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SITRANS CV

1. 5g Se z s u 02 85 60 TZ Pi STIES 260 Ep 05 60 TT 8p 60 6E 5h 60 202 7260 SE 0F 60 SEO 8 60 TE SE260 6S1 ZE160 Zi0 GGIZ fEZiS TS 2 6T 0 tipii STIST 60 ZpiZT 60 OT OT 60 8E120 60 90 60 60 pE Z0 60 20 00 60 TOE 25 80 60 60 60 60 60 60 60 80 80 80 80 80 80 SST IZE 80 Sep pei go FTT Z 80 6 62 80 20 22 80 GE P2280 EO ZZ 80 TE 6T 80 00 4T 80 82 PT 80 p isasA_euy foD92 eaunaeubLs dnies tpeacuddyion 131815 fDpavsa9ADIS ydeuborewouyd fOT 80 polJead SO TT 002 131k CVControl operating software 101 Operating Manual 11 2012 A5E01428676 03 Viewing and analysis of measured values 9 7 Calculation formulae 9 7 Calculation formulae 9 7 1 Calculation of response factors for the calibrated components The calculation is done using the following formula cal R Ay k cal k Meaning of the various parameters k Component index R Response factor of component k k cal Area of component k in the calibration sample recorded during the calibration A process This can be a mean area cal Concentration of component k in the calibration gas certificate k CVControl operating software 102 Operating Manual 11 2012 A5E01428676 03 Viewing and analysis of measured values 9 7 Calculation formulae 9 7 2 Calculation of stan
2. Stream Stream 1 ba Calculated Values Name Cur Hour 8 Last Hour 24 Cur Day 241 Last Day 567 Cur Month 997 Last Month 0 Cur Config 0 Last Config 0 Sup Calor Val MJ m3 39 9739 39 9756 39 9707 39 9944 39 9959 0 0000 0 0000 0 0000 Inf Calor Val MJ m3 36 0993 36 1009 36 0964 36 1177 36 1190 0 0000 0 0000 0 0000 Density kg m3 0 80706 0 80711 0 80706 0 80672 0 80670 0 00000 0 00000 0 00000 Rel Density unitless 0 6242 0 6243 0 6242 0 6239 0 6239 0 0000 0 0000 0 0000 Wobbe Index MJ m3 50 5951 50 5958 50 5912 50 6320 50 6343 0 0000 0 0000 0 0000 Comp Fac unitless 0 9973 0 9973 0 9973 0 9973 0 9973 0 0000 0 0000 0 0000 100 Nom unitless 0 9994 1 0002 1 0009 1 0014 1 0015 0 0000 0 0000 0 0000 m Components Name Cur Hour 8 Last Hour 24 Cur Day 241 Last Day 567 Cur Month 997 Last Month 0 Cur Config 0 Last Config 0 Oxygen 0 0493 0 0493 0 0492 0 0476 0 0474 0 0000 0 0000 0 0000 Nitrogen 3 9952 3 9954 4 0044 3 9427 3 9389 0 0000 0 0000 0 0000 Carbon Dioxide 1 4809 1 4812 1 4778 1 4793 1 4798 0 0000 0 0000 0 0000 Methane 88 9475 88 9416 88 9435 89 0088 89 0120 0 0000 0 0000 0 0000 Ethane 3 9877 3 9921 3 9854 3 9836 3 9838 0 0000 0 0000 0 0000 Propane 0 9890 0 9897 0 9895 0 9866 0 9867 0 0000 0 0000 0 0000 Butane 0 1983 0 1984 0 1983 0 1984 0 1984 0 0000 0 0000 0 0000 Isobutane 0 2011 0 2012 0 2010 0 2014 0 2014 0 0000 0 0000 0 0000 Pent
3. Device Id SICVEF7BES ee oreto croi General p AppValues Method Name Type Allow Writing Unit Group a Calibration CalibrationResult Actual CalibrationN orm REAL Calibration Settings CalibrationResult Actual CalibrationT ime DATETIME Calibration Gas CalibrationResult Actual Concentration Argon REAL Alarm Limits CalibrationR esult Actual Concentration Butane REAL Alarm Settings CalibrationResult Actual Concentration ButaneAndN eopentane REAL Hardware CalibrationR esult Actual Concentration CarbonD ioxide REAL E Modbus Configuration CalibrationR esult Actual Concentration CarbonM onoxide REAL sal eae CalibrationResult Actual Concentration E thane REAL z f Capabilities apabihtie Map Adapters Name REALtoSCALED REAL wi ScaleFactor Intl6 BadValue Intl6 EUHI Real EUHlAddr Address DWORDtow2 DWORD W2 v DWORDtow2ENRON DWORD W2ENRON v DWORDtow1 DWORD Wi v DINTtow2 DINT W2 v DINTtow2ENRON DINT W2ENRON MI DLI ati Lal m MbValueT ypes Name Base Type Count Byte Count Require Write Access R1 REGISTER 1 REGISTER 2 REGISTER 1 BIT 1 m Unit Groups Name its Dea a Apply Undo Chromatograph SICVEF7BES Connected CyclicRun 152 sec 210sec e AppValues contains all information which the device can provide with Modbus e Adapters maps data of the gas chromatograph AppValues in Modbus compatible data types and vice versa CVControl operating software Operating Man
4. Only the 2 marked components are calibrated Components which are not to be calibrated must have a response factor RF assigned to them Components which are to be neither measured nor calibrated are set to Ignored Components used to calculate the calorific values are set to Standard Components not used to calculate the calorific values are set to Additional CVControl operating software Operating Manual 11 2012 A5E01428676 03 Calibrating 4 2 Requirements for calibrating Note Adding new components e New components peaks are first assigned in the navigation area under the group Method and the property object Peaks The new components are then listed under Measured Components e Certified mode Entry of anew component may make the certificate invalid WA cvcontrol Transmitter User Interface NOT SEALED CONFIGURE 5 xj File Tools Help Device Status Report Mean Values Results Trend Calibration Result Chromatograms Logbook Device Setup E Device Id SICVEFTBES pete Mose ted Components General No EZChromName Usage PhysicalProperties Reported As Calibrated Name forRF RF Correction E Method 1 021 Standard Oxygen Oxygen v 02 1 1 00 Cycle Events 2 N21 Standard Nitrogen Nitrogen v N21 1 00 Integration Events 3 CO2_4 Standard CarbonDio
5. Cancel Calibration Enable Streams 1 500 1 200 0 600 1 400 Ready Ready Name Status Value FlushLoop C_CH1 Ready Sample C_CH2 Ready Backflush C_CH3 Injection C_CH4 Electronics Name Status MMI1 Ready Ready Active Alarms and Warnings Status Description Chromatograph SICVEF7B48 Connected CVControl operating software Operating Manual 11 2012 A5E01428676 03 Operation 3 3 Locking of operation for calibrated mode 3 3 Locking of operation for calibrated mode Note Noting of password Each password can only be used once When locking is repeated a new password must be assigned If you forget the password you cannot leave calibrated mode If the chromatograph is to work in calibrated mode the calibration official will assign a password Tools menu gt Set new password Access Mode must be set to MONITOR In calibrated mode you can only use MONITOR mode In MONITOR mode only a few parameters can be changed e g the enabling of samples Calibrated mode is exited as soon as you change to CONFIGURE mode using the password menu Tools gt Change Access Mode Note You can also use the lock in non calibrated mode e g to protect against unauthorized access CVControl operating software
6. BA cvControt Transmitter User Interface NOT SEALED CONFIGURE Fle Tools Help Device Status Repot MeanValues Rests Trend CaibrationResut Chromstogrems Logbook Device Setup r Alum Log Modde GENERALI SampleSteam Alam Rased 2 2507 2007 135955 Modde ETC3 Deviation exceeded Gone _ 3 25 07 2007 135944 Modde ETC2 Deviation exceeded Gone 42507 2007 135930 Module ETC2 Deviston exceeded Ramed _ 5 25 07 2007 135930 Modde ETC1 Devistion exceeded Gone 6 25 07 2007 1359 25 Modde ETC2 Deviation exceeded Gone 25 07 2007 13 59 14 Modde ETC Deviation exceeded Raived 2507 2007 1359 09 Modde ETC1 Deviation exceeded Gone 9 25 07 2007 135754 Modde EPC1 No oss supply Gone 10 25 07 2007 1357 50 Modde ETC1 Deviston exceeded Razed 11 25 07 2007 135750 Modde ETC2 Deviation exceeded Raised Message mM 14082 y ChangeSetup new Setup CRC is DESD 13 08 2007 1819 33 ChangeSetup new Setup CRC is CREB 2507 2007 1527 19 ChangeSetup new Setup CRC is 7080 25 07 2007 132400 SetTimeZore new time zore is GMT 01 00 Amsterdam Berin Bom Rome Stockholm Vienna tbh DaybghtSaving 25 07 2007 152535 SetTma new time is Mittwroch 25 Juk 2007 13 24 00 25 07 2007 152523 ToMode rew mode is CycicRhun 25 07 2007 150027 ToMode raw mode it SingleAun 25 07 2007 150023 ChangeSarpleEnsble Sample 1 enabled 2507 2007 150023 ChangeSarmpleEnable Sample 1 enabled 25 07 2007 13 59 30 ChangeSetup new Setup CRC is DF41 25 07 2007
7. Chromatograph SICVEF7BE6 Connected CyclicRun 62sec 150sec CVControl operating software 84 Operating Manual 11 2012 A5E01428676 03 Analysis control and operating modes 8 7 Possible operations e Alternatively this checksum is displayed under WA cycontrol Connected CVControl operating software Operating Manual 11 2012 A5E01428676 03 85 Analysis control and operating modes 8 7 Possible operations e In addition to the total checksum a partial checksum is assigned as follows by the operating software to each part of the factory setting Control Transmitter User Interface NOT SEALED CONFIGURE File Tools Help Device Status Report Mean Values Results Trend Calibration Result Chromatograms Logbook Device Setup E Device Id SICV6F7B4C p General Setup Integy E General Setup Part Checksum Setup Item Checksum a Clock Fix Setup FAZAIBFC INITIAL VALUES FA7AIBFC Versi ii Une Individual Setup SC3006E8 REFERENCE VALUES 5C3006E8 ii il Streams APPROVED_VALUES 5ADE95BE Data Storage EXPECTATION_RANGES 3B324646 iapploved yates CALCULATION_SETTINGS 5B16ACRE Pipay CALIBRATION_LIMITS 9637ECB2 Alarm Settings ARAA A CALIBRATION_SETTINGS AQEDBE77 Ewpecialiii Annas DISPLAY_SETTINGS 193D0FCE pansy STORAGE_SETTINGS 15910319 Standb
8. RSP firmware 00014024 SITRANS CV as of version 2 01 00 e CVControl can only be used with the following Siemens chromatographs SITRANS CV e The following Siemens chromatographs are not supported by CVControl MAXUM edition II MicroSAM CVControl operating software 10 Operating Manual 11 2012 A5E01428676 03 Installing the software 2 2 Minimum PC requirements 2 2 Minimum PC requirements Pentium 800 MHz 128 MB RAM 256 MB recommended Hard disk 250 MB vacant capacity depends on data quantity produced CD ROM or DVD drive Graphics card and monitor with 1024 x 768 pixels resolution and 16 bit color depth Display of fonts in normal size Mouse and keyboard Network card or Ethernet interface integrated on the motherboard Windows XP or Windows 7 operating system CVControl operating software Operating Manual 11 2012 A5E01428676 03 11 Installing the software 2 3 Installing the operating software 2 3 Installing the operating software Note Administrator privileges are necessary for installation of the CVControl software program Scope of delivery The scope of delivery of the software package includes the following CDs e Control software e Country Specific Setups e Parameter Backup Installing the software Procedure 1 Turn on the PC and start Windows 2 Place the Control Software CD into the drive If the installation program on the CD does not start up automatically start
9. 89E9 88 990S TO 8p80 pO PETTS O fOTST OF 60 988 966h TO SETZO PO F6STTS O f PSST OF 9029 88 266 TO TSZ0 p0 6STT8 0 62ST OF 8599 88 f46r TO O840 PO 6STT8 O cesTt Or TESPO BS ZEOS TO SOOO Z8TT8 0 F89ST Or TES99 RS STZOS TO 2640 PO FPOTTS O FZ0ST OF BE6O BS 496h TO 2T40 PO F8ETTS O FEBPT OF PSS9 B8 B00S TO 6S 40 PO FTATTS O FT ST Or SEQO BR FZTOS TO 0440 PO S69TTS O frrST OF 6ES9 88 SOLOS TO SZTRO PO EZTT8 0 fPZST Or Tr 9 88 POOS TO SEZO PO fPSTTS O S80ST OF t989 88 GOGP TO 8490 FO GETT8 O SSTST Or T2 9 88 O86h TO 4940 PO fPSTTS O FTTST Or PTZ9 88 O66h TO SEP40 PO FOSTTS O 29ZST OF SPSO BS8 FEZOS TO S 40 PO FEZTTS O FTSST OF 6EE9 BSB 6POS TO OT8O HO FE6TTS O fPaST OF OT99 88 TOOS TO 6940 PO EOTT8 O FZEST OF PBS9 88 E0OS TO 2080 FO pOTT8 O STTST Or OS0Z 88 SEGP TO 650 FO SZTT8 0 ErST Or 6SP9 S8 ZZOS TO ETRO PO Z8TT8 0 fEZsT Or OT69 88 OrGh TO 96S0 pO FZ2PTT8 O f809T OF BEEQ BS iZpOS TO SSTRO PO STETTS O fPasT OF Z2PS9 88 686h TO 9 40 PO FZATT8 0 FZE9T OF BEZO BE BEOS TO 4 80 PO IS6TTR O fS4ST OF T269 88 T26 PTO 2990 pO GETT8 0 FETST OP TS69 88 4 6P TO 9E90 pO TRTT8 O 64ST OF 09p9 88 OTOS TO 6TB0 PO ZATT8 O f4SST Or 9T29 88 fES6p TO fZTZO O fZSTT8 0 f68ST Op
10. Note Administrator privileges You require administrator privileges on your computer in order to set the IP address of your PC Ask your system administrator or read the Windows help For communication between the PC and the gas chromatograph set the IP address of the chromatograph such that it matches the IP address of the PC CVControl operating software 14 Operating Manual 11 2012 A5E01428676 03 Installing the software 2 4 Setting the IP addresses 2 4 1 Changing the IP address of the chromatograph e The factory set IP address in the gas chromatograph is 161 218 51 xx xx corresponds to the last two digits of the serial number on the rating plate e The preset subnet mask is 255 255 255 0 Example If the serial number of the gas chromatograph is HX R5 347 the IP address is then 161 218 51 47 Procedure NOTICE Device damage through incorrectly set network transmission rate e Seta maximum of 10 Mbps for the network transmission rate e lf you set a higher rate than 10 Mbps the device will be damaged and no longer function correctly e You must then return the device to Siemens AG for repair If you require an IP address and subnet mask for the device other than the preset values 1 Start the program Remote IP Configurator start bar Start gt Programs gt Siemens AG gt CVControl gt Tools gt RemotelPConfig Remote IP Configurator x Device Type Netmask Device
11. e Byte Formats e Constant Values e Map Entries WAcvcontrol Transmitter User Interface NOT SEALED CONFIGURE e You can shift the offset using the drop down list Modbus Address Offset e In the drop down list you can select between 0 and 1 0 no shift of offset e g start at 1000 1 shift of offset by 1 e g start at 1001 CVControl operating software Operating Manual 11 2012 A5E01428676 03 111 Transmission of results over Modbus 10 2 Changing MODBUS parameters Byte Formats In Byte Formats you can define the sequence and arrangement of a 16 bit or 32 bit register 1 Click Byte Formats in the navigation area 2 Enter your required values for SBO SB1 SB2 and SB3 in the respective lines WA cY Control Transmitter User Interface NOT SEALED CONFIGURE Mije xj Fie Tools Help Device Status Report MeanValues Results Trend Calibration Result Chromatograms Logbook Device Setup Modbus Configuration Map Byte Formats E Device Id SICVEF7BE8 General Method E Calibration Calibration Settings Calibration Gas Alarm Limits Alarm Settings Hardware E Modbus Configuration Device Settings Capabilities E Map Constant Values Map Entries Bhromstograph SICVEFTBES Connected Rey odn oseese 3 To confirm your inputs click Apply Constant Values In this dialog box set the constants to be transmitted wi
12. start bar Start gt Programs Siemens AG CVControl gt CVControl WA cYControl Transmitter User Interface NOT SEALED CONFIGURE File Tools Help Report Mean Values Results Trend Calibration Result Chromatograms Logbook Device Setup M Current State M Mode Select m Streams a are Wane yclicRun DE f Calibration Single Run Actual stream gt Samplet lt Next stream Elapsed Time Run Time 2 Sample2 Hold Sample3 CI oe Osec 150 sec Cancel Calibration Enable Streams Temperatures Status Heater Temperature C Setpoint C Ready v 66 9 Ready 66 9 Ready 65 3 78 141 0 527 Status Pressure kPa Setpoint kPa Ready 288 5 290 0 Ready 219 6 221 7 Ready 227 4 230 0 FlushLoop C_CH1 Sample VE_CH2 Backflush C_CH3 Injection VC_CH4 Description Electronics Name Status MMI1 Ready Chromatograph SICVEF7B48 Connected CyclicRun 17 sec 150sec 2 Select the Load Setup command in the File menu Control Transmitter User Interface NOT SEALED CONFIGURE l File Tools Help Save Setup s N Save Results As Mean Values Results Trend Calibration Result Exit 3 Load your previously saved configuration data 4 Check the configuration and functionality of your de
13. 2 4 2 Procedure 2 5 Requirements 2 5 SITRANS CV software upgrade Setting the IP address of the PC Start the program Network connections start bar Start gt Control Panel Network connections Click on the right on the associated Ethernet connection e g Local Area Connection 2 Select Properties in the dialog box Click in the list on Internet Protocol TCP IP and then the button Properties Select the checkbox Specify an IP address and enter the IP address and subnet mask SITRANS CV software upgrade Note Only start a software upgrade when this is absolutely necessary e g if the new software functions are essential for the gas chromatograph A software upgrade could possibly result in malfunctions on your gas chromatograph and you would then have to adapt and parameterize it for the new functions Note Upgrading the Flash memory Back up all data and device parameters before starting a software upgrade All data present in the Flash memory are permanently deleted by the software upgrade Upgrading of the SITRANS CV process gas chromatograph is only permissible if a corresponding supplement for the device is present in your local approval Never interrupt the Flash process since the Flash memory in this case can only be reestablished by Siemens AG The SITRANS CV process gas chromatograph the PC and the Windows operating system are in operation CVControl op
14. 4 3 Start calibration cycle 4 3 1 Start calibration cycle manually You can start a calibration cycle manually e g for the annual calibration by a calibration official The chromatograph then calculates the calibration factor for every component Procedure e Inthe window CVControl of the tab Device Status click in the Mode Select dialog box on Calibration Mode Select Cyclic Run T Standby Single Run Hold Calibration Cancel Calibration e The calibration cycle begins once the ongoing analysis has been completed or immediately if the chromatograph was at Hold e Following the calibration cycle the chromatograph returns to the state it was in prior to the calibration CVControl operating software 46 Operating Manual 11 2012 A5E01428676 03 Calibrating 4 3 Start calibration cycle 4 3 2 Starting the calibration cycle with digital input Procedure Setting the digital input in the gas chromatograph starts the calibration procedure 4 3 3 Starting the calibration cycle with Modbus You can also start the calibration cycle with Modbus The description for calibration can be found in Section Transmission of results over Modbus Page 105 4 3 4 Automatic tracking of calibration factors The chromatograph starts a calibration cycle at a defined time of day at intervals of one or more days The calibration factors are corrected automatically in the process The calibration cyc
15. Address area 113 Industry standard 107 Mode SEALED 84 MONITOR 83 Operating mode 27 N Natural gas 10 Network Connection establishment 14 Hub 15 IP address 14 15 Subnet mask 15 Switch 15 Topology 14 Transmission rate 15 ngcontrol config 100 NGControl config Configuration file 20 Non standardized values 122 CVControl operating software Operating Manual 11 2012 A5E01428676 03 Index O Operating mode Calibrating 75 CONFIGURE 26 27 Cyclic analysis 75 MONITOR 26 27 Single analysis 75 Standby 75 80 Operating software Installation 12 Scope of delivery 12 Optimization of method Cycle events 52 Integration events 52 Optimization procedure 53 P Parameter Calculated values 49 Parameters 47 Calibration cycle 37 Calibration Details 48 Calibration of limits 41 Changing 30 Commands 30 Concentration 48 Deviation 48 Input 30 Logical values 30 Monitoring 62 Numerical values 30 Result of analysis 87 Saving 13 Password 29 PC Hardware requirements 11 Operating system 11 Peak 53 Printing Starting 100 Stopping 100 Process control system 107 Product information on the Internet 129 PTB approval 17 Q Qualified personnel 7 CVControl operating software Operating Manual 11 2012 A5E01428676 03 R Rating plate Serial number 15 Remote IP Configurator 15 RemoteFlasher 18 19 Response factor 103 105 Restore Application data 20 Reten
16. Chromatograms Logbook Device Setup M Method Cycle Events Events El Device Id SICVEF7B48 General Name Event Use Det Mode Time Cur Rue Shift Relative Weioht Peak1 Peak 2 E Method _Stream Step_01 Stream Step Mo All AllModes At gt 9 00 Fixed 0 00 0 500 1 000 E Cycle Events _Balance Detector Balance Detector V Al AllModes At gt 20 00 Fixed 0 00 0 500 1 000 Detectors AlarmOft Flow AlamOFF M Al AllModes At gt 30 00 Fixed 0 00 0 500 1 000 Pressures AlarmO low Alarm ON CER c oo00 0 500 1 000 Valves Integration Events Peaks Groups Measured Components Auxiliary Components Calibration Hardware Modbus Configuration Chromatograph SICV6F7B48 Connected Ready CyclicRun 144 sec 150 sec Example Change Follow Alarm Off to 30 s Change Follow Alarm On to 30 s Result A time interval of 60 seconds is set and can be used CVControl operating software Operating Manual 11 2012 A5E01428676 03 Status 6 5 Sample tlow monitoring 5 Activate alarm In the navigation area open the General group Click on the property object Alarm Settings Select the line SampleStream Alarm in the list General Alarm Settings Select Alarm in the drop down list BA cyControt Transmitter User Interface NOT SEALED CONFIGURE Fle Tools Heb Device Status Repot MeanValues Resuts Trend CaltrationResut Chromatograms Logbook
17. Click the option box Cyclic Run in the dialog box Device Status of the option box Mode Select In operating mode Cyclic Run the gas chromatograph executes the sample stream sequence list cyclically Once the analysis has been finished the analysis clock is reset to zero and the gas chromatograph automatically starts the next analysis Note Power failure If a power failure occurs in Cyclic Run mode the gas chromatograph restarts automatically Cyclic Run is continued following a calibration cycle CVControl operating software Operating Manual 11 2012 A5E01428676 03 77 Analysis control and operating modes 8 3 Stopping the analysis 8 3 Stopping the analysis Note It is not possible to immediately stop an ongoing analysis by means of an operator input Click the option box Hold in the dialog box Device Status of the option box Mode Select e The chromatograph continues up to the end of the current analysis e The chromatograph then switches to the Hold state 8 4 Analysis clock The chromatograph controls the analyses using device internal timebase Analysis duration Run Time Note You must enter the point in time Injection Lag as a negative value in the time program This time is added as a positive value to the Cycle Time in order to calculate the analysis duration e The analysis duration Run Time is the total of the parameter values Injection Lag and Cycle Tim
18. Cycle Events 0 00 Fixed soj 100 Sooo OE manm Evens _Mindrea_1_01 TCD_1 Mindrea 40 0000 ae 2 hoe bees cheer Components _Threshold_1_01 TCD_1 Threshold 20 0000 2 a Fred ron a peer oni ros hon cum gt DESY 8 8 ae E Modbus Configuration TangentSkim_1_01 TCD_1 TangentSkim 1 0000 a a Reeve gu a fed st CHAT moe Tog or camo it BON 30 aan y ValleyValley 101 TCD_1 ValleyValley 1 0000 2 a an a fee a ar _ResetBL_1_01 TCD_1 ResetBL mo 00000 Sx an anit ae asm on c21 _Threshold_2_01 TCD_2 Threshold 30 0000 2 om Frea a a es wna 02 wah tom Sa 9d r ol 02 mk oom Sa Bnd OOH am Theshold_3 01 TCD_3 Threshold A 30 0000 a i fed an a aw wn 0 9 win tao gt GR 00 gao mo COO gt Md G0 Tae wnt 1 4 win tat gt E r _Threshold_4_01 TCD_4 Threshold MM 20000 a 2 TE is a coe i Chromatograph SICV6F7BE6 Connected Ready FlashPending Cyclic Run 37 sec 150 sec CVControl operating software Operating Manual 11 2012 A5E01428676 03 53 Optimization of method 5 2 Parameterization of events Select optimization procedure 54 There are three optimization procedures Fixed Shift and Relative In addition generation of a mean value is possible between the existing and new values Weight Fixed directly uses the retention time entered under Current Shift adds the entered value in seconds to the retention time of the peak specified under Peak 1 Relative specifies the pos
19. Data loss A system restore with data from the parameter backup CD overrides the country specific setup in the manner described here See also Calibrating Page 33 Optimization of method Page 51 Transmission of results over Modbus Page 105 CVControl operating software 22 Operating Manual 11 2012 A5E01428676 03 Installing the software 2 7 Restoring data 2 7 3 Setting the calibration gas Requirements The composition of the calibration gas must match the optimization instructions of the country specific setting Also refer to the Readme Pdf file on the CD Country Specific Setup Procedure Proceed as follows 1 Enter the concentration of the calibration gas 2 Calibrate and optimize the device according to the information in the Sections Calibrating Page 33 ff and Optimization of method Page 51 ff 3 Check the repeatability 2 7 4 Parameterization and saving of Modbus See Section Transmission of results over Modbus Page 105 ff CVControl operating software Operating Manual 11 2012 A5E01428676 03 23 Installing the software 2 7 Restoring data CVControl operating software 24 Operating Manual 11 2012 A5E01428676 03 Operation 3 Requirements for operation e The chromatograph must be correctly connected to the PC e The CVControl software must be installed e The IP address of the chromatograph must match the PC 3 1 Fundamentals for operation Which parameters y
20. Device Senp Cheomatogeph SIOVEFTBEG Corrected Ready oan aee CVControl operating software Operating Manual 11 2012 A5E01428676 03 69 Status 6 5 Sample flow monitoring 70 Effect 1 A red box with the wording ALARM is displayed in the tag menu Device Status if no sample flow or an insufficient flow is present C Control Transmitter User Interface NOT SEALED CONFIGURE ioj x File Tools Help Device Status Report MeanValues Results Trend Calibration Result Chromatograms Logbook Device Setup M Current State Mode Select Streams Cyclic Run aa a iSite 1 X_ Calibration Single Run Actual stream gt 1 X Samplet lt Next stream Elapsed Time ____ 65 Run Time 2 Sample2 O Hold 3 Sample3 s Osec 150 sec Cancel Calibration Enable Streams TCD1 TCD2 Ready 1 202 1 200 78 141 TCD3 FlushLoop C_CH1 Sample C_CH2 Backflush VC_CH3 Active Alarms and Warnings Injection C_CH4 Posted Time Status Description 27 09 2007 14 50 42 Alarm GENERAL1 SampleStream Alarm Name Status MMI1 Ready Chromatograph SICV6F7B48 Connected CVControl operating software Operating Manual 11 2012 A5E01428676 03 Status 6 5 Sample tlow monitoring The entry Sample Stream Alarm is then made in the logbook
21. E Hardware Temperature Controller Pressure Controller Detectors Valves Electronics Modbus Configuration Chromatograph SICV6F7BE6 Connected Ready Calibration 101 sec 150 sec In this example you are analyzing daily between 10 00 and 12 00 a m as well as between 03 00 and 08 00 p m CVControl operating software 80 Operating Manual 11 2012 A5E01428676 03 Analysis control and operating modes 8 6 Standby Result In Standby mode the device returns to the initialization pressures and thus reduces the consumption of carrier gas helium Example The initialization pressure setpoint initial kPa is set to 50 kPa for the pressure controllers EPC1 EPC2 and EPC3 see the following window WA cYControl Transmitter User Interface NOT SEALED CONFIGURE 15 x Fie Tools Help Device Status Report Mean Values Results Trend CalbrationResut Chromatograms Logbook Device Setup E Device Id SICVEF7BE6 poeeun General Parameter Name EPC2 EPC3 Method Status ooo Ready Calibration Actor ooo v E Hardware Temperature Controller E Pressure Controller Absolute Limite aaam Limas Alart Settings Danna Valves Electronics Modbus Configuration Fo A Chromatograph SICVEF7BE6 Connected Ready CyclicRun 89 sec 150 sec CVControl operating software Operating Manual 11 2012 A5E01428676 03 81 Analys
22. Standby mode if you only wish to analyze at certain times This saves carrier gas Note Standby mode can only be selected manually in CONFIGURE mode If Standby mode cannot be selected e g in calibrated mode parameterization of the country specific setting is carried out CVControl operating software Operating Manual 11 2012 A5E01428676 03 79 Analysis control and operating modes 8 6 Standby Starting standby mode 1 Click the option box Mode Select in the tab Device Status and then the option box Standby M Mode Select Cyclic Run I Standby Single Run Hold Calibration Cancel Calibration 2 Click the tab Device Setup and select Standby Settings in the navigation box 3 Enter the Standby values under Number e g in lines 1 and 2 WA cYControl Transmitter User Interface NOT SEALED CONFIGURE 5 x Fie Tools Help Device Status Report Mean Values Results Trend Calibration Result Chromatograms Logbook I Device Setup Device Id SICVEF7BES pemaes Sates General Number Enabled Begin Analyze Time of Day End Analyze Time of Day Clock cS Version Units Streams Data Storage Approved Values Display Alarm Settings Expectation Ranges E Meth E Cycle Events Detectors Pressures Valves Events Integration Events Peaks Groups Measured Components Auxiliary Components Calibration
23. The chromatogram The retention time The component peak name The peak markers CVControl operating software Operating Manual 11 2012 A5E01428676 03 Viewing and analysis of measured values 9 2 Displaying chromatograms Scaling the chromatogram in the window fn Te TCD2 Sample1 13 09 2007 15 57 38 Drag the desired section using the mouse Clicking with the right mouse button cancels one step at a time The horizontal shift bar indicates the position of the zoomed area You can also shift increase or decrease the scaled area here You can shift the chromatogram vertically by dragging the Y scale with the mouse Printing the chromatogram If a printer is connected to the PC you can print out the chromatogram which is currently displayed in the window Click the Print button The Windows print dialog is displayed CVControl operating software Operating Manual 11 2012 A5E01428676 03 91 Viewing and analysis of measured values 9 3 Mean values 9 3 Mean values The chromatograph saves the mean values of all components and the calorimetric values It is thus possible to track changes in the sample composition Displaying of mean values e Select the tab Mean Values WA cvcontrol User Interface NOT SEALED CONFIGURE a isl 3 File Tools Help Device Status Repot ican Values Resuts Trend Calibration Resut Chromatograms Logbook Device Setup
24. 1357 27 MearVahuesDifeetChsnged new offset is 6 2 The analysis is invalid i e e All concentrations are set to zero e This analysis is not included in generation of the mean value Note Alarm remains present If the alarm remains present the device stops and no new analyses can be started Remedy e Eliminate the source of the error or the cause of the alarm Following elimination of the causes the device continues working without a restart CVControl operating software Operating Manual 11 2012 A5E01428676 03 71 Logbook T The chromatograph automatically saves all faults and events in a chronological list To provide a better overview it lists faults and manual interventions separately e The Alarm Log list records all alarms Warnings are not recorded Examples deviations of temperature or pressure controllers e The Event Log lists manual interventions Examples changes in the factory settings switching on switching off change to calibrated mode Note Synchronization of logbook Using the Refresh button you can synchronize the contents of the logbook on the PC with the gas chromatogram Printing of logbook If a printer is connected to the PC you can print out the logbook Click the Print button in the Logbook tab in the Alarm Log or Event Log area The Windows print dialog is displayed Saving of logbook on hard disk 1 Click the Save As button in the
25. If the device state changes to alarm the 14th bit is set to 1 Device OEM1 Errors 3047 Always zero Device OEM1 StreamMask 3035 Bit 2 1 implies that Masking of sample streams sample stream n is combined with the table of connected components Bit 2 1 means that sample stream n is connected All bits are currently set to 1 for all sample streams 10 2 2 2 General sample stream information Applicable for Calibration Stream Sample1 Sample2 and Sample3 Sample stream parameter Values value range Description Sample1 Enabled value 0 e Correct if the sample stream is approved e Writable CVControl operating software Operating Manual 11 2012 A5E01428676 03 117 Transmission of results over Modbus 10 2 Changing MODBUS parameters 10 2 2 3 118 Result values Result parameters Sample1 AnalysisID Values value range Description Number representing the change for the last result of this sample stream Sample1 InjectionTime Date and time at which the injection took place Sample1 0EM1 CalOrAnalysisF lag 3059 e 1 for all valve streams e 0 for the calibration stream Value to differentiate between measurement and calibration Sample1 0EM1 NewDataFlag 3058 value 0 e New data present e Correct if a new result is available for this stream e Writable can be deleted to 0 by the reader Modbus master Sample1
26. Logbook tab in the Alarm Log or Event Log area 2 Select the directory and file name The logbook entries are saved as a csv file Ifyou specify txt as the file name extension the logbook is saved as a text file CVControl operating software Operating Manual 11 2012 A5E01428676 03 73 Logbook CVControl operating software 74 Operating Manual 11 2012 A5E01428676 03 Analysis control and operating modes 8 1 Overview 8 The selected operating mode determines whether the gas chromatograph carries out one or more analyses The gas chromatograph has the following operating modes e Single analysis e Cyclic analyses e Calibrating e Standby CVControl operating software Operating Manual 11 2012 A5E01428676 03 75 Analysis control and operating modes 8 2 Starting an analysis 8 2 Starting an analysis Before starting Prior to the analysis the initial state for it must be established Wait until the chromatograph signals Ready If you start the analysis while the chromatograph is still in the Not Ready state the chromatograph will only start the analysis when the Ready state has been reached Start single analysis Single Run WA cYControl Transmitter User Interface NOT SEALED CONFIGURE File Tools Help Device Status Report Mean Values Results Trend Calibration Result Chromatograms Logbook Device Setup M Current State M Mod
27. Status Alarm value 0 Correct if an alarm occurs during the analysis Sample1 Status DataNotValid value 0 Correct if the result is invalid Sample1 Status Revision value 0 Correct if the revision bit switch was set for this result The revision analysis does not contribute to the mean values Sample1 Status Warning value 0 Correct if a warning has occurred during the analysis This value is not currently set by the device Sample1 100PercentNorm Standardization factor see Section Calculation formulae Page 102 Sample1 Status OutOfRange value 0 Is correct if the result is outside the expected range CVControl operating software Operating Manual 11 2012 A5E01428676 03 Transmission of results over Modbus Component values 10 2 Changing MODBUS parameters e Component values are the area concentration and dwell time These three values are available for each supported component e The operating software for the gas chromatograph supports 23 individual components and 3 group components Note Not all of these components can be measured using all analysis modules Individual components Acetylene Air Ammonia Argon Benzene 1 2 Butadiene 1 3 Butadiene Butane 1 Butene cis 2 Butene trans 2 Butene Carbon dioxide Carbon disulfide Carbon monoxide Carbonyl sulfide Cyclohexane Cyclopentane Decane 2 2 Dimethylobutane 2 3 D
28. Version 08 00 06 6f 7b e8 WinCE 10 116 38 108 255 255 254 0 SICV 1 04 00 retail bu 08 00 06 6 7b 4d WinCE 10 116 38 109 255 255 254 0 SAM 2 07 00 retail bu 08 00 06 6f 7b b4 WinCE 10 116 38 90 255 255 254 0 SAMC 1 23 00 retail Scan Close J 2 Click the Scan button Note No gas chromatograph visible in the Remote IP Configurator If no chromatograph appears check the physical connections A common physical network with hub switch must be present If a PC with several network adapters is used make sure that the network connection is assigned correctly CVControl operating software Operating Manual 11 2012 A5E01428676 03 15 Installing the software 2 4 Setting the IP addresses 3 Select the desired chromatograph under Device 4 Click on Modify The Set device configuration dialog box opens x device MAC address 08 00 06 6f 7b b4 fio MBit s x Halt duplex x Obtain an IP address from a DHCP server Specify an IP address IP address 161 218 51 90 Subnet Mask 25 25 255 0 Default Gateway 0 0 0 DO 5 Specify the desired IP address and the desired subnet mask 6 Confirm with OK 7 Exit the program Remote IP Configurator using Close Restart Following confirmation with OK the gas chromatograph restarts automatically CVControl operating software 16 Operating Manual 11 2012 A5E01428676 03 Installing the software
29. e Current date and time of device e Writable Device OperationMode Actual 0 unknown 1 hold 2 cyclic 3 single run 4 calibration Current operating mode of device Device OperationMode Next 0 unknown 1 hold 2 cyclic 3 single run 4 calibration e Current operating mode of device e Writable Device Sampleld Actual 1 set stream 0 unknown 1 sample stream 1 2 sample stream 2 3 sample stream 3 The number assignments of the streams currently being analyzed Device Sampleld Next 1 set stream 0 unknown 1 sample stream 1 2 sample stream 2 3 sample stream 3 The number assignments of the streams to be analyzed next Device CyclelsRunning value 0 Correct if an analysis is currently running Device CycleLength Total duration of current analysis in seconds Device CycleTime Expired seconds since start of current analysis Device CalibrationCycle Current Number assignment of analyses during calibration CVControl operating software Operating Manual 11 2012 A5E01428676 03 Transmission of results over Modbus 10 2 Changing MODBUS parameters Device parameter Values value range Description Device CalibrationCycle Required Number of analyses required for a calibration procedure Device OEM1 Errors 3046 Only the 14th bit Analyzer Failure of the gas chromatograph is used
30. is an open protocol Modbus is used to connect a master e g a PC and several slaves e g measuring and control systems There are two versions of Modbus one for the serial interface and one for Ethernet Non standardized values Concentrations prior to 100 standardization Process gas chromatography Process gas chromatography e Is one of the most powerful measuring and analysis methods for process engineering e s a procedure which is both discrete and extractive e Is frequently used for online monitoring of processes since the sequences are easy to automate and a large number of components can be measured simultaneously e Can be used to separate and quantify the components of almost all homogenous gaseous or liquid mixtures It must be possible to vaporize the liquid components without decomposition The individual components of a discrete sample pass through the column system at different velocities and are recorded in succession by a detector The time between sample introduction and recording of a substance at the detector the retention time is characteristic of the substance and is used to identify it The magnitude of the detector signal is a measure of the volume concentration of the component in the gas CVControl operating software Operating Manual 11 2012 A5E01428676 03 133 Glossary Retention time In contrast to the carrier gases most chemicals interact with the stationary phase i e they are reta
31. keyboard and screen are required to use the CVControl software The manual applies as of software version V02 01 00 NOTICE Qualified personnel Only qualified personnel may use the CVControl operating software and thus the SITRANS CV process gas chromatograph Insufficient or no knowledge of the User s Manual results in cancellation of all liability claims toward Siemens AG Owners are therefore recommended to have the training of personnel confirmed in writing Following installation and starting of the CVControl operating software you see the following startup screen as the GUI for the SITRANS CV WA cY Control Transmitter User Interface NOT SEALED CONFIGURE joj x File Tools Help Curent State Mode Select _ Streams C me E A Nane yclicRun D Eia 5 Calibration Single Run Actual stream gt Samplet lt Next stream Elapsed Time Run Time 2 Sample2 Hold Sample3 s a A Osec 180 sec Cancel Calibration Enable Streams Temperatures Status Heater Temperature C Setpoint C Ready v 66 9 Ready 66 9 Ready v 65 3 TCD1 E 1 500 TCD2 if 1 200 TCD3 0 600 1 400 Pressures Status Pressure kPa Setpoint kPa Ready 288 5 290 0 Ready 219 6 221 7 Ready 227 4 230 0 FlushLoop C_CH1 Sample C_CH2 Active Alarms and Wamings Backflush C_CH3 Inje
32. stream Elapsed Time 0 Run Time 150 Snel 2 Sange Calibration 0 sec 150 sec Cancel Calibration Enable Streams ic Status Warning I k ETC1 Waring Warming Ready Warming Waring Warming Waring Warning FlushLoop C_CH1 Sample C_CH2 Backflush C_CH3 Injection C_CH4 Description TCD1 No gas supply 05 10 2007 14 58 50 Warning 05102007 145BSD Waring TCD2 eae 05 10 2007 14 58 50 Warming TCD4 No gas supply Name Status 05 10 2007 14 58 50 Alarm EPCI No gas supply MMI1 Ready 05 10 2007 14 58 50 Warning EPC2 No gas supply Chromatograph SICV6F7B48 Connected o sec 150 sec e Ifthe carrier gas supply is reestablished the chromatograph is not automatically restarted e A manual restart is necessary in this case CVControl operating software Operating Manual 11 2012 A5E01428676 03 63 Status 6 4 Gas supply 64 e Open the tab Device Setup the group Hardware in the navigation area the property object Pressure Controller and click on the button Reset no gas supply Alarm WA cYControl Transmitter User Interface NOT SEALED CONFIGURE 15 xi File Tools Help Device Status Report Mean Values E Device Id SICVEF7B48 General Method Calibration E Hardware Temperatur
33. stream to pass through the column Deviation of retention time RT Dev This is the deviation of the retention times of this calibration referred to the retention times entered in the window Device Setup gt Method gt Named Peaks Concentration These are the concentrations resulting with the response factors of the previous calibration in each case Deviation of concentration Conc Dev This is the deviation of the concentrations of the respective calibration referred to the concentrations entered in the window Device Setup gt Calibration gt Calibration Gas and Calculated Values Average calibration factor CF Average Average calibration factor of the measured component during the calibration cycles See also formula 5 of the GOST standard 31371 7 2008 Deviation of calibration factor CF Dev This is the relative deviation of the calibration factors of the individual analyses of a calibration referred to the mean calibration factor See also formula 4 of the GOST standard 31371 7 2008 Calculated values This box displays the current calculated values and their deviation from the values displayed in the window Device Setup Calibration gt Calibration Gas and Calculated Values Calculation formulae Page 102 CVControl operating software Operating Manual 11 2012 A5E01428676 03 Optimization of method Optimization of method 5 The automatic optimization of method increases the ava
34. the tag Device Setup and the navigation area Modbus There are three setting options available here Device Settings Capabilities M ap WA cY Control Transmitter User Interface NOT SEALED CONFIGURE 15 xf File Tools Help Device Status Report Mean Values Results Trend Calibration Result Chromatograms Logbook Device Setup M Modbus Device Settings E Device Id SICVEF7BD4 General Method Calibration Hardware E Modbus Capabilities Map Byte Formats Constant Values Map Entries MOD Driver File Name s is the default setting RTU Frame End Timeout ms his fault setting ASCII No Data Timeout ms his e default setting is is the default setting s is the default setting s is the default setting his is the default setting Device SICV6F7BD4 10 116 38 92 connected Ready CyclicRun 89sec 110 sec CVControl operating software Operating Manual 11 2012 A5E01428676 03 107 Transmission of results over Modbus 10 2 Changing MODBUS parameters 10 2 1 10 2 1 1 Procedure 108 Interface specification with Modbus Configuration Parameterizing interfaces with Device Settings The procedure is described using an example with a transmission rate of 19200 bps 1 Select the desired Baud rate in the drop down list in the dialog box Modus Configuration Device Settings 2 Confirm your entries by clicking on App
35. usually nitrogen or helium The carrier gas is passed through a tube or capillary with a defined internal diameter the so called column Older columns are made of metal newer columns of quartz glass which are coated to increase the resistance to breakage The column is internally lined with a defined stationary phase frequently with viscous polysiloxanes Russian Gosudarstvennyy Standart GOST in original TocyfapcTBeHHbIN CTaHAapr translated Government standard is the soviet at time of former USSR or Russian standard CVControl operating software Operating Manual 11 2012 A5E01428676 03 Glossary ISO Abbreviation for International Organization for Standardization This is the international association of standards organizations and processes international standards in all sectors with the exception of the electrical and electronics industries for which the International Electrotechnical Commission IEC is responsible and the telecommunications industry for which the International Telecommunications Union ITU is responsible Together these three organizations comprise the WSC World Standards Cooperation The ISO headquarters is in Geneva Switzerland Modbus The Modbus protocol is a communications protocol based on a master slave or client server architecture The Modbus protocol was defined by Modicon in 1979 for communication with its programmable controllers Modbus is a de facto standard in industry since it
36. work can then also be determined by multiplying with the specific calorific value The Wobbe index also known as the Wobbe value or Wobbe number provides information about the quality of combustion gases with different compositions such as natural gas and town gas The Wobbe index is a corrected heating value calorific value and is calculated from the quotient of the heating calorific value and the root of the fuel air density ratio CVControl operating software Operating Manual 11 2012 A5E01428676 03 Index A Access mode 83 Address area Modbus 113 Administrator privileges 12 14 Alarm 59 Alarms Calibration 127 Detector 125 General 125 Hardware 125 Pressure 126 Temperature 126 Valve 126 Analysis Chromatogram 89 Analysis duration 78 Analysis time 78 Application data Restore 20 B Baud rate 109 Biogas 10 C CAC 10 Calibrated mode 83 Calibrating 33 Calibration 45 Calibration sample 34 Calorimetric value 36 Detail alarm 40 Deviations 47 Digital output 46 Expectation range 42 Limits 40 Peaks 34 Response factor 34 47 With digital input 46 With Modbus 46 CVControl operating software Operating Manual 11 2012 A5E01428676 03 Calibration concentration 104 105 Calibration cycle 37 Parameters 37 Calibration deputy 8 26 Calibration gas 23 Calibration official 8 26 Calorific value measuring instrument 10 Carrier gas Helium 81 Carrier gas pressure 63 Cer
37. 0 00 9050 00 pTS0 00 825000 EZS0 OO 2050 00 ZT50 00 z S0 00 ETS0 00 505000 805000 925000 TS0 0O 6050 00 OTSO 00 8250 00 T6000 9050 00 TTSO0 00 225000 0Z 00 TB0Z 00 8900 TO TOZO tO fEEOZ OO 2202 00 8900 TO 2590 p0 fZEOZ O0 8802 00 90TO TO ZZ6O0 tO 0 02 00 T80Z 00 8800 TO 8990 p0 H02 09 ie802 00 ETe00 T0 E580 0 S 6 7 TPOZ 00 S80Z 00 f9TTO TO 9560 FO 4 02 00 pZ02 00 2900 TO 8690 FO 02 00 0202 00 Z800 TO sp20 FO 0 02 00 0802 00 9800 TO 680 FO 9202 00 8 02 00 TS00 TO 4260 PO Tooo jE80 00 zeon To iodo ro fprOZ OO 2802 00 0600 TO S060 p0 TE0Z 00 620Z 00 T800 TO 0620 t0 fTEOZ 00 Z80Z 00 EOTO TO 8820 PO 020200 TZ0Z2 00 f 00 TO 6EGO tO 8202 00 202 00 SpOO TO 8650 r0 6202 00 0802 00 9900 TO ST60 FO 0090 ieeog oo TITO 72 ieseo mo 6Z0Z 00 2802 00 pZ00 TO 6TZO tO 7 20Z 00 620Z 00 0800 TO 2920 FO 8Z0Z 00 2802 00 6200 TO 9820 t0 2 0Z 00 EBOZ O0 8600 TO TP80 FO 0 0Z 00 8202 00 2600 TO 0690 F0 202 00 0802 00 EZ00 TO f 850 FO i502 00 TB02 00 12200 T0 TEZ0 yO 0 02 00 8802 00 OOTO TO 6S20 t0 7 7 8202 00 0802 00 S200 TO 8020 PO 20Z 00 6902 00 f 900 TO 8TZ0 PO 8202 00 pZ02 00 0200 TO s220 tO 20Z 00 2802 00 T800
38. 000 pTS0 00 O S0 00 T5000 205000 OTS0O 00 2z50 00 OZSO O0 2S050 00 TTSO 00 0ES0 00 ZTS0 00 9050 00 ETSO 00 925000 9T50 00 FS0S0 00 FETSO OO 6z250 00 T50 00 9050 00 OTSO O0 8z250 00 8TS0 00 9050 00 6050 00 9250 00 T50 00 2050 00 pTS0 00 4750 00 TZ50 00 TTS0 00 9T50 00 6z50 00 T50 00 6050 00 OTSO 00 8Z50 00 8TS0 00 9050 00 TTSO 00 825000 PTSO 00 4050700 ETSO 00 0ES0 00 T5000 2S 050 00 TTSO 00 9250 00 6T50 00 Z050 00 Z05000 Szs0 00 0Z50 00 Z0S0 00 ETSO0 00 6z50 00 8T50 00 2050 00 9T50 00 8Z60 00 TS0 00 9050 00 605000 925000 TS0 00 0S0 00 ZTS0 00 TESO 0O0O OZSO O0 S050 00 ETSO 00 6260 00 6TS0 00 24050 00 ZTS0 00 9250 00 T50 00 6050 00 6T60 00 0E50 00 T50 00 9050 00 ZTS0 00 05000 TS0 00 p0S0 00 805000 825000 8T50 00 2050 00 STS0 00 8Z50 00 STS0 00 2050 00 605000 825000 TZS0 00 OTSO 00 OTS0 00 FTESO OO ZTS0 00 0S0 00 OTSO 00 0ES0 00 T5000 8050 00 805000 8250 00 T50 00 0S0 00 TTSO 00 6z50 00 STS0 00 pOSO 00 pTS0 00 925000 OZS0 00 805000 6TS0 00 2zS0 00 ZZ50 00 ETS0 00 ETS0 00 05000 ZTS0 00 9050 00 ST50 00 925000 OZSO O0 9050 00 OTSO O0 SZ50 00 9TS0 00 8050 00 Z0S0 00 9250 00 6TS0 00 OTSO 00 FZ2TS0 00 6250 00 T50 00 505000 OTSO OO TESO O0O0 8T50 00 ZTS0 00 pTS0 00 zES0 00 T5
39. 03 41 Calibrating 4 2 Requirements for calibrating Description of parameters 42 Conc in cycle RT in cycle These are the limits for the concentration and retention time relative to the setpoint CF in cycle deviation of calibration factor in the cycle Maximum permissible relative deviation of the calibration factors Also refer to the significance of the parameters in the Calibration Details window in Section Results of the calibration Page 48 and formula 6 of the GOST standard 31371 7 2008 Conc to prev RT to prev These are the limits for the concentration and retention time relative to the last calibration cycle Conc to sealed RT to sealed These are the limits for the concentration and retention time relative to the first calibration cycle The first calibration cycle is the last calibration prior to the change to calibrated mode This monitoring is only effective in calibrated mode during software locking Max Deviation This is the total permissible deviation of the calorimetric values Superior Calorific Value Inferior Calorific Value Density Relative Density Wobbe index Compression Factor 100 standard Note Limits for alarm triggering e The value 0 is unsuitable as a limit An alarm is always triggered by this value e Enter the value 100 for the parameters for which no alarm is to be triggered CVControl op
40. 03 83 Analysis control and operating modes 8 7 Possible operations Note e The calibration deputy records the checksums and the password e The checksums are saved in the device and are monitored 1 Change the access mode to MONITOR 2 Select the function Set new password in the Tools menu Each password can only be used once When locking is repeated you must assign a new password For more information refer to Section Locking of operation for calibrated mode Page 29 SEALED MONITOR is displayed in the title line Checksums e The checksum for the complete programming of the factory setting is generated by the CVControl operating software The checksum is monitored in SEALED mode e The checksum is visible in tab Device Setup in the line GC Setup Signature in the group General property object Version WA cYControl Transmitter User Interface SEALED MONITOR ioj xi File Tools Help Device Status Repot Mean Values Results Trend Calibration Result Chromatograms Logbook Device Setup E Device Id SICV6F7BE6 p General Version E General Clock SICVEF7BEB Version CAC 1 1 RSP Hardware 1 4 RSP Firmware 00014024 SICV 1 05 00 Units GC Software Signature 9780 Streams Data Storage Approved Values Display Alarm Settings Expectation Ranges Setup Integrity Standby Settings Method Calibration Hardware Modbus Configuration A
41. 12 A5E01428676 03 Status 6 2 Assignment of status signals 6 2 Assignment of status signals Procedure explained using an example 1 In the window CVControl of the tab Device Setup first click on the left in the navigation area on Hardware and then e g on Temperature Controller and Alarm Settings Micy Control Transmitter User Interface NOT SEALED CONFIGURE zloj xi Fie Tools Help Device Status Report MeanValues Results Trend Calibration Result Chromatograms Logbook Device Setup E Device ld SICVEFTBES Pee E AE E E NE E General Clock Version ETC2 ETC3 Warning Warning Waring Alarm Alarm Alarm Units Alarm Alarm Alarm Streams Ignore Ignore Data Storage ir Warming Warming Approved Values Display Alarm Settings Expectation Ranges Setup Integrity Method E Calibration Calibration Settings Calibration Gas Alarm Limits Alarm Settings B Hardware E Temperature Controller Controller Parameters Absolute Limits Alarm Limits Alarm Setting E Pressure Controller Absolute Limits Alarm Limits Alarm Settings Detectors Valves Electronics Modbus Configuration Chromatograph SICV6F7BE8 Connected Alarm Hold Osec 210 sec Click in the box you wish to change and select Alarm Warning or Ignore 3 Click Apply to confirm A fault in the associated parameter then either triggers an alarm a warning or nothing a
42. 2 for the Compression Factor The supplied product is set to SO 6976 Conversion to other standards is carried out using country specific setups Further information on the loading of country specific setups can be found in Section Installing the country specific settings Page 22 WA cY Control Transmitter User Interface NOT SEALED MONITOR 15 xf File Tools Help Device Status Repot MeanValues Results Trend Calibration Result Chromatograms Logbook Device Setup E Device Id SICVEFTB4C pp aaner Cae danon petra B General Clock Version Units Streams Data Storage Approved Values Display Alarm Settings Calculation Settings Expectation Ranges 101 325 Setup Integrity Standby Settings Method Calibration Hardware Modbus Device SICV6F7B4C 10 116 38 104 connected Waming Hold Osec 100 sec CVControl operating software Operating Manual 11 2012 A5E01428676 03 45 Calibrating 4 3 Start calibration cycle Description of parameters e Gas Metering Temperature Is a reference variable for calculating the calorimetric values and is described in the standard The range can be selected as 0 15 or 20 C e Gas Combustion Temperature Is a reference variable for calculating the calorimetric values and is described in the standard The range can be selected as 0 15 20 or 25 C e Calculation Method Is set to the international standard ISO 6976 1995 E
43. 3 4 1 OVGIVIOW T olde rice dete eneheul A T E T 33 4 2 Requirements for Calibrating ceeceeeteeeeeeene cece tenn ee ee eases ee taeee ee eaeeeeetaeeeeesieeeeetiaeeeestnaeeeeee 34 4 3 Start Calibration CYCIG aaa i aT a ead haste staat ee eet eel eee ETAT 46 4 3 1 Start calibration cycle manually 0 0 eee eee eeeeeeee ee eeee eter eeeeeeeeeeeeeeeesaeeeeeseeeeeeeseeeaeeeseeaeeeseeaees 46 4 3 2 Starting the calibration cycle with digital input ee cece ee estes ee eeeeeeeeeeeeeeeeseeeeeeseneaeeeseeeaees 47 4 3 3 Starting the calibration cycle With MOCDUS 0 cccceeeeceeeeeeeeeeeeeeeeeeeseeeeeeseneeeeeseeeaeeeseneaeeeseenaees 47 4 3 4 Automatic tracking of calibration factors 0 c cc ceeeeceeeeeeeeneeeeeeeeeeeeeeaeeeeeeaeeeeeeaeeeeeeaeeeetenaeeeeneaas 47 4 4 Results of the Calibrations onset r ole ae ainda leet 48 CVControl operating software Operating Manual 11 2012 A5E01428676 03 Table of contents Optimization of method se ci0s cess shen seeks aea y ces elewesdadeastusceuaecdsadacsaieace AEA EEAS AA PKO E ATOLA ARRS 51 5 1 Switching the automatic optimization of method on and Off eee eee eeeeeeeeeeeeeeeeeeaeeeeeetaeeeeeeaes 52 5 2 Paramelenzation 0f evemMS sen i EE E AERE EEE 53 5 3 Peaks and peak listist gesaai nuena eee act tas ees ccc eee E a aaa ee ae ete 55 6 Stat Siei eaid a ea e ee aa e nesteadac tise aii dee iat Gemeente 59 6 1 Status messages and lOQDOOK ceeeeeceeeeeeneeeeeeen
44. 53 3333 0 0500 0 0498 0 0002 10 Isopentane 25220 0000 25173 3333 0 0500 0 0498 0 0002 11 Hexane 32926 6667 32753 3333 0 0500 0 0496 0 0004 Device SICV6F7B48 10 116 38 109 connected Ready CycicRun fi37sec 150sec e Ifthe chromatograph is in calibrated mode the deviations are shown as follows Green if the deviations are within the defined limits Red if the deviations exceed the limits e If limits have been exceeded you can click the Details button to change to the window Calibration Details in order to obtain more detailed information Note The Details list is deleted as soon as you change from Configure mode to calibrated mode 48 CVControl operating software Operating Manual 11 2012 A5E01428676 03 Calibrating 4 4 Results of the calibration Meaning of parameters in the window Calibration Result Computed RF These are the calculated response factors of the current calibration Previous RF These are the calculated response factors of the previous calibration Sealed RF These are the response factors of the calibration following which a change was made to calibrated mode Nominal Concentration These are the concentrations of the calibration sample entered in the window Device Setup Calibration gt Calibration Gas and Calculated Values Actual Concentration These are the concentrations resulting with the response factors of the previous calibration Deviation T
45. 6F7B48 peee E General Component Value Unit Method Oxygen 0 0493 x i Name Value Unit Superior Calorific Value 39 9754 MJim3 Inferior Calorific Value 36 1007 MJim3 Density 0 80709 kgim3 Relative Density 0 6242 unitless Webbe Index 50 5961 Miim3 Compression Factor 0 3973 unitless 100 Norm 1 0010 unitless Device SICV6F7B48 10 116 38 109 connected Ready CyeticRun 54sec 150sec 2 Enter the corresponding concentration value in percent for the associated components in the Value column Confirm the input using the Enter key on the PC keyboard Note The total of the concentrations is displayed in the last line of the component table The total is usually 100 3 Click the Apply button when you have entered all values The chromatograph then automatically updates the bottom table in the window with the calorimetric values of the calibration gas The unit for the component concentrations is fixed as percent for the calculation method in accordance with ISO 6976 The units of the calorimetric values in the bottom table can be selected in the tab Device Setup in the navigation area under General and Units CVControl operating software Operating Manual 11 2012 A5E01428676 03 Calibrating 4 2 Requirements for calibrating Parameterization of calibration cycle 1 2 In the window CVCon
46. Continuation of measurement and display of the name and retention time of the peak s IM SICV6F7BE6 TCD4 Calibration 28 09 2007 15 48 24 CB CB CB 0 023 0 022 0 021 0 020 0 019 0 018 0 017 0 016 0 015 0 014 0 013 0 012 0 011 0 010 0 009 0 008 0 007 0 006 0 005 0 004 0 003 0 002 0 001 0 000 yia HelpStart_C6 7977 8 373 12 789 16 643 18 601 7 8 9 10 11 12 13 14 15 16 17 18 19 20 CVControl operating software Operating Manual 11 2012 A5E01428676 03 57 Optimization of method 5 3 Peaks and peak list Detector 4 Continuation of measurement and display of the name and retention time of the peak s IM SICY6F7BE6 TCD4 Calibration 28 09 2007 15 48 24 cut_ON _Cut_OFF C34 i C4_4 n C4_4 neo C5_4 i C5_4 n C5_4 0 11 HelpP HelpP 0 10 CVControl operating software 58 Operating Manual 11 2012 A5E01428676 03 Status Ready Alarm The chromatograph monitors all actions which can cause faults and displays the current state in the tab Device Status The device generates a group message from all signals and displays this in the tab Device Status under Current State You can define in the tab Device Setup whether a fault will trigger an alarm a warning or nothing If the device status is OK the chromatograph displays the message STATE OK on a green background in the tab Device Status under Current State At the same
47. Operating Manual 11 2012 A5E01428676 03 29 Operation 3 4 Entering the parameters 3 4 30 e Numerical values e Commands Entering the parameters Parameters can be e Logical values yes no positive negative Note Changing of parameters e Certified mode Make sure when changing parameters that the certificate remains valid despite the change The parameters are described in the certificate e You must click the APPLY button following each change If you change several parameters on a tab you must click APPLY and OK at the latest before leaving the tab Wacvcontrol Transmitter User Interface NOT SEALED CONFIGURE File Tools Help Device Status Report Mean Values E Device Id SICV6F7BBE General E Method B Cycle Events Detectors Pressures Valves Integration Events Peaks Groups Measured Components Auxiliary Components Calibration Hardware Modbus Configuration Results Trend Calibration Result Chromatograms Logbook Device Setup f Method Cycle Events Events Name Event Use Det Mode Time Cur Rule Shift Relative Weight Peak1 Peak 2 _Stream Step_01 Stream Step M Al AllModes At gt 9 00 Fixed 0 00 0500 1 000 _Balance Detector Balance Detector V All AllModes At gt 20 00 Fixed 0 00 0500 1 000 Flow Slam OFF M All AllModes At gt 30 00 Fixed 0 00 0 500 1 000 All AllMode Upload Setup xj i Successfully u
48. SITRANS CV CVControl operating software Operating Manual 11 2012 Process gas chromatography SIEMENS SIEMENS Process Analytics Process gas chromatograph CVControl operating software Operating Manual 7KQ3105 11 2012 A5E01428676 03 Introduction Installing the software Operation Calibrating Optimization of method Status Logbook Analysis control and operating modes Viewing and analysis of measured values O O N O 0O IA W IN Transmission of results over Modbus ER O Alarm fault and system messages Service and support 12 List of abbreviations 13 Legal information Warning notice system This manual contains notices you have to observe in order to ensure your personal safety as well as to prevent damage to property The notices referring to your personal safety are highlighted in the manual by a safety alert symbol notices referring only to property damage have no safety alert symbol These notices shown below are graded according to the degree of danger PAO indicates that death or severe personal injury will result if proper precautions are not taken WARNING indicates that death or severe personal injury may result if proper precautions are not taken CAUTION indicates that minor personal injury can result if proper precautions are not taken NOTICE indicates that proper
49. Sample Steam E Injection Time 28 09 2007 15 48 24 TeD1 MTD 2 0 55 T 0 50 8 0 45 30 0 40 4 aes 25 0 30 5 20 0 25 an 0 20 015 10 010 05 0 05 i c lt lt ___ ay unn a0 a_a 30 20 10 0 10 20 30 40 50 60 70 80 90 100 110 30 20 10 0 10 20 30 40 50 60 70 80 90 100 110 mTcD3 TCD 4 3 wi E x ee 2 oY 20 mc 3 15 7 10 A 2 05 ae 3 Br ane or 4 0 0 i Ko mra 30 20 10 0 10 20 30 40 50 60 70 80 90 100 110 120 30 20 10 0 10 20 30 40 50 60 70 80 90 100 110 Chromatograph SICVEF7BE6 Connected Ready CyclicRun 120 sec 150se 2 Select the desired sample in Sample Stream Increasing the chromatogram window Click in one of the four small chromatogram symbols The associated chromatogram is displayed in a separate scalable window CVControl operating software Operating Manual 11 2012 A5E01428676 03 89 Viewing and analysis of measured values 9 2 Displaying chromatograms Parameterizing the representation 90 1 Click the Color Properties button 2 Here you can select which information is to be displayed Retention time Component peak name Peak markers WA chromPropertiesForm x M Chromatogram Display M Retention Time v Peak Name M Peak Marker M Color Settings E Retention Time i Peak Start Marker ee Peak End Marker mi Retention Time Marker Cancel 3 You can select the colors for
50. TO PEZO tO 4 02 00 2802 00 8600 TO 6640 FO 3202 00 2802 00 800 T0 982070 820Z 00 T80Z 00 p800 TO E620 PO 7 0 02 00 6202 00 TS00 TO 8 90 FO 6 02 00 T60Z2 00 P600 TO OE8O tO T20Z 00 6202 00 ZS00 TO 8s20 FO 2 0Z 00 P60Z 00 80TO TO 9760 ro 8202 00 p802 00 0800 TO p980 PO ZE07 00 640600 ESTIO TO 948040 TE0Z 00 G80Z 00 8900 TO TGO0 tO AAE AA EE EE 0 02 00 GBOZ 00 s600 TO 6580 t0 0229 88 G 6P TO 29740 PO OSTT8 O erst Or Op89 88 O8GP TO OEZO PO FZ2PTTS O fa PT Or P6Z9 BSB FESOS TO 9980 FO FO6TTS O frrST OF 09 988 466h TO 8r40 PO FPSTT8 O fSOST OF 2 Z7P9 B8 I TTOS TO Ep8O pO FORTTS O FESST OF p99 88 ipOOS TO T440 PO S6STTS O f80ST OF T Z79 88 EEOS TO ESR0 FO pGTT8 O TaST Or t229 88 886p TO fO4Z0 PO ZSTT8 0 SOTST OF SE99 88 OTOS TO 7440 PO O9TT8 0 f4ZST Or 6PP9 S8 O8GP TO OZ80 FO FORTTS O f86ST Or 809988 S 96h TO 0990 p0 TOTT8 O FZE9T OF 865988 8 6h TO 2640 PO EOTT8 O FGEST OF TOPS 88 S9POS TO POBO PO FEBTTS O F2ZST OF 0P9 88 205 TO T80 p0 T8TT8 0 EST OP 099 88 G66Pr TO 8440 PO SOTT8 O TRST OF TEPPO SB ZGOS TO SPSB0 PO OSTT8 O SEOST OF ZSTZ 88 O 6P TO 9090 FO pZTT8 0 fPZST Or 900288 ESGP TO 4990 PO OETT8 O F22ST OF 8059 88 S 86h TO 2540 PO FO4TTS O fPz9T OF
51. Value Interior Calorific Value Density Relative Density Wobbe Index Expand display e Enter the desired lower limit for Min Value and the upper limit for Max Value e Alternatively you can click on the Auto Min Max button to allow automatic selection of the smallest and largest values from the history for Min Value and Max Value Enter scale Enter the vertical range in the window for Min Scale and Max Scale 0 right at bottom 100 right at top such that the lines do not overlap Set line color e Click the Set Color button and select the color e Confirm with OK CVControl operating software 96 Operating Manual 11 2012 A5E01428676 03 Viewing and analysis of measured values 9 5 Collecting and exporting results 9 5 Collecting and exporting results Continuous saving of chromatograms as mbd file on the hard disk 1 Mark the parameter Chromatograms as Measured Binary Data mbd with a tick in the menu Tools gt Log Settings x Logging IV Chromatograms as Measured Binary Data mbd J Continuous Print Log of Results 2 Enter the directory with drive in which the results are to be saved A file is produced in this directory for each analysis The file name is generated according to the pattern Date_Time_Sample_Consecutive number e g 20070928_121605_Stream1_000017 mbd The consecutive number is rese
52. alibrations Maximum number of faulty calibrations permissible in succession CVControl operating software 38 Operating Manual 11 2012 A5E01428676 03 Calibrating Calibration sequence 4 2 Requirements for calibrating The figure below illustrates the calibration sequence Cycles to skip Cycles for optimizing cycle events E p amp pn N oO N KS S gt 8 T 2 ke je lt x CVControl operating software Operating Manual 11 2012 A5E01428676 03 max number of cycles with alarm 0 Cycles for optimizing integration events peaks and groups n cycles to average Cere n Additional cycles for averaging Limit check Deviation checking mode Limit exceeded Limit check Deviation checking mode Limit exceeded Calculation of response factor Average based on last n cycles Limit check Deviation to previous calibration Deviation to sealed calibration Limit exceeded STOP y n Calibration successfully finished 39 Calibrating 4 2 Requirements for calibrating Setting the detail alarm of the calibration 40 You can individually assign the significance of the alarm to each function e Ignore e Warning e Alarm A cvcontrol User Interface NOT SEALED CONFIGURE lolx File Tools Help Device Status Report Mean Values E Device Id SICV6F7BDF General E Method E Cycle Ev
53. ane 0 0505 0 0503 0 0504 0 0505 0 0505 0 0000 0 0000 0 0000 lsopentane 0 0500 0 0502 0 0503 0 0504 0 0504 0 0000 0 0000 0 0000 Neopentane 0 0000 0 0000 0 0000 0 0000 0 0000 0 0000 0 0000 0 0000 Hexane 0 0501 0 0500 0 0501 0 0506 0 0505 0 0000 0 0000 0 0000 Hexane And Higher 0 0506 0 0506 0 0502 0 0506 0 0506 0 0000 0 0000 0 0000 Device SICV6F7B48 10 116 38 109 connected Ready CycicRun 145sec 150sec The chromatograph displays the components and the calorimetric values for all sample streams The mean values of the current hour the current day the current month and the configured time period The mean values of the last hour the last day the last month and the configured time period Resetting of mean values Note All mean values are reset to zero Click the Clear Mean Values button in the tab Mean Values CVControl operating software 92 Operating Manual 11 2012 A5E01428676 03 Viewing and analysis of measured values 9 3 Mean values Configurable mean value e Inthe tab Device Setup open the property object Data Handling in the group General e Here you can define your desired mean value Time offset Interval Start date Start time MA cvcontrol User Interface NOT SEALED CONFIGURE o x File Tools Help E Device Id SICV6F7B48 B General Data Handling O Approved Values Configured Mean Interval 0 744 hours Transmit Zero instead Stand
54. anguage Rules of courtesy and language are covered by the term Modbus e Understand what the partner says Common memory area in the process control system flow computer The process control system flow computer contains a memory area which the chromatograph can write via the Modbus interface The software of the process control system flow computer can read this information The chromatograph and process control system flow computer therefore communicate through this memory area This memory is structured in 16 bit registers which are accessed using addresses The maximum address range is 0 to 65535 Agreement on memory division During programming of the devices the meaning of each register must be defined The results of each component in each sample must be written by the chromatograph into a specific position of the process control system flow computer memory The process control system flow computer can find the results there These address declarations depend on the number of chromatographs samples and components connected to the process control system flow computer These are therefore defined separately for each plant CVControl operating software Operating Manual 11 2012 A5E01428676 03 Transmission of results over Modbus 10 2 Changing MODBUS parameters 10 2 Changing MODBUS parameters Procedure 1 Start the program CVControl start bar Start Programs gt Siemens AG gt CVControl gt CVControl 2 Open
55. ard for linking measuring and control instruments to process control systems and volume conversion devices flow computers People use the telephone This only functions if certain prerequisites are fulfilled e Electrical connection An electrical connection must be present between the two telephones The electrical characteristics of the telephones must correspond e Control of conversation Rules of courtesy must be observed to control the conversation and both partners must agree on the rules e Language and understanding of what the partner says The two partners must speak the same language or at least understand the other partner s language The partners must understand the context And they must be aware of what they should do with the information CVControl operating software Operating Manual 11 2012 A5E01428676 03 105 Transmission of results over Modbus 10 1 The Modbus interface chromatographs use interfaces 106 Chromatographs and process control systems flow computers use special electronic circuits which we call interfaces Certain prerequisites must also be fulfilled here e Electrical connection The interfaces of the devices are connected by electric cables The electrical properties of the interfaces are standardized but there are different types of interface Only interfaces of the same type may be connected together We use RS 232 RS 485 e Control of conversation and l
56. ase that a commenced input cannot be exited You must then continue to the end of the input cycle and subsequently click the UNDO button The previous value is then displayed again Input during ongoing analysis The terms Setpoint and Setpoint Initial are present in many windows Inputs are only possible in the Setpoint Initial box As soon as the ongoing analysis has been completed the gas chromatograph first copies this value to Setpoint The modification is therefore always only active in the next analysis CVControl operating software Operating Manual 11 2012 A5E01428676 03 31 Operation 3 4 Entering the parameters 32 CVControl operating software Operating Manual 11 2012 A5E01428676 03 Calibrating 4 4 1 Overview Note The calibration sample should correspond to the gas used unless your certificate specifies something else This procedure results in the best performance for your device Procedure 1 To carry out a calibration you analyze a calibration sample of known composition Make sure that the composition of the calibration sample corresponds to the requirements of your local approval and the data in the Readme pdf file on the CD Country Specific Setup 2 Enter the concentrations of the components The chromatograph then calculates the calibrated response factor for each component from the ratio between concentration and peak area For details refer to Section Calculati
57. ation may be trademarks whose use by third parties for their own purposes could violate the rights of the owner Disclaimer of Liability We have reviewed the contents of this publication to ensure consistency with the hardware and software described Since variance cannot be precluded entirely we cannot guarantee full consistency However the information in this publication is reviewed regularly and any necessary corrections are included in subsequent editions Siemens AG Order number A5E01428676 Copyright Siemens AG 2010 2011 Industry Sector 11 2012 Technical data subject to change All rights reserved Postfach 48 48 90026 NURNBERG GERMANY Table of contents 1 IntrOGUiCtiOni a E E ETEO oite e RA Hae A ds hea Nag ieee A cides Saar 7 2 Installing the software fei s h csscee eet Sec ee REELS y chet Ee dc ee eee 9 2 1 Operating software and requirements placed on the chromatograph ccceeeestesteeeeeees 10 2 2 Minimum PC requirement sssrin maea aeea ap taana daaa aaa e aaa aaaea y 11 2 3 Installing the operating software eee eee eeeteeeeeeteeeeeeaeeeeetaaeeeeeeaaeeeeeeaaeeeeeeaaeeeesenaeeeeeenaeeeeeaaas 12 2 4 Setting the IP addresSes csssc cieseseeedietet eiia n ibani iata a o ng aaa ia iaaea aaa 14 2 4 1 Changing the IP address of the chromatograph ssssssssssssssssrrrsserrssrirrssttrrssttnrssttnnssternssennnnenn 15 2 4 2 Setting the IP address of the PC assesssnsciisesrrriieerriersnsn
58. ation on whom to contact at this Internet address www siemens com automation partner www siemens com automation partner Product information on the Internet Training center The instructions are included on the CDs which are already supplied or may be ordered In addition the instructions are available on the Internet on the Siemens homepage A signpost to the range of technical documentation the online catalog and the online ordering system for individual products and systems is available at www siemens com processanalytics www siemens com processanalytics Here you will find e Products amp solutions including our newsletter containing up to date information on your products e Electronic trading over the Internet e Support with e g instructions and manuals certificates brochures and catalogs Siemens offers corresponding courses for newcomers to process gas chromatography Please contact the central Training Center in Karlsruhe Training Center Europe Process Instrumentation and Analytics Siemensallee 84 D 76181 Karlsruhe Germany Internet www sitrain siemens com www sitrain siemens com CVControl operating software Operating Manual 11 2012 A5E01428676 03 127 Service and support Technical support e You can access technical support for all IA amp DT products using The Web form for Support Request at www siemens com automation support request www siemens com automation suppor
59. below which the gas chromatograph displays in the tab Device Status in the box Active Alarms and Warnings and which are recorded in the logbook General alarms e CRC error Only occurs in Sealed Mode Occurs if the current method does not provide the expected checksum Indicates a change in the method due to hardware faults Flash memory or manipulation e Method error Occurs if parts of the current method cannot be interpreted e SampleStream Alarm The DI for the sample stream test has not been set typically D11 e Modbus Alarm Occurs if the current Modbus configuration cannot be interpreted Occurs if the serial interface is not used by Modbus Hardware alarms e Heartbeat lost Internal communication interrupted e Heartbeat dead Internal communication aborted e Communication error Communication error due to wiring or software fault CVControl operating software Operating Manual 11 2012 A5E01428676 03 123 Alarm fault and system messages Detector alarms Pressure alarms 124 Internal deactivated Gas chromatograph deactivated Sensor shortcut Short circuit in sensor Sensor interrupted Interruption in sensor No gas supply Gas supply interrupted Data Cycle lost Occurs if the data transmission from the RSP trace data from a detector is intermittent Trace data are replaced by baseline data in the corresponding period Data Phase lost Occurs if the synchronization of data trans
60. by Sellin jii Generate alarm log entry Method Calibration Hardware Modbus Device SICV6F7B48 10 116 38 109 connected Ready FashPending Influence of results exceeding the measuring range on calculation of the mean value Forwarding of results exceeding the measuring range Printing of mean values 1 Click in the dialog box Mean Values and select the sample stream 2 Click the Print Mean Values button the Windows print dialog is shown CVControl operating software Operating Manual 11 2012 A5E01428676 03 93 Viewing and analysis of measured values 9 4 Trends 9 4 Trends Displaying a trend view A trend display is possible over a maximum period of two weeks e Select the tab Results Trend Eix File Tools Help Device Status Report Mean Values Results Trend Calibration Result Chromatograms Logbook Device Setup m Legend bas Sid Component __ 1 Nitrogen 1 CarbonDioxide Ea 1900 1 Butane 1850 1800 Properties SS a EEE AE GE GEIE aI AOT E ERA ERE KORRA FQ a N aE OE a SES E E E 15 36 00 15 40 00 15 44 00 15 48 00 15 52 00 15 56 00 16 00 00 16 04 00 16 08 00 Refresh Trends Chromatograph SICVEF7BE8 Connected 0 sec 210 sec The legend on the right in the window shows the line colors for the components Scaling a trend vie
61. ction C_CH4 Description Name Status MMI1 Ready Chromatograph SICV6F7B48 Connected CVControl operating software Operating Manual 11 2012 A5E01428676 03 7 Introduction NOTICE Leave factory settings unchanged e Never change the factory settings of the functions e lf you nevertheless change the factory settings This corresponds to intentional manipulation and therefore a non approved application of the device The accuracy of the measurements will become less exact The device may no longer match the certification e The device is delivered non calibrated The calibration must be carried out by a calibration official or deputy at the location of use in the owner s country History This history establishes the correlation between the current documentation and the valid firmware of the device Release Remarks Firmware ID 03 Description of new functions FW 02 01 00 11 2012 02 Description of new functions FW 01 60 01 02 2010 01 First release FW 01 40 00 10 2007 CVControl operating software 8 Operating Manual 11 2012 A5E01428676 03 Installing the software 2 Note Secure operation of the device For its automation and drives product portfolio Siemens provides IT security mechanisms to support secure operation of the plant machine However for secure operation of a plant machine it is necessary to i
62. d see Section Optimization of method Page 51 Cycles for Averaging Specifies how many analyses are to be used to determine the average value Max additional cycles for averaging if limits exceeded Specifies how many additional cycles are executed if the limit monitoring function has been triggered CVControl operating software Operating Manual 11 2012 A5E01428676 03 37 Calibrating 4 2 Requirements for calibrating e Max number of cycles with alarm Specifies the maximum number of analyses of the calibration mixture which may be repeated following a device alarm e Calibration Timeout minutes Maximum duration of a complete calibration including all applicable repetitions resulting from the above mentioned points e Deviation checking mode Specifies the deviation strategy according to which the result of the calibration is to be evaluated The following are possible Deviation of Min from Max deviations between minimum and maximum are evaluated Deviation of Min and Max from Mean deviations of minimum maximum from mean value are evaluated e Autocalibration Interval days Specifies the interval between two calibration cycles in days e Autocalibration DayOfWeek 7 days Interval only Specifies the day of the week of the calibration if Autocalibration Interval days is 7 e Autocalibration Time Specifies the time at which the calibration cycle is to start e Maximum number of consecutive failed c
63. dardized areas for calibration This factor is calculated in accordance with the GOST standard The calculation is carried out using the following formula CF Ce A Meaning of the various parameters cal k CVControl operating software Component index k Calibration factor of component k Area of component k in the calibration sample recorded during the calibration process This can be a mean area Concentration of component k in the calibration gas certificate Operating Manual 11 2012 A5E01428676 03 103 Viewing and analysis of measured values 9 7 Calculation formulae 9 7 3 Calculation of standardized concentration from the peak area The calculation is carried out using the following formula fa Ae _ 100 n Ce CY n k 100 M k k 100 R EG Meaning of the various parameters k Component index k R Response factor of component k k AM Area of component k in the measured sample recorded during the k measurement M Concentration of component k calculated from the measured area and the k associated response factor 100 standardization factor calculated from the concentrations of all No0 measured components C nor Concentration corrected by standardization factor n100 k CVControl operating software 104 Operating Manual 11 2012 A5E01428676 03 Transmission of results over Modbus Transmission of results over Modbus 1 10 1 The Modbus interface Modbus MODBUS is an industry stand
64. e of the time program Device Setup gt Method gt Events e Injection Lag allows commands to be executed prior to the injection time Current analysis time Elapsed Time The current analysis time Elapsed Time is a relative time which starts with a value of zero at the starting time and ends with the value of the Run Time End of analysis e The analysis stops at the time Run Time and the analysis clock is reset to zero e In Cyclic Run mode the next analysis starts as soon as the chromatograph has reached the Ready state e in Single Run mode the chromatograph switches to the Hold state CVControl operating software 78 Operating Manual 11 2012 A5E01428676 03 Analysis control and operating modes 8 5 Calibrating 8 5 Calibrating Starting the calibration The exact sequence is described in Section Calibrating Page 33 ff Click the option box Calibration in the dialog box Device Status of the option box Mode Select e The chromatograph executes a complete calibration process Stopping the calibration Click the option box Mode Select in the dialog box Device Status and then the option box Cancel Calibration e The chromatograph still continues up to the end of the current analysis e The results of the calibration analyses are subsequently rejected e The chromatograph then returns to the state it was in prior to the calibration Hold or Cyclic Run 8 6 Standby Select
65. e Controller Pressure Controller Detectors Valves Electronics Modbus Configuration Results Trend Calibration Result Chromatograms Logbook Device Setup f Hardware Pressure Controller EPC2 Alarm v Try to restart Controllers in case of internal deactivation due to a no gas supply alarm Chromatograph SICV6F7B48 Connected Alarm Hold Osec 150 sec CVControl operating software Operating Manual 11 2012 A5E01428676 03 Status 6 4 Gas supply e The device is ready for operation again if the value Pressure is equal to the value Setpoint and if Ready is displayed in the Status line WA cvcontrol Transmitter User Interface NOT SEALED CONFIGURE 15 xi File Tools Help Device Status Report Mean Values Results Trend CalbrationResut Chromatograms Logbook Device Setup f Hardware Pressure Controller E Device Id SICVEF7B48 General Method Calibration E Hardware Temperature Controller Pressure Controller Detectors Valves Electronics Modbus Configuration Chromatograph SICVEF7B48 Connected Ready CyclicFlun 23 sec 150 sec CVControl operating software Operating Manual 11 2012 A5E01428676 03 65 Status 6 5 Sample flow monitoring 6 5 Sample flow monitoring Note The following descripti
66. e Select m Streams ee OSES ra E Calibration SP Single Run N 1 Sample1 lt Next stream Elapsed Time a Run Time 150 S Actual stream gt 2 Sample o E tte 0 i Temperatures Status Heater Temperature C Setpoint C Ready 67 0 Ready 67 0 Ready 65 0 1 600 98 671 1 000 62 665 0 600 0 520 1 400 Status Pressure kPa Setpoint kPa Ready 289 3 290 0 Ready 218 6 218 7 Ready 225 5 226 0 FlushLoop C_CH1 Sample C_CH2 Backtlush C_CH3 Injection VC_CH4 Name Status MMIT Ready Chromatograph SICVEF7BE6 Connected CyclicRun 25sec 150se Note e In operating mode Single Run the command Stream Step changing of sample stream is ineffective e You must switch on the desired sample stream manually e In operating mode Single Run you must manually start each analysis individually CVControl operating software 76 Operating Manual 11 2012 A5E01428676 03 Analysis control and operating modes 8 2 Starting an analysis Proceed as follows 1 Check whether the desired sample stream is selected 2 Click the option box Single Run in the dialog box Device Status of the option box Mode Select The chromatograph starts an analysis After the analysis the chromatograph switches to the Hold state Start cyclic analysis Cyclic Run
67. e operations Access mode Which parameters you can change depends on the access mode There are three access modes e MONITOR In MONITOR mode most of the operating functions are disabled to prevent errors in measurement due to unintentional operations You can still change a number of parameters e g the enabling of samples e CONFIGURE You can change all parameters in CONFIGURE mode e Calibrated mode In calibrated mode you can only use MONITOR mode Changeover to CONFIGURE mode is password protected How this functions is described in detail in Section Calibrating Page 33 Changing to MONITOR in access mode 1 Select the Tools menu in the window CVControl and then the function Change Access Mode 2 Select the access mode MONITOR in the box Login Then click OK NOT SEALED MONITOR is displayed in the title line Changing to CONFIGURE in access mode Note If the gas chromatograph is in calibrated mode this mode is terminated when changing to CONFIGURE mode 1 Select the Tools menu in the window CVControl and then the function Change Access Mode 2 Select the access mode CONFIGURE in the box Login 3 Enter the password and then click OK NOT SEALED CONFIGURE is displayed in the title line Calibrated mode Note If you forget the password you cannot leave calibrated mode CVControl operating software Operating Manual 11 2012 A5E01428676
68. e1 CV Wobbelndex Wobbe index Sample1 CV Density Density Sample1 CV RelativeDensity Relative density Sample1 CV CompressionFactor Compressibility factor Sample1 CV UnnormalizedTotal Non standardized total 120 CVControl operating software Operating Manual 11 2012 A5E01428676 03 Transmission of results over Modbus 10 2 Changing MODBUS parameters 10 2 2 4 Mean values The concentrations of all components and the calculated values are combined as mean values and saved by the device Four different types of mean values are available e Hourly mean values MeanHour e Daily mean values MeanDay e Monthly mean values MeanMonth e A variable mean value interval MeanVariable The variable interval can be set such that up to 744 values of MeanHours can be combined The mean values for the last completed interval of each type are made available by the gas chromatograph in the following manner lt Name Product stream gt lt Mean value type gt Concentration lt Component name gt and lt Name Product stream gt lt Mean value type gt CV lt Name of calculated value gt Examples e Sample1 MeanDay Concentration Hexane e Sample1 MeanMonth CV Wobbelndex Furthermore the number of combined analyses for each type of mean value is made available in the following form lt Name Product stream gt lt Mean value type gt Number of analyses Example Sample1 MeanHour A
69. eeeeeeaeeeeeeaaeeeeeeaaeeeeeeaeeeeeenaeeeeeeiaeeeeeenaeeeeeeaas 60 6 2 Assignment of status signals ao gaie ae EE R EAE E A ERE 61 6 3 Monitored parameters is apensas a apana eaaa aaae ata a eaae eke eh in eee ea 62 6 4 Gas S pDly srs eee a aaa a a a aa a a a a aa 63 6 5 Sample flow MOMItOLING asii a eran eean aaan ba daea iaa ari i A 66 Ero o 010 EEEE E E E E AT 73 Analysis control and operating modes cccccccccsccccecceeccececceeccecceeeeceeeseeceeecceeceseeseeeseeceseeseeesaeeeeeseeseess 75 8 1 OVEIVIOW rar A E A pac a A E A N AA 75 8 2 Starting AN ANALYSIS 2 220 seseseeeegeseedeiege cee esued cece esedeeevusdecee septa ceelwaedei epics EAEE ANETE N AEE N 76 8 3 slopping the analysis ora a aa a a e E iia ah aden aides 78 8 4 AnialySis TIOR aa a a a A E N hi eee aR ETEA R TE 78 8 5 walibraingeesn soena a a A Seed east ee ee 79 8 6 Standby oaii aa aiaa a t a ei aaa a a a A a dneeveh adhe 79 8 7 POSS e opera O S ia a a aa a a r Taaa a a ae a a aa aa a aata 83 Viewing and analysis of measured values ccccccssssssssseeceeecesssseseeececeesesseseeseeeeeeseesssseeseeeeeeeeessseneees 87 9 1 Displaying the results list Report ee eee eeeeeeeeeeeeeeeeeeeeeaeeeeeeeaeeeseeaaeeeseeaaeeeeeeaeeeseenaeeeeeeaas 87 9 2 Displaying Chromatograms areetan aiaa aaa aaa aa aiaa 89 9 3 Mean Values sci hcesen ise chert eek hecea dant leads ee he anes tle heats Ae arta ei te 92 9 4 Tend otra arate ee ee Ae neh ae ee a i ee 94 9 5 C
70. ents Integration Events Peaks Groups Measured Components Auxiliary Components E Calibration Calibration Settings Calibration Gas Alarm Limits Alarm Setting Hardware Modbus Results Trend Calibration Result Chromatograms Logbook Device Setup Calibration Alarm Settings Alarm Warming Warning Warming Warning Waming Warming Alarm Alarm Ignore Device SICV6F7BDF 10 116 38 106 connected Ready CyclicRun 116 sec 150 sec CVControl operating software Operating Manual 11 2012 A5E01428676 03 Calibrating 4 2 Requirements for calibrating Parameterization of limits 1 In the window Device Setup first click on the left in the structure on Calibration and then on Alarm Limits MA cvcontrol User Interface NOT SEALED CONFIGURE 151xi File Tools Help Device Status Repot Mean Values Results Trend Calibration Resut Chromatograms Logbook Device Setup Calibration Alarm Limits E Device Id SICV6F7B48 General Method B Calibration Calibration Settings Calibration Gas Alarm Settings Hardware Modbus Device SICVGF7B48 10 116 38 109 connected Ready ycicRun f125sec 150sec 2 Enter the parameters Confirm the input using the Enter key on the PC keyboard Click the Apply button when you have entered all values CVControl operating software Operating Manual 11 2012 A5E01428676
71. ents Trend Calibration Resuk Chromatograms Logbook Device Setup Method Cycle Events Valves Nome Valve Use Duration Switch Mode Tme Cue Shilt Relative Weight Pesk1 Peak 2 1FlushLoop_0t Fazihioop AlModes s 0 00 0 500 I FlushLoop_02 Fhuhloop AlModes FlushLoop03 Flushloop AlModes LTCD_4 Irvvest Si TCD_A4 Irvvenrt AlModes LTCD_4 Irveest Si TCD_4 Irvvert Semple Sangia Sample BackFlush BackFlush Ingection lrgection Irgection BackFlush AlModes AlModes AlModes AlModes SSSR AERO ERAS Sr ReERERERPRRPEREEPE Creomslograph SICVEFTBES Connected Rey Oan Stee 150 CVControl operating software Operating Manual 11 2012 A5E01428676 03 67 Status 6 5 Sample flow monitoring 68 3 Read sample flow interruption Read the value Current time in lines I_Sample_02 and I _Sample_03 Example Switching on Line _Sample_02 4 s Switching off Line _Sample_03 24 s Result The minimum interval absolute value for alarm suppression is 28 seconds This interval of 28 seconds defines the minimum value This value can be increased by the user in Events 4 Define time interval in Events Open the group Method and Cycle Events in the navigation area Click on the property object Events WA cYControl Transmitter User Interface NOT SEALED CONFIGURE ioj xi File Tools Help Device Status Repot MeanValues Results Trend Calibration Result
72. ents for calibrating Page 34 Loading parameters 1 Place the CD Parameter Backup with the parameters for system restoration into the CD drive 2 Select the Load Setup command in the File menu 3 Select the file Setup xx xx yyy mbb XX xx yyy corresponds to the serial number of your chromatograph Note Do not switch off the chromatograph during the saving process The following message is displayed in the status line for about one minute Flash pending The chromatograph then saves the data into the Flash memory The save process takes about 20 seconds and is indicated by the message Flashing If you switch off the device during this phase or if the power supply fails the data in the memory are of no use Saving parameters 1 Select the Save Setup As command in the File menu WA cvcontrol Transmitter User Interface NOT SEALED MONITOR File Tools Help Injection Time 13 09 2007 15 57 38 100 Norm 2 Select a directory and a file name If you have loaded country specific settings these will now be saved together with the basic parameters CVControl operating software Operating Manual 11 2012 A5E01428676 03 13 Installing the software 2 4 Setting the IP addresses 2 4 Setting the IP addresses Note Firewall If a firewall is activated in the network this may possibly block establishment of the connection Therefore match the firewall to your network topology
73. erating software Operating Manual 11 2012 A5E01428676 03 Calibrating 4 2 Requirements for calibrating Defining expectation ranges Note Limits of expectation range Certified mode The upper and lower limits are defined by the PTB Physikalisch Technische Bundesanstalt certified and set when the device is delivered However you can change the values within these limits according to your application 1 In the navigation area open the General group 2 Click on the property object Expectation Ranges 3 Define the lower and upper limits for the gases and the calculated values CVControl User Interface NOT SEALED CONFIGURE 15 xl File Tools Help General Expectation Ranges E Device Id SICV6F7B48 E General Clock Version Units Streams Data Handling Approved Values Standby Settings Method Calibration Hardware Modbus Device SICVEF7B48 10 116 38 109 connected Ready The following units apply e Calorific values MJ m kWh m and BTU ft e Density kg m and lb ft e Concentration mol e Temperature C and F CVControl operating software Operating Manual 11 2012 A5E01428676 03 43 Calibrating 4 2 Requirements for calibrating Approved Values Measured values which are relevant to certification according to the directives of the country of use can be identified here as Approved This iden
74. erating software Operating Manual 11 2012 A5E01428676 03 17 Installing the software 2 5 SITRANS CV software upgrade Procedure for upgrading the Flash memory 1 Start the program RemoteFlasher Start bar Start gt Programs gt Siemens AG gt CVControl gt Tools gt RemoteFlasher RemoteFlasher 1 05 10 x C Application J z Device iP Version Infomation Application pernime 08 00 06 6f 7b e6 10 116 38 103 1 13 01 Dec 15 2006 1 SICV 1 05 00 retail built Se Part Number A5E00324827 05 04 Iv RS232 J Debug Serial J EDBG Flash Start Application Reset Device il N Done 2 Click and select the CELO x y BIN file x y version number from the Operating System directory of the Control Software Interrupt the power supply for about one second Wait until the device is indicated under Device and then select it Select the option button Loader and activate the option box RS232 ao a A O Click on the Flash button the software upgrading of the Flash memory will then begin The procedure terminates with the message Flashed The message appears at the bottom left in the corner of the dialog box RemoteFlasher 7 To conclude click the Reset Device button CVControl operating software 18 Operating Manual 11 2012 A5E01428676 03 Installing the software 2 5 1 Procedure 2 5 SITRANS CV software upgrade Transferring the operat
75. et the following option in the tab Tools gt Folder options gt View Hidden files and folders Display all files and folders e If several users operate the chromatograph with their own access each user must carry out this procedure because the configuration file is saved in the user profile 1 So that this configuration file NGControl config is generated automatically you must start the CVControl once and exit it again 2 Browse for the configuration file NGControl config using the Windows search function under C Documents and Settings 3 Open the configuration file NGControl config using the Windows Editor The first lines look as follows lt xml version 1 0 encoding utf 8 gt lt UISettings xmlns xsd http www w3 org 2001 XMLSchema xmlns xsi http www w3 org 2001 XMLSchema instance gt lt IP Number gt 161 218 51 47 lt IP Number gt lt Port Number gt 8500 lt Port Number gt lt CSVFi le gt C Program Files Siemens AG SamNG Bin DataLogging Data csv lt CSVFile gt 1 Enter the IP address of your chromatograph in the line lt IP Number gt Otherwise do not change anything and then save the file CVControl operating software 20 Operating Manual 11 2012 A5E01428676 03 Installing the software 2 7 Restoring data 2 7 Restoring data 2 7 1 Restoration of the application data Execute the CVControl operating software in order to restore your application data Procedure 1 Start the program CVControl
76. g Manual 11 2012 A5E01428676 03 Operation 3 2 Procedure Starting of operation 1 Start the program CVControl start bar Start gt Programs gt Siemens AG gt CVControl gt CVControl 3 2 Starting of operation The program requires about 5 seconds to load the Start dialog box A cvcontrol Connected M Chromatograph Device Id Software Version Software Signature Setup Signature Seal State SICVEF7B48 CAC 1 1 RSP Hardware 1 4 RSP Firmware 0001 4024 SIC 1 05 00 NOT SEALED User Interface Software Version Software Signature 1 25 2 0 7BFISBEA 9780 FDOS Login Access Mode Password MONITOR b MONITOR h CONFIGURE el Access Mode MONITOR CONFIGURE CVControl operating software Operating Manual 11 2012 A5E01428676 03 Cancel In the start dialog box CVControl select an operating mode in the drop down list 27 Operation 28 3 2 Starting of operation 3 Confirm your selection with OK The CVControl Transmitter User Interface window is displayed WAcvcontrol Transmitter User Interface NOT SEALED CONFIGURE File Tools Help Osec 150 sec M Curent State M Mode Select M Streams Ce e PPa Tane yclicRun Ei i Calibration Single Run Actual stream gt Sample1 lt Next stream Elapsed Time Run Time Hold oceete 215 x Sample2 Sample3
77. ges and logbook If an alarm occurs the chromatograph has a serious fault Example The carrier gas pressure is too low The results can no longer be trusted The chromatograph does not start a new analysis An alarm is shown in red by the chromatograph in the tab Device Status and by the red LED Failure behind the window Warning The chromatograph has detected a fault However the results can still be trusted Warnings are shown in yellow by the chromatograph in the tab Device Status and by the yellow LED Maintenance Request behind the window They do not have an effect on Ready and do not stop cyclic operation 6 1 Status messages and logbook Fault message e Current faults are displayed by the gas chromatograph in the tab Device Status under Current State by the message ALARM on a red background e The fault description is present in the box Active Alarms and Warnings e The status message or fault message is saved in the logbook Active Alarms and Warnings Posted Time Status Description o 12 09 2007 14 18 06 Alarm CAL1 Optimization of CycleE vents failed Note e Once the cause of the alarm has been eliminated the corresponding message is deleted from the box Active Alarms and Warnings e However all status messages remain saved in the logbook even if the cause of the alarm has been eliminated See also Section Logbook Page 73 CVControl operating software 60 Operating Manual 11 20
78. his is the deviation of the Actual Concentration from the Nominal Concentration CVControl operating software Operating Manual 11 2012 A5E01428676 03 49 Calibrating 4 4 Results of the calibration Meaning of parameters in the window Calibration Details See also 50 You can view the following parameters for the current previous and original calibrations Sealed Calibration Calibration Cycle 1 Calibration Cycle 2 ne RT_ RT Dev Concentration Conc Dev 1 4 RT Conc Dev 4 RT Area Concentration RT Area Concentration RT Oxygen 49 18 00340 49 17 3387 00 0 0491 49 17 3392 00 0 0491 49 18 Nitrogen 51 54 0 0280 51 45 29556 00 40089 51 45 29589 00 4 0100 51 46 Carbon Dioxide 42 64 0 0338 42 65 25073 00 14765 4265 25078 00 14756 42 65 Methane 58 54 0 0034 58 48 587970 0 88 9491 58 48 588424 00 88 9443 58 48 Ethane 50 71 0 0957 50 72 70088 00 39773 50 72 70239 00 39826 50 73 Propane 20 99 0 0473 20 99 19513 00 0 9887 20 99 19515 00 0 9890 21 00 19521 00 0 1106 24 39 0 1978 24 39 0 1982 24 40 0 0853 22 89 I 0 2010 2289 0 2007 22 89 0 7511 32 08 0 0507 32 08 0 0501 32 09 0 9846 29 55 I 0 0498 29 55 0 0503 29 55 0 1418 0 1879 3 60 0 0501 3 60 i 0 0501 3 61 OK Retention time RT is the time required by the components in the sample
79. his value component is required or essential for fiscal metering Name Is the name of the component or calorimetric value Value Is the calorimetric value Unit Is the unit of the calorimetric value Concentration The chromatograph calculates the component concentration from the peak area and the calibration factor Retention Time Is the actual retention time which the peak had in this analysis Area Is the peak area in counted units Results which cannot be trusted If faults have occurred during the analysis the chromatograph indicates this in the tab Report by a tick at the top right for Alarm The corresponding results are zero for these analyses These values are not included in generation of the mean value Printing of current result If a printer is connected to the PC you can print out the results currently shown on the screen Click the Print Report button in the tab Report the Windows print dialog is shown 88 CVControl operating software Operating Manual 11 2012 A5E01428676 03 Viewing and analysis of measured values 9 2 Displaying chromatograms 9 2 Displaying chromatograms Display chromatograms of last analysis 1 Select the tab Chromatograms WAcvcontrol Transmitter User Interface NOT SEALED CONFIGURE loj xj Fie Tools Help Device Status Report Mean Values Results Trend Calibration Result Chromatograms Logbook Device Setup
80. iag C Concentration Deviation C Calorific Values O Sample 3 O Mean Values Month C Calorific Deviations O Mean Values Configurable m Calibration Result Types O Calibration C Area C Retention Time _ Response Factor CalGas Concentration Separator Semicolon Comma C Program Files Siemens 4G C Control Bin E Exporting will create csv files in the selected directory Naming pattern lt Now gt lt Result type gt lt Stream name gt csv Downloading the requested data may take several minutes oT Cancel Export Close 3 Start the data saving with the Start Export button 4 Following selection of the save options click the Close button to exit the dialog box Export Result History Saving of current result on hard disk In the report window click on the Save Results As button or select the function Save Results As in the File menu 98 1 Select the directory and file name The current result is then saved as a mbd file Maxum Binary Data CVControl operating software Operating Manual 11 2012 A5E01428676 03 Viewing and analysis of measured values 9 6 Continuous printout of data relevant to calibration 9 6 Continuous printout of data relevant to calibration Requirements 1 The PC with the CVControl operating software and the sealed SITRANS CV process gas chromatograph are connected together and in operation 2 An interval for the printout is set for a co
81. ilability and repeatability of the analysis The gas chromatograph optimizes the column switching commands and integration parameters depending on the current retention times Optimization is carried out without time loss for the first two analyses of the calibration sequence which are normally rejected This improves the repeatability of the calorific value measurement and the aging process is compensated Note Cancellation of certification The optimization of method is part of the country specific settings and is usually activated Certified mode The settings of the automatic optimization of method must not be changed otherwise the certification is canceled Note Optimization Error The chromatograph signals an Optimization Error if not all peaks are detected which are referenced for the optimization CVControl operating software Operating Manual 11 2012 A5E01428676 03 51 Optimization of method 5 1 Switching the automatic optimization of method on and off 5 1 52 Finally click the Apply button WA cvcontrol User Interface NOT SEALED CONFIGURE Switching the automatic optimization of method on and off The automatic optimization of method can be activated for Cycle Events and Integration Events The parameters Optimize CycleEvents and Optimize IntegrationEvents Peaks amp Groups are available for activation in the tab Device Setup Calibration gt Calibration Se
82. imethylobutane Dinitrogen monoxide CVControl operating software Operating Manual 11 2012 A5E01428676 03 Ethane Ethylbenzene Ethylcyclohexane Ethylcyclopentane Ethylene Helium Heptane Hexane Hydrogen Hydrogen cyanide Hydrogen sulfide Isobutane Isopentane Krypton Methane Methanethiol Methanol Methylcyclohexane Methylcyclopentane 2 Methylpentane 3 Methylpentane 2 Methylpropene Neon Neopentane Nitrogen Nonane Octane Oxygen Pentane 1 Pentene Propadiene Propane Propylene Sulfur dioxide Toluene Xenon o Xylene Water 119 Transmission of results over Modbus 10 2 Changing MODBUS parameters Group components e Hexane Group e Hexane and higher e Heptane Group e Heptane and higher e Octane Group e Octane and higher e Nonane Group e Nonane and higher e ConfigurableGroup 1 e ConfigurableGroup 2 e ConfigurableGroup 3 e ConfigurableGroup 4 e ConfigurableGroup 5 e ConfigurableGroup 6 The component values are specified in the following manner lt stream name gt lt component value type gt lt component name gt In addition the non standardized values of the individual components can be scanned lt stream name gt ConcentrationRaw lt component name gt Calculated values The gas chromatograph calculates 7 values see the following table Parameter for the calculation Sample1 CV Inferior Calculated value Heating value Sample1 CV Superior Calorific value Sampl
83. ined in the stationary phase for a certain length of time Their duration in the stationary phase is added to the duration in the mobile phase dead time and they therefore require longer to pass through the complete GC column The term Retention was formerly used to indicate that the stationary phase retains the components in the sample stream for a certain period Nowadays the term is simply used to describe the time required by the components in the sample stream to pass through the column and therefore includes the dead time The terms are therefore defined as follows e Retention time Time required by the components in the sample stream to pass through the column This corresponds to the time which passes between injection and detection tR ts to e Net retention time Time for which the components in the sample stream are retained in the stationary phase ts e Dead time Time for which the components in the sample stream are retained in the mobile phase to Volume conversion device Wobbe index 134 The volume conversion device is a measuring instrument for calculating the gas volume flow at standard conditions derived from the measurement in the operating state The volume conversion device determines the volume flow at standard conditions of the medium to be measured based on the quantity measurement in the operating state and its temperature and pressure The quantity determined in this manner is specified in Nm The
84. ing system to the device Click and select the SICVxyyzz file xyyzz version number gt 20000 or higher from the Operating System directory of the Control Software Select the desired process gas chromatograph under Device in the window RemoteFlasher Note If the device is not displayed switch off the power supply for approx 10 seconds using the external power switch Then switch on the power supply again and wait until the device is displayed Activate the option box RS232 Click on the Flash button the RemoteFlasher program will then transfer the operating system The procedure is concluded by the message Flashed The message appears at the bottom left in the corner of the dialog box RemoteFlasher To conclude click the Reset Device button Exit the program RemoteFlasher using the Done button The SITRANS CV software upgrade has now been completed CVControl operating software Operating Manual 11 2012 A5E01428676 03 19 Installing the software 2 6 Selecting the chromatograph 2 6 Selecting the chromatograph Note The CVControl operating software only communicates with one chromatograph Therefore set the IP address for the chromatograph you wish to operate in the file NGControl config The communication settings are defined in a configuration file Procedure Note e To display the directory Local Settings in the Windows Explorer s
85. is control and operating modes 8 6 Standby Switching procedure in the following window e g between 229 kPa and 214 4 kPa WA cYControl Transmitter User Interface NOT SEALED CONFIGURE e xd File Tools Help Device Status Report Mean Values El Device Id SICVEF7BES General E Method B Cycle Events Detectors Valves Events Integration Events Peaks Groups Measured Components Auxiliary Components Calibration Hardware Modbus Configuration Results Trend Calibration Result Chromatograms Logbook Device Setup Method Cycle Events Pressures Name EPC Use Reference Setpoint MaxDev Use MaxDev Time Cum Rule _Shift Relative Weight Peak 1 LEPC EPCI EPCILSPI 2800 Sp gt Tan ed nmt oso imo ream lea m ream aw go Sa gt mopa oo omo tom LEPa EPC3 EPCASPL 2280 aoise gt oe san eo ne 0 ape LEPC302 EPC3 W EPCRSP2 2125 oo 2 2 au ant sa 0 500 _1 000 HelpP_Cu Stop gt Chromatograph SICVEF7BE6 Connected Ready CyclicRun 118 sec 150 sec Note Whenever measurements are being carried out the pressures setpoint 1 and setpoint 2 can switch back and forth between EPC3 e g between 229 kPa and 214 4 kPa 82 CVControl operating software Operating Manual 11 2012 A5E01428676 03 Analysis control and operating modes 8 7 Possible operations 8 7 Possibl
86. ition between two reference peaks Peak 1 and Peak 2 The value 0 5 for example means that the time average is between the two peaks Weight is a weighting factor for corrections The mean value is generated between the previous and new retention times Example With a value of 1 0 the new retention time is applied directly With a value of 0 5 the new retention time has a 50 effect CVControl operating software Operating Manual 11 2012 A5E01428676 03 Optimization of method 5 3 Peaks and peak list 5 3 Peaks and peak list e All peaks of the peak list must be identified correctly Note e The name of the peak and the retention time must appear on the chromatogram e The x axis shows the retention time and the y axis the signal strength e The following example refers to the analysis module C09 e Detector 3 is not activated for the analysis module C09 Detector 1 Measurement and display of the name and retention time of the peak s MA SICY6F7BE6 TCD1 Calibration 28 09 2007 15 48 24 CVControl operating software Operating Manual 11 2012 A5E01428676 03 55 Optimization of method 5 3 Peaks and peak list Detector 2 Display of Dossier peak without measurement MA sICV6F7BE6 TCD2 Calibration 28 09 2007 15 48 24 CVControl operating software 56 Operating Manual 11 2012 A5E01428676 03 Optimization of method 5 3 Peaks and peak list Detector 4
87. l compound belonging to the group of alkanes saturated hydrocarbons It is a colorless and odorless gas with the formula C2He Ethane is primarily used for heating and combustion purposes Ethane is a main component of natural gas in addition to methane Ethernet is a fixed cable data network technology for local area networks It enables data transfer in the form of data frames between all devices that are connected in a local area network e g computers printers Ethernet covers definitions for types of cables and connectors describes the signaling for the physical layer and defines packet formats and protocols A firewall also referred to as a network or hardware firewall is a network security component in information technology which permits or prohibits network traffic using defined directives The objective of a firewall is to protect the data traffic between network segments according to various levels of trustworthiness A typical application is to control the transition between a local network high trustworthiness and the Internet no trustworthiness The gas density p specifies the mass of gas present in a defined volume GC Gas chromatography GOST FOCT 132 Gas chromatography is an analytical method used worldwide to separate mixtures into individual chemical compounds GC can only be used for components which are gaseous or can be vaporized With this type of chromatography an inert gas is used as the mobile phase
88. l operating software Operating Manual 11 2012 A5E01428676 03 129 List of abbreviations 130 Abbreviation symbol Explanation m Meter ms Cubic meter max Maximum MB Megabyte mbd File format abbreviation for Maxum binary data Mbit 106 bits MHz Megahertz min Minute MJ Mega joule ml Milliliter MMI Man machine interface Mol Mol is the SI base unit for amount of substance MPa Megapascal PC Personal computer PTB Physikalisch Technische Bundesanstalt German Technical Inspectorate RAM Random access memory RF Response factor ROM Read only memory RS Recommended standard RS 232 also EIA 232 Identifies an interface standard for a sequential serial data transmission RS 485 also EIA 485 Identifies an interface standard for a differential serial data transmission RSP Real time signal processing RTD Resistance temperature detector s Second TCP IP Transmission Control Protocol Internet Protocol a reference model for communication on the Internet V Volt V n n n Version with version number VC_CH Valve CVControl operating software Operating Manual 11 2012 A5E01428676 03 Glossary AGA AGA 8 Backspace Calorific value Combustion gas Abbreviation for American Gas Association This is an amalgamation of companies producing and processing natural gas AGA 8 is a standardized algorithm for calc
89. le must be parameterized for this and limits must be entered for the components If the limits are violated the chromatograph triggers an alarm and continues to use the previous calibration factors Note Digital output in the gas chromatograph automatically switches on the calibration flow CVControl operating software Operating Manual 11 2012 A5E01428676 03 47 Calibrating 4 4 Results of the calibration 4 4 Results of the calibration e You can view the response factors of all components for the current previous and original calibrations in the window Calibration Result WA cvcontrol User Interface NOT SEALED CONFIGURE 3 Ele Tools Help Device Status Repot Mean Values Resuts Trend f Result of Computed Calibration ses E Calibration Time 17 09 2012 10 06 26 Chromatograms Logbook Device Setup Response Factor Calibration Gas pas Seen Sealed Previous Computed Nominal Measured with Previous Deviation 1 Oxygen 68769 4388 69107 5051 0 0483 0 0495 0 0002 2 Nitrogen 7412 3642 7487 193 3 9900 4 0232 0 0332 3 Carbon Dioxide 16946 3964 17065 7658 1 4800 14877 0 0077 4 Methane 6621 3485 6637 1986 88 8533 88 9026 0 0493 5 Ethane 17594 0685 17648 6216 3 9900 3 9950 0 0050 6 Propane 19733 4007 19846 6464 0 9890 0 9929 0 0039 7 Butane 23095 9596 23200 3367 0 1980 0 1985 0 0005 8 Isobutane 22228 8557 22318 4080 0 2010 0 2014 0 0004 9 Pentane 26220 0000 261
90. ly The settings will be saved in the gas chromatograph WA cYControl Transmitter User Interface NOT SEALED CONFIGURE Mei xj Fie Tools Help Device Status Report Mean Values Results Trend Calibration Result Chromatograms Logbook I Device Setup Er Device Id SICVEFTBES pleaser Deve Soe General Modbus Enabled Method Slave Id B Calibration Mode Calibration Settings RS Type Calibration Gas Baudrate Alarm Limits Data Bits Alarm Settings Stop Bits Modbus Configuration MOD Driver File Name corer RTU Frame End Timeout ms eames ASCII No Data Timeout ms Sp App Answer Timeout ms AX TX Wait ms Caw Chromatograph SICY6F7BE8 Connected Ready CyclicRun 95 sec 210 sec CVControl operating software Operating Manual 11 2012 A5E01428676 03 Transmission of results over Modbus 10 2 Changing MODBUS parameters 10 2 1 2 Capabilities The following non editable information is displayed in the property object Capabilities e AppValues e Adapters e MbValueTypes WA cYControl Transmitter User Interface NOT SEALED CONFIGURE 15 x Fie Tools Help Device Status Report Mean Values Results Trend Calibration Result Chromatograms Logbook Device Setup
91. mission trace data from a detector with the RSP was faulty Internal deactivated Gas chromatograph deactivated A D failure A D converter failure Low supply pressure Supply pressure is low Pressure out of limits Pressure violates the range limits Supply pressure out of limits Supply pressure outside the range limits Pressure out of control Pressures out of control Voltage out of control Power supply out of control No gas supply Gas supply interrupted CVControl operating software Operating Manual 11 2012 A5E01428676 03 Alarm fault and system messages Valve alarms Temperature alarms Flashloop faulty Sample faulty Backflush faulty Injection faulty Control error RTD error Deviation exceeded Internal deactivated Gas chromatograph deactivated No gas supply Gas supply interrupted CVControl operating software Operating Manual 11 2012 A5E01428676 03 125 Alarm fault and system messages Calibration alarms 126 Unspecified Error An unspecified error has occurred Analyses out of limits The concentration of one or more components determined during a single relevant calibration analysis is outside the range specified by Calibration Limits A relevant analysis is one that is used to determine the response factor Calorific values out of limits Only occurs in Sealed Mode The calorific values calculated from the calibration analyses with the current re
92. mmercially available printer Note Printing interval We recommend setting of the interval to 2 hours since a printout for this period approximately fits on a DIN A4 page Set the time interval to 2 hours in the ngcontrol config file of the CVControl operating software Starting of printing 1 Mark the parameter Continuous Print Log of Results with a tick in the menu Tools gt Log Settings x Logging Chromatograms as Measured Binary Data mbd IV Continuous Print Log of Results 2 Click OK to confirm Stopping of printing 1 Remove the tick from the parameter Enable Continuous Print Log in the menu Tools gt Log Settings 2 Click OK to confirm CVControl operating software Operating Manual 11 2012 A5E01428676 03 99 Viewing and analysis of measured values 9 6 Continuous printout of data relevant to calibration Description of functions e The values relevant to calibration for all analyses of the last completed interval are printed out at defined intervals e g 1 to 2 hours e A successful printout is recorded in a log file on the PC e Ifa printout fails it is not recorded in the log file e Ifa printout has not yet been made the last 4 days are printed e Prior to printing a check is made to see whether previous print jobs are missing in the log file If print jobs are not more than e g 4 days beforehand they are repeated This guarantees that all
93. nalysisCount The number of hours for the variable average interval is also available as Sample1 MeanVariable IntervalHours CVControl operating software Operating Manual 11 2012 A5E01428676 03 121 Transmission of results over Modbus 10 2 Changing MODBUS parameters 10 2 2 5 10 2 3 122 Result of the last analysis A further result range is available which saves all result values of the last analysis independent of the product stream number Each time a new result is available for one of the four product streams the values of this area are also updated Examples LastResult Analysisld LastResult Status DataNotValid LastResult Concentration Butane LastResult OEM1 NewDataFlag 3058 LastResult Status Alarm The gas chromatograph provides a value as additional information which saves the sample stream number of the last result LastResult Sampled Data backup and restoration 1 Start the program CVControl start bar Start gt Programs gt Siemens AG gt CVControl gt CVControl Select the tab Tools Save the data for the gas chromatograph using the menu commands Save Modbus Device Settings and Save Modbus Map Load the data for the gas chromatograph using the menu commands Load Modbus Map and Load Modbus Device Settings CVControl operating software Operating Manual 11 2012 A5E01428676 03 Alarm fault and system messages 1 1 The fault and alarm messages are listed
94. ninnneennrndstenneaitnansdennaannaadtenadadiu annaed aaan 17 2 5 SITRANS CV software upgrade coas aani E E EE E N 17 2 5 1 Transferring the operating system to the device sssssseesseeeirssserrsstirrssttrrssttrrssttnrsstennssten nent 19 2 6 Selecting the chromatograph esssseessessssssiresnrnsieindaetinnnntnntaennnadstenadadtanaddennaanaaddaaaaaad anand aiana 20 2 7 Restoring daldaran a a aa aia a a e ale 21 2 7 1 Restoration of the application data cccceccccccceeeeeeecencaeceeeeeeeeecaeaeceeeeesesecaacaeeeeeeesesecsiaeeeeess 21 2 7 2 Installing the country specific Settings 2 0 eee rniii niei nnee Enae EAE aE 22 2 7 3 Setting the Calibration Gass renine a O a 23 2 7 4 Parameterization and saving Of Modbus ccceeceeeeeeeene eter entree ee taeee ee taeeeeesaeeeeetnaeeeenenaeeeeee 23 3 OPOratiOMs savcccdedeses ee caval sy edhe ed ce cea dea A EAA aAa sis oe SAA nad an A es Mee deeeiaea dives 25 3 1 Fundamentals for operation ccccceceeeeeeeeececeeeeeeececacaeceeeeeeesecqacaeceeeeesesecanaeeeeeeesesensinaeeneess 25 3 2 Starting Of OPSration c scssccccsscse cece cites eddie ceeded a aa a a aa aa Hiedebdhdeenieeedderneaddinitees 27 3 3 Locking of operation for calibrated MOdE ecececeeeeeeeee ener ee erent cece teeter tases eetaeeeeetaeeeeeeneeeeees 29 3 4 Entering the parameters scx ised saecdedeudei noe hides acti nevada hee netinds 30 4 Calibrating sic siiva Meet kiana onan ean AET 3
95. ntegrate the automation components into a holistic IT security concept for the entire plant machine You can find information on this at http www siemens com industrialsecurity Note Malfunctions resulting from older versions of the software described here in the device or on the PC Observe the installation instructions of the software described here on the supplied CD If necessary uninstall any older versions prior to installation of the new software CVControl operating software Operating Manual 11 2012 A5E01428676 03 9 Installing the software 2 1 Operating software and requirements placed on the chromatograph 2 1 Operating software and requirements placed on the chromatograph CVControl operating software CVControl is the operating software for the SITRANS CV process gas chromatographs This is a measuring instrument for the calorific value and composition of combustion gases such as natural gas or biogas The CVControl software program contains the following functionalities described in the User s Manual e Calibration e Automatic optimization of method e Status e Logbook e Analysis control and operating modes e Viewing and analysis of measured values e Transmission of results over Modbus e Loading and saving the parameters Installation requirements e Atleast the following hardware and firmware versions must be installed in the chromatograph CAC A5E01052942 RSP hardware A5E00315395
96. ollecting and Exporting reSUlts eion n i E A O A iS iat 97 9 6 Continuous printout of data relevant to calibration cccececeecceceeeeeeeeeeeeeeeeeeeeeeeeeeneeeeeeeeeeees 99 9 7 Calculation formulae raunir E lantecubuatecesaadecechuuacteendtantecwbuadicensnictectetanncend laa 102 9 7 1 Calculation of response factors for the calibrated component ccccceeeeeeeeteeeeeeeeeeeees 102 9 7 2 Calculation of standardized areas for calibration ccecceeeeeeeeeeeeneeeeeeeneeeeeseaeeeeetaeeeeetnaeeeene 103 9 7 3 Calculation of standardized concentration from the peak area ccecceceeeeeeeeeeeeeeeeeeeettees 104 CVControl operating software Operating Manual 11 2012 A5E01428676 03 Table of contents 10 Transmission of results Over MODUS ccccssceccssseeeecssseeeeeesseneeeesseneeeesseneeesssenneeseseaneesessaeeesesenseeeess 105 10 1 The Modbus interface cccccceceeeeeccceceeeeeeeeeeeaneeceeeeeceeeanaeeeeeeeeeseesanaeceeeeeseseeninaeeeeeeeeseensaees 105 10 2 Changing MODBUS parameters eseti e EEE EEEE TE 107 10 2 1 Interface specification with Modbus Configuration seesseseessesieeseerrssrrresetrresrerrssrernsseennene 108 10 2 1 1 Parameterizing interfaces with Device Settings ss eeesessrrssserresrerrssttrresttrrssrtnrsstrnsstennnnt 108 10212 Capables nra E E E S 109 10 2 1 3 Parameterizing interfaces with Map seseesssssesssrneserrrsnrirnrernnnne
97. on for setting the sample flow monitoring function is only to provide users with a better understanding The sample flow of e g 20 ml min is monitored permanently It is interrupted once in each analysis cycle by the injection process The sample flow alarm is present at digital input 1 24 V DC Requirements 1 The sample preparation must have a sample flow monitoring function 2 The device and the CVControl operating software have been started CVControl operating software 66 Operating Manual 11 2012 A5E01428676 03 Status Procedure 6 5 Sample tlow monitoring Select CONFIGURE in the drop down list in the CVControl program and confirm with OK The CVControl Transmitter User Interface window is displayed WA cY Control Transmitter User Interface NOT SEALED CONFIGURE 15 xi File Tools Help Device Status Repot MeanValues Results Trend Calibration Result Chromatograms Logbook Device Setup M Curent State M Mode Select m Streams Run C a E 1 X Calibration Single Run Actual stream gt 1X Samplet lt Nest stream Elapsed Time 79 Run Time 2 Sample2 O Hold 3 Sampled ee Osec 150 sec Cancel Calibration Enable Streams Select the Device Setup tab Open the groups Method and Cycle Events in the navigation area Click on the property object Valves WA C Control Transmitter User Interface NOT SEALED CONFIGURE R
98. on formulae Page 102 CVControl operating software Operating Manual 11 2012 A5E01428676 03 33 Calibrating 4 2 Requirements for calibrating 4 2 Requirements for calibrating Preparing the calibration 1 34 The calibration flow must be activated in the CVControl operating software If this is not the case click on the Enable Streams button on the right in the tab Device Status WA CY Control Transmitter User Interface NOT SEALED CONFIGURE ife x File Tools Help Device Status Report MeanValues Results Trend Calibration Result Chromatograms Logbook Device Setup m Current State M Mode Select Streams C e e pe ETN yclicRun ame mo 1 X Calibration Single Run Actual stream gt 1 X Samplet lt Next stream Elapsed Time Run Time 2 Sample2 O Hold 3 Sample3 eee Osec 150 sec Cancel Calibration Next Stream Name Status Bridge i v Calibration M W Samplet C Sample2 O Sample3 Valves Name Status Value FlushLoop C_CH1 Ready Sample C_CH2 Ready a Backflush VC_CH3 Ready o Injection C_CH4 Ready oO Name Status MMI Ready Chromatograph SICVEF7B48 Connected Ready CyclicRun 89 sec 150sec A column Calibrated is present in the component list Device Setup gt Method gt Measured Components Here you must mark all components to be calibrated with a tick
99. ou can change depends on the operating mode e In MONITOR mode most of the operating functions are disabled to prevent errors in measurement due to unintentional operations It is still possible for example to change the enabling of samples e In CONFIGURE mode all parameters can be accessed The tabs of the CVControl window listed below are used to check correct functioning of the chromatograph or to view the results e Device Status e Report e Mean Values e Results Trend e Calibration Result e Chromatograms e Logbook CVControl operating software Operating Manual 11 2012 A5E01428676 03 25 Operation 3 1 Fundamentals for operation Complete parameterization of the chromatograph is possible in the tab Device Setup Parameterization may only be carried out by experts or calibration officials NOTICE Leave factory settings unchanged e The factory settings of the functions must not be changed by the user e lf the factory settings are changed nevertheless This corresponds to intentional manipulation and therefore a non approved application of the device The accuracy of the measurements will become less exact The device may no longer match the certification e The device is delivered non calibrated The calibration must be carried out by a calibration official or deputy of the country in which the device is used CVControl operating software 26 Operatin
100. ploaded Setup to chromatograph i 0 500 1 000 Chromatograph SICVEF7BBE Connected pasa a e During this time the chromatograph waits for further inputs e tthen saves the data into the Flash memory Data saving takes about 20 seconds and is indicated by the message Flashing e f you switch off the device during this phase or if the power supply fails the data in the memory are of no use CVControl operating software Operating Manual 11 2012 A5E01428676 03 Singin f sta After clicking the APPLY button the note Flash pending is displayed in the status line for about three minutes Operation 3 4 Entering the parameters Entering numerical values 1 Click in the input box 2 Enter the value using the digit keys Entering logical values names or numbers from a drop down list Click in the parameter box and then on the arrow on the right in the input box A drop down list is displayed Click on the desired value in this list Commenced input The input is not effective until you click on the APPLY button the existing values still applies You recognize this in that the APPLY and UNDO buttons are still active and not pale as was the case prior to commencement of inputs Incorrect input e An incorrect numerical input can be deleted in steps using the backspace key on the PC keyboard e Drop down lists can be exited by clicking in a different box e tis sometimes the c
101. pproved Name Value Unit 1 x Superior Calorific Value 39 9742 MJ m3 2 Inferior Calorific Value 36 0996 MJ m3 3 x Density 0 80710 kg m3 4 Relative Density 0 6242 unitless 5 Wobbe Index 50 5945 MJ m3 6 Compression Factor 0 9973 unitless 7 100 Norm 1 0006 unitless No Approved Name Concentration Retention Time s Area 1 X Oxygen 0 0493 49 16 3391 11 2 X Nitrogen 3 9957 51 43 29617 41 3 X Carbon Dioxide 1 4818 42 64 25111 61 4 X Methane 88 9410 58 47 588909 10 5 X Ethane 3 9930 50 71 70252 67 6 X Propane 0 9896 20 99 19528 14 7 X Butane 0 1981 24 39 4574 84 8 X Isobutane 0 2013 22 88 4473 78 9 X Pentane 0 0508 32 08 1331 83 10 X lsopentane 0 0494 29 54 1246 78 11 X Neopentane 0 0000 25 19 0 00 12 X Hexane And Higher 0 0501 0 00 1649 03 Device SICV6F7B48 10 116 38 109 connected You can view the results list of the last analysis in the display Report Select the desired sample in Sample Stream CVControl operating software Operating Manual 11 2012 A5E01428676 03 87 Viewing and analysis of measured values 9 1 Displaying the results list Report Description of parameters Calorimetric values Calculated Values These are the calculated values from the component concentrations according to the procedure entered in the tab Device Setup Calibration gt Calibration Settings under Calculation Method Approved Value If this column is ticked t
102. ransmit with 1 Select Map Entries in the navigation area and click the Add Line button in the dialog box WA cvcontrol Transmitter User Interface NOT SEALED CONFIGURE ioj xi File Tools Help Device Status Repot MeanValues Results Trend Calibration Result Chromatograms Logbook Device Setup E Device Id SICV6F7BE8 pMechus Contoustion AN EON General Application Value Method Missing lunspecified B Calibration Calibration Settings Calibration Gas Alarm Limits Alarm Settings Hardware E Modbus Configuration Device Settings Capabilities Map Byte Formats Constant Values Map Entries Chromatograph SICV6F7BE8 Connected Ready CyclicRun 161 sec 210 sec 2 In the dialog box select in succession the desired value for Application Value e g HealthState 3 Select a suitable adapter CVControl operating software 114 Operating Manual 11 2012 A5E01428676 03 Transmission of results over Modbus 10 2 Changing MODBUS parameters 4 Depending on the application the parameters must be set under Adapter Parameters iaix WAcvcontrol Transmitter User Interface NOT SEALED CONFIGURE Fie Tools Help Device Status Report MeanValues Results Trend Calibration Result Chromatograms Logbook Device Setup m Modbus Configuration Map Map Entries Application Value Adapter Adapter Parameters E Device Id SICVEF7BE6 General Addre
103. required values are printed out even with problems such as a power failure or no paper in the printer Contents of the printout 100 Line 1 Text Description Date Date of analyses Period Monitoring period Chromatograph ID of the gas chromatograph State Approved state means measured values are subject to obligation of verification Setup Signature Checksum of factory settings Analyses Number of analyses Page Page number Line 2 Text Description Text Description Time hh mm ss Time in seconds C1 Mol Methane S Sample Sample stream C2 Mol Ethane O Out of Range Expected range C3 Mol Propane violated A Alarm Alarm during an nC4 Mol Butane analysis R Revision Digital input was set to iC4 Mol 2 methyl propane revision GHV MJ m3 Calorific value nC5 Mol Pentane Dens kg m Density iC5 Mol 2 methyl butane N2 Mol Nitrogen neoC5 Mol 2 2 dimethyl propane CO2 Mol Carbon dioxide C6 Mol Hexane and higher hydrocarbons CVControl operating software Operating Manual 11 2012 A5E01428676 03 ing and analysis of measured values Viewi intout of data relevant to calibration iNUOUS pri 9 6 Cont Example of a printout 8TS0 00 805000 TTSO 00 25250 00 PTSO OO 05000 SETSOOO 6250 00 T50 00 805000 FETSO OO 4750 00 OZS0 00 805000 TTS0 00 f4250 00 9T50 00 805
104. rrinneetrannnnnnnesnnnuertannnanaena anna aa 111 10 2 2 Description of the application parameters cccceccceeeeeeeeeeeeeceeeeetesecaeceeeeeeeseeennaeeeeeeeeteees 116 10 2 21 Device Information mne nn ae a e e a a a E EE E A a e ela A 116 10 2 2 2 General sample stream information cccccccceeeceeee cece eeeeseneaeeeeeeesesecaeeeeeeeeeseseenaeeeeeeeetenes 117 10 22 39 Result VAIUGS prsi nnne aa aa a aaa a aa aaa aeaa a tects cdavlde r e hikes aad 118 102 244Mean Value Si sa a a sh cd aaa a NA 121 10225 Result ofthelastanaly IS aeiia T E E E EEE O 122 10 2 3 Data backup and restoration cccceceececce cee eeeeeeeeceeeceeeeeeeeeaeaeeeeeeeseccaaeeeeeeeeeeecennieeeeeeeeteeea 122 11 Alarm fault and system messages ccccccessssssseseeeeeeessseseeeeeeeeeesssceueesseeneeesseceeeesseeeeeessssseeseeeeess 123 12 lt Serviceand SUPPO A tre rn Deis coh a ties ie nt eae a eaa e 127 13 _ListiOf abbreviati nS s 25 55 innie eaaa dee hen Seca ada nbd oes dase donate 0k bab gh aves ce aedskcbiacdovanisbevstticbessenioaa ai 129 GIOSSAIY E EP EEE E E E E EE TE AA EE AA E EE AT 131 ae er E E A EA TET A E E A E E E EAS 135 CVControl operating software Operating Manual 11 2012 A5E01428676 03 5 Table of contents CVControl operating software 6 Operating Manual 11 2012 A5E01428676 03 Introduction This manual describes the CVControl software for the SITRANS CV process gas chromatograph The
105. sponse factors are outside the specified range Difference to sealed calibration Only occurs in Sealed Mode Occurs if the concentrations calculated using the response factors of the sealed calibration are outside the specified range compared to the concentrations of the current calibration gas Difference to last calibration Only occurs in Sealed Mode Occurs if the concentrations calculated using the response factors of the previous calibration are outside the specified range compared to the concentrations of the current calibration gas Optimization of CycleEvents failed Optimization of the CycleEvents has failed A common cause is the non recognition of a peak required for optimization Optimization of IntEvents Peaks and Groups failed Optimization of the IntegrationEvents Peaks and Groups has failed A common cause is the non recognition of a peak required for optimization Reached Calibration timeout The maximum permissible duration for a calibration has been reached Reached maximum number of failed calibrations The maximum permissible number of failed calibrations has been reached CVControl operating software Operating Manual 11 2012 A5E01428676 03 Service and support Service and support Worldwide contact partners If you have any further questions relating to the products described in this documentation contact your local representative at the Siemens office nearest you You will find inform
106. ss Write Access Unit Method LastResult RetentionTime Argon REALtoSCALED ScaleFactor 9999 BadValuel Calibration Hardware E Modbus Configuration Device Settings Capabilities Map Byte Formats Constant Values Map Entries Name EUHIAdd 3034 None Adapter Parameters xj Chromatograph SICV6F7BE6 Connected Ready CyclicRun 60 sec 150 sec Specify the register address Specify the access mode Write Access True ticked Holding Register Coil Write Access False not ticked Input Register gt Single Input 7 Sets the units for the results depending on the application 8 To save the data in the gas chromatograph confirm your inputs by clicking OK and Apply CVControl operating software Operating Manual 11 2012 A5E01428676 03 115 Transmission of results over Modbus 10 2 Changing MODBUS parameters 10 2 2 10 2 2 1 116 Device information Description of the application parameters Device parameter Device HealthState Values value range 0 unknown 1 ready 2 warning 3 alarm Description Current state of device Device SealedState value value 0 Is correct if the device is currently in calibrated mode Device DateTime Read Local time referred to time zone of device e Current date and time of device e Readable Device DateTime Write Local time referred to time zone of device
107. t all CVControl operating software Operating Manual 11 2012 A5E01428676 03 61 Status 6 3 Monitored parameters 6 3 Monitored parameters Note The analysis and the results can no longer be trusted if there are faults in the parameters The following device parameters are monitored during operation e Temperature controllers 1 to 3 Ready Alarm e Pressure controllers 1 to 3 Ready Alarm e Detectors 1 to 4 Ready Alarm e Electronics with signal processing watchdog and communication e Gas supply e Expectation ranges e Checksum during calibrated mode e Monitoring of sample flow e Method e Modbus e Gas supply e Expectation ranges e Calibration e Standardization factor See also Calibrating Page 33 CVControl operating software 62 Operating Manual 11 2012 A5E01428676 03 Status 6 4 Gas supply 6 4 Gas supply Function e The gas chromatograph monitors the carrier gas pressure e Ifthe carrier gas fails the gas chromatograph switches off all heaters and detector power supplies The status display ALARM is then output in the CVControl operating software WA cY Control Transmitter User Interface NOT SEALED CONFIGURE 15 x Fie Tools Help Device Status Report Mean Values Results Trend Calibration Result Chromatograms Logbook Device Setup M Current State M Mode Select m Streams aan Hal Sens Wane 1 Calibration y Single Run Actual stream gt Samplet lt Next
108. t request Phone 49 180 5050 222 Fax 49 180 5050 223 0 14 min from German landline mobile charges may differ e You can find the latest information concerning your device on the Internet at www siemens com automation www siemens com automation CVControl operating software 128 Operating Manual 11 2012 A5E01428676 03 List of abbreviations Abbreviation symbol Explanation S Degrees C Degrees Celsius Percent hundredth part A D Analog digital AGA American Gas Association Bit Binary digit ca Approx CAC Communication and analytical control CD Compact disk CF Calibration factor CH4 CH4 methane cm Square centimeter CO2 CO2 carbon dioxide CRC Cyclic redundancy check an error detection procedure used for data processing CSV File format abbreviation for comma separated values or character separated values CV Calorific value DC Direct current Dens Density DVD Digital versatile disk e g For example EIA Electronic Industries Alliance EPC Electronic pressure controller ETC Electronic temperature controller ff and following e g pages paragraphs IEEE Institute of Electrical and Electronics Engineers IP Internet Protocol ISO International Organization for Standardization J Joule kg Kilogram kPa Kilopascal l Liter LED Light emitting diode CVContro
109. t to 1 if the chromatograph is switched off or reset The file in mbd format contains the results in Measured Binary Data format This data is only provided for service purposes and cannot be read using CVControl Saving of analysis results as CSV file on the hard disk 1 Open the menu command Export Result History in the Tools menu WA cvcontrol Transmitter User Interface File Tools Help Log Settings De g g Export Result History Change Access Mode Set new Password Load Modbus Map Save Modbus Map Save Modbus Capabilities Load Modbus DeyiceSettings Save Modbus DeviceSettings CVControl operating software Operating Manual 11 2012 A5E01428676 03 97 Viewing and analysis of measured values 9 5 Collecting and exporting results Define the desired save options by selecting The time interval for saving results The desired sample stream The desired results mean values or calibration values The saving location Export Result History ioix Destination Folder m Esport Interval From To foe 1 0 2007 z 08 00 00 08 10 2007 7 15 20 00 a M Stream Selection Result Types M Analysis Results M Concentration Area M Sample 1 O ji O Area not 100 normalized O Retention Time M Calorific Values M 100 Normfactor O Sample 2 O Mean Values Hour C Concentration Mean vaen D
110. th Modbus Example of a constant Value Modbus Type Address 100 1 R2 3200 CVControl operating software 112 Operating Manual 11 2012 A5E01428676 03 Transmission of results over Modbus 10 2 Changing MODBUS parameters 1 Select Constant Values in the navigation area and click the Add Line button in the dialog box 2 Enter the constant under Value and select the Modbus Type and Address When assigning addresses note the number of occupied registers e g R2 occupies 3200 and 3201 R2 ENRON occupies only 3200 WA cYControl Transmitter User Interface NOT SEALED CONFIGURE 15 xi Fie Tools Help Device Status Report Mean Values Results Trend Calibration Result Chromatograms Logbook Device Setup Er Device Id SICV6F7BE8 peee e LE Ae General Method B Calibration Calibration Settings Calibration Gas Alarm Limits Alarm Settings R2 Hardware E Modbus Configuration Device Settings Capabilities Map Byte Formats Constant Values Map Entries Chromatograph SICV6F7BE8 Connected Ready CyclicRun 19 sec 210 sec 3 Confirm the input of all required constants by clicking on Apply CVControl operating software Operating Manual 11 2012 A5E01428676 03 113 Transmission of results over Modbus 10 2 Changing MODBUS parameters Map Entries Use Map Entries to select the application values which you wish to t
111. the setup exe program in the folder Workstation on the CD 3 Follow the onscreen instructions of the installation program Note Recommended installation path The software is automatically installed by the installation program in the directory c Program Files Siemens AG CVControl Do not change the suggested path If you have support inquiries the Siemens AG employees will find and solve problems more easily with the standard installation Loading and saving parameters Note Changing device parameters All changes in the factory settings are written by the gas chromatograph in the logbook as a signature The calibration official need only check the signature in the logbook If the signature has changed the factory settings have also been changed CVControl operating software 12 Operating Manual 11 2012 A5E01428676 03 Installing the software 2 3 Installing the operating software e The parameters which have been factory set for your chromatograph are saved on the CD Parameter Backup If you have changed parameters unintentionally and wish to restore the factory parameters download the parameters from this CD into the gas chromatograph again e Inthe opposite direction you can also save parameters from the gas chromatograph onto the hard disk of the operating PC e If you are using a new calibration gas cylinder you must match the component concentrations The procedure is described in Section Requirem
112. tification 26 Checksums 84 Chromatogram 55 Abscissa 55 Analysis 89 Ordinate 55 Print 91 Representation 90 Scaling 91 Column switching command 51 Combustion gas 10 Component k Area 103 Concentration 103 Compressibility factor 122 Compression factor 122 Configuration file NGControl config 20 CONFIGURE 83 Operating mode 27 Contact partner 129 Country specific settings Installation 22 CSV file 98 CVControl Operating software 10 CVControl operating software 10 Cyclic Run 77 D Data Load 124 Saving 124 Detector 55 135 Index E Electronic pressure regulator 81 End of analysis 78 Expectation range Calibration of limits 42 External power switch 19 F Factory setting 12 84 Signature 12 Factory settings 8 26 Fault 59 Alarm 73 Saving 73 Warning 73 Fault description 60 Fault message 60 Firewall 14 Firmware 10 Firmware ID 8 Flash memory 17 Upgrade 18 G Gas composition measuring instrument 10 GOST Calibration alarms 41 Calibration details 49 H Hardware 10 History 8 Initialization pressure 81 Injection Lag 78 Injection process 66 Installation Country specific settings 22 Procedure 12 Interval 100 IT security 9 136 L Limits Calibrating 40 Location of use 8 Logbook 12 73 M Malfunction 9 Manipulation 26 mbd file 97 Mean value Interval 93 Start date 93 Start time 93 Time offset 93 Modbus 23
113. tification appears in the report along with the selected measured value The measured values identified in this manner are also represented in the device display Proceed as follows to assign the identification 1 In the navigation area open the General group 2 Click on the property object Approved Value 3 Mark the gases and calculated values to be checked by a tick in the dialog box Approved CVControl User Interface NOT SEALED CONFIGURE ioj xi File Tools Help M General Approved Values E Device Id SICV6F7B48 E General Clock Version Units Streams Display Alam Settings Calculation Settings Epectation Ranges Setup Integrity Standby Settings Method Calibration Hardware Modbus K K K K K K K K K K K K Device SICV6F7B48 10 116 38 109 connected Ready CyoicRun sec 150 sec CVControl operating software 44 Operating Manual 11 2012 A5E01428676 03 Calibrating 4 2 Requirements for calibrating Calculation standard SITRANS CV automatically calculates calorific values in accordance with the following standards e ISO 6976 1995 e GOST 30319 1996 e AGA8B 1994 Note AGA 8 also includes the standards GPA 2172 and ASTM 3588 AGA 8 also includes ISO 12213 and API Chapter 14
114. time the green LED Ready lights up behind the window of the gas chromatograph WAcvcontrol Transmitter User Interface SEALED MONITOR Eile Tools Help Device Status Report Mean Values Results Trend Calibration Result Chromatograms Logbook Device Setup M Current State Elapsed Time Run Time 150 0 sec 150 sec M Mode Select Cyclic Run I Standby Single Run O Hold Calibration Cancel Calibration m Streams Name Calibration Samplet Actual stream gt lt Next stream Sample2 Sample3 Enable Streams Nest Stream Temperatures Status Heater Temperature C Setpoint C TCD1 TCD2 TCD3 Ready Ready Ready Status Pressure kPa 67 0 66 9 65 4 Setpoint kPa FlushLoop C_CH1 Sample C_CH2 Backtlush C_CH3 Injection C_CH4 Ready Ready Ready v Description 290 2 230 0 221 5 221 7 229 1 230 0 Active Alarms and Warnings Name Status MMI1 Ready Chromatograph SICV6F7B48 Connected CyclicRun 108 sec 150sec Note If an alarm occurs during an analysis the measured values are set to a value of 0 This analysis is not included in generation of the mean value CVControl operating software Operating Manual 11 2012 A5E01428676 03 59 Status 6 1 Status messa
115. tion time 48 RSP firmware 10 RSP hardware 10 S Sample flow alarm 66 Sample stream sequence list 77 Serial number Rating plate 15 Single Run 76 Software Upgrade 17 Software version 7 Standardized response factor 104 105 Status display 63 System restoration 22 T Technical support 130 Training center 129 Trend View 94 137 Index U Upgrade Flash memory 18 Software 17 User interface 7 V Volume conversion device 107 W Warning 60 Wobbe index 42 138 CVControl operating software Operating Manual 11 2012 A5E01428676 03 Siemens AG Subject to change Industry Sector A5E01428676 03 Sensors and Communication Siemens AG 2007 2010 2012 P O Box 48 48 D 90026 NUREMBERG GERMANY www siemens com processautomation
116. trol of the tab Device Setup first click on the left in the navigation area on Calibration and then on Calibration Settings WA cvcontrol User Interface NOT SEALED CONFIGURE Ele Tools Help ETT Calibration Calibration Settings General Parameter Value Method Cycles to Skip Cycle for Optimizing Cycle Events m Cycle for Optimizing Integration Events Peaks and Groups w Cycles to Average 3 Max additional Cycles for Averaging if limits exceeded 0 Max number of Cycles with Alarm 100 Calibration Timeout minutes 20 Deviation Checking Mode Deviation of Min and Max from Mean Autocalibration Interval days 1 Autocalibration Day of Week 7 days interval only Monday Autocalibration Time 08 00 00 Maximum number of Consecutive Failed Calibrations 2 Device SICV6F7B48 10 116 38 109 connected Ready CyeticRun 13sec 15sec Enter the parameters Confirm the input using the Enter key on the PC keyboard Click the Apply button when you have entered all values Description of parameters Cycles to skip Number of initial analyses carried out prior to the valid calibration cycles and whose results are rejected Cycle for Optimizing Cycle Events Additional analysis used for optimization of method see Section Optimization of method Page 51 Cycle for Optimizing Integration Events Peaks amp Groups Additional analysis used for optimization of metho
117. ttings By activating the checkboxes Cycle for Optimizing Cycle Events and Cycle for Optimizing Cycle IntegrationEvents Peaks amp Groups you can switch the optimization on sf Ciba Gel 3 0 100 20 Deviation of Min and Max from Mean RK 1 08 00 00 2 Device SICV6F7B48 10 116 38 109 connected Ready ycicRun 113 sec 150 sec CVControl operating software Operating Manual 11 2012 A5E01428676 03 Optimization of method 5 2 Parameterization of events 5 2 Parameterization of events In the navigation area Method of the tab Device Setup the optimization parameters are included for every line in the property objects Peaks Integration Events and Cycle Events The associated parameters can be found in the columns e Rule e Shift e Relative e Weight e Peak 1 e Peak 2 All components or events to be optimized must be parameterized in these lists WA cYControl Transmitter User Interface NOT SEALED CONFIGURE E 5 xj File Tools Help Device Status Report Mean Values Results Trend Calibration Result Chromatograms Logbook Device Setup E Device Id SICVEF7BES poene Ene E General Name Shift Relative Weight Peak 1 E Method dh 101 0 ETE 0 00 0 00 1 000
118. ty damage can result if proper precautions are not taken If more than one degree of danger is present the warning notice representing the highest degree of danger will be used A notice warning of injury to persons with a safety alert symbol may also include a warning relating to property damage Qualified Personnel The product system described in this documentation may be operated only by personnel qualified for the specific task in accordance with the relevant documentation in particular its warning notices and safety instructions Qualified personnel are those who based on their training and experience are capable of identifying risks and avoiding potential hazards when working with these products systems Proper use of Siemens products Trademarks Note the following WARNING Siemens products may only be used for the applications described in the catalog and in the relevant technical documentation If products and components from other manufacturers are used these must be recommended or approved by Siemens Proper transport storage installation assembly commissioning operation and maintenance are required to ensure that the products operate safely and without any problems The permissible ambient conditions must be complied with The information in the relevant documentation must be observed All names identified by are registered trademarks of Siemens AG The remaining trademarks in this public
119. ual 11 2012 A5E01428676 03 109 Transmission of results over Modbus 10 2 Changing MODBUS parameters 110 e MbValueTypes indicates the data types which can be displayed on Modbus MbValueType Interpretation Type of access Modbus protocol type write access BIT 1 bit FALSE 1 single input BIT 1 bit TRUE 1 coil w1 16 bit integer FALSE 1 input register signed or unsigned W1 16 bit integer TRUE 1 holding register signed or unsigned W2 32 bit integer FALSE 2 input register signed or unsigned W2 32 bit integer TRUE 2 holding register signed or unsigned W2 ENRON 32 bit integer TRUE 1 holding register signed or unsigned R1 16 bit floating point FALSE 1 input register scaled EUHI not IEEE R1 16 bit floating point TRUE 1 holding register scaled EUHI not IEEE R2 32 bit IEEE floating point FALSE 2 input register R2 32 bit IEEE floating point TRUE 2 holding register R2 ENRON 32 bit IEEE floating point TRUE 1 holding register CVControl operating software Operating Manual 11 2012 A5E01428676 03 Transmission of results over Modbus 10 2 Changing MODBUS parameters 10 2 1 3 Parameterizing interfaces with Map Using Map you define which application values are to be written into which address area You make a selection for the Modbus Address Offset in the dialog box Map The following drop down menus are additionally available in the navigation area
120. ulating the gas density The backspace is a key on the PC keyboard which shifts the cursor back by one position when pressed and deletes the character present there This corresponds to the correction key function on a typewriter The calorific value formerly referred to as gross calorific value or higher heating value is a measure of the thermal energy contained in a specified amount of material The calorific value of a fuel specifies the amount of heat generated upon burning of the fuel with subsequent cooling of the combustion gases down to 25 C with release of condensation Combustion gas is a flammable gas that is mainly or frequently used as fuel The most well known combustion gas nowadays is natural gas Compression factor Density The compression factor also referred to as compressibility factor real gas factor or real factor describes the deviation of the behavior of a real gas from that of an ideal gas For ideal gases the compression factor 1 as derived from the ideal gas law However simplifications have been included in the law which only correctly describe the response of gases in limit cases at low pressures high temperatures and volumes tending toward infinity With real gases the compression factor therefore deviates from 1 See gas density CVControl operating software Operating Manual 11 2012 A5E01428676 03 131 Glossary Ethane Ethernet Firewall Gas density Ethane is a chemica
121. vice in accordance with the following section of this manual CVControl operating software Operating Manual 11 2012 A5E01428676 03 21 Installing the software 2 7 Restoring data 2 7 2 Installing the country specific settings Country specific setups are predefined device configurations which set the device appropriate to the required measurement in accordance with the gas composition and method of calculation Detector settings and pressures of the analysis module are not part of the setup and therefore remain unchanged Installing the country specific settings 1 Check that the process gas chromatograph the PC and the Windows operating system are in operation 2 Place the CD Country Specific Setups into the CD drive 3 Start the program CVControl start bar Start gt Programs gt Siemens AG gt CVControl gt CVControl 4 Select the Load Setup command in the File menu WA cvcontrol Transmitter User Interface NOT SEALED CONFIGURE File Tools Help Save Setup As N Saye Results 4s Mean Values Results Trend Calibration Result Exit 5 Select the corresponding file on the CD for the desired measurement The Readme pdf file in the root directory of the CD contains a list of available device configurations for various countries and the standardized methods of calculation The measurements and the requirements for calibration are also described in detail here Note
122. w 1 Click on one end of the bottom shift bar and make smaller by dragging with the mouse 2 Click on the reduced shift bar and shift it to the desired position on the time axis CVControl operating software 94 Operating Manual 11 2012 A5E01428676 03 Viewing and analysis of measured values 9 4 Trends Parameterizing the trend display 1 Click the Properties button in the tab Results Trend W Trend Properties x No Id_ Sample Stream Value Type Component Calorific Value Unit Min Value Max Value Min Scale Max Scale Color Nitrogen unitless 57540 546 63597 446 Calorific kg m3 1 240 1 260 CVControl operating software Operating Manual 11 2012 A5E01428676 03 95 Viewing and analysis of measured values 9 4 Trends 2 You can make the following settings in the dialog box Trend Properties Setting Procedure Define the time interval of the display e Select in the drop down list Interval One hour 12 hours One day One week two weeks Add Line Click the Add Line button Remove Line First select the line and then click on the Remove Line button Edit type of line e Click on the right in the box Sample Stream and select the sample e Inthe box Value Type select between Concentration Area Retention Time Calorific e Select the component in the box Component Calorific Value or select between Superior Calorific
123. xide CarbonDioxide v c02_4 1 00 Peaks 4 CH4_1 Standard Methane Methane v CH4_1 1 00 Groups 5 C24 Standard Ethane Ethane v C 1 00 Measured Components 6 c3_3 Standard Propane Propane v 1 00 Auxiliary Components 7 nC4_3 Standard Butane Butane 1 00 Calibration B ic4_3 Standard Isobutane Isobutane v 1 00 Hardware N 9 nC5_3 Standard Pentane Pentane v 1 00 Modbus Configuration 10 i C5_3 Standard sopentane Isopentane v 1 00 11 neo C5_3 Standard Neopentane Neopentane 1 00 12 C6_4 Additional Hexane Hexane 1 00 13 C6 _4 Standard Hexane HexaneAndHigher v 1 00 14 HelpP_C6_4 Ignored Unknown Unknown 0 00 15 HelpP_N2_4 Ignored Unknown Unknown 0 00 16 HelpP_C1_4 Ignored Unknown Unknown 0 00 Chromatograph SICVEF7BE8 Connected Alarm Hold 3 You must enter the concentrations of the calibration gas components CVControl operating software Operating Manual 11 2012 A5E01428676 03 35 Calibrating 4 2 Requirements for calibrating Entering concentrations of calibration gas components Entering units 36 1 In the window CVControl of the tab Device Setup first click on the left in the navigation area on Calibration and then on Calibration Gas WA cvcontrol User Interface NOT SEALED CONFIGURE File Tools Help Device Status Repot Mean Values Resuts Trend Calbration Resut Chromatograms Logbook Device Setup E Device Id SICV
124. y Settings Regional Setup D10BF6D8 ALARM_SETTINGS C3702262 H Method CYCLE_EVENT_TEMPLATES 9B3D600D Calibration INT_EVENT_TEMPLATES 23494132 E Hardware _PEAK_T 25086849 E Modbus GROUP_TEMPLATES 32698589 PEAK_MAP F77FABCE GROUP_MAP 0D43525 FIXED_MAP ASAATACZ ii il OPERATION_SETTINGS 19FB0941 STANDBY_SETTINGS BA4C1579 PEAK_CONC 3323A1E0 User Specific Setup 151314C0 GROUP_CONC B69B83C3 MODBUS_DEVICE_SETTINGS 9DC9FC33 MODBUS_CAPABILITIES BCI7C7CB MODBUS_MAP 12021126 af j CYCLE_EVENT_TIMES 50885654 INT_EVENT_TIMES BA ADS7C Calibration Values Setup D194D1BA PEAK_TIMES 09C87749 GROUP_TIMES 19870571 PEAK_RAF 93124376E GROUP PE BAGEDICA X Apply Undo Device SICV6F7B4C 10 116 38 104 connected Waming 0 sec 100 sec 86 CVControl operating software Operating Manual 11 2012 A5E01428676 03 Viewing and analysis of measured values 9 1 Procedure At the end of each analysis the chromatograph saves the results of all components the calorimetric values all mean values and the current chromatogram Displaying the results list Report The following example shows a gas mixture with 12 components WA cvcontrol User Interface NOT SEALED CONFIGURE sid x File Tools Help Device Status Repot Mean Values Results Trend Calibration Result Chromatograms Logbook Device Setup Stream v Injection Time 14 09 2012 10 18 41 O Revision O Alarm B Out Oi Range m Calculated Values No A

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