815 Robotic Soliprep for LC
Contents
1. 36 Dosino COMIS GHTIOI etie Sunsets 34 35 MOTUN G cesis seeriana 39 Bijiouoi ieget nee meee A 24 E Electrostatic charge veces 4 External DoSITTOTla s estre teat 48 F gi MN TEN 36 45 G GUI 6 CNA Gaeta A 28 Installing MaglC Net 8 L LIM ADOS TUO sisa 44 Luer adapter GNO RN 40 MOUNTING Mee T EE NM IE 21 Luer connector 16 50 M Mains cable COMMOCTING aiuscscu edu cadem Ds 6 Mains voltage succ oet 4 Membrane filter 36 45 Mount PONTON See tatu eu orioneu 30 RODOUG SIT caste tia eds 23 Mounting DOSING eret SCA 33 Bi gio 8y ame MP EHE MES 24 Luer adapter seo oer 21 RODOUC GUM Kaea a 20 Safety shield 32 SPACE a A tiui tous 32 Swing Head ole ete 12 Washing station 24 N yes 45 O OT SB s actuect ore orate tentent 42 43 P Peristaltic pump COMMECIING duit Gl tanc col 26 POW UPON sosistrsuteeenetutt oves atus 51 GOES xstsbadesesat dila 56 CONTOU parinn idend 54 CORBIS aae a 31 CORON ect 55 MOUNT ceceo inana 30 POSITIONING Teticle nion 40 TAS ep s UAE sea 26 R RACK dt RR TEE 36 ach DI rd ate opu 38 Back DOSITD Td eb UN o EUER 38 Robotic arm CODIGO sees 2 ces ates 9 AOUE co Atari ceta cited ede T 25 MOUNN zirien 20 Rotational speed 55 E T A E E taste 54 S Safety instructions 3 Safety shield 32 Sample Ta CK bus teen deleti2. Sample rack insert for 24xsyringe needles luer connection 9 9 9 9 e 1 Material PEEK gt 6 2067 020 Insert for 12x30 mm syringe filters for Soli prep Sample rack Sample rack insert for 12x30 mm syringe filters luer connection Material PEEK 6 2068 020 Sample rack 24x120 mL for Soliprep Sample rack for Soliprep with 24 x 120 mL PP beakers 6 1459 300 2 x 250 mL 6 1432 320 glass beakers and inserts for 30 x 11 mL 6 2743 050 24 x syringe needles luer connection as well as two inserts for 12 x 30 mm syringe filters luer connection Material PVC Outer diameter mm 480 Hole diameter mm 422 6 2134 110 Cable RS 232 DB9 socket f DB9 plug Connecting Metrohm RS 232 interface DB9 to a Custom DP40 printer For Titrinos or 756 831 KF Coulometer RS 232 extension cable 1 1 Length m 1 8 6 2151 000 Cable USB A mini DIN 8 pin Controller cable Length m 1 8 815 Robotic Soliprep for LC Qty Order no 1 6 2621 030 Length mm 1 6 2621 070 5 mm Length mm 1 6 2621 120 1 6 2621 140 815 Robotic Soliprep for LC Description Hexagon key 4 mm 79 Hexagon key 5 mm 80 Hexagon key 1 5 mm Hexagon key 2 5 mm 7 Accessories NINIS 65 7 1 Scope of delivery 2 815 4110 Qty Order no Description 1 6 2711 070 Drip pan for 789 815 855 Drip pan for 789 815 855 Robotic Sample Processors XL Material PVC 3 6 2740 020 Spray nozzle For the fin
3. Dosing unit with integrated data chip with 50 mL glass cylinder and light protection mountable on reagent bottle with ISO DIN GL45 thread FEP tubing connection anti diffusion buret tip Volume mL 50 T 240 0102 Ferrite cores Anti interference adapters V 024 4012 Countersunk head screw 6 2122 0x0 Mains cable with C13 line socket IEC 60320 C13 Cable plug according to customer requirements Switzerland Type SEV 12 6 2122 020 815 Robotic Soliprep for LC 7 Accessories 67 7 2 Optional accessories Qty 7 2 Qty Order no Description Germany Type CEE 7 VII 6 2122 040 USA Type NEMA ASA 6 2122 070 8 815 8002EN Manual 815 Robotic Soliprep for LC Optional accessories Order no Description 6 6059 201 MaglC Net 2 0 Compact CD 1 Licence Professional PC program for controlling one intelligent Compact IC system and one Professional Sample Processor or one 771 Compact Interface The software permits control data acquisition evaluation and monitoring as well as report generation for ion chromatographic analyses Graphic user interface for routine operations extensive data base programs method development configuration and manual sys tem control highly flexible user administration efficient database operations extensive data export functions individually configurable report generator control and monitoring of all system components and the chromatographic results MaglC Net C
4. Filters or injection needles should be able to be picked up with the transfer robotic arm The 6 1808 220 adapter is used for this purpose Mount it as follows 815 Robotic Soliprep for LC 21 22 2 6 Mounting the transfer robotic arm 6 1562 130 6 1808 000 6 1808 220 1 Loosen the screw and the washer of the adapter and guide the adapter into the robotic arm head from below 2 Screw the adapter tightly with the screw and the washer If needed tighten carefully with a wrench 3 Screw the tubing adapter with 2x M6 inner thread supplied with the adapter tightly onto the adapter 4 Fasten the previously mounted 6 1562 130 transfer tubing to the 6 1808 000 tubing adapter 815 Robotic Soliprep for LC 2 Installation 2 7 Mounting the Polytron robotic arm 6 1462 250 Mount the 6 1462 070 robotic arm to tower 2 as follows 1 Hold the robotic arm in such a way that the holder faces to the left and and slip it over the guide pins of the drive disc from below While doing so let the robotic arm point outwards as far as possible i e towards the tower see above i Note Take care to ensure that you do not twist the drive disc thus causing pressure against the drive 2 Screw the robotic arm to the Swing Head tightly with the screws and washers provided 815 Robotic Soliprep for LC 23 2 8 Washing station and drip pan TTT TTT ETE EET 2 8 Washing station and drip pan To mount the washin
5. 5 Equip the connection cable of the Dosino with an anti interference adapter made of ferrite T2400 102 see drawing Connect the connection cable to the MSB connector 1 MSB 1 on the rear of the Sample Processor 815 Robotic Soliprep for LC 2 Installation MSB 1 i Made by Metrohm Herisau Switzerland T 2400 102 Preparing the Dosino 2 for diluting Install the Dosino 2 in the same way as Dosino 1 Use the 50 mL dosing unit Fill the clear glass bottle with a suitable dilution medium e g water 1 Screw an adsorber tube filled with cotton to the Vent connector on the 50 mL dosing unit 2 Equip the dosing unit with a filling tubing Port 2 on the underside of the dosing unit and screw it onto a 6 1808 070 clear glass bottle with GL 45 thread The bottle should be filled with the dilution medium e g water 3 Connect the inlet tubing on the Polytron robotic arm tower 2 with the end that is still free to port 3 on the dosing unit 4 Place the Dosino dosing drive on the dosing unit 5 Equip the connection cable of the Dosino with an anti interference adapter made of ferrite T2400 102 and connect it to the MSB con nector 2 MSB 2 on the rear of the Sample Processor 815 Robotic Soliprep for LC 35 2 17 Equipping the rack TTT TTT EET EEE ETL 2 17 Equipping the rack In addition to sample vessels the sample rack can also be equipped with various so called Inserts which can act as receptacles for various
6. Number of positions 105 Rack parameters Lift positions Special beakers Beaker radius samples mm Beaker sensor Rack offset cy 4 Select the tab Special beaker 815 Robotic Soliprep for LC 3 Defining rack positions Special beaker on the sample rack 6 2068 020 x Number of positions Rack parameters Lift positions Special beakers Special beaker Rack position Work position Tower 1 Work position Tower 2 mm e e 2 3 4 5 6 D B8 a oO oO oF oO A oO oO AJA oo oOo oOo 8 oO oO oF oO A AAAA oo oOo oO 8 1 Select the 1st line Special beaker 1 and click on Edit x R ack position a03q Work position Tower 1 mm Work position Tower 2 mm Beaker radius mm Beaker sensor OK Cancel 2 Under Rack position select 103 UJ Close the dialog window with OK A Assign the rack position 104 to Special beaker 2 as described above Ul The last position of the sample rack is conceived as Adjusting posi tion Assign rack position 105 to Special beaker 16 6 Close the rack data table with OK 815 Robotic Soliprep for LC 39 4 Adjusting rack and robotic arm The Luer adapter must be positioned precisely on the robotic arm for picking up membrane filters or syringe needles In order to ensure this it is necessary to align the sample rack and the robotic arm precisely in relation to one another The control software MagIC Net allows the user to enter a so called offse
7. The 815 Robotic Soliprep for LC may not be operated without a safety shield Install it as follows 1 Mounting the spacer for the safety shield with the screws supplied to tower 1 according to the following figure 2 Unscrew the black nuts on both sides of tower 1 3 Pullthe green 6 2751 150 safety shield over tower 1 starting from the top 32 815 Robotic Soliprep for LC BEEHEEENEENHENHENHENHENHEEHEEN 2 Installation 4 Screw the safety shield tightly with the two nuts as shown in the fol lowing illustration 5 Adjust the safety shield on the spacer see the following figure 2 16 Installing the Dosino For the transferring and diluting of the sample two Dosinos with a 10 mL and a 50 mL dosing unit is used They are being installed as follows 815 Robotic Soliprep for LC BEEBEEEB 33 2 16 Installing the Dosino Preparing the Dosino 1 for sample transfer n B 3 W1 2 1 Screw an adsorber tube filled with cotton to the Vent connector on the 10 mL dosing unit 2 Equip the dosing unit with a filling tubing Port 2 on the underside of the dosing unit and screw it onto a 6 1808 070 clear glass bottle 2 L with GL 45 thread The bottle should be filled with the solvent water or an organic solvent which is also used for sample dispersion 3 Connect the transfer tubing to tower 1 with the end that is still free to Port 1 on the dosing unit 4 Place the Dosino dosing drive on the dosing unit
8. button down until the lift 1 has moved approx 180 mm downwards Lift position mm Start EA Robotic arm position 0 0 s Start The two lifts are now in a favorable position permitting easy access to all of the screws for mounting the Swing Heads 13 14 2 4 Mounting the Swing Heads Removing the titration head holders 1 Release both the outside and the inside holder screws on tower 2 left 2 Loosenand remove the holder from the holder plate of the guide chain 3 Remove the holder from tower 1 as well Use the hexagon key provided The screws will be needed again later 815 Robotic Soliprep for LC 815 Robotic Soliprep for LC 2 Installation Mounting the Swing Heads Screw the Swing Head without reinforcement tightly to the holder plate of the guide chain on tower 2 with two V 024 4012 countersunk screws Clamp the Swing Head between the guide jaws and screw it tightly Screw the second Swing Head with reinforcement tightly to the holder plate of the guide chain on tower 1 with two V 024 4012 countersunk screws Clamp the Swing Head between the guide jaws and screw tight the two screws on the left hand side 6 2058 040 15 2 5 Mounting the deflector Luer connector and collection container 5 Fasten the 6 2058 040 robotic arm reinforcement to the right hand side while at the same time fixing the Swing Head in place Use for this purpose the two screws
9. distin 36 AAEN rrna uf ates 8 Sample tubes 36 SONCE PME UN 3 SEED sicnt iscstonda tutus boues 32 Special beakers 39 46 Swing Head CONTOUR Fe RR 9 COMMCGUING ses cette am cme ts 6 Mounting 2 codes tot Reet et 12 Syringe needle 45 TRANSFER command 55 W Washing station cesses 24 52 WINTON NNNM aa eee ane te 9 WOrking NeoN Suse a eee 44 Work POSION dona besote teta ext 44 815 Robotic Soliprep for LC
10. tip for the additiona of solvent or titrant and three spray nozzles for cleaning The swing arm allows the usage of the Polytron for sample preparation on multi row racks Material PP black Material 2 Metal 815 Robotic Soliprep for LC Qty Order no Description 1 6 1546 030 Extractor rod For PTFE piston of dosing unit 1 6 1562 130 Transfer Tubing with holder 2 x M6 10 mL to Sample Processors Transfer tubing for dilution and preconcentration using a Dosino and Advanced IC Sample Processor Material FEP Inner diameter mm 2 Length m 5 Volume mL 10 2 6 1608 070 Eluent bottle 2 L GL 45 Material Clear glass Height mm 262 Volume mL 2000 3 6 1621 000 Container 10 L As rinsing or waste container in automated systems Material PE Width mm 265 Height mm 400 Volume mL 10000 815 Robotic Soliprep for LC 7 Accessories 59 7 1 Scope of delivery 2 815 4110 Qty Order no Description 1 6 1625 010 Collection container for Soliprep Container for safe collection of used tools in automated systems Material PP 2 6 1801 120 PVC tubing 4 mm 6 mm 2m Material PVC transparent Outer diameter mm 6 Inner diameter mm 4 Length m 2 1 6 1803 030 PTFE capillary 0 5 mm i d 3 m Capillary for inline dialysis for Dialysis Unit IC Dialysis Sample Pro cessor IC Liquid Handling Dialysis Unit Material PTFE Outer diameter inches 1 16 Inner diameter mm 0 5 Le
11. utensils 6 2067 000 6 2067 010 6 2067 020 E ae The inserts illustrated above are 6 2067 000 Insert for 6 2743 050 sample tubes 11 mL 6 2067 010 Insert for injection needles with Luer connector maximum length 50 mm 6 2067 020 Insert for disposable membrane filters with Luer connector maximum diameter 30 mm This insert has a positioning reticle for adjusting the rack and the robotic arm Each insert is provided with a recess that prevents it from being inserted with the incorrect alignment Two positions on the sample rack are reserved for rinsing and waste beakers 6 2037 070 36 saessenn 815 Robotic Soliprep for LC 815 Robotic Soliprep for LC 2 Installation The lid with the hole belongs on the waste beaker position 103 into which a preliminary filtrate of the sample solution is to be disposed of when mem brane filters are used The filter can be placed on the hole in the lid with the robotic arm and pressure can be applied to force the sample solution through the filter The sample beaker can be defined as a special beaker for the purpose of dabbing off the Polytron aggregate if required 37 38 3 Defining rack positions 1 In MaglC Net select Configuration 2 Double click on the device name 815 Robotic USB 3 Switch over to the tab Rack and click on Rack data to open the rack parameter settings Rack data Rack name 6 2068 020 Rack code O010011
12. 5 Robotic Soliprep for LC 1 Introduction Caution This symbol draws attention to a possible damage of instruments or instrument parts Note This symbol marks additional information and tips 1 4 Safety instructions 1 4 1 General notes on safety N Warning This instrument may only be operated in accordance with the specifica tions in this documentation This instrument has left the factory in a flawless state in terms of technical safety To maintain this state and ensure non hazardous operation of the instrument the following instructions must be observed carefully 1 4 2 Electrical safety The electrical safety when working with the instrument is ensured as part of the international standard IEC 61010 N Warning Only personnel qualified by Metrohm are authorized to carry out service work on electronic components A Warning Never open the housing of the instrument The instrument could be dam aged by this There is also a risk of serious injury if live components are touched There are no parts inside the housing which can be serviced or replaced by the user 815 Robotic Soliprep for LC 3 1 4 Safety instructions Mains voltage A Warning An incorrect mains voltage can damage the instrument Only operate this instrument with a mains voltage specified for it see rear panel of the instrument Protection against electrostatic charges A Warning Electronic components are se
13. 815 Robotic Soliprep for LC 2 815 4110 Manual 8 815 8002EN LL Metrohm 2 Metrohm Metrohm AG CH 9101 Herisau Switzerland Phone 41 71 353 85 85 Fax 41 71 353 89 01 info metrohm com www metrohm com 815 Robotic Soliprep for LC 2 815 4110 Manual 8 815 8002EN 02 2010 dm Teachware Metrohm AG CH 9101 Herisau teachwaregmetrohm com This documentation is protected by copyright All rights reserved Although all the information given in this documentation has been checked with great care errors cannot be entirely excluded Should you notice any mistakes please send us your comments using the address given above Table of contents Table of contents 1 Introduction 1 1 1 Instrument description ssseessseeeeee 1 t2 Intended use oie io tal E academies 2 1 3 About the documentation sssseeuseesuesssee 2 ds SW MOS drig one Pit Saison mda a eese NP ta RR E cad 2 1 4 Safety instructions sseesssssss 3 1 4 1 Generali Notes on sal ely e secco niai an eeN EE doe sio ondes 3 TAZ SEIGEMed Salou aar ai ivt E a E bct aes 3 kA E i o unus Miesen n a O O 4 1 5 Recycling and disposal ssseseseseseeessssee 5 2 Installation 6 2 1 Preparing the Sample Processor sssssssssee 6 2 2 Installing MaglC Net uuuttt uU tuse 8 2 3 Configuring the Swing Heads se
14. LC anmmumum 17 2 5 Mounting the deflector Luer connector and collection container TTT TT TTT TTT TTT 3 Fasten the 6 2057 150 holder for the collection container and the sta bilizing square of the 6 2843 000 Luer connector together to the fastening plate of the tower see figure 6 2057 150 6 2843 000 4 Fix the holder of the Luer connector with both knurled screws supplied to the stabilizing square 5 Guide the 6 1625 010 collection container with opened cover into the holder 18 nunnunuunun 815 Robotic Soliprep for LC EEHEEENHENHENHEEHENHEENHEEEN 2 Installation 6 1625 010 6 Connect a PTFE capillary with the aid of a 6 2744 014 pressure screw from below to the Luer connector Connect the PTFE capillary to the injection valve of the ion chromatograph Select a capillary which is as short as possible 7 Reattach the sample rack onto the instrument 815 Robotic Soliprep for LC mummumum 19 2 6 Mounting the transfer robotic arm 2 6 Mounting the transfer robotic arm Prepare the Swing Head After initialization the drive disc of the Swing Head is positioned as though the robotic arm were located in the outermost position In order to be able to mount the robotic arm in a favorable position rotate the drive disc with Manual control in MaglIC Net as follows 1 Open the manual control In the symbol bar of MagIC Net click the hand symbol 2 Under Device selection first select All devices and then
15. MagIC Net 2 0 Configuration File View Tools Help ea Mee C IN 7 Deene D a Amanla mf amp 1 E Mew Workplace Delete Properties Z Column display N Print PDF Initialize s Database Ignored devices The Sample Processor is initialized The settings of the Swing Heads and robotic arms are now valid 2 4 Mounting the Swing Heads Preparing the towers Both lifts must be moved into an appropriate position in order to ensure that the mounting of the Swing Heads and the robotic arms can be carried out without problem 1 Opening the manual control In the symbol bar of MagIC Net click the hand symbol 815 Robotic Soliprep for LC 815 Robotic Soliprep for LC 2 Installation 2 Under Device selection first select All devices and then the 815 Robotic USB Click the tab Tower 1 Manual control All devices 815 Robotic USB Sample Processor XL2 nml xl levices WOT Tower 1 Rack Peripherals tower 1 Peripherals tower 2 Input Rack position Start Lift position mm Start Robotic arm position 5 5 2 Start gt Configure rack Moving the lift into position Under Rack position click on Start Current Value Input The sample rack moves to a defined position Now the lift can be moved Under Lift position click on the arrow
16. alled tubing of the robotic arm is used to add solvent to the sample Connect a 6 1805 120 to it and connect the other end of the tubing to to the port 1 of the Dosino with a 50 mL dosing unit 2 14 Connecting the Polytron The Polytron PT 1300 D is comprised of a control module and a disper sion drive with a dispersion aggregate for mixing and shredding solid samples The control device is directed by a PC software e g tiamo via a serial RS232 connector Consult the Polytron user manual for details about setting up the connec tions The Polytron is connected as follows 1 Connect the connection cable of the dispersion drive to the front side of the control module 2 Check the mains voltage setting on the connection socket on the rear side of the control module Switch the device off Plug in the mains cable and connect with a socket 3 Connect the 6 2134 040 RS232 connection cable to the 9 pin con nection socket on the rear side of the control module Plug in the other 815 Robotic Soliprep for LC 31 2 15 Mounting the safety shield end of the cable to the COM1 or COM2 port on the PC The port on the PC is usually marked with IOIOIL If the PC has no serial interface then a USB port on the PC can be used with the aid of an RS232 USB converter e g the 2 145 0320 Edgeport i Note The Polytron must be registered manually in tiamo as an RS232 device 2 15 Mounting the safety shield Safety shield 6 2751 150
17. an additional correction must be made and the rack offset needs to be corrected 42 815 Robotic Soliprep for LC 4 Adjusting rack and robotic arm Correcting the rack offset If there is a deviation on the R Line proceed as follows 1 In MaglC Net select Configuration 2 Double click on the device name 815 Robotic USB 3 Switch over to the Rack tab and open the rack parameter settings with a click on Rack data Number of positions Rack parameters Lift positions Special beakers Beaker radius samples orf rm Beaker sensor off Rack offset ey 4 Correct the value for Rack offset according to the observed deviation from the positioning reticle One tick mark corresponds to approxi mately 0 5 5 Close the rack data configuration and the Sample Processor properties dialog each with OK 6 In manual control select the same rack position again and lower the lift down to the positioning reticle Now the adapter tip should point to the middle of the positioning reti Cle If this is not the case then an additional correction must be made 815 Robotic Soliprep for LC 43 5 1 Lift position for sample beakers 5 Setting lift positions Various lift positions must be defined before process methods are created for the Soliprep The simplest way to accomplish this is by having the individual positions established in MaglC Net with the aid of the Manual control The established position can
18. d tubings and cables into the guide chain 3 Close the guide chain Close the clip for each chain link again by hand and apply forceful pressure to snap them into place Caution Take care to ensure that any cables and tubings that are fixed in the guide chain are not able to hinder the free movement of the lift or of the robotic arm This could lead to damage to the affected drive The clip of one chain link can be removed entirely if required by releasing it on both sides 815 Robotic Soliprep for LC 29 2 12 Assembling and mounting the Polytron drive 2 12 Assembling and mounting the Polytron drive Please consult the Polytron user manual for details how to mount the aggre gate to the Polytron PT 1300 D Mounting the Polytron Mount the Polytron as follows 1 Insert the Polytron with the aggregate already mounted into the robotic arm holder on tower 2 from above 2 Readjust the position of the holder if necessary Press down the fixing lever of the holder to accomplish this 2 13 Mounting the rinsing tubings for the Polytron For rinsing the Polytron aggregate rinsing nozzles must be mounted on the robotic arm Proceed as follows 30 815 Robotic Soliprep for LC 2 Installation 6 1805 120 1 Replace the three stoppers on the Polytron robotic arm with 6 2740 020 rinsing nozzles 2 Connect the three rinsing tubings that are connected to the tower 2 distributor to the rinsing nozzles 3 The preinst
19. dow of the connection test you can check the data transfer to the Polytron by sending a command to the device A list of possible commands can be found below see page 56 7 Close the window with OK and then quit the configuration dialog with OK Control The Polytron can be switched off and on with the communications com mand TRANSFER In addition the rotational speed of the aggregate can also be set in revolutions per minute This can be accomplished when the Polytron is in either switched on or switched off status The control commands for the Polytron are comprised of a three digit numerical code A TRANSFER command for switching on the device could look as follows 815 Robotic Soliprep for LC 55 56 Switch on Polytron Write 254 x Name Command LINER C max waiting time 1 OK Cancel Comment OK Cancel Table 1 Command list of the Polytron 1300 D Command sening Command seting 254 13000 r min 293 14000 r min 00 7000rmin 080 15000 r min 007 22000 r min oos 25000 rimi 200 2 000 r min 050 220 29000 r min 00 230 30000 rimi 815 Robotic Soliprep for LC 7 Accessories 7 Accessories d Note Subject to change without notice 7 1 Scope of delivery 2 815 4110 Qty Order no Description 1 2 136 0100 Polytron PT 1300 D Metrohm version Homogenizer with digital display Included are d
20. e If you wish to pull out the plug you will first need to pull back the outer plug sleeve marked with arrows Attaching the sample rack 1 Attach the sample rack in such a way that the two openings in the bottom of the rack engage with the guide bolts on the turntable 2 lightly screw in the handle of the sample rack 2 2 Installing MaglC Net Installing MagIC Net Intelligent lon Chromatography for Professionals IVE TH 1 Insert the MagIC Net CD into the CD drive of the PC and carry out the installation following the instructions After this start MagIC Net 8 815 Robotic Soliprep for LC 2 Installation 2 3 Configuring the Swing Heads Connecting the controller cable to the PC 1 Connect the controller cable to a USB port on the computer For Windows 2000 the instrument is recognized and the driver is installed automatically For Windows XP the instrument is recognized and the installation assistant for the driver is started automatically Select the option Install software automatically and click on Next Exit the assistant with Finish For Windows Vista the instrument is recognized and the installation assistant for the driver is started automatically Select the option Find and install driver software Agree to all of the requests that fo
21. e software permits control data acquisition evaluation and monitoring as well as report generation for ion chromatographic analyses Graphic user interface for routine operations extensive database programs method development configuration and manual system control highly flexible user administration efficient database operations extensive data export functions individually configurable report gen erator control and monitoring of all system components and the chromatographic results MaglC Net Multi complies with FDA regu lation 21 CFR Part 11 as well as GLP Dialogue languages German English French Spanish Chinese Korean Japanese and more Client Server version with 3 licences 6 9012 000 Dispersing aggregate for Polytron Length mm 115 6 9012 010 Dispersing aggregate for Polytron Length mm 157 815 Robotic Soliprep for LC 7 Accessories 69 70 Index Index A Ad Us UNO scs saa sear taint Maa qs 40 Adjusting position 40 C Collection Container 16 Configuration RODOUC ELTE e opto nie deis 9 SWING Head sucssascireurdndiusis 9 Connect POYON stasera usate 31 Connecting Controller cable 7 JOSIl10 n cos ole oeste beate 34 35 Mains cable o n 6 Peristaltic pump 26 Swing Head 6 Controller cable COMMECUING uis seht ite 7 D Deflector sssssss 16 48 Disposable filter
22. e spraying of the rinsing solution Material ETFE Outer diameter mm 10 Length mm 47 1 6 2743 057 Sample tubes 11 mL 200 pieces For IC Sample Processors and VA Autosampler Material EP Outer diameter mm 16 Length mm 108 Volume mL 11 1 6 2744 014 Pressure screw 2x With UNF 10 32 connection For the connection of PEEK capillaries Material PEEK Length mm 26 66 i gt 815 Robotic Soliprep for LC Qty Order no Description 6 2751 150 Splash protection for Robotic Soliprep Splash protection for the Robotic Soliprep systems Filtration and Flex ible these pick up and drop on tower 1 different tools such as syringe needles The protection also prevents possible injury by the pivoting arm as well as contact with any accidentally escaping solutions Material Plexiglas PMMA 6 2841 000 External Polytron washing station for Robotic Sample Processors The external washing station can be mounted on the side of the Robotic Sample Processor tower and allows the external cleaning of the Polytron while other actions can be carried out on the sample rack Material PP Material 2 PVC 6 2843 000 Luer connector with holder for Soliprep 6 3032 210 Dosing Unit 10 mL Dosing unit with integrated data chip with 10 mL glass cylinder and light protection mountable on reagent bottle with ISO DIN GL45 thread FEP tubing connection anti diffusion buret tip Volume mL 10 6 3032 250 Dosing Unit 50 mL
23. eeeeessssesee 9 2 4 Mounting the Swing Heads sssseeueuesesssee 12 2 5 Mounting the deflector Luer connector and collection CONTAINER oria p ouch Ane vas vto edi De ope benc dadan 16 2 6 Mounting the transfer robotic arm 20 2 7 Mounting the Polytron robotic arm 23 2 8 Washing station and drip pan sssssseusss 24 2 9 Connecting and setting up the peristaltic pump 26 2 10 Setting up the rinsing tubings c eee 28 2 11 Opening guide chain 0 cccccecceccc ce eeeeeeeeeeeeeeeeeeeaes 28 2 12 Assembling and mounting the Polytron drive 30 2 13 Mounting the rinsing tubings for the Polytron 30 2 14 Connecting the Polytron 2 31 2 15 Mounting the safety shield uueueuueueuuueussss 32 2 16 Installing the Dosino sseseesessseesssessee 33 2 17 Equipping the rack oed be i ette oti Ces tie 36 3 Defining rack positions 38 4 Adjusting rack and robotic arm 40 815 Robotic Soliprep for LC Table of contents 5 Setting lift positions 5 1 5 2 5 3 5 4 5 5 5 6 5 7 6 Controlling the Polytron 7 Accessories Index 7 1 7 2 44 Lift position for sample beakers 44 Lift position for picking up needles and filters 45 Lift positions fo
24. entry New in the pull down menu and then in the device selection under Miscellaneous set up a new RS232 device 4 Enter a device name and the device serial number of the Polytron under General Properties RS 232 device RS 232 device 1 x General RS 232 GLP COM Port COMI Baud rate Data bit Parity None Stop bit Handshake None Timeout p Terminator For send OD 04 RS 232 Device Terminator For receive OD 04 Code page ASCII il Send characters one by one 3 in Delay time Connect OK Cancel 5 Enter the following settings in the dialog window RS 232 COM Port COMI or the interface on the PC at which you have connected the Polytron Baud rate 2400 Data bit 8 Parity None Stop bit 1 815 Robotic Soliprep for LC Handshake None Timeout 2000 ms Terminator for send OD OA CR LF 6 Controlling the Polytron Terminator for receive OD OA CR LF Code page ASCII Properties RS 232 device RS 232 device 1 x General RS 232 GLP COM Port Baud rate Data bit Parity Stop bit Handshake Timeout 1 Terminator For send RS 232 Device Terminator For receive Code page COMI None None 2400 al i 7 2000 ms 10D10A 1ODADA ASCII Send characters one by one Delay time Connect OK Cancel 6 Click on Check connection In the dialog win
25. g station and the drip pan remove the sample rack Now proceed as follows 1 Mount the washing station to the left next to tower 2 on the assembly rail and screw it tightly 2 Fasten the enclosed tubing to the drainage nipple on the drip pan and guide the free end of the tubing into a drain or a waste container 3 Place the drip pan over the stirrer rail The correct alignment of the drip pan can be seen from the following illustration Correct the position of the washing station slightly as needed 4 Reattach the sample rack 24 nunnunun 815 Robotic Soliprep for LC 2 Installation 5 Fasten the 6 1820 020 screw connector with the M6 connector to the upper larger tubing connector of the washing station 6 Connect the green 6 1805 120 FEP tubing 1 m length to the screw connector This is the feed line of the washing station Connect the other end of the tubing to the distributor of tower 2 see Rinsing tub ings at tower 2 page 26 7 Fasten a 6 1812 000 PTFE tubing to the lower tubing connector of the washing station This is the outlet of the washing station Shorten the tubing to a suitable length so that it can be connected to a peristaltic pump 772 Pump Unit Remove the union nut of lower tubing connector and guide it over the end of a 6 1812 000 PTFE tubing You may have to extend the tubing end in order to be able to better mount the tubing see the following note Pull the end of the
26. hing station 6 Click on the associated Assign button 7 Click on Close 5 7 Lift position for the washing station External position 1 These settings apply to tower 2 1 Move the lift upward until the Polytron is at a suitable height for swing ing to the washing station Click on the arrow button Arrow down and also if required Arrow up under lift position in order to set a suitable position 2 Under Robotic arm position click on the button Arrow left until the robotic arm stops 3 Click on Configure rack 4 Under Robotic arm position select External position 1 5 Click on the associated Assign button 6 Click on Close Work position 1 Under Robotic arm position select External 1 and click on Start 2 Move the lift downwards button Arrow down until the Polytron is at the right height for rinsing If the Polytron does not fit in the middle of the washing station then the latter can be shifted laterally 3 Click on Configure rack 4 Under Lift position select the Work position for External 1 815 Robotic Soliprep for LC 815 Robotic Soliprep for LC 5 Click on the associated Assign button 6 Click on Close 5 Setting lift positions 53 54 6 Controlling the Polytron Configuration Once the Polytron has been set up it can be configured in MagIC Net Configuring the Polytron 1 Click the Configuration icon 2 Click on Edit in the Devices window 3 Select the
27. ight until both components fit to one another in the middle 5 Click on Configure rack 6 Under Robotic arm position select External position 3 7 Click on the associated Assign button 8 Click on Close 815 Robotic Soliprep for LC 5 Setting lift positions Work position 1 Move the lift upwards by several mm 2 Fasten a membrane filter to the Luer adapter of the robotic arm 3 Under Lift position actuate the arrow key Arrow down several times until the membrane filter is tightly placed on the Luer connector 4 Click on Configure rack 5 Under Lift position select the Work position for External 3 6 Click on the associated Assign button 7 Click on Close 8 Move the lift to the Shift position and remove the membrane filter from the Luer adapter 5 6 Lift position for the Polytron 815 Robotic Soliprep for LC Working height 1 Under Device selection gt All devices click on 815 Robotic USB and then select the tab Tower 2 2 Move to sample position 1 Under Rack position enter Target posi tion 1 and click Start 3 Move the lift downward until the Polytron is at a suitable height for sample dispersion Click on the arrow button Arrow down and also if required Arrow up under lift position in order to set a suitable position 4 Click on Configure rack 5 Under Lift position select Work position for tower if this is not yet selected 51 52 5 7 Lift position for the was
28. le from the Luer adapter 5 2 Lift position for picking up needles and filters 815 Robotic Soliprep for LC Picking up the needle Move to a rack position 25 Under Rack position enter Target posi tion 25 and click Start Place a plastic needle in the position established in the insert Move the lift downwards until the Luer adapter engages the needle and it is fixed in place Under Lift position click on the arrow button Arrow down in order to set a suitable position The needle must rest up close against the adapter The lift may not however be lowered too far because otherwise the lift drive could become overloaded and suffer damage Note the current lift position in mm This lift height must be entered in the method as absolute lift position 45 46 5 3 Lift positions for special beakers 5 Move the lift upward and remove the needle Picking up the filter 1 Move to rack position 49 Under Rack position enter Target posi tion 49 and click Start 2 Place a membrane filter on the established position in the insert 3 Move the lift downward until the Luer adapter engages the filter and it is fixed in place Under Lift position click on the arrow button Arrow down in order to set a suitable position The filter must rest up close against the adapter The lift may not how ever be lowered too far because otherwise the lift drive could become overloaded and suffer damage 4 Note the current lift positio
29. llow The installation assistant will be exited automatically Instrument registration The USB Sample Processor is automatically recognized by MagIC Net 815 Robotic Soliprep for LC 2 3 Configuring the Swing Heads Save device 009 108 The new device 815 Robotic USB Sample Processor xL with serial number 00108 has been detected Should iE be saved in Ehe device table 1 Confirm with Yes The properties window for configuring the instrument is displayed Properties 815 Robotic USB Sample Processor XL 815 Robotic USB Sample Processor XL 1 Program version 581500204 sid Update Device serial number onos OOOO O Set to work 2009 05 20 10 58 57 UTC 2 Remarks 2 Confirm with OK Configuring Swing Heads Now configure the robotic arms for both towers 1 Click the Configuration icon MaglIC Net 2 0 Configuration File View Tools Help BS G D t me gt Accessory name A Set to work Expiry date Next GLP test 10 815 Robotic Soliprep for LC EEHHEEEENHEHEHEEHENHENHEEEEN 2 Installation 2 Double click on the instrument name 815 Robotic USB in the Devices window 3 First click on the Tower 1 tab and then on Configuration Properties 815 Robotic USB Sample Processor XL 815 Robotic USB Sample Processor XL 1 x 1 General Tower 1 Tower parameters BIEL EL EL EL EL EL ELE LE T L Max s
30. ly those manufactured by Metrohm Operation by the high performance tiamo or Magic Net software ensures not only user friendly operation and programming of automation sequences but also allows 10096 conformity for the entire automation system with FDA Federal Drug Administration regulations This applies in particular with regard to the regulation 27 CFR Part 11 electronic records and signa tures 815 Robotic Soliprep for Liquid Chromatography Dispersion filtration dilution and sample transfer The universal automation system for sample preparation in instrumental chromatography A workstation equipped with a dispersion device is used to shred the sample The dispersion aggregate is cleaned in a special rinsing station The second workstation is equipped for sample transfer with a uni versal robotic arm with a Luer adapter It is used for picking up syringe needles for aspirating the dispersed sample and bottling the filtrate in sealed vials and membrane filters for filtering and injecting the sample in a capil lary Needles filters are charged in replaceable inserts The needles and filters are automatically stripped off after use and disposed of in a waste container Two versatile dosing drives 800 Dosino are used as an auxiliary device for diluting the sample and for transferring the sample solution 1 2 Intended use 1 2 Intended use The 815 Robotic Soliprep for LC is designed for the automatic analysis of larger
31. m with the Luer adapter is located precisely above the positioning reticle The positioning reticle CD gt a u ua g The positioning reticle shows the directions of movement for the rack R and the Swing Head S The scale lines stand for approximately 0 5 rotation angle or swing angle deviation Determine the deviation of the adapter tip from the middle of the positioning reticle You can make the corresponding corrections in the MagIC Net configuration afterwards 815 Robotic Soliprep for LC 41 Correcting the swing offset If there is a deviation on the S line then proceed as follows 1 In MaglC Net select Configuration 2 Double click on the device name 815 Robotic USB 3 Switch over to the Tower 1 tab and open the robotic arm settings with a click on Configuration Confirm the safety prompt with Yes x Swing offset 2 Max swing bsc E Swing radius mm Rotation offset 2 Swing direction Ok Cancel 4 Correct the value for the Swing offset according to the observed deviation from the positioning reticle One tick mark corresponds to approximately 0 5 5 Close the robotic arm configuration and the Sample Processor prop erties dialog each with OK 6 In the manual control select the same rack position again and lower the lift down to the positioning reticle Now the adapter tip should point to the middle of the positioning reti Cle If this is not the case then
32. mple beaker The lid with hole is used in the Soliprep system to pre rinse applied syringe filters into the special beaker Material PP 62 815 Robotic Soliprep for LC Qty Order no Description 6 2053 000 Cable clip Cable clip for fastening cables and tubes 6 2057 150 Holder for collection container Holder for mounting collection container Material Aluminum 6 2058 040 Swing arm enhancement for Swing Head 786 The swing arm enhancement is for stabilizing the swing arm connected to the 786 Swing Head and working with various tools Material Aluminum 6 2058 050 Fastening plate for deflector and holder for collection container The fastening plate is mounted at the side of the Sample Processor tower and allows the mounting of a deflector for the automatic pulling off the used tools Material Aluminum 6 2058 060 Deflector for adapter 61808220 The deflector is mounted with the fastening plate 6 2058 050 at the side of the Sample Processor tower and allows the automatic pulling off the used luer tools into the collection container 6 1625 010 Material Aluminum 815 Robotic Soliprep for LC 7 Accessories 63 7 1 Scope of delivery 2 815 4110 Qty 64 Order no Description 6 2067 000 Insert for 30x11mL for Soliprep sample rack s Sample rack insert for 30x11mL 6 2743 050 J e Material PVC e a WC ur 6 2067 010 Insert for 24xSyringe needles for Soliprep sample rack DET rn b 275925
33. n in mm This lift height must be entered in the method as absolute lift position 5 Move the lift upward and remove the filter 5 3 Lift positions for special beakers Special beaker 1 1 Move to special beaker position 1 Under Rack position enter Target position 103 and click Start 2 Place a sample beaker on the established position Lay the cover with the hole on the sample beaker 3 Fasten a membrane filter on the Luer adapter of the transfer robotic arm 4 Move the lift downward until the filter rests against the cover of the sample beaker Under Lift position click on the arrow button Arrow down in order to set a suitable position 5 Click on Configure rack 815 Robotic Soliprep for LC 5 Setting lift positions 6 Under Lift position select the Work position for Special beaker 1 Work position For Special beaker il FA n Tower iA Rinse position Far Special beaker 1 OO Shift position For Special beaker 2 7 Click on the associated Assign button 8 Click on Close 9 Move the lift upward and remove the membrane filter Special beaker 2 1 Moveto special beaker position 2 Under Rack position enter Target position 104 and click Start 2 Place a sample beaker on the established position 3 Move the lift downward until the Luer adapter arrives at a suitable position for rinsing the transfer tubing Click on the arrow button Arrow down and also if required Arrow up under lift p
34. n Far Special beaker 15 Special beaker 16 External 1 O Swing position Extertal i External 3 External 4 2 Rinse position For Special position For 11 Click on the associated Assign button 12 Click on Close External position 2 1 Under Robotic arm position actuate the button Arrow right until the Luer adapter is standing to the right It should now be located in the of the deflector opening Move the lift upward arrow button Arrow up until the needle or the filter is stripped off and falls into the collection container Do not move the lift too far upward Under Robotic arm position select External position 2 Click on Configure rack Under Lift position select the Work position for External 2 Click on the associated Assign button Click on Close Move the lift to the Shift position 49 5 5 Lift position for the Luer connector 9 Under Robotic arm position as Target position select External 1 and click on Start 5 5 Lift position for the Luer connector External position 3 1 Under Device selection gt All devices click on 815 Robotic USB and then select the tab Tower 1 2 UnderRobotic arm position actuate the button Arrow right until the Luer adapter is located above the Luer connector 3 Move the lift downwards until the Luer adapter is located approx 1 mm above the Luer connector 4 Under Robotic arm position actuate the arrow buttons Arrow left and Arrow r
35. ngth m 3 3 6 1805 060 FEP tubing M6 60 cm With light and kink protection Material FEP Inner diameter mm 2 Length mm 600 60 815 Robotic Soliprep for LC Qty Order no Description 2 6 1805 120 FEP tubing M6 100 cm With light and kink protection Material FEP Inner diameter mm 2 Length mm 1000 1 6 1808 220 Luer adapter for transfer head Adapter with outside thread M6 and luer connection for 6 1462 240 Transfer head for using luer tools on multi row racks Material PEEK 1 6 1808 260 Distributor for pump tubings for Sample Pro cessors 2 6 1812 000 PTFE tubing 4 6 mm 4m Material PTFE Outer diameter mm 6 Inner diameter mm 4 1 6 1820 020 Screw connector M6 Connection piece with M10 thread for 6 1812 XXX tubing and M6 thread for 6 1805 XXX tubing Material PVDF 815 Robotic Soliprep for LC 7 Accessories 61 7 1 Scope of delivery 2 815 4110 Qty Order no Description 2 6 1820 050 Screw connector For 6 1826 100 pump tubing for peristaltic pumps 1 6 1826 100 PP pump tubing 6 4 mm 1 m Replacement tubing for the pump tubing in the 772 Pump Unit Material PP Outer diameter mm 9 6 Inner diameter mm 6 4 Length m 1 3 6 1828 000 PVDF connection nipple For 6 1621 000 container Material PVDF 2 6 1829 020 FEP aspiration tube M6 0 5 m For Dosing Unit Material FEP Inner diameter mm 2 Length mm 500 1 6 2037 070 Lid with hole for 250 mL sa
36. nsitive to electrostatic charges and can be destroyed by discharges Always pull the mains cable out of the mains connection socket before connecting or disconnecting electrical appliances on the rear panel of the instrument 1 4 3 Personnel safety N Warning Personnel are not permitted to reach into the working area of a Sample Processor while operations are running A considerable risk of injury exists for users who undertake manual interventions to the automatic running of the instrument The various drives of a sample processor including Swing Head exhibit considerable force in order to be able to operated without difficulty even with greater loads They are equipped with an electronic overload protection that is activated in the presence of excessive mechanical resistance A Warning The Sample Processor does not provide sufficient protection during the processing of potentially infectious samples or reagents Implement appropriate protective measures 815 Robotic Soliprep for LC 1 Introduction 1 5 Recycling and disposal 815 Robotic Soliprep for LC This product is covered by European Directive 2002 96 EC WEEE Waste from Electrical and Electronic Equipment The correct disposal of your old equipment will help to prevent negative effects on the environment and public health More details about the disposal of your old equipment can be obtained from your local authorities from waste disposal companie
37. ompact complies with FDA regulation 21 CFR Part 11 as well as GLP Dialogue languages German English French Spanish Chinese Korean Japanese and more 1 licence 6 6059 202 MaglC Net 2 0 Professional CD 1 licence Professional PC program for controlling intelligent Professional IC sys tems Compact IC instruments and their peripherals such as Professio nal Sample Processors model 800 Dosinos dosing systems 771 Compact Interface etc The software permits control data acquisition evaluation and monitoring as well as report generation for ion chro matographic analyses Graphic user interface for routine operations extensive database programs method development configuration and manual system control highly flexible user administration efficient database operations extensive data export functions individually con figurable report generator control and monitoring of all system com ponents and the chromatographic results MaglC Net Professional complies with FDA regulation 21 CFR Part 11 as well as GLP Dialogue languages German English French Spanish Chinese Korean Japa nese and more 1 licence 815 Robotic Soliprep for LC Qty Order no Description 1 6 6059 203 MaglC Net 2 0 Multi CD 3 licences Professional PC program for controlling intelligent Professional IC sys tems Compact IC instruments and their peripherals such as Professio nal Sample Processors 800 Dosino 771 Compact Interface etc Th
38. osition in order to set a suitable position 4 Click on Configure rack 5 Under Lift position select the Work position for Special beaker 2 6 Click on the associated Assign button 7 Click on Close 815 Robotic Soliprep for LC 47 5 4 Lift positions for stripping needles and filters 5 4 Lift positions for stripping needles and filters External position 1 1 Under Device selection All devices click on 815 Robotic USB and then select the tab Tower 1 2 Fasten a plastic needle or a membrane filter to the Luer adapter of the transfer robotic arm 3 Under Robotic arm position actuate the button Arrow right until the Luer adapter is approximately 2 cm in front of the deflector 4 Move the lift downward until the thick sleeve of the Luer adapter is approximately 1 cm underneath the deflector Click on the arrow but ton Arrow down and also if required Arrow up under lift position in order to set a suitable position 5 Click on Configure rack 6 Under Lift position select Swing position External positions 7 Click on the associated Assign button 8 Under Robotic arm position select External position 1 9 Click on the associated Assign button 10 Under Lift position select the Work position for External 1 815 Robotic Soliprep for LC 815 Robotic Soliprep for LC 5 Setting lift positions Work position For External ija Special beaker 13 a Special beaker 14 Shift positio
39. r special beakers 46 Lift positions for stripping needles and filters 48 Lift position for the Luer connector 50 Lift position for the Polytron ssueussessseeee 51 Lift position for the washing station 52 54 57 Scope of delivery 2 815 4110 sssseseueesusesss 57 Optional accessories sssessssenee 68 70 815 Robotic Soliprep for LC 1 Introduction 1 Introduction 1 1 Instrument description 815 Robotic Soliprep for LC The 815 Robotic Soliprep systems are automation systems with a multiple variety of applications They have been designed exclusively for usage in factories and laboratories and cover a wide range of applications Soliprep systems can be used for automation purposes wherever a complex sample preparation of solid substances is required e g for pharmaceutical or food analysis The Robotic Sample Processors which have proven their worth for many years form the basis for a versatile system that has been expanded to include opportunities for the dispersion filtration and bottling of samples of all sorts The versatile concept can be expanded practically at will Thanks to the integration of high performance communication interfaces USB RS232 they can be incorporated seamlessly into a variety of instru ment systems and not on
40. re clamp and clamp tightly with the fixing lever Tighten the set screw to an extent sufficient to ensure that the pump tubing is unable to shift position The flow rate of the pump can be regulated later with the set screw while the pump is running 6 Connect the connection cable of the pump to tower 2 The instrument must be switched off thereby 815 Robotic Soliprep for LC anmmmmum 27 2 10 Setting up the rinsing tubings 2 10 Setting up the rinsing tubings Rinsing tubings at tower 2 6 1805 060 6 1805 120 Install the tubing for rinsing the washing station as follows 1 Connect the green inlet tubing 6 1805 120 of the washing station to one of the four connectors on the tower 2 distributor 2 Connect three 6 1805 060 tubings 60 cm to the tower 2 distributor 3 Fasten a 6 1812 000 PTFE tubing to the tower 2 valve Connect the other end of the tubing to a canister with rinsing liquid e g water 2 11 Opening guide chain Tubings and cables can be placed into the guide chain of the towers You can open the individual chain links with a screwdriver as follows 28 815 Robotic Soliprep for LC 2 Installation 1 Open the guide chain a Insert a screwdriver into the groove located on the side of a chain link Loosen the clip with a forceful leverage movement Pull the clip out of the chain by hand Repeat the above actions for each chain link 2 Insert into the guide chain Place the require
41. rive and controller no dispersing aggregate see optional accessories 1 1 772 0110 772 Pump Unit Peristaltic pump for direct connection to Sample Processors 1 1 786 0010 786 Swing Head Auxiliary drive for Sample Processors for controlling a robotic arm 1 1 786 0110 786 Swing Head Auxiliary drive with stabilizer plate for Sample Processors for control ling a robotic arm 2 1 800 0010 800 Dosino Drive with write read hardware for intelligent dosing units 1 1 815 0110 815 Robotic USB Sample Processor XL Sample Processor with 2 towers 2 built in membrane pumps and 2 pump connectors 2 6 1432 320 Sample beaker 250 mL Material borosilicate glass 3 3 Height mm 111 Outer diameter mm 65 Volume mL 250 815 Robotic Soliprep for LC 57 58 7 1 Scope of delivery 2 815 4110 Qty Order no Description 1 6 1459 300 Sample beaker 120 mL 100 pieces Sample beaker with screw cap for sampling 100 pieces Material PP Height mm 113 Outer diameter mm 40 Volume mL 120 1 6 1462 240 Transfer head for 786 Swing Head bent and right swinging Transfer head bent and right swinging for 786 Swing Head In com bination with the 6 1808 220 Adapter the transfer head can be used on multi row racks to pick up tools with luer connection Material PP black 1 6 1462 250 Swing arm for Polytron and 786 Swing Head left swinging Swing arm for Polytron and 786 Swing Head left swinging with one buret
42. s or from your local dealer 2 1 Preparing the Sample Processor 2 Installation It is assumed for the purpose of these installation instructions that the required adjustment of turntable and Swing Heads has already been per formed for the present Robotic Sample Processor 2 1 Preparing the Sample Processor Plugging in the mains cable Pad l pw DD Ra tU E The mains connector is located on the rear side of the instrument Connecting the Swing Heads i Note The necessary settings must first be made in the MagIC Net control soft ware before the robotic arms can be mounted on the Swing Heads The two Swing Heads are connected for this purpose but the robotic arms are not yet mounted 6 815 Robotic Soliprep for LC 815 Robotic Soliprep for LC 2 Installation 1 Connect the Swing Head with reinforcement to tower 1 on the right the Swing Head without reinforcement to tower 2 on the left The connector is located in each case on the rear of a tower The Swing Heads can be laid down flat but not with the drive disc facing downward Connecting the controller cable USB 2 m USB 1 Contr 1 Connect the 6 2151 000 controller cable to the rear of the instrument 2 2 Installing MaglC Net i Note The plug on the instrument end of the 6 2151 000 controller cable is protected against accidental disconnection by means of a pull out pro tection featur
43. sized sample series in analytical laboratories The functioning of the automation system comprises crushing homogenizing and dissolving of solid samples as well as filtering and transferring the resulting sample solu tions Its main area of application is the sample preparation in instrumental chromatography It is not suitable for usage in biochemical biological or medical environments in its basic equipment version The present instrument is suitable for processing chemicals and flammable samples The usage of the 815 Robotic Soliprep for LC therefore requires that the user has basic knowledge and experience in the handling of toxic and caustic substances Knowledge with respect to the application of the fire prevention measures prescribed for laboratories is also mandatory 1 3 About the documentation 1 3 1 Symbols and conventions The following symbols and styles are used in this documentation Cross reference to figure legend The first number refers to the figure number the sec ond to the instrument part in the figure Instruction step Carry out these steps in the sequence shown Warning This symbol draws attention to a possible life hazard or risk of injury Warning This symbol draws attention to a possible hazard due to electrical current Warning This symbol draws attention to a possible hazard due to heat or hot instrument parts Warning This symbol draws attention to a possible biological hazard 81
44. supplied with the robotic arm reinforcement These are longer than the ones previously used Initializing the rack and the Swing Heads Both Swing Heads must be moved to the starting position for the mounting of the robotic arms 1 On the tab Rack click on Initialize rack Both lifts are moved upward The Swing Heads are now in starting position 2 5 Mounting the deflector Luer connector and collec tion container When injection needles and disposable filters are used these need to be stripped off the robotic arm again afterwards A deflector has been mounted for this purpose Proceed as follows Mounting the deflector 1 Loosen the uppermost two screws on the right hand side of Tower 1 2 Screw the 6 2058 050 fastening plate tightly with the aid of the screws supplied 16 815 Robotic Soliprep for LC BEEHEEENEENHENHEEENHENHEEHEENEN 2 Installation 2058 050 3 Screw the deflector tightly to the fastening plate with the screws and washers supplied It is recommended that the highest position be selected The deflector can be shifted laterally as required 6 2058 060 Mounting the Luer connector and collection container 1 Remove the sample rack 2 Fixthe holder with the 6 2843 000 Luer connector as illustrated to the mounting rail with the aid of the clamps The clamp on the right must enclose the spacer bolt of the mounting rail 6 2843 000 815 Robotic Soliprep for
45. t in the configuration of a robotic arm or a sample rack rack table This allows fine tuning to be performed The adjustment only needs to be made when a 6 2068 020 or 6 2068 030 sample rack is used The inserts for membrane filters which can be used with these racks have a positioning reticle This is the adjusting position Preparing the Sample Processor Proceed as follows 1 Putthe sample rack in place The insert or the inserts for membrane filters must be attached 2 Start MaglC Net 3 Open the Manual control with a click on the corresponding icon in the toolbar 4 Under Device selection gt All devices gt 815 Robotic USB select the tab Rack 5 Click on Initialize rack The sample rack moves into starting position The rack code is read and the rack table is loaded Moving to the positioning reticle Proceed as follows 1 In the Manual control in MaglC Net switch to the tab Tower 1 815 Robotic Soliprep for LC 4 Adjusting rack and robotic arm 2 Under Rack position select the target position Special beaker 16 and click Start Itis also possible to specify the target position as absolute rack position For the 6 2068 020 sample rack the adjusting position is no 105 for the 6 2068 030 sample rack the adjusting position is 115 3 Under lift position enter 160 mm as target position and click Start Afterwards move the lift further downwards millimeter by millimeter until the robotic ar
46. the 815 Robotic USB Click the tab Tower 1 3 Under Rack position click on Start The rack moves to a valid rack position 4 Click on the arrow button left under Robotic arm position until the drive disc is no longer moving Robotic arm position 0 0 x Start Ku p Mounting the robotic arm 1 6 1462 240 20 815 Robotic Soliprep for LC 2 Installation Mount the 6 1462 240 robotic arm to tower 1 as follows 1 Align the robotic arm parallel to the left hand edge of the Swing Head reinforcement and graze it across the guide pins of the drive disc of the Swing Head from below The correct position of the arm can be found in the previous illustration Take care to ensure that you do not twist the drive disc thus causing pressure against the drive 2 Screw the robotic arm to the Swing Head tightly with the screws and washers provided Mounting the transfer tubing A sufficiently long transfer tubing is required for aspirating or expelling sam ples The 6 1562 130 transfer tubing contains more than 10 mL of volume and is placed in a holder on the guide chain of tower 1 Mount it as follows N 6 1562 130 4 1 Use a screwdriver to open and remove one of the chain links on the guide chain see for this purpose see Chapter 2 11 page 26 2 Hangthe holder with the 6 1562 130 transfer tubing in the guide chain in place of the removed chain link and press it into place Mounting the Luer adapter
47. then be assigned to a predefined lift position The sample rack must be charged with all of the inserts Preparing 1 Opening the manual control In the symbol bar of MagIC Net click the hand symbol 2 Under Device selection gt All devices click on 815 Robotic USB and then select the tab Tower 1 5 1 Lift position for sample beakers Working height 1 Move to sample position 1 Under Rack position enter Target posi tion 1 and click Start 2 Fasten a plastic needle to the Luer adapter of the transfer robotic arm 3 Move the lift downward until the needle is at a suitable height for aspiration of the dispersed sample Under Lift position click on the arrow button Arrow down and also if required Arrow up in order to set a suitable position 4 Click on Configure rack 44 815 Robotic Soliprep for LC 5 Setting lift positions Rack position Current position 1 Special beaker 1 Assign Lift position Current position 171 mm Work position For Tower Rinse position For Tower z Shift position For Tower Special position For Tower Robotic arm position External positions z Assign Robotic arm position Current position 79 4 External position 1 Assign Close Under Lift position select Work position for tower if this is not yet selected Click on the associated Assign button Click on Close 8 Remove the need
48. troke path mm Min beaker radius mm Lift rate mmjs Axial distance mm Swing Head Serial number Swing position mm 2 Swing offset S Max swing range s Swing radius mm Rotation offset e Swing direction Enter the following settings Swing offset 8 6 a Maximum swing range 122 Swing radius 149 8 mm Rotation offset 0 0 Swing direction 4 First click on the Tower 2 tab and then on Configuration Properties 815 Robotic USB Sample Processor XL 815 Robotic USB Sample Processor amp L1 General Toweri Tower parameters Max stroke path mm Min beaker radius mm Lift rate mmjs Axial distance mm Swing Head Serial number 14228 Configuration Swing position mm Tower 2 Swing offset Max swing range Swing radius mm Rotation offset 9 Swing direction o o Enter the following settings 815 Robotic Soliprep for LC manmmmmum 11 12 2 4 Mounting the Swing Heads Swing offset 0 0 a Maximum swing rage 115 5 Swing radius 110 mm Rotation offset 0 0 m Swing direction Finish the settings with OK The instrument must be reinitialized in order to make the settings effective Click on OK Attach a sample rack on the turntable of the instrument Right click on the instrument name 815 Robotic USB in the Devi ces window and click on Initialize
49. tubing over the connection nipple of the distri butor and fasten in place with the union nut The opening of the tubing may need to be widened with a sharp object e g with a Phillips screwdriver A piece of sandpaper may be used to get a better grip on the tubing Do not extend the tubing end before having slid the union nut onto the tubing 815 Robotic Soliprep for LC 25 2 9 Connecting and setting up the peristaltic pump ENEEEENEEEHEEEEEEHEEEEEE 2 9 Connecting and setting up the peristaltic pump A peristaltic pump 772 Pump Unit is used for aspirating the washing station at tower 2 S9 OS 772 Pump Unit o p 6 1820 050 6 1826 100 6 1812 000 1 Cut one piece of 6 1826 100 pump tubing down to a length of approx imately 17 cm and attach a 6 1820 050 olive connector at both ends 2 Fasten apiece of 6 1812 000 PTFE tubing leading to a waste container to one of the olive connectors Attach the 6 1812 000 PTFE tubing that is connected to the washing station as a drain connection to the other olive connector 3 Release the fixing lever by rotating the set screw and fold open the pressure clamp 4 Sling the pump tubing around the rotor and fasten it with the tubing clamps The rotor turns in clockwise direction The inlet tubing must therefore be clamped below the outlet tubing above TELL 815 Robotic Soliprep for LC BEEHEEENEENHENHENHENHENHEEHEEN 2 Installation 772 Pump Unit 5 Apply pressure to the pressu
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