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240 Fld Instruction Manual - California Analytical Instruments, Inc.

1. 9 4 2 Menu Tree 10 4 3 Keyboard 11 4 4 Operation with Cursor KeyS 11 4 5 Operation with Function Keys 11 4 6 Read and Change Parameters 11 OPERATING STRUCTURE 12 els Main Menu 12 13 MENU STRUCTURE 020 02nenenenenenenenenenenene 14 6 1 User Functions Level 1 14 6 2 Advanced User Functions Level 2 14 6 3 Maintenance User Functions Level 3 14 6 4 system User Functions Level 4 14 MAIN MENU 2 2 22 02 220 nn nn nnn nn nnn m m 15 LA F1 Measurement 15 7 1 1 F1 NO or NOx Measurement
2. 16 7 1 2 F2 NO NO2 Measurement 15 16 7 1 3 F3 Diagnostics 16 7 1 4 Arrow Keys to Cycle Ranges and Auto Range 17 7 2 F2 Purge Analyzer 18 7 3 F3 DiaQnOStiCs nnn nnn nnn nnn nnn nn nnn nnn nnn a 18 7 4 F4 Calibrations 19 7 4 1 F1 Automatic Calibration 19 20 7 4 2 F2 Manual Calibration 20 21 7 4 3 F3 Display Deviations 21 22 7 4 4 F4 Check Calibration Values 22 7 4 5 F5 Reset Calibration Values 22 7 4 6 F6 Range Select 22 Fo FO SGIUD meedia 23 7 5 1 F1 Span Gas Concentrations 24 7 5 2 F2 Calibration Settings 24 TOLA F1 TIMES
3. 24 TOLA F2 Measuring Deviations 25 15 2 3 F3 Deviations 25 7 9 2 4 F4 Calibration via Valves 25 7 9 2 9 F5 Calibration via Probe 25 7 5 3 F3 Range Limits 25 1 Did F1 Change Upper Range Limits 25 1 90 39 2 F2 Change Auto Range Limits 26 7 5 4 F4 Change Alarms 26 7 5 5 F5 Password 27 CEN F1 Enter Password 27 TOOse F2 Change Password 27 7 9 9 3 Fo Reset PasswordS 2 22 22 nnn nnn nn nnn nnn nnn nnn ncn nnn 28 7 5 6 F6 Linearization 28 7 0 F7 System Settings n ne neon nnn nnn nn nnn nnn nnn en neces cnn 29 ESTE F1 Clock Setup 29 30 Tiled F2 TCP
4. 5 3 2 Site and Mounting 5 3 3 Electrical 5 3 4 I O Analog Connections 5 3 5 Required Gases 5 3 6 Gas Handling Equipment 5 3 7 Gas Connections 5 3 8 Sampling Requirements 7 3 8 1 Filtration 7 3 8 2 Condensation 7 3 8 3 Presence of Corrosive Gases 7 3 8 4 Gas Temperature 7 3 8 5 Flow Rate 7 3 8 6 Sample Gas Outlet 8 BASIC OPERATION 2 0 020000000 00000000 9 4 1 Display
5. Note For Analyzers Sold After June 2007 Please See Addendum starting After Page 71 of This Manual CAL Sa aye ay 1312 West Grae Avenue Orange CA 92865 4134 Phone 714 974 5560 Fax 714 921 2531 www gasanalyzers com Safety Alert Temperature Hazard Electrical Shock Hazard Caution or Warning Caution or Warning Caution or Warning Safety Information in this Manual Note caution and warning symbols appear on the instrument and throughout this manual to draw your attention to important operational and safety information A NOTE marks a short message to alert you to an important detail A CAUTION safety alert appears with information that is important for protecting your equipment and performance A WARNING safety alert appears with information that is important for protecting you others and equipment from damage Pay very close attention to all warnings that apply to your application The symbol an exclamation point in a triangle precedes a general CAUTION or WARNING statement The AN symbol wavy vertical lines with an under score in a triangle precedes an elevated temperature hazard CAUTION or WARNING statement The A N symbol a lightning bolt in a triangle precedes an electric shock hazard CAUTION or WARNING statement Some or all of the above symbols may appear in this manual or on the equipment This manual should be consulted whenever one of these symbols is encounter
6. Ales JE A p zj y es E3 m Q ONVERTER Vitreous Carbon Material 205 C gt 98 efficiency OZONATOR Ultraviolet Lamp AIR OR O Less than 0 01 ppm NOxat 350 cc Min 25 psig Dew Point lt 35 C REQUIREMENTS NO NOxControl Manual Remote Auto Cycle Remote NOx mode by dry contact closure OUTPUTS TCP IP RS232 Four Scalable Analog 0 10 V 4 20 mA Maximum DISCRETE ALARMS General Fault TTL Logic Ground True 0 5 VDC Maximum Local amp Remote Calibration Failure TTL Logic Ground True 0 5 VDC Maximum Adjustable High Concentration 2 each TTL Logic Ground True 0 5 VDC Maximum DIAGNOSTICS Temperatures Flow Parameters KEYPAD DISPLAYS Factory Settings Scalable Analog Output Voltages TCP IP Address Full Scale Range Select Passwords 4 Auto Cal Times SPECIAL FEATURES Calculated NO derived from NOx converter efficiency Auto Ranging Auto Calibration adjustable through internal clock Less than 3 cc Gold Plated Reaction Chamber DISPLAY 3 x 5 Back lit LCD en fo to 75 C Noncondensing Standard Higher temperature available upon TEMPERATURE request TEMPERATURE HUMIDITY 115V 60 Hz Option 230V 50 Hz 10 500W Note 5 to 1 5 l min flow rate options available upon request only California Analytical Model 600 HCLD C_ETL_US CE Operators Manual March 2006 Page 4 of 71 Section 3 INSTALLATION 3 Installation 3 1 General The instrument is designed for industrial app
7. Sample EPC Coil Voltage Air Ozone EPC Coil Voltage ADUF Flows Command Response Description _ADUF_KO _ADRU_s Zz y y_ All flows are responsed _ADUF_KO x _ADRU_s z z Flow of x is responsed Description of x Sample Flow AGRD Polynom coefficients Command Response Description _ AGRD_KO Mn AGRD s Mn a0 al a2 a3 a4 Polynom coefficients of range Mn are responsed AANG Deviation from zero point after autocalibration Command Response Description _AANG_KO _AANG_s M1 z z da_dr_ Deviation from zero point after M2 z z da dr M3 z z da _dr_ autocalibration M4 z z da dr_ AAEG Deviation from end point after autocalibration Command Response Description _AAEG_KO _AANG_s M1 z z da_dr_ Deviation from end point after M2 z z da dr M3 z z da dr_ autocalibration M4 z z da dr_ California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 56 of 71 Section 13 APPENDIX AFDA Purge and Autocalibration times Command Response Description _AFDA_KO_SATK _AFDAKO_SSPL AFDA_s z z APAR Request Autocalibration tolerance values Autocalibration times z Purge time y Calibration time x Total Calibration time w Verify time Z y X w in seconds Purge time will be responded Command Response Description _APAR_KO_SATK _APAR_s z z y y_x x_w w AKAL Deviations from calibration Autocalibration tolerance value z z Range 1 y y Range 2 x x Range 3 w w Range 4 Command Response Description AKAL
8. Section 4 BASIC OPERATION 4 2 Keyboard The keyboard looks as follows Combined control numeral keys To the main menu Display lighting F6 6 on off a Delete ke Endi y nra nd input open selected field for input Switch over of the keyboard numeral control keys Cancel back to the last menu Arrow keys for selecting the functions and editing fields and for scrolling possible input values Figure 2 Keyboard 4 3 Operation with the Cursor Keys and the Enter Key When operating the unit with the cursor keys you select the various functions with the up down cursor keys and start them with the Enter key This method is particularly suitable for less proficient users since the system displays a short on line help for nearly every function selected The actual cursor position is shown as a black horizontal bar TIP If you are not yet familiar with the screens and their fields just press any cursor key after a screen appears This moves the cursor from field to field and displays the corresponding online help 4 4 Operation with the Function Keys When using the function keys FI though F10 you call functions directly by pressing their corresponding function keys This method is suitable for the advanced user since it is faster than the operation with the cursor keys There is however no on line help for the various functions 4 5 Read Change Parameters To read and or change parameters you must s
9. d if the product claimed to be defective requires on site repair such warranty labor will be provided at no charge however transportation and living expenses will be charged to Buyer e if the product is a consumable or the like it is warranted only to conform to the quantity and content and for the period but not in excess of one year stated on the label at the time of delivery or 90 days f CAI may from time to time provide a special printed warranty with respect to a certain product and where applicable such warranty shall be deemed incorporated herein by reference g CAI shall be released from all obligations under all warranties either expressed or implied if any product covered hereby is repaired or modified by persons other than its own authorized service personnel unless such repair by others is made with the written consent of CAI IT IS EXPRESSLY AGREED THAT THE ABOVE WARRANTY SHALL BE IN LIEU OF ALL WARRANTIES OF FITNESS AND OF THE WARRANTY OF MERCHANTABILITY AND THAT CAI SHALL HAVE NO LIABILITY FOR SPECIAL OR CONSEQUENTIAL DAMAGES OF ANY KIND OR FROM ANY CAUSE WHATSOEVER ARISING OUT OF THE MANUFACTURE USE SALE HANDLING REPAIR MAINTENANCE OR REPLACEMENT OF ANY OF THE PRODUCTS SOLD UNDER THIS SALES ORDER SOME STATES DO NOT ALLOW THE EXCLUSION OR LIMITATION OF INCIDENTAL OR CONSEQUENTIAL DAMAGES SO THAT THE ABOVE LIMITATIONS OR EXCLUSIONS MAY NOT APPLY THIS WARRANTY GIVES YOU SPECIFIC LEGAL RIGHTS AND YOU MAY ALSO HA
10. 3 Tj Set Concentration Pressure and Voltage Alarms California Analytical Model 600 HCLD C_ETL_US CE March 2006 Page 26 of 71 Operators Mi Section 7 MAIN MENU 7 5 5 F5 Password After turning on the analyzer you are in access level 1 To change the access level or to change the passwords press F5 Setup in the main menu and Press F5 Password again The following screen appears Enter Change Password 7 5 5 1 F1 Enter Password To change access level press F1 The following screen appears Access Level Screen F1 to F4 selects an access level Move the cursor to the access level to be modified You must enter the correct password for the access level desired The passwords for the various operation levels consist of three numbers that must to be entered on the numeric keypad If the code word is incorrect you are asked to re enter the codeword IMPORTANT TIP When anew analyzer is powered up it defaults to access level 1 User To operate ALL parameters and gain complete access select F4 Press the Enter key twice and enter 444 7 5 5 2 F2 Change Password The passwords can only be changed if you are in access level 4 After F2 enter your new 3 digit passwords California Analytical Model 600 HCLD C_ETL_US CE Operators M March 2006 Page 27 of 71 Section 7 MAIN MENU IMPORTANT TIP You MUST remember and record this new password If this is lost you will need to consult the factory fo
11. 3LOWSY_S 3 NYYOLNY S SY NYdS SYO JIdJNYS syo 0432 yaONVE_S S3ONVE_S Z3ONVYH_S LSONVYe S Wov1 _N39 Wavy Wo Wav ZO WHVIW LO Sags rl_das l_das zV das LE dais OL das 6 das 3 das MONIC OD _ EdaS J NYYOLNY O g das voa S das VPSONVE_O y_das CAONVE_O daS ZAONWY_O zaas FSONVYO Wags CHS to Ol TANVd OVE E g A z S e Sea Ee E l fi NR E EE LIOA7Z_Od3 Oldi JOA Od3 Lass dws d1 Xivada JESH dL WYS3d3 438 AGL 334M0 uvoda dWaL_dWnd dS L_LYAO dWal 1139 diNSL_NAAO JAWIL EHN Z dwal ZO aog JAIL NITIH _ SVO TWS dWal Zo a 1HvYH dL dWaL ZO 13d aL lno zo GNOVY di A IJ NYY dWal3d0iG CJONYY LNO AGE 0 Z3ONYY amp YAINOLIANOS TWNOIS LIMS ON S wos _ MOTJO S JLOWJN S _ J NYYOLNV S SYD NVdS SV ONaZ PaONVe_S I NYY S ZAONVY_S LONVY S A NAVIY N39 navi yo way ZO wav LO SL_das PL das el das gt ZL_ddS ANTWA YALYSANOD LITdaS SATVA MO1SYSAO Ol das JAYA ANC LEM 6 das 2 8748S gods fdas Zoas g das gods g das sods p_das voas das e oas zaas zoas das Loads LYWHO dL tad dL GNOV dl Aavv N29 B Wav IY IYO E Wavy Zo Navi O 13M S ON S WOLS MOTOTS BLOWSBY_S FONVYOLNY S elas we zlas bias SY99 NVdS g vaONvy SVO dIdWVS eSONVY SVO OXYJZ g CAONVY _ ONO ANWA_YSLUSANOD 13M9 SAIVA_MO1NSAO NVdS J SAIWA ANC LIM oYaz TWOOLAW_O INNT MOTO O FONVYOLNY_O Wol
12. J31 Fan Power J32 J33 Chiller Power J34 J35 Detector J36 J37 Thermocouple J38 JP1 PGA Zero NOTE Connections are clearly labeled on the PCB California Analytical Model 600 HCLD C_ETL_US CE March 2006 Test Points EPC Air Valve Digital Output 2 DIDO Board Sample Transducer Spare Digital Output Main Back Panel NO NOx Valve Span Valve Zero Air Transducer Daisy Chain Input 1 DIDO Board Chiller Out Spare Analog Input Spare Back Panel Daisy Chain Output DIDO Board Relay Board Power O2 Detector RTD Page 41 of 71 Operators Mi Section 8 ANALYZER COMPONENTS 8 5 Reaction Chamber To Pressure Transducer Exhaust Inverting Amplifier M Power y 4 J Main Board Gain Zero Connection Adjust Adjust Reaction Chamber Pre Amplifier California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 42 of 71 Section 8 ANALYZER COMPONENTS 8 6 Relay Board Connections J32 Connects to Main Electronic Board J32 a4 oj qz 3 i gt i i Relay Board Connections J1 AC Input J2 Power Supply 1 J3 Power Supply 2 J4 Power Supply 3 J5 Ozone Lamp J6 Pump Power J7 Cell Heater J8 Oven Heater J9 Converter Heater J10 Pump Heater J11 Optional O2 Heater J12 Optional NH3 Heater J13 Aux J14 Aux California Analytical Model 600 HCLD C_ETL_US CE March 2006 Operators Mi Pa
13. March 2006 Page 50 of 71 Operators Mi Section 13 APPENDIX 13 Drawings 13 1 AK Protocol 13 2 Rear Panel Connections 13 3 Flow Diagrams 13 4 Block Electrical Drawing California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 51 of 71 Section 13 APPENDIX 13 1 Serial Interface and AK Commands The serial interface enables remote control of the Model 600 analyzer by a master computer It is implemented as an RS232 V24 interface and meets all requirements of the AK protocol A 9 pin male connector at the back of the unit is used to connect a master computer with the following pin assignment Pin 3 Txd transmit Pin 2 Rxd receive Pin 5 Gnd ground Interface Parameters Baud rate 9600 4800 2400 1200 600 300 baud Data bits 7ors Stop bit 1or2 Don t care 1 byte adjustable e g 32 Parity Even odd none XON XOFF Active or not active General AK Requirements If the command message contains no error the acknowledge message contains the echo of the function code and the error status number 1 to 9 If the transfer was faulty or the function code unknown the answer contains four question marks example 0 If the displayed value is not valid a is placed in front of the measured value example AIKG 0 9999 If a control or adjusting command is sent via the serial interface while the measuring device is in Manual mode it sends an answer like SLIN 0 KO
14. SMAH Z Manual Span 1 SARA B zero gas Use F3 To Toggle Span gas Use F3 To Togale Diagnostics Cal Wia Diagnostics Cal Wis Using Current Temp amp Press Using Current Temp amp Press 2ee Sayed Currente Outside Deviation Limits HOX 0 00 Rangel OO Oppm HO C kang B HOx 0 0 Fi Save value HOx Oo 1 ari al emu 02 My A F2 Man al Menu 02 0 0 4 Thu Mar 15 O68 F 16 17 2008 F Th 2 The above is shown using Zero Gas From Measurement use F5 Zero or F6 Span From Main Menu use F4 F2 F1 Zero or F2 Span California Analytical Instruments Model 600 HCLD Operators Manual January 10 2011 Page 20 of 24 ADDENDUM 4 2 Calibration Deviations MAIN F5 F2 F2 Deviations F3 Measuring Deviations 5 SHET a eee zl Deviations Measuring deyviatioanle dl oe eee ETE 1 00 i 1 OD ig HO O O Note These screens are used by the operator to define the maximum acceptable limits of the Zero and Span gas for both Manual and Automatic Calibrating 4 3 Flow Zero or Span Some analyzers have the above and the ability to flow Zero and Span Gas pete eee e EMAN EI Manual calib 1 SARA apai pan Cal Span 0 08 0 08 oggle zero F 4 Toggle span ZERO SPAN FS Measurements FS Cal zero OF F93 Cal Peo o2 Fe Range Pp Fr Range Down N x oo E i Dzi GO E ra z F CAI Tel 800 9353 0959 F Thu May 15 6 22 23 2008 The above is shown using Zero SPAN Gas From Cal Scre
15. 1 Baud from 300 to 9600 bps can be selected via the display 2 or 8 data bits 1 or 2 stop bits and the parity yes no 3 The data transmission is full duplex no echo with XON XOFF protocol 4 The don t care byte byte 2 is adjustable factory setting 20H Command Format lt STX gt 02H Example ASTZ KO don t care any byte default 20H function code code 4 byte long e g ASTZ Space 20H 20H channel N always KO for the analyzer space 20H only if followed by data otherwise lt ET X gt data data bytes depending on the commana lt ETX gt 03H Answer Format lt STX gt 02H Example STZ 0 SREM STBY don t care adjustable factory setting 20H function code same code as command package e g AST Z space 20H status O without error or 1 to 9 when error see also ASTF command space 20H only if followed by data otherwise lt ET X gt data parameter depending on the command lt ETX gt 03H Scans AKON Measured concentration value Command Response Description _AKON_KO _AKON s Z z y y_x x_wW W Measured concentration value is responsed z z current Measured Value y y NO x x NO2 w w Nox y y X X w W are only used in dual measure mode Otherwise O O will be returned AEMB Set measuring range California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 53 of 71 Section 13 APPENDIX Command Response Description _AEMB_KO _AEMB_s Mn Current measuring range is respon
16. 15 PSIG to a pre set capillary and consequently accurately predetermines the ozone flow rate The air supply cylinder should be set to 25 psig The sample is presented to the reaction chamber via a precision factory set electronically controlled proportional pressure valve through a capillary This pressure is factory set at approximately 3 85 PSIG A close coupled by pass capillary minimizes dead volume and improves response time Sample inlet pressure and regulated air pressures are monitored by internal pressure transducers and presented in PSIG via the diagnostics screen NOTE The correct pressures are determined by the factory for optimum analyzer performance and measured by N I S T traceable standards They are recorded on the Factory Settings Screen California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 47 of 71 Section 10 FUNCTION DESCRIPTION 10 4 Main Electronics Board The main electronics board contains the instrument power supplies and required instrument electronics A single transformer provides power to the main circuit board and includes provisions for 110 220 VAC at 50 60 Hz input 10 5 Relay Board The relay circuit board contains the logic circuitry required to control and switch the AC power to the required heaters and sample pump California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 48 of 71 Section 11 REACTION CHAMBER 11 Reaction Chamber 11 1 Disas
17. Analyzer Without Internal Heated Sample Pump California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 66 of 71 Section 13 APPENDIX To PEED 0 GN Or ERO L lt gt Kl BYPASS 2 sy CVI aea RI R2 SPAN gt lt O gt lt oy SV CONVERTER A RO IC rO R5 AIR 02 OA PH S DETECTOR BETZ E ARAUT ME 1 i SAMPLE Q H NOTE Standard Analyzer With LOW FLOW OPTION California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 67 of 71 APPENDIX Section 13 Fh SW PEATED OVEN 65 C a P lt 3YPASS C ayn G EPEY R3 RA IC R2 SPAN gt lt gt lt SS SANIP TE COOLER NOX CONVERTER DA AT IN z3 PRI PT at DRAIN A Bry d a ane
18. Channels output Hode I I mA Output hel cm Output Ranges California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 31 of 71 Section 7 MAIN MENU 7 5 7 5 F5 Turns Status Line On or Off The status line displays the AK Protocol action on the top line of the display Status Line System setup 23 SB Y Select Language 7 5 7 7 F7 Automatic Setup This screen brings up the automatic startup parameters If activated the analyzer will automatically start up the autocalibration cycle upon power on The function is toggled on and off with the Enter key The cycle timing number of cals range and NO Nox mode may be set After calibration the analyzer enters the sample mode and outputs a digital signal This is very useful in unattended applications 7 E MEZA T i minutes a HO x AU We ma au St H 3O cto t i x t a 7 _ Automatic Startup Parameters California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 32 of 71 Section 7 MAIN MENU 7 5 8 F8 Measure Settings This screen allows several of the system settings to be displayed and modified setup purge and measure time for dusl mode Wed Jan 29 13 26 12 2003 F Menu Settings Screen 7 5 8 1 F1 Set NO2 Mode Times et times Z purge time wa measure time Set NO2 Purge and Measure Time 7 5 8 2 F2 Converter Efficiency F2 on the Men
19. KO AKAL s M1_z z_y y_x x_w w Deviation ppm _AKAL_s M2 z z _y y_x x_w w _AKAL_s M3 z z _y y_x x_w w _AKAL_s M4 z z_y y_x x_w w ASYZ Respond System Time Command Response _ASYZ_K0O_ _ASYZ_s_yymmdd_hhmmss AT90 Respond Lowpass filter time Command Response _AT90_KO_ _AT90 s t ADAL Diagnostic alarm limits Command Response ADAL KO _ADAL_s_ai min_al max_ _f12 max _ADAL_KO x _ADAL_s_ x min_x max Alarm Limits Sample Pressure California Analytical Model 600 HCLD C_ETL_US CE March 2006 z z Zero gas relative to last calibration y y Zero gas factory calibration X X Span gas relative to last calibration w w Span gas factory calibration Description Respond system time yymmdd year month day each 2 characters wide no spaces hhmmss hour minutes seconds Description Respond lowpass filter time t filter time in seconds Description All alarms are responded Alarm limits of x Operators Mi Page 57 of 71 Section 13 Oven Temp Converter Temp Pump Temp Diode Temp Cell Temp Peltier Gas Temp EPC Coil Sample Voltage EPC Coil Air Ozone Voltage Reserved Sample Content ATCP Query TCP IP settings APPENDIX Command Response Description _ATCP_KO _ATCP_S 22Z 22Z 22Z 2Zz zzz TCP IP Address _ATCP_s_yyy yyy yyy yyy _ATCP_s_ XXXX AENT Query calibration gas flow setting yyy TCP IP subnet mask Xxxx TCP IP port Command Response Description _AENT_KO _AENT_s x x 10 Calibration through sa
20. Key p12 F1 Measurement F2 Range Select F3 Diagnostics F4 Calibration F5 Setup F6 Remote Manual F7 Standby F1 Toggles Between NO amp NOx p15 F2 Toggles on NO NO2 p15 F3 Displays Diagnostics Screen p16 Arrow Keys Cycle Ranges 1 4 and Auto Range p17 F1 NO NOx F2 Dual Mode F3 Diagnostics Up Down Range gt Purge Analyzer F2 Sets Analyzer in Purge Mode p18 Displays Diagnostics Screen F3 p15 F1 Auto Cal F1 Starts Auto Calibration on Range in Use p19 F2 Manual Cal F2 Zero Cal Span Cal Change Range p20 F3 Display Deviations F3 Displays Deviations p21 F4 F4 Check Calibration F4 Calibration Check p22 F5 Reset Cal Values F5 Reset to Factory Default p22 F6 Range Select F6 Range Change p22 F1 Span Gas Concentrations F1 Sets Calibration Gas Values p24 FO Fie AA Settings F2 Sets Auto Calibration Times p24 F5 F3 Range Limits F3 Sets Upper Range Limits p25 F4 Alarms F4 Set Range Concentration Limits p26 F5 Password F5 Sets User Password p27 F6 Linearization F6 Enters Curve Fit Polynomials p28 F7 System Settings F7 Displays System Settings p29 F8 Measure Settings F9 Displays Measure Settings p33 F10 Displays Version F10 Displays Converter Efficiency 034 Activates Remote or Manual Control Manual Local Control p36 F6 In Standby Sample Pump is OFF Toggles Pump ON OFF p36 F7 California Analytical Model 600 HCLD C_ETL_US CE Operators M March 2006 Page 10 of 71
21. R5 PT2 C EXHAUST Er P 1 MFI SAM NOTE Standard Analyzer With Internal Heated Sample Pump and Rear Mounted Chiller California Analytical Model 600 HCLD C_ETL_US CE March 2006 Page 68 of 71 Operators Mi APPENDIX Section 13 o ay HEATED OPN BoC FRO LX _ gt rt i i TEAS Gyo Owl CPO RZ R4dIC R2DIC OFANA D lt i e SAMPLE COOLER NOX o CONVERTER gt 7 IN 2 PRI aur DRAIN an pe Cy RS R4 R 02 lt A wo IEC e PT2 CVO EXHAUST MEI SAMPLE IK gt NOTE Standard Analyzer Without Internal Heated Sample Pump and Rear Mounted Chiller California Analytical Model 600 HCLD C_ETL_US CE March 2006 Operators Mi Page 69 of 71 APPENDIX Section 13 13 3 Electrical Block Diagram SLNANNYLSNI TWOILATYNV VINNOSIIVS SLNIOd LS3L Ir SLNIOd LS3L zr GOH 009 oa TKNOTNOOMDD TANMOMTNOKR DHS i LYVHO dL iad dL Lno zo LIOA_2_Oda LOA 1 Oda HOldL LISHI dL FLAS INS dL TAO St 13M7S ON_S wos MO1407S
22. The Air O2 flow is controlled by an EPC valve It requires 25 psig cylinder supply pressure and is factory set to deliver approximately 10 to 20 psig to the ozone capillary This pressure may be monitored by the diagnostics meter The flow rate from the capillary is very low and will require a bubble flow meter to accurately determine proper flow 12 2 Sample Supply The sample flow is controlled by an adjustable electronic proportional pressure valve This valve requires a 10 to 25 PSIG sample supply pressure to deliver the proper pressure to the sample capillary This pressure may be monitored by the diagnostics meter at any time after inlet sample has been applied The sample flow rate from the capillary is very low and will require a bubble flow meter to determine proper flow rate If the pressure is properly set and a clogged capillary is suspected replace the sample capillary NOTE lf the analyzer contains an optional internal sample pump the introduction of a pressurized sample gas in excess of 1 5 PSIG will damage the pump 12 3 NO NOx Converter Several published test procedures require periodic NOx efficiency tests to be performed on the converter to determine NO2 to NO conversion efficiency utilizing a NOx generator The CAI Model NOxGen may be used for this procedure A short test using NO2 calibration gas Is also defined in the U S Federal Register Title 40 Part 86 332 79 e California Analytical Model 600 HCLD C_ETL_US CE
23. User Defined NO Relay 2 User Defined NO Relay 3 User Defined NO Relay 4 User Defined NO Relay 5 User Defined NO Relay 6 User Defined NO Relay 7 User Defined NO Relay 8 User Defined NO Relay 9 User Defined NO Relay 10 User Defined NO Relay 11 User Defined NO Relay 12 User Defined NO Relay 13 California Analytical Instruments Model 600 HCLD Operators Manual January 10 2011
24. alarm limits _EDAL_KO_x_x min_xmax _EDAL s Set alarm limits of x Alarm Limits 7 10 1 Reserved California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 62 of 71 Section 13 APPENDIX Sample Content ETCP Set TCP IP Parameters Command Response Description zzz TCP IP address _ETCP_KO_22Z 22Z 222 2zz _ETCP_s _ETCP_KO _ yyy yyy yyy yyy yyy TCP IP subnet mask _ETCP_KO_xxxx xxxx TCP IP port All changes take effect after next power on cycle Abbrevations used Mn Measuring range number M1 M4 Measuring Range 1 4 W W Z Z Numerical value X Number t Numeric integer value a0 a4 Polynom coefficients S Status yyymmdd Date of format year month and day with 2 characters each and no spaces hhmmss Time of format hour minute and second with 2 characters each and no spaces California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 63 of 71 Section 13 APPENDIX 13 2 Rear Panel Connectors 28 Pin Main Connector Assignments Signal Type oin Analog GND analog Realtime 0 10 VDC Maximum NO 0 10 VDC Maximum NOx 0 10 VDC Maximum NO2 0 10 VDC Maximum GND Digital sense AutoRange Sense Range 1 Sense Range 2 Sense Range 3 Sense Range 4 set AutoRange Control Range 1 Control Range 2 Control Range 3 Control Range 4 Auto Cal Calibrate Zero Span Pump Span Gas Flow Sample Gas Flow Local Remote Read Cal M
25. analyzer contains the optional sample pump do not apply a pressurized sample The optional pump is capable of drawing a sample through a 1 4 inch heated sample line of approximately 75 feet The calibration span gas cylinder pressures should be set at 25 PSIG for delivery into the optional zero and span inlets located on the rear panel California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 7 of 71 Section 3 INSTALLATION 3 8 6 Sample Gas Bypass Outlet Vent A sample gas bypass outlet connector is located on the rear panel 1 4 Inch Tube Pressure at this outlet should be kept at atmospheric level ANY backpressure will Cause an error in reading The vent outlet is located on the rear panel and may contain high levels of ozone which should be vented away from the instrument California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 8 of 71 Section 4 BASIC OPERATION 4 Basic Operation The operation of the digital microprocessor conforms to the guidelines of the AK committee Originally developed in the German automotive industry Via the serial port of the MSR Card the analyzer can be remote controlled by a master computer The serial communication fully corresponds to the specifications of the AK protocol TCP IP communication is also available 4 1 Display The analyzer s LCD display can show 16 lines with 30 characters each The display also has background lighting that can
26. be switched on and off via the Display key on the keyboard The following example shows the measurement screen which is formatted into 4 information areas Measurement s Auto Rangel 0 100 ppm Mona Jan 27 15 23721 2003S Measurement Screen THE TOP INFORMATION AREA CONTAINS The AK Protocol Information This capability is for advanced uses and may be toggled on and off in the setup screen F5 Next to the symbol for the active operating mode the device status is indicated The status field is also displayed on all other screens SARE Autorange enabled SMGA Measuring gas is flowing SMAN Device is in manual operation status The level of Password Entry is shown on the right with 4 horizontal lines THE LARGE INFORMATION AREA CONTAINS The Concentration of the gas sample and mode of operation THE THIRD INFORMATION AREA CONTAINS The help information for the parameter selected ranges etc THE LOWER INFORMATION AREA CONTAINS The the time amp date and any error condition The symbol in the bottom right corner indicates the keyboard mode In the example shown the keyboard is in the function key mode For input fields the mode is usually switched to numerical input Then an N appears in the lower right of the screen This symbol is displayed on all screens California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 9 of 71 Section 4 BASIC OPERATION 4 2 Menu Tree Main Menu from Main
27. electronically excited state This reaction is immediately followed by reversion to a non excited state and emission of photons The photons impinge on a photodiode detector PHOTODIODE which generates a low DC current directly proportional to the NO contained in the sample gas This current is amplified by a precision electrometer and presented to digital panel meter and recorder output In the NOx mode the sample is first routed to the NOx converter where the NO2 component is reduced to NO The complete sample is analyzed by the PHOTODIODE as above The instrument contains heated sections which keep the sample at approximately 100 degrees C prior to the reaction chamber All temperatures are measured by N I S T traceable standards 10 2 Reaction Chamber The sample and ozone are delivered to the reaction chamber via the unique regulated flow system described below The sample and ozone are mixed together at the center of the chamber where the reaction takes place The sample is vented from the chamber through a 1 8 inch stainless steel tube The chamber contains a red filter which is sealed with an integral O Ring The chamber assembly is O Ring mounted to the PHOTODIODE The complete chamber and PHOTODIODE assembly is housed in an RFI shielded enclosure 10 3 Flow System The basic function is to deliver highly regulated flows of sample and air or O2 to the ozonator and reaction chamber assemblies An EPC valve delivers air at approximately
28. is on NOx is measured NMessurements Auto Rangei O 100 ppm Monedan or 15 27 1 ous Measurement sScreen 7 1 2 F2 NO NOx Measurement The F2 function activates the hold and sample feature which allows the analyzer to automatically switch between NO and NOx measurement The time duration for the sample read is set up in the Setup Menu The analyzer will read and display the NO converter is bypassed value At the predetermined time it will switch to the NOx mode through converter and read and display the NOx value while the last 15 second NO average is displayed The top value will be real time values and will change between NO and NOx The difference between the two average values is shown as NO2 All three values are sent to the analog and digital outputs California Analytical Model 600 HCLD C_ETL_US CE Operators M March 2006 Page 15 of 71 Section 7 MAIN MENU Measurements NO NOx NO2 Screen 7 1 3 F3 Diagnostics F3 activates the diagnostic screen where pressures flow rates temperatures and EPC control voltages are displayed in real time The units are psig degrees C ml min and voltage Use the arrow key to switch between diagnostic screens Second Diagnostics Screen California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 16 of 71 Section 7 MAIN MENU 7 1 4 Range Select With the arrow keys the ranges 1 to 4 can be selected and locked in which w
29. selected and set to a HOLD or CLEAR mode In the HOLD mode an activated signal is retained until the operator returns to the Digital Output Screen and selects the appropriate output signal and performs a manual CLEAR After performing a Clear Operation the operator must press F2 again to put the outputs back into the Hold mode User DO I 4 SEHO ee EE 5et Unused Channels OF fF Se E EEEE Clear 2 15 DOts HO O 1 H CK to SAVE 02 O 0 z E I ra m i 0i 40 397 2001 F z1 T Dj THe TNA In the CLEAR mode the signal will automatically change state when the microprocessor detects that the noted condition no longer exists User DO II S SDR Z 3 Of fF J Off 16 off ii Hes Oe Ly OF Zet Unused 13 Off Channels Of F i4 off SE EEEEEEE 15 ii Fi to T DOs HO Oo 1 MAIN BACK to SAVE O27 D D z CAI Tel 500 959 0959 F California Analytical Instruments Model 600 HCLD Operators Manual January 10 2011 Page 15 of 24 ADDENDUM The operator can select from the following the desired SERVICE or STATUS groups that are to be digitally monitored Index CO NO OF OO N 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 26 TABLE B Service Group Sample Pressure Failure Air Pressure Failure Oven Temp Failure hcld only Converter Temp Failure Pump Temp Failure Diode Temp Failure Cell Temp Failure Peltier Gas Temp Failure hcld only O2 Tem
30. the electronics cover The chiller has a 1 4 inch drain which MUST be held at a bleed pressure either through an external peristaltic pump or needle valve Drain flow rate of 10 ml min should be sent to facility drain An optional Wet Dry switch is available CAUTION Never supply a wet sample to a cold analyzer as damage may occur 9 Sample Pump If the analyzer is supplied with the optional internal heated sample pump it is always on in the measure mode It is turned off during calibration and may be manually turned off by putting the analyzer in standby 10 Heated Sample Line Make certain the heated sample line is up to temperature and flushed before connecting to the analyzer sample inlet 11 Instrument Power Turn instrument power on and allow the oven temperature to stabilize before turning on the sample pump and or connecting the heated sample line California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 45 of 71 Section 9 OPERATION 12 Sampling System Prepare and check the sample system Check the sample pressure as indicated in the factory settings screen 13 Air or O2 Pressure Check the Air O2 pressure for proper setting as indicated in the factory setting screen Readjust internal pressure as required Note Cylinder pressure should be set at 25 PSIG 14 Zero amp Span Calibration Zero and span adjustment should be checked every 24 hours by either manual or automatic calib
31. value for the lower ranges is zero calibration parameters will be copied to this range To calibrate all ranges with the same span gas you must enter the gas concentration in the Span Gas Calibration screen for ALL RANGES You must also calibrate each range Offsets and scalors are NOT copied to other ranges ET lel in PYARQYSBBe Gee anu nagl ca rt 1 bre tina 4 r ope pem 2S ONS Lai ses Sug f Min E rm 5 Auto Calibration Screen 7 4 2 F2 Manual Calibration From the Calibration screen F2 starts manual calibration If auto range is selected calibration is not possible and the appropriate range can be selected In the manual calibrations menu three options are possible F1 Flow zero gas F2 Flow span gas F3 Range select Manual Calibration Screen When zero or span gas is flown the measured value can be saved by pressing F1 If the screen is left by pressing the buttons Main or Back the measured value is not saved Solenoids are closed by pressing F2 From the manual calibration menu the range to calibrate can be chosen by pressing F3 California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 20 of 71 Section 7 MAIN MENU Manual calib Manual calib 0 c0 NO Rangel 100 ppm Rangel 100 ppm pave Value 2 Close zero gas solenola 2 Close span gas solenoid Tue Jan 28 08 16 03 2005 merjan 20 08 Lo ss 2003 Manual Zero and Span Calibrat
32. 6 1 User Functions Level 1 Main Menu F5 Setup F5 Password F1 Measurements F5 Password F1 Enter password F2 Purge Analyzer F10 Version F3 Diagnostics F4 Calibrations F5 Setup F7 Standby 6 2 Advanced User Functions Level 2 Main Menu F5 Setup F5 Password F1 Measurements F3 Range Limits F1 Enter password F2 Purge Analyzer F5 Password F3 Diagnostics F10 Version F4 Calibrations F5 Setup F7 Standby 6 3 Maintenance Functions Level 3 Main Menu F5 Setup F5 Password F7 System Settings F1 Measurements F1 Span Gas Conc F1 Enter password F1 Real Time Clock F2 Purge Analyzer F3 Range limits F2 Reset password F5 Status Line on off F3 Diagnostics F5 Password F7 Auto Startup F4 Calibrations F7 System Settings F5 Setup F8 Measure Settings F7 Standby F10 Version 6 4 System User Functions Level 4 All Function described in this manual may be accessed from Level 4 California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 14 of 71 Section 7 MAIN MENU 7 Main Menu Function Descriptions 7 1 F1 Measurements A m wv Ti LL 3 Re St 7 1 1 F1 NO or NOx Measurement The measurements screen is activated by pressing F1 on the Main Menu screen The NO NOx content is displayed in ppm Pressing F1 switches between measuring the sample gas for NOx or NO only When the converter is off only NO is measured When the converter
33. 8 of 24 ADDENDUM 3 3 Offset amp Gain Main F4 F3 F5 Offset and Gain B zero Span applied correction R Boe i gaan Rangel a Ronee MT 1 G Rangest Oo OO 1 90 Ranged fb OO i OO Thu Mayr 83 12 40 03 2007 F This screen can be used to provide an additional means to display calibration deviations The OFFSET is the value stored during zero calibration The GAIN is the value stored during span gas calibration using the operator defined calibration gas An increasing or decreasing change to the OFFSET or GAIN when used in conjunction with Deviations will provide insight to both short and long term changes to system performance Note Reset calibration values will reset OFFSETS amp GAINS to zero and 1 respectively 3 4 Calibrate the Analog Outputs Main F5 F7 F8 D A Calibration Main F5 F7 F3 Output Assignment e Overview The 600 CLD Series is designed to provide four analog outputs that can be configured as 0 1 VDC 0 5 VDC 0 10 VDC 4 20 mA or 0 20 mA This screen Main F5 F7 F8 is used to select the scaling of the current mA or voltage 1 5 10 range that is required by a remote recording device The outputs can be calibrated to exactly match the results obtained on a PLC Recorder Data Logger or other remote recording device that may be connected to the analyzer The operator will first select the OUTPUT ASSIGNMENT Main F5 F7 F3 screen and choose the output that is set
34. AIN NUSER OSMSR Device info Air Pressure Failure F Software Version 7 6 F7 Remote Manual Control The analyzer can be remote controlled by either a master computer or via contact closures The TCP IP and serial communication fully corresponds to the specifications of the AK protocol To change remote manual control press F6 in the main menu This toggles between remote and manual control mi a iT ul art gue Ti Do Tore K me TH ieee iii aS iz may i ut 7 7 F8 Standby Main Menu Fi Measurements pv Purge analrzei FS Diagnostics F 4 Calibrations gt ES Setup gt F Remote Manual gt rr Stands Sia Standbyr mode Tue Jan 28 12 20 10 2003 Main Menu User Level 4 In Standby mode pump is turned off and the solenoids are closed The CAI logo is displayed California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 35 of 71 Section 8 ANALYZER COMPONENTS 8 Analyzer Components 8 1 Rear Panel The following details the rear panel connections Ny ns SF Gye ep oe e Figure 32 Rear Panel om Sample Gas Inlet Feeds sample gas to the analyzer 1 4 Inch Tube Sample Gas Bypass Outlet Vent Exhaust for sample 1 4 Inch Tube Ozone Air Inlet For feeding hydrocarbon free air or oxygen to the ozone generator Power Entry Module Power connection power switch fuse compartment 2 Amp Rear Panel Power ON OF
35. AP Addres ee ee ee eee 31 10 11 12 7 9 7 3 F3 Output Signal Assignments 31 7 9 9 4 F4 Output Ranges 31 TOAD F5 Protocol On Off 32 7 9 7 6 F6 Set Langauge 32 TOLT F7 Automatic Setup 32 7 0 8 F8 Measure Settings 33 7 9 8 1 F1 Set Purge Time Before Measure 33 7 5 8 2 F2 Set Converter Efficieny 33 7 9 8 3 F3 Set Time Constant 34 7 9 8 4 F4 Set Purge Time Before Calibration 34 7 5 10 F10 Display Software Version 34 35 7 6 F7 Remote Manual Operation 35 77 F8 Standby 29 20 22 n nnn nnn nnn nnn nn nnn nnn nnn nnn nnn nnn nnn nc enna 35 ANALYZER COMPONENTS 2 2 2 220 20 2 36 8 1 Rear Panel Connections 37 8 1 1 Main Analog Connectio
36. ATK Start automatic calibration Command Response _SATK_KO _SATK_ _SATK_KO Mn _SATK s SEMB Set measuring range Command Response _SEMB KO Mn _SEMB s SARE Auto range on Command Response California Analytical Model 600 HCLD C_ETL_US CE March 2006 Description Switch chiller on Description Start automatic calibration of all ranges Start automatic calibration using range Mn Description Set measuring range Autorange is disabled Description Operators Mi Page 59 of 71 Section 13 APPENDIX _SARE_KO SARE_s Set auto range on SARA Auto range off Command Response Description _SARA_KO SARA s Set autorange off SREM Remote mode for AK commands Command Response Description SREM KO SREM s SMAN Manual control to control device manually Set device in remote mode Command Response Description _SMAN_KO _SMAN s Set device in manual mode SMGA Start measuring Command Response Description _SMGA_KO _SMGA_s Start measuring SNKA Saves measured value as new offset Turn on pump for sample gas Command Response Description _SNKA_KO _SNKA_s Saves measured value of actual range SEKA Saves measured value as new span value Command Response _SEKA_KO SEKA s SENO Converter off Command Response SENO KO SENO s SNOX Converter on Command Response _SNOX_KO _SNOX_s SNO2 Converter on Command Response _SNO2_KO _SNO2_ gt s California Analytical Model 600 HCLD C_ETL_US CE March 2006 as new offset if z
37. Archiving Time F5 F7 F1 F5 Use ENTER to change record time User Digital Outputs F5 F9 e MODIFICATIONS Saved Not good F4 F2 F1 or F2 To flow Zero or Span Gas California Analytical Instruments Model 600 HCLD Operators Manual January 10 2011 Page 2 of 24 ADDENDUM 2 0 OPERATION OF MEASUREMENT KEYS Note The amp Keys continue to be used to view a complete list of menu items 2 1 Over Range 888888 In the MEASUREMENT mode only any value that exceeds the range by more than10 will be displayed as 888888 2 2 Diagnostics Use F3 to toggle between MEASUREMENT and DIAGNOSTIC 2 3 Zero From the MEASUREMENT Screen select the required range for calibration then press F5 Note For instruments with an internal Zero Solenoid select Calibration by Valves Main F5 F2 F4 Manual Zero 4 SENO B Manual zero 3 SMAH EI Zero gas Use F3 to Toggle zero gas Use F3 To Toggle Diagnostics Cal Wia Diagnostics Cal ia Using Current Temp amp Press 375 00 Ho HOx a R i 100 0 Range4 3000ppMm ange PPM em E ee Oo 1 an al enu 0z Ba B x H i Thu May 15 06 15 11 2008 ia HO an Ca Ov Check Air EPC Coil VW 2 versions Zero Gas will be enabled and the observed results can be used to evaluate instrument performance Press F3 to toggle to the Diagnostic screen for additional information Press F1 to save the value and complete a ZERO calibration for this channel and range Press MAI
38. Chl Zero Temp Set RP2 EPC 9 5V Air Set RP11 Chiller Span Temp Set RP3 O3 Cutoff RP12 Chiller Temp Set RP4 Cell Temp Set RP13 12VDC Adjust RP5 Oven Temp Set RP14 Sample Pressure Set RP6 Pump Temp Set RP15 Air Pressure Set RP7 Converter Temp Set RP16 Not Used RP8 O2 Temp Set RP17 Not Used RP9 NH3 Temp Set RP18 Coarse Zero Adjust NOTE Potentiometers are clearly labeled on both sides of the PCB California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 40 of 71 Section 8 ANALYZER COMPONENTS 8 4 Main Electronics Board Connectors Test Points Clearly Labeled Voltage Output at qii A A SEN mia f ka kd gt gt gt g T Tiy l EJ ee i m e REF Jsi n DAST LEER gt t a aa z ig Rap Eat Boone m be d Sii iliii Hiii IRI Uiit yi Resistor Stand Offs l K tte a a Ss r r hter s mi qi i eT ES i nn Maj tw rh et rit sh te ae ler ewe ken E ie Pi i EHHHETT Main Electronic Board Connectors J1 Test Points J2 J3 Test Points J4 J5 Test Points J6 J7 EPC Sample J8 J9 Aux Back Panel J10 J11 Diluter J12 J13 Digital Input 2 J14 J15 Diluter Transducer J16 J17 Digital Output 1 J18 J19 Aux Power J20 J21 Sample Overflow Valve J22 J23 Wet Dry Valve J24 J25 5 Volt Detector J26 J27 Chiller Temp Sense J28 J29 Spare Digital Input J30
39. F Switch Turns ON OFF line power to instrument Zero Gas Inlet For feeding hydrocarbon free zero air to the analyzer Span Gas Inlet For feeding calibration gas to the analyzer Vent Exhaust from reaction chamber 1 4 inch tube fitting eo oO NN Po fF YS N Output Connectors Analog Outputs and Remote Functions 10 TCP IP Connection Connect Network Connector 11 Serial Connector Connect Serial Connector 12 Filter Analyzer Filter Housing California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 36 of 71 Section 8 ANALYZER COMPONENTS 8 1 1 Main Connector Standard 28 Pin Connector a 5 OONOORWNDN in OONOOaRWND Signal Function Pin Analog Output Ground Analog 15 Analog Output Realtime 16 Analog Output NO 17 Analog Output NOx 18 Analog Output NO2 19 Digital Output Digital Output Ground Digital sense AutoRange 21 Digital Output Sense Range 1 22 Digital Output Sense Range 2 23 Digital Output Sense Range 3 24 Digital Output Sense Range 4 25 Digital Input set Auto Range 26 Digital Input Control Range 1 27 Digital Input Control Range2 28 Signal Digital Input Digital Input Digital Input Digital Input Digital Input Digital Input Digital Input Digital Input Digital Output Digital Output Digital Output Digital Output Digital Output Digital Output Function Control Range 3 Control Range 4 Auto Cal Calibrate Zero Span Pump Zero Gas Flow Span
40. F9 to select the first seven outputs Use the to select the desired output Press ENTER and use to select desired item Press ENTER to save selection Note The 600 CLD has 15 user selectable isolated digital outputs from the list of 40 in TABLE B amp C User DO I bi Press F1 to observe the remaining eight outputs Program as desired per the above User DO TAI S SDR Z 5 Off J Off i off ii off PEPEPEPE EEEE EEE i2 Off Set Unused Cag 13 Off Channels OFf 14 off Ce ee 15 EZS FE t to T D0 2 HO O 1 MAIN BACK to SAUE 02 0 0 CAI Tel 800 959 0959 F California Analytical Instruments Model 600 HCLD Operators Manual January 10 2011 Page 18 of 24 ADDENDUM 3 7 Cal Analog Output Main F5 F8 TEET Te r rag tim to oim mpensation LEER aye Limes Use F8 to toggle on off Normally during Auto Cal the Sample and Hold Outputs NO NOx and NO2 are held at the last process value If Cal Analog Output is set On then the values are not held and the Real Time value is Output California Analytical Instruments Model 600 HCLD Operators Manual January 10 2011 Page 19 of 24 ADDENDUM 4 0 CHANGES TO EXISTING FUNCTIONS 4 1 Saved or Outside Limits During Manual Calibration the following screens will be displayed to indicate the instruments response to the value of the zero or span gas using the amount that the operator defined in the deviation table Manual Zero 3
41. Gas Flow Sample Gas Flow Local Remote Read Cal Mode Reserved Reserved Auxiliary Connector Standard 28 Pin Connector Signal Function Pin Analog Input Ground 15 Analog Input External Analog1 16 Analog Input External Analog2 17 Analog Input Spare Analog 18 Analog Input Spare Analog 19 Digital Output Ground Alarm 20 Digital Output General Alarm 21 Digital Output Ch 1 Conc Alarm 22 Digital Output Ch 2 Conc Alarm 23 Digital Output Reserved 24 Digital Output Reserved 25 Digital Input Reserved 26 Digital Input Reserved 27 Digital Input Reserved 28 Signal Digital Output Digital Output Digital Output Digital Output Digital Output Digital Output Digital Output Digital Output Digital Input Digital Input Digital Input DI DO DI DO DI DO Function Ground Alarm Calibrate Alarm 1 Reserved Reserved Reserved Read Wet Mode Read Overflow Read NO Mode Set Wet Mode Set Overflow Mode Set NO Mode Spare Spare Spare 8 1 3 Digital Outputs RS 232 Standard 9 Pin DIN Connector Pin O o NOoQ QGAAOUON California Analyt March 2006 Function DCD Carrier Detect RxD Receive Data TxD Transmit Data DTR Data Terminal Ready Ground DSR Data Set Ready RTS Ready to Send CTS Clear to Send RI Ring Indicator ical Model 600 HCLD C_ETL_US CE Operators Mi Page 37 of 71 Section 8 ANALYZER COMPONENTS 8 1 4 Digital Outputs TCP IP 8 Pin RJ 47 Connector Pin Function TDX TDX RXD Ope
42. N F1 to return to the MEASUREMENT screen to select other channels and ranges and repeat the process Or press F2 to return to the Manual Calibration Screen California Analytical Instruments Model 600 HCLD Operators Manual January 10 2011 Page 3 of 24 ADDENDUM 2 4 Span From the MEASUREMENT Screen select the required range then press F6 Note For instruments with an Internal Span Solenoid select Calibration by Valves Main F5 F2 F4 Manual Span 2 SHET H Manual Span 3 SHET Z gran ga Use Fy i to Toggle Span gas Use F3 To Toggle iagnostics Ca Diagnostics Cal_Wia 3 7 5 0 0 Using Current Temp amp Press Cone 0 0 0 ae HO x Range4 S000PpPm Fangel i1 Fi Save valve 3454 9 Fi Save value NOx 0 0 F2 Han Cale Menu 02 F2 Man Cal Menu 02 0 0 F CAI Tel 800 959 6959 E 2 versions Span Gas will be enabled and the observed results can be used to evaluate instrument performance Press F3 to toggle to the Diagnostic screen for additional information Press F1 to save the new value and complete the SPAN calibration for this Range Note The span gas value used for this range is highlighted and can be changed if necessary Use the Enter key and the numeric keys as required Press MAIN F1 to return to the MEASUREMENT screen to select other ranges and repeat the process or press F2 to return to the Manual Calibration screen California Analytical Instruments Model 600 HCLD Ope
43. NOTE To change device identification you must first rename the device to RESET Now a name up to 40 letters can be given NOTE The device name must not have any blanks between f e CAl CLD is not allowed You can use undersline i e CAI_CLD EGRD Set polynom coefficients Command Response Description _EGRD_KO Mn_a0 al_a2 a3 a4 _EGRD_s_ Set polynom coefficients of range Mn California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 61 of 71 Section 13 APPENDIX EFDA Set autocalibration and purge times Command Response Description _EFDA_KO SATK_z yxw _EFDA_s Set autocalibration times z Purge time y Calibration time x Total calibration time w Verify time Z y X w in seconds _EFDA_KO_ SSPL z EFDA s Set analyzer purge time to z seconds EPAR Set autocalibration tolerance values Command Response Description _EPAR_KO_SATK_z z_y y_x x_w _EPAR_s Autocalibration Tolerance value Ww z z Range 1 y y Range 2 x x Range 3 w w Range 4 ESYZ Set System Time Command Response Description _ESYZ KO yymmdd_hhmmss ESYA s Respond system time yymmdd year month day each 2 characters wide no spaces hhmmss hour minutes seconds ET90 Set Lowpass Filter Time Command Response Description _ET90_ KO t ET90 s Set lowpass filter time t filter time in seconds EDAL Diagnostic alarm limits Command Response Description _EDAL KO_a1 min_a1 mas_ a12max _EDAL s Set all
44. OF If a channel does not exist the answer for control and adjusting commands is e g ATEM 0 3 NA in which 3 is the number of the sub channel If the device is busy with a running function SLIN for example every arriving control command is ignored except SRES and STBY and the response message Is e g SMAN 0 BS If In the mode SINT an additional SINT KO command is received the integrator is reset to 0 and the integration is restarted lf the command message contains data that the measuring device cannot process ESYZ KO ABC for example the response message is ESYZ 0 SE A syntax error is recognized if the data does not match the expected format or if the parameters do not fit the expected size Numbers are in floating point format with decimal point The decimal point can be dropped for integers If you switch from Manual to Remote at the device it remains in Manual mode until a SREM KO is received by the control computer On the display this mode is indicated by REME Remote enable on the status line In manual mode query commands via the serial interface are possible at any time California Analytical Model 600 HCLD C_ETL_US CE March 2006 Page 52 of 71 Operators Mi Section 13 APPENDIX AK Protocol Format The master computer and the Model 600 analyzer communicates via the RS232 serial link The Model 600 analyzer acts as a slave and only responds to commands Serial Interface Parameters
45. Ranges 265 100 200 Ranged 29325 roo soaa Change Span Gas Settings 7 5 2 F2 Calibration Settings In the calibration settings menu times deviations and methods can be changed Setup Z 7 5 2 1 F1 Times There are four times in seconds for auto calibration that can be changed Purge measuring calibration and verifying time Changes are made and saved as above California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 24 of 71 Section 7 MAIN MENU 7 9 2 2 F2 Measuring Deviations During auto calibration the measured value is only saved if it is within a certain time within an upper and a lower limit These two limits format a working window In the setup menu the deviation is in percent 7 5 2 3 F3 Deviations Here you can change absolute and relative deviation in percent After auto calibration it is checked to assure the deviations are within this limit If the deviations are not in this limit a warning Deviation error appears 7 5 2 4 F4 Calibrations via Valves Calibrations can be made by using the solenoids for zero and span gas or by using the pump Calibration via valves means that the zero gas is flown by the zero gas solenoid and the span gas is flown by the span gas solenoid 7 5 2 5 F5 Calibration via Probe Calibration via probe means that the zero and the sample gas is flown by the pump the solenoids for zero and span gas are not used 7 9 3 F3 Range Limits There are 4 di
46. VE OTHER RIGHTS WHICH VARY FROM STATE TO STATE Representations and warranties made by any person including dealers and representatives of CAI which are inconsistent or in conflict with the terms of this warranty shall not be binding upon CAI unless reduced to writing and approved by an expressly authorized officer of CAI California Analytical Model 600 HCLD C_ETL_US CE Instruction M March 2006 Page 2 of 69 Section 2 FEATURES AND SPECIFICATIONS 2 Features 2 1 Description The CAI Model 600 HCLD Analyzer is a highly sensitive heated chemiluminescent CLD gas analyzer for measuring gas concentrations in industrial and vehicle emission applications The analyzer includes a unique internal oven which maintains ALL plumbing components in contact with the sample gas before the detector at an elevated temperature between 65 and 100 degrees Centigrade Temperature is Customer Specified 2 2 Features General The Model 600 HCLD analyzer has a 3 by 5 inch liquid crystal display and a 20 key data operation input keyboard The 16 bit microprocessor control board consists of the MSR Card with 16 digital inputs 16 digital outputs 16 analog inputs and 4 analog outputs The analyzer can be manually operated from the keypad or remotely via TCP IP or Rs 232C communications After turning on the analyzer it needs at least 30 seconds for initialization During this time the screen is illuminated but clear The analyzer is available with a
47. advanced system user TIP Because of the user settings some of the parameters shown in this manual may not appear on your analyzer Check the access level 5 1 The Main Menu Upon power up the CAI logo is first displayed and then the main menu appears as below NOTE Access Main Menu _ Level Indication Main Menu onPower Up Screen NOTE F6 is not available because on initial start up the analyzer reverts to ONLY Level 1 access See Section 7 5 5 for Password information California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 12 of 71 Section 5 OPERATING STRUCTURE All functions can be selected with the cursor keys and activated by pressing the Enter key or directly with the function keys F1 through F7 A gt to the right of a function means that one or more sub menus are available If this sign is missing the function starts immediately after the activation NOTE Access level is 4 Main Menu Su 2 urge analyze FS Diagnostics F 4 Calibrations gt FS setup gt Fe Remote MNanus gt FT Standby Measure sample Main User Menu Level 4 California Analytical Model 600 HCLD C_ETL_US CE March 2006 NOTE Access Level Indication Page 13 of 71 Operators Mi Section 6 MENU STRUCTURE 6 Menu Structure There are 4 operating levels based on the level of your password This section shows the access rights of the single levels
48. arrants that the products sold under this sales order shall be free from defects in workmanship and materials for one year after delivery of the product to the original Buyer by CAI and if any such product should prove to be defective within such one year period CAI agrees at its option either i to correct by repair or at CAIs election by replacement with equivalent product any such defective product provided that investigation and factory inspection discloses that such defect developed under normal and proper uses or ii to refund the purchase price The exceptions and conditions mentioned above are as follows a components or accessories manufactured by CAI which by their nature are not intended to and will not function for one year are warranted only to give reasonable service for a reasonable time which constitutes reasonable time and reasonable services shall be determined solely by CAI A complete list of such components and accessories is maintained at the factory b CAI makes no warranty with respect to components or accessories not manufactured by it in the event of defect in any such component or accessory CAI will give reasonable assistance to Buyer in obtaining from the respective manufacturer whatever adjustment is authorized by the manufacturer s warranty c any product claimed to be defective must be returned to the factory transportation charges prepaid and CAI will return the repaired or replaced product freight collect
49. ation that will be monitored by a remote reordering device Note NO only active in the Switching Mode SEE TABLE D California Analytical Instruments Model 600 HCLD Operators Manual January 10 2011 Page 6 of 24 ADDENDUM 3 0 NEW FUNCTIONS 3 1 Auto Start Up Main F5 F7 F7 Auto Startup S SHET Auto Startup Off Wait for min 1 Calibrations 2 5Startrange 4 Access Level I z Remote Manual anual HO HOx Mode HO MAIN SAVE H 22 5 BACK SAVE Cheek Air Pressure F All key analyzer parameters are stored in a secure memory location and retained when power is removed In the event of an unexpected power failure it may be desirable to change some parameters until an operator can resume control This screen may be used to establish several desirable special instrument start up parameters that define how the analyzer recovers from loss of AC power When enabled this screen will define the following Wait The time delay in minutes before proceeding If Zero is selected the instrument will wait until all temperature warnings are cleared Calibrations The number of attempts to complete a successful calibration as required in the operator defined Deviation Tables If calibration is not successful the instrument will continue reporting results using the last completed calibration The analyzer will utilize the last completed calibration by selecting zero for Calibrations Starti
50. ations CERES CS c Sal ib pation Tue Jan 28 08 13 52 2003 Calibration Screen 7 4 1 F1 Automatic Calibration From the Calibrations screen F1 starts automatic calibration If auto range is selected the actual range in use will be calibrated Auto calibration works as follows First zero gas is purged a certain time called purge time Then the measurement begins The measured value must be a minimum time called measuring time and within an upper and a lower limit to be saved as new offset value The maximum length of measuring time is 9 seconds If the measured value was constant during calibration time it is checked to determine if this value deviates from the preceding value If the deviations are too large a warning Deviation error appears and the user can choose if the new value is saved or not At last the zero gas is flown a further time verifying time so it can be checked if the signal is still constant All of these times can be changed After zero gas calibration the same happens with span gas During auto calibration Calibration in progress is displayed It also shows California Analytical Model 600 HCLD C_ETL_US CE Operators M March 2006 Page 19 of 71 Section 7 MAIN MENU which gas is flowing and which time runs When auto calibration has finished it is displayed If the span value of the selected range is O see section 5 6 1 then it will not be calibrated If one range is calibrated and the span
51. ct closures NOTE The correct calibration gas values must be entered The instrument is available from the factory with four ranges 6 NO NOx Function The analyzer switches the NOx converter in and out of the sample stream and is controlled from the measurement screen In the NO mode the sample by passes the converter and the resultant analysis produces the value of NO Only in the sample In the NOx mode the sample passes through converter and the resultant analysis produces the value of NOx NO NO2 in the sample The NO mode may be switched in and out remotely by a contact closure or computer Remote control wiring is terminated in the rear panel connector See Appendix California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 44 of 71 Section 9 OPERATION 7 Sample Pressure Check With sample gas flowing through the instrument check the sample pressure setting by referring to the diagnostic screen The sample pressure should read as indicated in the factory pressure settings screen 8 Optional Rear Mounted After NOx Converter Chiller With gas flowing through the instrument at 85 to 100 degrees C the sample is passed through the heated NO2 to NO converter the rear mounted chiller and to the reaction chamber This allows for a dry measurement IFFT FF TFE FFF EERE T Drain Line This chiller is self contained and has a single temperature adjust potentiometer which is accessible through
52. e 1 TTL low true D Output Sense Range 2 TTL low true D Output Sense Range 3 TTL low true D Output Sense Range 4 TTL low true set Auto Range Control Range 1 Control Range 2 Control Range 3 Control Range 4 Auto Cal Calibrate Zero Span Sample D Output OC 24vdc if internal SV D Output OC 24vdc if internal SV D Output OC 24vdc if internal SV D Output 25 Local Remote TTL low true D Output 26 Read Cal Mode TTL low true D Output 27 Reserved D Output 28 Reserved saso boas Slszanzs eene onm od wom o California Analytical Instruments Model 600 HCLD Operators Manual January 10 2011 Page 23 of 24 Section 13 ADDENDUM TABLE D CONT 600 SERIES CLD IO CHART 28 PIN AUXILLIARY CONNECTOR ASSIGNMENTS NO Normally Open oPTO Signal CLD vo Type Analog LEVELS G 1 spre fone ooo l o A Input GND analog A Input External Analog 1 A Input External Analog 2 A Output GND Isolated analog D Output Relay RTN 1 Rag Nouoank O lt 0 10V 0 10V 9 10 11 12 use RTN 1 Status go CLOSED when active Alarms go OPEN when present 13 14 15 16 use RTN 2 17 18 19 20 use RTN 3 21 27 28 use RTN 4 D Output D Output D Output 6 Relay RTN 2 7 Relay RTN 3 8 Relay RTN 4 COM 0 1 2 3 4 5 6 f 8 9 D Output D Output D Output D Output D Output D Output D Output D Output D Output D Output D Output D Output D Output D Output User Defined NO Relay 1
53. e press BACK to save the new value 3 4 10 Press F8 to return to the D A Calibration screen and note the results on the remote device 3 4 11 Repeat steps 3 4 8 thru 3 4 10 until a satisfactory ZERO calibration is achieved 3 4 12 Complete steps 3 4 8 thru 3 4 10 for each of the remaining outputs that require calibration 3 4 13 Press F5 to produce a full scale 100 signal 3 4 14 Use the arrow keys to position the curser at the require GAIN value 3 4 15 Observe the results on the remote device and make a correction to the GAIN value for the output of interest Press BACK to save this new value 3 4 16 Press F8 to return to the D A calibration screen 3 4 17 Observe the results on the remote device and repeat the steps to change the GAIN value by repeating steps 3 4 14 thru 3 4 16 as needed for each output 3 4 18 Return to the OUTPUT Assignment screen F5 F7 F3 from the main menu and change the output signals from CALIBRATE to their original values as defined in step 3 4 1 California Analytical Instruments Model 600 HCLD Operators Manual January 10 2011 Page 12 of 24 ADDENDUM 3 5 Save Data Archiving Time Main F5 F7 F1 F5 Archive Time is the Time in seconds between each set of data points If zero no data is stored in the SEC data files The SEC data files are in CSV format for direct import into Excel CAI can provide the tools necessary to download these files Use ENTER to change recording
54. e span gas deviation is span gas bottle value minus span gas value calculated by the factory polynom related to the range limit of the calibrated range 7 4 3 4 Relative Span Gas Deviation Relative span gas deviation is the actual deviation minus the deviation of the previous calibration related to the range limit of the calibrated range 7 4 4 F4 Check Calibration There is a default calibration Pressing F4 activates an automatic zero and span check for verification 7 4 4 F5 Reset Calibration Values There is a default calibration Pressing F5 a new screen appears and asks if the user is sure to reset calibration values to the default calibration values F1 confirms and the calibration values are reset to default calibration values F2 leaves this menu without resetting to default values This function will overwrite all calibrations with factory values Also the linearization polynom will be overwritten with the factory values 7 4 5 F6 Range Select This allows a range change to be activated from the calibration menu California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 22 of 71 Section 7 MAIN MENU 7 5 F5 Setup From the Main Menu F5 brings up the setup menu Span gas concentrations calibration settings range limits alarms password linearization system and measure settings can be changed The Setup menu begins as shown below A description of each parameter is shown in the information bo
55. ection 3 INSTALLATION NOTE A defective ground may affect the operation of the instrument The output voltages are connected per Table 8 1 1 Shielded wiring is recommended for outout signals Replace fuses with recommended fuse size indicated on rear panel of instrument Replacement with any other size fuse may cause damage to the instrument and possible injury to operating personnel 3 4 Analog Output Connections Appendix See Appendix for connector pinouts located on the analyzer rear panel Remote range identification and range selection are obtained by the rear panel connections Whena range is selected the corresponding control line is pulled low to zero VDC Ranges not selected will remain at approximately 5 VDC When remote range control is selected through the front panel keypad a contact closure is provided at the rear panel connector Remote range selection is made by connection of the control line for the desired range to the analyzers zero VDC line provided in the connector Five VDC is also provided Remote NOx On is selected by connection to the common line This contact closure turns on the NOx function by flowing the sample first through the NO NOx converter 3 5 Gases 1 Air or O2 Ozone Air lt 1 ppm C in pressurized cylinder 2 Nitrogen or zero air in pressurized cylinder 3 Standard span gas es near full scale concentration with a nitrogen balance ina pressurized certified cylinder 3 6 Gas Handli
56. ed on the equipment ALWAYS REMOVE POWER BEFORE CONNECTING OR DISCONNECTING SIGNAL CABLES OR WHEN SERVICING THE EQUIPMENT The 600 series HCLD instruments meet or exceed the following directives and standards Application of Council Directive s Electrical Safety Low Voltage Directive 73 23 EEC Electromagnetic Compatibility EMC Directive 89 336 EEC Standard s to which Conformity is Declared Electrical Safety Standard for Electrical Equipment for Measurement Control and Laboratory Use EN 61010 1 2001 2nd Edition Electromagnetic Compatibility EN 61326 1997 Electrical equipment for measurement control and laboratory use EMC requirements Amendment A1 1998 to EN 61326 1997 Amendment A2 2001 to EN 61326 1997 A Do not apply power to the analyzer or attempt to energize the ozone supply or converter until ALL leak checks have been performed and until the analyzer environment has been determined to be non hazardous This analyzer is designed for use in a NON HAZARDOUS environment This analyzer is designed for use with a HAZARDOUS sample Tampering or use of substitute components may cause a safety hazard Use only factory authorized replacement parts Do not operate without the cover secured Servicing requires access to live electrical components which can cause death or serious injury Refer servicing to qualified service personnel For safety and proper performance this instrument must be connected to a
57. en use F2 or Main or Back From Main Menu use F4 F2 California Analytical Instruments Model 600 HCLD Operators Manual January 10 2011 Page 21 of 24 ADDENDUM 4 4 Reset Calibration Values When the re set calibrations value function is used all recorded deviations will be set to zero Def cal value Span gas devs Span gas devs I Span gas devs verifying Span gas deviations 2 measured ayiation abs rel ee fe F Rangel G Q 00 fates panses F OG 0 DO anges Ranges See MT MET Range4 CAI Tel 800 959 0959 F Main F4 F3 F4 Main F4 F3 F2 Used to observe Auto Cal Results Used to observe Manual Cal results The above are the new deviations after the operator elects to re set the calibration values California Analytical Instruments Model 600 HCLD Operators Manual January 10 2011 Page 22 of 24 Section 13 ADDENDUM TABLE D 600 SERIES CLD IO CHART 28 PIN MAIN CONNECTOR ASSIGNMENTS AO Analog Output OC Open Collector SV Solenoid Valve TTL Transistor Logic OPTO 600 CLD HCLD 1 0 Type Analog Levels ping COM A Output GND Isolated analog Isolated Al A Output User Defined AO 1 1v 5v 10v mA A Output User Defined AO 2 1v 5v 10v mA A Output User Defined AO 3 1v 5v 10v mA A Output User Defined AO 4 1v 5v 10v mA bad Q D Output GND Digital D Output Sense Auto Range TTL low true D Output Sense Rang
58. ero valve is opened Description Saves measured value of actual range as new span value if span valve is opened Description Set converter off Only NO is measured Description Set converter on All kinds of NOx are measured Description Activates dual measure mode Analyzer switches periodically between Operators Mi Page 60 of 71 Section 13 APPENDIX NO and NOx mode and displays NO NO2 NOx SFGR Reset calibration settings to factory defaultConverter on Command Response Description _SFGR_KO _SFGR_s Reset all calibration settings to their factory settings SENT Set calibration gas flow Command Response Description SENT KO x SENT s x 10 Calibration through sample gas inlet oump y 11 Calibration through zero span valves Settings EKAK The four span gas concentration values are set Command Response Description _EKAK KO M1i_w w M2 x x M3_y y_ M4 z z _EKAK s Setendgas values EMBE The four measuring range end values are set Command Response Description EMBE KO M1 w w M2 x x M3_ y y M4 z z _ EMBE s Set range limits EMBU The upper and the lower range switchover for autorange are set Command Response Description EMBU_KO_ M1i_w w W W_M2 x x X X _ M3 _ y y _EMBU_s_ Set lower and upper range YY M4 z z Z Z switchover limits EKEN Set new device identification Command Response Description _EKEN_KO_new device name EKEN _ s Set new device identification Maximum length of device name are 40 characters
59. es that can be used for start points for offsets and gains for different output types OUTPUT OFFSET GAIN 0 20 ma 0 000 0 927 4 20 ma 1 820 0 740 0 1 V 1 300 0 820 0 5 V 1 100 0 820 0 10 V 1 050 0 820 California Analytical Instruments Model 600 HCLD Operators Manual January 10 2011 Page 10 of 24 ADDENDUM e Procedure 3 4 1 From the Main Menu press F5 F7 F3 to obtain following screen assignment 1 SARA Output Signal 3 4 2 Use the to highlight the outputs that require calibration 3 4 3 Press enter so you provide access to all the menu of signals that are available Real Time NO NOx Calibration Sample Pressure etc 3 4 4 Select Calibration and press ENTER to complete the selection Note In the example below only Output 1 will be calibrated Record the name of these signals they will be restored Output CAI Tel 800 959 0959 Note Any or all of the four outputs can be selected for calibration This screen will not be used again until calibration has been completed California Analytical Instruments Model 600 HCLD Operators Manual January 10 2011 Page 11 of 24 ADDENDUM 3 4 5 Press BACK to return to the SYSTEM SETUP screen Main F5 F7 3 4 6 Press F8 to obtain the following screen Main F5 F7 F8 3 4 7 Use the to select the desired output press ENTER 3 4 8 Press F1 to select a ZERO signal and observe the results on the remote device 3 4 9 Change the offset valu
60. fferent ranges The user can define the upper range limits in ppm Auto range Change Range Limits 7 5 3 1 F1 Range 1 4 Change Upper Range Limits In this menu the upper range limits can be changed The new settings are saved by pressing MAIN or BACK The auto range limits are automatically adapted This means that if the upper range limit of range 1 for example has reached 90 of the upper range limit in the auto range mode it is switched automatically to the second range Setup Z Upper range limits ppm Rangel CA Rangez TUL Ranges 300 Ranged 3000 Change Upper Range Limits California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 25 of 71 Section 7 MAIN MENU 7 5 3 2 F2 Change Auto Range Limits Although the auto range limits are adapted automatically it is possible to define them manually Up means the value when the next higher range is selected in auto range mode down the value when the next lower range is selected Setup down up ppr Rangel py aaa Rangez 27 ge Ranges 90 270 Ranged 270 Change Auto Range Limits 7 5 4 F4 Alarms Error reports are always displayed In the lowest line of the screen There are two pressures three temperatures one concentration and two voltages with alarm limits that can be defined The user can define the range limits and If exceeded will display an error Message Alarms alarms y PRC ia Tro cg i
61. ge 43 of 71 Section 9 OPERATION 9 Operation 9 1 Preparation for Operation Check that the external plumbing and wiring have been connected correctly as described in this manual NOTE The internal ozone generator requires approximately 1 hour of continuous operation for the analyzer to achieve full zero and span calibration stability A pressure switch will turn off the ozonator when air or oxygen is not present at the analyzer rear panel 9 2 Operation 1 Power On Turn ON the power switch on the rear panel The digital display should illuminate 2 Introduce Ozone Supply Air or 02 Adjust the cylinder output pressure to 25 PSIG The internal air pressure is factory set to deliver the air pressure required for optimum analyzer performance as indicated in the factory settings screen 3 Air or O2 Pressure Settings Check the air pressure setting by referring to the diagnostic screen to check air pressure The pressure should read as indicated in the factory settings screen 4 Zero Adjustment Flow zero gas through the instrument by selecting the calibration screen and select either manual or auto calibrate NOTE The instrument may also be operated by an external computer or by remote contact closures 5 Span Adjustment Flow span gas through the instrument by selecting the calibration screen and select either manual or auto calibrate NOTE The instrument may also be operated by an external computer or by remote conta
62. ill disable the auto range capability Continue pressing the arrow keys will recycle the analyzer back to auto range The range and or auto range is displayed on the measurement screen If the limits are exceeded while not in the auto range mode a warning Over Range appears on the screen HI D H 13 Hi D Ho 1 100 2 n ion Sa a FAAA MSNomedan 27 15 27 i7 Set to Auto Range Analyzer Set to Range 3 California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 17 of 71 Section 7 MAIN MENU 7 2 F2 Purge Analyzer 7 Cis a ib Purge Screen F2 from the Main Menu activates the Purge analyzer function if equipped 7 3 F3 Diagnostics F3 from the Main Menu activates the Diagnostics function As described in Section 7 1 3 F3 brings up the two diagnostics screens The Diagnostics screens may be brought up from EITHER the Main Menu or the Measurements screen ma tll si H nnmnnn _ Tin a Main User Menu Level 4 Operators Mi California Analytical Model 600 HCLD C_ETL_US CE March 2006 Page 18 of 71 Section 7 MAIN MENU 7 4 F4 Calibrations F4 from the Main Menu activates the Calibrations screen Calibrations may be automatic or manual Deviations can also be displayed Calibration values can be reset to default values and the range to be calibrated can be changed Galibrate CLI Meahan 2s 12619 Main Menu User Level 4 Calibr
63. ilure Peltier Gas Temp Failure Reaction Chamber Temp Failure EPC Coil Sample Failure EPC Coil Air Failure Range Overflow ADC Range Overflow ADC Range Underflow Range 1 is not calibrated Range 2 is not calibrated Range 3 is not calibrated Range 4 is not calibrated AKEN Device identification Current error number is responsed Command Response Description _AKEN_KO _AKEN_s_devicename Device identification is responsed AKEN K1 _AKEN_s_ model _AKEN_K2 _AKEN_s_serialno AKEN _ K3 _AKEN _s airpressure _ AKEN K4 _AKEN_s_samplepressure ARMU Rawvalue Command _ARMU_KO Response _ARMU _s z z ATEM Temperatures Command Response _ATEM_ KO _ATEM 3s zz y y_ _ATEM_KO x _ATEM s z z Description of x Converter Temp Pump Temp Diode Temp California Analytical Model 600 HCLD C_ETL_US CE March 2006 Device model Device serial number Suggested input air pressure Suggested input sample pressure Description Raw value before linearization and offset span correction is responsed Description All Temperatures in degrees celsius are responsed Temperature of x in degrees celsius is responsed Page 55 of 71 Operators Mi Section 13 APPENDIX Cell Temp 6 Peltier Temp Reaction Chamber Temp ADRU Pressures Command Response Description _ADRU_KO _ADRU_s Zz y y_ All pressures are responsed _ADRU_KO x _ADRU_s z z Pressure of x is responsed Description of x Sample Pressure Air Pressure
64. ion Screens 5 4 3 F3 Display Deviations After every calibration the deviations are calculated for zero and for span gas F1 shows zero gas deviations F2 shows span gas deviations F3 Deviations of zero gas during verifying F4 Deviations of span gas during verifying F1 and F2 deviations are displayed in percent l H ero ga 1 ons eia Zaks pias nieces BW1 ons FS Werifring devs zero abs rel F4 Verifying devs span Rangel oO OO A 0A RkRanaez A AA Oo OG Ranges GH Oo A AA Ranged Oo 0A Oo Oo Wed Jan 29 09 44 00 2003 led Tan 29 A9 47 27 Deviation Screen Zero Gas Deviations During calibration there is a verification for zero and span gas With option F3 and F4 you can view the deviations during the verification time Absolute deviation is the absolute average difference from the saved value in ppm Relative deviation is the absolute average difference in percent related to the range limit California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 21 of 71 Section 7 MAIN MENU 7 4 3 1 Absolute Zero Gas Deviation Absolute zero gas deviation is zero gas content calculated by the factory polynom related to the range limit of the calibrated range 7 4 3 2 Relative Zero Gas Deviation Relative zero gas deviation is the actual deviation minus the deviation of the previous calibration related to the range limit of the calibrated range 7 4 3 3 Absolute Span Gas Deviation Absolut
65. lications These installation instructions are for a typical site Any questions regarding specific installation situations should be directed to Technical Service of California Analytical Instruments Inc 3 2 Site and Mounting NOTE The following precautions must be carefully observed 1 Select a site free from direct sunlight radiation from a high temperature surface or abrupt temperature variations This analyzer is not suitable for installation outdoors Select a site where the air is clean Avoid exposing the instrument to corrosive or combustible gases 4 The instrument must not be subject to severe vibration If severe vibration is present use isolation mounts 5 The instrument is designed for rack mounting Optional rack mount slides are available 6 Do not install near equipment emitting electromagnetic interference EMI NOTE A rear supporting brace or equivalent is required if the optional rack mount slides were not purchased The power on off switch is accessible from the rear of the instrument only DO NOT mount such that the power on off switch is inaccessible 3 3 Electrical All wiring is connected at the rear of the instrument Connect outputs etc as shown in Table 3 1 on the following page The AC power is connected to the power fuse switch as shown below AC Power Switch Connector and Fuse California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 5 of 71 S
66. mple gas inlet oump y 11 Calibration through zero span valves Control commands SRES Reset Command Response Description _SRES_KO _SRES s Reset SPAU Pause Command Response Description _SPAU_KO _SPAU_s Pause mode STBY Standby Command Response Description _STBY_KO _STBY_s Standby mode SNGA Open valve for zero gas calibration Command Response Description _SNGA_KO _SNGA_s Open valve for zero gas calibration of _SNGA_KO_Mn _SNGA s SEGA Open valve for end gas calibration California Analytical Model 600 HCLD C_ETL_US CE March 2006 actual measuring range Open valve for zero gas calibration of range Mn Operators Mi Page 58 of 71 Section 13 APPENDIX Command Response Description _SEGA_KO SEGA s Open valve for end gas calibration of _ SEGA KO Mn _SEGA s actual measuring range Open valve for end gas calibration of range Mn SSPL Purge Analyzer with zero gas Command Response Description _SSPL_KO _SSPL_s Open valve for zero gas and purge the analyzer SLIN Linearization mode Command Response Description SLIN_KO SLIN s SKOP Converter Check Change status to SLIN only for compatibility Command Response Description _SKOP_KO _SKOP_s Change status to SKOP and activate SWET Chiller off Wet mode measuring sample pump only for compatibility Command Response Description _SWET_KO SWET s Switch chiller off SDRY Chiller on Dry mode measuring Command Response _SDRY_KO _SDRY_s S
67. n Open RXD LNLED LNLED CONOORWND IMPORTANT TIP For direct connect to a PC a crossover cable is required Connection to a hub requires a straight cable California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 38 of 71 Section 8 ANALYZER COMPONENTS 8 2 Internal Component Locations Major Internal Components Electronics Includes instrument electronics See Main Electronic Board NO NOx Solenoid Valve Switches flow between the NO and NOx mode Optional Internal Sample Pump Provides sample to analyzer Ozonator Contains UV Lamp Ozonator High Voltage Supply Produces High Voltage to UV lamp Proportional Flow Pressure Regulator Regulates flow of ozone Proportional Flow Pressure Regulator Regulates flow of sample ere oa Pe YS Reaction Chamber amp Detector Assembly See Figure 8 10 NO NOx Converter Converts NO2 to NO for total NOx 11 Relay Control Board Provides AC Voltage to Heaters Pump and UV Transformer California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 39 of 71 Section 8 ANALYZER COMPONENTS 8 3 Main Electronics Board Potentiometers RP1 to RP17 oe ee i a _ i p Pe hag at Ti i at iw f ti n arr 7 e r W mini Cy ings tal ei iti EPIHA Eu Uan aatia mini N a n i ti iliii Hih FRE TETN piy p 7 L st i tnmHNURHEL he Main Electronic Board Potentiometers RP1 EPC 9 5V Sample Set RP10
68. n optional internal heated sample pump IMPORTANT TIP When the analyzer is powered up it defaults to access level 1 User To operate ALL parameters check the access level See Section 5 5 5 The contents of this manual include e Electrical Specifications e Installation Requirements Mechanical amp Electrical e Operation amp Calibration Instructions e Reaction Chamber Description with Procedures for Disassembly of its Component Parts e Function Explanation of the Electronic Circuitry e Block Electrical Diagram California Analytical Model 600 HCLD C_ETL_US CE Instruction M March 2006 Page 3 of 69 Section 2 FEATURES AND SPECIFICATIONS Chemiluminescence CLD Photodiode thermally stabilized with Peltier cooler 0 1 to 3 000 ppm NO or NOx Four user programmable ranges Higher Ranges Available upon Request T90 lt 2 Seconds to 60 Seconds Adjustable 10 ppb NO NOx Displays 5 significant digits Better than 0 5 of Full Scale Better than 0 5 of Full Scale NOISE Less than 1 of Full Scale ERO amp SPAN DRIFT Less than 1 of Full Scale per 24 Hours ERO amp SPAN ADJ Via front panel TCP IP or RS 232 NH3 HCN amp SO Not detectable with 100 ppm EFFECT O EFFECT LOW CONTROL INEARITY NZ 5 SRE SE Sol Zs SIRO Qla meZ 3 gt N JIO wam ol O Z Ez amp s S me es N N Less than 0 5 with 10 CO Electronic Proportional Pressure Controller to 3 0 LPM See footnote below
69. ng Equipment 1 Pressure regulators for zero gas Air or N2 ozone supply air or O2 and span gas cylinders 2 Corrosive resistant gas tubing High levels of Ammonia greater than 10 PPM NH may reduce the NO to NO Converter s conversion efficiency to a level that is unacceptable It is therefore recommended that the customer purchase a commercially available NH3 scrubber and install it in the path of the sample gas prior to its introduction into the analyzer California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 6 of 71 Section 3 INSTALLATION 3 7 Gas Connections The tubing from the sampling system to the gas analyzer should be made from corrosive resistant material such as Teflon stainless steel Even when the gases being sampled are corrosive themselves rubber or soft vinyl tubing should not be used since readings may be inaccurate due to gas absorption into the piping material To obtain fast response the tube should be as short as possible Optimum tube internal diameter is 0 16 inch 4 mm Couplings to the instrument are 1 4 Inch tube NOTE Be sure tubing and joints are clean Dust entering the instrument may cause it to malfunction 3 8 Sampling Requirements 3 8 1 Filtration Dust must be eliminated completely Use filters as necessary The final filter must be capable of removing particles larger than 4 microns 3 8 2 Condensation Dew point of the sample gases must be lower than
70. ng Range When all defined actions are completed the analyzer will return to the Measurement Screen and at the range specified Access Level The user level at Start Up Remote Manual Put the analyzer in either Remote or Manual at Start Up NO NOx Mode Put the analyzer in NO or NOx or NO2 mode at Start Up California Analytical Instruments Model 600 HCLD Operators Manual January 10 2011 Page 7 of 24 ADDENDUM 3 2 Alarms On Off Main F5 F7 All key analyzer parameters are stored in a secure memory location and retained when power is removed In the event of an unexpected power failure it may be desirable to change some parameters until an operator can resume control This screen may be used to establish several desirable special instrument start up parameters that define how the analyzer recovers from loss of AC power When enabled this screen will define the following On 5 Alarms NOx 43 T Use F6 to toggle ON OFF The instrument has an extensive library of warning messages that will aid in the identification of various anomalous events and are displayed at the bottom of the screen These messages will assist in diagnostics and indicating the need for preventative maintenance This screen provides an option to disable these messages during initial start up or as may be desired for a particular application California Analytical Instruments Model 600 HCLD Operators Manual January 10 2011 Page
71. ns 37 8 1 2 Auxillary Analog Connections 37 8 1 3 Digital RS 232 Connections 37 8 1 4 Digital TCP IP Connections 38 8 2 Internal Components 39 8 3 Main Electronics Board Potentiometers 40 8 4 Main Electronics Board Connections 41 8 5 Reaction Chamber 42 8 6 Relay Board Connections 43 OPERATION 2 2 2222 nnn nnn nn nnn nn nn nn nnnnnnnnnennnennnnnnnnns 44 9 1 Preparation Aa 9 2 Operation 44 45 9 3 Shut Down Procedure 46 FUNCTIONAL DESCRIPTION 47 10 1 Operating Principle 47 10 2 Reaction Chamber A
72. o bIONVY_O eSONVY_O ZaONVY_O LZONVE O Ol YOSSHOONd Operators Mi Page 70 of 71 ical Model 600 HCLD C_ETL_US CE California Analyt March 2006 ADDENDUM TABLE OF CONTENTS ADDENDUM STARTING AFTER JUNE 2007 Section Title Page 1 0 IIE OGUICTION se8csag sess ersece secre peae noose ce saa ene eee acon er a ean eee geen 2 0 Operation of Measurement Keys Palle OVE RANJE adaise a 22 DiagNOSUGS arians EAAS Ra ae S 2A Spansion 229 RANJE LIMIS a seeeaaee seein reese eee Ser sarase se eee 20 SPAN NAUES seraa eee ea ee eee ane aes ene ee ease eee eee see ae 2af OUPS ae 3 0 New Functions Ih AWO StA Up R eee eee a 9222 AAS ONON ee a ae 90 OSETE AANE A E e a a 9 4 Calibrate The Analog QUIPUTS at esa inan a 9 02 Save Data Archiving TME sareti TABLE Asses Asam at see saree ease eases aeaenad es ateeee arenes 9 05 USEF Digita UNDUIS lt e2ss2 seas saat sane e cae sateen aes eens eases aaee a aa TABLE Oe ee a Beis Call AMAlOG OUUTE 4 0 Changes To Existing Functions 0 0 tela Saved OF OUISIGE LIMILS saraaa 4 2 Calibration DCVlalOnS sses csareseceecesasess os ateasetecsacera ste eeepeeasessenacaaseas A3 FOW Zero Ol oP di GaS A eE ea eae Seren eeee ee cee 4 4 Reset Calibration Value
73. ode Reserved Reserved 28 Pin Auxiliary Connector Assignments Signal Type Analog Spare _fpin GND analog External Analog 1 External Analog 2 Spare analog Spare analog GND Alarm General Alarm Ch 1 Conc 1 Alarm Ch 1 Conc 2 Alarm Reserved Reserved Reserved Reserved Reserved GND Alarm Calibration Alarm 1 Reserved Reserved Reserved Read Wet Mode Read OverFlow Set Wet Mode Set OverFlow Set NO Mode Spare Spare Spare Note All digital outputs and inputs are 0 5 VDC ONLY All analog inputs are 0 10 VDC ONLY Connecting analog outputs to existing current loop systems or voltage loop systems WILL DAMAGE the instrument California Analytical Model 600 HCLD C_ETL_US CE March 2006 Page 64 of 71 Operators Mi Section 13 APPENDIX MODEL 600 HCLD Flow Diagrams BYPASS R31 R4 dC R2 DK NC SV3 KEE NO Pa ete a aie salen 2 NOX CONVERTER F3 P Be Er CVZ R5 R AIR O2 PA AMP DETECTOR EXAAU ST E MF 1 P1 mass gt Q NOTE Standard Analyzer With Internal Heated Sample Pump California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 65 of 71 Section 13 APPENDIX et BYPASS AIR O2 i MY CV2 EXHAUST NOTE Standard
74. p Failure 650 only EPC Coil Sample Failure EPC Coil Air Failure Range overflow ADC Range Overflow ADC Range Underflow Range 1 is not calibrated Range 2 is not calibrated Range 3 is not calibrated Range 4 is not calibrated Reaction chamber pressure Low concentration Warning High concentration Warning NH3 Converter Temp Failure 605 only dummy text for RTC General Alarm Cal Alarm California Analytical Instruments Model 600 HCLD Operators Manual January 10 2011 User DO Screen Display SampleP AirP OvenT ConvT PumpT DiodeT CellT DryT O2T SEV AEV OR AO AU RINC R2NC R3NC R4NC RCP LoC HiC NH3T Off GenAlarm CalAlarm Page 16 of 24 Index 25 27 28 29 30 31 32 33 34 35 36 37 38 39 40 TABLE C Status Group In Remote AutoRange Range 1 Range 2 Range 3 Range 4 In Calibrate In Zero In Span In Sample In NO Mode In NOx Mode 605 only In Wet Mode HCLD only In Overflow not used In NH3 Mode 605 only TYPICAL RELAY 600 SERIES ADDENDUM User DO Screen Display InRem AutoR R1 R2 R3 R4 InCal Zero Span Sample INNO InNNOx InWet InOflow INNH3 Digital Out These contacts 3 4 will drive continuously up to 500 MA using a customer voltage supply that does not to exceed 60 VDC California Analytical Instruments Model 600 HCLD Operators Manual January 10 2011 Page 17 of 24 ADDENDUM e OPERATION Use Main F5
75. properly grounded three wire receptacle A This analyzer produces high levels of ozone 4 maximum that can be dangerous to the health of the operator and serounding personnel Be sure to only use this instrument with proper ventilation And exhaust lines Section Title 1 TABLE OF CONTENTS Page INTRODUCTION 222222 22200000000 00000000202eeeeeee 1 1 1 OvervieW 1 1 2 Unpacking Instructions 1 1 3 Reporting Damage 1 1 4 Contact Information 1 1 5 Warranty Certificate 2 FEATURES AND SPECIFICATIONS 3 oul DescriptionS 3 2 2 Features 3 2 3 Specifications 4 INSTALLATION 222222 00000000000000eeeeeesseeeeenee 5 3 1 General
76. r the default password 7 5 5 3 F3 Reset Passwords The passwords can only be changed if you are in access level 4 Reset passwords will revert back to the factory defaults 7 5 6 F6 Linearization Pressing F6 on the Setup screen brings up the Linearization screen The analyzer can be linearized by a polynom with 5 coefficients By pressing F1 these 5 coefficients can be changed for each range By pressing F2 the raw value can be displayed This is the value before linearization and offset span correction There are two values on the screen The value at the top is the linearized offset span corrected value and the other value is the raw value Tue Jan 268 14 50 01 2003 Coefficients Range Select xa i wooo g HiAk 1 Switch HNOr NOx Rau wal Change Linearization Coefficients Example of Linearized and of Selected Range Raw Data with F2 California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 28 of 71 Section 7 MAIN MENU 7 5 7 F7 System Settings This screen allows all the system settings to be displayed and modified Red ime oc 2 Bera Sebo ngs F3 Output assignment F 4 Ootput Range rn F5 status line oneofrt Fe Language FT Aute Startup setup real time clock and autocalibration scheduler Poeman 29 L158 1st 49 2005 System Setup Screen 7 5 7 1 F1 Real Time Clock This brings up the clock time set screen auto cal and auto cal enable screens Fi Sho
77. rations 15 Reaction Chamber Assembly Dust water droplets or mist entering the reaction chamber assembly may cause drift due to contamination If the calibration procedures fails to bring the instrument to zero check the chamber for contamination 9 3 Shut Down Procedure 1 Turn off the zero span and air O2 cylinders 2 Ifthe analyzer contains the optional internal heated sample pump disconnect the sample line from the rear inlet port Do NOT turn off the sample pump or analyzer power at this point 3 Allow the analyzer to draw in room air for approximately 5 minutes This will flush out any remaining sample which may cause condensation as the analyzer cools 4 Turn off the pump switch 5 Turn off the optional internal sample pump by setting the analyzer to standby 6 Back flush the heated sample line and filter of any sample before disconnecting and powering down California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 46 of 71 Section 10 FUNCTION DESCRIPTION 10 Functional Description 10 1 Operating Principle The California Analytical Model 600 CLD Analyzer utilize the chemiluminescent method of determination of oxides of nitrogen NO or NOx in a sample gas In the NO mode the NO in the sample is quantitatively converted to NO2 by gas phase oxidation with molecular ozone produced by the UV reaction of cylinder air Generally 10 to 15 percent of these NO2 molecules are elevated to an
78. rators Manual January 10 2011 Page 4 of 24 ADDENDUM 2 5 Range Limits F8 From the MEASUREMENT Screen CAI Tel 800 959 0959 2 versions The standard analyzer is factory configured with 4 Physical Ranges of 3 30 300 3 000 PPM The optional high level analyzer is factory configured with 4 Physical Ranges of 5 50 500 500 The operator can change the number of ranges and select a more convenient full scale concentration if required Note Do not exceed the maximum range set by the factory and always use ascending order as shown Example a For a single range instrument set Range to the desired value and all others to zero b For a two range instruments set Range to the lowest value Range 2 to the highest value and the others to zero 2 6 Span Values F9 From the MEASUREMENT Screen i SARA Use to define the concentration of the span gas that will be used to calibrate each range Note The span gas value used for this range is highlighted and can be changed if necessary Use the Enter key and the numeric keys as required California Analytical Instruments Model 600 HCLD Operators Manual January 10 2011 Page 5 of 24 ADDENDUM 2 Outputs F10 From the MEASUREMENT Screen assignment Cal Tel 800 959 0959 Use the to select the desired Output Press Enter to select Use the to select the desired Signal Press Enter to select Use this screen to define the signals and their loc
79. s and thank you You have just purchased one of the most reliable gas analyzers in the world Before using the analyzer please familiarize yourself with its operation by reading this manual If you have any questions please do not hesitate to call California Analytical Instruments for assistance We want you to be a member of our thousands of satisfied customers 1 2 Unpacking Instructions Open the shipping container and carefully remove the analyzer from the packing materials Inspect the instrument for any sign of damage Remove the Top Cover retaining screws Visually check for loose parts or connectors that are not properly seated Verify all circuit boards and circuit board connections are secure If all internal components look normal re install the cover 1 3 Reporting Damage Should there be any apparent damage to either the inside or outside of the instrument due to shipping or handling immediately notify the shipper The shipping container or packing materials should be retained for inspection by the shipper 1 4 Contact Information California Analytical Instruments Inc 1312 West Grove Avenue Orange CA 92865 714 974 5560 Fax 714 921 2531 Website www gasanalyzers com California Analytical Model 600 HCLD C_ETL_US CE Instruction M March 2006 Page 1 of 69 Section 1 INTRODUCTION 1 5 Warranty Certificate Subject to the exceptions and upon the conditions stated below California Analytical Instruments CAI w
80. s serssz se sees secesersaesc cee eeaeee ee a ee ee California Analytical Instruments Model 600 HCLD Operators Manual January 10 2011 Page 1 of 24 ADDENDUM 13 5 Starting With SERIAL NUMBER UO6081 1 0 INTRODUCTION The Model 600 CLD Series Instruments starting with Serial Number U06081 have several new Hardware and Software features The Hardware includes the use of anew memory system isolation of the analog output signals and 15 relays that are used to buffer the many new digital output signals that are now available SEE TABLE D The available digital signals consist of a SERVICE group to externally monitor a number of parameters that provide insight for preventative maintenance and diagnostics decisions A second STATUS group is provided to define the operation of the instrument such as Spanning Zeroing Calibrating and the Current Range 1 2 3 4 AUTO The Software includes modifications to existing functions changes to the Measurement screen additional Short Cut Keys and several New Functions that are listed as follows e MEASUREMENT Over Range 888888 Zero F5 Span F6 Range Limits F8 Span Values F9 Outputs F10 Note The operator can use these Short Cut Keys or continue to use existing procedures e NEW FUNCTIONS Auto Startup F5 F7 F7 ALARMS F5 F7 Use F6 to toggle ON OFF Offsets amp Gains F4 F3 F5 D A Calibration F5 F7 F8 Cal Analog Outputs F5 F8 Use F8 to toggle ON OFF Save Data
81. sed AMBE Measuring range limit Command Response Description _AMBE_KO _AMBE_s M1_w w_M2 _ x x M3_y y_ All existing measuring range limits are M4 z z responsed _ AMBE KO Mn AMBE s Mn z z Range limit of Range Mn is responsed AKAK Calibration gas concentrations Command Response Description AKAK KO _ AKAK s M1 w w M2 x x M3_y y M All existing calibration gas values are 4 Z Z responsed AKAK _ K0 Mn AKAK_s_Mn z z Calibration gas value of Range Mn is responsed AMBU Upper and lower range switchover values for autorange Command Response Description _AMBU_KO _AMBU_s M1_w w_W W_M2 x x X Lower and upper range switchover X M3 _y y_Y Y_M4 z z Z Z value of autorange are responsed ASTZ Normal device status Command Response Description _ASTZ_KO _ASTZ_s SREM_STBY__SENO SARE Device status is responsed _SDRY Possible states remote standby NO mode Autorange on Chiller on manual pause NOx mode Autorange off Chiller off measuring gas SNGA zero gas SEGA end gas O Enua zero gas during autocal D e end gas during autocal For compatibility only SSPL purging SKOP measure ASTF Error status Command Response Description California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 54 of 71 Section 13 APPENDIX _ASTF_KO _ASTF_s f1_f2 13 f15 Sample Pressure Failure Air Pressure Failure Oven Temp Failure Converter Temp Failure Pump Temp Failure Diode Temp Failure Cell Temp Fa
82. sembly Procedure 9209 5 gt j Shut off ALL gas flow Remove power from the instrument Remove the top cover retaining screws Remove all 4 tubes from the 4 way cross Remove the 4 screws securing the photodiode and reaction chamber from the oven Remove the photodiode electrical connector from the main circuit board Remove the chiller connection from the photodiode reaction chamber Separate the photodiode and heat sink assembly from the reaction chamber by removing the 4 Allen screws from the front of the heat sink Save the 2 black rubber O rings Separate the mounting plate and the glass filter from the reaction chamber Save the 2 Teflon spacers and O ring Separate the manifold from the gold reaction chamber NOTE the position of the holes in the Tefoln gasket relative to the assembly screw holes The large hole is ozone 11 2 Assembly Procedure a Wash the reaction chamber glass filter and manifold separately in detergent using a test tube brush Be careful of the sample tube in the manifold Do not use abrasives Dry by blowing clean with dry nitrogen Reassemble the chamber assembly in reverse order per the above Make certain the sample tube is centered when assembling the manifold to the reaction chamber California Analytical Model 600 HCLD C_ETL_US CE March 2006 Page 49 of 71 Operators Mi Section 12 TROUBLESHOOTING 12 Troubleshooting 12 1 Ozone Air O2 Supply
83. ssembly 47 10 3 Flow System 47 10 4 Main Electronics Board 48 10 5 melay BOA QA ra E 48 REACTION CHAMBER 2 2 22 nn2 nnenennnen 49 11 1 Reaction Chamber Disassembly 49 11 2 Reaction Chamber Assembly 49 TROUBLESHOOTING 2 2 22 ennn nnn n nnn nnnnnnnnnnnennn 50 12 1 Ozone Air O2 Supply 50 12 2 Sample Supply 50 12 3 NO NOx Converter 50 13 APPENDIX 13 1 13 2 13 3 13 3 Soca na gas nanan eases easaseasesnasensasensssesnasesnssessasessssasnssansssessscessssssnes 51 AK Protocol esiin ea eeaeee ieee en ened 52 63 Output Connections 64 Flow Diagrams 65 68 Electrical Block Diagram Section 1 INTRODUCTION 1 Introduction 1 1 Overview Congratulation
84. the temperature of the oven to prevent accidental condensation within the instrument When sample dew point is greater than the oven s preset temperature pass the sample through a dehumidifier to reduce the dew point to prevent condensation If the sample contains an acid mist use an acid mist filter cooler or similar device to remove all traces of the mist 3 8 3 Presence of Corrosive Gases Useful service life of the instrument will be shortened if high concentrations of corrosive gases such as Clo SO2 F2 HCI etc are present in the sampled gas 3 8 4 Gas Temperature When measuring high temperature gases take care that the maximum rating of the instrument 122 F 100 C is not exceeded 3 8 5 Pressure and Flow Rates The air or oxygen supply entering the instrument is controlled by an electronically controlled proportional flow EPC controller The regulator is factory adjusted for optimum analyzer performance The ozone supply Air or 02 air cylinder pressure should be set at approximately 25 PSIG The sample entering the instrument is controlled by a factory set precision electronically controlled proportional flow EPC controller The EPC is factory set for optimum analyzer performance as indicated by the sample pressure If the analyzer does not contain the optional heated sample pump the sample gas entering the instrument should be at a pressure between 10 and 25 PSIG with a flow capacity at a minimum of 3 liters min If the
85. time SEE TABLE A California Analytical Instruments Model 600 HCLD Operators Manual January 10 2011 Page 13 of 24 ADDENDUM TABLE A 600 SERIES CLD DATA ARCHIVE FILES Time Date Month Year Error Index TimeStamp NO Conc NO2 Conc NOx Conc NH3 Conc Concentration Detector Volts Range Auto Manual Span Gas Offset Gain Sample Pressure Sample Flow Sample EPV Volts Air Pressure Ozone Flow Ozone EPC Volts Diode Temp Cell Temp Oven Temp Pump Temp Converter Temp Dryer Temp O2 Detector Temp NH3 Conv Temp O2 Concentration O2 Detector Volts O2 Offset O2 Gain Wet Dry Meas Mode Local Remote Converter California Analytical Instruments Model 600 HCLD Operators Manual January 10 2011 Page 14 of 24 ADDENDUM 3 6 User Digital Outputs e Overview The 600 CLD Series of instruments have 15 solid state optically coupled isolated relays that can be programmed by the operator to indicate the status of numerous digital conditions The available digital signals consist of a SERVICE group that can be used to externally monitor a number of conditions to aid in preventative maintenance and diagnostics SEE TABLE B amp D A second STATUS group is provided and is used to define the operation of the instrument such as Spanning Zeroing Calibrating and the current Range 1 2 3 4 AUTO etc SEE TABLE C amp D The individual output signals can be operator
86. to be calibrated By selecting calibrate as the output all outputs of interest may be selected When calibration is competed the operator will return the outputs to their original assignment California Analytical Instruments Model 600 HCLD Operators Manual January 10 2011 Page 9 of 24 ADDENDUM The D A CALIBRATION screen will then be used to complete the calibration procedure This screen provides a section that is used to record the zero signal corrections zero offset and a second area to record the 100 signal corrections Gain for each of the four output signals that may be defined to develop a voltage or current signal Since this is a Digital to Analog conversion the calibration will require the completion of a simple trial and error procedure The operator will observe the results of a zero or span Gain signal generated by the analyzer to the remote recording device and select a correction factor The operator will save this value and then observe the results on the attached remote recording device The process of selection and saving for zero and span will be repeated until a satisfactory calibration is achieved For 0 1VDC 0 5VDC 0 10VDC and a 0 20 mA outputs the Offset and Gain values are independent and do not interact With the 4 20 mA output the Offset zero and Gain Span values interact and may require a few more trials The following is a table of typical valu
87. u Settings screen allows the NO to NO2 converter efficiency to be set to the actual measured converter efficiency A value of 100 equals 1 00 F2 will prompt the operator through the NOx efficiency test using a NOx generator Setup z Converter efficiency current RRC EC i Fi trun suto calculation Set Converter Efficiency California Analytical Model 600 HCLD C_ETL_US CE March 2006 Page 33 of 71 Operators Mi Section 7 MAIN MENU 7 5 8 3 F3 Low Pass Filter Time Constant F3 on the Menu Settings screen allows the software time constant to be set between 1 and 60 seconds This is very useful in eliminating noise when measuring low level concentrations enter time constant af sample loupass filter Time constant CO 60 ify used for calculating the sliding average Wedman 2o s126257 2005 ll Set Time Constant 7 5 8 4 F4 Purge Time F4 on the Menu Settings screen the sets the purge time before continuing with a zero or span calibration Purge Time Purge time Set Purge Time 7 5 10 F10 Displays the Current Analyzer and Software Versions This displays the analyzer s information including the factory recommended air and sample pressure settings Weresian Model 600 CLI 2inobeoo4 ES ESAI Sto hoe version gt m m m T eiS Analyzer Information Version California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 34 of 71 Section 7 MAIN MENU UWersion NM
88. w time Set actual time Titeewan 28 FS rS 06 2005 Fi Clock and Timing Setup Screen F1 brings up the clock set screen Set time Z Re Weekday tue E f fdd mm vrv 28 Ja 2003 Date iaa MMi Ss 15 19 10 Set Clock Screen California Analytical Model 600 HCLD C_ETL_US CE March 2006 Page 29 of 71 Operators Mi Section 7 MAIN MENU The current time may be set by using the cursor to highlight the entry and using the numeric keys to change the values F2 brings up the auto cal time set As above the date and times can be set by using the cursor to highlight the entry and using the numeric keys to change the values F3 Sets autocalibration ranges sc a 2 Els Ww T E Sed e an sa Euver amp sk houri sl change to weekly Es change to daily Rosee Change to hourly z MAIN or BACK to exit Eis E25 FS to save changes 1 3 2003 Enter Range Converter Mode F4 Toggles Auto Cal ON of OFF California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 30 of 71 Section 7 MAIN MENU 7 5 7 2 F2 Displays TCP IP Address TCP IP Address 7 5 7 3 F3 Displays Output Signal Assignments Used to Adjust Analog Output Channels epee aa Crier mT RUD tT jn lt a Se Aichi l iO Oke on ty mts bet Smv9 nm en W 4 s b f b a Output Assignments 7 5 7 4 F4 Displays Output Ranges Used to Adjust Scale of Analog Output
89. witch to the parameter input mode by pressing the Enter key after calling the corresponding parameter screen The input cursor horizontal bar under the first character then appears in the active edit field black background The cursor can be positioned with the right and left cursor keys and the value displayed number or letter can be changed with the up and down cursor keys or entered directly Every inout has to be concluded by pressing the Enter key again which causes the cursor to disappear California Analytical Model 600 HCLD C_ETL_US CE Operators M March 2006 Page 11 of 71 Section 5 OPERATING STRUCTURE 5 Operating Structure The analyzer s operation can be divided into up to 4 operating levels The current level is always displayed as a stack of 1 to 4 horizontal bars in the top right corner of the screen In the access level menu you can choose between the following operating levels F1 User operating level 1 F2 Advanced user operating level 2 F3 Maintenance operating level 3 F4 System user operating level 4 A password can be assigned to each operating level Only the system user who normally has the highest operating priority can assign the password At the factory the default passwords for the CAI analyzers are set as follows User 111 Advanced user 222 Maintenance 333 System 444 The default setting can be changed only by the system user This manual is written to include all information for the
90. x NOTE Use the down arrow key to obtain the additional setup parameters mi gt 2 mM a b gt lt o U d i poe Lt ih aaa ie oo Dba T iT Setup Menu 2 California Analytical Model 600 HCLD C_ETL_US CE Operators Mi March 2006 Page 23 of 71 Section 7 MAIN MENU 7 5 1 F1 Span Gas Concentration For calibration it is necessary to input the concentration of the span gas in ppm For every range the span gas concentration can be changed After pressing F1 in the setup menu a screen appears in which changes can be made Select with the cursor buttons the range to change The selected field turns black To change parameters switch to parameter input mode by pressing the Enter key The input cursor horizontal bar under the first character then appears in the active edit field black background The cursor can be positioned with the right and left cursor keys and the value displayed number or letter can be changed with the up and down cursor keys or entered directly Every input has to be concluded by pressing the Enter key again Then the input cursor disappears and a new range can be selected The changes are saved by leaving the screen by pressing Main or Back At the right side of the screen the range limits of the 4 ranges are displayed They cannot be changed in this screen Setup Z Span gas conc range limites Rangel 20 2 UU 30 Range2z po A OTS 100

240 Fld Instruction Manual - California Analytical Instruments, Inc.

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