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Milli-Q Synthesis and Milli-Q Synthesis A10 User Manual

1. 2 72 6 8 HOW TO REPLACE THE ATO UV LAMP 2 2 2 22 20225 522 202 0 0 2 22 202 72 6 9 HOW TO CLEAN THE ATO TOC MONITORING He 72 How long does ATO Cleaning take 2 1 242 22 2 0 2000 eene eene enne nennen nnns 72 Why would need to do an ATO Cleaning sssse tette 72 Would an ATO Cleaning ever happen automatically 2 72 How do do an A10 Cleaning 73 How do cancel the ATO CLEANING once it is 74 6 10 HOW TO PERFORM AN AIR PURGE 2 22 2 22 2502 0 20222 2 0 2022 0 205 0 202 2022224 75 6 11 HOW REPLACE THE UV IH m I nmn e hene e hene ne een nnne 76 CHAPTER 7 TROUBLESHOOTIMO sss A A bleko ka 77 The problem is low No Flowrate from the POU Dispenser ff The problem is low Resistivity of the Product 2222222 022002222 002225 0222 eene 78 The problem is there is no power to Milli Q 5 nennen enne 79 The problem is there is an ERROR Number Alarm displayed 79 Continuation of ERROR Number Alarm 2222222 2222222222200022222 2222222 022 80 The problem is a message is displayed with a Flashing Service or Alarm esenee 8 Cher
2. gt 3 P Sg Character S Back Forward Up Address ca C Program FilessAccessoriessHype E gj MGhPoweDex gt G DialUp Networking E favis Onine Services B9 Direct Cable Connection EE gj Sp AT amp T CompuServe Documents Internet Explorer Imaging Microsoft Binder Notepad B i 2 No Microsoft Excel Pant Find Microsoft NetMeeting Phone Dialer Microsoft Photo Edtor 29 Synchronize Hep Microsoft PowerPoint WordPad 1 Microsoft Word w 9 z 5005 Prompt 4 4 MCI Mail ht fizer TXT 119 AJ Wndons Ero d 3 Windows Messaging 1 object s selected Q Double Click on the HYPERTRM EXE icon Entero name example MQ and then choose an icon You can use this later for future downloads 7 New Connection HyperTerminal File Edit View Call Transfer Help File Edit View Call Transfer Help 918 scies Dl e XU Mee m Bo Enter a name and choose an icon for the cor Enter details for the phone number Name Country code Area code A Choose Direct to COM 1 or COM 2 then click on OK Q For the COM properties change the settings to be 89 Bits Per Second 9600 Data bits 8 Parity none Stop bits 1 Flow Control none
3. 24 2 2 422 122 22 0202200000000 50000 7 When do change the Q Gard Purification Paek esse esr esas ana 8 Whendo lehange he UV reus ERREICHEN 8 Cena a s M 8 What are the different types of Quantum 9 52 124 2 4 42 0 2 0100 8 When do change the Quantum Ultrapure Cartridge 2 1 2202 2 020222220200000002 00000 8 ESOR ODO Iq amm 9 KS SV OBSOLETE 2 Resistivity and temperature meqosurements ann ee enne 9 Temperature Compensation Conductivity 0 22 1202 02 22020 20 5 9 Point DIESO OPE A E rrr rrr r UG a ds UG I I I Dol a So US Lebl 2 TABLE OF CONTENTS iso s TN DREE 70 What types of Millipak Filters are Ihere9_ 10 When do change the 2 4 2 22 2 2 422 202 2 02220028 000020222200 10 ALO LOC MONNE p asha suas ENO bende ens 72 What does the 10 00 2 0 2 0000000 00 12 What maintenance is involved with the 100 2 12 2 4 TECHNICAL SPECIFICATIONS m 13 Dimensions System and Cfearance
4. tese en en do re E ete 13 Sc TEF ROE Oe OTe E s 13 Lerno ae eg cl gcc cece 13 Measurement Ranges for TOC Resistivity Conductivity and Temperature 12 Materials of Construction 2 2 2 2 2222 665050000000 eene nennen eene erra nnne 14 o I a as ha ata oo 14 CHAPTER PRE INSTALLATION seuss siste tke e EYE FRED enk FE APR HERR GI 15 ssp EBERT a duret riter oe et orte Roth Das dle teg ask Ur lh Rio 15 3 2 PRE INSTALLATION CHECKUST ARMIESS MILI sus er eer terrere rne en ie en nope eni 16 3 3 OPIIONAL EQUIPMENT YOU MAY NED a na en kada sn aa la a anino 17 EVO ANODO Ena akana n ave x duc d od ka e la 17 e desde no IZ Ball Valve for shutting off the feedwater supply 222 2222222 22222 2 20 022222202022 7 Remote Point Use Dispenser 17 Remote Point Of Use Dispenser used a Production 2 222022222202222202 18 LOWI uM ME 18 Riner or Jay xd eee ne 18 Remote Display with 22222222222222 002222 0222 0222220 22 18 SEN tse REQUIREMENTS PME 20 Consumables needed for installation EE
5. or the last measured TOC value is not stored in the system s memory 82 ORDERING INFORMATION Chapter 8 ORDERING INFORMATION 8 1 CATALOGUE NUMBERS FOR CONSUMABLES Consumable Catalogue Number Q Gard 1 Purification Pack QGARDOORI 1 box used for RO Elix Milli RX Milli RO distilled Feedwaters Q Gard 2 Purification Pack QGARDOOD2 l box used for Dl Service DI Feedwaters Q Gard B1 Purification Pack Q GARDOOB 1 l box used specifically for Boron Removal Q Gard VX Purification Pack Q GARDOOVX l box used specifically for volatile organic species removal Quantum Cartridge QTUMOOOIX 1 box Millipak not included used for applications needing trace levels of ions Quantum EX Cartridge QTUMOOOEX 1 box Millipak not included used for applications needing trace levels of ions and trace levels of organic species Quantum VX Cartridge QTUMOOOVX 1 box Millipak not included used for applications needing trace levels of volatile organic species and ions Quantum ICP Cartridge QTUMOOICP 1 box Millipak not included used for sub ppt level elemental analysis Quantum IX Cartridge with Non sterile QTUMMPEIX 1 Quantum Cartridge 1 Non sterile Millipak Express 20 Millipak Express 20 per box Quantum EX Cartridge with Non sterile QTUMMPEEX 1 Quantum Cartridge 1 Non sterile Millipak Express 20 Millipak Express 20 per box Millipak 40 Sterile MPGLOASK2 2 box used for Science Applications Millipak 20 Expre
6. 2 Unplug the Powercord from the Milli Q System 3 Obtain the correct replacement fuse There is a spare fuse located in the fuse holder See step 4 It is very important to use the correctly sized replacement fuse Failure to use the correct replacement fuse could result in system damage or an electrical fire System Voltage Main Power Fuse Size 120 VAC 10 2 Amp Time Lag 250 VAC 5 mm x 20 mm 230 VAC 10 1 Amp Time Lag 250 VAC 5 mm x 20 mm 1 Use a small flathead screwdriver to open the Fuse Holder This is located immediately above the point where the Powercord plugs in 2 Remove the entire fuse holder Replace the blown fuse you can check the fuse for electrical continuity with an Ohmmeter Place the Fuse Holder back into the Milli Q System Put the Powercord back in Tum on the Power Switch 4 The LCD will show the type of system the system serial number and software version for a few seconds Wait about 10 seconds for this to go away 5 Place the system back to PRE OPERATE Mode or whatever mode it was previously in CONTACT MILLIPORE IF THE MAIN POWER FUSE BLOWS AGAIN A ATTENTION 85 REPLACEMENT OF MAIN POWER FUSE APPENDIXES Milli Q Synthesis Synthesis ATO 86 APPENDIXES APPENDIX2 HOW TO TRANSFER INFORMATION TO PRINTER It is possible to transfer download information to a printer from the Milli Q REQUIREMENTS NEEDED A cable is needed to connect between the Milli Q and a printer
7. Check tubing connections on back of Milli Q See plugged into the Milli Q instructions that came with Remote POU Dispenser 77 TROUBLESHOOTING THE PROBLEM IS LOW RESISTIVITY OF THE PRODUCT WATER CAUSE REMEDY lon Exchange Capacity of Q Gard Pack and Quantum Replace Q Gard and Quantum at the same time Cartridge exhausted used up Non Temperature Compensated Resistivity values e Check the Temperature Compensated Resistivity shown and water temperature is gt 25 C Value See Section 4 13 Conductivity values uS cm displayed Nothing wrong Change to a NEAJ Display to check values See Section 4 1 Something other than a Q Gard Pack is installed by e Check 2 Number of installed Pack See mistake Section 8 1 lon Exchange Resin was fouled by high levels of e Switch to a feedwater such as RO Elix Colloidal Species in Feedwater Occurs with Deionised Feedwater i e Service Deionised Feedwater Problem with internal component Contact Millipore UF Cartridge is dirty Perform a SAN CYCLE Sanitisation and Cleaning of the UF Cartridge See Section 6 5 for more information UF Cartridge is slightly dirty e Perform an AIR PURGE See Section 6 10 for more information Resistivity is low immediately following the completion Perform an AIR PURGE and then go to PRODUCT of a Sanitisation and Cleaning of the UF Mode for several minutes to rinse the UF Cartridge Repeat the
8. Click OK 1 Properties Port Settings APPENDIXES L Bits per second 3600 Data bits 8 Stop bits 1 Elow control None Advanced By default the data will be saved in the directory Restore Defaults Open the TRANSFER menu and click on CAPTURE TEXT Choose a file name for the data to be downloaded C ProgramFiles Accessories Hyperterminal txt Now click on START File Edit View Call 20 Help D Send File Text Send File Capture to Printer in PRE OPERATE or STANDBY Mode 18 2MQ cm TOC 4 ppb 25 C Elixdata txt is an example name shown below L2 x Folder C NProgram Files Accessories HyperT erminal 1 erminal Elixdata tt Browse Make sure the Milli Q is in PRODUCT Mode It is not possible to download to a computer while the Milli Q is Press the MENU Keypad Button for about 2 seconds The LCD will change as shown here PRESET VOLUME 0 00 Press MENU for about 2 seconds 90 APPENDIXES Press the MENU Keypad Button one more time LCD will change as shown here PRESET VOLUME 0 00 SERVICE PRINTER PRESS MEASURE Press MENU Press the MEASURE Keypad Button Information wi
9. PRODUCT INFORMATION A10 TOC MOoNITOR WHAT DOES THE A10 po The ATO TOC Monitor called ATO in this manual is used to measure the TOC of the Milli G Product Water The ATO is located inside the Milli Q System Cabinet Any Milli Q system with an A10 inside will have A10 on the end of the name of the Milli Q i e Milli Q Synthesis A10 vs Milli Q Synthesis An 10 TOC measurement is initiated every time the Milli Q is brought from PRE OPERATE to PRODUCT Mode when the POU Dispenser Trigger is brought forward single TOC Measurement will take approximately 5 minutes lt is possible to have a TOC analysis time of either 9 or 12 minutes when the TOC levels are high The ATO will continuously perform TOC measurements while the Milli Q is in PRODUCT Mode The ATO will perform a TOC measurement once per hour while the Milli Q is in PRE OPERATE Mode The ATO will not perform any measurements when the Milli Q is in STANDBY Mode WHAT MAINTENANCE IS INVOLVED WITH THE A10 The 10 uses a small UV light during its TOC Analysis Mode 10 UV lamp needs to be replaced periodically The normal useful lifetime of the ATO UV Lamp is 1 year The Milli Q system uses a calendar day timer to record age of the AIO UV lamp service message is prompted after 365 Days EXCHANGE ATO UV to remind you to change the ATO UV lamp The Catalogue Number for the A10 UV Lamp is 7 100 01 There is a Cleaning Mode for the ATO This
10. Standard Specitication Reagent Water Designation D 1193 99 American Society For Testing And Materials pH not specified The measurement of pH has been eliminated for this standard because this grade of water does not contain constituents in sufficient quantity to alter pH PRODUCT INFORMATION 2 2 SCHEMATIC OF MAIN COMPONENTS The water flow through Milli Q Synthesis Water Purification System is shown here a flow diagram description of each item is in the next section below X RECIRCULATED WATER PATH 4 I I I I I I I I I I I MILLI Q 9 PRODUCT FEEDWATER l WATER A pla T D E Y 7 Y PRESSURE RELIEF UF DRAIN The water flow through a Milli Q Synthesis A10 is shown here in a flow diagram 4 4 ERE 7 RECIRCULATED WATER PATH I I I I I I I I MILLI Q p PRODUCT FEEDWATER WATER I D E F E PRESSURE RELIEF UF DRAIN A 10 REJECT WATER PATH Identification of lettered items in the flow schematic above UV Lamp and Resistivity Housing Sensor Quantum Electric 2 way Ultrapure Cartridge Pyrogard amp Millipak Purification 5000 UF Membrane Cartridge Filter PRODUCT INFORMATION 2 3 DESCRIPTION OF MAIN COMPONENTS INLET SOLENOID VALVE The Inlet Solenoid Valve is used to control the flow of feedwater into the Milli Q system The Inlet Solenoid Valve is open when the system is delivering wa
11. A message EXCHANGE A10 UV will appear after 365 Calendar Days indicating that the A1O UV Lamp needs to be replaced It is recommended to have a Millipore Field Service Representative change the ATO UV Lamp The replacement of ATO UV Lamp involves removing the cover of the system instructions for replacing the ATO UV lamp are not included in this manual The instructions are included with the replacement ATO UV Lamp Contact Millipore for a copy of these instructions if you would like to see them before ordering a replacement ATO UV Lamp 6 9 How TO CLEAN THE A10 TOC MONITORING DEVICE The A10 TOC Monitoring Device may need to be cleaned sometimes This cleaning does not involve any chemical reagents This cleaning is initiated with the Milli Q software and is simple to perform HOW LONG DOES THE A10 CLEANING TAKE The A10 Cleaning takes 60 minutes to complete The ICD will show a countdown timer indicating the remaining time until the Cleaning is finished WHY WOULD NEED TO DO AN A O CLEANING The A10 Cleaning is recommended when 1 the Q Gard and Quantum have been replaced see the next question below 2 the displayed TOC values are fluctuating 3 the displayed TOC values are higher then normally seen 4 the Milli Q has been in STANDBY Mode or powered off for more than 12 hours WOULD AN 10 CLEANING EVER HAPPEN AUTOMATICALLY An ATO Cleaning will occur automatically after Q Gard Pack and Qua
12. This item is not part of a Millipore Catalogue Number a Will the Milli Q System Cabinet and the Remote POU Dispenser be located within 2 5 meters of each other a Will the Milli Q System Cabinet and the Remote Display be located within 2 4 meters of each other PRE INSTALLATION 3 3 OPTIONAL EQUIPMENT YOU MAY NEED WALL MOUNTING BRACKET Millipore Catalogue Number for the Wall Mounting Bracket is SYSTFIX01 The mounting hardware for attaching the bracket to wall is not included and must be supplied The bracket is attached with at least 2 bolts or screws Width of bracket 23 Height of bracket 2 5 4 cm Thickness of bracket 0 4 cm Diameter of holes in the bracket for bolts or screws 0 7 cm Mounting holes on bracket are approximately 5 4 cm from either edge PRESSURE REGULATOR The Millipore Catalogue Number for a Pressure Regulator with Pressure Gauge and 8 mm tubing connections is ZFMQOOOPR It is important that the Pressure Regulator is adjusted while water is A ATTENTION flowing through it A range between 0 1 bar and 0 3 bor 1 5 to 4 5 psi is the normal setting of the Pressure Regulator while water is being dispensed from the Milli Q The Pressure Regulator is factory pre set to 0 3 bar while water at 80 LPH is flowing through it BALL VALVE FOR SHUTTING OFF THE FEEDWATER SUPPLY It is highly recommended to use a ball valve on the Feedwater Tubing The ball valve will be used to shut off
13. OPEN THE VALVE AIR PURGE 5 mn Q Bring the POU Dispenser Trigger down The AIR PURGE will begin A sharp click will be heard This is the opening of a UF Cartridge Reject Solenoid Valve Water will begin to flow through the UF Cartridge Reject tubing Q The AIR PURGE will last for 5 minutes When the timer reaches O minutes the Milli Q will go into STANDBY Mode The LCD will prompt you to CLOSE THE VALVE SERVICE UF STANDBY AIR PURGE 0 mn CLOSE THE VALVE Close The Valve by bringing the POU Dispenser Trigger back to the upright position The Milli Q will now go to PRE OPERATE Mode STANDBY PRE OPERATE CLOSE THE VALVE You have finished performing an AIR PURGE 6 11 HOW TO REPLACE THE UV LAMP The UV lamp is normally replaced once a year every 365 Days A message EXCHANGE UV will appear after 365 Calendar Days indicating that the UV lamp needs to be replaced It is recommended to have a Millipore Field Service Representative change the UV lamp The replacement of the UV lamp involves removing the cover of the system The instructions for replacing the UV lamp are not included in this manual The instructions are included with the replacement UV Lamp Contact Millipore for a copy of these instructions if you would like to see them before ordering a replacement UV Lamp 76 TROUBLESHOOTING Chapter 7 TROUBLESHOOTING THE PROBLEM IS LOW OR NO F
14. PRE OPERATE position if you were using the system to get Product Water The Close The Valve message will go away and the timer will count down from 400 mn SAN CYCLE CLOSE THE 400mn VALVE SAN CYCLE 399mn 67 MAINTENANCE It is very important that the POU Dispenser is closed now The Sanitisation A timer will not count down from 400 minutes until the valve is kept closed When the timer reaches 1 mn the Milli Q will automatically go into PRE OPERATE Mode SAN CYCLE 1mn gt PRE OPERATE Sanitisation and Cleaning of the UF Cartridge is now finished The water inside the Milli Q will be recirculated for 5 minutes every hour of PRE OPERATE Mode When you use the system i e the morning after the UF was Sanitised dispense enough water until the Resistivity values are satisfactory Remember to leave the Milli Q in PRE OPERATE Mode during times of non use i e evenings weekends holidays 68 SANITISATION OF THE UF MAINTENANCE 69 MAINTENANCE 6 6 HOW TO CLEAN THE SCREEN FILTER The Screen Filter is located in the Assembly of Blue Fittings that came in the Accessories Bag from the Shipping Box The purpose of the Screen Filter is to prevent a large particle or other debris from entering the Inlet Solenoid Valve of the Milli Q System This will allow the Inlet Solenoid Valve to open and close correctly If
15. gt 18 2 Air in the Product Water tubing near the Resistivity Sensor can cause this Make sure the Quantum Cartridge is Air Purged See Section 4 7 for more information SYSTEM ERROR 7 displayed Contact Millipore The POU Dispenser will not dispense water You will not be able to dispense water SYSTEM ERROR 8 displayed Contact Millipore The POU Dispenser will not dispense water You will not be able to dispense water SYSTEM ERROR 10 displayed There was a problem reading or writing data to the Data Storage Prom E Prom Placing the system into STANDBY Mode then back to PRE OPERATE Mode will erase this message for a few days The system will still produce high quality water Continue to use the system Contact Millipore to have this error fixed A10 ERROR 0 ATO E Prom defective Turn off on the Milli Q and dispense water for gt minutes If the message continues contact Millipore A10 ERROR 1 A10 PCB A D converter defective Turn off on the Milli Q and dispense water for gt 6 minutes the message continues contact Millipore A10 ERROR 2 Thermistor defective Tum off on the Milli Q and dispense water for gt 6 minutes If the message continues contact Millipore A10 ERROR 3 Problem occurred with temperature compensation Turn off on the and dispense water for gt 6 minutes If the message continues contact Millipore A10 ERROR 4 The water entering ATO is lt 4 C
16. AIR PURGE if necessary 78 TROUBLESHOOTING THE PROBLEM 15 THERE IS NO POWER TO THE SYSTEM CAUSE REMEDY No voltage at Wall Electrical Outlet e Check Voltage at Wall Electrical Outlet Powercord not plugged into Milli Q e Confirm that the Powercord is plugged in System not turned on e Confirm Power Switch is turned on Main Power Fuse blown e Replace Main Power Fuse See Chapter 9 Appendix A Problem with internal component e Contact Millipore THE PROBLEM IS THERE IS AN ERROR NUMBER ALARM DISPLAYED CAUSE REMEDY SYSTEM ERROR 1 displayed The voltage going to the Motor is gt 49 VDC CONTACT MILLIPORE SYSTEM ERROR 2 displayed The measured temperature is 0 C 5 the feedwater very cold CONTACT MILLIPORE SYSTEM ERROR 3 displayed The measured temperature is gt 45 C The system will still produce high quality water if the water is not really this warm i e Error coming from a Thermistor problem ls the feedwater really this warm CONTACT MILLIPORE SYSTEM ERROR 4 displayed The measured Resistivity Value 25 C is between 3 5 and 2 5 See the Section above The problem is low Resistivity of the Product Water for further information 79 TROUBLESHOOTING CONTINUATION OF ERROR NUMBER ALARM DISPLAYED CAUSE REMEDY SYSTEM ERROR 5 displayed The measured Resistivity Value 25 C is gt 65 5 The displayed Resistivity may not show
17. Cleaning Mode can be initiated with the Milli Q software The ATO CLEANING Mode does not use a chemical reagent of any kind The 10 Cleaning is explained in further detail in Maintenance Section of this manual PRODUCT INFORMATION 2 4 TECHNICAL SPECIFICATIONS DIMENSIONS SYSTEM AND CLEARANCE The height width and depth of a Milli Q Synthesis and Synthesis are shown here 74 4 T lt 2569 T 4 445 0 N 296 mm WEIGHT Milli Q Synthesis Operating weight wetted Q Gard Quantum and Millipak 16 kg Milli Q Synthesis ATO Operating weight 10 8 kg ELECTRICAL electrical requirements for a Milli Q Synthesis or Milli Q Synthesis are 120 10 50 60 Hz 100 VA 0 5 amp source 2 amp Time lag fuse used ref ZMQS6VFTI ZNQPOVFTI ZMQS6VFO1 ZMGPOVFO1 230 VAC 10 50 60 Hz 0 26 amp source 1 amp Time lag fuse used ref ZMQS5VFTI ZMGP5VETI ZMQS5VFO1 ZMQP5VFO 1 The source of electrical power should be within 1 meter of the Milli Q source of electrical power must be earth grounded MEASUREMENT RANGES FOR TOC RESISTIVITY CONDUCTIVITY AND TEM
18. Contact Millipore A10 ERROR 5 The water entering the 10 is gt 41 C Contact Millipore he conductivity of the water entering the ATO is gt 1 1 uS cm Contact Millipore h m A10 ERROR 6 T A10 ERROR 7 T A10 ERROR 9 The TOC is very low or a problem occurred with the 10 Contact Millipore 80 temperature inside the 10 during its analysis ode reached gt 55 C Contact Millipore TROUBLESHOOTING THE PROBLEM IS A MESSAGE IS DISPLAYED WITH A FLASHING SERVICE OR ALARM LED LCD MESSAGE DISPLAYED REMEDY EXCH CARTRIDGES Q Gard Pack and Quantum Cartridge have been installed for 180 Calendar Days or the Resistivity is lt 16 Resistivity Setpoint e Replace the Q Gard Pack and Quantum Cartridge e Check the value of the Calendar Day timer and the Resistivity Setpoint Contact Millipore to do this START SANIT e Perform Sanitisation of UF Cartridge See Section 6 5 for information on how to do this TOC SETPOINT displayed TOC value is greater than the TOC Setpoint Contact Millipore about changing the Setpoint CARTRIDGE OUT e Either the Q Gard Pack or the Quantum Cartridge is not pushed in far enough or is absent NO FEED WATER e Someone has installed a level sensor device to the Milli Q level of Feedwater is too low according to the level sensor device REBOOT SYSTEM e The AIO has been trying to process TOC Analysis unsu
19. Graduated Cylinder then use a container which could hold up to 2 of water Use an accurate measuring device to measure the total water that was dispensed from the Milli Q Q Bring the POU Dispenser Trigger down Press the MEASURE Keypad Button FLOW MEASURE PRESS MEASURE second to 60 seconds FLOW MEASURE DISPENSING 1 a The Milli Q will dispense water for 60 seconds Wait until this is finished The timer will count up from When the 60 second timer is finished the Flow Calibration Factor display will be shown Measure the total volume of water in litres dispensed from the Milli Q Use the Arrow Keypad Buttons the MEASURE and CLEANING Keypad Buttons to change the FLOW value to the amount of dispensed water 36 INSTALLATION In the example below you measured 1 15 lpm The flow measured during the manufacturing of the Milli Q was 1 00 lpm SERVICE CALIB SERVICE CALIB 1 001 1 15 1 J J 44 4 Flow Calibration i Flow you measured 2 Use arrow keypad fom Factory o Move the POU Dispenser Trigger back to its upright position Q Escape the Customer Service Software by pressing the MENU Keypad Button for about 2 seconds You should be back to PRE OPERATE Mode SERVICE CALIB FLOW 1 151 mn PRE OPERATE Press MENU for about 2 seconds You have finished ca
20. HOWTO USE THE FOOTSWITCH OPTIONAL 55 50 5 5 HOW TO DISPENSE AN EXACT AMOUNT OF PRODUCT WATER 2 222 50 5 6 HOW TO VIEW THE AGE OF THE CONSUMABLES 2 9 52 57 HOW TO UNDERSTAND MIHO MESSAGES e orko te erbe 54 6 MAINTENANCE eerie sasssssasaswaqaaasayaqwawaaasssaqasqaysaswaqsasassassaqayasa S 57 6 2 HOW TO REPLACE THE Q GARD 2 2 2 00 0 1190 22220222228000 hen n s e enne ern e es eren enne 58 6 3 HOW TO REPLACE THE QUANTUM CARTRIDGE e rene es rennen 60 6 4 HOW TO REPLACE THE TTT TTT TTTTTTTTTT e 65 TABLE OF CONTENTS 6 5 HOW TO SANITISE AND CLEAN THE UF CARTRIDGE 2 22 2 1 0 22200222 252222220200 66 How often would normally and Clean the UF 220 222222222222222 66 Things to know BEFORE you sanitise the UF 2222 222200222220 66 SEmi gran Cleaning the UF o OO UEU EA AO 66 FIOW TO CIEAN THE SCREEN PINTER Rs 70 6 7 HOW TO TIGHTEN THE POU DISPENSER
21. IMPLIED THERE IS NO WARRANTY OF MERCHANTABILITY OR FITNESS FOR A PARTICULAR PURPOSE The warranty provided herein and the data specifications and descriptions Millipore products appearing in Millipore s published cotalogues and product literature may not be altered except by express written agreement signed by an officer of Millipore Representations oral or written which are inconsistent with this warranty or such publications are not authorised and if given should not be relied upon In the event of a breach of the foregoing warranty Millipore s sole obligation shall be to repair or replace at its option the applicable product or part thereof provided the customer notifies Millipore promptly of any such breach If after exercising reasonable efforts Millipore is unable to repair or replace the product or part then Millipore shall refund to the customer all monies paid for such applicable product or port MILLIPORE SHALL NOT BE LIABLE FOR CONSEQUENTIAL INCIDENTAL SPECIAL OR ANY OTHER INDIRECT DAMAGES RESULTING FROM ECONOMIC LOSS OR PROPERTY DAMAGE SUSTAINED BY ANY CUSTOMER FROM THE USE OF ITS PRODUCTS Copyright 2003 CORPORATION PRINTED IN FRANCE All RIGHTS X RESERVED THIS BOOK OR PARTS THEREOF MAY NOT BE REPRODUCED IN ANY FORM WITHOUT THE WRITTEN PERMISSION OF THE PUBLISHERS Rev 3 03 06 Trademarks Millipore is a registered trademark of Millipore Corporation Elix Q Gard Millipak and Milli Q are reg
22. Millipore if you need to dispense water for more than 30 continuous minutes When you are finished dispensing water move the POU Dispenser Trigger back to the upright position The Milli Q will continue to operate but will not dispense water for 90 seconds After 90 seconds the Milli Q will automatically go to PRE OPERATE Mode 7 Leave the Milli Q in PRE OPERATE Mode Do leave it in STANDBY Mode unless you are going to perform some sort of maintenance i e changing the Q Gard and Quantum 46 USING THE MiLLI Q POU DISPENSER IN PRE OPERATE MODE POSITION POU DISPENSER IN PRODUCT MODE POSITION Milli Q Synthesis Synthesis 47 USING THE MiLLI Q 5 2 STANDBY PRE OPERATE AND PRODUCT MopE WHAT IS STANDBY MopE STANDBY Mode is selected before attempting maintenance the system For example you would select STANDBY Mode before removing the Q Gard Pack The Inlet Solenoid Valve is closed in STANDBY Mode The Milli Q will not have an hourly 5 minute recirculation of water in STANDBY Mode A Milli Q Synthesis A10 will not perform a TOC analysis during STANDBY Mode In STANDBY Mode you can move the POU Dispenser Trigger forward and then close it This will open the POU Dispenser Electric Valve for seconds This will allow the system to depressurise An example of when this would be needed is when you are about to remove a Q Gard Pack WHAT IS PRE OPERATE MODE PRE OPERATE Mode is selected when the s
23. PRESET VOLUME SERVICE PRINTER SERVICE CARTR 0 DAYS Press MENU each time 52 USING THE MILLI Q Stop when you see AGE display In the example above the AGE of the Cartridges CART is O Days installed in the last 24 hours This is referring to both the Q Gard and the Quantum It is being assumed that the Millipak was changed when the Q Gard and Quantum were changed Press the OPERATE STANDBY Keypad Button once to change to the age of the UV Lamp The AGE of the UV Lamp is O Days in the display below SERVICE AGE CARTR 0 DAYS SERVICE AGE UV LAMP 0 DAYS Milli Q Synthesis 10 only Press the OPERATE STANDBY Keypad Button once to change to the age of the ATO UV Lamp The AGE of the ATO UV the small UV lamp on the ATO device is O Days in the display below SERVICE AGE UV LAMP 0 DAYS SERVICE AGE UV A10 0 DAYS Press OPERATE STANDBY once Escape the Customer Service Software by pressing the MENU Keypad Button for about 2 seconds You should be back to PRE OPERATE Mode You have finished viewing the age of the consumable items 53 USING THE MiLLI Q 5 7 UNDERSTAND MILLI Q MESSAGES It is possible for various messages to be displayed on the Milli Q LCD while you are using the Milli Q While message is being displayed either the Yellow Service LED or the Red Alarm L
24. REPLACE THE Q GARD The Q Gard is normally replaced every 180 Days or when the Product Water quality is not optimal i e drop in Resistivity increase in TOC ionic breakthrough For Milli Q Synthesis Systems A Service Message EXCH CARTRIDGES will be shown after 180 Calendar Days For Milli Q Synthesis 10 Systems The Milli Q Synthesis ATO systems will not display a message EXCH CARTRIDGES It is up to the user of the Milli Q system to verify that the Resistivity and TOC values of the Product Water are still within specification When the Q Gard is replaced the 180 Day Age is reset to O Days This will remove the EXCH CARTRIDGES message from the LCD Follow the steps below to replace the Q Gard Pack Removing the used Q Gard Q Place the Milli Q into STANDBY Mode See Section 5 1 for more information if necessary While in STANDBY Mode move the POU Dispenser Trigger forward This will open the electric valve inside POU Dispenser residual water pressure will be released Allow any water to flow from the POU Dispenser in STANDBY Mode Move the POU Dispenser Trigger back to the upright position a Locate the Q Gard on the front right side of the Milli Q Locate the Pack Adapter Lid at the top of the Q Gard lift up the Pack Adapter Lid and remove the Metal clip from the metal rod Q Gently pull the Q Gard from the metal rod Installing the new Q Gard Remove the Q Gard from its shipping box Ver
25. The Millipore Catalogue number for this cable is PRNTCBLO1 This Printer Cable is an accessory for the Milli Q and needs to be ordered separately A Printer with a Serial Port is necessary It is not possible to use Parallel Transmission from the Milli Q 20 24 Column Serial Port Printer can be used An example of a Serial Port Printer that has been used with Milli Q systems is the Epson 1 300 WHAT TO DO STANDBY Mode 18 2MQ cm 25 C TOC 4 ppb Q Make sure the Printer is on line and has paper and so forth Make sure the Printer Cable is installed between the Milli Q and the Printer The installation instructions for this cable are not provided in this manual The installation instructions come with the Printer Cable Make sure the Milli Q is in PRODUCT Mode It is not possible to print while the Milli Q is in PRE OPERATE Press the MENU Keypad Button for about 2 seconds The LCD will change as shown here PRESET VOLUME 0 00 Press MENU for about 2 seconds Press the MENU Keypad Button one more time LCD will change as shown here PRESET VOLUME 0 00 SERVICE PRINTER PRESS MEASURE Press MENU Press the MEASURE Keypad Button The Printer will start to print The Milli Q will return to PRODUCT Mode automatically SERVICE PRINTER PRESS MEASURE lt Press MEASURE 18 2MQ cm 25 T
26. cartridges in the system The ALARM LED is red This will flash when an alarm condition is indicated on the LCD i e PAK NOT IN PLACE meaning a purification pack is not fully in place or is absent INTRODUCTION COMMONLY USED ABBREVIATIONS IN THIS MANUAL This manual will use abbreviations for text that is commonly repeated i e Liquid Crystal Display is abbreviated as LCD The table below shows a list of the abbreviations used in this manual microSiemens per centimeter measurement unit describing the electrical conductivity of water 10 a Millipore device which measures Ultrapure Water NPT National Pipe Thread the type of thread used on a fitting G ge vo eo 7 INTRODUCTION 1 2 SAFETY INFORMATION Your Milli Q Water Purification System should be operated according to the instructions in this manual In particular the hydraulic and electrical specifications should be followed and met lt is important to use this equipment as specified in this manual using this equipment in a different manner may impair the safety precautions of the Water System THis HAZARD symbol is used to refer to instructions in this manual that need to be done safely and carefully THIS ATTENTION symbol is used to refer to instructions in this manual that need to be done carefully Other safety symbols Danger Danger UV radiation Electrical Danger Ground Connection INTR
27. e cu VE m 82 CHAPTER 8 ORDERING INFORMATION 83 8 1 CATALOGUE NUMBERS FOR CONSUMABLES 83 8 2 CATALOGUE NUMBERS FOR 55 2 22 2 020 0 022222222222 84 8 3 CATALOGUE NUMBERS FOR ALL 5 2 93 m meme emen e 84 CHAPTER 9 APPENDIXES 9 85 APPENDIX 1 HOW TO REPLACE THE MAIN POWER FUSE aaa E I meme e hen 22222000 85 APPENDIX 2 HOW TO TRANSFER INFORMATION TO A PRINTER aaa Ie nme 002222210 87 APPENDIX HOW TO TRANSFER INFORMATION TO A COMPUTER 2 22 12 202 2202 2 22228000020 89 APPENDIXZE MOVWTOUSEA REMOTE DISPLAY ess speso sno teer tree e eee A tee Ehe te e ee 92 APPENDIX 5 HOW TO USE A REMOTE POU DISPENSER 2 22 2042 2 50 22002 92 APPENDIX6 COMP MODE AND COMP MODE 2 93 INTRODUCTION Chapter 1 INTRODUCTION 1 1 USING THIS MANUAL MATCHING THIS MANUAL WITH YOUR MiLLI Q This manual is intended for use with a Millipore Milli Q Synthesis or Milli Q Synthesis ATO Water Purification System This User Manual is a guide for use during the installation normal operation and maintenance of a Milli Q Synthesis or Milli Q Synthesis ATO Water Purification System lt is highly recommended to comple
28. is lt O C The meosured temperolure is gt 45 C The measured 25 is 2 5 resistivity valve 8 between 3 5 measured resistivity is too high gt 65 5 The displayed USING THE MILLI Q What to do Turn off the elecirical power Turn it on 20 to 30 seconds later If the message appears again then contact Millipore Replace the UV Lamp Replace the UV Lamp Contact Millipore Contact Millipore Check the feedwater temperatur lower if necessary Contact Millipore if the measured temperature is incorrect Contact Millipore for assistance Dispense water from the Milli Q to remove any air bubbles that could be resistivity may not show higher than 18 2 MQ cm The voltage being sent to the UV Ballast Power Supply on the Interface PC Board is lt 5 VDC or gt 39 VDC This is also the Power Supply for the Solenoid Valve in the POU Dispenser trapped in the Resistivity Sensor Cell Contact Millipore if the messag continues Contact Millipore 29 USING THE MiLLI Q Message and System What to do Status SYSTEM ERROR 8 The electrical intensity being sent to the Contact Millipore UV Ballast Power Supply on The POU Dispenser will not dispense Interface Board is lt 5 mA or water You will not be able to gt 950 mA This is also the Power dispense walter Supply for the Solenoid Valve
29. may be a leakage of caustic NaOH solution out the Sanitisation Port 66 A HAZARD Remove the Millipak from the POU Dispenser MAINTENANCE Make sure the Sanitisation Port Cap is tightened after putting in the Sodium Hydroxide Pellets Additionally make sure that the UF Reject Tubing is in a sink or drain and that it is fastened securely in place Q Screw the Barbed Fitting onto the end of the POU Dispenser Attach the clear Tygon Tubing to the Barbed Fitting Place the other end of the Tygon Tubing into a sink or drain Q While in STANDBY Mode press the CLEANING Keypad button for about 2 seconds The display wil as shown here STANDBY Press for about 2 seconds SAN CYCLE Wait about 10 seconds LCD will now prompt you to OPEN THE VALVE SAN CYCLE 421 mn position SAN CYCLE OPEN THE VALVE SAN CYCLE OPEN THE VALVE SAN CYCLE 420mn change Q Open the valve by moving the POU Dispenser Trigger forward Water will come out of the Tygon Tubing for a while A 421 minute timer will be shown Make sure the POU Dispenser Trigger is pulled forward If this is not done then the timer will not move from the Wait until the timer has reached 400 minutes When the timer is at 400 mn it will ask you to Close Valve Bring the POU Dispenser Trigger back to the upright position
30. see an increase in the Pressure Regulator setting while water is not flowing through it i e STANDBY or PRE OPERATE Mode The Milli Q will now go to STANDBY Mode and will remind you to close the POU Dispenser Valve Q Move the POU Dispenser Trigger back its upright position The Milli Q will now go to PRE OPERATE Mode STANDBY PRE OPERATE CLOSE THE VALVE Milli Q Synthesis ATO only When you Close The Valve the Milli Q will go to PRE OPERATE Mode and then will start an automatic 60 minute A10 CLEANING The 0 CIEANING is a way of flushing out any particles that may have been present STANDBY PRE OPERATE CLOSE THE VALVE 10 CLEANING 60 Q Milli Q Synthesis A10 only Allow the CLEANING to count down to O minutes The remaining steps of this section apply to both the Milli Q Synthesis and the Milli Q Synthesis 10 Q Any remaining air in Quantum Cartridge can be hand purged out now Q Geta screwdriver with a very thin shaft and small head Q Locate the small hole on the top part of the Quantum Cartridge Door 32 INSTALLATION Gently insert screwdriver into the Quantum Cartridge This will open a small vent that will expel any air in the Quantum Cartridge Be very careful when pushing the tip of the screwdriver into the A ATTENTION Vent Hole of the Quantum Cartridge The Vent Hole only needs to be opened a very small amoun
31. the Milli Q in PRODUCT Mode Verify that you have several Litres of feedwater i e full Reservoir or full Distribution Loop Bring the POU Dispenser Trigger down towards you You should hear a sharp click noise This is the opening of the Inlet Solenoid Valve The LCD will change and will look like PRODUCT STANDBY AIR PURGE 5 mn EB lose THE VALVE let the AIR PURGE continue for its 5 minute duration It will count down to O minutes 5 4 O mn Pressurised Feedwater Only Check the Pressure Gauge on the Pressure Regulator While water is flowing through it the Pressure Gauge should show 0 3 bar If it is not set to 0 3 bar then turn the round handle on the Pressure Regulator clockwise until the pressure gauge the regulator shows O 3 bar Check this again when water is flowing through the Pressure Regulator A ATTENTION STANDBY CLOSE THE VALVE The setting of the Pressure Regulator should not exceed 0 3 bar The feedwater pressure reaching the Milli Q in PRODUCT Mode should not exceed 0 3 bar The Pressure Regulator should only be set while water is flowing through it It is perfectly normal to see an increase in the Pressure Regulator setting while water is not flowing through it i e STANDBY or PRE OPERATE Mode The Milli Q will now go to STANDBY Mode and will remind you to close the POU Dispenser Valve Q Move the POU Dispenser Trigger ba
32. the length of the black 8 mm OD tubing will be used for the UF Reject tubing Install one end of this tubing to the Reservoir Push one end of the tubing into the collar of the fitting until it will go no further Pull on it slightly to insure it is fully seated inside the collar FEEDWATER IS FROM A PRESSURISED SOURCE SUCH AS A PIPE A LOOP a Get the roll of PTFE Tape and the 8 mm tubing plus Screen Filter from the Accessories Make sure that pipe end is a 1 2 inch NPTM connection If this connection is not ready then you will need to obtain the proper fittings to be able to attach the fittings from the Milli Q Accessories Bag Wind about 3 to 4 turns of PFTE Tape on the end of the pipe connection The tape should be wound in a clockwise direction same direction the fittings will be turned Screw the Screen Filter to the end of the pipe You may want to remove the attached 8 mm tubing to facilitate the turning of the Screen Filter Assembly Measure the distance needed for the Feedwater Tubing This is the distance between the Screen Filter and the back of the Milli Q Allow some extra distance so the Milli Q could be rotated or moved without stretching the tubing Cut the appropriate length of 8 mm tubing as determined above The remainder of the length of the black 8 mm tubing will be used for the UF Reject tubing You will now need to install the Feedwater Pressure Regulator Millipore Catalogue Number ZFMQOOO
33. to change a Q Gard Pack is based upon time calendar days with Milli Q Synthesis system The Milli Q Synthesis will indicate a message EXCH CARTRIDGES after 180 Calendar Days The Milli Q Synthesis ATO will never display a message EXCH CARTRIDGES It is up to the user to change the Q Gard Quantum and Millipak based upon resistivity and TOC values UV LAMP The dual wavelength UV Lamp emits light at 185 nm for TOC reduction and 254 nm Germicidal action The UV Lamp is used to kill bacteria and to reduce the levels of organic molecules in the water stream between the Q Gard Pack and the Quantum Cartridge The UV Lamp has a Millipore Catalogue Number of ZMQUVLPO1 WHEN DO CHANGE THE UV LAMP It is recommended to change the UV Lamp every 365 Days once per year The Milli Q LCD will show a message EXCHANGE UV after 365 Calendar Days indicating it is time to replace the UV Lamp QUANTUM The Quantum Ultrapure Cartridge is used to remove trace levels of ions and organic molecules WHAT ARE THE DIFFERENT TYPES OF QUANTUM CARTRIDGES The Quantum IX contains only Mixed Bed lon Exchange resin This type of Quantum Cartridge is used when maintaining absolutely trace levels of ions is critical The Millipore Catalogue Number for a Quantum IX is QTUMOOOIX Section 8 1 for more information The Quantum EX contains ion exchange resin and synthetic carbon These purification media are used when the Milli Q Product Water n
34. valve is only open for 30 seconds every 3 hours of PRE OPERATE Mode or when the AIR PURGE Mode is active This valve will also open for portions of the Sanitisation Mode RESISTIVITY SENSOR RESISTIVITY AND TEMPERATURE MEASUREMENTS The resistivity sensor is used to measure the electrical resistivity of the Milli Q Product Water Additionally a thermistor temperature sensor is located the resistivity sensor The temperature displayed on the Milli Q LCD during PRODUCT Mode is measured by this thermistor TEMPERATURE COMPENSATION CONDUCTIVITY MEASUREMENTS The resistivity and temperature are measured while water is flowing through the sensor The Milli Q microprocessor will then temperature compensate the resistivity to a 25 C value It is possible to use the Milli Q software to display non temperature compensated resistivity lt is also possible to display conductivity nS cm temp compensated non temp compensated on the LCD by using the Milli Q software The software be changed by using the Keypad POINT OF USE VALVE The Point Of Use POU Dispenser has a 2 way electric valve inside This valve is closed when the POU Dispenser Trigger is in the upright position This also places the Milli Q into PRE OPERATE Mode after 90 seconds if you were using the Milli Q in PRODUCT Mode When the POU Dispenser Trigger is pushed down the electric valve is powered This allows water to be dispensed out of the Milli Q System inste
35. 20 SAGA am Weigh AO A EA 20 BEEN REDDERE s 20 Feedwaler cci tert ben Cort best kaw raan 21 Environmehtadl T I MER 21 TT T m m 2 3 5 UNPACKING THE BOX WHAT SINBIDEG anasa Rea na an Ra 22 CHAPTER 4 INSTALLATION 24 4 CONNECTING TO A SUPPLY OF FEEDWATER 225 55 t ER 24 Feedwater is fom a ESEON EE 24 Feedwater is from a pressurised source such as a pipe a 24 TABLE OF CONTENTS 4 2 CONNECTION OF TUBING AND THE 2002 1505 900525512220 0 26 Feedwaler o s IPC 26 Feedwater Pressure Relief Tubing 22 2 222222 2 22 10 0 02 520222222002 2 2 Wu 26 Nr MED 27 Z EMEN NS Weemide 2e m 27 4 4 TURNING ON THE SYSTEM POWER 2 222 2 222222 30 4 5 INSTALLATION OF THE QUANTUM CARTRIDGE 2 1 22 2 2 9 5960055 2222221 30 A O INSTAUATIONCOF THE TYGON TUBING es he ete e tee eet hat recte 30 4 7 PURGING THE AIR FROM THE SYSTEM eet ee ee etri eei ere o ed iei fee bees 32 A8 FAYDRATING THE SYSTEM 33 49 INSTALLATION AND RINSING OF TH
36. CULATION press the STANDBY OPERATE Keypad Button about 2 seconds This will place the Milli Q into STANDBY Mode Then press the STANDBY OPERATE Keypad Button again The Milli Q will now be in PRE OPERATE Mode Press the MENU Keypad Button again for 2 seconds fo enter the Customer Service Software Press the MENU Keypad Button 5 times 6 times for a Milli Q Synthesis ATO LANGUAGE under SERVICE OPTIONS display INSTALLATION Press for 1 second each time PRESET VOLUME SERVICE PRINTER SERVICE AGE 5 FLOW MEASURE Stop when you see the SERVICE OPTIONS LANGUAGE ENGLISH Q Press the OPERATE STANDBY Keypad twice 2 times The RES COMP choice will be shown SERVICE OPTIONS LANGUAGE ENGLISH Press the CLEANING Keypad Button twice to change from MODE 1 to OFF Compensation will now be off SERVICE OPTIONS RES COMP MODE 1 Press OPERATE STANDBY 2 times SERVICE OPTIONS PROD UNIT MQ cm SERVICE OPTIONS RES COMP MODE 1 SERVICE OPTIONS RES COMP OFF t Press CLEANING The Resistivity Temperature 42 INSTALLATION Press the MENU Keypad Button for about 2 seconds to return to PRE OPERATE Mode SERVICE OPTIONS RES COMP OFF ree OPERATE Press MENU for about 2 seconds When the Milli Q is in PRODUCT Mode POU
37. Dispenser Trigger forward the Display will look like PRE OPERATE 31 8MO cm 15 C Note that 259C is missing in non temperature compensated display mode You have finished changing to non temperature compensated Resistivity or non temperature compensated Conductivity displays 43 INSTALLATION 4 14 HOW TO SET THE DATE AND THE TIME OF DAY The date day month year can be printed out or downloaded to a computer along with other operating data pertinent to the Milli Q The date is changed at midnight of each day The time of day is not printed out or downloaded to a computer it is used only to advance the date Follow the steps below to change the date or the time of day Press the MENU Keypad button for about 2 seconds LCD will change as shown here PRE OPERATE PRESET VOLUME 0 00 Press MENU for about 2 seconds You have entered the Customer Service Software of the Milli Q If you do not see this display then turn off then on the system power When the LCD shows PRE OPERATE and RECIRCULATION press STANDBY OPERATE Keypad Button for about 2 seconds This will place the Milli Q into STANDBY Mode Then press the STANDBY OPERATE Keypad Button again The Milli Q will now be in PRE OPERATE Mode Press the MENU Keypad Button again for 2 seconds to enter the Customer Service Software Press the MENU Keypad Button 7 times 8 times for a Mil
38. E 210 0 550 022222210 35 4 10 HOW TO CALIBRATE THE FLOWRATE FROM THE 2 222202 02222 2222222022220020220 35 4 11 HOW CHANGE THE DISPLAYED 2 0 035 2 38 4 12 HOW TO SHOW EITHER OR p S CM RESISTIVITY OR CONDUCTIVITY UNITS 39 4 13 HOW TO SHOW NON TEMPERATURE COMPENSATED RESISTIVITY OR CONDUCTIVITY VALUES 41 What is temperature compensation 7 2 02 2 0 002 0022050 0000020 41 4 14 HOW TO SET THE DATE AND THE TIME OF DAY I II supai 22200 44 CHAPTER 5 HOWTO GET WATERFROMTHEMIUFO es aal Ko hintere eniris EEEREN 46 5 2 STANDBY PRE OPERATE AND PRODUCT MODE t 48 What is STANDBY 22 2 2 2222222222222222 nsns sss III I I sss s sss ses senes sepes 48 What is PRE OPERATE Modeg aaa asnasan asas s sese es esses senes 48 Whatis PRODUCT 48 5 3 HOW TO VIEW THE RESISTIVITY TEMPERATURE AND TOC e eee ee rennen nis 49 VIEWING phot gl He 49 kn es o ETT 49 49 5 4
39. ED can be blinking The table below provides a summary of these messages what they mean and what to do when you see them You may also refer to Chapter 7 Troubleshooting for more information about these messages and other troubleshooting items Please contact Millipore if you desire more information regarding what to do when a message appears on the Milli Q Message and System Status EXCH CARTRIDGES START SANIT EXCH UF TOC 5 SETPOINT You can still use the system if the water quality resistivity and is fine for your application CARTRIDGE OUT The Milli Q will not operate This message must be resolved before th Milli Q can operate NO FEED WATER The Milli Q will not operate This Milli Q Synthesis The Q Gard and Quantum have been installed for more than 180 Calendar Days A sanitisation of the UF Cartridge should be performed This message appears because of a timer This message normally appears 4 weeks after the UF Cartridge Sanitisation previous The age of the UF Cartridge is greater than the UF Cartridge timer established in the software The displayed TOC Milli Q Synthesis ATO only is greater than the TOC Setpoint established in the software Either the Q Gard Pack or the Quantum Cartridge is not installed correctly or one of them is absent What to do Replace the Q Gard and the Quantum and the Millipak Perform Sanitisation the UF Cartridge See
40. LOWRATE FROM THE POU DISPENSER CAUSE REMEDY System is in PRE OPERATE Mode Place Milli Q into PRODUCT Mode See Section 5 1 No feedwater to the Milli Q from the Reservoir Reservoir is empty Remove the Feedwater Tubing from the Milli Q e Fitting on bottom of Reservoir is too tight gasket Confirm that there is water coming to the Milli Q fitting is flattened and restricts water flow Reservoir is located lower than the Milli Q e Kink in Feedwater Tubing e Valve on bottom of Reservoir is closed by mistake No feedwater to the Milli Q from Pressurised Pipe No water in Loop Loop Remove the Feedwater Tubing from the Milli Q Water is not pressurised in Loop Contirm there is water coming to the Milli Q Pressure Regulator on Feedwater Tubing is not adjusted to between 0 1 and 0 3 bar while water is flowing through it Milli Q in PRODUCT Mode See Section 4 7 e Pressure Regulator is installed backwards See Section 4 1 Millipak is airlocked Vent air out while system is in PRODUCT Mode See Section 4 9 Millipak is clogged and will not allow water through it e Measure water flow with and without Millipak installed Change Millipak and vent air out See Section 4 9 Screen Filter Clogged e Clean the Screen Filter See Section 6 6 Problem with internal component motor not operating Contact Millipore Inlet Solenoid Valve not opening etc Remote POU Dispenser connected wrong or
41. Maximum Feedwater Pressure lt 0 3 bar use a Pressure Regulator if necessary Minimum Feedwater Pressure gt 0 0 bar reservoir lt gt same level as the Milli Q Feedwater temperature Between 5 and 35 C Items to note about feedwater ion exchange capacity of the Q Gard Purification Pack and the Quantum Ultrapure Cartridge are a strong function of the conductivity and the dissolved gas level of the Feedwater Source Fouling Index Silt Density Index of the Feedwater when gt 5 can effect the ability of the lon Exchange Resin to remove ions TOC level of the Milli Q Product Water could be affected by the type of feedwater Contact Millipore for additional information regarding the 3 items noted just above It is highly recommended to use a feedwater source treated by RO or EDI Millipore RiOs or Elix Water Purification Systems are examples of RO or EDI feedwater sources respectively ENVIRONMENTAL REQUIREMENTS Indoor use only Storage and operating temperature 5 lt T lt 40 C Humidity Should not exceed 80 for temperatures below 31 Should stay within 50 to 80 between 31 C and C Altitude lt 2000 Meters Installation category l Pollution degree 2 OTHER REQUIREMENTS Reservoir is the feedwater source If you are using a reservoir as the feedwater source then you will need ball valve on the reservoir This ball valve is normally supplied on the standard Millipor
42. Milli Q Synthesis and Milli Q Synthesis A10 User Manual Q Notice The information in this document is subject to change without notice and should not be construed as a commitment by Millipore Corporation Millipore Corporation assumes no responsibility for any errors that might appear in this document This manual is believed to be complete and accurate at the time of publication In no event shall Millipore Corporation be liable for incidental or consequential damages in connection with or arising from the use of this manual We manufacture and sell water purification systems designed to produce pure or ultrapure water with specific characteristics uS cm T TOC CFU ml Eu ml when it leaves the water purification system provided that the Elix Systems are fed with water quality within specifications and properly maintained as required by the supplier We do not warrant these systems for any specific applications It is up to the end user to determine if the quality of the water produced by our systems matches his expectations fits with norms legal requirements and to bear responsibility resulting from the usage of the water Millipore s Standard Warranty Millipore Corporation Millipore warrants its products will meet their applicable published specifications when used in accordance with their applicable instructions for period of one year from shipment of the products MILLIPORE MAKES NO OTHER WARRANTY EXPRESSED OR
43. NCE 6 3 HOW TO REPLACE THE QUANTUM CARTRIDGE The Quantum Cartridge is replaced whenever the Q Gard Pack is replaced This is important for maintaining optimum water quality Follow the steps below to replace the Quantum Cartridge Removing the Quantum Cartridge from the Milli Q sure the Milli Q is in STANDBY Mode See Section 5 1 for more information if necessary Q Since the Q Gard was just replaced see Section 6 2 it is not necessary to release the residual water pressure in STANDBY Mode Q Open the top and bottom latches of the door on the front of the Milli Q system cabinet Fully open the door Remove the Quantum Cartridge from Milli Q Installing a new Quantum Cartridge Remove the Quantum Cartridge from its shipping box Confirm that you have the desired type of Quantum Cartridge by viewing the label on the Quantum Cartridge Remove the 2 plastic covers on the ports of the Quantum Cartridge There should be a black rubber O ring in each port Make sure these are pushed firmly in place Wet the Quantum Cartridge O rings with water It is preferable to wet them with Ultrapure Water DO NOT WET THE O RINGS WITH A LUBRICANT SUCH AS OIL OR SILICON GREASE Push the Quantum firmly into place Both the top and bottom ports of the Quantum Cartridge have to be fully seated Close the door Make sure that both the top latch and the bottom latch of the door A ATTENTION are fully closed E
44. OC 4 ppb 87 APPENDIXES WHAT DOES THE PRINTOUT LOOK LIKE An example Printout is shown here ki MILLIPORE SYSTEM SYNTHESIS 10 SERIAL N FIJW8765A PROGR VERSION V3 01 QUALITY REPORT DATE JUL 13 01 USER NAME TEMPERATURE 17 89C 25 C CORRECTION ON PRODUCT 18 2 MO cm TOC 3ppb 88 APPENDIXES APPENDIX HOW TO TRANSFER INFORMATION A COMPUTER It is possible to transfer download information to a computer from the Milli Q REQUIREMENTS NEEDED A cable is needed to connect between the Milli Q and a computer The Millipore Catalogue number for this cable is COMPCBLO1 This Computer Cable is an accessory for the Milli Q and needs to be ordered separately The computer end of this cable has 9 pin connection lt installs into either the COMI or COM2 Port of your computer HOWTO DOIT Q Connect the Computer Cable COMPCBLO1 between the Water System and the Computer The installation instrucfions are not in this manual The installation instructions come with the Computer Cable Using Windows 95 or 98 click on START then PROGRAMS then ACCESSORIES then HYPERTERMINAL Sr HyperT erminal oj x Eile Edit View Go Favorites gt i Adobe Acrobat A Fa d AutoSketch 3 Games B New Offce Document 2 DiagAndZp Z Mulimeda E Internet Explorer System Tools Opm fceDoomei
45. ODUCTION 1 3 MILLIPORE INTERNET AND EMAIL The Millipore Internet Site can be used to find addresses telephone fox numbers and other information Internet Site Address www millipore com www millipore com techservice MANUFACTURING SITE Millipore SAS 67120 Molsheim FRANCE PRODUCT INFORMATION Chapter 2 PRODUCT INFORMATION 2 1 MILLI Q PRODUCT WATER SPECIFICATIONS WATER PRODUCED BY THE MILLI Q SYNTHESIS OR SYNTHESIS A1 0 FLOWRATE IOC O 8 1 2 IPM with Millipak Express 20 Maximum 5 ppb this specification came from test conditions where a Milli Q Synthesis was fitted with a RESISTIVITY Q Gard 1 Purification Pack and a Quantum EX Minimum 18 0 259C Ultrapure Cartridge and the feedwater came from a Millipore RIOs Water System feedwater TOC value was lt 50 ppb The TOC of the Milli Q PARTICLES Product Water can vary as a function of the feedwater Typically 18 2 25 C lt 1 particle size gt 0 22 um MICRO ORGANISMS PYROGENS lt 1 CFU ml lt 0 001 Eu ml COMPARISON OF MiLLI Q WATER AND ASTM STANDARD SPECIFICATIONS Milli Q Product Water Quality will meet or exceed ASTM Type Standard Specifications for Reagent Grade Water The specifications for ASTM Type Reagent Grade Water are shown below Note that the Water Quality Specifications for a Milli Q Synthesis or Milli Q Synthesis A10 are listed in the section just above From
46. OF CONTENTS CHAPTER INTRODUCTION VV A DU Fd a d Maii Tid 1 eur NU RM cc Lc EE Matching this manual with your How to use the keypad and Comment used abbreviations in this manual A a AO dose dpt petere 2 152 SAFETY INFORMATION e tee he EO T dd Eee be 3 53 m 4 Memel na eter 4 MMVII RN T T ET PI 4 CHAPTER 2 PRODUCT INFORMATION sss ERRE VK EA KRA 5 2 PRODUCT WATER SPECIFICATIONS 2222 2 2 2 2 Water produced by the Milli Q Synthesis or Synthesis E de IMMER 5 SEMEN LP 5 TE 5 M E 5 o cM 2 Micro Organisms 1 1 5 Comparison of Milli Q Water and ASTM Standard Specifications 220220 22222222222222 2 2 SCHEMATIC OF MAIN COMPONENTS 8 2 3 DESCRIPTION OF MAIN COMPONENTS a eee 7 Inlet Solenoid Vahe os cee elie ig tnd see TETTE TTT TTT I 7 Pressure Relief VIS W Z FUMP rr P 7 SSS PUS ESTES MET D NCC PTS 7 What are different types 52
47. PERATURE The Milli Q can display various Product Water quality parameters The range of measurement of each parameter is written below Resistivity Measurement Range 2 4 18 2 compensated to 25 C values Conductivity Measurement Range 0 055 0 294 5 Temperature Measurement Range O 45 C not the system temperature operating range TOC Measurement Range 1 999 ppb PRODUCT INFORMATION MATERIALS OF CONSTRUCTION Please contact Millipore for o list of the materials of construction for wetted components NoisE LEVEL The Milli Q has a noise level of 42 dB at a distance of 1 meter away PRE INSTALLATION Chapter 3 PRE INSTALLATION 3 1 PRE INSTALLATION CHECKLIST The installation of your Milli Q will go much easier if certain pre installation requirements are met and followed The checklist below can be used to facilitate the pre installation of your Milli Q system You can refer back to this checklist as you read the sections on Optional Equipment Installation Requirements and Unpacking the Milli Q Box D D D D D D UD D D D DO O DO UD Do you have a Q Gard Purification Pack Do you have a Quantum Ultrapure Cartridge Do you have a Millipak Do you have Milli Q and all items in its Accessories Bag Do you have a source of electrical power close enough to the Milli Q 5 the electrical source earth grounded Are you feeding with a Reservoir if feeding from a pressurised pipe see bel
48. PR Locate the Pressure Regulator Turn it over so you can see the arrow that indicates the direction of water flow through the Pressure Regulator It is important not to reverse the water flow through the Pressure Regulator The Pressure Regulator is installed between the Screen Filter now attached to the pipe end and the back of the Milli Q You will check and or set the Pressure Regulator later see Section 4 7 below Normally the Millipore Pressure Regulator is pre set to 0 3 bar and will not need adjustment You may want to flow some feedwater through the tubing and Pressure Regulator to check for leaks 24 INSTALLATION CONNECTION TO A PRESSURISED PIPE 25 INSTALLATION 4 2 CONNECTION OF TUBING AND THE POWERCORD FEEDWATER TUBING a a Rotate the Milli Q so you can see the back of the system cabinet Look below the place where the Powercord would be plugged in You will see some holes ports where tubing can be plugged The large ports are 8 mm in OD The smaller ports are 6 mm in OD locate the left side 8 mm Port labelled as FEED 1 this lettering is located just above the collar of the port It may be difficult lo see unless you are close to the system Make sure the Feedwater Tubing is connected to the FEED 1 Port A ATTENTION Make sure the Feedwater Tubing is not connected to the DRAIN 3 Port the right side 8 mm OD Port Remove the red plug that is in the FEED 1 To do this pus
49. S each time LANGUAGE ENGL I SH Q Use the Arrow Keypad Buttons to change the language Q Press the MENU Keypad Button for about 2 seconds to return to PRE OPERATE Mode SERVICE OPTIONS LANGUE FRANCAIS PAUSE i e you want to see French PRE OPERATE in French Press MENU each time You have finished changing the displayed language 38 INSTALLATION 4 12 HOW TO SHOW EITHER OR HuS CM RESISTIVITY OR CONDUCTIVITY UNITS It is possible to display Conductivity Units on the Milli Q LCD Conductivity uS cm is the reciprocal of Resistivity Follow the steps below to change from a Resistivity Display to Conductivity Display Press the MENU Keypad button for about 2 seconds The LCD will change as shown here PRE OPERATE PRESET VOLUME 0 00 MEASURE Press MENU for about 2 seconds You have entered the Customer Service Software of the Milli Q If you do not see this display en turn off then on the system power When the LCD shows PRE OPERATE and RECIRCULATION press the STANDBY OPERATE Keypad Button for about 2 seconds This will place the Milli Q into STANDBY Mode Then press the STANDBY OPERATE Keypad Button again Milli Q will now be in PRE OPERATE Mode Press the MENU Keypad Button again for 2 seconds fo enter the Customer Service Software Pres
50. TE STANDBY Keypad Button for about 2 seconds This will change the Milli Q from STANDBY Mode to PRE OPERATE Mode See the drawing below for more information STANDBY PRE OPERATE is shown below PRE OPERATE on Milli E vikoj Q systems with an ATO 2 seconds 2 Move the POU Dispenser Trigger forward and then back up This will place the Milli Q in PRODUCT Mode but water will not be dispensed at the moment very small amount of water i e 5 may be dispensed out 3 lt is recommended to dispense about 150 to 200 ml of Product Water to the drain or into a sink every morning After this use the Milli Q Product Water for your specific application NOTE If you are using the Milli Q frequently i e few times an hour then you will not have to dispense 150 to 200 ml of Product Water to the drain 4 When the green LED stops blinking move the POU Dispenser Trigger forward to dispense water It will stop blinking when the Product Water Resistivity compensated to 25 C is greater than the Resistivity Setpoint and less than the setpoint ATO system only Normally the Resistivity Setpoint is 16 0 It is recommended but not necessary to wait until the green LED stops blinking on the POU Dispenser 5 The Milli Q will dispense water continuously for a maximum of 30 minutes After 30 continuous minutes the Milli Q will stop dispensing water and will go into STANDBY Mode Contact
51. ach latch should click when it is fully closed The Quantum Cartridge is now installed You now need to perform an AIR PURGE with the Milli Q system in order to remove all air from the newly installed Q Gard Quantum Remove the used Millipak from the POU Dispenser locate the clear Tygon Tubing and the Barbed Fitting from the Accessories Bag Q Screw the Barbed Fitting onto the bottom end of the POU Dispenser Do not use any PTFE Tape on the threads of the Barbed Fitting An O ring is located inside the POU Dispenser to insure water tightness A ATENTON between the threads of the POU Dispenser and the Barbed Fitting Push one end of the Tygon Tubing onto the end of the Barbed Fitting Place the other end of the Tygon Tubing into a sink a this time you should have installed the Q Gard Pack Quantum Cartridge Barbed Fitting and the Tygon Tubing The system power should be on The POU Dispenser Trigger should be upright The LCD should be showing STANDBY 60 MAINTENANCE Put the Milli Q into PRE OPERATE Mode Press the OPERATE STANDBY Keypad Button for about 2 seconds This will change the Milli Q from STANDBY Mode to PRE OPERATE Mode the drawing below for more information STANDBY Move the POU Dispenser Tri PRE OPERATE OPEN THE VALVE PRE OPERATE OPEN THE VALVE Press for about 2 seconds er forward This will place
52. ad of being recirculated back to the pump see flow diagram PRODUCT INFORMATION MILLIPAK The Millipak Final Filter is membrane based filter that removes all particles and bacteria with a size greater than 0 22 um by a sieving mechanism All contaminants larger than the filter pore size are retained on its surface This essentially will block and retain any bacteria present in the water flowing through it WHAT TYPES OF MILLIPAK FILTERS ARE THERE There are 2 types of Millipak Filters sometimes called the Final Filter The Sterile Millipak 40 is generally used for some Life Science applications This has a Millipore Catalogue Number of MPGLOASK2 See Section 8 1 for more information The Non Sterile Millipak Express 20 is generally used for Analytical Science Applications including applications where trace levels of Volatile Organic Compounds are desired or with Life Science Applications where Endocrine Disrupter Analysis is being done The Non Sterile Millipak Express 20 has a Millipore Catalogue Number of MPGPO2001 See Section 8 1 for more information WHEN DO CHANGE THE MILLIPAK The Millipak is changed when the Q Gard Purification Pack and the Quantum Ultrapure Cartridge are changed However it may be necessary to change the Millipak if it becomes clogged with particles or bacteria and reduces the flowrate of Milli Q Product Water PRODUCT INFORMATION Q GARD QUANTUM MILLIPAK Milli Q Synthesis Synthesis ATO 11
53. alue measured is out of range 18 2MQ cm 25 C 18 2 25 C TOC 4 ppb C TOC 6 ppb s ABOUT 5 MINUTES h AFTER ENTERING This is the previously measured PRODUCT A new TOC value is displayed after 10 TOC Analysis Cycle This TOC valve lt was just measured in PRODUCT Mode cycle will continue while the Milli Q is in PRODUCT Mode or it was measured in the last hour of PRE OPERATE Mode 49 USING THE MiLLI Q 5 4 HOW TO USE THE FOOTSWITCH OPTIONAL ACCESSORY The Footswitch is an optional accessory the Milli Q system The instructions for installing the Footswitch are inside the shipping box of the Footswitch and are not in this manual The Footswitch can be installed so that you can have either Hands Free operation of the POU Dispenser that comes with the Milli Q system Hands Free operation of a Remote POU Dispenser another accessory It is not possible to have one Footswitch controlling 2 different POU Dispensers It is not possible to have two different Footswitches on a single Milli Q System The Milli Q will go from PRE OPERATE Mode to PRODUCT Mode when the Footswitch is depressed The Milli Q will remain in PRODUCT as long as the Footswitch is depressed When the Footswitch is released the Milli Q will go back to PRE OPERATE Mode after 90 seconds 5 5 HOW TO DISPENSE AN EXACT AMOUNT OF PRODUCT WATER It is possible to dispense pre set
54. be very dangerous for your eyes and for your skin Wear Eye Safety Glasses and Laboratory Gloves and other appropriate safety equipment when working with Sodium Hydroxide SANITISING AND CLEANING THE UF CARTRIDGE a Place the Milli Q into STANDBY Mode See Section 5 1 if you need further instructions on how to do this click will be heard and water will flow for a few seconds out of the UF Reject tubing While in STANDBY Mode move the POU Dispenser Trigger forward This will open the electric valve inside POU Dispenser Any residual water pressure will be released Allow any water to flow from the POU Dispenser in STANDBY Mode Move the POU Dispenser Trigger back to the upright position Locate the Removal Tool from the Accessories Bag Locate the Sanitisation Port Cap on the top of the Milli Q system It is located towards the back top end of the system cabinet Unscrew the cap using the Sanitisation Port Removal Tool found in the Accessories Bag Place 3 grams of Sodium Hydroxide crystals pellets in the Sanitisation Port Screw the cap back on Do not use the Removal Tool to tighten the Sanitisation Port Cap It may overtighten it There are 2 rubber O rings which provide a seal to prevent water leakage Handtighten the cap until it will not turn any further f the cap is overtightened then it may become very difficult to remove it later for the next Sanitisation If the cap is not tight enough then there
55. bed Fitting and the Tygon Tubing The system power should be on The POU Dispenser Trigger should be upright The LCD should be showing PRE OPERATE Verify that you have several litres gt 15 Litres of feedwater i e full Reservoir or full Distribution Loop Open any valves on the feedwater supply i e valve on the bottom of the Reservoir Q Bring the POU Dispenser Trigger down towards you You should hear a sharp click noise This is the opening of the Inlet Solenoid Valve Water will start flowing out of the UF Reject tubing Q The LCD will change and will look like PRE OPERATE PRODUCT STANDBY OPEN THE VALVE AIR PURGE 5 mn CLOSE THE VALVE Let the AIR PURGE continue for its 5 minute duration It will count down to O minutes 5 4 mn Pressurised Feedwater Only Check the Pressure Gauge on the Pressure Regulator While water is flowing through it the Pressure Gauge should show 0 3 bar If it is not set to 0 3 bar then tum the round handle the Pressure Regulator clockwise until the pressure gauge the regulator shows 0 3 bar Check this again when water is flowing through the Pressure Regulator The setting of the Pressure Regulator should not exceed 0 3 bar The feedwater pressure reaching the Milli Q in PRODUCT Mode should not exceed 0 3 bar The Pressure Regulator should only be set while water is flowing through it It is perfectly normal to
56. ccessfully for 15 minutes e off then on the electrical power to the Milli Q e Contaci Millipore if this frequently occurs EXCHANGE A10 UV e The small UV Lamp on the TOC Monitoring Device has been installed for 365 Days e You can continue to use the system to produce high quality water until the UV Lamp is replaced EXCH UF CARTR e You can continue to use the system to produce high quality water Contact Millipore OTHER TROUBLESHOOTING ITEMS TROUBLESHOOTING WHAT HAPPENED REMEDY Nothing shows up on the Printer System stops dispensing wqter qfter 30 minutes Water drips out of the Millipak when you back to PRE OPERATE Mode from PRODUCT Mode You have used the automatic volume dispenser feature see Section 5 5 The dispensed volume is not accurate The displayed TOC is xxx ppb The Printer will not print out Temperature and Resistivity values unless the system is in PRODUCT Mode Wrong Baud Setting on Milli Q Contact Millipore The Printer is not plugged into the Milli Q system Perfectly normal The Milli Q will stop dispensing water from the POU after 30 continuous minutes Contact Millipore if you want to dispense water for more than 30 continuous minutes There is air in the Millipak Vent the air out Calibrate the Flowrate of Product Water Purge air from the Quantum Cartridge Vent the Millipak of trapped air The measured TOC value is out of range gt 999
57. ced later The Q Gard is now installed 27 FEEDWATER TUBING CONNECTION lAT 250 V INSTALLATION T 250 V 28 INSTALLATION OF THE INSTALLATION Milli Q Synthesis Synthesis 29 INSTALLATION 4 4 TURNING ON THE SYSTEM POWER Q Turn on the Milli Q system electrical power The Power Switch is located on the rear of the Milli Q system cabinet The is the on position of the Power Switch Make sure the POU Dispenser Trigger is in the upright position When the system power is on but the Quantum Cartridge is not installed the LCD should look like NOTE The display messages may be in English on your Milli Q system go to Section 4 11 to change your display language SYNTHESIS V3 03 PRE OPERATE SR NO 6 45 37 RECIRCULATION The RECIRCULATION System type software version display appears for and serial number displayed for PRE OPERATE only 5 minutes about 10 seconds CARTRIDGE OUT The Red ALARM LED will be flashing 4 5 INSTALLATION OF THE QUANTUM CARTRIDGE Q locate the 2 latches on the front door of the Milli Q Cabinet Push each latch to the left and then open the door Q Remove the 2 yellow plastic inserts that are inside Pull them out and remove them Remove the Quantum Cartridge from its shipping box Confirm that you have the desired type of Quantum Cartridge by viewing the label on the top of the Qua
58. ck its upright position The Milli Q will now go to PRE OPERATE Mode PRE OPERATE MAINTENANCE Milli Q Synthesis A10 only When you Close The Valve the Milli Q will go to PRE OPERATE Mode and then will start an automatic 60 minute CLEANING The CLEANING a way of flushing out any particles from A10 that may have been present Milli Q Synthesis A10 only Allow the ATO CLEANING to count down to O minutes The remaining steps of this section apply to both the Milli Q Synthesis and the Milli Q Synthesis ATO Q Any remaining air in Quantum Cartridge can be hand purged out now STANDBY PRE OPERATE CLOSE THE VALVE A10 CLEANING 60 Q Geta screwdriver with a very thin shaft and small head Q Locate the small hole on the top part of the Quantum Cartridge Door Q Gently insert the screwdriver into the Quantum Cartridge This will open a small vent that will expel any air in Quantum Cartridge Be very careful when pushing the tip of the screwdriver into the A ATTENTION Vent Hole of the Quantum Cartridge The Vent Hole only needs to be opened a very small amount Ifall of the air does not expel out do not worry You can repeat this step later after more water has flowed through the Milli Q Remember to have the Milli Q in STANDBY or PRE OPERATE Mode You now need to allow the Q Gard Pack and the Quantum Cartridge to hydrate overnight This h
59. e 30 or 60 litre or 100 litre Reservoirs The end of the ball valve should terminate with a fitting that accepts 8 mm tubing This fitting is not supplied on the standard Millipore 30 Litre or 60 Litre or 100 Litre Reservoirs You can order a fitting from Millipore with a 1 4 inch NPTM connection on one end and an 8 mm tubing insert on the other Contact Millipore if your reservoir has another thread size on the port you want to use for the feedwater connection to the Milli Q PRE INSTALLATION 3 5 UNPACKING THE MILLI Q BOX WHAT S INSIDE Open the Milli Q Shipping Box Use the checklist and illustrations below to make sure all items were shipped and are accounted for It is highly suggested to become familiar with the items that are shipped in the Accessories Bag since these will be used in the Installation Section of this manual Check box item is present Contact Millipore if an item is missing Do you have Milli Q Water Purification System a Electrical Powercord Inside the Accessories Bag Black Tubing 8 mm OD about 5 meters in length An assembly of blue fittings is attached to one end of this tubing The assembly of blue fittings has a Screen Filter inside The term Screen Filter will be used for the remainder of this manual to refer to the assembly of blue fittings Fitting 1 4 inch NPTM one end and a hose barb on the other end Clear Tygon Tubing Roll of PTFE Tape D o DO 3 E
60. e Q Gard Pack the Quantum Cartridge Millipak and the UV lamp The Milli Q Synthesis ATO has 5 consumable items These include the UV Lamp plus the Q Gard Pack the Quantum Cartridge Millipak and the UV Lamp The age of these consumables can be viewed The age of a consumable is the number of calendar days that have passed since the consumable was installed The age is displayed as a number of days The number of days will increase by 1 every 24 hours The maximum recommended age of the Q Gard Quantum and Millipak is 180 days The maximum recommended age of the A10 UV Lamp is 365 days The maximum recommended age of the UV Lamp is 365 Days 1 year Follow the steps below to view the age of the consumable items Press the MENU Keypad button for about 2 seconds LCD will change as shown here PRE OPERATE PRESET VOLUME 0 00 Press MENU for about 2 seconds You have entered the Customer Service Software of the Milli Q If you do not see this display then turn off then on the system power When the LCD shows PRE OPERATE and RECIRCULATION press the STANDBY OPERATE Keypad Button for about 2 seconds This will place the Milli Q into STANDBY Mode Then press the STANDBY OPERATE Keypad Bulton again The Milli Q will now be in PRE Mode Press the MENU Keypad Button again for 2 seconds to enter the Customer Service Software Press the MENU Keypad Button 2 times
61. e sure the electrical power is off to the Milli Q system The Q Gard is installed on the Milli Q front right side Locate the white Q Gard Pack Adapter lid Look below the lid and locate the 2 yellow plastic inserts Pull them out and remove them Remove the Q Gard from its shipping box Verify the Millipore Catalogue Number by looking at the sticker top of the Q Gord The sticker should be blue Remove the plastic covers on the 2 ports of the Q Gard Pack Look inside the ports to locate the black rubber O rings Make sure these are pushed so they are firmly in place Wet the Q Gard O rings with water lt is preferable to wet them with ultrapure water DO NOT WET THE O RINGS WITH A LUBRICANT SUCH AS OIL OR SILICON GREASE Locate the small protruding piece of plastic near the bottom of the Q Gard Push this into the small hole in the Milli Q Cabinet This will aid in holding the Q Gard Pack upright Push the Q Gard Pack onto the Pack Adapter The Q Gard Pack rubber O rings will be making a water tight seal lt is important that the Q Gard is pushed in fully The notch on the end of the metal rod on the Pack Adapter should come through the hole on the Q Gard Pack Locate the metal clip that is attached to the Pack Adapter with a piece of filament wire Push the metal clip onto the notch of the metal rod see the step above The top of the Metal clip should bend towards you This will allow you to easily remove it when the Q Gard is repla
62. e than 30 continuous minutes During PRODUCT Mode there is no water coming out of the UF Reject tubing on the back of the Milli Q system 48 USING THE MILLI Q 5 3 HOW TO VIEW THE RESISTIVITY TEMPERATURE AND TOC VIEWING RESISTIVITY The Resistivity 25 C of the Milli Q Product Water is seen while the Milli Q is in PRODUCT Mode 18 2MQ cm 25 C 18 2MQ cm 25 C TOC 3 ppb Milli Q Synthesis PRODUCT Milli Q Synthesis in Mode PRODUCT Mode VIEWING TEMPERATURE Press the MEASURE Button while the Milli Q is in PRODUCT Mode 18 2 25 C TEMP 19 1 C TOC 4 ppb 4 Milli Q Synthesis or Milli Q Synthesis A 10 in PRODUCT Mode Milli Q Synthesis or Milli Q Synthesis A10 showing the PRESS MEASURE The temperature will be displayed for about 10 seconds LCD will return to the resistivity display VIEWING TOC is only displayed if you have a Milli Q Synthesis 10 system The TOC of the Milli Q Product Water is measured about every 5 minutes When you go from PRE OPERATE Mode to PRODUCT Mode a TOC Analysis is started The displayed TOC will not change until the next TOC Analysis is completed The TOC measurements will be repeated continuously during PRODUCT Mode The range of TOC values is from 1 ppb to 999 ppb in 1 ppb increments A display of ppb means that the TOC v
63. eeds to have both trace levels of ions and trace levels of organic species The Millipore Catalogue Number for a Quantum EX is QTUMOOOEX See Section 8 1 for more information The Quantum VX contains media that removes Volatile Organic Carbon species and maintains trace levels of ions The Millipore Catalogue Number for a Quantum VX is QTUMOOOVX See Section 8 1 for more information WHEN DO CHANGE THE QUANTUM ULTRAPURE CARTRIDGE It is recommended to change the Quantum Ultrapure Cartridge when the Q Gard Purification Pack is changed See When do change the Q Gard Purification Pack see the section above for more information PRODUCT INFORMATION PYROGARD 5000 UF CARTRIDGE Pyrogard 5000 UF Cartridge called UF Cartridge in the remainder of this manual is used to remove any Pyrogens or Endotoxins in the Milli Q Product Water The UF Cartridge will also remove bacteria from the water passing through it The maintenance of the UF Cartridge involves sanitising and cleaning it every 4 weeks with Sodium Hydroxide The Sanitisation of the UF Cartridge is described in the Maintenance Chapter of this manual The UF Cartridge has a Reject Water Stream which is plumbed via a piece of 8 mm OD tubing from the back of the Milli Q to a sink or a drain This stream is used to transport the bacteria pyrogens particles that are rejected by the UF Cartridge The flow through this piece of tubing is controlled by a solenoid valve This
64. elps to produce high quality Product Water a Ar this time the Millipak is not installed The Barbed Fitting and Tygon Tubing should still be attached to the end of the POU Dispenser Q Leave the Milli Q in PRE OPERATE Mode overnight or for several hours This will aid in rinsing off the purification media inside the Q Gard Pack and the Quantum Cartridge The next morning Bring the POU Dispenser Trigger forward to put the Milli Q into PRODUCT Mode Allow about 10 to 15 litres 7 to 10 minutes of PRODUCT Mode of water to be dispensed from the Milli Q Bring the POU Dispenser Trigger upright The Milli Q will go into PRE OPERATE Mode after 90 seconds Leave the Milli Q in PRE OPERATE Mode The Q Gard Pack and Quantum Cartridge are now fully air purged and hydrated D D DO D Proceed to Section 6 4 for instructions on installing the Millipak 62 MAINTENANCE INSTALLATION OF THE QUANTUM CARTRIDGE Milli Q Synthesis Synthesis ATO 63 INSTALLATION OF BARBED FITTING AND TYGON TUBING MAINTENANCE PURGING AIR FROM THE QUANTUM CARTRIDGE 64 MAINTENANCE 6 4 HOW TO REPLACE THE The Millipak is normally replaced when the Q Gard Pack and Quantum Cartridge are replaced The Millipak may need to be replaced at an earlier time if it becomes clogged clogged Millipak will considerably reduce the Milli Q Product Water flowrate Follow the steps below to replace the Millipak Make su
65. eneric immunity standard EN 61000 3 2 1995 and A2 1998 A14 2000 Electromagnetic compatibility Part 3 2 limits Limits for harmonic current emissions equipment input current up to and including 16A per phase EN 61000 3 3 1995 Electromagnetic compatibility 3 limits Section 3 limitation of voltage fluctuation and flicker in low voltage supply systems for equipment with rated current inferior or equal EN 61010 1 1993 A2 1995 Safety requirements for electrical equipment measurement control and laboratory use Guy REYMANIN Quality Assurance Manager Millipore S A S Milli Q Synthesis Milli Q Synthesis ATO Directive 2002 96 EC For European users only The symbol crossed bin on a product or its packaging indicates that the product should not be treated like household waste when discarded Instead the product should be disposed of at a location that handles discarded electric or electronic equipment Proper disposal of equipment containing electric or electronic components will help to reduce pollution effects to the environment or to human health Proper recycling of these products helps in environmental preservation and helps to protect natural resources For more information about recycling of products containing electric or electronic components please contact your local recycling representative or organisation Milli Q Synthesis Milli Q Synthesis ATO TABLE
66. g Box Q Apply 3 4 turns of new PTFE Tape to the threads of the Feedwater Pipe Apply the tape in a clockwise direction Screw the Screen Filter back onto the Feedwater Supply Pipe Attach the Feedwater Tubing back onto the Barbed Fitting Make sure the tubing is securely fastened Open the Feedwater Supply Valve Q Place the Milli Q into PRODUCT Mode to dispense some water from it See Section 5 1 for more information on how to do this During this time check the setting of the Feedwater Pressure Regulator It should be set to a value between 0 1 bar and 0 3 bar Leave the Milli Q in PRE OPERATE Mode when you are done dispensing water You have finished cleaning the Screen Filter 70 MAINTENANCE SCREEN FILTER CLEANING TIGHTENING OF THE POU DISPENSER ARM Milli Q Synthesis Synthesis ATO Z MAINTENANCE 6 7 HOW TO TIGHTEN THE POU DISPENSER ARM The POU Dispenser Arm is moved up and down during the times that water is dispensed from the Milli Q System Follow these instructions to tighten the POU Dispenser Arm locate the Allen Wrench 6 sided black wrench from the Accessories Bag from the Shipping Q Locate the 2 bolts that hold the various pieces of the Dispenser Arm in place Tighten these bolts until the arm is secure You have finished tightening the POU Dispenser Arm 6 8 HOW TO REPLACE THE A10 UV LAMP The ATO UV lamp is normally replaced once a year every 365 Days
67. h in on the collar that holds the plug in place At the same time pull the red plug out Locate the elbow shaped fitting from the Accessories Bag Install it into the FEED 1 Port Push it in all the way The use of this elbow fitting will allow the tubing to fit better especially if the system is wall mounted Plug the Feedwater Tubing into the elbow fitting installed in the FEED 1 Port If your feedwater is a reservoir then plug in the end of the tubing that is originally attached to the bottom of the Reservoir If your feedwater is from a Pressurised Pipe then plug in the end of the tubing that is initially attached to the outlet of the Pressure Regulator FEEDWATER PRESSURE RELIEF TUBING This procedure does not need to be done if the Milli Q is being fed from a Reservoir It is highly recommended to perform this procedure if the Milli Q is being from a pressurised source such as a loop a a a a D Locate the roll of clear mm OD tubing thot came in the Accessories Bag Locate the smallest elbow shaped fitting from the Accessories Bag Locate the OUT 5 Port on the back of the Milli Q Synthesis or Milli Q Synthesis system Install the 6 mm Elbow into the OUT 5 Port Push it in all the way The use of this elbow fitting will allow the tubing to fit better especially if the system is wall mounted Plug the clear 6 mm OD tubing into the elbow fitting Place the other end of the clear mm OD tubing into a sink o
68. he PRE SET VOLUME value 50 USING THE MILLI Q Press the OPERATE STANDBY Keypad Button to validate your volume selection The Milli Q will now go to PRE OPERATE Mode PRESET VOLUME 6 50 PRE OPERATE OPERATE STANDBY Move POU Dispenser Trigger forward The Milli Q will go from PRE OPERATE Mode to PRODUCT Mode The LCD will show lower right corner the amount of water being dispensed PRE OPERATE A counter shows the total volume being dispensed 0 02 litres at this time D Allow the water to be dispensed D You can cancel the dispensing of water by moving the POU Dispenser Trigger upright back to the PRE OPERATE position Q When the pre set total volume of water has been dispensed from the Milli Q the system will automatically go to STANDBY Mode The LCD will prompt you to CLOSE THE VALVE o Bring the POU Dispenser Trigger to the upright position The Milli Q will now be in PRE OPERATE Mode 18 2 25 STANDBY PRE OPERATE 6 501 CLOSE THE VALVE If you want to automatically dispense the same volume of water again then follow all of the steps above You will not need to change the selected volume It will remain the same from the prior selection D USING THE MiLLI Q 5 6 HOW TO VIEW THE AGE OF THE CONSUMABLES The Milli Q Synthesis has 4 consumoble items These include th
69. ide below for the typical maintenance that needs be performed on your Milli Q Synthesis or Milli Q Synthesis ATO The Catalogue Numbers and other ordering information can be found in Sections 8 1 and 8 2 Detailed information about the various consumable items can be found in Sections 2 2 and 2 3 Item or action Maintenance How to needed Q Gard Pack Replacement When the system resistivity or See Section 6 2 TOC values are outside of specification or the EXCH CARTRIDGE message displayed Quantum Cartridge Replacement Replace when the Q Gard Pack See Section 6 3 is replaced Millipak Replacement Replaced when the Quantum See Section 6 4 Cartridge and Q Gard Pack are replaced or when the Product Water Flowrate drops Sanitisation and cleaning of Cleaning Every 4 weeks See Section 6 5 the UF Cartridge Screen Filter 2 times a year or as necessary See Seclion 6 6 Flow Calibration Perform a calibration When the Millipak is See Section 4 11 replaced After an AIR PURGE After a dirty UF Cartridge is cleaned Periodically POU Dispenser Arm Tightening See Section 6 7 A10 UV Every 365 Days See Section 6 8 A10 Cleaning Perform a cleaning Automatic when the Quantum is See Section 6 9 replaced necessary Air Purge of UF Cartridge Perform an Air Purge Automatic when the Quantum is See Section 6 10 replaced necessary UV Lamp Every 365 Days See Section 6 11 57 MAINTENANCE 6 2 HOW TO
70. ify the Millipore Catalogue Number by looking at the sticker on top of the Q Gard Remove the plastic covers on the 2 ports of the Q Gard Pack Look inside the ports to locate the black rubber O rings Make sure these are pushed in so they are firmly in place Wet the Q Gard O rings with water It is preferable to wet them with Ultrapure Water DO NOT WET THE O RINGS WITH A LUBRICANT SUCH AS OIL OR SILICON GREASE Locate the small protruding piece of plastic near the bottom of the Q Gard Push this into the small hole in the Milli Q Cabinet This will aid in holding the Q Gard Pack upright Push the Q Gard Pack onto the Pack Adapter The Q Gard rubber O rings will be making a water tight seal It is important that the Q Gard is pushed in fully The notch on the end of the metal rod on the Pack Adapter should come through the hole on the Q Gard Pack locate the metal clip that is attached to the Pack Adapter with a piece of filament wire Push the metal clip onto notch of the metal rod see the step above The top of the metal clip should bend towards you This will allow you to easily remove it when the Q Gard is replaced later The Q Gard is now installed Since the Quantum Cartridge is replaced whenever a Q Gard Pack is replaced roceed to Section 6 3 How to replace the Quantum Cartridge 58 INSTALLATION OF THE MAINTENANCE Milli Q Synthesis Synthesis 59 MAINTENA
71. in the POU Dispenser SYSTEM ERROR 10 error occurred with data transfer to Turn off the Milli Q Turn it back on or from the Milli Q microprocessor about 20 to 30 seconds later If the message continues then contact Millipore A10 ERROR O A10 PCB E Prom defective off on the Milli Q and dispense water for gt minutes If the message continues contact Millipore A10 ERROR 1 A10 PCB A D converter defective off on the Milli Q and dispense water for gt minutes If the message continues contact Millipore A10 ERROR 2 A10 Thermistor defective off on the Milli Q and dispense water for gt 6 minutes If the message continues contact Millipore A10 ERROR 3 Problem occurred with temperature Tum off on Milli Q and dispense compensation water for gt minutes If the message continues contact Millipore A10 ERROR 4 The water entering the ATO is 4 Contact Millipore A10 ERROR 5 The water entering the ATO is Contact Millipore gt 41 C 10 ERROR 6 conductivity of the water entering Contact Millipore the ATO is gt 1 1 uS cm A10 ERROR 7 The temperature inside the ATO during Contact Millipore its analysis mode reached gt 55 C A10 ERROR 9 The is very low or a problem Contact Millipore occurred with the ATO 56 MAINTENANCE Chapter 6 MAINTENANCE 6 1 MAINTENANCE SCHEDULE See the Maintenance Gu
72. ious components such as the Q Gard Purification Pack and the Quantum Ultrapure Cartridge Q GARD The Q Gard Purification Pack is used to remove ions and organic molecules from the feedwater The Q Gard is a consumable device A consumable device is something that is periodically changed out for a new one during the maintenance of the Water System WHAT ARE THE DIFFERENT TYPES OF Q GARDS The Q Gard 1 is used when the feedwater comes from RO distillation or Electrodeionisation EDI An example of RO or EDI feedwater is the water coming from either a Millipore RiOs or Elix Water Purification System This type of feedwater typically has some ions but contains little organic particulate and colloidal contamination The Millipore Catalogue Number for a Q Gard 1 is See Section 8 1 for more information The Q Gard 2 is used whenever the feedwater comes from a source other than those mentioned above An example of feedwater requiring a Q Gard 2 would be Service Deionised Water this is the process of deionising water by connecting bottles of ion exchange directly to tap water and deionising the tap water Deionised Water produced by multiple regeneration ion exchange resins may have a high level of organic particulate and colloidal contamination The Millipore Catalogue Number for a Q Gard 2 is QGARDOOD2 See Section 8 1 for more information PRODUCT INFORMATION WHEN DO CHANGE THE Q GARD PURIFICATION PACK The decision
73. istered trademarks of Millipore Corporation Quantum and RiOs are trademarks of Millipore Corporation A10 is a registered trademark of Millipore Corporation Tygon is a registered trademark of the Norton Company ASTM is a registered trademark of the American Society for Testing and Materials Allen is a registered trademark of the Holo Krome Technology Corporation Windows and EXCEL are registered trademarks of Microsoft Corporation All other trademarks are trademarks of their respective manufacturers Milli Q Synthesis Milli Q Synthesis ATO Milli Q Synthesis and Milli Q Synthesis A10 DECLARATION OF CONFORMITY EUROPEAN UNION EC DIRECTIVES C Directive 89 336 CEE Directive 73 23 CEE The system mentioned above is manufactured in Millipore SAS 67120 Molsheim FRANCE facilities whose quality management system is approved by an accredited registering body to the ISO9001 Quality System Standards e We certify that these lab Water Systems are designed and manufactured in application of the following European Council directives 89 336 CEE relating to Electromagnetic compatibility 73 23 relating to electrical equipment designed for use within certain voltage limits Standards to which conformity is declared as applicable are the following EN 55022 Classe B 1998 limits and method of radio disturbance characteristics of information technology equipment EN 50082 1 1997 Electromagnetic compatibility g
74. lay APPENDIX 5 HOW TO USE A REMOTE POU DISPENSER The Remote POU Dispenser is an accessory that allows you to dispense Milli Q Product Water up to 2 5 meters away from the Milli Q system The Remote POU Dispenser uses the same POU Device found on the front of the Milli Q The Remote POU Dispenser Arm is fixed to a Base The Base can be wall mounted or the Base can be fitted with a metal weight for placement on a table or countertop The Millipore Catalogue Number for a Remote POU Dispenser is ZMQSPOURI It is also necessary to have an Installation Kit for the Remote POU Dispenser This kit allows an interface between the Remote POU Dispenser and the Milli Q The Millipore Catalogue Number for the Remote POU Dispenser Installation Kit is ZMQSPOU01 The installation instructions for the Remote POU Dispenser are not included with this manual These instructions are included with the Remote POU Dispenser Please contact Millipore if you would like a copy of these instructions ahead of time The use of the Remote POU Dispenser is exactly the same as one mounted on the Front of the Milli Q Cabinet It is suggested to recalibrate the flowrate from the Milli Q if you are using the Remote POU Dispenser more often than the Front POU Dispenser The flowrate from the Remote POU Dispenser may be slightly lower than from the Front POU Dispenser 92 APPENDIXES APPENDIX 6 COMP MODE 1 AND MODE 2 Section 4 13 in this manual explains how to dis
75. lbow shaped fittings black with yellow coloured collar one fitting will be smaller than the other two fittings Allen Wrench 6 sided black wrench Removal Tool used to remove the Sanitisation Port on top of the system cabinet Clear tubing 6 mm about 2 5 meters in length 22 PRE INSTALLATION ACCESSORIES SAN PORT REMOVAL TOOL Milli Q Synthesis Synthesis 23 INSTALLATION Chapter 4 INSTALLATION 4 1 CONNECTING TO A SUPPLY OF FEEDWATER FEEDWATER IS FROM A RESERVOIR a Make sure the Reservoir is full of purified water i e RO or water Make sure the Milli Q is located either beside or lower than the Reservoir lt is not advisable to locate the Reservoir below the Milli Q you are using 30 or 60 100 Reservoir from Millipore then install connector fitting which is 1 4 inch NPTM on one end and has an 8 mm tubing insert collar on the other end This connector fitting should be installed on the middle valve located on the bottom side of the 30 60 100 litre Reservoir The Millipore fitting referenced above has an O ring on its thread You will not need to use PTFE Tape on this fitting Simply screw this connector into place Measure the distance between the Reservoir and the back of the Milli Q Allow some extra distance so the Milli Q could be rotated or moved without stretching the tubing Cut an appropriate sized length of the black 8 mm OD tubing The remainder of
76. li Q Synthesis ATO Stop when you see the CALENDAR display PRESET VOLUME SERVICE PRINTER SERVICE AGE SERVICE CALIB FLOW MEASURE Press MENU SERVICE OPTIONS eoch time SERVICE UF CALENDAR 09 07 WED AUG 1 01 Hour will be flashing Hour is flashing CALENDAR 07 1701 WED AUG 44 INSTALLATION Chonge the Hour by using the MEASURE or CLEANING Keypad Buttons CALENDAR 09 07 WED AUG 1 01 CALENDAR 10 07 WED AUG 1 01 increase the Hour Press the OPERATE Keypad Button to validate select the Hour The Minutes will now be flashing CALENDAR 7907 WED AUG 1 01 CALENDAR 10 07 WED AUG 1 01 Minutes flashina Repeat the two steps above to change the Day Of Week the Month the Day and the Year When you are finished press MENU for more than 2 seconds to go back to PRE OPERATE Mode CALENDAR 10 07 WED AUG 1 01 PRE OPERATE You have finished setting the Date and the Time Of Day 45 USING THE MiLLI Q Chapter 5 USING THE MiLLI Q 5 1 HOW GET WATER FROM THE MILLI Q These instructions are written for the Milli Q user who already has completed all of the installation steps Chapter 4 1 Make sure the Milli Q is PRE OPERATE Mode f the Milli Q is in STANDBY Mode then press the OPERA
77. librating the Product Water Flowrate from the Milli Q See the MAINTENANCE Chapter see Chapter 6 of this manual to see when to perform a Flow Calibration 37 INSTALLATION 4 11 HOWTO CHANGE THE DISPLAYED LANGUAGE It is possible to have different languages displayed These include English French Spanish German Italian Japanese and Portuguese If you change the displayed language remember that the Customer Service Software remains in English Follow the steps below to change the displayed language Press the MENU Keypad button for about 2 seconds LCD will change as shown here PRE OPERATE PRESET VOLUME 0 00 4 Press MENU for about 2 seconds You have entered the Customer Service Software of the Milli Q If you do not see this display then turn off then on the system power When the LCD shows PRE OPERATE and RECIRCULATION press the STANDBY OPERATE Keypad Button about 2 seconds This will place the Milli Q into STANDBY Mode Then press the STANDBY OPERATE Keypad Button again The Milli Q will now be in PRE OPERATE Mode Press the MENU Keypad Button again for 2 seconds fo enter the Customer Service Software Press the MENU Keypad Button 5 times 6 times for a Milli Q Synthesis 10 Stop when you see the LANGUAGE under SERVICE OPTIONS display PRESET VOLUME SERVICE PRINTER SERVICE AGE SERVICE CALIB FLOW MEASURE Press MENU SERVICE OPTION
78. lipak The Millipak should be turned until it is handtight Do not overtighten the Millipak Do not use PTFE Tape on the threads of the Millipak The POU A ATTENTION Dispenser has an O ring inside which provides q watertight seal D Move the POU Dispenser Trigger forwards This will bring the Milli Q system into PRODUCT Mode D Locate the air vent valve on the top side clear side of the Millipak Open this slowly but do not remove it from the Millipak Allow any air on the clear side of the Millipak to be vented out Q Dispense about 5 litres of water Make sure all air is purged out Air will not pass through the membrane filter in the Millipak lf there A ATTENTION is trapped air in the Millipak then a reduction in Product Water flowrate can result Move the POU Dispenser Trigger back to the upright position Milli Q should now in PRE OPERATE Mode 90 seconds later Leave the Milli Q in PRE OPERATE Mode It is highly recommended not to put Tygon Tubing or any other type VAN ATTENTION of tubing on the end of the Millipak This can compromise the Product Water quality bacteria can grow in the Tygon Tubing The Millipak is now installed and rinsed out 4 10 How TO CALIBRATE THE FLOWRATE FROM THE MILLI Q It is possible to calibrate the flowrate of Product Water from the POU Dispenser Q Make sure the Millipak is vented of all trapped air Q Make sure the Quantum Cartridge is vented of all trapped air o Press
79. ll be sent to the Computer The Milli Q will return to PRODUCT Mode automatically SERVICE PRINTER 18 2 25 PRESS lt MEASURE lt 1 4 Press MEASURE When the data transfer is complete open the TRANSFER menu and then click on CAPTURE TEXT STOP To transfer this data into an EXCEL file 1 2 3 4 Open Microsoft EXCEL Open the you downloaded it will have a txt file extension Choose DELIMITED for the FILE TYPE of your data Press NEXT TAB is the Delimiter Press INEXT and then FINISH Save the new file as a Microsoft Excel Workbook if you want to graph the data or do any calculations with the data APPENDIXES APPENDIX 4 HOW TO USE REMOTE DISPLAY The Remote Display is an accessory that allows you to have the LCD and Keypad and LEDs located up to 2 4 meters away from the Milli Q System The Millipore Catalogue Number for the Remote Display is ZMQSRMDS1 The Remote Display Installation Instructions are not included with this Owner s Manual These Installation Instructions are included with the Remote Display Please contact Millipore if you would like a copy of these instructions ahead of time All of the instructions given in this manual will work with the Remote Display For example suppose you wanted to use the Volumetric Dispenser Function of the Milli Q See Section 5 5 The use of the Keypad is exactly the same when using the Remote Disp
80. low the steps below to perform an AIR PURGE a If the Milli Q is in STANDBY Mode then go to PRE OPERATE Mode It is not possible to access the AIR PURGE Mode from STANDBY Mode Q Press the MENU Keypad button for about 2 seconds The LCD will change as shown here PRE OPERATE PRESET VOLUME 0 00 OPERATE STANDEY MEASURE CLEANING 9 Press MENU for about 2 seconds You have entered the Customer Service Software of the Milli Q If you do not see this display en turn off then on the system power When the LCD shows PRE OPERATE and RECIRCULATION press the STANDBY OPERATE Keypad Button for about 2 seconds This will place the Milli Q into STANDBY Mode Then press the STANDBY OPERATE Keypad Button again The Milli Q will now be in PRE OPERATE Mode Press the MENU Keypad Button again for 2 seconds fo enter the Customer Service Software Press the MENU Keypad Button 6 times 7 times for a Milli Q Synthesis A10 Stop when you see the AIR PURGE display PRESET VOLUME SERVICE PRINTER SERVICE AGE SERVICE CALIB FLOW MEASURE Press MENU SERVICE OPTIONS each time 5 AIR PURGE 5 mn Wait about 10 seconds The 5 minute AIR PURGE will start automatically 75 MAINTENANCE LCD will show a message OPEN THE VALVE alternating with AIR PURGE 5 mn SERVICE UF SERVICE UF
81. mber ZMQSPOUO1 when A ATTENTION you have a Milli Q System beginning with ZMQP Catalogue Number FOOTSWITCH The Millipore Catalogue Number for the Footswitch plus cable is ZMQSFTSO1 The Footswitch allows you a hands free operation where you could change the Milli Q from PRE OPERATE Mode to PRODUCT Mode The length of the Footswitch Cable is 5 meters You will use about 0 3 meters of the Footswitch Cable inside the Milli Q PRINTER OR COMPUTER CABLE The Millipore Catalogue Number for the Printer Cable is PRNTCBLO1 lis length is 2 79 meters The Millipore Catalogue Number for the Computer Cable is 01 lis length is 1 65 meters You will use about O 6 meters of either cable for its connection inside the Milli Q cabinet REMOTE DISPLAY WITH KEYPAD The Millipore Catalogue Number for a Remote Display is ZMQSRMDS1 The Remote Display allows you lo view the LCD and to use the Keypad Buttons remotely The dimensions of the Remote Display are length 204 mm height 112 mm and depth 48 mm Its weight is 2138 The Remote Display comes with a 3 meter cable that plugs into the Milli Q System inside You will use about 0 6 meters of the cable inside the Milli Q The Remote Display be wall mounted There are 2 Stainless Steel Brackets that are attached to either side of Remote Display These brackets can be fastened to the wall The Hardware necessary to attach these brackets to a wall i e screws bolts does no
82. n 4 10 How to calibrate for more information Remember to leave the Milli Q in PRE OPERATE Mode during times of non use i e evenings weekends holidays 65 MAINTENANCE 6 5 HOW TO SANITISE AND CLEAN THE UF CARTRIDGE HOW OFTEN WOULD NORMALLY SANITISE AND CLEAN THE UF CARTRIDGE The Milli Q Synthesis and Milli Q Synthesis ATO will show an LCD message START SANIT every 4 weeks once per month The yellow Service LED will be blinking also This message is based on a day to day timer THINGS TO KNOW BEFORE vou sANITISE THE UF CARTRIDGE l You will need a minimum of a full 30 Reservoir fed at 3 LPH i e a full 30 Reservoir fed with an 3 or RiOs 3 You will need 3 grams of Sodium Hydroxide every time you sanitise the system Do not use any type of chlorine for the sanitisation Millipore does not sell NaCH but it is readily available through most Scientific Apparatus Supply Companies You will need the Barbed Fitting and clear Tygon Tubing from the Accessories Bag the same items you used when the Q Gard Pack and Quantum Cartridge were air purged and hydrated The Milli Q system will not be able to make Product Water for a minimum of 421 minutes while the UF is sanitised and cleaned lt is best to plan to perform the Sanitisation of the UF Cartridge during an overnight or weekend time frame Sodium Hydroxide will form a caustic high pH solution when mixed with water This solution can
83. ntum Cartridge Remove the 2 plastic covers on the ports of the Quantum Cartridge There should be a black rubber O ring in each port Make sure these are pushed firmly in place Q Wet the Quantum Cartridge O rings with water lt is preferable to wet them with ultrapure water DO WET THE O RINGS WITH A LUBRICANT SUCH AS OIL OR SILICON GREASE Push the Quantum firmly into place Both the top and bottom ports of the Quantum Cartridge have to be fully seated Close the door Make sure that both the top latch and the bottom latch of the door A ATTENTION are fully closed Each latch should click when it is fully closed The Quantum Cartridge is now installed 4 6 INSTALLATION OF THE TYGON TUBING a Locate the clear Tygon Tubing and the Barbed Fitting from the Accessories Bag Q Screw the Barbed Fitting onto the bottom end of the POU Dispenser Do not use any PTFE Tape on the threads of the Barbed Fitting A ATTENTION An O ring is located inside the POU Dispenser to insure water tightness between the threads of the POU Dispenser and the Barbed Fitting Push one end of the Tygon Tubing onto the end of the Barbed Fitting Place the other end of the Tygon Tubing in a sink 30 INSTALLATION INSTALLATION OF THE QUANTUM CARTRIDGE Milli Q Synthesis Synthesis 31 INSTALLATION 4 7 PURGING THE AIR FROM THE SYSTEM At this time you should have installed the Q Gard Pack Quantum Cartridge Bar
84. ntum Cartridge are exchanged Normally a 5 minute AIR PURGE Mode is started after the Quantum Cartridge is replaced When the AIR PURGE is finished the 60 minute ATO CLEANING Mode is started See Section 4 7 for more information about the AIR PURGE and the automatic ATO CLEANING Mode 72 MAINTENANCE How po DO AN 10 CLEANING Follow these steps below to perform an A TO CLEANING a IF the Milli Q is in STANDBY Mode then press the OPERATE STANDBY Keypad Button for about 2 seconds This will change the Milli Q from STANDBY Mode to PRE OPERATE Mode the drawing below for more information STANDBY PRE OPERATE Press for about 2 seconds Press the MENU Keypad button for about 2 seconds The LCD will change as shown here PRE OPERATE PRESET VOLUME 0 00 9 Press MENU for about 2 seconds You have entered the Customer Service Software of the Milli Q If you do not see this display then turn off then on the system power When the LCD shows PRE OPERATE and RECIRCULATION press the STANDBY OPERATE Keypad Button for about 2 seconds This will place the Milli Q into STANDBY Mode Then press the STANDBY OPERATE Keypad Button again The Milli Q will now be in PRE OPERATE Mode Press the MENU Keypad Button again for 2 seconds fo enter the Customer Service Software Press the MENU Keypad Button 5 times Stop when you see the SERVICE ATO ATO CLEANING displa
85. or Organics removal Quantum VX QTUMOOOVX 1 box Volatile Organics removal ion exchange resin Quantum Ultrapure Cartridge with 1 non sterile Millipak 20 Express gt Quantum IX QTUMMPEIX 1 box Quantum QTUMMPEEX 1 box Millipak 40 Final Filter Millipak 40 sterile MPGLOASK2 2 box Millipak Express 20 Final Filter Millipak Express 20 non sterile 2001 1 box SPACE AND WEIGHT REQUIREMENTS See Section 2 4 for a drawing showing the dimensions of a Milli Q Total Height needed includes POU Dispenser being fully upright 53 cm Total Width needed includes room needed to remove 45 cm Total Depth needed includes POU when it is fully upright 53 cm Operating weight for a wet Milli Q Synthesis Synthesis ATOJ 16 kg 16 8 kg ELECTRICAL REQUIREMENTS The electrical requirements for a Milli Q Synthesis or Milli Q Synthesis are 120 VAC 10 50 60 Hz 100 VA 0 5 amp source 2 amp Time lag fuse used ref ZMQS6VFTI ZMQPOVFTI ZMQS6VFO1 ZMGPOVFO1 230 VAC 10 50 60 Hz 0 26 amp source 1 amp Time lag fuse used ref ZMQSSVFTI ZMQPS5VFTI ZMQS5VFOT ZMQP5VFOI source of electrical power should be within 1 meter of the Milli Q The source of electrical power must be earth grounded 20 PRE INSTALLATION FEEDWATER REQUIREMENTS Feedwater Conductivity lt 100 uS cm 25 C Feedwater Flowrate The source of feedwater should deliver 2 1 5 lpm
86. ow ls the reservoir full of water ls the source of water filling the reservoir fully operational Q Does the reservoir have 8 mm tubing connection on one of its valves Are you feeding the Milli Q from a pressurised pipe loop Do you have a pressure regulator ready to connect between the pipe and the Milli Q ls the water system feeding the pipe fully operational Does the pipe have a valve ending with 1 2 inch NPTM connection If not do you have a fitting or connection that will attach to the pipe and will end in a 1 2 inch NPTM connection ls there a way to shut off water from the pipe to the Milli Q not did you order a ball valve from Millipore to install on the Feedwater Tubing Are you mounting the Milli Q on a wall wall mounting bracket may be needed in specific conditions Will the wall support the weight of the Milli Q plus full reservoir ls the Milli Q accessible at this height viewing the LCD using the keypad Did you include space on the right side of the Milli Q to remove and replace the Q Gard Did you want a location so as to dispense water over a sink ls the Milli Q located within 2 5 meters of a drain for the UF Reject tubing 5 the Milli Q located within 2 5 meters of a drain for the Feedwater Pressure Relief Valve tubing Are the room environmental conditions adequate humidity temperature If you are going to connect a printer or comp
87. peration with an independent calibrated Resistivity Meter 93
88. play Non Temperature Compensated Resistivity or Non Temperature Compensated Conductivity Displays When you are using the Milli Q Software to make this change you may notice the terms COMP MODE 1 COMP MODE 2 and OFF What do these mean OFF means that the Temperature Compensation is off The displayed Resistivity or Conductivity will not be temperature compensated The temperature of the water will be shown at the same time as the non temperature compensated Resistivity or Conductivity value COMP MODE 1 is the normal setting This setting will display Resistivity or Conductivity values that are temperature compensated to 25 The values are normalised The Software of the Milli Q eliminates small fluctuations of temperature compensated Resistivity or Conductivity due to the fact that these two parameters are not measured at the same time COMP MODE 2 is a setting that gives the actual temperature compensated Resistivity or Conductivity values In some operating conditions the feed water can be warmer or cooler than the water temperature inside the Milli Q This can cause small fluctuations of the resistivity and Conductivity values Resistivity values could fluctuate between 18 0 MQ cm and 18 4 25 while the actual resistivity value is 18 2 MQ cm 25 The 2 setting should be used in applications that require the detection of trace ionic levels or when performing the verification of the Milli Q Resistivity Meter O
89. r drain Shorten the tubing if necessary UF REJECT TUBING Read the steps above conceming the installation of the Feedwater Tubing Locate the DRAIN Port on the back of the Milli Q Synthesis or Milli Q Synthesis system Measure the distance between this port and a sink or drain The maximum recommended distance is 2 5 meters Remove the red plug that is in the DRAIN 3 Port To do this push in on the collar that holds the red plug in place Atthe same time pull the red plug out Locate another elbow shaped fitting from the Accessories Bag Install it into the DRAIN Port Push it in all the way The use of this elbow fitting will allow the tubing to fit better especially if the system is wall mounted Install a length of black 8 mm OD tubing into this elbow fitting Place the other end of the UF Reject tubing into a sink or drain 26 INSTALLATION CONNECTING THE POWERCORD a a a a Locate the Milli Q Power Switch lt is located on the back of the system cabinet It is located just above the Feedwater Tubing connection Make sure your Milli Q System Power Switch is in the OFF position The Power Switch is off when the O position is selected Plug the Powercord into the Milli Q It plugs in next to the Power Switch Plug the other end of the Powercord into an appropriate source of electrical power i e wall outlet 4 3 INSTALLATION OF THE Q GARD a a a a a a Mak
90. re the Q Gard Pack and Quantum Cartridge have been air purged Make sure they have been hydrated overnight Remove the Barbed Fitting and Tygon Tubing from the POU Dispenser Screw the Millipak onto the POU Dispenser Turn it until it is handtight Do not overtighten the Millipak Do not use PTFE Tape on the threads of the Millipak The A ATTENTION POU Dispenser has an O ring inside which provides a watertight seal Q Move the POU Dispenser Trigger forwards This will bring the Milli Q system into PRODUCT Mode D Locate the air vent valve on the top side clear side of the Millipak Open this slowly but do not remove the air vent from the Millipak Allow any air on the clear side of the Millipak to be vented out Q Dispense about 5 litres of water Make sure all air is purged out Air will not pass through the membrane filter in the Millipak there is trapped air in the Millipak then a reduction in Product Water flowrate can A ATTENTION result Move the POU Dispenser Trigger back to the upright position The Milli Q will go into PRE OPERATE Mode after QO seconds Leave the Milli Q in PRE OPERATE Mode It is highly recommended not to put Tygon Tubing or any other type A ATTENTION of tubing on the end of the Millipak This can compromise the Product Water quality The Millipak is now installed and rinsed out At this time it is highly recommended to recalibrate the Product Water flowrate from the Milli Q See Sectio
91. s the MENU Keypad Button 5 times 6 times for a Milli Q Synthesis ATO You should press the MENU Keypad button each time Stop when you see the LANGUAGE under SERVICE OPTIONS display PRESET VOLUME SERVICE PRINTER SERVICE SERVICE CALIB FLOW MEASURE Press MENU eoch SERVICE OPTIONS time LANGUAGE ENGL I SH Press the OPERATE STANDBY Keypad once The PROD UNIT choice will be shown SERVICE OPTIONS LANGUAGE ENGLISH SERVICE OPTIONS PROD UNIT MQ cm L off Press OPERATE STANDBY 39 INSTALLATION Press the CLEANING Keypad Button to change the PROD UNIT from to uS cm SERVICE OPTIONS PROD UNIT MQ cm SERVICE OPTIONS PROD UNIT 5 5 5 PROD UNIT 5 m Press MENU for about 2 seconds When the Milli Q is put into PRODUCT Mode the LCD will look like PRE OPERATE 0 055 5 25 C Note that a Conductivity Measurement of 0 055 uS cm is the same as a Resistivity measurement of 18 2 You have finished changing to units of Conductivity 40 INSTALLATION 4 13 HOW TO SHOW NON TEMPERATURE COMPENSATED RESISTIVITY OR CONDUCTIVITY VALUES It is possible to show non temperature compensated Resistivity non temperature compensated Conduc
92. ss Non sterile MPGPO2001 l box see Section 2 3 for more information UV Lamp ZMQUVLPO1 1 gloves included 83 ORDERING INFORMATION 8 2 CATALOGUE NUMBERS FOR ACCESSORIES See Section 3 2 for information about the various accessories that can be used with a Milli Q Accessory Catalogue Number Wall Mounting Bracket SYSTFIXO1 8 3 CATALOGUE NUMBERS FOR ALL MILLI QS 5 230 VAC System V with UV Lamp 120 VAC System O without UV 7 100 VAC System S with Front Arm F with UF P without Front Arm O without UF T with 10 O without A 10 E Milli Q Element NOTE 1 A Milli Q System with a Front Arm comes with a POU Dispenser 2 Milli Q System without a Front Arm does not come with a POU Dispenser A Remote POU Dispenser would be needed Milli Q Synthesis Synthesis ATO Gradient and Gradient ATO Systems have a UV Lamp inside 4 Milli Q Synthesis Synthesis ATO Biocel Biocel ATO Systems have a UF inside 84 APPENDIXES Chapter 9 APPENDIXES APPENDIX HOW TO REPLACE THE MAIN POWER FUSE Follow the steps below to the moin Power Fuse the Milli Q into STANDBY it is in PRE OPERATE or PRODUCT Section 5 1 more information 1 Tum off the Milli Q Power Switch It is located on the back of the Milli Q cabinet just above the location where the Powercord is plugged into the Milli Q
93. t If all of the air does not expel out do not worry You can repeat this step later after more water hos flowed through the Milli Q Remember to have the Milli Q in STANDBY or PRE OPERATE Mode while you are expelling air out of the Quantum Cartridge 4 8 HYDRATING THE SYSTEM a D D D this time the Millipak is not installed The Barbed Fitting and Tygon Tubing should still be attached to the end of the POU Dispenser Leave the Milli Q in PRE OPERATE Mode overnight or for several hours This will aid in rinsing off the purification media inside the Q Gard Pack and the Quantum Cartridge Do not leave the Milli Q in STANDBY Mode The next morning Bring the POU Dispenser Trigger forward to put the Milli Q into PRODUCT Mode Allow about 10 to 15 litres about 7 to minutes of water to be dispensed from the Milli Q Bring the POU Dispenser Trigger upright The Milli Q will finish dispensing water The Milli Q will continue to operate for 90 seconds after which it will go into PRE OPERATE Mode Leave the Milli Q in PRE OPERATE Mode 33 INSTALLATION OF BARBED FITTING AND TYGON TUBING INSTALLATION PURGING AIR FROM THE QUANTUM CARTRIDGE 34 INSTALLATION 4 9 INSTALLATION AND RINSING OF THE MILLIPAK Obtain a Millipok Remove the Tygon Tubing and the Barbed Fitting from the POU Dispenser Q Screw the Millipak onto the POU Dispenser Do not use any PTFE Tape on the threads of the Mil
94. t come with the Remote Display The instructions for installing the Remote Display are inside its shipping box The instructions for installing a Remote Display are not inside this manual Contact Millipore for these instructions if you would like to see them before obtaining the Remote Display PRE INSTALLATION FOOTSWITCH WALL MOUNTING BRACKET BALL VALVE PRESSURE REGULATOR REMOTE DISPLAY REMOTE POU DISPENSER Milli Q Synthesis Synthesis ATO 19 PRE INSTALLATION 3 4 INSTALLATION REQUIREMENTS CONSUMABLES NEEDED FOR INSTALLATION You will need one Q Gard Pack Quantum Cartridge and Millipak for installation These items do not come with the Milli Q system These items need to be ordered separately The Catalogue Numbers and options for these items are written below Some of the items below be ordered as part of a kit An example might be a kit consisting of a particular type of Quantum Cartridge plus a Millipak Express 20 See Section 8 1 for the catalogue numbers and descriptions of various kits See Section 2 3 for technical information regarding the Consumables for a Milli Q system Q Gard Purification Pack Q Card 1 QGARDOOR 1 1 box RO Elix distilled Milli RX Milli RO feedwater gt QGard 2 QGARDOOD2 1 box DI Service DI feedwater Quantum Ultrapure Cartridge Quantum IX QTUMOOOIX 1 box 700 lon Exchange Resin Quantum EX 1 box lon Exchange Resin media f
95. tely read this manual and to fully comprehend its contents before attempting installation normal operation or maintenance of the Water Purification System You can easily identify your type of Water Purification System if you do not see the Catalogue Number The Milli Q Synthesis and Synthesis A1O Water Purification Systems have an Orange Door on the front cabinet If this manual is not the correct one for your Water Purification System then please contact Millipore HOW TO USE THE KEYPAD AND THE LCD The Keypad and LCD liquid crystal display are located on the front of the Water System Cabinet The Keypad buttons sometimes have a slight delay when pressed As an example suppose you want to change the Milli Q from STANDBY Mode to PRE OPERATE Mode This is done by pressing the OPERATE STANDBY Keypad button for about two seconds There are four Keypad buttons These are labelled as OPERATE STANDBY MEASURE CLEANING and MENU 0 POWER 0 POWER STANDBY SERVICE SERVICE ALARM OPERATE STANDBY MEASURE CLEANING OPERATE STANDBY MEASURE CLEANING See the drawing above for their placement The LCD is a backlit dual line 16 character display The LEDs are located to the right of the LCD see above The POWER LED is green This is lit when the Water System microprocessor has electrical power The SERVICE LED is yellow This will flash when a service type of LCD message is displayed i e EXCH CARTRIDGES is shown meaning to change the
96. ter from the Point Of Use Dispenser and during RECIRCULATION Mode PRESSURE RELIEF VALVE The Milli Q system has a Feedwater Pressure Relief Valve inside The purpose of this is to vent out any Feedwater that has a pressure higher than 0 75 bar 11 psi This would prevent any excessive Feedwater pressure that could build up in the Milli Q system during RECIRCULATION Mode A piece of tubing is included in the Accessories Bag This tubing is attached to the Milli Q system and then placed in a drain or sink When the incoming Feedwater has a pressure greater than 0 75 bar the Pressure Relief Valve will open up and Feedwater will be vented to drain via the attached tubing The water will stop flowing to drain when the Feedwater Pressure drops to less than 0 75 bar If a Pressure Regulator is installed on the Feedwater Tubing between the Milli Q and a Loop then it is unlikely that the Feedwater Pressure will get this high The installation of this tubing is described in more detail in Chapter 4 Installation A Milli Q fed from a Reservoir will not need the Pressure Relief Valve tubing A Milli Q fed from a Pressurised Pipe a Loop should have the Pressure Relief Valve tubing installed during installation Please note that the Pressure Relief Valve is factory installed inside all Milli Q systems and only the tubing needs to be attached during installation PUMP The Pump is used to bring water into the Milli Q and then to send it through the var
97. the Feedwater Supply if necessary Contact Millipore for information regarding the ball valve lt is usually necessary to have fittings installed on both ends of the ball valve to be able to connect it to the Feedwater Tubing REMOTE PoiNT Or UsE DISPENSER A Remote POU Dispenser can be added to the Milli Q This allows you to dispense water a maximum distance of 2 5 meters away the Milli Q The Remote POU Dispenser is rested on a moveable arm that allows 1802 rotation The Millipore Catalogue Number for a Remote POU Dispenser plus arm and weighted base is ZMQSPOURI It is also necessary to order an installation kit with the Remote POU Dispenser This Installation Kit has a Millipore Catalogue Number of ZMQSPOUO The Remote POU Dispenser can be either wall mounted or set on a benchtop The Installation Instructions for the Remote POU Dispenser are included with it PRE INSTALLATION REMOTE POINT OF USE DISPENSER USED ON A PRODUCTION MILLI Q A Production type Milli Q System needs to have Remote Point Of Use Dispenser added to it Without one you would not be able to dispense water from the Milli Q All of the information in the above section Remote Point Of Use Dispenser applies to a Production type of Milli Q System You will not need to order the Installation Kit however The items in the Installation Kit are Factory installed on Production Milli Q Systems Do not order Installation Kit Catalogue Nu
98. the Maintenanc Chapter of this Manual See Chapter 6 Section 6 5 for information on how do this Contact Millipore to replace th UF Cartridge A TOC value above the TOC Setpoint Contact can have many causes Millipore Reinstall either or both the Q Gard Pack or the Quantum Cartridge An optional accessory has detected that there is no feedwater going to th Make sure the Reservoir or the Pressurised Pipe feeding the Milli Q Milli Q This accessory is not factory has a supply of feedwater that can be message must be resolved before th Milli Q can operate installed and needs to be installed in the system delivered to the Milli Q 54 Message and System Status REBOOT SYSTEM EXCHANGE UV EXCHANGE A10 UV SYSTEM ERROR 1 SYSTEM ERROR 2 SYSTEM ERROR 3 SYSTEM ERROR 4 The ionic levels in the Milli Q Product Water are elevated and it is the decision of the Milli Q user whether to use the water or not SYSTEM ERROR 5 SYSTEM ERROR 7 The POU Dispenser will not dispense water You will not be able to dispense walter Milli Q Synthesis A10 only The ATO has tried for gt 15 minutes to process a TOC value but was successful The UV lamp has been installed for 365 days Milli Q Synthesis A10 only The A10 has a small UV lamp inside It has been installed for 365 calendar days The Motor Voltage is too gt 49 VDC high The measured temperature
99. the Screen Filter becomes blocked with debris clogged then feedwater will not flow freely to the Milli Q It is recommended to clean the Screen Filter twice a year or whenever it may have become clogged example of this would be if there were a large amount of debris introduced into the feedwater supply i e plumbing work done on the feedwater pipe Follow the instructions below for cleaning the Screen Filter a Make sure the Milli Q is in PRE OPERATE Mode locate the Shut Off Valve on the feedwater supply Turn off the valve Bring POU Dispenser Trigger forward for about 5 seconds The Milli Q will go into PRODUCT Mode This will depressurise the Feedwater Tubing Bring the POU Dispenser Trigger back a Place the Milli Q into STANDBY Mode Locate the Screen Filter This will be located where the feedwater 8 mm OD tubing originates i e where the 8 mm tubing meets a pressurised pipe Q Unscrew the collar that holds the Feedwater Tubing to the barbed end of the fittings Pull the tubing off of the fitting Q Unscrew the Screen Filter from the Feedwater Pipe Loop Q Go toa sink and flush tap water backwards through the Screen Filter The water would flow through the barbed end first Any trapped debris on the Screen Filter would be flushed out Q Stop flushing the Screen Filter View inside to make sure it is now clear of debris Locate the Roll of PTFE Tape from the Milli Q Accessories Bag from the Shippin
100. tivity Product Water values on the LCD WHAT IS TEMPERATURE COMPENSATION Suppose the feedwater to a Milli Q is 15 C The Milli Q Resistivity Sensor will measure a Resistivity Value of 31 756 or a Conductivity of 0 032 uS cm This is the actual Resistivity of the Milli Q Product Water 15 The Milli Q will perform a temperature compensation for Resistivity measurement lt will be compensated to measurement that would be seen at 259C When a Resistivity measurement of 31 756 15 C is temperature compensated to a measurement at 25 C then the Milli Q will display 18 2 25 C Temperature compensation is a way of standardising Resistivity or Conductivity to measurements that would be seen if the water temperature was 25 C Follow the steps below to display non temperature compensated Resistivity or Conductivity values Choose whether you want to display Resistivity MQ cm or Conductivity uS cm See Section 4 12 in this Chapter for information on how to change between these types of measurement units Q Press the MENU Keypad button for about 2 seconds The LCD will change as shown here PRE OPERATE PRESET VOLUME 0 00 Press MENU for about 2 seconds You have entered the Customer Service Software of the Milli Q If you do not see this display then tum off then on the system power When the LCD shows PRE OPERATE and RECIR
101. urised Feedwater only Make sure the Feedwater Pressure Regulator is set correctly between 1 bar and 0 3 bar Make sure the Milli Q is in PRE OPERATE Mode it is STANDBY Mode then press the OPERATE STANDBY Keypad Button for about 2 seconds to go to PRE OPERATE Mode If the Milli Q is in PRODUCT Mode dispensing water then move the POU Dispenser Trigger back to the upright position D Press the MENU Keypad button for about 2 seconds The LCD will change as shown here PRE OPERATE PRESET VOLUME 0 00 Press MENU for about 2 seconds 35 You have entered the Customer Service Software of the Milli Q INSTALLATION If you do not see this display then turn off then on the system power When the LCD shows PRE OPERATE and RECIRCULATION press the STANDBY OPERATE Keypad Button tor about 2 seconds This will place the Milli Q into STANDBY Mode Then press the STANDBY OPERATE Keypad Button again The Milli Q will now be in PRE OPERATE Mode Press the MENU Keypad Button again for 2 seconds to enter the Customer Service So ware Press the MENU Keypad Button 4 times Stop when you see the FLOW MEASURE display PRESET VOLUME SERVICE PRINTER SERVICE Press MENU each time SERVICE CALIB FLOW MEASURE PRESS MEASURE a Place a 2 litre Graduated Cylinder under the Millipak If you do not have a 2 Litre
102. uter to the Milli Q later did you leave room for this If you are using a footswitch accessory to control the Milli Q did you leave room for this PRE INSTALLATION 3 2 PRE INSTALLATION CHECKLIST ARMLESS MILLI Q Milli Q Systems can be ordered from Millipore without the Front Arm and without the Front Point Of Use Dispenser These are called Production or Armless Milli Q Systems These Milli Q Systems always begin with ZMQP instead of ZMQS When a Production Milli Q is ordered you ordered Millipore Catalogue Number 2 for example the Milli Q arrives in a box without a Front Arm and without a Front Point Of Use Dispenser It is necessary to have a Remote Point Of Use Dispenser with these types of Milli Qs Section 3 3 of this manual has more information regarding the Remote Point Of Use Dispenser It may be desired to have Remote Display with the Production Milli Q System example of when this would be needed is when the Milli Q System is being mounted underneath a Lab Bench In this instance the Remote Display Remote Point Of Use Dispenser could be mounted on top of the Lab Bench When you have a Production type of Milli Q System use the same Pre Installation Checklist on the previous page Additionally you should review the items below also Do you have a Remote Point Of Use Dispenser this item is not part of a ZMGP Millipore Catalogue Number Do you have a Remote Display
103. volumes of water from the Milli Q 0 25 Litre to 63 75 Litre in 0 25 Litre increments The accuracy of this is dependent upon the accuracy of the Flow Calibration performed in Section 4 10 Q Make sure the Milli Q POU Dispenser Flowrate is calibrated Make sure the Millipak is vented of air Make sure the Quantum Cartridge is vented of air Make sure you are in PRE OPERATE Mode Move the POU Dispenser Trigger forward and then back up This will place the Milli Q into PRODUCT Mode but water will not be dispensed the moment A very small amount of water i e 5 ml may be dispensed out oO E B EB The green LED on the side of the POU Dispenser will begin to blink It will stop blinking when the Product Water Resistivity compensated to 25 C is greater than the Resistivity Setpoint and less than the setpoint system only Normally the Resistivity Setpoint is 16 0 It is recommended but not necessary to wait until the green LED stops blinking on the POU Dispenser Q Press MENU for about 2 seconds The LCD should change as shown below PRE OPERATE PRESET VOLUME 0 25 Press MENU for about 2 seconds Q Use the Keypad Arrow Keys MEASURE or CLEANING to set the volume of water you want to dispense from the Milli Q 18 2MQ cm 25 C PRESET VOLUME 6 50 6 50 L is the desired volume to be dispensed Use the Arrow Keypad Buttons to change t
104. y PRESET VOLUME SERVICE PRINTER SERVICE SERVICE CALIB FLOW MEASURE Press MENU SERVICE A10 each time 10 CLEANING 73 MAINTENANCE WAIT Do not press the Keypad The ATO CLEANING Mode will start automatically after 5 seconds The 60 minute timer will be shown SERVICE 10 SERVICE A10 SERVICE 10 A10 CLEANING A10 CLEANING 60 A10 CLEANING 59 Wait for the ATO CLEANING Mode to finish a The Milli Q will automatically go to PRE OPERATE Mode at the end of the ATO CLEANING Mode You have finished performing an 10 CLEANING How DO CANCEL THE ATO CLEANING ONCE IT IS STARTED Press the MENU Keypad Button for about 2 seconds during the ATO CLEANING Mode to cancel it The Milli Q will return to PRE OPERATE Mode SERVICE ATO ill OPERATE A10 CLEANING 43 Press MENU for about 2 seconds 74 MAINTENANCE 6 10 How TO PERFORM AN AIR PURGE An Air Purge is performed when there is trapped air in the UF Cartridge Trapped air will reduce the Product Water flowrate from the Milli Q An Air Purge will allow the trapped air to be sent out of the Milli Q system via the UF Reject tubing An Air Purge is also useful in flushing out any trapped Pyrogens bacteria particles from the feedwater side of the UF Cartridge Membrane This may help when the Product Water resistivity is low Fol
105. ystem is not dispensing wqter For exomple the Milli Q would be left in PRE OPERATE Mode during the evenings and weekends and during other periods of non use The Inlet Solenoid Valve is closed during PRE OPERATE Mode The Milli Q will have an hourly 5 minute recirculation of water in PRE OPERATE Mode This will enhance the quality of the Product Water delivered from the Milli Q A Milli Q Synthesis ATO will perform a single TOC analysis immediately following the hourly 5 minute recirculation of water The Inlet Solenoid Valve is open during RECIRCULATION Mode The Milli Q will have 30 second FAST FLUSH mode every 3 hours of PRE OPERATE Mode The FAST FLUSH mode cleans the feedwater side of the UF Cartridge This aids in reducing any built up layers of bacteria pyrogens and colloids WHAT IS PRODUCT PRODUCT Mode is selected when you want to dispense water when you want to get ready to dispense water from the Milli Q PRODUCT Mode is when you can see the resistivity and temperature of the Milli Q product water This is when you can see the Resistivity and Temperature of the Milli Q Product Water This is when you would see the TOC values with Milli Q Synthesis systems PRODUCT Mode occurs because the POU Dispenser Trigger was moved forward The Inlet Solenoid Valve is open in PRODUCT Mode The Milli Q will dispense for a maximum of 30 continuous minutes in PRODUCT Mode Contact Millipore if you need to dispense for mor

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