QDI 1000 Microspectrophotometer User`s Manual
Contents
1. Always wear Safety goggles rated for OD6 at 785nm Call CRAIC technologies for assistance in selecting appropriate laser safety goggles 2002 2014 CRAIC Technologies Inc J A Confidential C Do not reproduce without permission of CRAIC Technologies TECHNOLOGIES Page 1 CRAIC Raman Software Upon software launch the main window will be displayed Figure 1 Data can be taken while simultaneously viewing the sample via digital camera There are various parts to the LambdaFire main window which can be broken down as Drop Down Menu List From here all the main software settings and features can be accessed in their respective category Quick Access Icons From here all the most used features can be readily accessed by pressing the corresponding icon Spectral Graph Display Spectral response populates in this graph whether viewing past files or using live view Camera Image Live camera feedback for viewing area Filename List List contains running notation of all filenames open in the spectral display graph Measurement Control se See Buttons activate measurement Darkscan Collect Sample etc es Er Cite TE f BODENA PIA bina File Edt View Tools Applications Mathematics UserMode Help iil Fa ANJ ey FO Quick Access Icons CAIL TECHNOLOGIES 1700 1600 1500 1400 1200 1100 1000 700 z 200 100 Counts 120 200 300 400 SOO 600 700 800 W0 1000 12. Confidential a Do not reproduce without permission of CRAIC Technologies TECHNOLOGIES Page 5 m Laser Enable Indicator LED 15 14 Main Power Toggle Switch Je DETAIL F SCALE 2 3 0 Degree Position 90 Degree Position Laser Enable Key Switch 17 Instructions 14 Flip the Main Power Toggle Switch to the Raman Control Unit only after making all of the connections discussed thus far The switch will light up red and will indicate the unit 5 on 15 The Laser Enable Indicator LED will be on only when the laser is active will light up blue and works in conjunction with the Laser Enable Turn Key Switch and the Laser Engaging Rod 16 Hip Imaging Toggle Switch to utilize the reflectance imaging of the raman system Turn on and off as needed view a sample Make sure that the Imaging Is turned off before faking any raman spectra as if may interfere with aquiring a signal Turn off imaging when notin use 17 The Laser is enabled when the Key Switch is in the 90 Degree Position as shown in the detailed view above The Laser Enable Kev Switch must be in the 90 Degree position and the Laser engaging rod musi be pulled outward in order turn the Laser on 2002 2014 CRAIC Technologies Inc J A Confidential a Do not reproduce without permission of CRAIC Technologies TECHNOLOGIES 6 6 6 3 SPECIFICATIONS GENERAL BEHAVIOR Instrument Range 80cm 1 to 2100cm 1 Resolution 9 8 cm 1 0
3. however the default is set to 1 For extremely noisy images it may be necessary to increase the average Settings Signal Processing Video Modes Configurations Video Modes BY8 1280x960 7 Frame Rates 15 000015 z Objective 10X Add Delete Figure 8 Video Modes Video Modes Initial Video Modes are set by default If the camera is capable of various resolutions and colorspaces those options will be displayed in the Video Modes dropdown list The camera Frame Rate can also be changed from this menu Objectives can be chosen in the dropdown menu In order to add a new objective press Add and enter the objective label along with a pixel length ratio if available To delete an objective choose it in the dropdown list and press Delete 20 30 PV will arrive with purchased objective ratios already entered by default 2002 2014 CRAIC Technologies Inc J A Confidential C Do not reproduce without permission of CRAIC Technologies TECHNOLOGIES Page 0 Settings Signal Processing Video Modes Configurations Select Camera Configuration Factory Default Load Settings Save Settings Delete Save As New Figure 9 Camera Configurations Configurations Settings added to all three previous camera tabs can be saved as a Configuration Along with a factory default configuration the 20 30 PV will arrive with preset configurations for purchased objectives To Load Settings choose the des
4. 6 nm full width half max at 1000cm 1 LASER SPECIFICIATIONS Center Wavelength 785 nm Power 100 mW Typical Spectral Linewidth lt 0 02 nm 0 3 cm 1 Polarization S polarized Polarization ratio Min 2005 typ gt 30dB Output Power Variation lt 1 after 3 minute warm up period Lifetime gt 10 000 hours IMAGING SPECIFICATIONS WITH SHIPPING ZEISS EC PLAN NEOFLUAR 20X OBJECTIVE Horizontal field of view 300 micron Vertical field of view 240 micron Illumination wavelength 455 nm Illumination linewidth 20 nm CMOS Sensor resolution 1 4 MPixels ENVIRONMENTAL Mains voltage 115V ONLY Frequency 50 60 Hz Use Indoors only Operating temperature 10 30 C Relative humidity 0 80 to 30 C 2002 2014 CRAIC Technologies Inc J A Confidential a Do not reproduce without permission of CRAIC Technologies TECHNOLOGIES Page 7 IMPORTANT SAFETY INFORMATION This manual is an integral part of the product and must be read carefully before switching on and using the CRAIC Raman spectrometer It contains important instructions and information for the safe operation and maintenance of the product and must therefore be kept in a safe place The information in the manual is extremely important and should be adhered to under all circumstances Hazardous radiation exposure may result if the instructions in this manual are not obeyed A When using the CRAIC Apollo instrument diffuse Laser Radiation scattering of t
5. key A Never leave the laser on when it is not in use This is a fire hazard and may cause wear on the optical coatings used in the head unit Always remove and store the key when the instrument is not used 2002 2014 CRAIC Technologies Inc Confidential Do not reproduce without permission of CRAIC Technologies TECHNOLOGIES Page 4 Use with the 20 30 To use the 20 30 s other features such as the eyepiece the LightBlade spectrometer or its visible camera make sure the illumination light is off to reduce stray light You must also ensure the laser handle is pushed all the way in This disables the laser regardless of the position of the Laser Enable turn key and allows light from the objective to reach the eyepiece and spectrometer Please note that by design no laser light can ever reach the eyepiece under any circumstance No after market filters are necessary Care and maintenance There are no user serviceable parts in this system and under no circumstances should the head unit or the control unit be opened Dust protection Protect the control unit and head unit from dust by putting on the flexible dust cover after each work session Dust and loose particles of dirt can be removed with a soft brush or lint free cotton cloth If you transfer the Raman system to a different microscope ensure that the laser aperture is covered with tape during transit Alignment The system is permanently aligned and should n
6. 100 1200 1300 1400 1500 1600 1700 1800 1900 2000 TONENE Raman Shift cm 1 Hide Cursor Center Cure 67852 XCursor 6742970 Y Cursor Filename List My 0 an vty aun lame Measurement Control Conert Spectrum Figure 1 LambdaFire Raman Main Window 2002 2014 CRAIC Technologies Inc Confidential a Do not reproduce without permission of CRAIC Technologies TECHNOLOGIES Page 2 Drop Down Menu List The Drop Down Menu List is located at the very top left corner of the main software window From here almost all of the software functions features may be accessed e File o Open Ctrl O Opens a browser window to select spectral file s for viewing 6 Close All Close all active spectral files 0 Save As Ctrl S Save the selected spectral file under a different name 0 Convert MSP Files to CSV Convert spectral file s for viewing in Microsoft Excel o Batch convert Folder to CSV Convert folder contents to CSV for viewing in Microsoft Excel o Export to GRAMS SPC Export files to GRAMS Print Ctrl P Print active spectral files Exit Ctrl Q Close LambdaFire window e Edit o Trace Limits Edit the X amp Y value range of active spectral files for viewing spectra only o Peak Picking Settings Edit the threshold and averaging parameters for automatic peak valley notation e View Paged View active spectral files on individual graphs Overlayed View active spectral files overlayed on top of each other Stacked View active spec
7. CRAIC Apollo 785 Raman Microspectrophotometer User s Manual Version 1 2 0 Page 2 CONTENTS INSTALLATION 3 eran eesnonenenenassnaens 6 IMPORTANT WARNINGS ssaxsusennscensnovavens se nenvunaweneateannetaaemeasdeaonsns 7 LABEL REPRODUCTIONS AND LOCATIONS ON PRODUCT 8 9 OPERATION OF THE CRAIC APOLLO SPECTROMETER 10 1 CRAIC Raman Softwar e csscccscsssssssssssecsnnesscnsnneeccnnnsesccenneescenneesesnsssescnnsseesenneses 11 2 Starting the 21 3 Raman MicrospectroScopy s sssscscesecessesecessesesceseceeceseceecesecencesecencevacenceseneneevareneess 21 USE WITH THE 20 30 PV ssessesseoseoseoseosecsecsecsecssossosscsecsscseoe 24 CARE AND MAINTENANCE cccecsccccscsccccscccsccscsccscscsccececs 24 2002 2014 CRAIC Technologies Inc pe A Confidential C Do not reproduce without permission of CRAIC Technologies TECHNOLOGIES Page 3 INSTALLATION DIAGRAM Main Power Jack G Raman Imaging USB Port 3 9 Pin Serial Port 2 DETAIL A SCALE 2 4 Laser Enable Rod 4 Laser Engaging kod DETAIL C SCALE 2 DETAIL B SCALE 1 2 Raman Fiber Optic Port 9 Head Unit Indicator 0 INSTRUCTIONS Attach the yellow cable from the Raman Control Unit to the Main Power Jack on the Raman Head Unit 2 Attach one end of the pin serial cable provided the Pin Serial Port on the Ram
8. D filter from the laser path for full power Typically lowering the power of the laser will lower the Raman signal LASER RADIATION AVOID DIRECT EXPOSURE TO BEAM 785nm Diode Laser Max Output lt 120 mW Class Laser Figure 10 Danger Laser Radiation Warning 2002 2014 CRAIC Technologies Inc J A Confidential a Do not reproduce without permission of CRAIC Technologies TECHNOLOGIES Page 2 Red radiation will be emitted at the sample Always wear protective eyewear that filters red light before engaging the laser Never place your hand in the laser s path as this can cause severe burns 3 Pull out the laser handle on the side of the instrument This directs the beam down through the objective Note that the laser will not turn on unless this handle is pulled out completely Turn on the imaging by flipping the imaging switch Use the stage and camera software to locate an area of interest In CRAIC Raman select Tools Set Parameters and set the integration time to 200 ms o gt UE Ja Turn off the imaging LED by flipping the imaging switch The intense blue light will distort the signal if it is left on 8 Enter real time continuous sample mode 9 Adjust stage height while looking at the signal in Real Time mode For a solid non transparent sample adjust for maximum count levels which means the laser is focused on the top surface If the signal is particularly weak you may try increasi
9. IES Page 5 4 Set Experimental Parameters mx Settings Modes Select Mode 200 818 Limits of Spectrum cm 1 200 818 Mode Average 25 Mode Resolution 2 New Delete Load Save OK Cancel D Figure 3 Parameter Modes The Modes tab of the Parameter window contains a selection of pre loaded measurement settings as well as the ability to create custom measurement settings If particular settings are preferred the modes tab is the ideal place to save the settings for easy loading into the software In order to apply a mode to the settings please do the following steps Press the Parameters icon from the quick access icons in the main window Press the Modes tab of the parameter window Choose the mode from the drop down list Press the Load button in the lower left corner of the Modes tab To create a custom mode please do the following steps Press the Parameters icon from the quick access icons in the main window Press the Modes tab of the parameter window Type in the selected values mode range average and resolution settings for both spectrometers Once desired settings are input press Save and give the mode a unique label This mode can now be accessed from the Select Mode drop down list 2002 2014 CRAIC Technologies Inc J A Confidential C Do not reproduce without permission of CRAIC Technologies TECHNOLOGIES Page 6 Peak Pic
10. an Head Unit 3 Connecto one end of the Type B USB cords provided the Raman Imaging USB Port and the other end the computer USB port 4 Push Laser Engaging Rod outward the engage the Laser on and the imaging LED The laser will only turn DETAIL D on when it has been enabled from the key switch on SCAIE 1 2 the Raman Control Unit and when the enable rod is aT pulled out Refer step 16 for instructions on how enable the laser Pull Laser Engaging Rod outward to turn the laser on and inward to turn off 5 Connect one end of the fiber optic cable provided to the Raman Fiber Optic Port on the Raman Head Unit Connect the other end of the cable to the Fiber Optic Port located on the Raman Control Unit 6 The Head Unit Laser Enable Indicator LED will only turn on only when the Laser is active will turn on and off with the Laser and serves as an indicator alert the user when the laser is on 2002 2014 CRAIC Technologies Inc J A Confidential C Do not reproduce without permission of CRAIC Technologies TECHNOLOGIES Page 4 _ Fiber Optic Port 7 LED Control Knob 8 BNC Interlock 9 DETAIL E SCALE 2 3 _ 9 Pin Serial Port 10 a TN _ 115V AC Power Receptacle 11 5 Pin Yellow Cable 12 Control Unit USB Port 13 Instructions Connect one end of the fiber optic cable provided fo the Fiber Optic Port on the Raman Con
11. ealtime Mode gt Live spectral response view Parameters Parameters My Folder e Choose where to save files by pressing My Folder in the measurement control panel 2002 2014 CRAIC Technologies Inc J A Confidential C Do not reproduce without permission of CRAIC Technologies TECHNOLOGIES Page 4 o The default directory path will display In order to change press Change Directory o Choose a directory in the file browser then press Select Current Directory Parameters e Press the Set Parameters icon in the Quick Access Icons panel o This window is divided into three tabs Settings Modes 4 Set Experimental Parameters Settings Modes Limits of Spectrum cm 1 200 2080 Scans To Average 5 Sampling Time in Milliseco Resolution Factor 0 to 15 Cancel Figure 2 Parameter Settings The Settings tab of the Parameter window will contain values for one or two spectrometers depending upon the system configuration Single soectrometer systems will look similar to Figure 2 without the additional column for the second spectrometer From the settings tab you may set the following items Left and right limits of spectral acquisition cm 1 Scans to Average Sampling time in milliseconds integration time Resolution factor boxcar averaging Per spectrometer 2002 2014 CRAIC Technologies Inc Confidential Do not reproduce without permission of CRAIC Technologies TECHNOLOG
12. es with FDA performance standards 21 CFR 1040 10 and 1040 11 Aperture label located on bottom of head unit not visible on 20 30 product 2002 2014 CRAIC Technologies Inc J A Confidential C Do not reproduce without permission of CRAIC Technologies TECHNOLOGIES Page 9 GENERAL INFORMATION Installation site A Make sure that the workplace is free from oil and chemical fumes Vibrations direct sunlight and major temperature deviations have a negative effect on measurements and spectrophotometry This and an ergonomically designed chair which can be adjusted in several positions are the basic prerequisites for fatigue free microspectroscopy Electric safety To ensure that the Spectrometer and accessories are in a perfectly safe condition please note the following advice and warnings The mains plug must only be inserted into a grounded 115V outlet If an extension cord is used it must be grounded as well Using the ground connection any accessories connected to the Spectrometer which have their own and or a different power supply can be given the same ground conductor potential Please consult our servicing personnel if you intend to connect units without a ground conductor Safety and Warranty Violations The instruments and accessories described in the manual have been checked for safety or possible risks Before making any alterations to the equipment or combining it with non CRAIC components in any
13. he laser presents a significant eye Avoid direct a hazard Users must wear appropriate goggles with OD Laser protective 6 blocking at 785 nm eyewear required Remote Interlock Connector In accordance with CFR 1040 10 f 3 a remote interlock connector has been provided The purpose of the remote interlock connector is to permit the user to connect a remote barrier interlock emergency stop switch or similar device The instrument ships with the interlock shorted via a BNC shorting cap Removing this cap will prevent the laser from being enabled To utilize the optional interlock you may connect a BNC cable to an emergency stop switch The interlock is entirely optional and may be left alone for normal operation 2002 2014 CRAIC Technologies Inc pe A Confidential a Do not reproduce without permission of CRAIC Technologies TECHNOLOGIES Page 8 LABEL REPRODUCTIONS AND LOCATIONS ON PRODUCT Identification label located on back of control unit Al Manufacturer CRAIC Tecnologies perunni ners f piece of Manufacture CRAIC CRAIC 945 N ATena Avenue SSN Amela San Dimas CA 91773 537 Dimas CA 91773 Month and Year of Manufacture DANGER logotype located on side of head unit LASER RADIATION AVOID DIRECT EXPOSURE TO BEAM 785nm Diode Laser Max Output lt 120 mW Class Illb Laser Certification label located on back of control unit This product comph
14. ions Auto Exposure Reference Level 08 33 58 83 108 133 158 183 208 233 5 Camera Whitebalance Figure 6 Camera Settings Settings The Settings tab contains prominent image adjustment tools such as exposure gain and white balance The Exposure Time can be manually set via the exposure slider or set to automatic by checking the box labeled Auto Figure 6 The Auto Exposure Reference Level slider is used to adjust what level of brightness the camera will attempt to achieve when exposure is set to auto The Gain level slider will affect the amount of gain in a picture Please note that this will only amplify the intensity in the image and could lead to a grainy or noisy image at high gain levels It is typically best to increase exposure before gain When Auto is checked for gain the system will automatically determine the gain level 2002 2014 CRAIC Technologies Inc Confidential Do not reproduce without permission of CRAIC Technologies TECHNOLOGIES Page 9 Settings Signal Processing Video Modes Configurations Modify the way the image ts represented Flip No Flip v Choose the number of frames to average Number of frames 1 Figure 7 Signal Processing Signal Processing Using the Flip setting the camera can be rotated and flipped vertically or horizontally This is preset at factory for 20 30 PV systems The Number of Frames to average can be set to higher numbers
15. ired configuration to the left which lists all saved default configurations Press Load Settings Once settings have been changed on a previously saved setting press Save Settings to update the configuration To delete configurations choose the configuration from the left list and press Delete Once custom settings have been applied for a new configuration press Save As New and enter a configuration name to create a new configuration Saving an Image To save a camera image press the Save icon located in the icon panel Choose the save location and the file name in a pop up file browser window 2002 2014 CRAIC Technologies Inc J A Confidential C Do not reproduce without permission of CRAIC Technologies TECHNOLOGIES Page 1 STARTING THE INSTRUMENT 1 Enable the power switch on the control unit 2 Turn the laser key 3 Pull out the laser handle two blue warning LEDs will come on indicating that the laser is live The laser is only live when the handle is pulled out all the way as soon as you push in the handle it is disabled regardless of the position of the key 4 Enable the Imaging power switch on the control unit 5 Turn onthe computer and monitor 6 Start the CRAIC Raman Software by clicking on the CRAIC icon RAMAN SPECTROSCOPY The following procedure is used to take Raman spectra of samples with the Apollo Spectrometer 1 Place your sample on the stage of the microscope 2 Remove a N
16. ith Legend Select Ternplate 7 Print with Template Default Save New Delete Company Date amp Tirne Click to Change Logo CRAIC Technologies 8 21 2013 12 45 PM Project Case Number Project 1 Operator Name Sample Name PL Test Sample Customize Add image Print Done 120 0 10 400 500 600 700 800 900 100 11 AN Raman Shift cm l Figure 5 Print Template Window Starting from the top of the preview box the spectra can be printed with a legend basically to include the colored filename list From Select Template you may add edit and delete print templates Customizable information appears below to include e Company Project Operator Sample Case Tag Customizable Company Logo To add an image press Add Image Use the pop up file browser to locate the desired picture Place the image by dragging the image box to the desired location and pressing Drop Image To add text double click where the text will be placed in the graph A text box will appear with formatting options Text cannot be deleted once placed on the graph In order to remove it the printing must be canceled and restarted 2002 2014 CRAIC Technologies Inc J A Confidential C Do not reproduce without permission of CRAIC Technologies TECHNOLOGIES Page 8 Camera Camera Settings is divided into 4 tabs Settings Signal Processing Video Modes Configurations Settings Signal Processing Video Modes Configurat
17. king Peak picking will automatically detect and notate peak valley locations Pressing the Peak Picking icon in the icon panel will activate deactivate the notation on screen To change peak picking settings choose Edit from the top dropdown menu and choose Peak Picking Settings 4 Peak Settings Choose Peaks or Valleys Peaks Eliminates peaks below threshold and Threshold 0 15 valleys above threshold Number of data points used in peak finding algorithm 3 minimum Width 5 Choose Range for Peak Picking 1700 Figure 4 Peak Picking Settings The software can be set to recognize either peaks or valley locations The Threshold can be set to either eliminate peaks below threshold or valleys above threshold The Width is by default to set to 5 however larger numbers will average peak locations over a wider range of data Realtime Mode To view a live spectral response choose the Realtime icon from the icon panel You may view the output as Counts Raw Intensity Press Escape to exit the live mode You will require a valid dark and reference scan to view these live modes 2002 2014 CRAIC Technologies Inc pe A Confidential C Do not reproduce without permission of CRAIC Technologies TECHNOLOGIES Page 7 Printing spectra To print active spectral files choose Print from the File dropdown menu in the main window A print preview box will appear Print Graph mesm 7 Print w
18. ng the integration time to improve sensitivity at the cost of a slower real time scan TAKING RAMAN SPECTRA 1 Push in the laser handle all the way or place a high ND gt 2 0 in the beam path to block the laser 2 Disable the imaging source by flipping the corresponding switch on the control unit If you do not do this stray light from the internal LED will influence your measurement 3 Select My Folder and choose your data directory This is where the program will store the spectrum files 4 Press the Collect Darkscan button 5 Restore the beam down onto the sample by pulling out the laser handle and or removing the high ND filter 6 Press the Collect Sample button A screen will appear for information entry 7 Select what kind of measurement is being acquired Fluorescence This will subtract the dark scan from the current scan 8 Select which objective is being used 2002 2014 CRAIC Technologies Inc J A Confidential a Do not reproduce without permission of CRAIC Technologies TECHNOLOGIES Page 3 9 Enter asample filename or use the last filename entered If the file exists the software will automatically add a number at the end of the filename and increment that number 10 Press Scan to take a spectrum 11 Place a high ND 2 0 filter in the beam path to temporarily block the laser For longer periods of disuse disable the laser by pushing in the handle or turning the laser enable
19. ot need any further servicing throughout its useful life However when moving the Raman system extreme caution should be taken to avoid sudden accelerations that might cause misalignment If the instrument has become misaligned please contact CRAIC Technologies immediately for servicing NEVER MANUALLY ATTEMPT RELAIGNMENT THE HEAD UNIT MUST NOT BE OPENED BY NON CRAIC PERSONNEL FOR ANY REASON ANY ATTEMPTS TO DO SO WILL VOID THE WARRANTY Laser health Our laser is designed for at least 10 000 hours of life Mains voltage The mains wall voltage must be 115 V North America If you are moving the instrument to a country that uses 230 V mains for example most of Europe you must take precautions to ensure that the instrument is not destroyed Furthermore you must always use surge protection technology All CRAIC instruments are manufactured and tested with extreme care If you do have cause for complaint 2002 2014 CRAIC Technologies Inc J A Confidential C Do not reproduce without permission of CRAIC Technologies TECHNOLOGIES Page 5 however do not try to repair the instruments and their accessories yourself Contact your national agency or our central servicing department in California directly CONTACT INFORMATION Postal address CRAIC Technologies 948 N Amelia Avenue San Dimas CA 91773 United States Tel 001 310 573 8180 Fax 001 310 573 8182 2002 2014 CRAIC Technologies Inc Confidential Do n
20. ot reproduce without permission of CRAIC Technologies TECHNOLOGIES
21. tral files soaced at even intervals on top of each other e Tools 0 Set Parameters Edit settings for measurement i e spectral range average scans etc Oo Set Coefficients Spectrometer coefficients Password protected set at factory Mathematics Statistics Create average of scans with options for 1 2 1 2 Standard Deviation Derivative Derivative of spectral file Integrate Area underneath curve of spectral file Smoothing Average of adjacent pixels averaging Spectral Math Spectral math functions i e multiply subtract divide etc Normalize Current Spectra Normalize a single active soectrum Normalize Multiple Spectra Normalize multiple active spectra O O O O O O O Baseline Correction Removes fluorescence from the measurement e Help 6 About Information about software version 2002 2014 CRAIC Technologies Inc Confidential Do not reproduce without permission of CRAIC Technologies TECHNOLOGIES Page 3 Icon Panel Icon functions from left to right BRS e gt Open File s Open spectral file s Close One File Close one file Close All Files mer Close all open files Choose measurement settings Peak Picking ae Activate Deactivate peak notation feature Camera Settings rel Various camera settings Save Image Save a camera image Swap Camera Graph Positions Switch graph and camera positions Camera image becomes more prominent than graph and vice versa R
22. trol Unit and the other end the Fiber Optic Port on the Raman Head Unit 8 Use the LED control knob adjust the light intensity for imaging samples by turning the knob on the back of the Raman control unit The BNC Interlock consists of a standard Female BNC connector Removing the shorting cap will permanenitlydisable the laser The Interlock has been provided to allow for an auxilary switch if one is desired Shorting the connection will enable the An laser and opening the circuit by removing the shorting cap will disable auxillary switch that makes use of the BNC Interlock is not provided by CRAIC Technologies 10 Connect the other end of the pin serial cable provided the Pin Serial Port localted on the Raman Control Unit 11 Use the black power cable provided and connect the male end of the cord into the 115V Power Receptacle of the Raman Control Unit Use in combination with a surge protector and provide only 115 AC for powering the unit 12 Connect the 5 Pin Yellow Cable to the Main Power Jack of the Raman Head Unit The cord is configured fit into the Main Power Jack in a specific orientation Insert the cable so that slips into place and screw secure 13 Connect one of the Type B USB cords provided to the USB Port on the Raman Control Unit and connect the other end toa USB port on the computer 2002 2014 CRAIC Technologies Inc J
23. way not described in this manual consult the CRAIC agency for your region or the main factory in California Any guarantee or warranty will be rendered invalid if the instrument is opened or modified in any way by unauthorized persons or if the instrument is used in any way other than described in these instructions CE Marking This instrument meets the requirements of Directives of Electromagnetic Compatibility EMC 89 336 EEC 92 31 EEC 93 68 EEC and Low Voltage Directives LVD 73 23 EEC 93 68 EEC RoHS and WEEE Directives X CRAIC Technologies is exempt from the RoHS Directive 2002 95 EC under Category 9 of Annex 1 a of Directive 2002 96 EC In the EC please contact your local Sales Representative regarding disposal FDA Compliance Statement This product complies with FDA performance standards 21 CFR 1040 10 and 1040 11 2002 2014 CRAIC Technologies Inc pe A Confidential a Do not reproduce without permission of CRAIC Technologies TECHNOLOGIES Page 0 Operation of the CRAIC Apollo Raman Spectrometer The operation portion of this manual is divided into sections There is the introduction overview of the software and checking the calibration of the instrument then there is a section for each type of spectroscopy that can be run using the CRAIC Apollo system Note on Laser Light Source LASER RADIATION AVOID DIRECT EXPOSURE TO BEAM 785nm Diode Laser Max Output lt 120 mW Class Laser
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