTrap and the scroll pump system To complete the installation connect the mains power supply cables to the scroll pump SpeedTrap and concentrator 04 5057 Issue 2 6 September 2012 41 miVac Modular Concentrator Series User Manual If required the miVac SpeedTrap can be set up as a Stand alone system without the need for a concentrator to be connected refer to front cover illustration In this case the isolation valve should be left permanently in the closed position and the concentrator pipe need not be connected If the miVac system features a pressure controller this can remain connected to the vacuum line between the pump and the SpeedTrap as shown 42 04 5057 Issue 2 6 September 2012 User Manual miVac Modular Concentrator Series Stand alone SpeedTrap If connecting a miVac SpeedTrap to
12. RICT 001 1 Removal Remove the damaged washer from the 2 Push down to form a conical shape at the concentrator spindle base of the spindle 36 04 5057 Issue 2 6 September 2012 User Manual SpeedTrap jar seal If the SpeedTrap jar fails to seal or does not miVac Modular Concentrator Series tighten when inserted and twisted a quarter Refitting turn the seal and thread inserts should be 1 replaced Parts required 9 Description Part number Replacement seal and thread insert kit MST SEALS 000 Removal 1 Remove the SpeedTrap jar 2 Using the screw driver undo the screws and remove the three thread inserts as Insert the O ring into the SpeedTrap moulding Insert one of the three retaining features of the PTFE seal into one of the three recesses in the SpeedTrap moulding and secure it in place using a thread insert and screw Do not tighten the screw Taking care to avoid creasing or distorting the PTFE seal fit the remaining two thread inserts shown 4 Check the PTFE seal and O ring are correctly fitted with no creases or bulges then tighten all three screws Testing 1 Fit the SpeedTrap jar and check it jar feels tight 2 Operate the miVac system to make sure 04 5057 Issue 2 6 September 2012 there are no vacuum leaks use dummy samples if necessary to make sure the concentrator operates correctly 37 miVac Modular Concentrator Series User Manual Unpacking an
13. SpeedTrap Type Single stage vapour compression Refrigerant R404a Ultimate low temperature 50 C Ultimate defrost temperature 60 C Rapid defrost Yes Rapid defrost over ride Yes after Feb 2011 Jar Plastic coated borosilicate glass Jar capacity 1 litre optional 2 litres Dimensions wxd xh 212 x 563 x 450 mm Weight 25 8 kg miVac Modular Concentrator Series Duo pump Ultimate vacuum 10 0 mbar 7 5 torr Flow rate 38 litres per minute Dimensions wxdxh 215x389 x 300 mm Weight 19 kg Quattro pump Ultimate vacuum 2 0 mbar 1 5 torr Flow rate 33 litres per minute Dimensions wxdxh 215x389 x 300 mm Weight 18 kg Super high vacuum pump Ultimate vacuum 0 15 mbar Flow rate 83 litres per minute Dimensions wxdxh 249 x 427 x 288 mm Weight 23 kg Storage transportation environment Ambient temperature 10 to 55 Relative humidity 0 to 95 Altitude Sea level to 12000 m Operating environment Ambient temperature Relative humidity Altitude 0 C to 30 C 0 to 95 Seal level to 1600 m Note This evaporator is designed for use ina pollution degree 2 environment normally only nonconduictive pollution occurs Emissions Noise levels typically 70 dB A at one metre from the concentrator during normal operation For the purpose of air conditioning requirement calculations it can be assumed that all power is dissipated as heat Note Dimensions include allowances for pipe connections and for lid opening figur
14. Warnings and cautions This symbol is used within this manual to highlight warnings and cautions n Warning highlights a risk of personal injury or material damage Caution highlights a risk of material damage The following symbols may be found on the equipment A This symbol means surfaces may be hot and could cause burns A This symbol means there is risk of hand entrapment LI Refer to the relevant part of the User Manual for additional information AG Precautions These Two symbols combined indicate hazards that can lead to serious material damage or potential serious injury Refer to the relevant part of the User Manual Observe the following safety precautions when using the miVac system Only use rotors that are approved for use by Genevac Do not leave the system unevenly loaded someone may start it Do not start or restart a system without checking it is evenly loaded Do not place objects on top of the system A Caution Incorrect loading may result in damage to samples and to the miVac system 4 04 5057 Issue 2 6 September 2012 User Manual miVac Modular Concentrator Series Only allow users who are familiar with all the issues outlined in this User Manual to operate the equipment If personnel lack the training or experience to comprehend the hazards that can arise when operating the miVac system do not allow them to use it personnel without such training require thorough instruction and the ins
15. acuum and the timer starts to count up indicating the time accumulated The concentrator continues until the STOP E button is pressed Auto mode To start in auto mode press the AUTO gt button The concentrator emits a single beep to confirm acceptance of the command and the rotor begins to spin if the lid is not closed a double beep sounds and the concentrator will not start The LED adjacent to the AUTO button lights up to show the system is operating in auto mode Once a safe rotor speed is reached the system begins to apply vacuum and the timer starts to count down from the set time indicating the time remaining The concentrator stops when the timer reaches zero or if the STOP button is pressed Evaporation in progress While the evaporation is in progress the LCD screen shows the elapsed time when operating in manual mode or the time remaining when operating in auto mode When the time displayed is greater than one hour it is shown in hours and minutes HH MM when the time displayed is less than one hour it is shown in minutes and seconds MM SS Stopping the concentrator To stop the concentrator press the STOP E button the concentrator emits a single beep to acknowledge acceptance of the command The STOP E button can be pressed at any time the system will always stop safely When operating in auto mode the concentrator stops automatically when the timer reaches zero The STOP button can also be used to stop
16. centration performance and a pressure controller can be added to enhance the system s flexibility still further A choice of oil free vacuum pump completes the system Speed Trap Pump DNA combined concentrator and pump Quattro concentrator Duo concentrator Optional pressure controller installed with system If required components from the miVac range may be used with similar equipment from other manufacturers All equipment is designed for ease of use offers very high performance and takes up the smallest possible amount of bench space in the laboratory 2 04 5057 Issue 2 6 September 2012 User Manual miVac Modular Concentrator Series Set up is simple with just one set and select control and a minimum number of push button controls When the system is operating a large LCD screen shows the sample temperature and elapsed time Sy lt gt k gt SE e n i RT Woes ce SS z e 6 Push buttons for art O stop start preheat LCD screen SELECT control This manual will explain the set up process and show you how to operate the system It will guide you through the maintenance requirements and provide information to facilitate the most efficient procedure to protect the integrity of your samples and ensure optimum performance from the system at all times 04 5057 Issue 2 6 September 2012 3 miVac Modular Concentrator Series User Manual Safety
17. d Setting Up On delivery please check the contents of the delivery as soon as possible against the delivery note and notify your distributor immediately if any parts are missing or damaged Refer to our web site for up to date contact details Installation site The miVac system must be placed on a level sturdy work surface Make sure there is enough space for a 50 mm air gap between each of the miVac units and the edge of the bench a wall or any other equipment DNA The DNA Concentrator with its built in pump can be easily positioned on most benches Fit the catch pot to the upper vent holes on the concentrator connect the short tube between the exhaust connector on the pump and the catch pot Connect the mains power cable supplied T Exhaust i connector Catch pot clips gt onto upper vent f holes ese 38 04 5057 Issue 2 6 September 2012 User Manual miVac Modular Concentrator Series Modular systems The following example refers to a Duo concentrator Speed Trap and Duo pump the set up process is much the same for the Quattro concentrator and Quattro pump Position the concentrator SpeedTrap and pump on the workbench as shown Allow 50 mm air gap around system Connect the pump catch pot by clipping it onto the cladding vent holes on the side of the vacuum pump Connect the units together using the 12 7 mm 72 vacuum hose supplied cut to length using the hose cutter Secure the hoses with hose cli
18. ent traces and wipe the lid seal clean before removal Note The seal may absorb significant quantities of some solvents 3 Manually remove the lid seal from the chamber by carefully pulling the seal away from the chamber Do not use tools that may damage the chamber coating Refitting 1 Unpack the replacement lid seal 2 Position the lid seal on top of the vacuum chamber 3 Work the seal firmly into position using only fingers press the seal fully home 04 5057 Issue 2 6 September 2012 miVac Modular Concentrator Series Testing 1 Close the lid 2 Select any method and start the concentrator 3 Make sure the pressure begins to drop the lid seal feels tight against the chamber and cannot be opened Note Manual pressure may be required on the lid to assist the new lid seal to bed in on the first use If the pressure fails to drop check the lid seal is correctly located on the vacuum chamber and repeat the test 4 Allow the concentrator to continue for a while checking for normal operation Completion Dispose of the defective seal and packaging 35 miVac Modular Concentrator Series User Manual Spindle friction washer The friction washer prevents rotor slippage during spin up and spin down Check the Refitting condition of the washer frequently and 1 replace it if damaged or worn Place the washer over the spindle Parts required Description Part number Quantit Friction washer RTR F
19. equipment other than a miVac modular system connect it as shown Solvent vapour in I from external equipment External vacuum 3 source Using the power cable supplied with the SpeedTrap connect the SpeedTrap to the mains power supply Stand alone pump If connecting a miVac pump to equipment other than a miVac modular system connect it as shown Vacuum connection to external equipment If using a catch pot fit it to pump by clipping it to the cladding vent holes on the side of the vacuum pump Using the power cable supplied connect the pump to the mains power supply 04 5057 Issue 2 6 September 2012 43 miVac Modular Concentrator Series User Manual Vapour trap To install the optional vapour trap remove the pump catch pot and replace it with the vapour trap Connect the pump exhaust to the vapour trap top connector inlet connect the outlet elbow connector to the laboratory fume extraction system Inlet connect to pump exhaust q m Outlet connect to we i laboratory fume extraction 4 s lt S system ats Final checks Carry out a safety assessment before operating the miVac system Make sure the exhaust hose takes solvent away from personnel and from the system in a safe manner If personnel lack the training or experience to comprehend the hazards that can arise when using the miVac system do not allow them to use it Personnel without such training require thorough
20. es quoted for weights are for guidance only actual weights vary with build options such as mains input voltage 04 5057 Issue 2 6 September 2012 49 miVac Modular Concentrator Series User Manual Electrical Power VA W Voltage Freq DUP amp DUC DUP amp QUC MST oe ae V Hz Peak Norm Peak Norm Peak Norm USA 120 60 590 390 850 470 495 452 250 150 UK amp Europe 220 60 520 340 800 430 495 441 250 150 Japan Japan 100 60 490 350 660 400 450 389 250 150 Key DUP DUC QUC SpeedTrap For DNA concentrator refer to Duo concentrator with Duo pump Figures for normal running power norm err on the high side based on the heater being on for 30 of the run time typically heat is on for 5 to 10 of the run Note The systems may momentarily take current in excess of these figures Genevac therefore recommend the use of appropriately rated type C or D circuit breakers on the main supply 50 04 5057 Issue 2 6 September 2012 User Manual miVac Modular Concentrator Series EC declaration of conformity EC Declaration of Conformity miVac Products Manufacturer s Name Manufacturer s Address Type of Equipment Genevac Ltd Farthing Road lpswich Suffolk IP1 5AP UK Laboratory Equipment This is to certify that the following product s DNA Concentrator models Duo Concentrator models Quattro Concentrator m
21. freely Check mains power supply within tolerance 08 Lid failed to lock Make sure lid is closed and engaged with latch Check lid seal is fully seated 09 Lid failed to unlock Make sure lid is closed and engaged with latch Make sure user not lifting lid against latch Check lid seal is fully seated 10 Software error sensor read error Clear error and attempt to restart 11 Software error chamber temperature low Clear error and attempt to restart 72 Software error chamber temperature high 04 5057 Issue 2 6 September 2012 Clear error and attempt to restart 45 miVac Modular Concentrator Series User Manual Clearing faults and errors To clear an error press and hold the STOP button for five seconds Alternatively switch the system power off wait five seconds and then switch the power back on again If the problem is still apparent contact your distributor or Genevac Service Opening lid without power In the event of a power supply failure the lid can be unlocked manually to allow access to samples Using a narrow tool inserted through the hole in the cladding above the top left hand side screw press on the lid lock actuator to open the lid vented to atmospheric pressure before opening the lid Wait at least two minutes following a power failure before opening the lid n Warning Risk of injury make sure the rotor is stationary and the system has 46 04 5
22. h 2010 Being the person appointed by Genevac Ltd to sign on their behalf Where X A B D or F and denotes the power lead code appropriate to the destination country 04 5057 Issue 2 6 September 2012 51 miVac Modular Concentrator Series User Manual Warranty statement This product is guaranteed for period of 12 months from the date of delivery In the unlikely event of any defect arising due to faulty materials or construction resulting in system failure the unit will be repaired free of charge This includes all labour and component costs incurred This warranty is subject to the following provisions e The system must be sited installed and operated in accordance with the user manual e The unit may only be used for the purpose it was sold and in accordance with Genevac published compatible solvent list e Regular cleaning and preventive maintenance schedule to be adhered to as detailed in the user manual See Maintenance e If items are replaced by the owner only Genevac approved parts may be used e Inthe event of a vacuum pump failure the pump may be exchanged for a refurbished unit The owner is responsible for the exchange and return of the failed unit Failure to adhere to the above would invalidate the warranty and result in the costs of repairs being charged This warranty does not cover accidental damage modification misuse or inappropriate repair by untrained personnel and does not cover consumable items
23. he following example the current chamber temperature is 24 C Select parameter 04 5057 Issue 2 6 September 2012 21 miVac Modular Concentrator Series User Manual Pre heat For solvents with a boiling point greater than 90 C the chamber should be pre heated to avoid solvent condensation in the evaporation chamber Prolonged exposure to certain solvents in liquid form may cause damage to the concentrator lid coating To pre heat the concentrator press the PRE HEAT button An LED adjacent to the PRE HEAT bution lights up to show the chamber heater is active and the chamber warms up to the currently set control temperature For best results place the empty rotor in the concentrator and leave the concentrator lid closed while pre heating Caution Bumping may occur if the sample temperature is too high when the concentrator is started To avoid the possibility of damage to samples do not pre heat the concentrator with samples loaded Once the concentrator is started by pressing either the MANUAL or AUTO P start buttons the chamber remains at the control temperature until the heat time elapses the chamber heater then switches off Latching pre heat Pre heat can be latched to stay on continually throughout the evaporation process and after the concentrator stops This function allows the chamber to be kept warm ready for the next use To latch on pre heat press and hold the PRE HEAT button for five seconds A co
24. instruction The instructions contained within this User Manual may form the basis of such training Maintain a solvent vapour free environment around the miVac system Do not use the free Space around the system for the storage of vessels containing solvents or acids This instruction applies even if the miVac system is installed in a fume cupboard Caution After setting up leave the SpeedTrap in the upright position for 24 hours before switching on 44 04 5057 Issue 2 6 September 2012 User Manual Troubleshooting Faults and errors miVac Modular Concentrator Series If the miVac system detects a problem an error number is shown on the LCD display When errors occur during operation the error number is shown when the system stops Rectifying faults and errors Errcode Cause of error 01 Software error memory failure Rectification Clear error and attempt to restart 02 Lid not closed during run Make sure lid is closed and engaged with latch Check lid seal is fully seated 03 Lid not locked during run Make sure lid is closed and engaged with latch Check lid seal is fully seated 04 Motor drive error Clear error and attempt to restart 05 Rotor failed to spin Manually rotate rotor approximately 45 and restart 06 Rotor failed to reach speed Make sure rotor spins freely Check mains power supply within tolerance 07 Rotor stops unexpectedly Make sure rotor spins
25. ll engaged to ensure that there is no condensed vapour in the pump Ultimately it is the responsibility of the user to check with the pump manufacturer as to how the pump should be operated 04 5057 Issue 2 6 September 2012 5 miVac Modular Concentrator Series User Manual Options The modular concentrator SpeedTrap and pump units can be installed in multiple combinations to form the basis of the evaporation system Duo concentrator The Duo concentrator is designed to accept a two swing position microplate holder or a range of disc rotors for tubes or vials Quattro concentrator The larger Quattro concentrator can accommodate a four swing position rotor larger capacity disc rotors and can also accept Duo rotors 6 04 5057 Issue 2 6 September 2012 User Manual miVac Modular Concentrator Series SpeedTrap SpeedTrap condenser can improve the performance of any miVac system by removing large volumes of vapour and condensing them to liquid The effect is a dramatic improvement in the system s ability to maintain vacuum and is reflected in reduced concentration times Duo Quattro pump A choice of either Duo 10 mbar or Quattro 2 mbar diaphragm pump can be selected to complement either Duo or Quattro concentrator Both pumps offer oil free low maintenance operation 04 5057 Issue 2 6 September 2012 F miVac Modular Concentrator Series User Manual Super high vacuum pump For exceptionally demandi
26. ments and to gain familiarity with the safe loading procedure outlined below Preparation To reduce concentration time the system can be pre heated before use If rapid concentration is important leave the empty rotor in the concentrator with the lid shut and pre heat enabled short evaporation runs in particular will benefit from this Refer to Pre heat for further details AN Caution To avoid damage to samples do not pre heat with the samples loaded The following graph shows the typical reduction in concentration time that can be achieved firstly by using a SpeedTrap and then by pre heating both chamber and rotor Typical miVac Duo Evaporation Times Water in centrifuge tubes hh mm DNA system No Speedtrap Duo with a pre Duo starting from Duo with a pre warmed chamber AND 30 04 5057 Issue 2 6 September 2012 User Manual miVac Modular Concentrator Series Loading e Balance the rotor within 10 g e Only load tubes or vials into the rotors that are specified on the rotor e For the Duo two position swing rotor use a maximum of three shallow well microplates with stackers or one deep well microplate per rotor location e For the Quattro four position rotor use a maximum of five shallow well microplates with stackers or two deep well microplates per rotor location e Only fill wells of microplates to 66 of their maximum fill level e When using swing rotors always load opposite swings with the same or
27. n with backlight 04 5057 Issue 2 6 September 2012 15 miVac Modular Concentrator Series User Manual LCD screen The LCD screen provides numeric information for setting control parameters and monitoring evaporation progress TOTAL a n E gt a aa TENE 2 LALLA a gt 1 Method indicator H20 water OH alcohol or full vacuum 2 Temperature Chamber temperature 3 Timing mode TOTAL time from start or HEAT time 4 Timer Time elapsed in manual mode or time remaining in auto mode 5 Adjustment mode Brackets appear around parameter to indicate it can be adjusted using the SELECT control Hon TOTAL am lt gt ue C morc Coma 6 Cr 6 Error The LCD screen also advises of any problems that occur during operation or with the settings being entered 16 04 5057 Issue 2 6 September 2012 User Manual miVac Modular Concentrator Series Getting started The following is a quick reference guide only Detailed descriptions of features and operating instructions are provided later on in this user manual 1 Switch on the power at the mains supply 2 If required use the SELECT control to set the pre heat temperature and press PRE HEAT 3 Open the lid for Quattro concentrator make sure the latch engages 4 Fit the rotor by sliding it on to the shaft 5 Load the rotor with samples make sure the rotor is evenly balanced 6 Close the lid for Quattro concentrator lift the lid
28. nfirmation beep sounds to acknowledge acceptance of the command the chamber warms up to the control temperature and the heater continues to control the chamber at the control temperature throughout the evaporation process and after the system stops even if the STOP E button is pressed To cancel the function press the PRE HEAT button again Note For older systems software versions pre V1 09 the chamber preheats to 40 C irrespective of the chamber control temperature 22 04 5057 Issue 2 6 September 2012 User Manual miVac Modular Concentrator Series Setting total time This feature allows the user to set the total time duration of the evaporation process when using auto mode Select the timer Set the time required The LCD display counts down the time remaining Hed TOTAL am eZ l MIC 1 _ 04 5057 Issue 2 6 September 2012 23 miVac Modular Concentrator Series User Manual Setting heat time This feature controls the time duration that chamber heating is applied Note The heat time e cannot be longer than the TOTAL time e has no effect if PRE HEAT is latched on Select the timer Select HEAT HEAT a mr j Set the heat time F Li fs The LCD display counts down the heat time remaining Han vide WIC NN Ir i 24 04 5057 Issue 2 6 September 2012 User Manual miVac Modular Concentrator Series Display mode The LCD display is factory set to show TOTAL time H
29. ng applications a 0 15 mbar super high vacuum Scroll pump can be selected This pump offers oil free low maintenance operation Pressure controller For enhanced performance a pressure controller can be added to any modular miVac system The device can automatically sense the control pressure for any solvent or can provide vacuum ramping to reduce the risk of bumping 8 04 5057 Issue 2 6 September 2012 User Manual miVac Modular Concentrator Series Lyo option A Lyo Option can be added to any modular miVac system that features a condenser with switchable defrost mode manufactured from March 2011 and must be installed in conjunction with a high vacuum pump The miVac Lyo Option consists of vacuum isolation valve and mounting bracket cascade condenser pot insulated vial holders three rubber valves Additional accessories can be ordered individually 04 5057 Issue 2 6 September 2012 9 miVac Modular Concentrator Series User Manual DNA concentrator The DNA concentrator offers an alternative to modular units combining a Duo concentrator and Duo pump into an integrated unit The DNA is capable of removing small volumes of water and organic solvents the unit is extremely compact and will easily fit on a bench top There is no option to add a SpeedTrap Rotors A full range of rotors is available for the miVac range including e open sample holders e solid aluminium JetRotors e swing rotors for microtitre
30. odels SpeedTrap models Duo Pump models Quattro Pump models Super Vacuum Pump models Control Valve model Serial Numbers from Conform to the Essential Health and Safety requirements of European Directives DNA 23050 x00 DBP 23050 x00 DUC 23050 x00 DPP 23050 x00 QLP 23050 x00 QUC 23050 x00 QHP 23050 x00 MST 23050 x00 DUP 23050 x00 QUP 23050 x00 SVP 23050 x00 UOP 00000 Y00 Individual declarations are available on request e Machinery Directive 2006 42 EC e EMC Directive 2004 108 EC and e Low Voltage Directive 2006 95 EC A technical construction file for this product is held at the above address Conformity is demonstrated by compliance to the following standards signed eg Name G Broadbent e BS EN 61010 1 2001 Safety requirements for electrical equipment for measurement control and laboratory use General requirements e BS EN 60204 1 2006 A1 2009 Safety of machinery Electrical equipment of machines General requirements e BS EN 61326 1 2006 Electrical equipment for measurement control and laboratory use General EMC requirements e BS EN 12100 1 amp 2 2003 A1 2009 Safety of machinery Basic concepts general principles for design amp technical principles e BS EN 378 2 2008 A1 2009 Refrigerating systems and heat pumps Safety and environmental requirements Design construction testing marking and documentation Position Chief Electrical Engineer Date 10th Marc
31. odes These units operate in periodic defrost mode only Collection jar Empty the collection jar after every use Do not empty the collection until the concentrator has stopped Take care when removing the collection jar it may be heavy when full of solvent Do not allow the solvent level to fill above the max line this may cause damage to the pump Inspect the collection jar for damage cracks etc before every use e Empty the drip tray regularly to avoid the risk of splashing To remove the collection jar grasp the handle to support the weight and rotate the jar a quarter turn to the left 28 04 5057 Issue 2 6 September 2012 User Manual miVac Modular Concentrator Series To refit the jar position it so that the handle is to the front lift the jar and rotate a quarter turn to the right tighten the jar until there is light resistance Waste solvents normally collect as liquid in the SpeedTrap jar however ice may form under certain conditions If this happens allow it to thaw naturally if necessary add cold water to the jar to accelerate the thawing process Caution Do not use implements to break the ice in the SpeedTrap jar as this may damage the Jar 04 5057 Issue 2 6 September 2012 29 miVac Modular Concentrator Series User Manual Loading Samples Samples in the concentrator chamber are subjected to accelerations of up to 250 G Itis therefore important for the operator to understand the safety require
32. or no defrost When operating in periodic defrost mode defrosting of the condenser coil is fully automatic The green LED on front of the SpeedTrap indicates when the defrost cycle is operating After defrost the SpeedTrap switches to chilling then condensing LED Condition Fast flash Defrosting Slow flash Chilling Steady Condensing The system automatically defrosts for three minutes in every hour without the need for any intervention When the switch is set to no defrost the SpeedTrap operates continually without periodic defrost The mode may be switched while the SpeedTrap is operating If the mode is switched from periodic defrost to no defrost the SpeedTrap performs a short three minute defrost before continuing to operate in no defrost mode If switched from no defrost to periodic defrost the SpeedTrap chills for 57 minutes before performing a short three minute defrost When choosing which mode of operation to select consider the solvent being condensed for further information refer to Method Guide 04 5057 Issue 2 6 September 2012 27 miVac Modular Concentrator Series User Manual Manual defrost To manually initiate a defrost momentarily press the switch down to the defrost position The defrost cycle takes approximately 30 minutes to complete or can be cancelled manually by momentarily pressing the switch down again Note SpeedTraps manufactured before February 2010 do not have switchable defrost m
33. otary SELECT control and an LCD screen Q G g Q 1 MANUAL Press once to start the system in manual mode the concentrator emits a single beep starts and continues to operate until the STOP button is pressed Whilst operating in this mode the respective LED lights up and a timer counts up to show the total time accumulated 2 PRE HEAT Press once to pre heat the chamber to the control temperature PRE HEAT is disabled when either the MANUAL or AUTO button is pressed Alternatively press and hold for five seconds to latch on chamber heater continually 3 AUTO Press once to start the system in auto mode the concentrator emits a single beep starts and continues to operate until the TOTAL time set has elapsed Whilst operating in this mode the respective LED lights up and the timer counts down to show the time remaining 4 STOP Press once to stop the system the concentrator emits a single beep and stops The STOP button can be pressed at any time and the system will shutdown safely If the STOP button is pressed when the system is idle it will enter standby mode Press any button to bring the system out of standby 5 SELECT Turn the control to select a parameter frame it with brackets then press it to select brackets flash to indicate adjustment mode Turn the control to increment the setting up or down and press again to enter the new value The display reverts back to normal mode after 30 seconds 6 Display LCD scree
34. plates Your local miVac distributor will be happy to offer advice or information on the full range of miVac rotors available 10 04 5057 Issue 2 6 September 2012 User Manual miVac Modular Concentrator Series Vapour trap For neutralising ammonia or acid vapours on systems with Duo or Quattro pumps the vapour trap replaces the pump exhaust catch pot and comes complete with all connectors required to fit it to the pump Order using Genevac part number VAP TRAPO 100 lt t Pa I eg q 3 me dd EE LP IG n r Fs Lae f v Ko Note Requires neutralising solution see Accessories 04 5057 Issue 2 6 September 2012 11 miVac Modular Concentrator Series User Manual Accessories Part number STJ 10000 000 Description 1 litre jar for miVac SpeedTrap MCK 00000 Y00 System connection kit for connection of pump and or SpeedTrap trap to concentrator complete with a 2 5 m length of vacuum hose hose cutter power lead to control pump and catch pot for pump RTR FRCTN 001 spindle friction washer prevents rotor slippage during spin up spin down 04 4783 Vacuum hose specify length when ordering 04 5016 Exhaust hose specify length when ordering 04 6095 Clip for vacuum hose VAP TRAPO 100 Vapour trap requires neutralising solution NH3 REFOO 100 Neutralising solution for amonia 4 x 500 ml ACD REFO0 100 12 Neutralising solution for acid 4 x 500 ml 04 5
35. ps as shown To fume extraction system Pump catch pot Hose clips If the modular system does not have a SpeedTrap connect a single vacuum hose between the concentrator and the pump Note Hoses hose clips and the hose cutter are available in the miVac connection kit extra lengths of vacuum and exhaust hose are also available Refer to the Options section for details 04 5057 Issue 2 6 September 2012 39 miVac Modular Concentrator Series User Manual Once the hoses are fitted refer to the following diagram and connect the electrical cables Pump Speed Trap Concentrator Connect the pump to the concentrator using the interconnecting cable A Connect two mains power cables B and C one to the concentrator and one to the Speed Trap Note Do not connect the pump directly to the mains power supply If a cable is supplied this is for standalone use of the pump only Irrespective of the model of miVac pump the connections and function are the same When used with the miVac series of concentrators the electrical power is supplied and controlled by the concentrator using the interconnecting lead When used with non miVac concentrators the power lead is connected to the mains power supply adjuster on the rear of the SpeedTrap is set to the correct frequency for the local mains power supply Caution If setting up a system for use in Japan make sure the frequency 50Hz 60Hz Frequency adjuster 40 04 50
36. re controller which allows automated pressure control and vacuum ramping If a pressure controller is used the miVac concentrator must be set to no venting SpeedTrap The SpeedTrap mode can be set to optimise conditions for the solvent Switch position SpeedTrap Mode When to use oe ii Periodic defrost For water or water mixtures No defrost For organic solvents that will not freeze 32 04 5057 Issue 2 6 September 2012 User Manual Acceptable solvents miVac Modular Concentrator Series Solvent Abbreviation Recommended SpeedTrap All systems method mode Acetic acid ae oe v Acetonitrile ACN OH oe v Acetone OH oe v Ammonium Hydroxide H20 k u v Butan 1 ol or H20 oe v Butan 2 ol or H20 oe v Butyl Acetate H20 k u v Chloroform TCM OH oe v 1 2 Dichloroethane OH oe Dioxane H20 k u v Ethanol EtOH H2O or OH oe v Ethyl Acetate OH oe Formic Acid k u Heptane OH oe Hexane Hex OH oe v Methanol MeOH H20 oe v Methyl Tertiary Butyl Ether OH oe Methylene Chloride DCM OH oe v Propan 1 ol or Propanol OH oe v Propan 2 ol or isopropyl OH v Alcohol IPA OH oe v Tetrahydrofuran OH Toluene or H20 oe Water H20 k u v only be used in systems where all units concentrator SpeedTrap and pump were manufactured after April 2007 The date of manufacture is shown on the instrument s serial plate n Caution Sol
37. rnnnnnrnnvvvnnn 37 Unpacking and Setting Up 0 38 Installation site rrrrrnnrrrranrrrrannernarrnnnnnenn 38 PN ae 38 Modular Systems rrnrrrerrrnnnrrrvrvrnnnnnrrnnnnnn 39 EYO OPON NE ENN 41 Stand alone SpeedTrap rrrrrrnnnnnevnrnnnnnne 43 Stand alone pump ccccceeeesseeeeeeeeeeeeeeaes 43 VP Perser 44 PUTTE ner 44 Troubleshooting ranxevanurnnnennnnennnnnnnnennnnen 45 Faults and CrrOrs ccccceeccceceeeeeeceseeeeeeeeees 45 Rectifying faults and errors rrnnrrenrnnrrvrnnnn 45 Clearing faults and errors eceeeeeeeeeees 46 Opening lid without power rrnnrrrrnvevnnnnnnnn 46 Other troubleshooting ccccccccceeeeeeeeeees 47 Technical IDA A vasansiciassnsdwnsrsasisnarsnsicnascaciosaan 49 Specifications rrrrrrrrrnnnnnrrvrrrrvrrnnnnnrnnvvnnnn 49 EC declaration of conformity cc008 51 Warranty statement rrrrrrnnrnrrrnnnnerrnnnnennnnn 52 GU EE 52 Amendment Control cccccceeceeeeeeeeeeeeees 53 Useful Information cccccscecececcecececeenees 54 miVac Modular Concentrator Series User Manual Introduction miVac is a modular range of centrifugal concentrators that can be combined in different ways to provide great flexibility for a variety of applications Concentrators feature built in methods for alcohol and water and come in two different sizes an optional SpeedTrap can dramatically improve con
38. rrrrnnnnnrnrvvnnrrnnnnnnnnre 18 Starting the concentrator ccccseeseeeeeees 19 Evaporation in PrOQreSs cscccceeeeseeeeeees 19 Stopping the concentrator rrrrrnrnnnnnnnnn 19 Advanced Operation cccsseseseeeeees 20 Method choice cc cceccccceeeeeeeeeeeeeeeeeeeeeeas 20 Setting chamber temperature 0008 21 Poe 22 Latching pre Neat cccccssseecsssseeeseeseeeees 22 Setting total time rrrrrrrrrrnnnrrnvvvrrrrrnnnnnnnrr 23 Setting heat time rrrrrnrrrnnnnnnnrrvvnrrnnnnnnnnrr 24 Display mode rrrnrrrnnnrrvvnrnnnnnvvnnrnnnnnvrnnnnnnnre 25 Specat mms 26 Waste solvent rrrnnnnnrnnannonnnnnonnnnrnnnnnnnnnnrr 26 BL os 10 EE 27 Manual defrost rrrrrnnnnrorrrnnnrnronrrnnnnnvennnnnn 28 Collection jaf ae 28 Loading Samples rannennnnnrnnnnonnnnnnnnnnennnnner 30 Preparation rrnnnnvnnnnnnvnnnnnnvnnnnnnrnnnnnnsvnnnnnne 30 20 AGING EE EEE 31 FINALGNECKS maren 31 Method Guide nsessavrnnsanonnennensunnensunvansennnn 32 Pre programmed methods rrrrrernnnnnvrvvnn 32 SPeed Trap oo eseccsscecsseeceeeeeeeeeeseeseeeees 32 Acceptable SolventS rrrrrnrrrnnnrrnrnnnrnnnnre 33 LE Ti sd g 5 Io 34 Recommended practice ccccccseeeeeeeeees 34 CNS SNS EE 34 Concentrator lid seal rrrrrnnrrrrnnnnnrnnvvvnnn 35 Concentrator spindle washer 0 0066 36 Speed Trap jar seal rrrrnnrrnrrr
39. t I TOTAL I MIC REN LI VL But it can be changed to show HEAT time when operating in auto mode Hed HEAT DLC MM IM gt a To change the display mode hold down the SELECT control for five seconds a single beep sounds to acknowledge acceptance of the command The display changes to indicate HEAT until the count down reaches Zero then reverts to showing the TOTAL time remaining eC _ To change the display mode back from HEAT time to TOTAL time hold down the SELECT control again for five seconds 04 5057 Issue 2 6 September 2012 25 miVac Modular Concentrator Series User Manual SpeedTrap The miVac SpeedTrap offers Unique frost free cold trap Selectable automatic defrosting all solvents including water collect as liquids Easy to empty collection jar Ideal for use on all concentrators except freeze driers A Caution Refer to list of acceptable solvents before use Waste solvent Waste solvents normally collect as liquid in the SpeedTrap jar however ice may form under certain conditions Refer to Collection Jar for further information Occasional sudden boiling within the jar is normal and solvent will re condense 26 04 5057 Issue 2 6 September 2012 User Manual miVac Modular Concentrator Series Defrosting The SpeedTrap has two possible modes of operation which can be selected using the switch located on the SpeedTrap splash back panel periodic defrost
40. to disengage the latch 7 Using the SELECT control set the chamber temperature Set the method type Set the total run time Set the heat time Note if the above parameters are not set the system will use the last settings entered 8 Press the MANUAL or AUTO button to start the concentrator 04 5057 Issue 2 6 September 2012 17 miVac Modular Concentrator Series User Manual Selecting a method To select the required method turn the SELECT control until brackets appear around the method indicator Press the SELECT control the brackets begin to flash to indicate the parameter may be adjusted Turn the control until the required method is shown then press to select The LCD display shows the selected method tt TOTAL WIC NM C I 18 04 5057 Issue 2 6 September 2012 User Manual miVac Modular Concentrator Series Starting the concentrator The concentrator can be started in either manual mode or auto mode Select the required method and set the temperature before starting the concentrator Manual mode To start in manual mode press the MANUAL P button The concentrator emits a single beep to confirm acceptance of the command and the rotor begins to spin if the lid is not closed a double beep sounds and the concentrator will not start The LED adjacent to the MANUAL button lights up to indicate the system is operating in manual mode Once a safe rotor speed is reached the system begins to apply v
41. tructions contained within this User Manual may form the basis of such training Combustible solvents Warning Risk of vapour ignition Only operate the miVac system in a well A ventilated environment and consider safety when evaporating any combustible solvents Genevac s position regarding the evaporation of such solvents particularly with respect to the European ATEX directive is available on our website at www genevac com or from your local Genevac distributor Electrical earthing Warning Risk of electric shock This equipment must be earthed the miVac system is a safety class 1 product according to IEC classification It must never be used with any interruption to the safety earth conductor It is an installation category II product and is intended to operate from a normal single phase supply Strong acids attempt to evaporate strong acids such as HCI TFA or HBr at any concentrations Caution The miVac concentrator is unsuitable for use with strong acids Do not Limitations of use Caution Rotary vane oil filled vacuum pumps are not recommended for use with miVac systems Vapours from the system may cause damage to the pump Notwithstanding the above advice if a rotary vane oil pump is used the pump should be run with the gas ballast set to position 1 this will help to prevent damage to the pump Oil pumps should then be run for one hour after the end of the concentration process with ballast sti
42. vents that do not have a symbol v in the All systems column can 04 5057 Issue 2 6 September 2012 33 miVac Modular Concentrator Series User Manual Maintenance In order to provide trouble free operation Genevac recommend the miVac pump Is serviced annually Any servicing or repair of miVac products other than that which is specified within this User Manual should be carried out by Genevac personnel or approved representatives of Genevac using only approved spare parts Recommended practice Check before use All hose joints are secure e The SpeedTrap collection jar empty if necessary e The catch pot is connected to the pump exhaust empty if necessary Cleaning e Clean the SpeedTrap collection jar at regular intervals o Collection jar is dishwasher safe but not suitable for an autoclave e Clean the lid lid seal exterior paintwork and inside of the chamber with a soft lint free cloth slightly dampened with o Detergent solution o Bleach solution if using biological agents o Methanol o Ethanol e Do not use abrasives 34 04 5057 Issue 2 6 September 2012 User Manual Concentrator lid seal Parts required Description Part number Quantit Lid seal Duo 04 4722 1 Lid seal Quattro 04 4793 1 Warning Risk of contamination Solvent traces may be present that could be harmful to health or lead to material damage Removal 1 Switch on the miVac concentrator and open the lid 2 Check for solv
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