User`s Manual
Contents
1. CI SS 3 5 lt 2 N o o Q I D D ZINIO 512 2 5 2 7 lt lt ZSSS Zle Bl o E o 5 00 o TI O C0C o gt gt 5 COMPONENT MATERIAL lt miu T 2 Elbow N2 Polyamid Nylon D D D D D D Blower Impeller Polyamid Nylon D D D D D p Blower Housing Polypropylene IIIT Exhaust Hose Polyethylene l C1 N2 Supply Hoses Polyethylene Seele Block Guides UMHW Polyethylene C Window Seal PVC CID c b Lid Epoxy Coated Alum l CI Chamber amp Block JAluminum D p bip p Nozzle N2 Stainless Steel 000 D Exhaust Fitting Stainless Steel D D D Ducting Epoxy Coated Steel C Window Glass C Moderate Degradation Questionable Use D Severe Degradation Infrequent use recommended immediate thorough cleaning required joo lolo Trifluoroacetic Acid TFA B Bases OJO Potassium Hydroxide C E o 5 li O Bi M E C Solvents OJO Methylene Chloride 59 I Pal ad Hexanes 0 ety Acetate l j o ethan 10 Product Service 1 800 522 7658 Toluene O O O IO O Chapter 3 Getting Started e Glasslids are suitable for use with all common compounds When using compounds in the RapidVap Vertex Evaporator that are hostile to the materials of construction it is imperative that the equipment2. Product Service 1 800 522 7658 19 Chapter 4 Using Your RapidVap Vertex Evaporator Operational Notes The LCD display conveys various pieces of information When the RapidVap Vertex Evaporator is turned ON the RapidVap Vertex Evaporator will return to the same mode RUN or STOP that it was in when the power was turned off If the RapidVap Vertex Evaporator was in the RUN mode when the power was turned OFF when the power is turned ON the RapidVap Vertex Evaporator will attempt to return to the programmed set points If the previous run is to be duplicated it is important to press the Stop button prior to pressing Run This will reset the timer back to the programmed set point Without pressing the program set point button the time will not be reset and will continue to count down from the time at which it was stopped Interrupting a Cycle After it Has Begun At any time during a run the cycle may be stopped by pressing the Pause button This shuts off the nitrogen flow and pauses the timer but the heater remains active If it is necessary to re start the RapidVap Vertex Evaporator close the lid and press RESTART The RapidVap Vertex Evaporator will resume operation at the same set point parameters and the timer will continue to count down from the time at which the RapidVap Vertex Evaporator was paused 20 Product Service 1 800 522 7658 CHAPTER 5 MAINTAINING YOUR RAPIDVAP VERTEX EVAPORATOR Under n
3. PROG and the display will show PROG TEMP TIME 35 62 Press Back to return to the opening display press Run to start this program If the program temperature or time needs to be changed press either PROG TEMP or TIME The display will show PROG TEMP TIME 3 67 14 Back Up Down Run Ten different programs may be stored and then later recalled Press PROG or TEMP or TIME and the word will start to flash Press Up or Down to change the value Another word may be selected and the value under the word may be changed by pressing Up or Down Press either Run to begin the run or press Back to return to the opening display If TIME is set to ON the program will run continually until turned off by pressing STOP or PAUSE 16 Product Service 1 800 522 7658 Chapter 4 Using Your RapidVap Vertex Evaporator Pre Heat If it is necessary to pre heat the chamber before starting a run press Pre Heat This display will show SET BLOCK SAMP TEMP 52 51 85 Stop Press Stop to return to the opening display and turn off the heater or press SET TEMP to set the pre heat temperature The display will show SET BLOCK SAMP TEMP 52 51 90 The SET TEMP will flash Then press Up or Down to adjust the block temperature In this example 52 is the temperature of the sample block 51 is the upp
4. 7321600 Block 16 mm dia x 125 mm long tubes Holds 50 7322000 Block 20 mm dia x 150 mm long tubes Holds 50 7322800 Block 28 mm dia x 95 mm long tubes Holds 18 7322801 Block 28 mm dia x 140 mm long tubes Holds 18 32 Product Service 1 800 522 7658 Protecting vour PAN laboratory environment b 4 LABCONCO CORPORATION 816 333 8811 B 821 5525 8811 Prospect Avenue FAX 816 363 Kansas City MO 64132 2696 www labconco sng CE Declaration of Conformity We Labconco Corporation 8811 Prospect Avenue Kansas City MO 64132 USA Ph 816 333 8811 Fax 816 363 0130 labconco labconco com being the representative party in the EU solely responsible for this certification hereby declare that the following product Equipment Laboratory Equipment RapidVap Vertex Evaporator Type Model 7320030 230V EU 7320035 230V UK 7320037 230V China Manufacturer Labconco Corporation 8811 Prospect Avenue Kansas City MO 64132 USA Ph 816 333 8811 Fax 816 363 0130 labconco labconco com is in conformity with the standards listed below EN61010 1 EN61326 1 EN55022 EN61000 3 2 3 following the provisions of the following directives 89 336 EEC 2004 108 EC 2006 95 EC when installed and operated in accordance with the manufacturers installation and operating instructions Kansas ey USA 2 l6 20l Place and date of issue Mark Schm Vice President Research and Engineering Labconco Corporat
5. TO ATTACH MARK RELEASE TUBE PUSHING TUBE IN BEFORE PULLING IT OUT HELPS TO RELEASE TUBE THE NITROGEN SUPPLY PRESSURE MUST NEVER BE Ya ALLOWED TO EXCEED 50 PSI 345 KPA HOSE CLAMP EXHAUST HOSE ROUTED TO VENTILATION DEVICE HOSE ATTACHED TO GAS SUPPLY Exhaust Port Ifthe RapidVap Vertex Evaporator is not located in a fume hood attach one end of the two inch diameter venting hose that is supplied with the RapidVap Vertex Evaporator to the exhaust port on the rear of the unit Clamp securely Route the other end to a fume hood or other laboratory ventilation device Product Service 1 800 522 7658 Chapter 3 Getting Started Electrical Connection Plug the power cord into the receptacle on the back of the RapidVap Vertex Evaporator and plug the other end into a suitable wall power receptacle Chemical Attack on RapidVap Vertex Evaporator Components Your RapidVap Vertex Evaporator is designed to be chemical resistant to most compounds that are commonly used in the concentration processes that are performed in it However by necessity the RapidVap Vertex Evaporator is comprised of a number of different materials some of which may be attacked and degraded by certain chemicals The degree of degradation is obviously dependent on the concentration and duration of exposure Some of the major components of the RapidVap Vertex Evaporator that are susceptible to degradation are as follows Acids 3
6. Vertex Evaporator Vacuum models 7320030 7320035 7320037 7320040 4A Frequency all models 50 60 Hz Phase Single Heater power 900 watts Environmental Conditions Indoor use only Maximum altitude 6562 feet 2000 meters Ambient temperature range 41 to 104 F 5 to 40 C Maximum relative humidity 80 for temperatures up to 88 F 31 C decreasing linearly to 50 relative humidity at 104 F 40 C Main supply voltage fluctuations not to exceed 10 of the nominal voltage Transient overvoltages according to Installation Categories II Overvoltage Categories per IEC 1010 Temporary voltage spikes on the AC input line that may be as high as 1500V for 115V models and 2500V for 230V models are allowed Product Service 1 800 522 7658 29 Appendix C RapidVap Vertex Evaporator Specifications e Used in an environment of Pollution degrees 2 i e where normally only non conductive atmospheres are present Occasionally however a temporary conductivity caused by condensation must be expected in accordance with IEC 664 Nitrogen Consumption e Gas flow RapidVap Vertex Evaporator with 10 active nozzles 0 74 SCFM 15 psi 21 L min 103 KPA 1 00 SCFM 24 psi 28 3 L min 165 KPA e Gas flow RapidVap Vertex Evaporator with 50 active nozzles 4 5 SCFM 20 psi 127 L min 138 KPA 5 00 SCFM 24 psi 141 5 L min 165 KPA 30 Product Service 1 800 522 7658 Appendix C RapidVap Vertex Evaporator Specifica
7. is properly maintained e After each run clean up all residues spills and materials that might have splashed in the chamber using agents suitable for the substance involved With prudent maintenance your RapidVap Vertex Evaporator will provide many years of service Warranty on the affected parts will be void if maintenance has obviously been neglected If you have questions about using specific compounds in your RapidVap Vertex Evaporator contact Labconco Technical Service at 1 800 821 5525 or 816 333 8811 or e mail labconco labconco com Solvent Safety Precautions The RapidVap Vertex Evaporator is not classified as explosion proof It has been designed with safety as a primary consideration and should be used in a prudent manner using good laboratory practices It has been designed for use with compounds as described in the United States National Electrical Code Class I Group D The block that holds the sample tubes may be programmed to run as hot as 100 C however the heater element may normally run at 135 C A thermal fuse limits the heater to a maximum temperature of 152 C It is important that the solvents used are compatible with these temperatures Do not evaporate solvents that have an autoignition temperature below 180 C Do not evaporate solvents that Ei are classified as Group A B or C by the National Electrical Code Evaporate only non flammable or Group D solvents with autoignition temperatures 180 C
8. 1 800 522 7658 7 Chapter 3 Getting Started Setting Up Your RapidVap Vertex Evaporator After you verify the RapidVap Vertex Evaporator components move your RapidVap Vertex Evaporator to the location where you want to install it Then follow the steps listed below Sample Block The RapidVap Vertex Evaporator was shipped without the sample block installed See Appendix D for available blocks Vials must be snug in the holes in the block Select the appropriate block to fit the vials that will be used Make certain that the bottom of the chamber is clean and free of debris The sample block slides in on the two guides on the front and MUST rest securely on the bottom Make certain that the small 21 dia temperature sensor hole is in the upper left hand corner Placing the block in the chamber improperly will effect performance Insert the tubular temperature sensor into the 21 dia hole to monitor upper block temperature The actual sample temperature may be monitored throughout a run by placing the sensor directly into a sample vial SAMPLE HOLDING BLOCK 8 Product Service 1 800 522 7658 Chapter 3 Getting Started Nitrogen Gas Connection Mark the gas supply hose 3 4 19 mm from the end and push the hose into the fitting in the back of the RapidVap Vertex Evaporator Attach the other end of the hose to user supplied nitrogen supply OPERATION OF QUICK CONNECT FITTINGS SIMPLY PUSH IN TO INSERT TUBE TO 3 4 PUSH IN COLLET
9. 58 CHAPTER 4 UsiNG YouR RAPIDVAP VERTEK EVAPORATOR After your RapidVap Vertex Evaporator has been installed as detailed in Chapter 3 Getting Started you are ready to begin using your RapidVap Vertex Evaporator Read this chapter to learn how to set operating parameters operate the controls properly select and position glassware Inside your RapidVap Vertex Evaporator understand the display interrupt a cycle after it has begun not specified by the manufacturer refer to Appendix C RapidVap Vertex Evaporator Specifications The electrical Fi Do not use the RapidVap Vertex Evaporator in a manner protection properties of the RapidVap Vertex Evaporator may be impaired if the RapidVap Vertex Evaporator is used inappropriately Product Service 1 800 522 7658 13 Chapter 4 Using Your RapidVap Vertex Evaporator Planning Thoroughly understand procedures and the equipment operation prior to beginning work The unique performance of the RapidVap Vertex Evaporator is dependent upon the proper balance of heat and nitrogen flow If the proper balance is not established it is possible to damage or lose a portion of the sample Therefore if you are unfamiliar with the RapidVap Vertex Evaporator or are attempting a new protocol it may be helpful to make a trial run that is void of the sample you are attempting to concentrate Select the size of the sample tube so it is compatible with the block Tubes should not be loose in
10. TER 4 USING YOUR RAPIDVAP VERTEX EVAPORATOR Planning Loading Glassware into the RapidVap Vertex Evaporator RapidVap Vertex Evaporator Controls Operating the RapidVap Vertex Evaporator Controls Operating the RapidVap Vertex Evaporator Operational Notes Interrupting a Cycle After it has Begun CHAPTER 5 MAINTAINING YOUR RAPIDVAP VERTEX EVAPORATOR Ne 13 14 14 14 15 19 20 20 21 CHAPTER 6 TROUBLESHOOTING APPENDIX A RAPIDVAP VERTEX EVAPORATOR COMPONENTS APPENDIX B RAPIDVAP VERTEX EVAPORATOR DIMENSIONS APPENDIX C RAPIDVAP VERTEX EVAPORATOR SPECIFICATIONS Evaporation Rates APPENDIX D RAPIDVAP VERTEX EVAPORATOR ACCESSORIES DECLARATION OF CONFORMITY 22 25 28 29 31 32 33 CHAPTER INTRODUCTION Congratulations on your purchase of a Labconco RapidVap Vertex Evaporator Models are available for operation on 115V or 230V Superior evaporation rates are achieved by the unique blending of several gentle forces on the sample The vials containing the sample are held at an angle to increase the surface area of the sample thereby increasing the evaporation rate A precisely controlled amount of thermal energy can be supplied to the sample to heat it Finally a stream of nitrogen or dry gas is directed downward onto the surface of the sample This reduces the partial pressure directly over the liquid to speed evaporation and helps remove the solvent as it evaporates In summary the RapidVap Vertex Eva
11. User s Manual RapidVap Vertex Evaporator Models 73200 Series To receive important product updates complete your product registration card online at register labconco com Protecting your laboratory environment LS LABCONCO Labconco Corporation 8811 Prospect Avenue Kansas City MO 64132 2696 800 821 5525 816 333 8811 FAX 816 363 0130 E MAIL labconco labconco com HOME PAGE www labconco com Please read the User s Manual before operating the equipment Copyright 2011 Labconco Corporation All rights reserved The information contained in this manual and the accompanying products are copyrighted and all rights reserved by Labconco Corporation Labconco Corporation reserves the right to make periodic design changes without obligation to notify any person or entity of such change Warranty Labconco provides a warranty on all parts and factory workmanship The warranty includes areas of defective material and workmanship provided such defect results from normal and proper use of the equipment The warranty for all Labconco products will expire one year from date of installation or two years from date of shipment from Labconco whichever is sooner except the following e Purifjer Logic Biological Safety Cabinets and PuriCare Lab Animal Research Stations carry a three year warranty from date of installation or four years from date of shipment from Labconco whichever is sooner SteamScru
12. bber amp FlaskScrubber Glassware Washers carry a two year warranty from date of installation or three years from date of shipment from Labconco whichever is sooner Blood Drawing Chairs carry a ten year warranty Carts carry a lifetime warranty Glassware is not warranted from breakage when dropped or mishandled This limited warranty covers parts and labor but not transportation and insurance charges In the event of a warranty claim contact Labconco Corporation or the dealer who sold you the product If the cause is determined to be a manufacturing fault the dealer or Labconco Corporation will repair or replace all defective parts to restore the unit to operation Under no circumstances shall Labconco Corporation be liable for indirect consequential or special damages of any kind This statement may be altered by a specific published amendment No individual has authorization to alter the provisions ofthis warranty policy or its amendments Lamps and filters are not covered by this warranty Damage due to corrosion or accidental breakage is not covered Returned or Damaged Goods Do not return goods without the prior authorization from Labconco Unauthorized returns will not be accepted If your shipment was damaged in transit you must file a claim directly with the freight carrier Labconco Corporation and its dealers are not responsible for shipping damages The United States Interstate Commerce Commission rules require that claim
13. below Operating the RapidVap Vertex Evaporator 1 Turn the power switch ON Turn the nitrogen supply on Select a program or set the temperature and time parameters Solvents will evaporate quicker at warmer temperatures Use care to avoid damaging the samples Preheat the block if desired Open a nitrogen control valve for the row of nozzles to be used Make sure the lid is closed Set the nitrogen pressure by first selecting the rows of nozzles to be used during the run Then press run to open the gas supply valve Pull out the regulator knob and turn the knob until the desired pressure is displayed in the center ofthe knob Evaporation rates will be higher at increased pressure However splashing of the sample may occur It is advisable to perform a set up run void of analytes to determine the optimal pressure for the tube and sample size being used Push the knob in Turn off the gas supply by pressing Stop or open the lid Place samples in vials and place vials into the block If monitoring actual sample temperature place the temperature probe into sample vial making sure the wires do not cover any nozzles Close the lid Press Run on the display At the end of the programmed time the heater and nitrogen flow will turn off Ifthe display time was set to ON the run continues until Stop or Pause is pressed 10 The lid may be opened and samples removed Use caution because the block and samples may be hot
14. ent parts If other parts are required contact Product Service Product Service 1 800 522 7658 25 Appendix A RapidVap Vertex Evaporator Components RapidVap Vertex Evaporator Components Item Quantity Part No Description 1 5 7320400 Manifold 2 1 7323700 Blower 3 1 7353300 Temperature Sensor Lower 4 1 7325100 Over Temperature Cut Out 5 2 1544600 Inlet Fitting 6A 1 7321800 Control Valve 115V 6B 1 7321801 Control Valve 230V 7 1 3823803 Power Supply SA 1 1289310 Circuit Breaker 10A 115V 8B 2 1289306 Circuit Breaker 6A 230V 9 1 1302300 Power Switch 10 1 7321400 Label Control Panel 11 1 7321900 Pressure Regulator 12 5 7322500 Valve Toggle 13 1 7323100 PCB 14 1 7323000 LCD 15 1 7355301 Temperature Sensor Upper 26 Product Service 1 800 522 7658 Appendix A RapidVap Vertex Evaporator Components Product Service 1 800 522 7658 27 APPENDIX B RAPIDVAP VERTEX EVAPORATOR DIMENSIONS INCHES CENTIMETERS LID SHOWN IN OPEN POSITION 28 Product Service 1 800 522 7658 APPENDIX C RAPIDVAP VERTEX EVAPORATOR SPECIFICATIONS This Appendix contains technical information about the RapidVap Vertex Evaporator including specifications environmental operations conditions wiring diagrams and evaporation rates Electrical Specifications Nominal amperage for 115V RapidVap Vertex Evaporator model 7320020 8A Nominal amperage for 230V RapidVap
15. er block or sample temperature The heater will heat the block and maintain it at the set temperature Press Stop to turn the heater off and to return to the opening display Product Service 1 800 522 7658 17 Chapter 4 Using Your RapidVap Vertex Evaporator Run To re run the last program while in the opening display press Run The heater will be powered the master nitrogen control valve will open the time will start to count down and the display will show BLOCK SAMP TIME 52 51 124 Pause Stop Prog In this example 52 indicates the sample block temperature 51 indicates the upper block temperature or sample temperature and 124 indicates the time remaining for this programmed run Press Pause to temporarily halt the run BLOCK SAMP TIME 57 55 67 Re Start Stop Prog The word Pause will be replaced with Re Start which when pressed will continue the run from the point where it was paused Press Stop to halt the run entirely The display will show the opening screen 18 Product Service 1 800 522 7658 Chapter 4 Using Your RapidVap Vertex Evaporator If PROG is pressed in the middle of a run the display will show the programmed parameters for that run PROG TEMP TIME 3 84 103 Parameters may not be altered Press Back to return to the operating screen Then if the run parameters must be altered press Stop and re program the display as described
16. evel and of solid construction In addition an exhaust means must be provided and a source of nitrogen or dry gas must be available An electrical source must be located near the installation site Carefully read this chapter to learn e the electrical supply requirements e the exhaust requirements e the nitrogen supply requirements Refer to Appendix C RapidVap Vertex Evaporator Specifications for complete RapidVap Vertex Evaporator electrical and environmental conditions specifications and requirements Product Service 1 800 522 7658 3 Chapter 2 Prerequisites Electrical Requirements A dedicated electrical outlet is required Minimum requirements for an outlet is a 15 Amp circuit breaker or fuse for models rated at 115V 60 Hz or an 8 Amp circuit breaker or fuse is required for 230V 50 60 Hz models 115V models are equipped with a 15 Amp NEMA 5 15P plug 230V models are available with a NEMA 6 15P plug for use in the United States a PS 1363 plug for use in the United Kingdom a CEE 7 7 plug for use in Europe or a CHI 10P plug for use in China It may be necessary to remove the plug and install a different plug to match the available receptacle if one of these models does not meet your needs Location and Exhaust Requirements The RapidVap Vertex Evaporator must be located within a fume hood if hazardous or flammable solvents are used In all cases regardless of the solvent used it is recommended that the exhaust hose is ven
17. he control valves that will be used during the run Turn the unit ON and press Run the main gas supply valve will open Pull the knob of the Pressure Regulator out and rotate the knob clockwise to Increase pressure counter clockwise to decrease the pressure The operating pressure is displayed on the knob Once the pressure is set push the regulator knob in and press Stop The pressure can be adjusted at any time during the run Also note that opening or closing any of the Nitrogen Control Valves without adjusting the pressure will change the flow rate at each nozzle The flow rate of gas is approximately 1 cfm 28 3 L min per row of 10 nozzles when pressure is set at 24 PSI 165 KPA Digital Display The touch screen LCD is used to control run time and temperature preheat temperature and other functions as described below Operating the RapidVap Vertex Evaporator Controls When the power switch on the left hand side is turned ON the opening display will show BLOCK SAMP 52 51 C Run Pre Heat Prog In all diagrams the numbers are Just examples and will vary Press open area above C or F symbol to change the degree display to show C or F All parameters that are entered will be remembered in the microprocessor memory and will remain entered until reset Product Service 1 800 522 7658 15 Chapter 4 Using Your RapidVap Vertex Evaporator Program To enter a new program while in the opening display press
18. ion Labconco P N 3696080 Rev Product Service 1 800 522 7658 33
19. or above Use of other compounds could cause an explosion Solvents used in the RapidVap Vertex Evaporator may be flammable or hazardous Use extreme caution and keep sources of ignition away from the solvents When using flammable or hazardous solvents the RapidVap Vertex Evaporator should be operated inside a fume hood If a sample is spilled in the chamber it must immediately be cleaned up Hazardous materials such as strong acids or bases radioactive substances and volatile organics must be handled carefully and promptly cleaned up if spilled Product Service 1 800 522 7658 11 Chapter 3 Getting Started 12 Several components of the RapidVap Vertex Evaporator which are located inside the chamber are made of stainless steelor aluminum which can be attacked by acids Use of acids such as trifluoroacetic acid can result in degradation of the product Use care when using aggressive liquids which can damage the RapidVap Vertex Evaporator and thoroughly clean the RapidVap Vertex Evaporator after each use Contact Labconco before evaporating acids WARNING The disposal of substances used in connection with this equipment may be governed by various Federal State or local regulations All users of this equipment are urged to become familiar with any regulations that apply in the user s area concerning the dumping of waste materials in or upon water land or air and to comply with such regulations Product Service 1 800 522 76
20. ormal operation the RapidVap Vertex Evaporator requires little maintenance The following maintenance schedule is recommended As needed 1 3 Clean up all spills remove liquids from chamber Clean lid and viewing window using soft cloth sponge or chamois and a mild non abrasive soap or detergent Clean block using non abrasive soap or detergent Monthly 1 4 The rubber components on the RapidVap Vertex Evaporator may eventually deteriorate and require replacement The effective life of rubber parts depends upon both their usage and the surrounding environment Check all rubber hoses and gaskets and replace any that show signs of hardening permanent set or deterioration Using a soft cloth sponge or chamois and a mild non abrasive soap or detergent clean the lid and viewing window Using a soft cloth sponge or chamois and a mild non abrasive soap or detergent clean the exterior surfaces of the unit Liquid spray cleaners and polishes may be used on the exterior surfaces Do not use solvents to remove stains from the exterior surfaces as they may damage the finish Blocks should be cleaned Product Service 1 800 522 7658 21 CHAPTER TROoUBLESHOOTING Refer to the following if your RapidVap Vertex Evaporator fails to operate properly If the suggested corrective actions do not solve your problem contact Labconco for additional assistance PROBLEM Unit will not operate Sample odor in lab Sol
21. porator performance is maximized by increasing the sample s surface area increasing temperature and directing gas over the sample The microprocessor provides excellent regulation of the heater and reproducibility of protocols Product Service 1 800 522 7658 1 iS 7 Chapter 1 Introduction Typographical Conventions Recognizing the following typographical conventions will help you understand and use this manual e Book chapter and section titles are shown in italic type e g Chapter 3 Getting Started e Steps required to perform a task are presented in a numbered format e Comments located in the margins provide suggestions reminders and references e Critical information is presented in boldface type in paragraphs that are preceded by the exclamation icon Failure to comply with the information following an exclamation icon may result in injury to the user or permanent damage to your RapidVap Vertex Evaporator e Important information is presented in capitalized type in paragraphs that are preceded by the pointer icon It is imperative that the information contained in these paragraphs be thoroughly read and understood by the user 2 Product Service 1 800 522 7658 CHAPTER 2 PREREQUISITES Before you install your RapidVap Vertex Evaporator you need to prepare your site for installation Carefully examine the location where you intend to install your RapidVap Vertex Evaporator You must be certain that the area is l
22. roduct Service 1 800 522 7658 Chapter 3 Getting Started Unpacking Your RapidVap Vertex Evaporator Carefully unpack your RapidVap Vertex Evaporator and inspect it for damage that may have occurred in transit If your RapidVap Vertex Evaporator is damaged notify the delivery carrier immediately and retain the entire shipment intact for inspection by the carrier Do not discard the carton or packing material for your RapidVap Vertex Evaporator until you have checked all of the components and installed and tested the RapidVap Vertex Evaporator DO NOT RETURN GOODS WITHOUT THE PRIOR AUTHORIZATION OF LABCONCO UNAUTHORIZED RETURNS WILL NOT BE ACCEPTED IF YOUR RAPIDVAP VERTEX EVAPORATOR WAS DAMAGED IN TRANSIT YOU MUST FILE A CLAIM DIRECTLY WITH THE FREIGHT CARRIER LABCONCO CORPORATION AND ITS DEALERS ARE NOT RESPONSIBLE FOR SHIPPING DAMAGES RapidVap Vertex Evaporator Components Locate the model of RapidVap Vertex Evaporator you received in the following table Verify that the components listed are present and undamaged Catalog Description 7320020 RapidVap Vertex Evaporator 115V Plus the Following Part Component Description 7913100 Exhaust Hose 1966000 Clamp 1334500 Power Cord NEMA 5 15P 7324400 User s Manual 1533301 Tubing 6 Product Service 1 800 522 7658 The United States Interstate Commerce Commission rules reguire that claims be jiled with the delivery carrier within fifteen 15 days of delive
23. ry Chapter 3 Getting Started Catalog Description 7320030 RapidVap Vertex Evaporator 230V EU Plus the Following Part Component Description 7913100 Exhaust Hose 1966000 Clamp 1336100 Power Cord CEE 7 7 7324400 User s Manual 1533301 Tubing Catalog Description 7320035 RapidVap Vertex Evaporator 230V UK Plus the Following Part Component Description 7913100 Exhaust Hose 1966000 Clamp 1332600 Power Cord PS 1363 7324400 User s Manual 1533301 Tubing Catalog Description 7320037 RapidVap Vertex Evaporator 230V China Plus the Following Part Component Description 7913100 Exhaust Hose 1966000 Clamp 1332700 Power Cord CHI 10P 7324400 User s Manual 1533301 Tubing Catalog Description 7320040 RapidVap Vertex Evaporator 230V US Plus the Following Part Component Description 7913100 Exhaust Hose 1966000 Clamp 1338000 Power Cord NEMA 6 15P 7324400 User s Manual 1533301 Tubing Since users preference of sample size varies the sample holding block is not included with the RapidVap Vertex Evaporator The correct size block must be selected and ordered separately Refer to Appendix D RapidVap Vertex Evaporator Accessories for block selection If you do not receive one or more of the components listed for your RapidVap Vertex Evaporator or if any of the components are damaged contact Labconco Corporation immediately for further instructions Product Service
24. s be filed with the delivery carrier within fifteen 15 days of delivery Limitation of Liability The disposal and or emission of substances used in connection with this equipment may be governed by various federal state or local regulations All users of this equipment are required to become familiar with any regulations that apply in the user s area concerning the dumping of waste materials in or upon water land or air and to comply with such regulations Labconco Corporation is held harmless with respect to user s compliance with such regulations Contacting Labconco Corporation If you have questions that are not addressed in this manual or if you need technical assistance contact Labconco s Customer Service Department or Labconco s Product Service Department at 1 800 821 5525 or 1 816 333 8811 between the hours of 7 00 a m and 6 00 p m Central Standard Time Part 7324400 Rev ECO F205 TABLE Or CONTENTS CHAPTER 1 INTRODUCTION Typographical Conventions CHAPTER 2 PREREQUISITES Electrical Requirements Location and Exhaust Requirements Nitrogen Supply Requirements Space Requirements Tools Required CHAPTER 3 GETTING STARTED Unpacking Your RapidVap Vertex Evaporator RapidVap Vertex Evaporator Components Setting Up Your RapidVap Vertex Evaporator Sample Block Nitrogen Gas Connection Exhaust Port Electrical Connection Chemical Attack on RapidVap Vertex Evaporator Components Solvent Safety Precautions CHAP
25. ted into a fume hood or other laboratory ventilation device Nitrogen Supply Requirements The 1 4 I D hose on the rear of the RapidVap Vertex Evaporator should be attached to a regulated source of nitrogen or other suitable gas Pressure must NOT exceed 50 psi The nitrogen supply must be capable of 6 5 CFM flow rate A suitable barb or compression fitting must be supplied by the user Space Requirements Refer to Appendix B RapidVap Vertex Evaporator Dimensions for dimensional drawings of the RapidVap Vertex Evaporator Tools Required Common hand tools are required to set up the RapidVap Vertex Evaporator A screwdriver or 5 16 socket is needed to attach hose clamps A tubing cutter or knife is needed to shorten exhaust hoses 4 Product Service 1 800 522 7658 CHAPTER 3 GETTING S TARTED Now that the site for your RapidVap Vertex Evaporator is properly prepared you are ready to unpack inspect install and test your RapidVap Vertex Evaporator Read this chapter to learn how to unpack and move your RapidVap Vertex Evaporator setup your RapidVap Vertex Evaporator connect the nitrogen source to your RapidVap Vertex Evaporator connect the electrical supply source to your RapidVap Vertex Evaporator properly exhaust your RapidVap Vertex Evaporator solvent safety precautions The RapidVap Vertex Evaporator weighs over 35 Ibs 16 Kg The carton allows for lifting with a mechanical lift truck or hand truck P
26. the block Blocks are available with holes for various size tubes Loading Glassware Into the RapidVap Vertex Evaporator There are 5 control valves that control nitrogen to the 5 horizontal rows of nozzles Samples should be positioned in complete rows as much as possible This will minimize the number of rows of nozzles and reduce gas consumption RapidVap Vertex Evaporator Controls The control panel for the RapidVap Vertex Evaporator is shown below with a description about their function DIGITAL DISPLAY amp TOUCH SCREEN OQO O O 000 O O 000 060 0009000060 G3 080 O O 080 O O 000 AQ 080 O 080 O O 000 NITROGEN ma 060 0 O 080 O O oeo PRESSURE REGULATOR NITROGEN CONTROL VALVES 14 Product Service 1 800 522 7658 Chapter 4 Using Your RapidVap Vertex Evaporator Nitrogen Control Valves Used to turn nitrogen flow ON or OFF to the nozzles above the sample vials The top valve controls the 10 nozzles on the top row The second valve controls the second row of 10 nozzles The third valve controls the middle row of 10 nozzles The fourth valve controls the fourth row of 10 nozzles The bottom valve controls the bottom row of 10 nozzles Push the lever to the right to turn nitrogen flow ON Nitrogen Pressure Regulator Used to adjust the gas pressure and gas flow rate to the nozzles To adjust the gas pressure to the nozzles the gas supply must be connected Open all of t
27. tions Evaporation Rates Solvent Tube Size Number of Sample Temp C N Pressure Avg Time to mm Samples Size ml PSI Dry min Acetonitrile 12x 75 10 2 35 16 19 12x 75 10 2 45 16 lt 15 12x75 10 2 60 16 1l 12x 75 10 2 80 16 lt 8 Methanol 12x75 10 2 35 24 s12 12 x75 10 2 45 24 10 12x 75 10 2 60 24 lt 7 12 x75 10 2 80 24 lt 6 12 x 75 50 2 80 24 lt 6 20 x 150 10 10 52 37 lt 42 Water 12x 75 10 2 45 24 125 12x 75 10 2 60 24 80 12x 75 10 2 80 24 lt 40 12 x75 10 2 100 24 lt 25 20 X 150 10 4 100 24 lt 60 20 X 150 50 4 100 24 lt 64 Toluene 12x 75 10 2 35 16 24 12x 75 10 2 45 16 18 12x 75 10 2 60 16 13 12x 75 10 2 80 16 9 Methylene 12x 75 10 2 35 20 lt 8 Chloride 12 x 75 10 2 45 22 lt 7 20 x 150 10 10 38 31 22 Hexane 20 x 150 10 10 52 37 1I Ethyl Acetate 20x 150 10 10 52 37 22 Time to Dry is the time for samples in each of the indicated number of sample tubes to evaporate The time to dry for any individual sample tube may be considerably longer or shorter Product Service 1 800 522 7658 31 APPENDIX D RAPIDVAP VERTEX EVAPORATOR CCESSORIES PART DESCRIPTION 7324100 Block 10 mm dia x 75 mm long tubes Holds 50 7321200 Block 12 mm dia x 75 mm long tubes Holds 50 7321300 Block 13 mm dia x 100 mm long tubes Holds 50
28. vent in bottom of chamber Poor recovery rates CAUSE Unit not connected to electrical power Circuit breaker blown Lid open Vent hose exhausting into lab area Inoperable blower Gas pressure too high Sample going to dryness Sample splashing out of tube Heat setting is too high CORRECTIVE ACTION Connect unit to proper electrical receptacle Correct electrical problem and reset circuit breaker by pressing button Close lid Redirect hose to fume hood Replace blower Reduce pressure Program time to prevent dryness Decrease Nitrogen pressure Decrease heat 22 Product Service 1 800 522 7658 Chapter 6 Troubleshooting PROBLEM CAUSE Evaporation rate is Gas supply depleted reduced Heater inoperable No gas flow Gas depleted Sample position not activated Nozzle clogged Valve inoperable Gas flows Valve inoperable continuously Control inoperable CORRECTIVE ACTION Replenish gas supply Contact Labconco Install new supply of gas Activate position per operating instructions Unplug nozzle with fine wire Contact Labconco Contact Labconco Contact Labconco Product Service 1 800 522 7658 23 Chapter 6 Troubleshooting 24 Product Service 1 800 522 7658 APPENDIX A RAPIDVAP VERTEX EVAPORATOR COMPONENTS The following pages list components that are available for your RapidVap Vertex Evaporator The parts shown are the most common replacem
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