Agilent 1290 Infinity Thermostat - User Manual
Contents
1. Waste tube in leak channel Figure 10 Hydraulic Connections 1290 Infinity Thermostat User Manual Installing the Thermostat 3 Stage 4 Installing the Sample Tray Load the sample tray with sample vials as required 2 Slide the sample tray into the autosampler so that the rear of the sample tray is seated firmly against the rear of the sample tray area 3 Press the front of the sample tray down to secure the tray in the autosampler If the tray pops out of its position the air channel adapter is not inserted correctly Figure 11 Installing the Sample Tray Half Tray Combinations In the autosampler only the 100 vial tray is supported for temperature control of the vials Nevertheless the half trays of the standard autosampler G1329A B can be used in the thermostatted autosampler as well However when these trays are installed cooling or heating of the vials in the tray will not work Half trays can be installed in any combination enabling both 1 8 ml and 6 ml vials to be used simultaneously 1290 Infinity Thermostat User Manual 29 3 Installing the Thermostat Numbering of Vial Positions The standard 100 vial tray has vial positions 1 to 100 However when using two half trays the numbering convention is slightly different The vial positions of the right hand half tray begin at position 101 as follows Left hand 40 position tray 1 40 Le2. p n 03396 61010 Pin 33XX Pin Agilent Signal Name Active module TTL 9 1 White Digital ground NC 2 Brown Prepare run Low 8o 3 3 Gray Start Low 2 E NC 4 Blue Shut down Low e n NC 5 Pink Not i connected NC 6 Yellow Power on High 14 7 Red Ready High 4 8 Green Stop Low NC 9 Black Start request Low 13 15 Not connected 1290 Infinity Thermostat User Manual 73 8 Cable Identification Agilent Module to Agilent 35900 A D Converters p n 5061 3378 Pin 35900 Pin Agilent Signal Name Active A D module TTL 1 White 1 White Digital ground 2 Brown 2 Brown Prepare run Low 3 Gray 3 Gray Start Low 4 4 Blue Shut down Low 5 Pink 5 Pink Not connected 6 Yellow 6 Yellow Power on High 7 Red 7 Red Ready High 8 Green 8 Green Stop Low 9 Black 9 Black Start request Low Agilent Module to General Purpose p n 01046 60201 Wire Color Pin Agilent Signal Name Active module TTL White 1 Digital ground A 1 Dn Brown 2 Prepare run Low 00 em OB KEY Gray 3 Start Low oo o0 Blue 4 Shut down Low HE Pink 5 Not connected S BE 15 Yellow 6 Power on High Red 7 Ready High Green 8 Stop Low Black 9 Start request Low 74 1290 Infinity Thermostat User Manual BCD Cables Cable Identification 8 One end of these cables provides a 15 pin BCD connector to be connecte
3. e Agilent Technologies Notices Agilent Technologies Inc 2011 2014 2015 No part of this manual may be reproduced in any form or by any means including elec tronic storage and retrieval or translation into a foreign language without prior agree ment and written consent from Agilent Technologies Inc as governed by United States and international copyright laws Manual Part Number 61330 90014 Rev B Edition 05 2015 Printed in Germany Agilent Technologies Hewlett Packard Strasse 8 76337 Waldbronn Warranty The material contained in this docu ment is provided as is and is sub ject to being changed without notice in future editions Further to the max imum extent permitted by applicable law Agilent disclaims all warranties either express or implied with regard to this manual and any information contained herein including but not limited to the implied warranties of merchantability and fitness for a par ticular purpose Agilent shall not be liable for errors or for incidental or consequential damages in connection with the furnishing use or perfor mance of this document or of any information contained herein Should Agilent and the user have a separate written agreement with warranty terms covering the material in this document that conflict with these terms the warranty terms in the sep arate agreement shall control Technology Licenses The hardware and or software described in this
4. CN China Alphabetic character A Z used by manufacturing Alpha numeric code 0 9 A Z where each combination unambiguously denotes a module there can be more than one code for the same module Serial number 83 9 Hardware Information Electrical Connections Rear View of the Module Relay contacts CAN cable to next module Vial number output Therm Autosampler cable Remote RS232C CAN bus Thermostat Autosampler cable Figure 17 Electrical Connections 84 1290 Infinity Thermostat User Manual Hardware Information 9 Early Maintenance Feedback Maintenance requires the exchange of components which are subject to wear or stress Ideally the frequency at which components are exchanged should be based on the intensity of usage of the module and the analytical conditions and not on a predefined time interval The early maintenance feedback EMF feature monitors the usage of specific components in the instrument and provides feedback when the user selectable limits have been exceeded The visual feedback in the user interface provides an indication that maintenance procedures should be scheduled EMF Counters EMF counters increment with use and can be assigned a maximum limit which provides visual feedback in the user interface when the limit is exceeded Some counters can be reset to zero after the required maintenance procedure Using the EMF Counters The
5. Installing the Thermostat Damaged Packaging 18 Delivery Checklist 18 Optimizing the Stack Configuration 19 Installing the Thermostat 21 Stage 1 Preparing the Thermostat and Autosampler Fraction Collector 22 Stage 2 Power Cable and Interface Cable Connection 25 Stage 3 Flow Connections 27 Stage 4 Installing the Sample Tray 29 Stage 5 Installing Tray Cover and Front Cover 31 Stage 6 Turning on the Thermostatted Autosampler Fraction collector 31 Transporting the Thermostatted Autosampler or Fraction Collector 32 RE Agilent Technologies 3 Installing the Thermostat Damaged Packaging CAUTION If the delivery packaging shows signs of external damage please call your Agilent Technologies sales and service office immediately Inform your service representative that the instrument may have been damaged during shipment Defective on arrival problems If there are signs of damage please do not attempt to install the module Inspection by Agilent is required to evaluate if the instrument is in good condition or damaged gt Notify your Agilent sales and service office about the damage gt An Agilent service representative will inspect the instrument at your site and initiate appropriate actions Delivery Checklist 18 Unpack the module Ensure all parts and materials have been delivered The delivery checklist is shown in Table 3 on page 18 Please report missing or damaged parts to your local Agilen
6. Sound Pressure Lp lt 70 dB At Operator Position Normal Operation e According to ISO 7779 1988 EN 27779 1991 Type Test 1290 Infinity Thermostat User Manual 93 10 Appendix Agilent Technologies on Internet For the latest information on products and services visit our worldwide web site on the Internet at http www agilent com 94 1290 Infinity Thermostat User Manual Index A Agilent Lab Advisor software 34 Agilent Lab Advisor 34 Agilent oninternet 94 ALS thermostat parts and materials accessory kit 63 main assemblies 62 63 ALS thermostat repairs power supplyfuses 58 ambient non operating temperature 15 ambient operating temperature 15 analog cable 70 Autosampler Thermostat Operation 8 auxiliary cable 77 B BCD cable 75 benchspace 14 C cable analog 70 auxiliary 77 BCD 75 CAN 78 external contact 79 78 remote 72 RS 232 80 cables 1290 Infinity Thermostat User Manual analog 68 BCD 68 CAN 69 external contact 69 LAN 69 overview 68 remote 68 RS 232 69 CAN cable 78 cautions and warnings 54 cleaning 57 compensation sensor open 44 compensation sensor short 45 condensation 6 14 14 D defect on arrival 18 delay volume 19 delivery checklist 18 18 dimensions 15 E electrical connections descriptions of 82 electronic waste 91 EMF early maintenance feedback 85 environment 12 14 error messages ALS thermostat 48 bad cooling heating performance
7. 41 Timeout 41 Shutdown 42 Remote Timeout 42 Lost CAN Partner 43 Leak Sensor Short 43 Leak Sensor Open 44 Compensation Sensor Open 44 Compensation Sensor Short 45 Fan Failed 45 Leak 46 Open Cover 46 Cover Violation 47 Thermostat Error Messages 48 Fan Failed 48 Temperature Control Failed 1 4 49 Temperature Sensor Failed 1 4 49 Lost Contact to Autosampler Thermostat 50 Power Fail for Autosampler Thermostat Module 50 Temperature out of Range 51 Bad Cooling Heating Performance 52 This chapter describes the meaning of error messages and provides information on probable causes and suggested actions how to recover from error conditions oh Agilent Technologies 39 5 Error Information What Are Error Messages 40 Error messages are displayed in the user interface when an electronic mechanical or hydraulic flow path failure occurs which requires attention before the analysis can be continued for example repair or exchange of consumables is necessary In the event of such a failure the red status indicator at the front of the module is switched on and an entry is written into the module logbook If an error occurs outside a method run other modules will not be informed about this error If it occurs within a method run all connected modules will get a notification all LEDs get red and the run will be stopped Depending on the module type this stop is implemented differently For example for a pump the
8. 52 compensation sensor open 44 Index compensation sensor short 45 fan failed 45 48 ignition without cover 46 46 leak sensor open 44 leak sensor short 43 leak 46 lost CAN partner 43 lost contact to ALS thermostat 50 power fail ALS thermostat 50 remote timeout 42 shutdown 42 temperature control failed 49 temperature out of range 51 temperature sensor failed 49 timeout 41 external contact cable 79 F failure 35 fan failed 45 flow path 19 frequency range 15 fuses 12 58 G general error messages 41 H half tray combinations 29 humidity 15 injection 6 95 Index installation thermostatted autosampler 21 installation benchspace 14 installing the thermostat preparation 22 installing the thermostatted autosampler flow connections 27 power cable and interface cable 25 sampletray 29 tray cover and front cover 31 turning on the instrument 31 internet 94 introduction to the thermostat 6 L LAN cable 78 leak sensor open 44 leak sensor short 43 le ak 46 line frequency 15 line voltage 15 lost CAN partner 43 M m 3 3 aintenance definition of 56 feedback 85 essage ignition without cover 46 46 remote timeout 42 issing parts 18 ulti draw option 6 Non operating altitude 15 non operating temperature 15 96 0 operating Altitude 15 operating temperature 15 optimizing the stack configuration 19 19 P packaging damaged 18
9. BNC Connector p n 8120 1840 Pin BNC Pin Agilent Signal Name module Shield Shield Analog el Center Center Analog 1290 Infinity Thermostat User Manual Agilent Module to General Purpose Cable Identification p n 01046 60105 Pin Agilent Signal Name module Not connected Black Analog p Red Analog we 1290 Infinity Thermostat User Manual 71 Cable Identification Remote Cables 72 One end of these cables provides a Agilent Technologies APG Analytical Products Group remote connector to be connected to Agilent modules The other end depends on the instrument to be connected to Agilent Module to 3396A Integrators p n 03394 60600 Pin 3396A Pin Agilent Signal Name Active module TTL 9 1 White Digital ground NC 2 Brown Prepare run Low 8o A 3 3 Gray Start Low z NC 4 Blue Shut down Low e Be NC 5 Pink Not Ls connected NC 6 Yellow Power on High 5 14 7 Red Ready High 1 8 Green Stop Low NC 9 Black Start request Low 13 15 Not connected Agilent Module to 3396 Series II 3395A Integrators Use the cable Agilent module to 3396A Series I integrators 03394 60600 and cut pin 5 on the integrator side Otherwise the integrator prints START not ready 1290 Infinity Thermostat User Manual Cable Identification Agilent Module to 3396 Series 3395B Integrators
10. BO EEE 22 Primary fuses Pull the fuse holder out of the socket Remove the fuse from the fuse holder Insert a new fuse in the fuse holder Reinsert the fuse holder and fix with the screwdriver Reinsert the power cables Switch ON the power switch 1290 Infinity Thermostat User Manual 59 6 Maintenance Exchanging the Power Supply Fuses 60 1290 Infinity Thermostat User Manual 1290 Infinity Thermostat User Manual 7 Parts for Maintenance Main Assemblies External Parts 62 Accessory Kit 63 HPLC System Tool Kit 64 Plastic Parts 65 RE Agilent Technologies 61 7 Partsfor Maintenance Main Assemblies External Parts Main Assemblies External Parts Figure 15 Main Assemblies ltem p n 1 2110 0015 2 2110 0029 3 5065 9982 G1330 81600 62 Description Fuses T2 5 A 250V CSA UL listed Fuse TCA Board T3 A 250 V CSA UL listed Plastics kit includes base top left and right sides Cable Autosampler Fraction Collector to Thermostat 1290 Infinity Thermostat User Manual Parts for Maintenance 7 Accessory Kit ltem p n Description 1 G1330 67300 Waste Tube Assy 2 G1330 81600 Cable Autosampler Fraction Collector to Thermostat 1290 Infinity Thermostat User Manual 63 7 Partsfor Maintenance HPLC System Tool Kit HPLC System Tool Kit G4203 68708 contains some accessories and tools needed for installation and maintenance of the module 64 1290 Infinity Thermostat User
11. CAN cable to previous module V GPIB Sono aA irs c 163 U A V n V n n ees ccce Ren P Thermostat to Autosampler Fraction Collector Cable Figure 9 Cable Connections Stage 3 Flow Connections WARNING When opening capillary or tube fittings solvents may leak out The handling of toxic and hazardous solvents and reagents can carry health risks gt Observe appropriate safety procedures for example wear goggles safety gloves 3 and protective clothing as described in the material handling and safety data sheet supplied by the solvent vendor especially when toxic or hazardous solvents are used 1290 Infinity Thermostat User Manual 27 3 28 Installing the Thermostat Installing the Thermostat To column compartment Pump From pump To metering device Plug To waste From needle seat Column compartment The following procedure describes the installation of the flow connections of the G1329A B Autosampler For information about other autosampler or fraction collector modules see the Installing chapter in the corresponding manuals 1 Connect the pump outlet capillary to port 1 of the injection valve 2 Connect column compartment inlet capillary to port 6 of the injection valve 3 Ensure that the waste tube is positioned inside the leak channel
12. Infinity Thermostat User Manual 1290 Infinity Thermostat User Manual 6 Maintenance Warnings and Cautions 54 Introduction to Maintenance 56 Cleaning the Module 57 Exchanging the Power Supply Fuses 58 RE Agilent Technologies 53 6 Maintenance Warnings and Cautions CAUTION Damaged electronics Disconnecting or reconnecting the autosampler fraction collector to thermostat cable when the power cords are connected to either of the two modules will damage the electronics of the modules In such a case mainboards of both instruments must be exchanged otherwise they can damage the other instrument gt Make sure the power cords are unplugged before disconnecting or reconnecting the autosampler fraction collector to thermostat cable WARNING Module is partially energized when switched off as long as the power cord is plugged in Risk of stroke and other personal injury Repair work at the module can lead to personal injuries e g shock hazard when the module cover is opened and the instrument is connected to power gt Never perform any adjustment maintenance or repair of the module with the top cover removed and with the power cord plugged in gt The security lever at the power input socket prevents that the module cover is taken off when line power is still connected Never plug the power line back in when cover is removed WARNING Sharp metal edges Sharp edged parts of the equipment may cause in
13. are in the tray In cooling mode condensation is generated on the cooled side of the Peltier elements This condensed water is safely guided into the leak system 1290 Infinity Thermostat User Manual Introduction Introduction to the Thermostat Heat sink fans TCA board Power supply Heat sink Heat exchanger Heat exchanger fan Condensation leak drain Figure 1 Overview of the Thermostat 1290 Infinity Thermostat User Manual 1 Introduction Thermostat Operation Thermostat Operation Heat exchanger Special sample tray Air channel in autosampler sampling unit Air outlet Heating cooling module Peltier elements Ambient air in Thermostatted air Heated air out Figure 2 Thermostat Principle 8 1290 Infinity Thermostat User Manual Introduction 1 The thermostat is equipped with cooling heating module which uses Peltier elements for efficient air cooling When turned on the front side of the Peltier elements is heated cooled according to the temperature setting fan draws air from the sample tray area and blows it through the channels of the heating cooling module The fan speed is determined according to the environmental conditions e g ambient temperature humidity In the heating cooling module the air reaches the temperature of the Peltier elements and this thermostatted air is blown underneath the special sample tray where it is ev
14. be impaired gt The operator of this instrument is advised to use the equipment in a manner as specified in this manual Safety Standards This is a Safety Class I instrument provided with terminal for protective earthing and has been manufactured and tested according to international safety standards Operation Before applying power comply with the installation section Additionally the following must be observed Do not remove instrument covers when operating Before the instrument is switched on all protective earth terminals extension cords auto transformers and devices connected to it must be connected to a protective earth via a ground socket Any interruption of the protective earth grounding will cause a potential shock hazard that could result in serious personal injury Whenever it is likely that the protection has been impaired the instrument must be made inoperative and be secured against any intended operation Make sure that only fuses with the required rated current and of the specified type normal blow time delay and so on are used for 1290 Infinity Thermostat User Manual 89 10 Appendix 90 replacement The use of repaired fuses and the short circuiting of fuse holders must be avoided Some adjustments described in the manual are made with power supplied to the instrument and protective covers removed Energy available at many points may if contacted result in personal injury Any adjust
15. park transport assembly 32 parts and materials 18 performance specifications 16 physical specifications 15 power consideration 12 power consumption 15 powercords 13 power requirements 12 power supply indicator 36 R radio interference 92 remote cable 72 repairs cautions and warnings 54 RS 232C cable 80 S safety class 89 safety general information 89 standards 15 symbols 88 sample tray 6 sample trays numbering of vial positions 30 serial number information 83 83 shipping 32 shutdown 42 site requirements 12 12 power cords 13 sound emission 93 specification physical 15 specifications 16 status indicators 36 status indicator 35 storage 14 T temperature sensor 46 temperature 14 timeout 41 tool kit hplc system 64 transport mechanism 6 transport 32 32 troubleshooting error messages 40 V vialracks 6 vial tray 32 vials 6 voltage range 15 Ww warnings and cautions 54 waste electrical and electronic equipment 91 WEEE directive 91 weight 15 1290 Infinity Thermostat User Manual Index 1290 Infinity Thermostat User Manual 97 www agilent com In This Book This manual contains information about the Agilent 1290 Infinity Thermostat This manual describes the following introduction site requirements and specifications installing the thermostatted autosampler optimizing performance troubleshooting and diagnostics maintenance parts and materials for mai
16. representative 2 Leak sensor incorrectly routed being Please contact your Agilent service pinched by a metal component representative 1290 Infinity Thermostat User Manual 43 5 44 Error Information Leak Sensor Open Error ID 0083 The leak sensor in the module has failed open circuit The current through the leak sensor is dependent on temperature A leak is detected when solvent cools the leak sensor causing the leak sensor current to change within defined limits If the current falls outside the lower limit the error message is generated Probable cause Suggested actions 1 Leak sensor not connected to the main Please contact your Agilent service board representative 2 Defective leak sensor Please contact your Agilent service representative 3 Leak sensor incorrectly routed being Please contact your Agilent service pinched by a metal component representative Compensation Sensor Open Error ID 0081 The ambient compensation sensor NTC on the main board in the module has failed open circuit The resistance across the temperature compensation sensor NTC on the main board is dependent on ambient temperature The change in resistance is used by the leak circuit to compensate for ambient temperature changes If the resistance across the sensor increases above the upper limit the error message is generated Probable cause Suggested actions 1 Defective main board Please contact your Agilent service repre
17. 2003 is introducing producer responsibility on all electric and electronic appliances starting with 13 August 2005 This product complies with the WEEE Directive 2002 96 EC marking requirements The affixed label indicates that you must not discard this electrical electronic product in domestic household waste Product Category With reference to the equipment types in the WEEE Directive Annex I this product is classed as a Monitoring and Control Instrumentation product E Do not dispose off in domestic household waste To return unwanted products contact your local Agilent office or see www agilent com for more information 1290 Infinity Thermostat User Manual 91 10 Appendix Radio Interference Cables supplied by Agilent Technologies are screened to provide optimized protection against radio interference All cables are in compliance with safety or EMC regulations Test and Measurement If test and measurement equipment is operated with unscreened cables or used for measurements on open set ups the user has to assure that under operating conditions the radio interference limits are still met within the premises 92 1290 Infinity Thermostat User Manual Appendix 10 Sound Emission Manufacturer s Declaration This statement is provided to comply with the requirements of the German Sound Emission Directive of 18 January 1991 This product has a sound pressure emission at the operator position lt 70 dB
18. 6 integrators Agilent module to general purpose 1290 Infinity Thermostat User Manual CAN cables p n 5181 1516 5181 1519 LAN cables p n 5023 0203 5023 0202 Cable Identification 8 Description CAN cable Agilent module to module 0 5 m CAN cable Agilent module to module 1 m Description Cross over network cable shielded 3 m for point to point connection Twisted pair network cable shielded 7 m for point to point connection External Contact Cable p n G1103 61611 RS 232 cables p n G1530 60600 RS232 61601 5181 1561 1290 Infinity Thermostat User Manual Description External contact cable Agilent module interface board to general purposes Description RS 232 cable 2 m RS 232 cable 2 5 m Instrument to PC 9 to 9 pin female This cable has special pin out and is not compatible with connecting printers and plotters It s also called Null Modem Cable with full handshaking where the wiring is made between pins 1 1 2 3 3 2 4 6 5 5 6 4 7 8 8 7 9 9 RS 232 cable 8 m 69 Cable Identification Analog Cables 70 One end of these cables provides a BNC connector to be connected to Agilent modules The other end depends on the instrument to which connection is being made Agilent Module to 3394 6 Integrators p n 35900 60750 Pin 3394 6 Pin Agilent Signal Name module 1 Not connected 2 Shield Analog 3 Center Analog Agilent Module to
19. Defective electronic board in autosampler or autosampler thermostat Suggested actions Check cable connection between autosampler and autosampler thermostat Connect cable between autosampler and autosampler thermostat Exchange ASM board in the autosampler Exchange TCA board in the thermostat Contact the Agilent Technologies service organization Power Fail for Autosampler Thermostat Module Error ID 4113 The 36 that is generated in the autosampler thermostat power supply is checked by the autosampler electronics If this voltage is missing the error message will be generated Probable cause 1 Autosampler thermostat module not connected to line power 2 Autosampler thermostat module fuse s defective 3 Autosampler thermostat power supply defective Suggested actions Check correct power line connection Check fuse s and replace if defective Contact the Agilent Technologies service organization 1290 Infinity Thermostat User Manual Error Information 5 Temperature out of Range Error ID 4114 To protect the Peltier elements from damage their working range is limited to 3 to 65 The error message is generated when at least one of the four Peltier elements exceeds this limit Probable cause Suggested actions 1 The four main heat exchanger fans are not Clean the air filters and heat exchanger fins able to blow enough air through the in the autosampler thermostat Switc
20. Figure 4 on page 20 and Figure 9 on page 27 Refer to the documentation of the Agilent 1200 Infinity Series Instant Pilot or ChemStation for LC for more information In an Agilent 1290 Infinity or 1260 Infinity system the individual modules are connected by a CAN cable The Agilent 1200 Infinity Series Instant Pilot can be connected to the CAN bus at any of the modules in the system The control software can be connected to the system by one GPIB cable at any of the modules If an Agilent detector is part of the system the LAN connection must be at the detector For more information about connecting the instant pilot or control software refer to the respective user manual For connecting the Agilent 1290 Infinity equipment to non Agilent 1290 Infinity equipment see Autosampler manual 1290 Infinity Thermostat User Manual 25 3 Installing the Thermostat Installing the Thermostat 7 Connect additional cables as required see Figure 9 on page 27 0000000 Rutosampler Fraction ollector to hermostat Cable Power connector Safety lever Figure 8 Power Connectors and Safety Levers at Rear of thermostatted Autosampler Fraction Collector 26 1290 Infinity Thermostat User Manual Relay contacts Vial number output Installing the Thermostat Installing the Thermostat CAN cable to next module a C E Tu 5 B o a RR i RS232C CAN bus
21. Manual Parts for Maintenance 7 Plastic Parts Plastic Parts Figure 16 Plastic Parts Item p n Description 1 G1330 68723 Cover kit includes base top left and right 2 5065 9982 Plastics kit includes base top left and right sides 5042 8907 Leak pan solvent cabinet 1290 Infinity Thermostat User Manual 65 7 Partsfor Maintenance Plastic Parts 66 1290 Infinity Thermostat User Manual 1290 Infinity Thermostat User Manual 8 Cable Identification Cable Overview 68 Analog Cables 70 Remote Cables 72 BCD Cables 75 Auxiliary Cable 77 CAN LAN Cables 78 External Contact Cable 79 RS 232 Cable Kit 80 OE Agilent Technologies 67 Cable Identification Cable Overview 68 Never use cables other than the ones supplied by Agilent Technologies to ensure proper functionality and compliance with safety or EMC regulations Analog cables p n 35900 60750 35900 60750 01046 60105 Remote cables p n 03394 60600 03396 61010 5061 3378 01046 60201 BCD cables p n 03396 60560 G1351 81600 Description Agilent module to 3394 6 integrators Agilent 35900A A D converter Analog cable BNC to general purpose spade lugs Description Agilent module to 3396A Series integrators 3396 Series 11 3395A integrator see details in section Remote Cables on page 72 Agilent module to 3396 Series 3395B integrators Remote Cable Agilent module to general purpose Description Agilent module to 339
22. ater and mild detergent WARNING Liquid dripping into the electronic compartment of your module can cause shock hazard and damage the module gt Do not use an excessively damp cloth during cleaning Drain all solvent lines before opening any connections in the flow path 6 1290 Infinity Thermostat User Manual 57 6 Maintenance Exchanging the Power Supply Fuses When Tools required Parts required CAUTION The fuse holders are located on the rear panel of the thermostat If wrong fuses are installed Description Flat head screwdriver p n Description 2110 0015 Fuses T2 5 A 250V CSA UL listed Damaged electronics Disconnecting or reconnecting the autosampler fraction collector to thermostat cable when the power cords are connected to either of the two modules will damage the electronics of the modules In such a case mainboards of both instruments must be exchanged otherwise they can damage the other instrument gt Make sure the power cords are unplugged before disconnecting or reconnecting the autosampler fraction collector to thermostat cable 58 1290 Infinity Thermostat User Manual oo nN c Cc dA Maintenance Switch OFF the power switch at the front of the thermostatted autosampler Remove the power cable from the two modules Insert the flat head screwdriver in the fuse holder slightly press and turn counter clockwise to release the fuse holder from the socket
23. d to the Agilent modules The other end depends on the instrument to be connected to Agilent Module to General Purpose p n G1351 81600 Wire Color Pin Agilent Signal Name Digit module Green 1 BCD 5 20 p Violet 2 BCD 7 80 Ree Blue 3 BCD 6 40 a Yellow 4 BCD 4 10 E Black 5 BCD 0 1 MCN Orange 6 BCD 3 8 Red 7 BCD2 4 Brown 8 BCD 1 2 Gray 9 Digital ground Gray Gray pink 10 BCD 11 800 Red blue 11 BCD 10 400 White green 12 BCD 9 200 Brown green 13 BCD 8 100 notconnected 14 notconnected 15 5V Low 1290 Infinity Thermostat User Manual 75 8 Cable Identification Agilent Module to 3396 Integrators p n 03396 60560 Pin 3396 Pin Agilent Signal Name Digit module p 1 1 BCD 5 20 2 2 BCD 7 80 Se 15 o 3 3 BCD 6 40 So 4 4 BCD 4 10 E 5 5 BCDO 1 fre e9 6 6 BCD 3 8 Ex 7 7 BCD2 4 8 8 BCD 1 2 9 9 Digital ground NC 15 5V Low 76 1290 Infinity Thermostat User Manual Auxiliary Cable Cable Identification One end of this cable provides a modular plug to be connected to the Agilent vacuum degasser The other end is for general purpose Agilent Vacuum Degasser to general purposes p n G1322 81600 Color Pin Agilent Signal Name 1100 White 1 Ground Brown Pressure signal Green 3 Yellow 4 Grey 5 DC 5VIN Pink 6 Vent 1290 Infinity Thermostat User Manual TI Cable Identification CAN LAN Cables 78 Both ends of this cable
24. document are furnished under a license and may be used or copied only in accor dance with the terms of such license Restricted Rights Legend If software is for use in the performance of a U S Government prime contract or subcon tract Software is delivered and licensed as Commercial computer software as defined in DFAR 252 227 7014 June 1995 or as a commercial item as defined in FAR 2 101 a or as Restricted computer soft ware as defined in FAR 52 227 19 June 1987 or any equivalent agency regulation or contract clause Use duplication or dis closure of Software is subject to Agilent Technologies standard commercial license terms and non DOD Departments and Agencies of the U S Government will receive no greater than Restricted Rights as defined in FAR 52 227 19 c 1 2 June 1987 U S Government users will receive no greater than Limited Rights as defined in FAR 52 227 14 June 1987 or DFAR 252 227 7015 b 2 November 1995 as applicable in any technical data Safety Notices CAUTION A CAUTION notice denotes a hazard It calls attention to an operating procedure practice or the like that if not correctly per formed or adhered to could result in damage to the product or loss of important data Do not proceed beyond a CAUTION notice until the indicated condi tions are fully understood and met A WARNING notice denotes a hazard It calls attention to an operating procedure practice or the
25. e with full handshaking where the wiring is made between pins 1 1 2 3 3 2 4 6 5 5 6 4 7 8 8 7 9 9 RS 232 cable 8 m 1290 Infinity Thermostat User Manual 1290 Infinity Thermostat User Manual e Ove Hardware Information amp e e e amp Electrical Connections 82 Information on Instrument Serial Number 83 Rear View of the Module 84 Early Maintenance Feedback 85 This chapter describes the module in more detail on hardware and electronics NOTE manuals Details on electrical connections are described in the autosampler fraction collector Agilent Technologies 81 9 Hardware Information Electrical Connections 82 The CAN bus is a serial bus with high speed data transfer The two connectors for the CAN bus are used for internal module data transfer and synchronization The interface board slot is used for external contacts and BCD bottle number output or LAN connections The REMOTE connector may be used in combination with other analytical instruments from Agilent Technologies if you want to use features such as start stop common shut down prepare and so on With the appropriate software the RS 232C connector may be used to control the module from a computer through RS 232C connection This connector is activated and can be configured with the configuration switch The Thermostat Autosampler Fraction collector connection is used for control signal transfer and synchronization of the two m
26. e autosampler module G1329A B G1367A D G1367E G1377A G2260A G4226A G5667A G4303A or fraction collector G1364A C G1364D G5664A and the thermostat module G1330B Both modules have a separate power supply and a power plug for the line connections The two modules are connected by a control cable and both are turned on by the autosampler or fraction collector The autosampler or fraction collector power supplies have automatic voltage selectors Consequently there are no voltage selectors in the rear of the two autosampler or fraction collector modules The autosampler or fraction collector has no externally accessible fuses because automatic electronic fuses are implemented in its power supply The thermostat power supply has two externally accessible fuses Hazard of electrical shock or damage of your instrumentation can result if the devices are connected to a line voltage higher than specified gt Connect your instrument to the specified line voltage only CAUTION Inaccessible power plug In case of emergency it must be possible to disconnect the instrument from the power line at any time gt Make sure the power connector of the instrument can be easily reached and unplugged gt Provide sufficient space behind the power socket of the instrument to unplug the cable 12 1290 Infinity Thermostat User Manual Site Requirements and Specifications 2 Power Cords Different power cords are offered as opt
27. e displayed in the user interface when an electronic failure occurs with the autosampler thermostat module which requires attention In the event of such a failure the red status indicator at the front of the thermostatted autosampler is switched on and an entry is written into the instrument log book This section describes the meaning of autosampler thermostat module error messages and provides information on probable causes and suggested actions how to recover from error conditions Fan Failed Error ID 4109 Each fan in the thermostat is equipped with a speed sensor that allows monitoring and control the speed of the fans If the sensor shows no signal when the fan is activated it is very likely that the fan is defective The number in brackets indicates the fan position Position numbers of the fans are as follows seen from front of the thermostat fanfailed 1 left side fan in front position fan failed 2 left side fan back position fan failed 3 right side fan in back position fan failed 4 right side fan in front position fanfailed 5 small cooler fan on top of cooling heating module Probable cause Suggested actions 1 One of the 4 heat sink fans is defective See Service Manual for Exchanging the Heatsink Fans 2 The cooling heating module fan is defective Service Manual for Exchanging Heat Exchanger Fan 1290 Infinity Thermostat User Manual Error Information 5 Temperature Contro
28. enly distributed and streams back into the sample tray area From there it is again drawn into the thermostat This recycle mode assures a very efficient cooling heating of the sample vials In cooling mode the opposite side of the Peltier element will become very hot and to maintain the performance of the elements they have to be cooled down This is done with large heat exchangers in the back of the thermostat Four fans blow air from left to right through the instrument to remove the heated air The fan speed is controlled according to the temperature of the Peltier elements During cooling condensation will appear in the heating cooling module The condensed water will be guided out of the thermostat 1290 Infinity Thermostat User Manual 9 1 Introduction Thermostat Operation 10 1290 Infinity Thermostat User Manual 1290 Infinity Thermostat User Manual 0 2 Qeu9 Site Requirements and Specifications amp e 5 o i Site Requirements 12 Power Consideration 12 Power Cords 13 Bench Space 14 Environment 14 Physical Specifications 15 Performance Specifications 16 This chapter provides information on environmental requirements physical and performance specifications XE Agilent Technologies 11 2 Site Requirements and Specifications Site Requirements suitable site environment is important to ensure optimum performance of the instrument Power Consideration The autosamplers comprises two modules th
29. er should refer to the instruction manual in order to protect risk of harm to the operator and to protect the apparatus against damage Indicates dangerous voltages Indicates a protected ground terminal CAN Indicates eye damage may result from directly viewing the light produced by the deuterium lamp used in this product 9 The apparatus is marked with this symbol when hot surfaces are available and the user should not touch it when heated up p KITE UMS alerts you to situations that could cause physical injury or death gt Do not proceed beyond a warning until you have fully understood and met the indicated conditions CAUTION A CAUTION alerts you to situations that could cause loss of data or damage of equipment gt Do not proceed beyond a caution until you have fully understood and met the indicated conditions 88 1290 Infinity Thermostat User Manual Appendix 10 General Safety Information The following general safety precautions must be observed during all phases of operation service and repair of this instrument Failure to comply with these precautions or with specific warnings elsewhere in this manual violates safety standards of design manufacture and intended use of the instrument Agilent Technologies assumes no liability for the customer s failure to comply with these requirements WARNING Ensure the proper usage of the equipment The protection provided by the equipment may
30. flow will be stopped for safety reasons For a detector the lamp will stay on in order to avoid equilibration time Depending on the error type the next run can only be started if the error has been resolved for example liquid from a leak has been dried Errors for presumably single time events can be recovered by switching on the system in the user interface Special handling is done in case of a leak As a leak is a potential safety issue and may have occurred at a different module from where it has been observed a leak always causes a shutdown of all modules even outside a method run In all cases error propagation is done via the CAN bus or via an APG remote cable see documentation for the APG interface 1290 Infinity Thermostat User Manual General Error Messages Error Information General error messages are generic to all Agilent series HPLC modules and may show up on other modules as well Timeout Error ID 0062 The timeout threshold was exceeded Probable cause 1 The analysis was completed successfully and the timeout function switched off the module as requested 2 Anot ready condition was present during a sequence or multiple injection run for a period longer than the timeout threshold 1290 Infinity Thermostat User Manual Suggested actions Check the logbook for the occurrence and source of a not ready condition Restart the analysis where required Check the logbook for the occurrence and so
31. ft Non operating altitude Up to 4600 m 15091 ft For storing the module Safety standards IEC CSA Installation category Il Pollution degree 2 For indoor use only UL Using the module at high environmental temperatures may cause the rear panel to become hot Do not use the module at environmental temperatures higher than 50 122 F 1290 Infinity Thermostat User Manual 15 2 Site Requirements and Specifications Performance Specifications 16 Table2 Performance specifications Agilent 1290 Infinity Thermostat Type Specification Temperature range Settable from 4 C to 40 C in 1 increments Temperature accuracy at ambient 3 to 8 C at a setpoint of 4 C temperatures lt 25 C and humidity lt 50 Temperature accuracy at ambient 3 C to 9 C at a setpoint of 4 ap temperatures 30 and humidity 60 LER Measurement conditions G1329B with 100 Vial Tray in vial location 2 10 92 and 100 vials filled with water G1367A G1367B G1367C G1377A G1367E G5667A G2258A G4226A For vials Using the Thermostattable Tray G1329 60011 or 100 Micro Vial G4226 60021 both loaded with 100 vials Temperature is measured in vial locations 1 10 23 25 45 75 91 and 100 filled with 1 mL of water For well plates Standard Tray G2258 60011 for two Well Plates loaded with two Agilent 96 Well Plate 5042 1386 1290 Infinity Thermostat User Manual 1290 Infinity Thermostat User Manual 3
32. ft hand 15 position tray 1 15 Right hand 40 position tray 101 140 Right hand 15 position tray 101 115 Position 1 Position 101 Figure 12 Numbering of Tray Positions 30 1290 Infinity Thermostat User Manual Installing the Thermostat 3 Stage 5 Installing Tray Cover and Front Cover 1 Fix the tray cover in the clips of the left autosampler cover side by sliding it in position Do not close the tray cover 2 Position the front cover in the top left corner of the autosampler and turn it towards the instrument Press the stop fastener to secure it in the right side cover of the autosampler 3 Close the tray cover Tray cover pA Autosampler front door Figure 13 Installation of Tray Cover and Front Cover of the Autosampler Stage 6 Turning on the Thermostatted Autosampler Fraction collector 1 Depress the power switch to turn on the two modules The power switch stays depressed 1 and a green indicator lamp in the power switch is on when the module is turned on When the line power switch stands out 0 and the green light is off the module is turned off 1290 Infinity Thermostat User Manual 31 Installing the Thermostat Transporting the Thermostatted Autosampler or Fraction Collector When moving the autosampler or fraction collector around the laboratory make sure that any condensed water inside the thermostat is removed Tilt the module to the front so that the water inside the thermo
33. h off autosampler thermostat the thermostat and wait 10 min for the peltier elements to equilibrate Make sure that there is enough space on left and right side of the autosampler thermostat and that the air channel inlets and outlets are not blocked 2 Ambient temperature too high low Make sure that the ambient air temperature is within its specified limits 4 C to 55 1290 Infinity Thermostat User Manual 51 5 Error Information Bad Cooling Heating Performance Error ID 4120 When turned on the autosampler thermostat Peltier elements are activated according to the given setpoint or to given setpoint change The electronics check whether the actual temperature is moving in the correct direction e g decreasing when cooled down Probable cause Suggested actions 1 Peltier element s defective Contact the Agilent Technologies service organization 2 Peltier element s not connected or Check connections of the Peltier elements incorrectly connected e g after repair or maintenance 3 The four main heat exchanger fans are not Clean the air filters and heat exchanger fins able to blow enough air through the in the autosampler thermostat Switch off autosampler thermostat the thermostat and wait 10 min for the peltier elements to equilibrate Make sure that there is enough space on left and right side of the autosampler thermostat and that the air channel inlets and outlets are not blocked 52 1290
34. icates a not ready condition The module is in a not ready state when it is waiting for a specific condition to be reached or completed for example immediately after changing a set point or while a self test procedure is running An error condition is indicated when the status indicator is red An error condition indicates the module has detected an internal problem which affects correct operation of the module Usually an error condition requires attention e g leak defective internal components An error condition always interrupts the analysis If the error occurs during analysis it is propagated within the LC System i e a red LED may indicate a problem of a different module Use the status display of your user interface for finding the root cause module of the error A blinking indicator indicates that the module is in resident mode e g during update of main firmware A fast blinking indicator indicates that the module is in a low level error mode In such a case try to re boot the module or try a cold start then try a firmware update of the autosampler fraction collector for details see the manual of your autosampler fraction collector 1290 Infinity Thermostat User Manual 37 4 Troubleshooting and Diagnostics Status Indicators 38 1290 Infinity Thermostat User Manual 1290 Infinity Thermostat User Manual eo ee 5 909 Error Information e e e e What Are Error Messages 40 General Error Messages
35. ions with the module The female end of all power cords is identical It plugs into the power input socket at the rear The male end of each power cord is different and designed to match the wall socket of a particular country or region Absence of ground connection or use of unspecified power cord The absence of ground connection or the use of unspecified power cord can lead to electric shock or short circuit gt Never operate your instrumentation from a power outlet that has no ground connection gt Never use a power cord other than the Agilent Technologies power cord designed for your region Use of unsupplied cables Using cables not supplied by Agilent Technologies can lead to damage of the electronic components or personal injury gt Never use cables other than the ones supplied by Agilent Technologies to ensure proper functionality and compliance with safety or EMC regulations Unintended use of supplied power cords Using power cords for unintended purposes can lead to personal injury or damage of electronic equipment gt Never use the power cords that Agilent Technologies supplies with this instrument for any other equipment 1290 Infinity Thermostat User Manual 13 2 Site Requirements and Specifications Bench Space The module dimensions and weight see Table 1 on page 15 allow you to place the module on almost any desk or laboratory bench It needs an additional 25 cm 10 inches of space on eithe
36. juries gt To prevent personal injury be careful when getting in contact with sharp metal areas 54 1290 Infinity Thermostat User Manual Maintenance 6 WARNING Toxic flammable and hazardous solvents samples and reagents The handling of solvents samples and reagents can hold health and safety risks When working with these substances observe appropriate safety procedures for example by wearing goggles safety gloves and protective clothing as described in the material handling and safety data sheet supplied by the vendor and follow good laboratory practice gt The volume of substances should be reduced to the minimum required for the analysis gt Do not operate the instrument in an explosive atmosphere CAUTION Safety standards for external equipment gt If you connect external equipment to the instrument make sure that you only use accessory units tested and approved according to the safety standards appropriate for the type of external equipment 1290 Infinity Thermostat User Manual 55 6 Maintenance Introduction to Maintenance The module is designed for easy maintenance Maintenance can be done from the front with module in place in the system stack There are no serviceable parts inside Do not open the module 56 1290 Infinity Thermostat User Manual Maintenance Cleaning the Module To keep the module case clean use a soft cloth slightly dampened with water or a solution of w
37. l Failed 1 4 Error ID 4110 There are four Peltier elements built into the autosampler thermostat for efficient cooling heating The electronics monitor the current through the Peltier elements If the Peltier current is out of a specified limit the Peltier element is defective Probable cause Suggested actions 1 One of the four peltier elements is defective Peltier elements cannot be replaced on site Please contact Agilent Technologies service organization to initiate instrument exchange process Temperature Sensor Failed 1 4 Error ID 4111 The autosampler thermostat is equipped with four sensors to monitor the performance of the instrument The sensors are connected to both sides of the Peltier elements for control of the cooling heating efficiency As the positioning of the sensor is critical to meet the performance requirements of the autosampler thermostat the single sensors cannot be replaced separately Probable cause Suggested actions 1 Temperature sensor is defective See Service Manual for Exchanging the Sensors 1290 Infinity Thermostat User Manual 49 5 50 Error Information Lost Contact to Autosampler Thermostat Error ID 4112 The autosampler control electronics continuously check whether the autosampler thermostat is active or not Probable cause 1 Badcable connection between autosampler and autosampler thermostat 2 Cable between autosampler and thermostat module not connected 3
38. like that if not correctly performed or adhered to could result in personal injury or death Do not proceed beyond a WARNING notice until the indi cated conditions are fully under stood and met 1290 Infinity Thermostat User Manual Contents Contents 1 Introduction 5 Introduction to the Thermostat 6 Thermostat Operation 8 2 Site Requirements and Specifications 11 Site Requirements 12 Physical Specifications 15 Performance Specifications 16 3 Installing the Thermostat 17 Damaged Packaging 18 Optimizing the Stack Configuration 19 Installing the Thermostat 21 Transporting the Thermostatted Autosampler or Fraction Collector 32 4 Troubleshooting and Diagnostics 33 Agilent Lab Advisor Software 34 Overview of the Thermostat s Indicators and Test Functions 35 Status Indicators 36 5 Error Information 39 What Are Error Messages 40 General Error Messages 41 Thermostat Error Messages 48 6 Maintenance 53 Warnings and Cautions 54 Introduction to Maintenance 56 Cleaning the Module 57 Exchanging the Power Supply Fuses 58 1290 Infinity Thermostat User Manual Contents 7 Partsfor Maintenance 61 Main Assemblies External Parts 62 Accessory Kit 63 HPLC System Tool Kit 64 Plastic Parts 65 Cable Identification 67 Cable Overview 68 Analog Cables 70 Remote Cables 72 BCD Cables 75 Auxiliary Cable 77 CAN LAN Cables 78 External Contact Cable 79 RS 232 Cable Kit 80 Hardware Information 81 Elec
39. ment maintenance and repair of the opened instrument under voltage should be avoided whenever possible When inevitable this has to be carried out by a skilled person who is aware of the hazard involved Do not attempt internal service or adjustment unless another person capable of rendering first aid and resuscitation is present Do not replace components with power cable connected Do not operate the instrument in the presence of flammable gases or fumes Operation of any electrical instrument in such an environment constitutes a definite safety hazard Do not install substitute parts or make any unauthorized modification to the instrument Capacitors inside the instrument may still be charged even though the instrument has been disconnected from its source of supply Dangerous voltages capable of causing serious personal injury are present in this instrument Use extreme caution when handling testing and adjusting When working with solvents observe appropriate safety procedures for example goggles safety gloves and protective clothing as described in the material handling and safety data sheet by the solvent vendor especially when toxic or hazardous solvents are used 1290 Infinity Thermostat User Manual Appendix 10 The Waste Electrical and Electronic Equipment WEEE Directive 2002 96 EC Abstract The Waste Electrical and Electronic Equipment WEEE Directive 2002 96 EC adopted by EU Commission on 13 February
40. ntenance cable identification configuring the thermostatted autosampler appendix O Agilent Technologies 2011 2014 2015 Printed in Germany 05 2015 G1330 90014 Rev B Agilent Technologies
41. odules The cable must be installed for operation of the thermostat Make sure the power cords are unplugged before disconnecting or reconnecting the cable coupling between both modules The power input socket accepts a line voltage of 100 240 VAC 10 with a line frequency of 50 or 60 Hz Maximum power consumption varies by module There is no voltage selector on your module because the power supply has wide ranging capability There are no externally accessible fuses because automatic electronic fuses are implemented in the power supply Never use cables other than the ones supplied by Agilent Technologies to ensure proper functionality and compliance with safety or EMC regulations 1290 Infinity Thermostat User Manual Hardware Information 9 Information on Instrument Serial Number Serial Number Information 1200 Series and 1290 Infinity The serial number information on the instrument labels provide the following information CCYWWSSSSS CC YWW SSSSS Format country of manufacturing DE Germany Japan CN China year and week of last major manufacturing change e g 820 could be week 20 of 1998 or 2008 real serial number Serial Number Information 1260 Infinity The serial number information on the instrument labels provide the following information CCXZZ00000 CC ZZ 00000 1290 Infinity Thermostat User Manual Format Country of manufacturing DE Germany Japan
42. on Collector Cable THU Aii Remote cable Figure 4 Recommended Stack Configuration Rear View 20 1290 Infinity Thermostat User Manual Installing the Thermostat 3 Installing the Thermostat Module is partially energized when switched off as long as the power cord is plugged in Repair work at the module can lead to personal injuries e g shock hazard when the cover is opened and the module is connected to power gt Make sure that it is always possible to access the power plug gt Remove the power cable from the instrument before opening the cover gt Do not connect the power cable to the Instrument while the covers are removed Personal injury To avoid personal injury keep fingers away from the needle area during autosampler operation Do not bend the safety flap away from its position or attempt to remove the safety cover gt Do not attempt to insert or remove a vial from the gripper when the gripper is positioned below the needle CAUTION Defective on arrival problems If there are signs of damage please do not attempt to install the module Inspection by Agilent is required to evaluate if the instrument is in good condition or damaged gt Notify your Agilent sales and service office about the damage An Agilent service representative will inspect the instrument at your site and initiate appropriate actions 1290 Infinity Thermostat User Manual 21 3 Ins
43. ostat 3 Installing the Thermostat 3 If the thermostat is located on top of another Agilent 1200 Infinity Series module place the waste tube assembly into the top cover of the thermostat and locate the other end in the waste funnel of the module beneath Module locks Waste tube assembly Condensation leak tube Figure 5 Preparation of the Thermostat 4 Connect the condensation leak tube to the main waste exit of the thermostat and place into an appropriate vessel It is possible to either let the condensation leak tubing exit the module at the front or at the left side of the module Make sure that the leak tube is fully fixed on the outlet Condensation leak tube Waste bottle Figure 6 Condensation Leak outlet 1290 Infinity Thermostat User Manual 23 3 Installing the Thermostat Installing the Thermostat 5 Install the front cover of the thermostat 6 Place the autosampler fraction collector module on top of the thermostat Make sure that the autosampler fraction collector is correctly engaged in the thermostat locks 7 Remove the tray and place the air channel adapter into the autosampler fraction collector tray base Make sure the adapter is fully pressed down This assures that the cold airstream from the thermostat is correctly guided to the tray area of the autosampler or fraction collector Air channel adapter Figure 7 Air channel adapter 8 Install the diffusion plate on the air channel adap
44. perature sensors leak sensor and board mounted temperature compensation sensor are used by the leak algorithm to determine whether a leak is present When a leak occurs the leak sensor is cooled by the solvent This changes the resistance of the leak sensor which is sensed by the leak sensor circuit on the main board Probable cause Suggested actions 1 Loose fittings Ensure all fittings are tight 2 Broken capillary Exchange defective capillaries Open Cover Error ID 0205 The top foam has been removed Probable cause Suggested actions 1 Foam not activating the sensor Please contact your Agilent service representative 2 Defective sensor or main board Please contact your Agilent service representative 46 1290 Infinity Thermostat User Manual Error Information 5 Cover Violation Error ID 7461 The top foam has been removed The sensor on the main board detects when the top foam is in place If the foam is removed while the lamps are on or if an attempt is made to switch on for example the lamps with the foam removed the lamps are switched off and the error message is generated Probable cause Suggested actions 1 The top foam was removed during Please contact your Agilent service operation representative 2 Foam not activating the sensor Please contact your Agilent service representative 1290 Infinity Thermostat User Manual 47 5 Error Information Thermostat Error Messages 48 Error messages ar
45. product that can be used with or without data system Agilent Lab Advisor software helps to manage the lab for high quality chromatographic results and can monitor in real time a single Agilent LC or all the Agilent GCs and LCs configured on the lab intranet Agilent Lab Advisor software provides diagnostic capabilities for all Agilent 1200 Infinity Series modules This includes diagnostic capabilities calibration procedures and maintenance routines for all the maintenance routines The Agilent Lab Advisor software also allows users to monitor the status of their LC instruments The Early Maintenance Feedback EMF feature helps to carry out preventive maintenance In addition users can generate a status report for each individual LC instrument The tests and diagnostic features as provided by the Agilent Lab Advisor software may differ from the descriptions in this manual For details refer to the Agilent Lab Advisor software help files The Instrument Utilities is a basic version of the Lab Advisor with limited functionality required for installation use and maintenance No advanced repair troubleshooting and monitoring functionality is included 1290 Infinity Thermostat User Manual Troubleshooting and Diagnostics 4 Overview of the Thermostat s Indicators and Test Functions Status Indicators The thermostatted autosampler is provided with two status indicators which indicate the operational state prerun run and error states of
46. provide a modular plug to be connected to Agilent modules CAN or LAN connectors CAN Cables p n 5181 1516 5181 1519 LAN Cables p n 5023 0203 5023 0202 Description CAN cable Agilent module to module 0 5 m CAN cable Agilent module to module 1 m Description Cross over network cable shielded 3 m for point to point connection Twisted pair network cable shielded 7 m for point to point connection 1290 Infinity Thermostat User Manual External Contact Cable 10 6 One end of this cable provides a 15 pin plug to be connected to Agilent modules interface board The other end is for general purpose Cable Identification Agilent Module Interface Board to general purposes p n G1103 61611 Color Pin Agilent Signal Name module White 1 EXT 1 Brown EXT 1 Ecce Green 3 EXT 2 UI Yellow 4 EXT2 Grey 5 EXT 3 Pink 6 EXT 3 Blue 7 EXT 4 Red 8 EXT 4 Black 9 Not connected Violet 10 Not connected Grey pink 11 Not connected Red blue 12 Not connected White green 13 Not connected Brown green 14 Not connected White yellow 15 Not connected 1290 Infinity Thermostat User Manual 79 Cable Identification RS 232 Cable Kit 80 p n G1530 60600 RS232 61601 5181 1561 Description RS 232 cable 2 m RS 232 cable 2 5 m Instrument to PC 9 to 9 pin female This cable has special pin out and is not compatible with connecting printers and plotters It s also called Null Modem Cabl
47. r side and approximately 8 cm 3 1 inches in the rear for air circulation and electric connections If the bench shall carry a complete HPLC system make sure that the bench is designed to bear the weight of all modules The module should be operated in a horizontal position Environment Your modules will work at ambient temperatures and relative humidity as described in Table 1 on page 15 CAUTION Condensation within the module Condensation will damage the system electronics gt Do not store ship or use your module under conditions where temperature fluctuations could cause condensation within the module gt f your module was shipped in cold weather leave it in its box and allow it to warm slowly to room temperature to avoid condensation 14 1290 Infinity Thermostat User Manual Site Requirements and Specifications 2 Physical Specifications Table 1 Physical Specifications Type Specification Comments Weight 20 7 kg 46 Ibs Dimensions height x 140 x 345 x 435 mm 5 5 x 13 5 x 17 width x depth inches Line voltage 100 240 VAC 10 Wide ranging capability Line frequency 50 or 60 Hz 5 96 Power consumption 260 VA 210 W 717 BTU Maximum Ambient operating 4 40 C 39 104 F See warning temperature page 15 Ambient non operating 40 70 C 40 158 F temperature Humidity lt 95 r h at 40 104 F Non condensing Operating altitude Up to 2000 m 6562
48. sentative 1290 Infinity Thermostat User Manual Error Information 5 Compensation Sensor Short Error ID 0080 The ambient compensation sensor NTC on the main board in the module has failed short circuit The resistance across the temperature compensation sensor NTC on the main board is dependent on ambient temperature The change in resistance is used by the leak circuit to compensate for ambient temperature changes If the resistance across the sensor falls below the lower limit the error message is generated Probable cause Suggested actions 1 Defective main board Please contact your Agilent service representative Fan Failed Error ID 0068 The cooling fan in the module has failed The hall sensor on the fan shaft is used by the main board to monitor the fan speed If the fan speed falls below a certain limit for a certain length of time the error message is generated Depending on the module assemblies e g the lamp in the detector are turned off to assure that the module does not overheat inside Probable cause Suggested actions 1 Fan cable disconnected Please contact your Agilent service representative 2 Defective fan Please contact your Agilent service representative 3 Defective main board Please contact your Agilent service representative 1290 Infinity Thermostat User Manual 45 5 Error Information Leak Error ID 0064 leak was detected in the module The signals from the two tem
49. stat can safely flow into the leak funnel Otherwise no special precautions are needed for the modules Heavy weight The module is heavy 20 7 kg 45 6 Ibs Carry the module at least with 2 people gt Avoid back strain or injury by following all precautions for lifting heavy objects gt Ensure that the load is as close to your body as possible gt Ensure that you can cope with the weight of your load CAUTION Mechanical damage of the module If the transport assembly is not parked the module could be damaged due to excessive shock of the shipping container during transport gt Always park the transport assembly before shipment 32 If the autosampler or fraction collector needs to be shipped to another location via carrier ensure The two modules are shipped in separate boxes The transport assembly of the autosampler or fraction collector is parked see Park Arm Park Gripper in your respective Service Manual for more information The vial tray is secured 1290 Infinity Thermostat User Manual 1290 Infinity Thermostat User Manual 4 Troubleshooting and Diagnostics Agilent Lab Advisor Software 34 Overview of the Thermostat s Indicators and Test Functions 35 Status Indicators 36 Power Supply Indicator 36 Module Status Indicator 37 RE Agilent Technologies 33 4 Troubleshooting and Diagnostics Agilent Lab Advisor Software 34 The Agilent Lab Advisor software is a standalone
50. t Technologies sales and service office Table3 Thermostat Checklist Description Quantity Part Number Thermostat 1 Power cable 1 as ordered Accessory kit see Accessory 1 61330 68755 page 63 for more information HPLC System Tool Kit optional see 1 G4203 68708 HPLC System Tool Kit on page 64 for more information 1290 Infinity Thermostat User Manual Installing the Thermostat 3 Optimizing the Stack Configuration Optimizing the Stack Configuration If your autosampler fraction collector is part of a system you can ensure optimum performance by installing the autosampler fraction collector in the stack in the position shown in Figure 3 on page 19 and Figure 4 on page 20 This configuration optimizes the system flow path ensuring minimum delay volume As the autosampler thermostat is very heavy it should always be installed at the bottom of a stack Instant Pilot Detector le Column compartment TL rims IN Solvent cabinet Degasser optional Autosampler ALS Fraction collector Thermostat for the ALS Fraction collector optional Figure 3 Recommended Stack Configuration Front View 1290 Infinity Thermostat User Manual 19 3 Installing the Thermostat Optimizing the Stack Configuration LAN to control software RAN Bus cable to Instant Pilot xp u E Autosampler Fracti
51. talling the Thermostat CAUTION Damaged electronics Disconnecting or reconnecting the autosampler fraction collector to thermostat cable when the power cords are connected to either of the two modules will damage the electronics of the modules In such a case mainboards of both instruments must be exchanged otherwise they can damage the other instrument gt Make sure the power cords are unplugged before disconnecting or reconnecting the autosampler fraction collector to thermostat cable Stage 1 Preparing the Thermostat and Autosampler Fraction Collector Damage through condensation If the condensation tube is located in liquid the condensed water cannot flow out of the tube and the outlet is blocked Any further condensation will then remain in the instrument This may damage the instruments electronics gt Make sure the condensation tube is always above the liquid level in the vessel gt Make sure the waste container is not sealed gt Ensure the drain tube has no loops and leads directly into the waste bottle Even under average humidity conditions a significant amount of condensed water gathers every day A suitable container must be provided and emptied regularly in order to avoid overflow 1 Place the thermostat on the bench or in the stack 2 Remove the front cover Press the two snap fasteners on the sides of the cover and move it away 22 1290 Infinity Thermostat User Manual Installing the Therm
52. ter Diffusion plate 9 Re install the tray 24 1290 Infinity Thermostat User Manual Installing the Thermostat 3 10 If there is no Agilent 1260 1290 Infinity Series module located beneath the thermostat connect the waste tube to the central waste exit of the autosampler fraction collector and place in a waste vessel Stage 2 Power Cable and Interface Cable Connection CAUTION Damaged electronics Disconnecting or reconnecting the autosampler fraction collector to thermostat cable when the power cords are connected to either of the two modules will damage the electronics of the modules In such a case mainboards of both instruments must be exchanged otherwise they can damage the other instrument gt Make sure the power cords are unplugged before disconnecting or reconnecting the autosampler fraction collector to thermostat cable 1 Ensure the power switch on the front of the autosampler fraction collector is OFF and the power cables are disconnected 2 Connect the cable between the autosampler fraction collector and the thermostat see Figure 8 on page 26 3 Move the safety lever at the rear of the two modules to the right position see Figure 8 on page 26 4 Connect the power cables to the power connectors 5 Connect the CAN interface cables to other modules in the system see Figure 4 on page 20 and Figure 9 on page 27 6 If required connect additional interface and control cables to the autosampler see
53. the instrument Both are located on the autosampler module The status indicators provide a quick visual check of the operation of the thermostatted autosampler see Status Indicators on page 36 Error Messages In the event of an electronic mechanical or hydraulic failure the instrument generates an error message in the user interface For details on error messages and error handling please refer to the Agilent Lab Advisor software 1290 Infinity Thermostat User Manual 35 4 Troubleshooting and Diagnostics Status Indicators Two status indicators are located on the front of the autosampler The lower left indicates the power supply status the upper right indicates the thermostatted autosampler status Status indicator Power supply indicator Figure 14 Location of Status Indicators Power Supply Indicator The power supply indicator is integrated into the main power switch When the indicator is illuminated green the power is ON 36 1290 Infinity Thermostat User Manual Troubleshooting and Diagnostics 4 Module Status Indicator The Thermostat itself has no status indicator Any Error condition will only show up on the Autosampler Fraction Collector status LED s When the status indicator is OFF and power switch light is on the module is in a prerun condition and is ready to begin an analysis green status indicator indicates the module is performing an analysis run mode A yellow indicator ind
54. tly for analysis 2 Defective remote cable Exchange the remote cable 3 Defective components in the instrument Check the instrument for defects refer to the showing the not ready condition instrument s documentation 1290 Infinity Thermostat User Manual Error Information 5 Lost CAN Partner Error ID 0071 During an analysis the internal synchronization or communication between one or more of the modules in the system has failed The system processors continually monitor the system configuration If one or more of the modules is no longer recognized as being connected to the system the error message is generated Probable cause Suggested actions 1 CAN cable disconnected Ensure all the CAN cables are connected correctly Ensure all CAN cables are installed correctly 2 Defective CAN cable Exchange the CAN cable 3 Defective main board in another module Switch off the system Restart the system and determine which module or modules are not recognized by the system Leak Sensor Short Error ID 0082 The leak sensor in the module has failed short circuit The current through the leak sensor is dependent on temperature A leak is detected when solvent cools the leak sensor causing the leak sensor current to change within defined limits If the current increases above the upper limit the error message is generated Probable cause Suggested actions 1 Defective leak sensor Please contact your Agilent service
55. trical Connections 82 Early Maintenance Feedback 85 10 Appendix 87 General Safety Information 88 The Waste Electrical and Electronic Equipment WEEE Directive 2002 96 EC 91 Radio Interference 92 Sound Emission 93 Agilent Technologies Internet 94 1290 Infinity Thermostat User Manual 1290 Infinity Thermostat User Manual Introduction Introduction to the Thermostat 6 Thermostat Operation 8 de Agilent Technologies 1 Introduction Introduction to the Thermostat The Agilent 1290 Infinity Thermostat is designed for use with other modules of the Agilent 1200 Infinity Series or with other LC systems if adequate remote control inputs and outputs are available The thermostat is controlled from the Agilent 1200 Infinity Series Instant Pilot or from your Agilent control software for LC systems The specially designed thermostattable sample trays holds either 100 x 1 8 mL vials or two wellplates and 10 x 1 8 mL vials The thermostat contains Peltier controlled heat exchangers A fan draws air from the area above the sample vial tray of the autosampler and then blows it through the fins of the cooling heating module There it is cooled or heated according to the temperature setting The thermostatted air enters the autosampler through a recess underneath the specially designed sample tray The air is then distributed evenly through the sample tray ensuring effective temperature control regardless of how many vials
56. urce of a not ready condition Restart the analysis where required 41 5 5 42 Error Information Shutdown Error ID 0063 external instrument has generated a shutdown signal on the remote line The module continually monitors the remote input connectors for status signals A LOW signal input on pin 4 of the remote connector generates the error message Probable cause Suggested actions 1 Leak detected in another module with a Fix the leak in the external instrument before CAN connection to the system restarting the module 2 Leak detected in an external instrument Fix the leak in the external instrument before with a remote connection to the system restarting the module 3 Shut down in an external instrument with a Check external instruments for a shut down remote connection to the system condition Remote Timeout Error ID 0070 A not ready condition is still present on the remote input When an analysis is started the system expects all not ready conditions for example a not ready condition during detector balance to switch to run conditions within one minute of starting the analysis If a not ready condition is still present on the remote line after one minute the error message is generated Probable cause Suggested actions 1 Not ready condition in one of the Ensure the instrument showing the not ready instruments connected to the remote line condition is installed correctly and is set up correc
57. user settable EMF limits for the EMF Counters enable the early maintenance feedback to be adapted to specific user requirements The useful maintenance cycle is dependent on the requirements for use Therefore the definition of the maximum limits need to be determined based on the specific operating conditions of the instrument Setting the EMF Limits The setting of the EMF limits must be optimized over one or two maintenance cycles Initially the default EMF limits should be set When instrument performance indicates maintenance is necessary take note of the values displayed by the EMF counters Enter these values or values slightly less than the displayed values as EMF limits and then reset the EMF counters to zero The next time the EMF counters exceed the new EMF limits the EMF flag will be displayed providing a reminder that maintenance needs to be scheduled 1290 Infinity Thermostat User Manual 85 9 Hardware Information Early Maintenance Feedback 86 1290 Infinity Thermostat User Manual 1290 Infinity Thermostat User Manual 10 Appendix General Safety Information 88 The Waste Electrical and Electronic Equipment WEEE Directive 2002 96 EC 91 Radio Interference 92 Sound Emission 93 Agilent Technologies on Internet 94 RE Agilent Technologies 87 10 Appendix General Safety Information Safety Symbols Table4 Safety Symbols Symbol Description The apparatus is marked with this symbol when the us
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