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1. 5 1 Configuring the 5 1 Evaluation settings and ofeataateeemenss 5 5 Managing a sample rack under 5 6 Preparing for new 5 8 Starting and recording new 5 13 Managing measurements in the main 5 16 Measurements with pre defined sample 5 5 17 Ver 03 12 01 Page l 2 6 1 6 2 7 1 7 2 7 3 8 1 8 2 8 3 8 4 8 5 9 1 Contents Managing decomposition vessels and 6 1 Managing decomposition vessels under 6 2 Configuration and management of 6 3 Evaluation 7 1 Evaluations to DINKA sin 7 1 Evaluation to DIN 51900 1 20060 7 3 Evaluation to ASTM D1989 D240 D5865 D4809 D
2. 3 000621 3 000727 kwt 5 000801_1 pro 15 0008C 3 000717 kwt 9 000728 kwt 9 000802 kwt a oo08c 19 000718 kwt 5 000728 pro 15 000802_1 pro ooosc 3 000719 kwt 3 000731 kwt 3 000803 kwt a 0008 3 000725 kwt 000731_1 pro 15 000803_1 pro 15 ooosc 5 000726 ema 9 000801 9 000804 kwt a 0008 J 2 Dateiname Dateityp Abbrechen Enter a suitable name for the library file and click on Save Delete the whole library file in the calorimeter Click on the Delete library button and acknowledge the warning to delete the li brary in the calorimeter completely IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 8 6 Managing groupings 8 The CalWin library 8 4 Groupings In CalWin grouping means that successfully completed measurements can be managed in an extra table as well as in the standard table in the main window Whether and how measurements are to be grouped is entirely the user s decision Example of a grouping all samples of a ship s cargo of coal whose average calorific value is to be determined form a grouping Select Measurements gt Groupings in menu bar of the main window to open the Groupings window If no grouping is currently selected you can click on the Group ings button in the main window too Working directory Grouping files gruppe KWG hahah KW G E D gt Delphi5 gt work C 2000 M 2001 Drive
3. 3 6 Changing language To change language all windows except the main screen must be closed In the configuration program 8 you can choose between German and Eng lish for the user interface Click on the Language button to open the Language dia logue Language lel Es Selection C Deutsch English Cancel Ok Use local number format within files The language changes immediately you confirm with OK The names of devices and vessels must be changed individually see Section 3 5 Management of decomposition vessels After changing language user defined tables must be rewritten If files generated in Ca Win are to be exported to Microsoft Excel activate the option Use local number format within files Depending on the language of the operating system output data are then formatted with a decimal comma German or decimal point English IKA WERKE_ C 5040 CalWin Ver 04 05 02 Store configura tion data and close Close CalCFG without storing Page 3 15 3 7 Storing configuration data and closing CalCFG When you quit the Ca CFG configuration program you must decide whether the changes you have just made to the configuration should be stored or if the previous configuration should be retained To store the present configuration and quit Ca CFG In the main window click on the Save button That stores the present configuration and activates the Ready
4. 50 J cotton thread C 4000 80 J 50 J cotton thread 30 J ignition wire IEY The user can define a different standard value for QExtraneous1 see Section 5 1 Configuring the devices IKA WERKE 5040 CalWin Ver 04 05 02 Page 5 12 5 Preparing and Carrying Out Measurements QExtraneous2 external energy 2 External energy from a combustion aid can be entered here If a connected analytical balance is being operated in the With combustion aid mode the external energy from a combustion aid is already taken into account Sample sample name The sample name can have a maximum of 16 characters With a C 5000 calorimeter only the first 7 characters are transmitted which means that these 7 characters must be an unambiguous identification for the sample Characters that are not accepted by Windows Explorer lt gt and blanks are not accepted There must always be an entry in this field As standard Ca Win issues a unique sample name made up of Year Month Day Test number This sample name can be changed by the user If the option Double test is activated see Section 5 1 Configuring the devices the following also apply the sample name may not have more than 5 characters the sequence numbers _1 and 2 will be added automatically all status symbols are shown with a grey background during double testing Properties Any desired text max 40 characters can be entered it appears in the
5. A change of directory or drive cancels the current grouping selection For subsequent measurements that should be included in the current grouping the option Groupings in the window New Measurements see Section 5 4 Preparing for new measurements must be activated The results of these measurements are then automatically entered in the current grouping By clicking on the button Details you can see a list of all measurements in the cur rent or another selected grouping in the window Groupings with the selected File name added You can also access this window by clicking Groupings Grouping name in the main window Grouping heute No Sample WeighedinQty Ho Status Mean value 21 416 9 0 8080501 1 1111 21714 Selected PN 1 8080503 1 2222 19808 Selected Aver rel enor 6 62 2 8080504 1 0011 23190 Selected m 3 808050511122 20955 Selected 4 9111001 0 7280 41040 Max rel error 5 8907100000 0 fe 1579 6 1041801 1 0000 31380 gt Delete Protocol Evaluation Clipboard Excel Close The actions that can be carried out here are similar to the functions available in the main CalWin window so that they are not described again here When deleting se lected measurements in a grouping file it is important to remember that they con tinue to exist in the appropriate daily work file Individual measurements in the table can be marked by double clicking Statistics are calculated for the measurem
6. Measurement waiting and remains in the status gt Measuring cell Remedy Click on the Measuring cell button in the main window to send this measure ment again e The system signals an access violation with relevant address Remedy Acknowledge message with OK Close Ca Win and restart it iS As long as there is no measurement running in a calorimeter Ca Win can be re started at any time As a rule malfunctions and problem can be remedied by re starting IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 9 2 9 Troubleshooting 9 1 Service dialogue for the C 2000 calorimeter Service dialogue for the C 2000 calorimeter is intended exclusively for solving problems It should therefore only be used in close cooperation with IKA Service The service dialogue is opened by selecting Service in the C 2000 context menu status line and right mouse button 1 Service C2000 x System Setup Wartung Information Input Output Passwort I Info on Update Version Ablauf Temperatur 1 Temperatur 2 ea Stell E RPM Ticker iz eT TTT If there is no connection to the C 2000 calorimeter no actions are possible from this window If there is a connection to the C 2000 calorimeter then click on the Info on button This has the effect of transmitting all information that is important for service on a C 2000 with control unit in the info window to Ca Win and keeping it continu ally up
7. measurements protocol User Any desired text max 16 characters can be entered it appears in the measurements protocol Grouping When this box is activated this measurement is added to a table that contains grouped measurements as well as to the standard table This box can only be activated if an appropriate grouping has previously been entered The measurement is only entered in the currently active grouping if it is successfully completed For more information about grouping see Section 8 4 Grouping Calibrations cannot be grouped The Calibration box can therefore not be activated if Grouping is marked Calibration When this box is activated the new measurement will be carried out as a calibration Simulation No measurement will be carried out When this box is activated the field DT appears below it A fictitious temperature increase in Kelvin can be entered in this field This value is used to calculate the results for a simulated measurement The measurement is entered in the table in the main window with the status Measurement completed simulation and can be further processed as if it were a real measurement A decomposition vessel must be selected for the simulation all registered decomposition vessels are available IKA WERKE C 5040 CalWin Ver 04 05 02 Page 5 13 e Vessels decomposition vessels If decomposition vessels are not automatically recognised a list with all currently available decompositi
8. two additional crucibles have been placed in the rack This is indicated by the difference between the coloured boxes in the upper and lower sections of the window and in the missing sample designations in the upper box These two crucibles must be removed to return the sample racks to a valid condition 1 Sample rack 1 OF x rm imam m we Rack is connected Rack assignment is invalid Vv Activ Last valid assignment can be seen with lt Details gt Last valid assignment Rack assignment is valid Reset After clicking the Reset button you can continue work with the sample rack 5 4 Preparing for new measurements The following requirements must be fulfilled before a new measurement can be entered e The device on which the measurement is to be made must be switched on e The device on which the measurement is to be made has had an interface assigned to it using CalCFG see Section 3 Configuration with CalCFG e All the calorimeters on which the measurements are to be made have had decomposition vessels assigned to them How to assign decomposition vessels is explained in Section 3 Configuration with Ca CFG How to assign decomposition vessels and manage calibration using Ca Win is explained in Section 6 Managing decomposition vessels and calibrations How you enter a new measurement depends on the current situation The following situations are possible Working without sample rack balance
9. A mouse click on the button Calibrations in the window Managing decomposition vessels calls up the window Calibrations 4 Calibrations C2000 71 Vessell isoperibol 25 C 21x No Sample Weighedin Gty C Status Mean value 8822 2 2 2020131 1 0101 8806 3 3 2020139 1 0084 8806 0 Average rel error 3 0 04 4 2020401 0 5229 88207 Selected 5 2020406 0 5095 8823 6 Selected vanationrenge 114 6 2020412 0 4991 8822 0 Selected Max rel error 7 2020426 0 5100 8827 6 Selected 8 2020436 0 4984 8830 2 Accept fi 0500 Calibration sequence Protocol wies Delete Excel C Average of 3 Evaluation C DIN no calibration sequence Close Here all calibrations that were completed with a result are listed for the selected decomposition vessel All data refer to the current operating mode of the calorime ter Beside the list the mean value average relative error variation range and maximum relative error are given for the calibrations selected in the table A calibra tion is selected Status Selected or deselected no status for averaging by double clicking on the appropriate line of the table In addition a calibration sequence for a decomposition vessel can be set in this window 13 If you want to select calibrations manually the calibration sequence must be set to User mode In the modes Average of 3 and DIN calibrations are selected automati cally IKA WERKE 5040 CalWin Ver 04
10. E d M Groupings kwa current grouping No New Measurements 1091103 12345_1 1082902 1091104 12345_2 1083001 1091105 probe_2 1091101 1091106 probe_2 1091102 1091204 1091801 Details Delete Close In the Groupings window all files can be managed that were created by grouping measurements The management of existing groups follows the same principles as managing a library 2 Successfully completed measurements can be dragged out the Ca Win main win dow by clicking with the left mouse button and holding it down into any desired existing grouping shown in the field Grouping files To do this the required Grouping must be opened using the button in the main window If a grouping has been se lected as the current grouping you can only drag into that one A measurement can only be dragged once into any one grouping To manage groupings in Ca Win proceed as follows To define a new Grouping click on the New button and enter the name of the new grouping in the text field beside it Characters not accepted by Windows Explorer lt gt and blank spaces cannot be used Finally click on Accept IKA WERKE_ 5040 CalWin Ver 04 05 02 Grouping statistics Page 8 7 Double clicking on a grouping file makes this the current grouping But if it was al ready the current grouping its selection is cancelled The button Grouping in the main window will be labelled accordingly
11. Only values for acid correction are entered Evaluation is only possible for calibrations that are not in the list of experiments for the day Calibrations that are in this list must be evaluated in the main window IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 7 1 7 Evaluation of measurements Evaluation window Acid correction register Evaluation of a measurement is started from the main window To carry out an evaluation click first on the measurement concerned and then on the button Evaluation Evaluation is carried out on the basis of a standardised evaluation procedure which was selected in the window Settings Calculation see Section 5 2 Evaluation set tings and units There is a choice between evaluating to DIN IKA DIN 51900 1 2000 or ASTM D1989 D240 D5865 D4809 D5468 E711 For calibrations evaluation is only necessary if significant quantities of atmospheric nitrogen are found in the decomposition vessel Click on the Evaluation to start the procedure Only values for acid correction are entered For further information on evaluating calibrations please see Section 6 2 Configuration and management of calibrations If an already evaluated measurement is to be re evaluated using a different proce dure see Section 5 2 all evaluation parameters are automatically reset to zero Changing between calculation modes does not reset evaluation parameters to zero 7 1 Evaluations to DIN IKA The window Evaluat
12. Resesserssenscessenssesessees gt Evaluation DIN 51900 1 2000 C ASTM D1989 0240 05865 04809 05468 E711 IV Automatic selection for library measurements Unit 5 Joule g C calg C C kWh kg Cancel The Calculation register is independent of the calorimeter This means that the type of evaluation and the units set apply to all connected calorimeters and balances In the Calculation register the following settings are possible Evaluation You can choose to evaluate measurements to either of two different procedures The procedure set then applies to all measurements made thereafter and also to all measurements stored in the library but not yet evaluated e DIN IKA This procedure offers seven different modes for evaluating measurements These evaluation modes are used completely or partially for evaluations with the C 2000 C 5000 C 7000 calorimeters and C402 MULTICAL and CalWin 1 30 software e DIN 51900 1 2000 This procedure evaluates measurements to DIN 51900 1 2000 e ASTM D1989 D240 D5865 D4809 D5468 E711 This procedure takes into account current US standards for combustion calori metry of solid and liquid fuels and wastes Automatic selection for library measurements When this box is activated already evaluated measurements stored in the library will retain their original evaluation procedure if the procedure is subsequently changed IKA WERKE 5040 C
13. Ver 04 05 02 Page 8 2 8 The CalWin library CalWin saves files generated in the course of a day with specific extensions Ca Win uses the following types of files Measurement files A file name contains the day s date in the form Year Month Day The exten sion is KWT For example the file 980807 KWT is the measurement file from 7 August 1998 The files are saved in the directory that was selected in the window Current directory Library files The file name can be given by the user the extension is also KWT The files are saved in the directory that was selected in the window Library see Section 8 2 Managing measurements in the library Grouping files The file name can be given by the user the extension is KWG The files are saved in the directory that was selected in the window Groupings see Section 8 4 Groupings Protocol files The file names are given automatically A file name contains the day s date in the form Year Month Day The extension is PRO A file name thus has the form DATUM_X PRO where X is the device number These files are stored in the directory in which relevant measurement data are stored Calibration files A file name is an unambiguous designation for the appropriate decomposition vessel and mode of operation The extension is KWK For example the file B1ISO KWK is for the decomposition vessel numbered 7 and operating mode lsoperibol These files are stored in the Ca Win root direct
14. When the box gt Printer is activated in the window Preparing output the docu ment will be printed directly on the standard printer gt Editor A print command loads the document in the internal text editor where you can modify format store as a text or RTF file and finally print it If the box Coherent is also activated you can collect the data from several printing operations in the text editor and merge them together IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 4 7 2 Preparing for Print File Edit DHS e amp SD 1 A 1 A A 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Calorimetric Measurements Library 020131 Sample Weight QExtl 2 Bomb cell C J K Hol J g DT Status 2013132 2013133 1 0219 120 2013134 1 0031 120 2013135 1 0039 120 2013136 1 0078 120 2013137 1 0156 120 2013138 0 9949 120 2013139 1 0229 120 2013140 1 0131 120 2013141 0 9999 120 2013142 1 0049 120 2013143 1 0101 120 2013144 1 0151 120 2013145 1 0063 120 2013146 1 0093 120 2013147 1 0062 120 0 Bombe 1 C2000 1 26457 2 9881 Calibration completed jh 0 Bombe1 C2000 2 8824 8 26457 3 0773 Calibration completed jh 0 Bombel C2000 3 8789 9 26457 3 0329 Calibration completed 0 Bombe1 C2000 4 8788 8 26457 3 0357 Calibration completed 0 Bombel C2000 5 8888 7 26457 3 0132 Calibration completed 0 Bombe2 C2000 1 8795 5 26457 3 0686 Calibration completed 0 Bombe2 C2000 2 8826 4 26457 2 9958
15. a bomb Page 3 13 In the Number field you can unscroll a list which shows the numbers of the vessels for that calorimeter which have not been taken Select a suitable number The number must agree with the coding on the vessel The following numbers can be applied to vessels 1 4 for C 2000 C 5000 e 1 16 for C 4000 0 7 for C 7000 In the text field New name enter a name for the newly entered vessel and click on OK The new vessel is entered and assigned to the specified calorimeter To change the name of a vessel or calorimeter double click on the name in the ap propriate list A dialogue window appears in which you can enter the new name Click on the OK button when you have entered the new name Vessel Ed New name vesse s Cancel The change of name is only completely effective after closing Ca Win and restarting it To delete a decomposition vessel select it with the mouse and click on the Delete button Confirm with OK If you delete a decomposition vessel the assignment of calorimeter and ves sel for all previous measurements using that vessel will be erased Calibra tions with that vessel will also be erased For the C 5000 calorimeter both entering New and deleting Delete decomposi tion vessels must be carried out in parallel on the calorimeter display IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 3 14 Dialogue Language is 3 Configuration with CalCFG
16. button below it Close CalCFG with a mouse click on the Ready button To quit CalCFG without storing the present configuration Click on XI in the top right hand corner of the main window to close the program The following warning appears Confirmation x No configuration saved Retain previous configuration Clicking on Yes closes the program without storing changes just made Pressing No returns you to CalCFG IKA WERKE_ C 5040 CalWin Ver 04 05 02 IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 4 1 4 CalWin Fundamentals CalWin start screen for the C 5000 The CalWin calorimeter software is made up of two sub programs Ca CFG and CalWin To avoid confusion in this and subsequent sections CalWin refers to the sub program Ca Win unless otherwise stated 4 1 Starting CalWin When you switch a calorimeter on always wait to ensure that the self test C 2000 Control C 4000 C 7000 initialisation phase C 5000 C 5000 2 or system check C 2000 Basic are successfully concluded Only then should you start the CalWin software After starting check that the connection to the calorime ters has been established All connected units must be marked waiting in the status line of the main screen For the C 2000 Control and C 4000 the self test finishes when the stirrer is switched on for a short time and for the C 7000 when the menu display appears The initialisation phase for the C 5000 an
17. connected to a C 2000 calorimeter e Setup gt Balance When this menu item is selected the register Balance is activated There the connection of a balance to a C 2000 calorimeter can be set As described in Section 3 2 Configuring interfaces CalCFG the type of balance is selected and the other interface parameters entered Clicking on Apply transmits the in formation to the C 2000 e Maintenance This menu item enables a defined status to be achieved following an uncon trolled interruption mains failure etc In addition it is possible to test several basic functions This menu item is only available when no measurement is in progress and when the connected C 2000 is in the Waiting or Init conditions The sub menu items are as follows IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 9 4 9 Troubleshooting Open cover Opens the cover start stop or end contact Close cover Closes the cover start stop or end contact Cooling water Only possible when device is ready for measurement Water flows in outer vessel the cooling water tempera ture is shown in a window Process is ended with OK Tempering Only possible when device is ready for measurement Water flows in outer vessel and regulation is activated The current target value is used 25 C or 30 C The actual temperature is shown in a window Process is ended with OK Stirrer on off The stirrer is switched on and off the stirring speed is shown i
18. e Select Devices gt Decomposition vessels in the menu bar of the main window to open the Managing decomposition vessels window In this window all con nected calorimeters and all decomposition vessels used are displayed e Click with the right mouse button on the field in the status line of the main win dow in which the relevant calorimeter is displayed The context menu for the calorimeter opens Select the entry Decomposition vessels to open the window Managing decomposition vessels In this window you will now find only those decomposition vessels that are assigned to the selected calorimeter 1 Managing decomposition vessels 21x Measuring cell Decomposition vessels Delete Erotocal Calibrations Close In the left field the connected calorimeter systems are listed The right hand field shows the decomposition vessels that are assigned to the marked calorimeter IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 6 2 Decomposition vessel management Re naming vessels and devices 6 Managing decomposition vessels and calibrations 6 1 Managing decomposition vessels under CalWin Management of decomposition vessels for a configured calorimeter is carried out as follows To enter a new decomposition vessel mark the relevant calorimeter in the left hand field and click on the button New The dialogue New vessel opens 1 New vessel for C2000 Ioj Number E New name Vessel2 Ok Ca
19. enter d setup exe d must be the name of the CD ROM drive Confirm with and follow the instructions on the screen iS When entering the name of the installation directory it must not be more than 8 characters long During installation a directory named Ca Win will be created in the Windows Start menu It contains the start files CalCFG and CalWin If the installation was successfully completed the configuration program CalCFG starts automatically It is used to configure the system as described in Section 3 Configuration with CalCFG IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 2 2 2 Installation and de installation 2 2 De installation of CalWin Because CalWin software is not entered in the Windows system registry during installation a special de installation program is not required To de install CalWin software simply delete the complete CalWin directory for example using Windows Explorer IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 3 1 3 Configuration with CalCFG Using the program Ca CFG a system comprising a PC and connected calorimeters and balances can be set up The program can be used for e Configuration of the interfaces to connected devices e Configuration of the type of operation and test procedure for the calorimeter selected in the configuration window e Configuration of balances e Configuration of the basic set up for data evaluation Selecting the units of measureme
20. from a balance With combustion aid Activate this box so that for every sample first the weight of combustion aid and then the weight of combustion aid plus sample are transmitted External energy 2 is calculated from the weight and calorific value of the combustion aid Calorific value of combustion aid You must enter the correct value for the combustion aid in J g when the With combustion aid is activated Tara after comb aid Activate this box if the balance should be tared after it has transmitted the weight of the combustion aid 5 2 Evaluation settings and units The Calculation register enables you to select the type of evaluation to be used when making the calculations and the units to be employed 1 Settings HEI General Calculation Evaluation DIN 51900 1 2000 C ASTM D1989 0240 05865 04809 05468 E711 IV Automatic selection for library measurements Unit 5 Joule g C calg C BTU b C kwhkg Cancel The Calculation register is independent of the calorimeter This means that the type of evaluation and the units set apply to all connected calorimeters and balances In the Calculation register the following settings are possible Evaluation You can choose to evaluate measurements to either of two different procedures The procedure set then applies to all measurements made thereafter and also to all measurements stored in the library but
21. no effect on Access Regardless of the operating mode the user retains full control of Access Ca Win inserts data records in the background all other database specific actions must be carried out by the user within Access You can make the following transmission settings in the window Data transfer to Access Field name The field names of database tables are listed If there is no connection to Ac cess this column is empty Parameter In this column the parameters that can be transmitted after a measurement are listed with their order No In this column the order of the parameters is entered The number refers to the field name to its left Example parameter 7 calorific value appears under the field name Result in the Access database table In addition the sequence numbers 24 date and 25 date and time measure ment was started can be used These numbers can only be assigned to Access fields of the type date time dbDate In other cases an attempt is made to suit the type of parameter to the type of Access field assigned to it On the Access side only the field types double dbDouble or text dbText should be used Exception the parameter Status can only be assigned to fields of the type long dbLong File In a file window a database file can be selected Table A table from the selected database can be entered here IKA WERKE C 5040 CalWin Ver 04 05 02 Page 4 12 Language window Ike Ca
22. on the Print button or the Clipboard but ton writes it in the Windows clipboard 7 2 Evaluation to DIN 51900 1 2000 When using this evaluation procedure the sole calculation reference is the DIN standard The terms and formula numbers used are also taken directly from this standard With this procedure the Evaluation window contains the following regis ters Calorimetry Gross calorific value 4 Evaluation acc DIN 51900 1 2000 Calorimetry Gross calorific value Net calorific value and reference states Form of results Sample 2012501 Properties fe 7 Weighed in quarfi 1234 User jr Vessel Vessell Cell C2000 Calibration 24507 CYalue J K fiosooc J g 22855 Ext energies and acid correction GExtr 120 QExtr2 J 0 Ignition energy J Sulfur 2 3 fad 15 J 3 4 0 00 NO3 5 QN 68 0 00 Chlorine 10 aC 10 Fluorine 3 po OF fo Evaluation to DIN 51900 1 2000 Section 11 and DIN 51900 2 Section 5 3 5 6 Comments IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 7 4 7 Evaluation of measurements Net calorific value and reference states 4 Evaluation acc DIN 51900 1 2000 Hydrogen ad aq 74 Nittegen lea 0 0000 0 0000 0 0000 pa Evaluation window Net calorific value 21903 e1934 register ok Cancel Evaluation t
23. please see the operating instructions for your balance Jol x Type Port 6 None E CoH C Sartorius Si poo C Mettler E core C Ohaus Baud Baud Data bit C 300 Data bits fi C 1200 a 8 tf 2400 Parity C 4800 Stop bits Parity Stop bits Without Apply Even 2 Test Ok C Uneven odd IKA WERKE C 5040 CalWin Ver 04 05 02 Page 3 7 Clicking on the Apply button makes the balance ready for use Now the result of a weighing can be transmitted from the balance and the result assessed in the inter face window Clicking on the button Test Ok ends the balance setting procedure CalWin cannot be used to control a balance connected to a C 7000 calorimeter 3 3 Configuring devices In the configuration program Ca CFG the type of operation and test procedures for calorimetric measurements can be preset Configuration must be carried out sepa rately for each unit that is shown in the nterfaces window of the main CalCFG screen A mouse click on the Settings button opens the dialogue window for the interface selected on the main screen All calorimeters and balances to which an interface has been assigned can be configured in this way The dialogue Settings General shows only those setting options which can be con figured on the unit selected The settings Double test Restart measurement Take over last test and Ref calorific value are
24. transmission seizes one line of the worksheet and increases the number of the line for the next transmission by one You can determine from which position in a worksheet the insertion of measure ments starts and in which sequence the parameters of a measurement are trans mitted You can do this from the menu bar of the main screen by selecting Setup gt Excel which opens the window Data transfer to Excel IKA WERKE_ C 5040 CalWin Ver 04 05 02 Data transfer to Excel window Page 4 9 1 Data transfer to EXCEL 21x Starting line of EXCEL a Starting column of EXCEL e Positions of the experiment parameters in an EXCEL line Default Headline li hi Ignition energy 4 Wessel 8 Ce C Value J K 7 Calorific value J g 18 TempDitt 3 Sample properties H20 El Ana Whenever the box Connect with Excel at next run is activated Ca Win tries to create a connection to Excel every time it is started However two different cases must be considered Automatic operating mode Excel is not open when Cal Win is started When Ca Win starts Excel is started as well and opens the file that was last active in this mode When Ca Win is closed Excel is also closed The last file that was active will be used when the next connection is made in this mode Flexible operating mode Excel is already open when Ca Win is started Ca Win makes no changes to opened files or settings Closing Ca Win has no effect on Ex
25. 0 min 24 2770 C 5 0 min 24 2980 C 6 0 min 24 3030 C pan 7 0 min 24 3050 C 2 4 6 8 101214 1618 20 22 24 26 28 301 8 0 min 24 3040 C Time min New measurement BEN BON Print Cancel The appearance of this window and the parameters displayed depend on the type and operating status of the calorimeter used In all versions the progress of temperature measurement is displayed both graphically on the left of the window and in tabular form on the right In addition the current temperature inside the vessel is shown 2022701 26 No Temp C ho 5 2 22 A right mouse click in the Measuring cell window opens the same context menu as in the main window for the calorimeter shown in the status bar IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 5 15 The menu item nterface in the context menu available from the Measuring cell window must only be used for maintenance and service In the window it opens a connection can be checked and any problems corrected Scaling the temperature graph Selecting the menu item Scaling in the context menu right mouse click in the Measuring cell window produces the following dialogue 1 Scaling Iof x min temp value 22 00 max temp value 26 00 Start index End index MV Auto scale Line width Cancel Here you can modify the temperature graph to suit your requirements by entering t
26. 0000 Surface moist elementary analysis Cancel Because the data needed for hygroscopic moisture volatile components and ash content are determined by weighing it is also possible to transmit the results direct from a balance To do this either click on the appropriate parameter and press the transfer button on the balance to send a result or a double click on the parameter will call up a reading from the balance When the results of all weighings needed for a parameter are present it will be automatically calculated In the General register the results of calorimetric measurements are presented 1 Evaluation acc DIN IKA 91 General Acid correction Reference states Form Weighed in quantity g fi 1234 Ho J g 2666 QDExtraneous J 12 C Value K OFremd2 J 0 DT K 2 4567 Ignition energy J D Sample Properties User jit Calibration IKA WERKE_ C 5040 CalWin Ver 04 05 02 Evaluation window Form register Evaluation window Calorimetry GCV register The Form register displays the complete results protocol 1 Evaluation acc DIN IKA 91 General Acid correction Reference states Form Clipboard MEASURING PROTOCOL Fre Sample 2012501 User jf Sample properties Test Date of experim 25 01 2002 Start time of experim 07 53 Calorimeter c2000 Page 7 3 The results form can be printed by clicking
27. 05 02 Page 6 4 6 Managing decomposition vessels and calibrations Setting calibration sequence The results of every calibration measurement are automatically entered in the table for the decomposition vessel In the User mode the evaluation dialogue can be called up by the user when required and evaluation carried out as described in Section 7 Evaluation of measurements In addition the box Calibration in the win dow New measurement must be marked In the other cases all selections in the table are deleted and a calibration sequence for the decomposition vessel started After the calibration sequence has been completed the newly completed calibrations are automatically selected When a calibration sequence for a decomposition vessel is running the box Calibration in the window New measurement is marked automatically However this is not the case if the option Vessel identification is set in the configuration of the calorimeter The Calibration box must then be marked manually For the C 7000 calorimeter the Calibration box must always be marked manually In the mode Average of 3 the calibration sequence comprises three calibrations On completion of the third calibration the evaluation dialogue is called up automatically and the average of the three calibrations can be adopted by clicking on Accept The calibration sequence is then finished In the mode DIN five or six calibrations are carried out If the evaluation of five
28. 10 or higher e aC 5000 calorimeter has software version 1 24 or higher e aC 7000 calorimeter has software version 8 0 or higher iS C 5000 calorimeters with software version 2 00 or higher must be considered as a separate type and specially configured see Section 3 2 Configuring interfaces This means that there are two different C 5000 calorimeters which differ slightly in the way CalWin controls them e C 5000 with a software version lower than 2 00 This is designated C 5000 in all subsequent sections e 5000 with software version 2 00 or higher This is designated C 5000 2 in all subsequent sections IKA WERKE C 5040 CalWin Ver 04 05 02 Page 2 1 2 Installation and de installation 2 1 Installing CalWin Before starting to install the CalWin software ensure that all cables are connected to the calorimeters and that all units are ready for use If CalWin is installed for a calorimeter which has already been calibrated then the C values of all decomposition vessels must be noted before starting the installation because the CalWin software overwrites the C values stored in the calorimeter To install CalWin proceed as follows Load the CalWin CD ROM into the CD ROM drive The installation program normally starts automatically once the CD has been loaded If it does not start you must start the installation program on the CD ROM manually To do this click on the Windows Start button open the menu Run and
29. 2002 13 c2000 1 Vessell Operating mode isoperibol 25 C Calibration experiments Test No Date Time Result 2013132 31 01 2013142 31 01 2020131 01 02 2020139 01 02 2020401 04 02 2020406 04 02 2020412 04 02 2020426 04 02 2020436 04 02 8617 2 6600 7 6606 3 6606 0 6620 7 6623 6 6622 0 6627 6 8630 2 oooo0oorerrsa Aver value 8822 2 Aver rel error 0 04 Max Min H 10 4 Diff rel error 0 12 The C value 10500 0 J K will be used for the following measurements A mouse click on the Print button will print the calibration protocol shown in this win dow The various forms of output are explained in Section 4 5 Preparation for data output By clicking on the Clipboard button you can write the contents of the cali bration protocol in the Windows clipboard Deleting a calibration A marked calibration can be deleted by clicking on the Delete button if it is not se lected Transmission to Excel A marked calibration can be transferred to an Excel spreadsheet by clicking on the Excel button The Excel button is only available if there is a connection to Excel with a worksheet open IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 6 6 6 Managing decomposition vessels and calibrations Evaluation of calibrations For calibrations evaluation is only necessary if significant quantities of atmospheric nitrogen are found in the decomposition vessel Click on the Evaluation to start the procedure
30. 30 451 01 CalWin Vers 04 IKA WERKE Calorimeter Software C 5040 CalWin 12 min 24 5500 C 13 min 24 8500 C 0 Hi Zeit min 3 _ Stat Abbruch calWin software for IKA calorimeter systems OPERATING INSTRUCTIONS GB Page 0 1 Explanations of symbols This symbol indicates information which must be observed without fail This symbol indicates information which is important for technically correct operation of the software iS This symbol indicates information and recommendations for safe use of the software IKA WERKE_ C 5040 CalWin Ver 04 05 02 Contents 1 1 1 1 2 2 1 2 2 3 1 3 2 3 3 3 4 3 5 3 6 3 7 4 1 4 2 4 3 4 4 4 5 4 6 4 7 4 8 4 9 5 1 5 2 5 3 5 4 5 5 5 6 5 7 IKA WERKE C 5040 CalWin Page l 1 Page User ha 1 1 SCOPE Of SUPPLY roria ra E eye ot 1 1 System requirements acrgcorueaegenadeeacraragardeotapierensbeadiedaachas 1 2 Installation and de installation cccceeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeneenees 2 1 installing CAV Ge se 2 1 De installation Of 8 ese eesaeenenees 2 2 Configuration With 68 mnnn 3 1 S
31. 5468 E711 7 5 The GalWink ate ceed ws em ieee eee 8 1 Directories and files in 8 1 Managing measurements in the 8 8 3 Reading from the calorimeter 8 4 8 6 Printing protocol TES uty acacia aly clay baat Pes oa at hes 8 8 Troubleshooting ncccc enti 9 1 Service dialogue for the C 2000 9 2 IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 1 1 1 User notes Configuration of C 4000 Connecting a balance and sample racks The C 5040 CalWin calorimeter software is used when making calorimetric meas urements with any of the following IKA Calorimeters from a PC workstation C 5000 Control or DuoControl C 2000 C 7000 and C 4000 The types C 2000 C 5000 and C 7000 calorimeters do not have to be specially con figured However the C 4000 calorimeter must configured as described below be fore installing CalWin the settings are identical to those for IKA C 402 software and MULTICAL see the C 4000 Operating Instructions Using a PC Switch 21 Off Switch 24 REMOTE DIP switch 23 1 23 2 23 3 23 4 23 5 23 6 23 7 23
32. 8 O Odo O C 5040 CalWin permits control of an analytical balance which may be connected to a C 2000 or C 5000 calorimeter or to the serial interface of a PC It is not possible to control a balance connected to a C 7000 calorimeter C 5020 sample racks that are connected to C 2000 or C 5000 calorimeters can also be controlled with C 5040 CalWin 1 1 Scope of supply C 5040 CalWin software comprises Installation CD e Serial adapter cable C 5041 10 e Operating Instructions C 5040 CalWin A serial adapter cable C 5041 10 is included for each calorimeter C 2000 C 5000 and C 7000 FZ Further serial adapter cables cables for earlier models of calo rimeter C 4000 C 7000 and for balances are available as accessories Serial adapter cable 2 m Id No 3036000 Serial adapter cable 5 m Id No 3036001 Serial adapter cable 10 m Id No 3036002 Connection cable C 4000 2 m Id No 2349600 Connection cable C 4000 5 m Id No 2349601 Connection cable C 4000 10 m Id No 2349602 Connection cable C 7000 2 m Id No 7005800 Connection cable for Sartorius ScalTec balances 2m Id No 2361800 Connection cable for Mettler AE balance 2 m Id No 2408800 Connection cable for Mettler AT AM balances 2 m Id No 7047700 Connection cable for Mettler PR PS AG balances 2 m Id 7210500 IKA WERKE C 5040 CalWin Ver 04 05 02 Page 1 9 1 User Notes 1 2 System requirements For use of C 5040 CalWin your sys
33. Calibration completed 0 Bombe2 C2000 3 8786 5 26457 3 0937 Calibration completed 0 Bombe2 C2000 4 8787 1 26457 3 0640 Calibration completed 0 Bombe2 C2000 5 8937 7 26457 2 9733 Calibration completed 0 Bombel C2000 1 8800 7 26457 3 0346 Calibration completed 0 Bombe1 C2000 2 results Calibration running 0 Bombel C2000 3 8787 4 26457 3 0699 Calibration completed 0 Bombe1 C2000 4 8788 9 26457 3 0429 Calibration completed 0 Bombe1 C2000 5 8944 3 26457 2 9989 Calibration completed 2000 1 no results Calibration waiting CaS CG OOO Editor window Preparing for print 1 Cot 1 Modified gt Word A print command passes the document to Microsoft Word There you can also collect the data from several print operations together and modify format store as a Word file and finally print it This setting only becomes active after closing and restarting Ca Win If the box Print immediately is also activated the docu ment will be printed immediately by Word and then deleted This option can only be set when Word was automatically started by Ca Win For more information about the connection to Word please see the next section Connections to Microsoft Office e gt Print tables with legends If this option is active clicking the button Print list in the main window will print the table together with a legend that relates the user defined shortened head ings of table columns to the orig
34. Select the mode of operation you require e Modes of operation for C 2000 Isoperibol 25 C to DIN 51900 Part 2 Isoperibol 30 C to DIN 51900 Part 2 Dynamic 25 C soperibol at 25 C with shorter measuring time Dynamic 30 C Isoperibol at 30 C with shorter measuring time e Mode of operation for C 4000 No settings possible calorimeter measurements are always adiabatic to DIN 51900 Part 3 Modes of operation for C 5000 and C 5000 2 Isoperibol to DIN 51900 Part 2 Adiabatic to DIN 51900 Part 3 Dynamic adiabatic with shorter measuring time Adjustment for the C 5000 Duo Control the mode is set for measuring cell 1 and adopted for measuring cell 2 e Mode of operation for C 7000 No settings possible Ho comb aid If there is no balance connected and you are using a combustion aid the gross calorific value of the combustion aid can be entered here Activate this option and then enter the gross calorific value in the text field all types of calorimeter Ref calorific value Enter the gross calorific value of the calibration substance in J g all types of calorimeter User def QExt1 After activating this option a value for external energy can be entered in the text field for external energy QExtraneous1 This value is then used in subsequent calculations instead of the standard value see Section 5 4 Preparing for new measurements Combustible crucible Activate this box when using combustible crucibles The external e
35. able Cancel IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 4 5 In the list on the left of the window the parameters are shown that are not included in the table in the main screen and on the right the parameters that will be added To move a parameter from the left window to the right mark the parameter and click on the button gt Similarly with the lt button you can move a parameter from right to left A click on the Default button moves all parameters to the left hand window status as delivered You can also rename parameters and so modify the column headings in the main screen Double click on a parameter and enter the new heading in the Change text window that then opens All settings made in the Selection dialog box will be stored when you close Ca Win When the window is closed with OK the table in the main screen will be rewritten You can then modify the column widths to suit the new headings by clicking on the margins in the heading line and dragging The headings of the standard columns can also be changed Click on the column heading and enter the new title If you delete the text completely the original column heading will be restored If you print the table the user defined headings will be printed If required a legend can be printed with the table relating the new headings to the originals see Section 4 5 Preparation for data output After changing language a user defined table must be reconstructe
36. alWin Ver 04 05 02 Page 3 12 Ie Decomposition vessel management 3 Configuration with CalCFG Units Here you can select the units in which results are displayed on the screen and when printed Jg calorific values displayed in J g heat capacities in J K Calg calorific values displayed in cal g heat capacities in cal K BTU b calorific values displayed in BTU Ib heat capacities in BTU Ib g K KWh kg calorific values displayed in kWh kg heat capacities in J K 3 5 Management of decomposition vessels In the CalCFG configuration program you can specify decomposition vessels for all configured calorimeters Clicking on the button Vessels opens the dialogue Managing decomposition vessels S Managing decomposition vessels Measuring cell Decomposition vessels Close The calorimeters are listed in the field on the left of the window and decomposition vessels for that calorimeter on the right Decomposition vessel management can also be carried out using the Ca Win part of the program Management of decomposition vessels for a configured calorimeter is carried out as follows To enter a new decomposition vessel mark the relevant calorimeter in the left hand field and click on the button New The dialogue New vessel opens New vessel for C2000 Mel x Number New name WVessel2 Ok Cancel IKA WERKE_ C 5040 CalWin Ver 04 05 02 Re naming bombs and units Deleting
37. alorimeter to be carried out at different times After placing a crucible in the sample rack the sample is identified and registered Registration is retained until the sample rack is deactivated You can register as many samples as there are compartments in the rack Management of a sample rack with CalWin is carried out as follows With the right hand mouse button click in the status bar of the CalWin main window on the calorimeter whose sample rack is to be managed The appropriate context menu opens With the left hand mouse button click on the entry Sample rack in the context menu The dialogue window Sample rack opens In it the sample rack can be managed 4 Sample rack 1 Iof x rm mm m we Rack is being used Rack is connected IV Activ Last valid assignment Details Reset IKA WERKE 5040 CalWin Ver 04 05 02 Invalid assignment of sample rack Page 5 7 The box Active can be used to switch the sample rack on and off In the management window on the right messages about the current status or incorrect allocation are displayed By clicking on the Details button the difference between current and the last valid assignment can be seen Reset returns the sample rack to the ready for use condition after a valid allocation has been reinstated Allocation of the sample rack is shown symbolically Free compartments are green with the compartment designation rack number compartment nu
38. ated for each sample code 4 Calorimeter measurements x Setup Devices Measurements Help ti CvaluefJ K Hofa TempDitt Status Operator Sampl 6 samp1_1 0 0000 O not assigned no results 2 samp1_2 0 0000 O not assigned no results O samp2_1 0 0000 O not assigned no results 7 samp2_2 0 0000 O not assigned no results D samp3_1 0 0000 O not assigned no results 0 0000 O not assigned no results Main window with New measurement Evaluation Delete Print list Grouping Measurement samp3 predefined sample codes for double Repeat Clipboard Gell Database in testing C2000 not activ By clicking on a measurement in the list a button with the name Measurement Sample name appears where Sample name is the name of the sample you clicked on A click on this button or a double click on the measurement in the list opens the window New measurement with the name of the appropriate sample IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 6 1 6 Managing decomposition vessels and calibrations As in the configuration program Ca CFG you can manage decomposition vessels in CalWin CalWin provides the additional possibility of dealing with the calibrations for each individual decomposition vessel Starting point for the management of decomposition vessels and calibrations is the window Managing decomposition vessels There are two ways of opening this win dow
39. available for all calorimeters cS Settings for calorimeters are described in the section dealing with Ca Win too Settings General dialogue for calorimeters gt Settings HES General Calculation Operation mode C5000 Procedure Selection Selection lsoperibol Adiabatic Dynamic Combustible crucible C Adjustment IV Wessel identification Double test Hocomb 1 Take over last test Restart measurement User def J Dialogue Ref calorific valueJ g 26457 Settings General register for C 5000 without a balance Cancel IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 3 8 Dialogue Settings General register for C 7000 3 Configuration with CalCFG gt Settings 24 General Calculation Operation mode C7000 Ho comb aid J g m J User def GExtt p oo Ref calorific value J g 26457 Cancel Depending on the model of calorimeter the dialogue Settings General register gives access to the following possibilities Operation mode Select the mode of operation you require e Modes of operation for C 2000 Isoperibol 25 C to DIN 51900 Part 2 Isoperibol 30 C to DIN 51900 Part 2 Dynamic 25 C Isoperibol at 25 C with shorter measuring time Dynamic 30 C Isoperibol at 30 C with shorter measuring time e Mode of operation for C 4000 No settings possible calorimeter measurements are always adiabatic t
40. cel Regardless of the operating mode the user retains full control of Excel You can make the following transmission settings in the window Data transfer to Excel Starting line of EXCEL Measurements will be stored from this line in a worksheet Each transmission increases the number of the current line by one If an incorrect entry is made the line number is reset to the standard setting 5 Starting column of EXCEL Measurement parameters will be stored from this column in a worksheet If an incorrect entry is made this will be reset to the standard setting B IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 4 10 Window for Data transfer to Access 1 Data transfer to ACCESS 2x as _ 1 File D Delphi5 work calwin dbt mdb IV Connect at next run with ACCESS 4 CalWin Fundamentals Position of experiment parameters in an EXCEL line For every measurement parameter an Excel column number can be specified within an Excel line relative to the start column Example The C value is transmitted to the column B 8 J If the position field remains blank this parameter will not be transmitted The same applies for a mis entry Standard Resets all transmission data to the standard values Headline A heading line is transmitted to the line above the specified start line in the Ex cel worksheet It will contain the user definable headings for the parameters that ar
41. ction is complete the window Calorimeter library opens and the contents of the library are displayed The calorimeter con cerned must not be making a measurement The C 2000 or C 5000 2 calorimeter must not have been used to make a measurement Extracting a library can take several minutes IKA WERKE_ C 5040 CalWin Ver 04 05 02 Library extracted from a calorimeter Saving library as measurement file Page 8 5 4 Calorimeter library 91 Sample Weighe QExtem Bomb cell Hol g TempDitt Status 1120401 1 0000 120 0 Vessell C2000 9999 0 26531 2 6655 Measurement evaluate f 2012401 1 1234 120 0 Vessell C2000 10500 0 24816 2 6666 Measurement complet w 2012402 1 1111 120 0 Vessell C2000 10500 0 24041 2 5555 Measurement complet Evaluation Delete Print list Close Save Delete library Except for two actions the actions that can be carried out here are similar to the functions available in the main CalWin window so that they are not described again here The additions are buttons to save and delete library files Saving a library as a measurement file Libraries extracted from C 2000 C 5000 C 5000 2 and C 7000 calorimeters can be stored as CalWin measurement files and are then fully available in the CalWin library To save an extracted library click on it and then on the Save button The window Save file as opens Speichern nfa calwin c
42. d IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 4 6 Preparing output window 4 CalWin Fundamentals 4 5 Preparation for data output CalWin provides several procedures for printing the text and data in different dia logue windows You can set the way you choose in the window Preparing output Open this window by selecting Setup gt Preparing output in the menu bar of the main screen 1 Preparing output iof x Any Print command creates a document The processing of this document is controlled by the following options gt Printer The document is sent to the default printer immediatly gt Editor The document is opened and processed by the internal editor Coherent All documents are collected with the editor gt WORD The document is processed by WORD You have to restart Calin to make this option working print immediatly the document is printed by WORD immediatly After that it will be deleted Wia the button Open editor the editor window will be opened with the current content gt Printer gt Editor iz f Ghelent Open editor M gt WORD ae ae Print immediately fms 5 Cancel Ok Every print command whether it be initiated by clicking on a Print button or from an appropriate menu entry produces either a print out or a document that can be modi fied either with an editor or using Microsoft Word The following options are possible gt Printer
43. d C 5000 2 calorimeters is finished when the display shows waiting stable On the C 2000 Basic calorimeter the system check is finished when the display shows waiting ready CalWin is started during a system check on the C 2000 Ba sic the check will be broken off and restarted by CalWin Under unfavourable cir cumstances this can result in the system check not being successfully completed so that both calorimeter and software have to be restarted The program Ca Win is started by a mouse click on the appropriate symbol in the CalWin directory You will find the Ca Win directory in the Windows start menu On starting CalWin displays the screen shown below IKA Calorimetry IKA Calorimetry C5000 Copyright IKA Werke 1933 IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 4 2 Main CalWin screen 4 CalWin Fundamentals The type of calorimeter currently connected with Ca Win is shown on the right of the screen If several calorimeters are connected with Ca Win this is indicated by the word Multi Acknowledge the start screen with OK 4 2 The main CalWin window When the start screen closes the main Ca Win window opens This window is the starting point for all settings measurements and evaluations The Display field is empty when you start the program for the first time that day assuming that no cruci ble from the previous day is in the sample rack On restarting the current status for that day is always dis
44. d transmit its weight by pressing the transfer button on the balance Place the crucible with a weighed sample in the sample rack The sample will be identified and registered and the window New measurement opened automatically with the values already displayed in the fields Weighed in quantity and QExtraneous2 Click on OK in the window New measurement lf you later remove the crucible from the sample rack the window New measurement opens again so that all other parameters can be entered e The options With combustion aid and Tara after combustion aid are activated For these options the boxes With combustion aid and Tara after combustion aid must be activated in the Settings window for the balance and the calorific value of the combustion aid entered Weigh the combustion aid and transmit its weight by pressing the transfer button on the balance Then tare the balance before you weigh the sample and transmit its weight by pressing the transfer button on the balance Place the crucible with a weighed sample in the sample rack The sample will be identified and registered and the window New measurement opened automatically with the values already displayed in the fields Weighed in quantity and QExtraneous2 Click on OK in the window New measurement If you later remove the crucible from the sample rack the window New measurement opens again so that all other parameters can be entered IKA WERKE C 5040 CalWin Ver 04 05 02 Page 5 11 Enteri
45. e Data bits and Parity for the unit that is to be connected With the buttons Con nect and Disconnect an existing connection between the PC and a unit can be cut or reconnected The two Clear buttons remove any messages there may be in the text windows below them Click on the Test button again and if necessary change the parameters until the required message is displayed Quit the interface configuration window by clicking on the Close button IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 3 6 Connecting a balance to a C 2000 or C 5000 Balance on C 5000 C 2000 activated 3 Configuration with CalCFG If you want to connect a balance to a C 2000 or C 5000 calorimeter activate the box Balance on C5000 C2000 With the C 5000 calorimeter the type and settings for the balance are configured directly on the calorimeter For a C 2000 when the box Balance on C5000 C2000 has been activated a button Test appears This button will only be active when the interface at which the C 2000 calorimeter and balance both are connected is se lected 341 Configuration Iof x Interfaces Devices C5000 Duo Balance gt C5000 C2000 Mettler Ohaus LIMS customer request Test interface Settings se Help Language Vessels Ready Clicking on Test opens the interface configuration window and another window in which the type of balance and its interface parameters can be set For individual settings
46. e inactive at certain times 4 9 System check only for C 2000 If CalWin successfully created a connection to a C 2000 calorimeter when it was started a window for a system check will appear Cooling water C 16 00 Tests are not possible Please start up cooling water Checked lsoperibolic 25 C lsoperibolic 30 C C Dynamic 25 C C Dynamic 30 C 99 At initial start up the boiler and hose systems the calorimeter will be filled with water If you are working with a cooler you must now adjust the filling level of the thermostat During this process no measurement may be running and the inner boiler must not be filled If necessary empty the inner boiler Subsequent loss of water e g through evaporation must only be made good when the calorimeter is in this operating condition When using the Cooler KV 500 please take care that its filling level is not mo re than 1 cm below the rim IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 4 4 4 CalWin Fundamentals During the system check the functions of the C 2000 calorimeter are verified In particular the flow rate and temperature of the cooling water are tested The window shows on the left the mode of operation possible at the current cooling water tem perature and on the right the operating mode last used Measurements are only possible when both displays agree or are changed by the operator until they agree The system chec
47. e to be transmitted Data transmission to Access Every successfully completed measurement can be written once as a new data rec ord in an Access table You can determine which database or table is to be used and how the fields in the table are related to the measurement parameters You can do this from the menu bar of the main screen by selecting Setup gt Access which opens the window Data transfer to Access Sample 0 0 Weight in gantity 1 QExtraneous 2 21 Cell 3 20 Vessel 4 7 TempDiff 5 C Value 6 Calorific value 7 H20 Elna 8 H2 3 Ba OH 2 10 Na2C03 11 v Table Tabellet Cancel Whenever the box Connect at next run with Access is activated Ca Win tries to cre ate a connection to Access every time it is started However two different cases must be considered IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 4 11 Automatic operating mode Access is not open when CalWin is started When Ca Win starts Access is also started at the database table defined in the dialogue Both File and Table must be specified Within Access the database table is not opened automatically it is not necessary When Ca Win is closed Access will be closed as well The last database table that was active will be used when the next connection is made in this mode Flexible operating mode Access is already open when Ca Win is started Ca Win accepts the database currently open Closing Ca Win has
48. e3 BTU b g Evaluation window Calorimetry GCV register Net calorific value and reference bases 1 Evaluation acc ASTM Standards 2051420 ioj Calorimetry Gross calorific value Form of results Net heat of combustion 54 Ma do not include H in water 5 00 Qp net BTU Ib 7773 Input data for reference bases eE Jo 34 Ma do not include Ox in water 0 54 Maz faoo Tare 0 0000 Weighed in quantity 0 0000 Weighed out quantity 0000 Ash ad Ma o 00 Tae 00000 Weighed in quantity 0 0000 Weighed out quantity fo co00 air Dry Loss Ma 0 00 Tare 0 0000 Weighed in quantity 10 0000 Weighed out quantity o o000 Evaluation window Net calorific value register IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 7 6 7 Evaluation of measurements Form of results 1 Evaluation acc ASTM Standards 2051420 x Temperature increase 2 1284 K corrected 3 Print D 1989 96 Clipboard Air dry loss ADL ar Moisture M ar Moisture Mad Ash Aiad Hydrogen 8 Oxygen Ox ad Sulfur S ad Titration Evaluation window Form of results register The results form can be printed by clicking on the Print button and the Clipboard button writes it in the Windows clipboard IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 8 1 8 The CalWin library Determining the working directory 8 1 Directories and files in CalWin To manage the files that are created in the c
49. ed to calorimeter are also deleted in the calorimeter Measurements with the status Restart indicated in the Status column in the table in the main window are not deleted instead they are marked with the status measurement was interrupted Printing measurements listed in the main window By clicking on the Print list button the table with all measurements listed in the main window with additional heading information is printed The various forms of output are explained in Section 4 5 Preparation for data output Copying experiment table to Windows clipboard Click on the Clipboard button to copy the whole table of tests in the main window to the Windows clipboard as text IKA WERKE C 5040 CalWin Ver 04 05 02 Page 5 17 Repeat measurements for double tests The Repeat button is only active if the box Double test was marked in the calorimeter configuration see Section 5 1 Configuring the devices If the results of the two measurements of a double test differ by more than 100 J the test is marked with the status il measurement must be repeated In such a case it is necessary to carry out a third measurement Click on the measurement with the sequence number 1 and then click on the button Repeat A new measurement with the sequence number 3 will be created New measurement Ea Number Abbrechen If the result is still not satisfactory after preparing and carrying out this measurement the entire p
50. ements Copying a measurement protocol to the Windows clipboard Click on the menu item Clipboard in the context menu to activate it this copies the protocol of the last measurement to the Windows clipboard It is also possible to mark text in the protocol window with the mouse and use the key combination Ctrl C to copy them to the clipboard Cancelling a measurement With the C 4000 and C 7000 calorimeters measurements can be broken off by opening the calorimeter cover For the C 5000 calorimeter the Cancel button on the calorimeter is used and for the C 2000 and C 5000 2 the Ca Win Cancel button Both calorimeters and the program CalWin can break off measurements automatically if there is something wrong For measurements marked with the status iil measurement cancelled a new measurement must be prepared and carried out Measurements on the C 4000 calorimeter are an exception if they show Error 02 no ignition wire recognition they remain in waiting status and can be restarted when the fault has been corrected 5 6 Managing measurements in the main window In the main window you have the following alternatives for managing your measurements Deleting a measurement By clicking on the Delete button a selected measurement in the table in the main window can be deleted Measurements that are then running in the calorimeter cannot be deleted Measurements with the status Ef measurement waiting or parameters being transmitt
51. emperature limits y axis and the start and end indices x axis With Line width the curve can be made broader or narrower If the box Auto scale is activated CalWin scales automatically to suit the values measured Print diagram By selecting the menu item Print diagram in the context menu the current content of the temperature time graph will be printed The various forms of output are explained in Section 4 5 Preparation for data output Printing a report in the Measuring cell window By clicking on the Print button the information in the text field of the Measuring cell window for the last measurement can be sent to output when the test has been completed If the entry Auto print is activated in the context menu a report of the last measurement completed will be printed automatically Creating a protocol file If you activate this entry by clicking on it in the context menu a file with the name DATUM_x PRO x device number will be created and from this moment all lines that appear in the report will be stored in this file The name of the menu item changes to DATUM_x PRO Clicking on this menu item will now close the file again A protocol that is active when CalWin is closed will be continued when the program is next started How to call up and print protocol files is explained in Section 8 5 Printing protocol files IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 5 16 5 Preparing and Carrying Out Measur
52. ents marked and displayed in the appropriate fields IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 8 8 8 The CalWin library 8 5 Printing protocol files Generating protocol files was described in Section 5 5 Starting and recording new measurements To output protocol files select Measurements gt Protocol files to open the window Protocols 1 Protocols 24 Working directory Protocol files 000728 PRO E as gt Delphi5 E gt work E 2000 2001 Divs 000810 PRO E d1 1 1 PRO zl Protocols pro lt jon Ee As in Windows Explorer you can select a directory on the left side of the window in which the required protocol file is stored Then in the list on the right hand side of the window up to four protocol files can be marked at any one time and printed by clicking the Print For the various output possibilities please see Section 4 5 Prepa ration for data output IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 9 1 9 Troubleshooting In rare cases there may be interference in data transmission between calorimeters and the PC Possible causes are action of external interference on the connection cable cable to long e high demands on the PC system e high demands on the calorimeter processor when closing the cover or filling with water or oxygen Possible effects and remedies are e Ameasurement sent by Ca Win to the calorimeter fails to achieve the status
53. ere In this section all settings are described that are possible with Ca Win and are connected with preparing and carrying out calorimeter measurements They are e Configuration of operating modes and test procedures of a calorimeter e Configuration of a balance e Configuration of the basic set up for data evaluation Selecting the units of measurement e Use of sample racks e Preparing new measurements e Starting and monitoring new measurements 5 1 Configuring the devices If this has not been done in the configuration program Ca CFG the operating modes test procedures and calculation settings must first be determined before using a calorimeter These settings must be entered separately for each connected device All devices to which an interface was successfully assigned in CalCFG and which are switched on when Ca Win is started will be shown in the status bar of the main CalWin window A click with the right mouse button on a device in the status bar opens a context menu The menu items available depend on the device selected Vessels Settings Sample rack Scaling Print diagram Auto print Protocol file Clipboard Settings Service Auto print Library of the calorimeter Clipboard Interface Interface Calorimeters C 2000 C 5000 Balance IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 5 2 Dialogue Settings General for C 2000 without a balance 5 Preparing and Carrying Out Measurements With a click o
54. est interface button When a balance is connected to a PC a message specific to the balance in which the current weight can be read is displayed If the button Assign device is inactive or not present either the selected interface is not available n 8 or it is already assigned gt or the selected unit is not com patible with this version If you want to re assign an interface that is already occupied it must first be re leased To do this select the appropriate interface and click on the button Release If no message appears below the Test interface button check the connection cable In the case of a connection between a balance and a PC you can first try to transfer data from the balance Use the transfer or print button on the balance to send the displayed weight to the PC Make sure that the connection cable is in the correct sockets on both the unit and the PC Use only original cables If an incomprehensible message is shown the interface parameters of the unit and PC must be reset For calorimeters the following standard settings apply C 5000 2400 Baud rate 8 data bits parity none C 2000 2400 Baud rate 8 data bits parity none C 4000 4800 Baud rate 8 data bits parity odd C 7000 2400 Baud rate 8 data bits parity none A balance is tested by sending the result of a weighing from balance to PC For the interface parameters there are many possible variations which can only be usefully exploited gi
55. he contents of the selected file are displayed IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 8 4 Detailed Library window 8 The CalWin library 4 Library 020123 91 Sample Weighe Vessel Cell Cvalue K TempDitt Status 2012301 1 0000 120 Vessell C2000 10500 0 21238 2 0341 Measurement completed wo 2012302 1 0000 120 Vessell C2000 10500 0 21238 2 0341 Measurement completed wv 2012303 1 0000 120 Vessell C2000 10500 0 21238 2 0341 Measurement completed X 2012304 1 0000 1231 C2000 no results Measurement canceled Evaluation Delete Print list Close The actions that can be carried out here are similar to the functions available in the main CalWin window so that they are not described again here 8 3 Reading from the calorimeter library The C 5000 and C 7000 calorimeters have an integrated measurement library This library can be used both in stand alone operation and when the calorimeter is con trolled using CalWin It is especially valuable to be able to read from this library to extract information after stand alone operation This also applies to the C 2000 and C 5000 2 but this library cannot be used when the calorimeter is controlled by CalWin Using the menu item Calorimeter library in the context menu of the device window enables the libraries of calorimeter models C 2000 6 5000 6 5000 2 and C 7000 to be extracted completely When extra
56. he status Measurement prepared Only as many measurements can be prepared as there are decomposition vessels available For all such prepared measurements the button Measurement xxxxxx appears By clicking on this button parameters will be sent to the calorimeter Now start the measurement at the calorimeter The C 4000 and C 7000 calorimeters are started by manually closing the cover of the calorimeter The C 5000 can be started either using the start button on the device or as described below using CalWin The C 2000 and C5000 2 calorimeters must always be started using CalWin because by coupling the calorimeter with the software the calorimeter start button is deactivated To start a measurement using Ca Win click on the start button in the Measuring cell window For full details of the measurement procedure please consult the operating instructions for your IKA calorimeter system The process of measurement will be registered and recorded by Ca Win Progress is displayed both in the main Ca Win window and in the Measuring cell window To open the Measuring cell window click on that field in the status bar of the main window in which the calorimeter is marked 1 C2000 Measurement protocol 2022701 Prel experiment 8 0 min 22 2650 C 9 0 min 22 2670 C 10 0 min 22 2690 C 11 0 min 22 2710 C 12 0 min 22 2730 C Main experiment 0 0 min 22 2730 C 1 0 min 22 8500 0 2 0 min 23 9100 C 3 0 min 24 2000 0 4
57. ht already displayed e The option With combustion aid is activated If this option is used the box With combustion aid must be activated in the Settings window for the balance and the calorific value of the combustion aid entered Weigh the combustion aid and transmit its weight by pressing the transfer button on the balance The dialogue window New measurement opens automatically with the amount of combustion aid shown in the field QExtraneous2 Now weigh the sample and transmit its weight by pressing the transfer button on the balance The weight of the sample will be automatically displayed in the window New measurement e The options With combustion aid and Tara after combustion aid are activated For these options the boxes With combustion aid and Tara after combustion aid must be activated in the Settings window for the balance and the calorific value of the combustion aid entered Weigh the combustion aid and transmit its weight by pressing the transfer button on the balance The dialogue window New measurement opens automatically with the amount of combustion aid shown in the field QExtraneous2 Then tare the balance before you weigh the sample and transmit its weight by pressing the IKA WERKE C 5040 CalWin Ver 04 05 02 Page 5 10 5 Preparing and Carrying Out Measurements transfer button on the balance The weight of the sample will be automatically displayed in the window New measurement Working with sample rack balance
58. inal headings The button Fonts opens the window Typeface All typefaces with fixed character width that the printer accepts are displayed The typeface Courier New in character size 10 is preset Select the typeface and character size and click on Apply to make these settings effective for subsequent printing operations The Setup button opens the window Printer settings This is mainly of interest for selecting upright or landscape format The settings chosen here apply for printing tables and measurement protocols but not for results and calibration protocols With OK you store your entries in the window Preparing for print With the button Open editor depending on the setting you will open the editor window or Word with the current content IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 4 8 4 CalWin Fundamentals 4 6 Connections to Microsoft Office Connections to Microsoft Office make Ca Win an extremely flexible program be cause data can then for example be subjected to further evaluation or prepared for presentation While the connection to Word is used for storing and printing data results can be analysed and displayed in Excel and Access Direct connection to Office applications is dependent on correct system installation For example invalid registry entries which may be generated by any application can prevent connection Always close CalWin first and then an Office application If an Office applicat
59. ion contains several registers First the calculation mode is se lected under Acid correction and the necessary acid correction data entered De tails of the various calculation modes are given in the operating instructions for your calorimeter 1 Evaluation acc DIN IKA 91 General Acid correction Reference states Form Calculation mode Default without titration Default with titration Coal mout without titration Coal H2 input with titration Coal Volatile input without titration Coal Yolatile input with titration Coal Acid correction based on ASTM 198 Coal Acid correction based on ASTM 240 sleeve Sulfur 8 4 2 0 QExtraneousl J 120 Nitrogen an 0 00 QExtraneous2 J fo rl IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 7 2 Evaluation window Reference states register Evaluation window General register 7 Evaluation of measurements The register Reference states is used to enter the data needed to calculate the ref erence states raw and water and ash free waf X Evaluation acc DIN IKA 91 General Acid conection Reference states Form moist an 2 Tare 0 0000 Weighed in quantity 0 0000 Weighed out quantity Yolatiles tan CA 100 WEIGHED GUL 0 0000 Ash an jese Tare 0 0000 Weighed in quantity 0 0000 Hydrogen an ma Weighed out quantity 0
60. ion is closed while Ca Win is still open it will be impossible to make the connection after restarting Ca Win This can lead to a system crash The systems must then be restarted The connections have been tested using Office 97 with Windows 95 Windows 98 and Windows NT Connections to Word Whenever the box WORD is activated in the Preparing output window Ca Win tries to create a connection to Word every time it is started However two different cases must be considered e Automatic operating mode Word is not open when Ca Win is started When Ca Win starts Word is started as well and opens a blank document Every printing task is fed into the current document When Ca Win is closed Word is also closed but without storing e Flexible operating mode Word is already open when CalWin is started CalWin makes no changes to opened files or document settings Every printing task is fed into the current document and closed with a page break The actual printing operation must be initiated by the Word user Closing Ca Win has no effect on Word Regardless of the operating mode the user retains full control of Word Following a successful connection the button OK Open editor in the Preparing output window has the recognised Word version added to its label Data transmission to Excel From any table of measurements daily table library groups calibration a selected measurement can be transmitted to the current Excel worksheet Every
61. k takes about 3 minutes When agreement is reached the button OK is activated and after clicking on it you can start making measurements Con firmation occurs automatically after about five minutes When the current cooling water temperature only allows a different operating mode clicking on the button Change enables you to change to this mode Subsequent measurements will then be carried out in the new mode a warning appears to make this absolutely clear If the button Change is not used after about five minutes the dialogue is broken off In the status line for this calorimeter the message System check not OK appears and it is not possible to make measurements with the calo rimeter The dialogue is also broken off automatically if it is impossible to use the calorimeter in any mode The most frequent causes for this are a lack of flow or cooling water temperature above 28 C The system check is also broken off without result if the user clicks on the button Cancel In all cases the system check can be repeated by using the menu entry Settings in the context menu for this calorimeter 4 4 Extension of table headings by the user To extend the table containing measurements in the main screen you can deter mine which parameters should be displayed in addition to the standard information In the main menu bar select Setup gt Table The window Selection dialog box will open 1 Selection dialog box 21x not in the table in the t
62. lWin While working with a calorimeter system CalWin can be closed and restarted if no measurements are running in the calorimeters When you have finished work with a calorimeter system first all decomposition vessels should be removed from the calorimeters In addition for the C 2000 Control the cover must be closed by pressing Cancel in the CalWin window Measuring cell Then CalWin can be closed down Finally any other calorimeters must be closed and calorimeters and coolers switched off The covers of the calorimeters are closed e onthe C 2000 Basic by using the menu command Exit on the calorimeter e onthe C 2000 Control using CalWin e onthe C 4000 manually e onthe C 5000 and C 5000 2 by using the menu command Exit on the calorimeter e onthe C 7000 manually Click on X at the top right hand corner of the main screen to close CalWin The window shown below appears Confirmation x 2 Measurements complete By clicking on Yes you close the program If you click on No you return to CalWin IKA WERKE 5040 CalWin Ver 04 05 02 IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 5 1 5 Preparing and Carrying Out Measurements Context menus for calorimeters and balances Whereas configuration of the interfaces to the connected units can only be carried out in Ca CFG all other settings can be made in Ca Win therefore several of the settings already described in Section 3 Configuration with Ca CFG recur h
63. ll up CalWin version 4 CalWin Fundamentals 4 7 Changing the user interface language In CalWin you can choose between user interfaces in German and English In the menu bar of the main screen select Setup and the entry Language to open the win dow shown below 4 Language of Xx Selection Ok C Deutsch Cancel English Cancel M Use local number format within The language changes immediately you confirm with OK The names of units and vessels must be changed individually see Section 3 5 Ad ministration of decomposition vessels If files generated in Ca Win are to be exported to Microsoft Excel activate the option Use local number format within files Depending on the language of the operating system output data are then formatted with a decimal comma German or decimal point English 4 8 Calling up online help and CalWin version In CalWin you can call up a context sensitive online help for the current window at any time by pressing the F7 key Alternatively you can use Help gt Help contents in the main menu bar and then start a search for keywords as usual under Windows see the CalWin version installed on your computer use Help gt Info in the main menu bar Virtual memory2062396 kB free Platform Windows NT Excel version Cal in Version 1 40 040 Copyrigth IKA Werke 1933 IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 4 13 4 9 Closing Ca
64. mber occupied compartments are red with the sample designation of the crucible Checking sample racks when CalWin is started When CalWin is started it checks occupation of the sample rack and compares it with list of tests for the day If there are differences the following dialogue opens 4 Sample rack Iof x Crucibles have been placed in the sample rack but the list of experiments for the day is empty If you want to load the experiment list of the and assign the crucibles to this list click on Previous If you want to begin again remove the crucible and then click on New IF you want to work without sample rack click on Cancel New Previous day Cancel Follow the instructions given in this window Changing assignment when the sample rack is switched off When the sample rack is switched off do not make any changes to assignment If changes have been made this will be indicated in the management window for the rack 1 Sample rack 1 OF x Rack is connected a Rack assignment is invalid Last valid assignment can Last valid assignment be seen with lt Details gt IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 5 8 Sample rack returned to valid condition Potential situati ons for entering a new measure ment 5 Preparing and Carrying Out Measurements A click on the Details button will show the differences between the current and last valid assignments In the case shown here
65. measurements meets the requirements of DIN 51900 the evaluation dialogue is called up automatically after the fifth calibration and the calculated average can be adopted Otherwise the calibration furthest from the average is rejected and the evaluation dialogue automatically called up after an additional sixth measurement In both cases the calibration sequence is then terminated Adopting the average as C value If the average of the selected calibrations meets the requirements of the standard used it can be defined as the current C value for the decomposition vessel by clicking on Accept For the C 5000 and C 7000 calorimeters the C value is transmitted to the connected calorimeter C value entered by the user Instead of using an average the user can enter an externally determined C value in the field provided A value can only be entered after clicking on the Entry button The entry is confirmed by again clicking the button which is now marked Confirm For the C 5000 and C 7000 calorimeters the C value is transmitted to the connected calorimeter Displaying the calibration protocol By clicking on the Protocol button the calibration protocol for the selected decom position vessel is displayed You can find the Protoco button in the window Manag ing decomposition vessels too IKA WERKE C 5040 CalWin Ver 04 05 02 Calibration protocol Page 6 5 1 Sheet of test results 2x Calibration protocol Date Mittwoch 27 Feb
66. n a window Temp init The temperature sensor is re initialised IV empty The inner vessel is emptied for a specific time standard 90 s O2 fill An inserted decomposition vessel is filled with oxygen for a specific time standard 60 s after the cover is closed Then the cover is opened again IKA WERKE_ C 5040 CalWin Ver 04 05 02
67. n the menu item Settings the dialogue Settings opens in a form depending on the device selected All calorimeters and balances in the status bar can be configured in this way The dialogue Settings General shows only those setting options which can be configured on the device selected The settings Double test Restart measurement Take over last test and Ref calorific value are available for all calorimeters Settings General dialogue for calorimeters 1 Settings 21x General Calculation Operation mode C2000 Procedure Selection Selection 5 soperibol 25 C C Isoperibol 30 C Dynamic 25 C Combustible crucible Dynamic 30 C P Vessellidentification V Double test Ho comb aid J g Take over last test User def QExtt J fico Ref calorific value J g 26457 1 Settings 21x General Calculation Operation mode Duo MC2 Procedure Selection Selection soperibol Adiabatic Dynamic Combustible crucible Adjustment Vessel identification Double test i Take over last test Restart measurement User def GExtt J Ref calorific value J g 26457 Dialogue Settings General for C 5000 DuoControl Cancel IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 5 3 Depending on the model of calorimeter the dialogue Settings General gives access to the following possibilities Operation mode
68. ncel In the Number field you can scroll down a list which shows the numbers of the ves sels for that calorimeter which have not been taken Select a suitable number The number must agree with the coding on the vessel The following numbers can be applied to vessels 1 4 for C 2000 C 5000 e 1 16 forC 4000 0 7 for C 7000 In the text field New name enter a name for the newly entered vessel and click on OK The new vessel is entered and assigned to the specified calorimeter To change the name of a vessel or calorimeter double click on the name in the ap propriate list A dialogue window appears in which you can enter the new name Click on the OK button when you have entered the new name Vessel2 Ea New name Vessel Cancel The change of name is only completely effective after closing Ca Win and restarting it IKA WERKE_ C 5040 CalWin Ver 04 05 02 Deleting a vessel Page 6 3 delete a decomposition vessel select it with the mouse and click on the Delete button Confirm with OK If you delete a decomposition vessel the assignment of calorimeter and ves sel for all previous measurements using that vessel will be erased Calibra tions with that vessel will also be erased For the C 5000 calorimeter both entering New and deleting decomposition ves sels must be carried out in parallel on the calorimeter display 6 2 Configuration and management of calibrations
69. nergy 1 is then automatically reduced by 50 J no cotton thread However external energy 2 from the combustible crucible must be taken into account all types of calorimeter except C 4000 Vessel identification The C 2000 C 5000 C 5000 2 and C 7000 calorimeters all have decomposition vessel recognition When this box is activated a decomposition vessel is not assigned to a measurement assignment is carried out by the calorimeter at the start of measurement For the C 5000 calorimeter this option must also be set on the unit itself On the C 7000 decomposition vessel recognition cannot be switched off IKA WERKE C 5040 CalWin Ver 04 05 02 Page 5 4 Settings dialogue 5 Preparing and Carrying Out Measurements Double test When this box is activated and sample codes have already been entered see Section 5 7 Measurements with pre defined sample codes two measurements will be made for each sample code Two measurements increase the reliability of test results The option Double test gives a better overview of measurements Both measurements are assigned to the same sample code and placed one above the other in the table in the main window The symbol appears in the main window if the results of the two tests differ by more than 100 J In such a case a third measurement should be made see Section in Chapter 5 6 Repeat measurements for double tests all types of calorimeter except C 7000 Take over last test With
70. new measurement Otherwise proceed as follows Confirm your entries in the New measurement window with OK The window closes and the new measurement is written in the table in the main window with the status parameters being transmitted to the calorimeter When data transmission is complete the calorimeter acknowledges the action In the main window the status changes to Ea measurement waiting If data transmission is unsuccessful an appropriate message appears on the screen After acknowledgement data transmission can be repeated by clicking on the button gt Cell See also Section 9 Troubleshooting If the option Restart measurement is activated in the Settings General window for this calorimeter and a measurement is running or in Restart status indicated in the Status column of the table in the main window the measurement prepared at this time remains in the 8 status parameters being transmitted to the calorimeter By clicking on the button gt Cel this measurement cannot be transmitted to the calorimeter until the previous measurement has been completed or deleted IKA WERKE C 5040 CalWin Ver 04 05 02 Page 5 14 Starting a measurement Measuring cell window 5 Preparing and Carrying Out Measurements Only for C 2000 if the option Explosiv is activated in the Settings General window for this calorimeter the parameters for the measurement will not be transmitted to the calorimeter it remains in t
71. ng sample parameters After opening the window New measurement all the sample parameters that are still missing can be entered and a decomposition vessel selected for the measurement Weighed In Quantity fi 2345 QExtraneous 120 QExtraneous2 fo Sample 2012405 Properties Test User if Vessels Grouping Calibration C2000 Vessel2 Simulation C2000 Vessel3 Dialogue window New measurement Cancel Depending on the path by which the dialogue window New measurement was opened there may be some parameters already entered The descriptions here cover all possible entries in the New measurement window e Weighed in Quantity Only values greater than zero can be entered Enter 4 figures after the decimal point to ensure the necessary accuracy of the result Invalid characters are not accepted There must always be an entry in this field When you use a balance you can also try to call up a value from the balance by clicking or double clicking in this field Depending on the type of balance this may or may not work e QExtraneous external energy 1 For measurements without a combustion aid the following external energies must be taken into account according to the type of calorimeter C 5000 C 2000 software version 1 xx 120 J 50 J cotton thread 70 J electrical ignition energy C 5000 2 C 2000 software version 2 xx 50 J cotton thread ignition energy will be assigned separately C 7000
72. nition is deactivated The latter enables up to 20 decomposition vessels to be used per calorimeter and changes the procedure when starting measurements See Section 5 5 Starting and recording new measurements IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 3 10 Settings dialogue for balances 3 Configuration with CalCFG Settings dialogue for balances Settings 7 Sartorius IV Scale is being used With combustion aid Tiere after combustion aid Calorific value of the combustion aid g fo Scale is being used Activate this box if data are to be transmitted from a balance With combustion aid Activate this box so that for every sample first the weight of combustion aid and then the weight of combustion aid plus sample are transmitted External energy 2 is calculated from the weight and calorific value of the combustion aid Calorific value of the combustion aid You must enter the correct value for the combustion aid in J g when the With com bustion aid is activated Tara after comb aid Activate this box if the balance should be tared after it has transmitted the weight of the combustion aid IKA WERKE_ C 5040 CalWin Ver 04 05 02 Calculation register is Page 3 11 3 4 Evaluation settings and units The Calculation register enables you to select the type of evaluation to be used when making the calculations and the units to be employed Settings HES General Calculation
73. not in use Place the crucible with a weighed sample in the sample rack The sample will be identified and registered and the window New measurement opened automatically Manually enter the sample weight in the field Weighed in quantity Click on OK in the window New measurement lf you later remove the crucible from the sample rack the window New measurement opens again so that all other parameters can be entered Working with sample rack balance being used Here the procedure depends on whether you have configured the balance with or without a combustion aid see Section 5 1 Configuring the devices There are the following possibilities e Nocombustion aid is to be used Transmit the sample weight by pressing the transfer button on the balance Place the crucible with a weighed sample in the sample rack The sample will be identified and registered and the window New measurement opened automatically with the weight already displayed Click on OK in the window New measurement If you later remove the crucible from the sample rack the window New measurement opens again so that all other parameters can be entered e The option With combustion aid is activated If this option is used the box With combustion aid must be activated in the Settings window for the balance and the calorific value of the combustion aid entered Weigh the combustion aid and transmit its weight by pressing the transfer button on the balance Then weigh the sample an
74. not in use Working without sample rack balance being used Working with sample rack balance not in use Working with sample rack balance being used When using a balance there is also a distinction between whether or not a combustion aid is to be used and if so with which option IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 5 9 If you are using an analytical balance you can use the left mouse button during a measurement to click on the button Weighed in quantity in the status bar of the main window The dialogue Weighed in quantity opens it shows the current reading of the balance 1 Weighed in qua BES Weighed in quantity 1 2345 g Weighed in quantity Weighed in quantity Close the window Weighed in quantity by clicking on or by clicking again on Weighed in quantity in the status bar of the main window Working without sample rack balance not in use Click in the Ca Win main window on the button New measurement The dialogue New measurement appears in which you can enter the necessary data Working without sample rack balance being used Here the procedure depends on whether you have configured the balance with or without a combustion aid see Section 5 1 Configuring the devices There are the following possibilities e Nocombustion aid is to be used Transmit the sample weight by pressing the transfer button on the balance The dialogue window New measurement opens automatically with the weig
75. not yet evaluated DIN IKA This procedure offers seven different modes for evaluating measurements These evaluation modes are used completely or partially for evaluations with the C 2000 C 5000 C 7000 calorimeters and C402 MULTICAL and CalWin 1 30 software IKA WERKE C 5040 CalWin Ver 04 05 02 Page 5 6 5 Preparing and Carrying Out Measurements e DIN 51900 1 2000 This procedure evaluates measurements to DIN 51900 1 2000 e ASTM D1989 D240 D5865 D4809 D5468 E711 This procedure takes into account current US standards for combustion calori metry of solid and liquid fuels and wastes Automatic selection for library measurements When this box is activated already evaluated measurements stored in the library will retain their original evaluation procedure if the procedure is subsequently changed Units Here you can select the units in which results are displayed on the screen and when printed Jg calorific values displayed in J g heat capacities in J K Calg calorific values displayed in cal g heat capacities in cal K e BTU lb calorific values displayed in heat capacities in BTU Ib g K KWh kg calorific values displayed in kWh kg heat capacities in J K 5 3 Managing a sample rack under CalWin The sample rack in conjunction with C 2000 and C 5000 calorimeters is used for storing samples It enables the registration of samples after they have been weighed and their processing in the c
76. nt e Managing decomposition vessels in relation to the calorimeters used e Selection of the language the program uses 3 1 Starting CalCFG Before starting CalCFG all units connected to the PC must be ready for use A mouse click on the symbol in the Ca Win directory will start CalCFG The CalWin directory is in the Windows Start menu The CalCFG program starts automatically after successfully installing Ca Win When CalCFG starts the following window appears IKA Calorimetry IKA Calorimetry Configuration Copyright IKA Werke 1933 Start window after installing CalCFG without PCI 8 2 board Language T New configuration E Use Mora board IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 3 2 3 Configuration with CalCFG The start window offers two options and the Language button Language By clicking on this button the program goes to the Language screen You can choose to have the Ca CFG user interface in German or English Language Selection Ok C Deutsch E English __ Cancel If files generated in Ca Win are to be exported to Microsoft Excel activate the option Use local number format within files Depending on the language of the operating system output data are then formatted with a decimal comma Ger man or decimal point English By selecting English and confirming with OK you will remain with the English version of the Start window The follo
77. o DIN 51900 Part 3 e Modes of operation for C 5000 and C 5000 2 Isoperibol to DIN 51900 Part 2 Adiabatic to DIN 51900 Part 3 Dynamic adiabatic with shorter measuring time Adjustment for the C 5000 Duo Control the mode is set for measuring cell 1 and adopted for measuring cell 2 e Mode of operation for C 7000 No settings possible Ho comb aid If there is no balance connected and you are using a combustion aid the gross calorific value of the combustion aid can be entered here Activate this option and then enter the gross calorific value in the text field all types of calorimeter Ref calorific value Enter the gross calorific value of the calibration substance in J g all types of calo rimeter User def QExt1 After activating this option a value for external energy can be entered in the text field for external energy 1 This value is then used in subsequent calculations instead of the standard value see Section 5 4 Preparing for new measurements IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 3 9 Combustible crucible Activate this box when using combustible crucibles The external energy 1 is then automatically reduced by 50 J no cotton thread However external energy 2 from the combustible crucible must be taken into account all types of calorimeter except C 4000 Vessel identification The C 2000 C 5000 C 5000 2 and C 7000 calorimeters all have decomposition vessel recognition When thi
78. o DIN 51900 1 2000 Sections 15 16 Appendix A Results form 4 Evaluation acc DIN 51900 1 2000 MEASURING PROTOCOL Freitag 25 Jan 2 Sample 2012501 Sample properties Test Test date 25 01 2002 Start time Operator 5 J Calorimeter C2000 Vessel Ves C Value 10500 J K Evaluation window Form of results register The results form can be printed by clicking on the Print button and the Clipboard button writes it in the Windows clipboard C 5040 CalWin Ver 04 05 02 Page 7 5 7 9 Evaluation to ASTM D1989 D240 D5865 D4809 D5468 E711 For this evaluation scheme the sole calculation references are the quoted ASTM standards The terms and formula numbers used also refer directly to these stan dards It contains the following registers Calorimetry Gross calorific value 1 Evaluation acc ASTM Standards 2051420 olx Net calorific value and reference bases Form of results Sample 2051 420 Properties Weighed in quantity g 0332 User DTK 21254 E BTU b g K Ext energies and acid correction Vessel Bombe Cell Jc2000 Calibration Qy gross BTU Ib ASTM Standard O Ext energy e2 BTU Ib g 52 C 5865 01 Ext 4 BTU Ib xt energy e4 a fo C 5468 95 Ign energy 62 BTU Ib g C E711 87 96 Sulfur 150 Ext energy el BTU Ib g 2 76 g Na2c03 00 Ext energy
79. on the board can be assigned to each calorimeter and connected balance Regardless of whether the standard PC interfaces are used or those on the interface board the configuration program recognises which are assigned and which are still available Interfaces which are already used by the PC are marked n a Interfaces that have already been assigned to devices show an arrow and the name of the unit Free interfaces have no additional information If a calorimeter is removed when carrying out a new or re configuration the existing assignment of decomposition vessels to the calorimeter will be erased for all earlier measurements The settings and calibrations of a calorimeter that has been removed from a system configuration can be restored if you quit the configuration program without storing IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 3 4 Assigning an interface 3 Configuration with CalCFG How to assign a particular unit to a free interface Use the mouse to select a free interface in left hand window of the main screen Use the mouse again to mark a unit in the right hand window that is still free Click on the button Assign device The device you have selected is now assigned to the free interface At the same time the button changes from Assign device to Release If the connection is properly established when a calorimeter is connected to a PC the message Connection OK appears in the field below the T
80. on vessels is displayed A measurement can be assigned to every decomposition vessel in the list Decomposition vessels are not available in this list when they are assigned to a measurement which has not been completed in the calorimeter With the C 7000 calorimeter decomposition vessels are always automatically assigned and with the C 4000 always by the user For the C 2000 and C 5000 calorimeters with decomposition vessel recognition both possibilities exist Whether recognition is manual or automatic is controlled by the option Vessel recognition in the Settings dialogue for that calorimeter If a decomposition vessel is to be automatically recognised by the calorimeter then only that device must be selected the assignment of a decomposition vessel takes place at the start of measurement in the calorimeter In that case only one measurement per calorimeter can be prepared If a decomposition vessel is selected for which a calibration sequence is running the box Calibration is marked automatically This can only be prevented by interrupting the calibration sequence The subject of calibration sequences is explained in detail in Section 6 Managing decomposition vessels and calibrations 5 5 Starting and recording new measurements When all parameters have been entered in the New measurement window you can start testing If you want to reject data you can press the Cancel button to close the New measurement window without creating a
81. ory Configuration files Various files with the extension CFG and the file CALWIN N are also stored in the Ca Win root directory All these files have text format and can for example be imported into Excel or Word IKA WERKE C 5040 CalWin Ver 04 05 02 Page 8 3 8 2 Managing measurements in the library By selecting Measurements gt Library you can open the Library window 4 Library HEI Working directory MeasuremenFiles 011127 KWT E DS 05 Delphi5 Drive 0201 23 KWT 020124 KT 2 125 Measurements kwt z Measurements 2012406 Details 2012407 2012408 Delete Close 2012403 The CalWin library is used for administration of the files in which measurements are saved daily Any desired file can be selected using the fields Drive Working direc tory and Measurement files The sample names of measurements stored in this file are displayed in the field Measurements The buttons carry out the following actions Library overview e Deleting a measurement file Clicking on the Delete button deletes the selected file but asks you to confirm first This operation deletes all measurements stored in that file Additional sav ings of measurements in calibration or grouping files and the calorimeter library are not affected e Detailed display of a measurement Clicking on the Details button opens the Library window with the file names pre viously selected added T
82. ourse of a day a suitable directory structure is needed Under Ca Win you can either use the existing structure or de velop your own To make this choice select Measurements gt Working directory in the main screen menu bar This opens the window Working directory 1 Working directory 21 Current directory Drive 95 Delphid E d 5 gt work gt calwin Select gt 2002 C Default 5 Automatic User MeasurementFiles 020115 K WT 020124 KWT 020125 KWT Nev D Delphib work calwin 20024J an Close The directory shown in the field Current directory is the storage location of files generated on that day Selection of drive and current directory follows standard Windows practice The following options are available Default Files generated in the course of a day are stored in the Ca Win root directory Automatic Files generated in the course of a day are stored in a directory structure gener ated by Ca Win CalWin creates sub directories for the current year and months User With this option you can choose yourself in which directory files generated in the course of a day are stored Double click on the desired directory in the list Current directory f you want to define a new directory for the measurements click in addition on the button New and enter the name of the new directory in the text field beside it Then click on Accept IKA WERKE_ C 5040 CalWin
83. played Main menu bar Close CalWin Display field table Status symbol 1 Calorimeter etup Devices Measurements Wasi Bomb cell C valuelJ K Hold a TempDitt Status Operator Sampl 1 2345 120 Yessell C5000 9999 0 23914 3 0000 Measurement evaluate jf Sa 1 0123 120 Vessell C5000 8967 5 26457 3 0000 Calibration completed if 1 0124 120 Vessell C5000 8968 4 26457 3 0000 Calibration completed if 1 0121 120 YVYessell C5000 8965 7 26457 3 0000 Calibration completed if 1 0125 120 Vessell C5000 8969 2 26457 3 0000 Calibration completed if 1 0111 120 Vessell C5000 8956 9 26457 3 0000 Calibration completed jf 1 2345 120 Vessell C5000 9999 0 21501 2 6666 Measurement complet jf 1 2323 120 Vessell C5000 no results Measurement waiting if Grouping aluation Delete Print list Clipboard all i Settings Sample rack Scaling Print diagram Context menu P Auto print Protocol file Clipboard Service Library of the calorimeter Interface Status line Five main elements characterise the main Ca Win screen the Status symbols indi cate the status of measurements The symbols have the following meanings measurement waiting measurement running measurement running gt Restart parameters being transmitted to calo
84. rimeter measurement is evaluated sample in sample rack measurement prepared in Explosive mode for C 2000 measurement completed with result measurement should be repeated the results of duplicate measurements differ by more than 100 J 2 repeat measurement _ measurement was interrupted IKA WERKE_ C 5040 CalWin Ver 04 05 02 System check for C 2000 Page 4 3 e The menus in the Main menu bar are used to call up dialogue for administration and configuration In addition the Main menu bar gives access to the online help system e The Display field lists detailed information on the day s measurements in tabular form including the most important data and status The widths of columns in the table can be changed by the user by pulling on the margins in the heading line with the mouse The column headings can be changed by clicking on the name you wish to change and typing in a new one The status line shows the connected units and their current status The fields in the status line react to mouse clicks A left mouse click on a unit opens the win dow for it and a right mouse opens a Context menu for the same unit The menu item Interfaces in the context menu of the main screen must only be used for maintenance and service The window can be used to check the con nection and if necessary correct problems e Clicking on the Buttons carries out various actions To avoid incorrect operation some buttons ar
85. rocedure can be repeated for sequence number _ 2 Grouping measurements Successfully completed measurements can be dragged out of the Ca Win main window by clicking with the left mouse button and holding it down into any desired existing grouping shown in the field Grouping files of the Grouping window If a grouping has been selected as the current grouping you can only drag into that one A measurement can only be dragged once into any one grouping For more information please see Section 8 4 Groupings 5 7 Measurements with pre defined sample codes With Ca Win you can define sample codes in advance for planned measurements This is especially useful if you want to prevent the calorimeter automatically generating and issuing sample codes at the same time you do not have to enter a sample code for each individual measurement For example you can predefine codes in the morning for a whole day s measurements By clicking on Setup gt sample codes the window Sample codes opens in which a list sample codes can be entered IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 5 18 5 Preparing and Carrying Out Measurements 1 Sample codes 21x Enter your sample codes One code max 7 characters per line From this list the measurements to be carried out will be shown in the main window If the box Double test was marked in the calorimeter configuration see Section 5 1 Configuring the devices two measurements will be gener
86. s box is activated a decomposition vessel is not as signed to a measurement assignment is carried out by the calorimeter at the start of measurement For the C 5000 calorimeter this option must also be set on the unit itself On the C 7000 decomposition vessel recognition cannot be switched off Double test When this box is activated two measurements are made for each sample code For further information please see Section 5 1 Configuring the devices all types of calorimeter except C 7000 Take over last test With this option when a measurement is prepared QExt1 the sample characteris tics and the operator s name from the previous measurement are used all types of calorimeter except C 7000 Restart measurement When this box is activated interrupted measurements are returned to the Restart condition if ignition has not occurred and they can be restarted Even if a test is interrupted after ignition with the error message No temperature increase the test can still be restarted For the C 5000 calorimeter this option must also be set on the unit itself all tyoes of calorimeter except C 7000 Explosive This option applies only to a C 2000 which has been fitted with Calorimeter Conversion C 60 In addition only a Peters bomb modified with Electrode Set C 61 may be used The use of C 5010 and C 5012 standard vessels is not permitted in this mode This option can only be activated when decomposition vessel recog
87. tarting GalCPG ea ee ee ele ee eer 3 1 Configuring INTE dues side 3 3 6 9 7 Evaluation settings and 8 9 11 Management of decomposition 3 12 Changing language sears 3 14 Storing configuration data and closing 9 15 CalWin Fundamentals nnmnnn 4 1 Starting CalWin dias cade 4 1 The main CalWin WInGOW dledsaontest sede 4 2 System check only for C 2000 cc 4 3 Extension of table headings 6 4 4 Preparation for data cu 20 2 Soacedeencuees tovendudeaans Genes 4 6 Connections to Microsoft 66 teen ees 4 8 Changing the user interface 8 896 4 12 Calling up online help and CalWin 4 12 ace ten ae 4 13 Preparing and Carrying Out
88. tem must have the following minimum require ments Operating system Windows 95 Windows 98 Windows ME Windows NT 4 0 or Windows 2000 Available hard disc 50 MB capacity Interfaces Sufficient free serial interfaces for connection of calorimeters and balance If necessary a free PCI slot for a multi serial interface board If your PC does not have enough free serial interfaces for connection of all your calorimeters a multi serial interface board PCI 8 2 PClI Bus is available as an accessory Install this as described in the User s Manual which is included with the board CalWin does not support other boards Under Windows NT and Windows 2000 administrator s authority is necessary to install the board Normally your PC will have two serial interfaces designated COM1 and COM2 Following a standard installation of the multi serial interface board the connection at socket 1 of the interface box will be COMBS and that at socket 2 will be COM4 etc If only COM1 was present initially socket 1 becomes COM2 and socket 2 COMS etc When connecting the calorimeter to the PC start with the first free interface then make connections to the other sockets in numerical order A balance should be the last unit connected IE When using C 2000 C5000 or C7000 calorimeters the full scope of C 5040 CalWin functions is only available when the following conditions are fulfilled e aC 2000 calorimeter has software version 1
89. this option when a measurement is prepared QExtraneous1 the sample characteristics and the operator s name from the previous measurement are used all types of calorimeter except C 7000 Restart measurement When this box is activated interrupted measurements are returned to the Restart condition indicated in the Status column of the table in the main window if ignition has not occurred They can then be restarted For the C 5000 calorimeter this option must also be set on the unit itself all types of calorimeter except C 7000 Explosive This option applies only to a C 2000 which has been fitted with Calorimeter Conversion C 60 In addition only a Peters bomb modified with Electrode Set C 61 may be used The use of C 5010 and C 5012 standard vessels is not permitted in this mode This option can only be activated when decomposition vessel recognition is deactivated The latter enables up to 20 decomposition vessels to be used per calorimeter and changes the procedure when starting measurements See Section 5 5 Starting and recording new measurements Settings dialogue for balances 1 Settings HEI at C5000 C2000 IV Scale is being used With combustion aid after combustion aid Calorific value of the combustion aid J g Cancel IKA WERKE_ C 5040 CalWin Ver 04 05 02 Calculation register I Page 5 5 Scale is being used Activate this box if data are to be transmitted
90. to date A click on the Update button brings the display up to date at that moment The transmission of information can be stopped with the button nfo off or by closing the service dialogue On the nformation register all values returned by the C 2000 calorimeter except the assignment of the input and output ports are shown A password for more compre hensive service work can also be entered here The unauthorised entry of a pass word is recorded and can cause malfunctioning of the C 2000 calorimeter In the register Input Output the assignment of the input and output ports is shown The Output button switches the display between input and output If there is no con nection to the C 2000 calorimeter the text fields are white and after clicking on the Update button they change to red and green IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 9 3 1 Service C2000 Iof x System Setup Information Input Output atchdog res Hardware re Stirrer0 Bit1 515 down tes Hardware re Stirrerl Bit2 GLS up res Hardware re Stirrer2 Bit3 JIV filed Data ready res Stirrer3 Bit4 Bimetal Rack data res Stirrer4 Bit5 SData lan wire res Stier Bie esselld res Stirer6 TValid Printer busy res Index PHT HHT E A moo Soup M Se Menu items in service dialogue e System gt Exit Closes the cover of a waiting C 2000 calorimeter Setup gt Printer Protocol printing is activated on a printer
91. ven accurate knowledge of the balance interface and basic knowledge of serial interfaces See also the operating instructions for the balance IKA WERKE C 5040 CalWin Ver 04 05 02 Configuring interfaces Interface configuration window without PCI 8 2 board Page 3 5 How to configure calorimeter and PC interface parameters Click on the interface that is to be configured in the left hand window of the main screen and then on the Test interface button The interface configuration window appears COM 1 Jol x m COM Port Baud rate Data bits Parity oe as 1200 C 3600 C 5 f COMI Came 7 2400 C 19200 s o ESE ve C 4800 C 38400 C poH cone C mark Close C 7200 C 57600 5 8 C space Received data Clear Transmitted data Test Clear Connected Click on the Test button This tests the interface between the PC and unit that was selected on the main screen For a PC calorimeter connection the interface func tions correctly if the message Received data in the left hand window contains the following e G for C 2000 and C 5000 e for C 4000 and C 7000 For a PC balance connection the string of characters in the window must corre spond to the balance interface see the relevant operating instructions In the option fields in the upper part of the window set the specific parameters Baud rat
92. wing sections refer exclusively to the Eng lish dialogue windows New configuration If you want to reject the configuration last used activate this option To retain the configuration last used leave this option de activated Use Moxa board Activate this option if you are using the 8 2 multi serial interfaces board with its interface box Confirm and close the Start window with OK IKA WERKE_ C 5040 CalWin Ver 04 05 02 Page 3 3 3 2 Configuring interfaces When you close the Start window the main CalCFG window opens Configuration m E3 Interfaces Devices COM 1 gt C COM 4n a C5000 Duo C2000 C5000 2 C5000 Duo 2 Sartorius Test interface Balance on the C5000 C201 Connection Ok Settings ahs without PCI 8 2 board Help Language Vessels Ready The calorimeters C 5000 2 and C 5000 Duo 2 subsequently both are designated C 5000 2 are C 5000 calorimeters with software version 2 00 or higher The soft ware version is displayed when a C 5000 calorimeter is switched on There are several places in these Operating Instructions which refer to special fea tures of the C 2000 and C 5000 When special features of the C 5000 are mentio ned this will not apply to the C 5000 2 unless specifically stated Where the C 2000 and C 5000 are covered together then the C 5000 2 is also included With this screen one of the PC serial interfaces or an interface

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