HIAC Model 3000A Liquid Syringe Sampler
Contents
1. Note The stir bar will naturally center in the target area on the sampler Those customers who want to offset the stir bar may simply slide the sensor so that the probe is off center from the target This causes the sample bottle to be placed off center and the stir bar to be offset from the probe 7 While holding the sensor barrel and twisting the sensor slowly back and forth tighten the sensor capture bolt using the 3 16 Allen wrench Tighten the block until the sensor no longer twists easily in the block 8 Connect the sampler sensor tubing to the sensor by connecting the small captive bolt to the outlet side of the sensor Use a crescent wrench Note Steady the sensor holding block with your hand while attaching the sampler sensor tube to the sensor 9 Feed the sampler sensor tubing through the groove on the sensor holding block Secure in place by tightening the 3 32 bolt on the plastic washer using the 3 32 Allen wrench 10 Connect the sensor communications cable to the appropriate port on the rear panel of the particle counter Installation Location of sensor arm fastening bol Location of sensor capture bolt Figure 1 3000A Sensor holding block HRLD and MicroCount 05 3 5 MicroCount 05 sensor installation This section provides the operator with information to install a MicroCount 05 liquid particle sensor on the HIAC Model Model 3000A Liquid Syringe Sampler Model 3000A samplers modified to2. 232 cable from the sampler to the appropriate COM port on the rear panel of the PC 2 Open the Windows operating system and select the Terminal program by double clicking on the Terminal icon 3 Enter the Settings Communications dialog box Select the correct COM port then set the communications to 9600 baud rate 8 data bits no parity and 1 stop bit Click on the OK button to close this dialog box 4 Enter the Settings Terminal Preferences dialog box Select Line Wrap Local Echo and Inbound for CRACR LF These settings are optional for communications but help make the process more understandable for the operator 5 Begin sending commands to the sampler There is no need to phone the sampler the sampler is already listening after the operator established communications parameters 6 Type Q and press lt CR gt The sampler should respond with Q0 if everything is OK Any other number or character in the last position represents an error code and no response indicates a possible cable problem 19 Maintenance and Troubleshooting The table below shows the error codes for the 3000A sampler Meaning Sampler not initialized 1 Sampler plunger overload Sampler valve overload Sampler command overflow ICI 8 Litmechanismiammed ee Syringe drive COM error Note Error codes 1 2 6 7 and A require the operator to cycle power to the instrument before resuming operations If the sampler retu
3. 5 Maintenance and Troubleshooting 19 5 1 Using terminal emulation for diagnostics c ccc ccecccseccceeeeeeeeceeecececeecesaeesseesaeeseueeseeessusesaaes 19 9 2 Fuse le Ee reet 21 SA O ne dd dd ated atta taa Seales tater 21 54 Syringe malntenance ss ss need dc 22 ES tise anls te aee tale aatindeadeneainearues 22 Section 6 Warranty and Contact Information 23 6 1 MINES GWG AVY eset g cis ceclaetc eee re geste tues te fe fl dinar ne at fee Me is destin 23 6 2 Del VICE COMLACE le reien E te BEE 24 6 2 1 USA ere ae 24 6 22 International Custo Me Sisi aL 24 6 29 Information TE QUISO ui aa 24 0 9 SEET EE dese EE 24 Section Eet 25 Table of Contents Section 1 Specifications are subject to change without notice Instrument operation Specifications Flow rate accuracy Sample flow rate Volume accuracy Tare volumes for probes Wetted materials chemical compatibility 10 100 mL min Note actual flow rate determined by the particular sensor calibration flow rate lt 1 at 1 0 mL for 1 0 ml syringe lt 1 at 5 0 mL for 10 0 ml syringe lt 1 at 5 0 mL for 25 0 ml syringe 0 06 in small bore probe 0 172 mL 0 25 in 5 5 in long standard probe 0 25 in 8 5 in long extender probe 1 02 mL 1 57 mL PTFE Teflon TFE Teflon PFA Teflon Kel F Borosilicate glass Schott BK7 Stainless steel 316 Viton Emerson Cummings Stycast 2850 A
4. and unloading on page 12 4 3 2 BACK FLUSH 4 3 3 PRIME When the operator presses BACK FLUSH the 3000A will reverse flow through the sampling system forcing liquid back through the sensor with a high positive pressure supplied by the syringe drive Backflushing is a useful tool to clear a sensor blockage In addition the operator can backflush to clean the sampler system lines by placing the outlet line in water or some cleaning solution When the operator presses PRIME the 3000A will run 3 consecutive 2 ml samples through the sensor and sampling system Priming rids the sample line of air bubbles that could affect the particle counting process 4 3 4 TARE ONLY 16 When the operator presses TARE ONLY the 3000A will pull just the tare volume through the instrument This function is useful when performing the volumetric accuracy test required for USP lt 788 gt Operation 4 4 The 3000A setup screen The operator accesses the 3000A Setup screen by pressing the 3000A SETUP key After the operator presses the key the 8000A will display the following screen 3723 94 9 53 55 Hiac Rouco SJHHHA Sampler Parameters Flow rate el mL min syringe size 16 mL Tare volume 1 56 mL Auto unload No Enter value between 16 66 and 166 66 30884 DI gi TARE SETUP 408 WARES UV ON Figure 7 Model 8000A 3000A Sampler functions screen The operator then enters the flow rate syringe size and tare volume Note For a
5. bolt and washer from the back side of the sensor holding block using a 3 32 Allen wrench Remove the tubing from the groove 3 Attach this small bolt and plastic washer to the lower portion of the sensor holding block in the threaded hole provided 4 Remove the fastening bolt from the sensor holding block using a 3 16 Allen wrench Take the sensor holding block off of the sensor arm 5 Attach the sensor holding block to the extender arm The operator can install the sensor holding block in two positions an upper and lower position The lower position corresponds to use of the sampler without the extender arm The top position is closer to the wide section in the tubing groove The tubing grooves on the sensor holding block and the extender arm should match up when properly connected Put the aligning pin in the hole and tighten the fastening bolt with a 3 16 Allen wrench 6 Take the sensor arm out of the sampler by removing the two bolts with a 5 32 Allen wrench Use the bolts from the sensor arm to attach the extender arm to the sampler Installation 7 Connect tubing extension assembly to the sampler sensor tubing Thread tubing through the grooves in the extender arm and sensor holding block The fittings on the tubing extension assembly should fit in the wide area of the groove in the extender arm Note Do not pull on sampler tubing Pulling on the sampler tubing may cause flow problems with the Sampler 8 Tighten
6. hinges on the sides of the assembly and will swing down covering the power cord connector Inside the fuse box is a fuse holder that is brown with a white arrow Put the screwdriver on the side of the fuse box toward which the arrow points then pull in the opposite direction from the arrow to free the fuse holder from the fuse box Remove the fuse from the fuse holder and verify its failure Replace with a new fuse of the same rating and tolerances Replace the fuse holder in the fuse box Make sure that the arrow on the fuse holder points in the same direction as the arrows on the fuse box Close the fuse box The door will snap in place Figure 8 Fuse box and fuse holder 3000A rear panel With use the exterior of the instrument may become dirty or soiled If liquid spills on the exterior or the instrument becomes dirty follow the steps below to clean the instrument Note Verify all panels are in place and the interior components are not exposed before starting this procedure 1 Wipe the exterior surfaces with a moist rag 2 Ifthe instrument is still not clean wipe the exterior surfaces with soap and warm water Rinse thoroughly with water 3 Ifthe instrument is still not clean moisten a lint free tissue with Isopropyl Alcohol Wipe the exterior surfaces with the moistened tissue 21 Maintenance and Troubleshooting 5 4 Syringe maintenance 5 5 Spare parts 22 The Cavro syringes provided for the syringe dr
7. operate with the MicroCount 05 sensor are identified by a red sticker affixed to the rear panel on the instrument CAUTION A To prevent damage to the internal cell during MicroCount 05 sensor installation you must use the modified coupling p n 047156 03 with the Probe Assembly Adapter p n 084205 01 included in the accessory kit The Model 3000A sampler allows easy installation of a HIAC MicroCount 05 liquid particle sensor The sampler ships with all of the necessary adapters to perform the sensor installation To install the sensor the operator will need a 3 16 Allen wrench supplied in the accessory kit and an adjustable wrench 3 5 1 Sensor purchased with the Model 3000A 1 Loosen the sensor capture bolt on the sensor holding block using the 3 16 Allen wrench 2 Install the Probe Assembly Adapter p n 084205 01 into the sensor holding block from the rear of the sampler Center the probe over the target on the sampler and tighten the sensor capture bolt shown on the following illustration using the 3 16 Allen wrench 3 Remove both strips of Velcro from the accessory kit Remove the adhesive backing from the loop half of the Velcro strip and press to the baseplate of the MicroCount 05 body between the mounting screws opposite the communications cable Remove the adhesive backing from the second loop half and press to the baseplate of the MicroCount 05 body between the mounting screws next to the sensor inlet port Installa
8. rket med dette symbol ma ikke bortskaffes i europ iske offentlige affaldssystemer efter den 12 august 2005 henhold til europ iske lokale og nationale regler EU direktiv 2002 96 EF skal europeeiske brugere af elektriske apparater nu returnere gamle eller udtjente apparater til producenten med henblik pa bortskaffelse uden omkostninger for brugeren Bemeerk forbindelse med returnering til genbrug skal du kontakte producenten eller leverandgren af apparatet for at fa instruktioner om hvordan udtjente apparater bortskaffes korrekt 25 Certification 26 SVENSKA Elektronikutrustning som ar markt med denna symbol kanske inte kan lamnas in pa europeiska offentliga sopstationer efter 2005 08 12 Enligt europeiska lokala och nationella foreskrifter EU direktiv 2002 96 EC maste anvandare av elektronikutrustning i Europa nu aterlamna gammal eller utrangerad utrustning till tillverkaren for kassering utan kostnad for anvandaren Obs Om du ska terl mna utrustning f r tervinning ska du kontakta tillverkaren av utrustningen eller terf rs ljaren for att fa anvisningar om hur du aterlamnar kasserad utrustning for att den ska bortskaffas pa r tt s tt ESPANOL A partir del 12 de agosto de 2005 los equipos el ctricos que lleven este s mbolo no deber n ser desechados en los puntos limpios europeos De conformidad con las normativas europeas locales y nacionales Directiva de la UE 2002 96 EC a partir de esa fecha los usua
9. system consult the software operator s manual Connect the RS 232 communications cable between the RS 232 port on the rear panel of the 3000A and the J103 ADS port on the rear panel of the 9064 For information related to particle counting applications and 3000A sampler control commands with the 9064 and PharmSpec refer to the PharmSpec Operations Manual 17 Operation Section 5 Maintenance and Troubleshooting There are two main types of problems that can occur in the 3000A 1 Electrical such as power and communications 2 Mechanical such as syringe drive stall or sample line blockage The operator can diagnose most problems without difficulty using the information provided in this document For further assistance contact a local Hach Ultra service representative 5 1 Using terminal emulation for diagnostics The operator can use a PC with a terminal emulation program to identify many types of errors including e Communications errors e Error codes amp diagnostics sent by the 3000A e Local hangups where the sampler fails to respond to button presses Using a terminal emulation program the operator can send the sampler all of the commands available from a particle counter This document describes the use of a specific terminal emulation program Microsoft Windows Terminal MS Windows is a copyright of the Microsoft Corporation but any terminal emulation program will operate in a similar way 1 Connect the RS
10. 700 100 0062 HIAC Model 3000A Liquid Syringe Sampler USER MANUAL September 2008 Edition 5 EXCELLENCE IN PROCESS ANALYTICS Table of Contents DECOM aper 3 Section 2 General INfOorMAtION 2 28e dee 5 e SCAN a ee de ee esse de cn eee 5 AS a 5 2221 ISS Ol NaAZ Al Reeg le ita de 5 22 2 EEC AUN AMADO Se 6 2 39 Safety recommendations cnt lid andado 6 Section 3 RE CHE ON unir dd 7 3 1 RIAC Model 3000A Sampler e TEE T 32 General ei Eelere EEN T 39 ege EI Ee 6 1 tere A EE T 34 ER SENSOM INSTA ALON RE 8 Xo Tee elle fl E UE e std aos 9 3 5 1 Sensor purchased with the Model 3000A cccceccceseeeeeeeeeteeeceeeteneeeneceeeseeeteestaeeteeeees 9 3 0 2 SENSOr PUCNASEH Separate EE 10 3 07 DrAIN INS EE 11 3 7 Sampler cable CONMNMECLIONS SR an a A nc 11 3 60 OWED Cable COMEN iii etes 12 3 9 General notes on syringe loading and unloading 12 Section 4 OPETAN eai e ao ta di 13 A1 Rhett 13 ATA AICA OS A A Ad 13 EL AS e Ene o A cane yiwne hae eaten ensiecas gasanettiededs 13 43 SETa nd EDAD DUO a 13 41 4 SLOW and FAST EENS 13 iso Synge LOAD DURON Ae 14 40 o leier BO Ce EI TEE 14 4 27 8000A Wee e EE 14 4 3 Sampler functions available from the Model GOOOA 16 LS WR e GE LE EE 16 2 DAS FEUS H EE 16 ASS PERIME EE 16 LA TAE ON e io 16 4 4 The 3000A SetuP SON AAA 17 4 5 Running the particle counting system from the Model GOOUA 17 4 0 Q064 MOM ACS iii a is 17 Section
11. Indicators The indicators are a set of numbers from 0 to 9 The number light indicates the speed of the magnetic stir mechanism in the 3000A The number 9 represents maximum speed about 550 rpm the number 1 represents minimum speed about 170 rpm and the number 0 indicates that the stir bar motor is off The adjustment of the stir bar motor speed is explained under SLOW and FAST buttons below 4 1 2 STOP button Pressing the STOP button on the 3000A causes any sample run to abort and sensor lift operations to terminate The stir bar motor will continue to function A sample run may also be stopped from the particle counter refer to the particle counter operators manual for additional information 4 1 3 SET and LOAD buttons The operator uses the SET and LOAD buttons to manipulate the sensor lift mechanism The SET buttons establish the bottom position for sensor lift mechanism travel The operator will want to change this position depending upon the type of bottle or beaker used for sampling Two set speeds are available the operator can either press and hold a SET button for rapid motion or press and release a SET button for precise placement The bottom position determined with the SET buttons is saved by the 3000A until a new bottom position is established Pressing the LOAD button causes the sensor lift mechanism to travel from its bottom set point to home position the highest point in its range of motion or vice vers
12. R FITNESS FORA PARTICULAR NON CONTRACTUAL PURPOSE HACH ULTRA ANALYTICS RESPONSIBILITY TO REPAIR OR REPLACE DEFECTIVE PRODUCTS IS THE SOLE AND EXCLUSIVE REMEDY PROVIDED TO THE CUSTOMER FOR BREACH OF THIS WARRANTY HACH ULTRA ANALYTICS AND ITS VENDORS WILL NOT BE LIABLE FOR ANY INDIRECT SPECIAL INCIDENTAL OR CONSEQUENTIAL DAMAGES EVEN IF HACH ULTRA ANALYTICS OR ITS VENDORS HAS BEEN GIVEN ADVANCED NOTICE OF THE POSSIBILITY OF SUCH DAMAGES 23 6 2 Service contact information 6 2 1 U S A customers 6 2 2 By Telephone 541 472 6500 6 30 a m to 5 00 p m PST Monday through Friday By Fax 541 474 7414 By Mail Hach Ultra 481 California Avenue Grants Pass Oregon 97526 Email TechSupportGP hachultra com Website www hachultra com International customers By Telephone 41 22 594 64 00 By Fax 41 22 594 64 99 By Mail Hach Ultra service Department 6 route de Compois C P 212 CH 1222 V senaz Geneva Switzerland Website www hachultra com 6 2 3 Information required e Your name e Model number e Your phone number e Serial number e Your company name e Comment or question e Your fax number 6 3 Return for repair 24 To facilitate efficient handling of instruments returned for repair a Return Authorization Number RA is required Request a Return Authorization Number using the contact information shown above Have information on the type model of instrument and nature of the malfu
13. a 4 1 4 SLOW and FAST buttons The SLOW button decrements the stir bar motor speed by one position 48rpm for each button press For example if the current stir bar motor speed is 6 and the desired speed is 3 press SLOW three times The FAST button increments the stir bar motor speed by one position 48 rom for each button press For example if the current stir bar speed is 5 and the desired speed is 7 press FAST two times 13 Operation 4 1 5 Syringe LOAD button A When the operator presses the syringe load button a white syringe symbol and the word LOAD on a black background the sampler syringe drive will send the syringe plunger to either its bottom or top travel position When the syringe plunger is at its bottom travel point the operator can load or unload a syringe Note Early production samplers do not have the syringe LOAD button labelled The LOAD button is the blank button on the upper row of buttons on these units 4 1 6 Syringe CLEAN button 4 2 8000A interface 14 When the operator presses the syringe clean button a white syringe symbol and the word CLEAN on a black background the sampler will draw a full syringe of fluid into the sampler through the sensor and push this fluid out through the drain tubing The operator should use the syringe clean function to clean the sampler with a mild detergent then flush the sampler with clean particle free water Note Early production sa
14. anual for more information on the load syringe commands With the syringe drive plunger bolt set at its bottom travel point the operator can load or unload a syringe To load the syringe into the syringe drive 1 Remove the drive bolt from the syringe drive mechanism 2 Fasten the syringe to the drive by bolting the drive bolt through the syringe plunger 3 Pull up on the syringe until the luer fitting mates with the teflon fitting at the top of the syringe drive 4 Twist the syringe until the connection is secure Do not overtighten the connection A Overtightening may cause teflon extrusion and connector degradation Each size syringe has the same plunger travel distance so this procedure allows changing to different volume syringes When loading or removing a syringe twist the syringe into and out of the fitting Repeated lateral movement of the syringe will cause damage to the teflon syringe fitting To unload a syringe from the syringe drive use the load unload commands from the appropriate system to set the plunger bolt at its bottom point and reverse the steps of the procedure presented above For additional information on the syringe refer to Syringe maintenance on page 22 12 Section 4 Operation 4 1 User interface 5 The front panel of the 3000A contains 8 active buttons and 2 sets of indicators AUTO LIFT gt gt SLOW FAST STIR SPEED PRESSURE 23456 78 Figure 3 Setup dialog box 4 1 1
15. ben Hinweis Bitte wenden Sie sich an den Hersteller bzw an den Handler von dem Sie das Gerat bezogen haben um Informationen zur R ckgabe des Altger ts zur ordnungsgem en Entsorgung zu erhalten FRANCAIS A partir du 12 aout 2005 il est interdit de mettre au rebut le mat riel lectrique marqu de ce symbole par les voies habituelles de d chetterie publique Conform ment a la r glementation europ enne directive UE 2002 96 EC les utilisateurs de mat riel lectrique en Europe doivent d sormais retourner le mat riel us ou p rim au fabricant pour limination sans frais pour l utilisateur Remarque Veuillez vous adresser au fabricant ou au fournisseur du mat riel pour les instructions de retour du mat riel us ou p rim aux fins d limination conforme ITALIANO Le apparecchiature elettriche con apposto questo simbolo non possono essere smaltite nelle discariche pubbliche europee successivamente al 12 agosto 2005 In conformita alle normative europee locali e nazionali Direttiva UE 2002 96 EC gli utilizzatori europei di apparecchiature elettriche devono restituire al produttore le apparecchiature vecchie o a fine vita per lo smaltimento senza alcun costo a carico dell utilizzatore Nota Per conoscere le modalita di restituzione delle apparecchiature a fine vita da riciclare contattare il produttore o il fornitore dell apparecchiatura per un corretto smaltimento DANSK Elektriske apparater der er m
16. ccurate particle counting and sizing the operator must enter the flow rate at which the sensor was calibrated This information is available on the calibration curve supplied with the sensor Hach Ultra recommends a minimum tare volume of 5 of the syringe volume By drawing this tare volume before counting begins the sampler can establish a stable flow rate When the operator enters a syringe size the tare volume automatically defaults to this 5 value However the operator may increase or decrease the tare volume based on the application requirements 4 5 Running the particle counting system from the Model 8000A Once the operator has input the parameters for the sampler the operator returns to the main menu by pressing EXIT several times The operator then sets up run parameters as specified in the Model 8000A Operations Manual Refer to the Model 8000A Operations Manual for all particle counting related information After all parameters are established the operator runs the system by pressing the START key on the main menu of the Model 80004 As long as the setup remains the same operation is one touch only requiring use of the START key 4 6 9064 interface The 9064 particle counter interfaces with the 3000A sampler through RS 232 communications The 9064 is operated through a computer system and special software This manual does not address the software for more information on using particular software with the counting
17. dhesive Operating temperature range 5 40 C 40 104 F Operating humidity range Instrument Compatibility Physical characteristics Dimensions 0 80 relative humidity non condensing Model 8000A counter Model 9064 counter MicroCount 05 sensor HRLD 150 400 and 400HC sensors MicroCount 05 Sensor PharmSpec software 12 x 11 x 19 wxd xh 30 cm x 28 cm x 48 cm Weight 20 4 Ibs 9 3 kg Sample bottle clearance Standard unit 5 8 14 7 cm Extension kit 9 0 22 8 cm 630 mA 115 VAC 110 V unit 630 mA SB Specifications Section 2 2 1 Disclaimer General Information The information in this manual has been carefully checked and is believed to be accurate However Hach Ultra assumes no responsibility for any inaccuracies that may be contained in this manual In no event will Hach Ultra be liable for direct indirect special incidental or consequential damages resulting from any defect or omission in this manual even if advised of the possibility of such damages In the interest of continued product development Hach Ultra reserves the right to make improvements in this manual and the products it describes at any time without notice or obligation Copyright 2008 by Hach Ultra All rights reserved No part of the contents of this manual may be reproduced or transmitted in any form or by any means without the written permission of Hach Ultra 2 2 Safety information Read th
18. en Allen screw holding sensor sample tubing in place reroute tubing and attach to sensor using the modified coupling installed in step 5 above Tighten the nut finger tight plus one quarter turn with an adjustable wrench Fasten sensor sample tubing to the enclosure with 10 tie anchor and 6 32 X 1 2 Phillips head screw provided in the accessory kit Refer to Figure 2 on page 11 Connect the sensor communications cable from the MicroCount 05 to the SENSOR port on the rear panel of the particle counter Communications Velcro Strip Loop Half 2 Pics Velcro Strip Hook Half 2 Pics sensor Capture Bolt P O Cable ee na N sensor Sample Tubing Ss Installation Ini CH D AA bel Lal TT 10 Tie Anchor D and 6 32 X 1 2 3000A LSS Right Side View Figure 2 3000A with MicroCount 05 sensor installed Phillips Head Screw 11 Inch Teflon Tubing part of Probe Assembly Adapter Probe Assembly Adapter Probe part of Probe Assembly Adapter 3 6 Drain line Attach the drain line to the DRAIN port on the rear panel of the sampler The operator should place the other end of the drain line in a suitable waste fluid receptacle 3 Sampler cable connections The Model 3000A accessory kit contains an RS 232 communications cable with a DB 25 female connector on one end and a DB 9 male connector on the other end The cable connections differ depending upon whether the operator connects t
19. is entire manual before unpacking setting up or operating this equipment Pay attention to all danger and caution statements Failure to do so could result in serious injury to the operator or damage to the equipment To make sure that the protection provided by this equipment is not impaired do not use or install this equipment in any manner other than that specified in this manual 2 2 1 Use of hazard information DANGER Indicates a potentially or imminently hazardous situation which if not avoided will result in death or serious injury WARNING Indicates a potentially or imminently hazardous situation which if not avoided could result in death or serious injury CAUTION Indicates a potentially hazardous situation that can result in minor or moderate injury Important Note Indicates a situation which if not avoided can cause damage to the instrument Information that requires special emphasis Note Information that supplements points in the main text General Information 2 2 2 Precautionary labels Read all labels and tags attached to the instrument Personal injury or damage to the instrument could occur if not observed A symbol if noted on the instrument will be included with a danger or caution statement in the manual A This symbol if noted on the instrument references the instruction manual for operation and or safety information Electrical equipment marked with this symbol cannot be disposed of in European
20. ive will perform optimally only if these guidelines are followed 1 2 3 Do not run syringes for more than a few cycles without liquid in them Thoroughly flush the syringe with distilled or deionized water after use If the plunger is removed from the syringe wipe the plunger with alcohol before replacement Clean the syringes periodically with a mild detergent Allow the detergent to sit in the syringe for 30 minutes or more then flush the syringe with distilled or deionized water for at least 10 cycles If the plunger does not move easily in the barrel remove the plunger and wet the plunger seal with deionized water The following are Model 3000A spare parts Description Part Number Sampler extension arm kit 084X202 01 1 ml syringe 690 300 0005 10 ml syringe 690 300 0004 25 ml syringe 690 300 0003 Section 6 Warranty and Contact Information 6 1 Limited warranty Hach Ultra warrants this instrument to be free of defects in materials and workmanship for a period of one year from the shipping date If any instrument covered under this warranty proves defective during this period Hach Ultra will at its option either repair the defective part without charge for extra parts and labor or provide an equivalent replacement in exchange for the defective product If any diode covered under this warranty proves defective during this period Hach Ultra will at its option either repair the defective diode without charge fo
21. k using the 3 16 Allen wrench remove existing sensor Install the Probe Assembly Adapter p n 084205 01 into the sensor holding block from the rear of the sampler Center the probe over the target on the sampler and tighten the sensor capture bolt shown on the following illustration using the 3 16 Allen wrench Remove both strips of Velcro from the accessory kit Remove the adhesive backing from the loop half of the Velcro strip and press to the baseplate of the MicroCount 05 body between the mounting screws opposite the communications cable Remove the adhesive backing from the second loop half and press to the baseplate of the MicroCount 05 body between the mounting screws next to the sensor inlet port Remove the adhesive backing from the hook halves of the Velcro strips and press to the top of the Model 3000A cover so that the rear edge of the 3000A cover and the baseplate of the MicroCount 05 nearest the inlet port are flush Press MicroCount 05 onto top of Model 3000A See Figure 2 on page 11 for proper mounting Attach unterminated end of the 11 inch teflon tubing part of Probe Assembly Adapter to the inlet side the side facing away from the flow arrow of the sensor microcell using an adjustable wrench Tighten the nut finger tight plus one quarter turn with adjustable wrench Remove existing coupling fitting p n 570755 0256 from sensor sample tubing Attach modified coupling p n 047156 03 to the sensor sample tubing Loos
22. mplers do not have the syringe CLEAN button labelled The CLEAN button is the blank button on the upper row of buttons on these units Model 8000A particle counters with firmware versions 5 41 or higher can interface with and run functions on the 3000A sampler For information on how to operate a Model 8000A in general see the Model 8000A Operator s Manual P N 720 100 0032 When the 8000A is powered up the following initial screen will appear 2 H6 94 13 24 49 Hiac Royco Model 846668 Contamination Counter Front Panel Firmware Version 5 41 Number of online counters 1 Counter ID Firmware Version Model 3646844 Sampler Version 1 6 Main function menu This screen shows the current version of the Model 8000A front panel firmware as well as the current version of the 3000A sampler firmware The appearance of the sampler version number indicates to the operator that the sampler is properly connected to the particle counter and powered on lf the sampler version number does not appear check the power cable to the sampler and the communications cable between the sampler and counter Re seat connections as necessary If the sampler fails to respond consult the troubleshooting section Operation From this screen the operator should press the SET UP key The following screen will appear note the selection changes at the bottom of the screen 2080 94 13 27 19 Hiac Royco Model 6668 Contamination Counter Front Panel Fi
23. nction handy Mark the assigned Return Authorization Number on the outside of the package and prepay the freight Pack the instrument carefully using the original container and packing material or its equivalent Instruments received that were damaged in transit or with no malfunction found shall be subject to an inspection charge at the prevailing rate for such equipment Section 7 Certification This section contains a statement of conformity to WEEE requirements and copies of certification documents ENGLISH Electrical equipment marked with this symbol may not be disposed of in European public disposal systems after 12 August 2005 In conformity with European local and national regulations EU Directive 2002 96 EC European electrical equipment users must now return old or end of life equipment to the manufacturer for disposal at no charge to the user Note For return for recycling please contact the equipment manufacturer or supplier for instructions on how to return end of life equipment for proper disposal DEUTSCH Elektrogerate die mit diesem Symbol gekennzeichnet sind durfen in Europa nach dem 12 August 2005 nicht mehr Uber die offentliche Abfallentsorgung entsorgt werden In Ubereinstimmung mit lokalen und nationalen europ ischen Bestimmungen EU Richtlinie 2002 96 EC m ssen Benutzer von Elektrogeraten in Europa ab diesem Zeitpunkt alte bzw zu verschrottende Gerate zur Entsorgung kostenfrei an den Hersteller zuruckge
24. o a Model 8000A or a Model 9064 particle counter For the 8000A 1 Plug the DB 9 connector into the RS 232 port on the rear panel of the Model 3000A sampler Plug the DB 25 connector into the SLAVE port on the rear panel of the 8000A particle counter The sampler will not work if the DB 25 connector is plugged into the SAMPLER port 11 Installation For the 9064 1 Plug the DB 9 connector into the RS 232 port on the rear panel of the Model 3000A sampler 2 Plug the DB 25 connector into the J103 ADS port on the rear panel of the 9064 3 8 Power cable connection Connect the female end of the power cord to the male socket on the rear panel of the Model 3000A Plug the power cord into an appropriately rated AC line 3 9 General notes on syringe loading and unloading Note The sampler is shipped with the syringe drive positioned for loading a syringe THE A OPERATOR SHOULD LOAD THE SYRINGE PRIOR TO INITIALLY POWERING THE SAMPLER Failure to follow this rule will cause an instrument error requiring the operator to cycle power to the instrument After initial installation the operator must prepare the syringe drive for loading unloading a syringe either by using the syringe load button on the Model 3000A front panel see Figure 3 on page 13 or by using a command from the Model 8000A counter or the PharmSpec software package through the Model 9064 Refer to 8000A interface on page 14 or the PharmSpec Operations M
25. procedures may result in damage to this instrument and voiding of the warranty This instrument requires the operator to be familiar with the operation of analytical instrumentation and have an understanding of particle counting applications Note This instrument has been tested and found to comply with the limits for a Class A digital device pursuant to Part 15 of the FCC rules These limits are designed to provide reasonable protection against harmful interference when the instrument is operated in a commercial environment This instrument generates uses and can radiate radio frequency energy and if not installed and used in accordance with the Operations Manual may cause harmful interference to radio communications Operation of this instrument in a residential area is likely to cause harmful interference in which case the user will be required to correct the interference at his her own expense Note This instrument is Installation Category II as defined by IEC 1010 1 Annex J Section 3 Installation DANGER Tasks involving installation of this equipment have electrical related hazards associated with them These tasks must only be attempted by individuals trained and knowledgeable in this particular task and associated hazards 3 1 HIAC Model 3000A sampler overview The particle counting system consists of a particle sensor counter and sampler The HIAC Model 3000A sampler works with many HIAC particle sensors these sen
26. public disposal systems after 12 August of 2005 In conformity with European local and national regulations EU Directive 2002 96 EC European electrical equipment users must now return old or end of life equipment to the Producer for disposal at no charge to the user Note To return for recycling contact the equipment producer or supplier for instructions on how to return end of life equipment producer supplied electrical accessories and all auxiliary items for proper disposal This symbol when noted on a product enclosure or barrier indicates that a risk of electrical shock and or electrocution exists This symbol if noted on the product indicates the need for protective eye wear This symbol if noted on the product indicates a crush hazard Keep hands and fingers clear This symbol when noted on the product indicates the presence of devices sensitive to Electro static Discharge ESD and indicated that care must be taken to prevent damage with the equipment This symbol when noted on the product identifies the location of a fuse or current limiting device 2 3 Safety recommendations WARNING To reduce the risk of electric shock do not remove the cover or the back while the A instrument is powered Refer all servicing of this instrument to qualified service personnel Prior to operating this instrument read the Operations Manual to become familiar with the operation of this instrument Failure to follow the operating
27. r parts and labor or provide an equivalent replacement in exchange for the defective product To obtain service under this warranty the customer must notify the nearest Hach Ultra service support center on or before the expiration of the warranty period and follow their instructions for return of the defective instrument The customer is responsible for all costs associated with packaging and transporting the defective unit to the service support center and must prepay all shipping charges Hach Ultra will pay for return shipping if the shipment is to a location within the same country as the service support center This warranty shall not apply to any defect failure or damage caused by improper use or maintenance or by inadequate maintenance or care This warranty shall not apply to damage resulting from attempts by personnel other than Hach Ultra representatives or factory authorized and trained personnel to install repair or service the instrument to damage resulting from improper use or connection to incompatible equipment or to instruments that have been modified or integrated with other products when the effect of such modification or integration materially increases the time or difficulty of servicing the instrument THIS WARRANTY IS GIVEN BY HACH ULTRA ANALYTICS WITH RESPECT TO THIS INSTRUMENT IN LIEU OF ANY OTHER WARRANTIES EXPRESSED OR IMPLIED HACH ULTRA ANALYTICS AND ITS VENDORS DISCLAIM ANY IMPLIED WARRANTIES OF MERCHANTABILITY O
28. rios europeos de equipos el ctricos deber n devolver los equipos usados u obsoletos al fabricante de los mismos para su reciclado sin coste alguno para el usuario Nota S rvase ponerse en contacto con el fabricante o proveedor de los equipos para solicitar instrucciones sobre c mo devolver los equipos obsoletos para su correcto reciclado NEDERLANDS Elektrische apparatuur die is voorzien van dit symbool mag na 12 augustus 2005 niet meer worden afgevoerd naar Europese openbare afvalsystemen Conform Europese lokale en nationale wetgegeving EU richtlijn 2002 96 EC denen gebruikers van elektrische apparaten voortaan hun oude of afgedankte apparatuur kosteloos voor recycling of vernietiging naar de producent terug te brengen Nota Als u apparatuur voor recycling terugbrengt moet u contact opnemen met de producent of leverancier voor instructies voor het terugbrengen van de afgedankte apparatuur voor een juiste verwerking POLSKI Sprzet elektryczny oznaczony takim symbolem nie moze by likwidowany w europejskich systemach utylizacji po dniu 12 sierpnia 2005 Zgodnie z europejskimi lokalnymi i pa stwowymi przepisami prawa Dyrektywa Unii Europejskiej 2002 96 EC u ytkownicy sprz tu elektrycznego w Europie musz obecie przekazywa Producentowi stary sprz t lub sprz t po okresie u ytkowania do bezp atnej utylizacji Uwaga Aby przekaza sprz t do recyklingu nale y zwr ci si do producenta lub dostawcy sprz tu w celu uzy
29. rmware Version 5 41 Number of online counters 1 Counter ID Firmware Version 1 13 Model 346644 Sampler Version 1 B im Parameter setup functions menu sLOBL SKI HAGE PASS 644 SETUP SETUPRPR INT ORD SMPLE Figure 5 Model 8000A Setup screen The selection on the far right of Figure 5 is not available from Model 8000A counters below firmware version 5 41 3000A SMPLR Press this key to enter the 3000A sampler functions screen 3 23 94 9 26 43 Hiac Royco Model 8888 Contamination Counter Front Panel Firmware Version 5 5 Number of online counters 1 Counter ID Firmware Version 1 13 Model 38864 Sampler Version 1 8 3BBB sampler functions menu IT MX Li TARE SU SES oli os GI Figure 6 Model 8000A 3000A Sampler functions screen This screen provides the operator with three sampler functions and access to a sampler setup screen 15 Operation 4 3 Sampler functions available from the Model 8000A 4 3 1 LOAD SYRNG A LOAD SYRNG activates the load syringe function When the operator presses LOAD SYRNG the 3000A will pull the syringe plunger drive screw to its bottom travel point With the syringe drive in this position the operator can load or unload syringes from the 30004 All syringes used in the 3000A have the same plunger length Note The operator must follow certain procedures when loading and unloading syringes in order to prevent syringe sampler damage See General notes on syringe loading
30. rns Q0 the operator can set up and perform other sampler operations using the command set given below Command Response Function Check status model and version number IQVx 30004 ver x represents the error code and ver represents the version number ISPsy flow vol tare1 tare2 stir Set parameters sy syringe size in ml flow flow rate in ml min vol sample volume in ml tare1 tare volume in ml for first stroke tare2 tare volume in ml for every other stroke stir stir speed 0 is stop 9 is fastest Appears if error x error code Sampler start Sampler busy Appears if error x error code Sampler prime Sampler busy RE Appears if error x error code ILS Load Syringe LS Sampler busy oe Appears if error x error code IBF Back Flush BF Sampler busy 2BFx Appears if error x error code Unload Sensor Arm 2Ux Appears if error x error code 20 Maintenance and Troubleshooting 5 2 Fuse change procedure If the sampler still fails to respond the operator may need to change the fuse The operator needs a small flat head screwdriver to open the fuse box 5 3 Cleaning To replace a blown fuse A Unplug the sampler s power cord The fuse box is contained within the Power Cord Power Switch assembly on the rear panel of the sampler Place the screwdriver in the groove on the top of the assembly Pull out on the screwdriver so that the fuse box door opens The door has
31. skania instrukcji dotycz cych procedur przekazywania do utylizacji sprzetu po okresie u ytkownia PORTUGUES Qualquer equipamento el ctrico que ostente este s mbolo n o poder ser eliminado atrav s dos sistemas p blicos europeus de tratamento de res duos s lidos a partir de 12 de Agosto de 2005 De acordo com as normas locais e europeias Directiva Europeia 2002 96 EC os utilizadores europeus de equipamentos el ctricos dever o agora devolver os seus equipamentos velhos ou em fim de vida ao produtor para o respectivo tratamento sem quaisquer custos para o utilizador Nota No que toca devolu o para reciclagem por favor contacte o produtor ou fornecedor do equipamento para instru es de devolu o de equipamento em fim de vida para a sua correcta elimina o Global Headquarters 6 route de Compois C P 212 CH 1222 Vesenaz Geneva Switzerland Tel 41 0 22 594 64 00 Fax 41 0 22 594 64 99 Americas Headquarters 481 California Avenue Grants Pass Oregon 97526 USA Tel 1 800 866 7889 1 541 472 6500 Fax 1 541 472 6170 ay ULTRA TM www hachultra com 2007 Hach Ultra Analytics Inc All rights reserved Trademarks are property of their respective owners Specifications are subject to change without notice
32. sors mount directly on the Model 3000A The Model 3000A and the particle sensor are connected to the particle counter by RS 232 communications cables The particle counter controls many functions of the Model 3000A as well as the count START and count STOP instructions to the sampler and sensor Further information on particular particle counters can be found in their operations manuals only details related to the Model 3000A sampler are discussed here The Model 3000A sampler has a sensor arm that holds the sensor and the sample probe A lift mechanism controls the height of the sensor arm By raising and lowering the sensor and probe the operator can change sample bottles easily without disturbing the sample handling system In addition the sampler has a magnetic stir motor that allows the operator to use nine different stir speeds The operator can also turn off the stir motor 3 2 General considerations The operator should place all samplers and particle counters on dry level surfaces The operator should not power up any instruments until completing all electrical and communications connections 3 3 Optional extender arm If an optional extender arm has been purchased the operator can install the extender arm using the following procedure The operator needs 3 32 5 32 and 3 16 Allen wrenches for the procedure 1 Remove the sensor from the sensor holding block if the sensor was previously installed 2 Remove the small
33. the small bolts with the 3 32 Allen wrench The plastic washers will secure the tubing in the grooves The extender arm is now ready for sensor installation 3 4 HRLD sensor installation For instructions on installing a HIAC MicroCount 05 laser particle sensor please refer to MicroCount 05 sensor installation on page 9 The sampler ships with the sensor holding block in place on the lift mechanism To install the sensor the operator will need a 3 16 Allen wrench a 3 32 Allen wrench and a crescent wrench 1 Slide the adapter bolt onto the sensor probe with the bolt threads facing the stop on the probe Check that an O ring is in place on the sensor probe 2 Attach the sensor probe to the inlet side of the sensor microcell with the adapter bolt Use a crescent wrench Do not overtighten the bolt 3 Remove the connector from the sampler sensor tubing by loosening the small captive bolt Pull the yellow cover off of the connector fitting and verify that an O ring is in place on the fitting 4 Attach this connector to the outlet side of the sensor microcell using a crescent wrench 5 Loosen the sensor capture bolt on the sensor holding block using the 3 16 Allen wrench 6 Slide the longer end of the sensor barrel into the sensor holding block from the rear of the sampler Center the probe over the target on the sampler The bolt heads on the sensor body will fit into the appropriate notches on the sensor holding block
34. tion Remove the adhesive backing from the hook halves of the Velcro strips and press to the top of the Model 3000A cover so that the rear edge of the 3000A cover and the baseplate of the MicroCount 05 nearest the inlet port are flush Press MicroCount 05 onto top of Model 3000A See Figure 2 on page 11 for proper mounting Attach unterminated end of the 11 inch teflon tubing part of Probe Assembly Adapter to the inlet side the side facing away from the flow arrow of the sensor microcell using an adjustable wrench Tighten the nut finger tight plus one quarter turn with adjustable wrench Remove existing coupling fitting p n 570755 0256 from sensor sample tubing Attach modified coupling p n 047156 03 to the sensor sample tubing Loosen Allen screw holding sensor sample tubing in place reroute tubing and attach to sensor using the modified coupling installed in step 5 above Tighten the nut finger tight plus one quarter turn with an adjustable wrench Fasten sensor sample tubing to the enclosure with 10 tie anchor and 6 32 X 1 2 Phillips head screw provided in the accessory kit Refer to Figure 2 on page 11 Connect the sensor communications cable from the MicroCount 05 to the SENSOR port on the rear panel of the particle counter 3 5 2 Sensor purchased separately 10 1 10 Disconnect existing sensor s communications cable from the rear panel of the Model 3000A Loosen the sensor capture bolt on the sensor holding bloc
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