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FP92 5G2 Cleveland Automated Flash Point Analyser User and

1. Instrumentation Scientifique de Laboratoire Cleveland automated flash point Analyzer FP92 5G2 STANDARD METHODS ASTM D92 ISO 2592 IP 36 IP 403 EN 22592 NF T60 118 ET JIS K2265 Cleveland automated flash point Analyzer with SC6 sample changer Instrumentation Scientifique de Laboratoire BP 70285 14653 CARPIQUET CEDEX FRANCE T l 33 2 31 26 43 00 Fax 33 2 31 26 62 93 Web www isl france com Page 2 FP92 5G2 User and Maintenance Manual DOCV207A001 F z HISTORICAL REVIEW Version Concerned Part Dae e FP92 5G2 Analyzer use Part A Original issue 11 97 B Revision of the manual 05 00 FP92 5G2 Analyzer advanced use Part Original issue Revision of the manual Maintenance Part Original issue PPE Revision of the manual 05 00 Version concerned Modifications descriptive Date PartIV 1 4 Alarms list update Spare parts list insertion 06 10 02 Part 5 6 1 Language choice at power on Part Il 4 2 1 Barometric correction ISO 2592 2000 11 27 02 Part Il ae 6 4 1 Language locking Part IV Partivg4 4 Spare parts list update Part 3 1 1 3 2 3 Part Ill 2 3 Updating flash detection indicator red Part 3 Updating of the presentation of the test unit mechanical components 01 11 05 Part 5 3 5 Adding of the section FP92 5G2 PC link Part 5 6 1 Language selection at power on text software available in deutsche Adding of the section 6 2 2 R
2. Tmp 22 1 App Cup under test lt Cups data gt Next No Previous EFP lt Run START G gt lt Control gt lt Display gt lt Down gt 0 Screen 2 Run test display Note If the language choice is not possible at switching on the corresponding power on parameter is locked refer to the section 6 4 1 Power on parameters page 11 87 Selecting lt Exit gt leads to the following screen ISL FP92 5G2 Software Vxy I Vxy SC 6 On line Auto test OK lt Main menu gt S N 210 ISL 2000 lt Run menu gt Screen 3 Initial display 5 6 2 Auto test The auto test on switching on the Analyzer concerns the memories e PROM containing the system software e RAM the working area memory e NVRAM Non volatile RAM containing the Service Parameters and test programs The PROM and NVRAM checksums are verified by comparison at auto test The RAM verification is performed by writing in the memory and reading what has been written to check that it is correct If an error is detected during these tests an auto test error is signaled on the Initial Display Press the ALARM STOP key to display the memory fault s at the origin of the auto test error For more details on the Memory Failures see the relevant section of the Alarms appendix of the current manual Page 1 36 FP92 5G2 User and Maintenance Manual DOCV207A001 F z The Analyzer interface 6 The Analyzer i
3. C min 27 5 F min Selection during test creation flip flop Test Every Interval in C F between applications of the igniter The minimum value for a high heating rate is 6 C 12 F and maximum value is 10 C 20 F For the standard heating rate the test frequency can be from 1 to 10 C 2 to 20 F The operator should enter a value for the 2 categories of EFP EFP lt 110 C 230 F EFP gt 110 C 230 F Start test at this parameter is defined at the temperature of first flame application Format is TP XX T Page II 66 FP92 5G2 User and Maintenance Manual DOCV207A001 F DL Run environment definition the Runs environment menu Pa a 4 2 4 Final Phase Go No Go Only 1 presentation of the ignition source during the test run is allowed by setting this parameter to Y for yes If more than one presentation of the igniter should be allow as described in the usual standard methods then select N for no Selection during test creation Flip flop Pre safety Alarm at EFP flash and fire A pre safety intermittent alarm can be set for a given temperature above the EFP 0 to 50 C 0 to 90 F Although the test program prepared by the Lab Manager does not contain a fire pre safety parameter the operator will be warned if the fire safety parameter temperature is approaching This fire pre safety alarm can only be signaled after flash detection The fire pre
4. An increase of the heating bloc temperature should be observed and the heating indicator should light up the percentage time configured for the Heating parameter 5 2 2 Probe and flash detector e Select Probe and if the probe flash detector arm was in standby position it is lowered into the test position Check that the probe and the detector are correctly positioned in the cup To return the probe detector arm to the standby position select Probe again The Flame test command can be used to check that the flash detector is correctly positioned in the cup 5 2 3 Printer e Connect up the printer and put it On line e Select Printer The following should be printed out MM JJ AA HH MM ISL FP92 5G2 Software VX Y Z T S N NNN 5 2 4 RS 232C External link The host computer must be connected to the Analyzer serial link connector and ready for data reception e Select RS 232 Link to display ON The external link test message shown below should be displayed on the computer ISL FP92 5G 5 2 5 Damper e Select Damper e The damper is presented on the cup if it was retracted before Select Damper again to retract the damper to its standby position 5 2 6 Igniter e Select Flame test to present the igniter arm If the probe detector arm is in the upper position it is lowered The igniter is displaced to the out position e To return the igniter arm to the standby position select Flame test again
5. Note that in the case of fault alarms if the fault s still exists exist the red indicator remains illuminated 3 Alarm treatment Some fault alarms instances may involve a danger for the operator and or the Analyzer For this reason the system is programmed to immediately request standby However this does not mean that the system is safety proof If the Analyzer does not switch to standby the operator and or the Analyzer may not be free from all risk For example because of a faulty component a fault alarm that normally should switch the Analyzer to standby may not do so In such circumstances the operator must intervene and switch off the Analyzer The operator should also use his know how and discretion A In general when an audio alarm is triggered the operator should display the cause and check that everything is in order Page A 112 FP92 5G2 User and Maintenance Manual DOCV207A001 F aa DL Alarm review 4 Alarm review The FP92 5G2 can register up to 10 alarm messages These alarm messages can be displayed in the alarm review and also printed Activate the Review menu from the Faults and Alarms screen refer to the section 2 page 112 the following screens then appear FAULTS REVIEW 18 10 2004 12 15 Check test device positioning 18 10 2004 15 06 Abnormal flash detection lt Exit gt lt Print gt Screen 56 5 Fault alarms All failures are accompanied by a continuous audio
6. Referral to a particular document Standards or to another Referral manual L 1 3 About this manual This manual contains four parts e Part I Using the FP92 5G2 e Part Il Advanced use of the FP92 5G2 e Part IIl Maintenance e Part IV Appendix The first part of the manual allow the operator to perform easily and in few steps the his first flash point test with the FP92 5G2 Analyzer without having particular previous acknowledgments about flash tests The second part allow to finely configure the FP92 5G2 Analyzer in accordance with the user needs This part is thus intended to experienced operators Sensitive parts of the command software those related to test parameters can of course be protected in read and write mode by user chosen passwords The third part enable the user to handle usual maintenance operations in the safest way The Appendices A and B contain complementary information related to alarms and RS232C link The values given in the display illustrations in this manual are only included for explanatory purposes and should not be used by the operator ISL does not accept responsibility for any accidents resulting from the use of values given in such display illustrations This warning applies in particular but not exclusively to values for the creation of test programs Page 1 18 FP92 5G2 User and Maintenance Manual DOCV207A001 F General scope DL 2 General scope With the new FP92 5G
7. in the SERVICE menu SERVICE PRINTING Internal parameters list Measures Regulation check _ Printer reset lt Exit gt Screen 35 5 3 1 Service parameters list printing One of the first operations of a Service Engineer in charge of an Analyzer should be to print out the Service Parameters list e Select Service parameters list in the SERVICE PRINTING submenu The keys on either side of the screen opposite SERVICE PARAMETERS LIST are enabled for this command For a printout according to the configuration of the PRINTER SETUP of ANALYZER SETUP press the key to the left of the screen If ce the key on the right of the screen is selected an 80 column format printout is obtained In the latter case the Degree ASCII code will be presumed to be 248 For Printer setup information see the relevant section of chapter 6 Configuration Analyzer setup menu section 6 1 Printer setup page II 78 Page 11 76 FP92 5G2 User and Maintenance Manual DOCV207A001 F ay DL Diagnostics and measures the Service menu 5 3 2 Measures printing e To print the current measures select Measures of the Service printing submenu e If you first want to display the current measures select Measures display of the Service menu 5 3 3 Regulation check If a regulation check printout during heating up during a test is required it can be request using the SERVIC
8. out of spec it is stocked in the page defined during Samples editing If there is no specified page the result in stored in page 21 this page is the Out spec results storage default page Select Pages edit of the RUNS ENVIRONMENT menu to display an Output page From this display the list of Output pages names can be displayed by pressing lt Show List gt OUTPUT PAGES EDIT lt Show list gt No Title Spec Min Spec Max Storage 25 results 0 storage still available lt Exit gt lt Edit gt Screen 32 To display an existing page use the lt Show List gt function and then select the page no The specification page reappears filled out e Select the lt Edit gt function to switch the system to Edit mode lt Edit gt becomes lt Ok gt e Enter the title the mini and maxi specification result values and the maximum number of results that can be saved on the page For details on the latter entry see chapter 10 Printings the Printing menu page II 94 e Once all the entries are displayed press lt Ok gt and save the entries in a page between 1 and 20 The principle is the same as that described in section 4 3 page 11 67 above for saving a test program Pages display follows exactly the same principle as Samples display section 4 5 Samples edition page Il 70 e Select Pages display of the RUNS ENVIRONMENT menu to display the page in the memory if there is one e
9. page 111 105 of this chapter 3 5 1 Characteristics of the external alarm connection e Voltage 230 V e Current Contact ratings 230V AC 2A 115V AC 3A e Contact ratings 230V D C 0 5A 115V D C 1A DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 111 107 z FP92 5G2 Page intentionally blank Page 111 108 FP92 5G2 User and Maintenance Manual DOCV207A001 F Appendix A Alarms z FP92 5G2 Page intentionally blank Appendix A 110 Manuel d utilisation FP92 5G2 DOCV207A001 F DL Categories of alarms 1 Categories of alarms There are 3 categories of alarms e Fault continuous audio alarm e Report intermittent audio alarm e Warning intermittent audio alarm 1 1 Fault alarms Detection of a fault alarm may have one or more of the following consequences e A test cannot be started e A test that is running is stopped e The Analyzer switches to standby A continuous audio alarm is triggered and the red indicator on the keypad is illuminated As long as the fault exists even though the fault has been acknowledged the indicator remains illuminated 1 2 Report alarms e A report alarm signals a normal event e g End of test flash or an abnormal event e g Flash on first flame test In both cases an intermittent audio alarm is triggered and the red indicator on the keypad is illuminated The active pulse of the audio alarm can be set When the alarm is acknowledged the
10. 110 C the corrected value is 109 9 C i e calculated linearly between 100 and 120 C Page II 60 FP92 5G2 User and Maintenance Manual DOCV207A001 F Calibration the Quality menu DL CORRECTION TABLE IN T 0 C 32 F 0 0 100 C 212 F 0 0 20 C 68 F 0 0 120 C 248 F 0 0 40 C 68 F 0 0 140 C 284 F 0 0 60 C 140 F 0 0 160 C 320 F 0 0 80 C 176 F 0 0 180 C 356 F 0 0 lt Down gt Screen 19 e To enter a correction select the value type in the probe correction and press ENT e For values on the second page press lt Down gt If the sample temperature is below 0 C 32 F the temperature correction at 0 C is used If it is above 400 C 752 F the temperature correction at 400 C is used This correction will only be valid for the duration of the test 3 4 Atmospheric pressure measurement calibration To calibrate the atmospheric pressure measurement circuits a reference barometer is needed e Select Quality in the main menu and then select Atmospheric pressure calibration ATMOSPHERIC PRESSURE CALIBRATION Measured atm Pressure 763 7 mmHg 101 8 KPa Ext barometric pressure 101 3 Ext pressure unit KPa lt Exit gt Screen 20 e Select Ext barometric pressure and enter the reading taken on the reference barometer Press ENT to validate To modify the pressure unit kPa mmHg select Ext pressure unit flip flop selection
11. 232C link I 34 Service link I 34 Control unit I 22 Correction Temperature probe reading I 40 Cover Dismantling assembling III 105 Creating a test II 67 Customizing Run mode screen I 72 D Damper Diagnostics Il 75 Damper 1 25 Data flow control RS 232 I 81 Defective battery Troubleshooting III 105 Delete Page name and contents I 99 Detector Flash I 25 Diagnostics Different diagnostics 1 75 Displays 11 73 Dismantling assembling Maintenance III 105 Display I 38 Download Service parameters II 84 Download Principle of transfer I 85 Download Installation and starting of program II 85 Download Transfer requested by the operator I 85 Download Software Code Software texts II 86 Download Service parameters II 86 Download Unsuccessful transfer I 86 E Editing Text 1 39 Editing A sample II 70 Editing Specification pages II 71 Edition Operators I 72 EFP I 19 End of fast phase I 65 End of test No flash 118 End of test Flash 117 iSL FP92 5G2 Flash and fire 117 End of Transmission EOT Character RS 232 II 81 ENQ ACK protocol RS 232 II 82 125 Existing test Modification II 70 External Alarm Characteristics III 107 Connecting I 107 External link test RS 232C 128 F Fast Phase Test parameters II 65 Fault Low battery 116 Safe memory 114 Fault Fire detection 114 Flat battery III
12. 5G2 3 4 Sample Changer SC 6 AN Turn the Analyzer off before connecting the sample changer SC 6 The sample changer SC 6 is easy to install on the FP92 5G2 single post The right side panel is removed the SC 6 is electrically connected and it is then secured in position on the right side of the test unit The SC6 is then declared ON LINE and a ON OFF performed to update the configuration The sample changer control panel consists of e An ON OFF indicator on the right of the control panel e A photosensor push button to the left of the ON OFF indicator e 6 non available cup indicators if an indicator is illuminated the corresponding cup position is not available for test programming 3 5 Accessories e An optional sample changer e Anti draught anti draft Plexiglas shield e A special overflow cup avoids overfilling and avoids contact between the flash detector and the test specimen e Printer 3 6 Software configuration The non volatile memory of the Analyzer contains pre programmed tests in C and F for all the standard methods listed in the chapter 2 General scope page I 19 The standard version of the FP92 5G2 Analyzer is supplied with e A diskette containing The Service Parameters configuration on leaving the factory A PC program for 1 downloading from a host computer of the Analyzer program the display texts and the Service Parameters 2 uploading the Service Parameters from the non volatil
13. DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 11 61 ae DL FP92 5G2 4 Run environment definition the Runs environment menu 4 1 The ISL FP92 5G2 test principle A FP92 5G2 test program consists of a number of test guideline parameters and a sample ID The guideline parameters and the sample ID are saved in a Test numbered from 1 to 20 In general the guideline parameters depend on the type of sample being analyzed These parameters are defined in the various standard methods for example ASTM D 92 IP 36 It is also possible to create a test which does not correspond with a standard method The test program range of the ISL FP92 5G2 Analyzer on leaving the factory includes all the standard methods listed in the Part chapter 2 General scope page I 19 ASTM IP NF EN ISO and JIS The user can of course replace the factory configured test programs by his own test programs The other advantage of the FP92 5G2 is that the customer can update the test programs himself when the standard methods are modified without having to wait for a software update Having created test programs corresponding with the various standard methods and non standard test programs a number of sample families from 1 to 20 may be created A test program may be associated with each sample family Once the sample family has been edited it must be saved using a specific sample storage number which is selected from a displayed list In
14. FP92 5G2 User and Maintenance Manual DOCV207A001 F Index z FP92 5G2 Page intentionally blank Page 136 FP92 5G2 User and Maintenance Manual DOCV207A001 F Index A Abnormal heating rate 115 Access levels I 28 Adjusting Test flame I 25 Alan Network I 33 Alarmes Categories of 111 Alarms Fault 111 Alarms Report 111 Alarms Warning 111 Alarms Displaying 112 Alarms Stopping audio alarm 112 Alarms Treatment 112 Alarms Review 113 Alarms Fault 113 Alarms Summary 114 Alarms Report 117 Alarms Warning 119 Analyzer FP92 5G2 I 20 Analyzer dismantling assembling III 105 Analyzer ID Number RS 232 II 80 Arrow keys I 37 ASTM D92 IP 36 ISO 2592 NF EN22592 ET NF T60 118 methodes Standard summary I 19 Atmospheric pressure measurement cheks I 40 Atmospheric pressure Measurement calibration I 61 B Barometric correction Test parameters I 64 Barometric correction I 40 C Calibration Atmospheric pressure measurement I 61 Calibration Periodicity I 59 Periodicity and test start refusal II 59 Sample temperature measurement I 57 Sample temperature measurement calibration I 57 Calibration values Sample temperature Modification Il 84 Caution 7 Certified probe simulater Sample temperature measurement II 57 Cleaning I 49 Cleanup Page contents II 99 Computer on line RS 232 I 82 Connection Alan link RS485 I 33 RS
15. Real time clock Setup II 88 Regular maintenance I 51 Regulation Parameters I 84 Regulation check 11 77 Replacing Sample probe temperature III 104 Report Alarms 117 Report alarms Summary 117 Request and reception of results RS 232 125 Resistance Values Guaranteed Entry of exact values Temperature measure calibration II 57 Result out of spec 117 Results Cleanup I 99 Page cleanup II 99 Results pages allocation I 98 Send to a PC or a LIMS I 34 Results memory Display Printing 11 96 Results pages Organizing results 1 96 Rounded Test parameters I 64 RS 232C External link setup 11 79 RS 232C link I 34 Characteristics 123 Interface 123 RS 232 External Link Diagnostics 1 75 RS 232C Example of the use with a PC 129 Hardware setup I 80 Software setup I 80 Run default values Setup I 87 Run environment Definition Il 62 Run environment Printing II 94 Run environment definition I 62 Run mode screen Customizing 11 72 S Safe battery Troubles III 105 Safe memory Fault 114 Safeties FP92 5G2 Analyzer system I 27 Safety parameters Setup II 87 Sample Display I 70 Sample temperature measurement calibration II 57 Samples Edition and display II 70 Sampling I 41 Screen Do not switching on II 86 Service parameters I 83 Software code Download I 84 Up date II 84 Software flow control RS 232 I 82 Software texts Download II 84 Up dat
16. Select lt Show List gt to display the list of pages there are on 2 screen displays for the complete list press lt Down gt for the 2ndpage e Select the page to be displayed and the previous screen reappears with the page selected DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 11 71 ae DL FP92 5G2 4 7 Operators name edition and display The access to operators edition needs the level 1 access password For easy test start preparation it is possible to prepare up to 20 operator names At test start a name can then be rapidly selected and thus avoid text editing for each test e Select Operators edit of the RUNS ENVIRONMENT menu and the first page of the list of operators is displayed To display the second page press lt Down gt e Select the desired number and enter the operator name following the editing instructions of the section text editing of the chapter the Analyzer interface Part 1 of the current manual e Having confirmed the entry by ENT press lt Exit gt to return to the previous display The operators list display is done as follow e Select Operators display of the RUNS ENVIRONMENT menu to display the list of operator names 4 8 Customizing run mode screen A function is provided accessible at level 1 for configuration of the fast mode screen Five of the display items are left to the choice of the laboratory manager if he wishes to personalize the fast mode display As well hav
17. User and Maintenance Manual Page 11 87 ae DL FP92 5G2 6 5 Laboratory setup The access to laboratory setup needs the level 1 access password e Select Analyzer setup in the main menu e Select Lab manager setup in the ANALYZER SETUP menu e Fill out the Lab manager setup form amp Laboratory name enter letters 12 characters amp Laboratory manager name enter letters 12 characters amp Laboratory manager title enter letters 12 characters amp Laboratory manager password enter digits It is thus possible for the Laboratory Manager to modify the level 1 password Ex The master password is given in Appendix C Master passwords page 131 6 6 Real time clock e Select Analyzer setup in the main menu e Select Real time clock in the ANALYZER SETUP menu to display the Real time clock form The following are flip flop choices 1 The date format DDMMYY or MMDDYY 2 The clock format 12 or 24 3 The time format AM or PM The date and time should then be entered to correspond to the formats chosen See the following example REAL TIME CLOCK Date format JJ MM AA Date 20 02 96 12 24 12 AM PM AM Time HH MM 09 45 lt Cancel gt lt OK gt Screen 48 When all the entries are correctly displayed press lt OK gt to confirm them If there are any incoherent entries they will be indicated at this stage Page 11 88 FP92 5G2 User and Maintenan
18. alarm and have at least one of the consequences indicated in section 1 1 page 111 5 1 Switching to standby A number of fault alarms switch the Analyzer to standby e Fire detection Under all circumstances after auto test e Signal conditioning Under all circumstances after auto test e Memory failure At switching on under all circumstances e No test flame System tests for presence of the gas test flame for a maximum of 10 min at the start of a run and 1 min at the presentation of the test flame Refer to section 5 2 3 page 114 e Glow plug current failure Current tested 15s after run start for 2 minutes Refer to section 5 2 5 page 114 e Sample temperature failure During a test run e Flash detection failure At test start and during a test run e Heating block temperature measurement failure At test start and during a run e Heating block safety temperature During a test run e Motor board link failure At test start and during a test run e Failure Check test devices positioning Under all circumstances after auto test e Heating failure During a test run e Check probe positioning During a test run Switching to standby means that e The gas supply is cut off e The heating is stopped If the customer has connected his own fire extinguishing accessory to the safety relay provided then on fire detection this fire extinguishing system is triggered DOCV207A001 F FP92 5G2 User and Maintenanc
19. already existing tests are displayed from 1 to 20 as follows SAVE AS T01 T06 T02 T07 T03 T08 T04 T09 T05 T10 lt Exit gt lt Down gt Screen 30 e The second page test no 11 to 20 can be displayed by selecting lt Down gt e Select the desired test no key and the previous display Screen 29 above returns proposing the test no selected e Select lt Exit gt the screen CUSTOMIZE A TEST Screen 26 page Il 67 appears The chosen test number is displayed e To return to the first display of this section 4 3 Screen 26 page Il 67 without saving the program select lt Exit gt The test that was created has thus been saved under this test no If the program is modified afterwards the operator can save the modifications using SAVE DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 11 69 ae DL FP92 5G2 4 4 Modification of an already existing test Customizing a program needs the level 1 access password e Select Runs environment in the main menu e Select the submenu Customize a test The display becomes CUSTOMIZE A TEST Selected test 1 Show tests list New one lt Edit selected test gt KExit gt Screen 31 e Select Show tests list to display the list of existing tests e Select the test to be modified and the previous display returns with the no of the test displayed in the Selected test line e Select lt Edit selected test
20. authorizations access level 1 it is possible to associate the samples with results specifications pages Five hundred and fifty 550 results can be arranged in this way they can of course be printed or downloaded via the ALAN network for example for further analysis To this end the Analyzer is equipped as standard with a complete communications interface a printer port an ALAN network port which can be converted into an RS232C serial port by means of an adapter supplied and a service port through which data can be downloaded in either direction Beyond these standardized and pre installed tests it is of course possible to administer personalized tests which can be saved or ones linked to particular requests For this the Complete Test Manual can be accessed access level 1 via the main menu A compartmentalized testing mode of this kind which you must quit on finishing with it allows a new program to be created from an existing program the one currently open or any previously saved one This may be done all in one go if the values are known or more experimentally on a trial and error basis The resulting test can be saved and re used The testing unit is composed of the main following components the Pt100 platinum sample temperature sensor glass or stainless steel and the flash point detector ionization ring shaped electrode mounted on the test arm the test igniter arm gas igniter and the damper arm which automatically ret
21. calibration date has passed 4 The observed Fire Point result and corrected result or the corrected amp rounded result 5 The maximum minimum and the average results values for the page To print the displayed result press lt Print gt To validate this result for the transmission through the RS 232C link select lt Transmit gt To display the other results in this page use lt Previous gt or lt Next gt 11 4 Results pages allocation e To display the Results pages allocation e Select Results memory in the main menu e Then select Results pages allocation display to display all the results pages from 1 to 21 e Select lt Exit gt to return to the previous display Page 11 98 FP92 5G2 User and Maintenance Manual DOCV207A001 F Results and printing the Results memory menu 11 5 Page cleanup e Select Result memory in the main menu e Select Page cleanup in the RESULTS MEMORY menu e Select Selected page to choose the results page e Select the results page from the list of 21 pages e The following Screen 53 appears 11 5 1 One page contents cleanup Having selected a result as explained above e Select Delete page contents only and a warning display appears PAGES CLEANUP Delete contents of page _ ARE YOU SURE lt No gt lt Yes gt Screen 54 e To delete the page contents select Yes e To abandon the operation select No 11 5 2 Delete page name and contents
22. caution when handling these materials while operating the Analyzer Please read the manual wear proper protective clothing perform all suggested service procedures use care to prevent accidents The manufacturer accepts no responsibility for any damage or liability arising from the use of analyzers Use of Non ISL Products and Accessories Defects or damage that result from the use of Non ISL branded or certified Products Accessories Software or other peripheral equipment are excluded from warranty DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 7 z FP92 5G2 Page intentionally blank Page 8 FP92 5G2 User and Maintenance Manual DOCV207A001 F ey DL PART I USING THE FP92 5G2 1 2 4 Analyzer system safeties 5 Specifications installation and switching on 6 7 Measurements checks Table of contents OS CN CIAL cto NES D RENE ARE A nr Guth Ave athe avec tiea gab Rh De A Neue ht 1 1 ISL Company Profile 1 2 Symbols and typographical conventions 1 3 About this manual General SCOPE Eten au acess de RE de oe eee tee dde te 3 Presentation of the FP92 5G2 3 1 The FP92 5G2 Analyzer 3 1 1 The control unit 3 1 2 The test unit 3 2 Presentation of the Cleveland elements 3 2 1 The heating block 3 2 2 The ignition source 3 2 3 The flash detector 3 2 4 The sample temperature probe 3 2 5 The damper 3 3 Diagnostics 3 4 Sample Changer SC 6 3 5 Accessories 3 6 Software configur
23. e Flow Control None Software flow control XON XOFF or Hardware flow control RTS CTS e Transmitted data Results always sent and Conditions of run 7 2 PC Software configuration 7 2 1 Menu Port Settings e Settings 9600 baud 8 data bits 1 stop bit parity none e Flow Control Same as the Analyzer e Input buffer size 1024 octets Ee If the flow control is hard connect the RTS of the PC COM port to the CTS of the analyzer 7 2 2 Start and end of record e Select Input Data Record Structure of menu Define menu Start of record event Any character received End of record event Special character received 3 ETX 7 2 3 Input record structure Select the CONTINUE button in the previous display and select Multiple fixed length data fields DOCV207A001 F Manuel d utilisation FP92 5G2 Page appendix B 129 DL FP92 5G2 7 2 4 Input record definition e Select Continue in the previous display A maximum of 40 fields are allowed For our example 32 fields are entered Press the Next field button to advance through the fields There is also a Previous field button The file obtained is an ASCII delimited file and is compatible with Spreadsheets and Data Base management software The fields are delimited by commas strings of characters are in inverted commas and end of record by CR LF Ez Any of the above None fields that are not required can be replaced by Ignore t
24. e Select Delete page name and contents and a warning display appears e To delete the page contents select Yes e To abandon the operation select No DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 11 99 z FP92 5G2 Page intentionally blank Page 11 100 FP92 5G2 User and Maintenance Manual DOCV207A001 F Part III FP92 5G2 Maintenance z FP92 5G2 Page intentionally blank Page 111 102 FP92 5G2 User and Maintenance Manual DOCV207A001 F 2 General DOL 1 General Regular maintenance operations have already been tackled in previous parts e Cleaning the cup and accessories Part section 8 6 Cleaning the test set page l 49 e Test flame adjusting Part section 3 2 2 1 Test flame and pilot light page l 24 e Service parameters printing chapter 5 Diagnostics and measures the Service menu page ll 73 The last operation printing service parameters must be done on receiving of the Analyzer DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 111 103 en DL FP92 5G2 2 External operations 2 1 Replacing the sample temperature probe e Disconnect the sample temperature probe from the connection panel see Figure IIl 1 below e Unscrew the knurled flange then pull up the probe see Figure 11I 2 below e Replace by a new probe 2 2 Replacing the flash point detector e After having dismantled the temperature probe e Unscrew the flash point detector and take
25. higher than 20 of the heating rate setpoint programmed in the program in progress If the heating rate is not sufficient during more than one minute the system deduces the probe misses The analyzer tests for this failure until the test is completed It could be dangerous to increase the duration before the probe presence control by A verifying of the heating rate If this duration is modified to start a test with a warmed sample gt 100 C enter again the factory set value after the test is completed 6 Report alarms An intermittent audio alarm is triggered and the red indicator on the keypad is illuminated For active pulse setting of the audio alarm refer to the section 6 3 2 Buzzer pulse width page ll 84 Acknowledgement of the alarm extinguishes the indicator 6 1 Report alarms summery 6 1 1 Pre safety temperature reached flash and fire A flash Pre safety alarm at EFP must have been programmed in the Final Phase of the test program refer to the section 5 2 Different diagnostics page II 75 An alarm is triggered on reaching this temperature which is entered as a temperature value above EFP EFP T C F The run continues This error may be due to the entry of an erroneous EFP or if no flash has been detected The operator can modify the EFP during the run The test program prepared by the Lab Manager does not contain a fire pre safety alarm However the operator will be warned if the fire safety para
26. includes the elements specific to the Cleveland method for flash and fire points e The heating block e The heating plate and insulating sheet e The ionization ring temperature probe arm e The igniter arm e The choker damper automatically positioned after flash fire point detection e Ignition device for gas test flame e The Sample Changer SC6 accessory installed to the right of the test unit includes The 6 position carrousel turntable with heating plates and insulating sheets installed A feeler for detection of cup presence A special mobile sample changer damper presented at the end of the test It replaces the standard single post damper A 2 cup position safety damper cover for after test runs Draught protection for the sample changer SC 6 A sample changer control panel 3 Temperature probe Relight glow plug Pilot light Flash point detector Fire detection thermofuse Test cup Damper Heating plate Test arm and gas igniter Heating plate removable Test cup handle handle Figure l 2 Test unit DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 1 23 ae DL FP92 5G2 3 2 Presentation of the Cleveland elements 3 2 1 The heating block From the laboratory user point of view the heating block consists of e A low voltage heating element limited to 550 Watts eA metal heating plate with center hole The center hole is surrounded by an area of plane depression on
27. it off Sample temperature Flash point detector probe knurled screw knurled screw Sample temperature probe connector gt 4 Figure Ill 2 Sample temperature probe dismantling 2 3 Adjusting the flash point detection threshold 1 Use a small flat tipped screwdriver to adjust the Flash detection setting potentiometer screw beside the flash detector connector 2 Turn the screw clockwise until the red indicator beside the screw is illuminated Then give the screw 1 8 turn more 3 Carefully turn the setting screw anti clockwise until the red indicator goes off e Further verification Touch the ionization ring and the analyzer ground at the same time with your finger e g the ionization ring and the rim of the cup The red flash detection indicator should light up Page 111 104 FP92 5G2 User and Maintenance Manual DOCV207A001 F a DL Internal operations 3 Internal operations Switch off the Analyzer and disconnect it from the mains before removing the housing cover AN If the service operations require you to switch on the Analyzer switch it off again before disconnecting or removing any electrically powered components 3 1 Analyzer dismantling assembling for maintenance operations 3 1 1 Dismantling assembling of the Analyzer housing cover e Remove the 2 mushroom head screws on the bottom left corners of the Analyzer control unit e Remove the mushroom head screw from the top right re
28. large flame appears and cae instantaneously propagates itself over the surface of the specimen Extracts from the Annual Book of ASTM Standards D 92 90 1 This page contents extracts from the Annual Book of ASTM Standards DOCV207A001 F FP92 5G2 User and Maintenance Manual Page I 19 ae DL FP92 5G2 3 Presentation of the FP92 5G2 This new version of the Cleveland automatic flash point Analyzer FP92 5G2 is a complete redesign rather than just an improvement concerted attempt to simplify it has been undertaken with increased reliability and lifetime as the end in view At the same time its simplicity of use has been maintained and indeed enhanced Thus as soon as it is switched on and any key is touched the operator can start a test simply by entering the presumed temperature or recalling the presumed temperature of the previous test The type of test default will have been configured previously by the laboratory manager access level 1 The ergonomics of the device too make it easy to use Two sets of touch keys on either side of the screen protected by a film that is resistant to most petrochemical products allow direct access to the on screen menus The screen is very easy to read by means of two knobs under the screen brightness and contrast can be adjusted in line with the light conditions in the testing area The sample temperature may be read on the current test display screen at a distance of 5m To extend its
29. of the MEASURES screen see the above table permits rapid diagnostics of the different input circuits A flag can have the values 0 or 1 Interpretation is as follows Letter Flag concerns Interpretation of Flag A Motor board fault A 1 Fault indicated by the motor board B Damper position B 1 Damper on the cup C Damper position C 1 Damper in it s housing D Probe arm position D 1 Probe arm up E Probe arm position E 1 Probe arm down F Igniter position F 1 Test flame near the detector G Igniter position G 1 Test flame out H Igniter position H 1 Igniter applied l Ignition 1 0 amp J 1 Gas ignition with a glow plug J Ignition 1 1 amp J 1 non valid K Non used L Flash detection L 0 Flash detection with ring shaped electrode M Test flame M 1 Test flame detected Test flame M 0 Test flame not detected N Non used O Fire detection O 1 Fire detected P Non used e Press lt Exit gt to return to the diagnostics display Page Il 74 FP92 5G2 User and Maintenance Manual DOCV207A001 F k Diagnostics and measures the Service menu 5 2 Different diagnostics 5 2 1 Heating e Select Heating on the right of the screen and enter a value between 50 and 100 so as to have a noticeable temperature increase e Use the Heating key on the left of the screen to display ON Flip flop e Select lt Measures gt The Heating value will of course be the same as that entered in the DIAGNOSTICS display
30. operations 1 Adjustment of the test flame check at the beginning of the test and if necessary adjust by means of the valve setting knob 2 Temperature and atmospheric pressure measurement check at regular intervals see chapter 7 Measurements checks page I 40 3 The cup the flash detector the temperature probe the flame nozzle and the damper should always be clean Refer to the previous section 4 Real time clock setting refer to the section 6 6 Real time clock page Il 88 5 Temperature probe replacement refer to the Part Ill of the current manual 6 Flash detector replacement refer to the Part Ill of the current manual 7 Glow plug replacement refer to the Part III of the current manual 8 Regular uploading of the service parameters refer to the chapter 6 Configuration Analyzer setup menu section 6 3 Service service parametersll 83 9 Printer paper ink ribbon replacement see printer manual DOCV207A001 F FP92 5G2 User and Maintenance Manual Page I 51 z FP92 5G2 Page intentionally blank Page l 52 FP92 5G2 User and Maintenance Manual DOCV207A001 F Part II Advanced use of the FP92 5G2 z FP92 5G2 Page intentionally blank Page II 54 FP92 5G2 User and Maintenance Manual DOCV207A001 F General L 1 General This part deals with the advanced use of the FP92 5G2 i e These functions allow on the one hanad test results to be processed collection classification stat
31. operations III 105 3 1 1 Dismantling assembling of the Analyzer housing cover TH 105 3 2 Battery troubles replacing the battery III 105 3 3 Fire detection thermofuse replacing 111 106 3 4 Fuses HI 106 3 5 Connecting an external alarm device III 107 3 5 1 Characteristics of the external alarm connection IH 107 DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 11 DL FP92 5G2 APPENDIX A ALARMS i o cciss dovsscsnsosstucsonseosenvossescscecesnveseusevesustessleseuncsesdeonssovegevenus songs shnesveuseosncesstueebsadececseonesseses 109 T Categories Of alarms iiron e EEE EEEE E EO EE EEG LOE 111 1 1 Fault alarms 111 1 2 Report alarms 111 1 3 Warning alarm 111 2 Displaying alarm cause stopping audio alarm ses 112 FeAlarmtreatment Cereri inenen ait eii aa ae T the Laois e a ME sta tia 112 4 E V ANT AEE AE EEEE N EAE E EE 113 SEP UL GIANG esea SN ie aet ae beat NOM th wel ba el Es ee cathy sh the e oaaao Ge a the tete 23104 tt 113 5 1 Switching to standby 113 5 2 Summary of some failures 114 5 2 1 Fire detection 114 5 2 2 Signal conditioning failure 114 5 2 3 Memory failures 114 5 2 4 No test flame gas igniter 114 5 2 5 Glow plug current failure gas igniter 114 5 2 6 Sample temperature failure 115 5 2 7 Abnormal heating rate 115 5 2 8 Flash detection failure 115 5 2 9 Program checksum error 115 5 2 10 Abnormal flash detection 115 5 2 11 Abnormal atmospheric pressure 115 5 2 12 Mot
32. point 3 5 5 RS232 link test message The external link test message sent is ISL FP92 5G2 17 CR LF See section 5 2 4 RS 232C External link 11 75 page 11 73 for the procedure If the message is very rapid don t forget that when there isn t any protocol used the time between successive messages can be set section 6 2 1 4 Data flow control page II 81 of this chapter 6 External link test The external link test message sent is ISL FP92 5G2 17 CR LF See section 5 2 4 RS 232C External link page Il 75 for the procedure If the message is very rapid don t forget that when there isn t any protocol used the time between successive messages can be set section 6 2 1 4 Data flow control page II 81 of this chapter Appendix B 128 Manuel d utilisation FP92 5G2 DOCV207A001 F Example of the use of RS 232C link with a PC DL 7 Example of the use of RS 232C link with a PC It is possible to use a program like Software Wedge for Windows of TAL Enterprises This software permits you to record the results in a given format or to transfer them directly to a Windows application Spreadsheets Data Base via the DDE Example Reception of a Result and Test Run Conditions messages and preparation of a delimited ASCII file using Software Wedge Version 3 0 Editor Professional 7 1 Analyzer configuration e Hardware 9600 baud 8 data bits 1 stop bit parity none e Software setup EOT 3
33. running 1 47 8 4 1 Igniter check after pressing RUN START 1 47 8 4 2 Manual test stop I 47 8 5 Standard test stop triggered by automatic detection I 47 8 5 1 Flash on first flame test I 49 8 5 2 Detection before the standard phase I 49 8 6 Cleaning the test set I 49 9 Reg lar MAINeNANCe serein tin E A rene ut teen a E a ee I 51 PART II ADVANCED USE OF THE FP92 5G2 eeseeseeeessereesoeseroorseroesoreerseeeesoeeereorsereorseeoereeeeesorsereorsoreereoesee I 53 General Lien Learn e ee e E ad ook tat E E E er da atthe Lak Ok e da I 55 ATEA TEATA E AE EAE A E A EEE ad atl inl UAE H 55 3 Calibration the Quality SMON ts cvcs xia ha scedss cassis seneeias casas tele wieean ETEEN TE EAEE STEKTE E 11 56 3 1 Sample temperature measurement calibration I 57 3 2 Periodicity and test start refusal I 59 3 3 Probe correction table 11 60 3 4 Atmospheric pressure measurement calibration 11 61 4 Run environment definition the Runs environment Menu uses 11 62 4 1 The ISL FP92 5G2 test principle 11 62 4 2 Test parameters I 62 4 2 1 Identification and definition parameters I 64 4 2 2 Fast Phase II 65 4 2 3 Standard Phase 11 66 4 2 4 Final Phase 11 67 4 3 Customizing a test entering parameters II 67 4 4 Modification of an already existing test II 70 4 5 Samples edition and display II 70 4 6 Specification pages editing and display II 71 4 7 Operators name edition and display 11 72 4 8 Customizing run mode screen 11 72 5 Diagnost
34. the red indicator on the connection panel illuminates The flash detection threshold of the ionization electrode can be adjusted by qualified personnel see in Part Ill chapter 2 External operations page III 104 3 2 4 The sample temperature probe The Pt100 platinum temperature probe is mounted in a Teflon holder on the flash detector temperature probe arm It is connected to Rep on the connection panel of the test unit see Figure l 4 page 1 31 To assemble the temperature probe simply push it into place in the Teflon holder and connect it as indicated above The temperature probe is automatically positioned at the beginning of the test Measuring range 100 400 C 148 752 F The probe positioning command can be checked using diagnostics or lt Control gt of the RUN START screen To do so select Probe 3 2 5 The damper The third arm controlled by the 3 motion control mechanism is the damper arm The damper is automatically positioned after fire point detection To remove the cup after testing the operator simply flicks the damper with his finger to release it The damper positioning command can be checked using diagnostics or lt Control gt of the RUN START screen To do so select Damper 3 3 Diagnostics All diagnostics are presented in the chapter 5 Diagnostics and measures the Service menu page Il 73 DOCV207A001 F FP92 5G2 User and Maintenance Manual Page l 25 ae DL FP92
35. to display an edited sample e Select Samples display of the RUNS ENVIRONMENT menu to display the sample in the memory if there is one e Select lt Show List gt to display the list of samples there are 2 pages press lt Down gt for the 2nd e Select the sample to be displayed and the previous screen reappears displaying the selected sample Page 11 70 FP92 5G2 User and Maintenance Manual DOCV207A001 F DL Run environment definition the Runs environment menu Peo a 4 6 Specification pages editing and display The access to results pages needs level 1 access password Results pages from 1 to 20 are reserved for the pre programmed samples A results page 21 which can receive a maximum of 50 results also exists Flash point result specifications can be edited for pages 1 to 20 In this way an upper and a lower results limit can be associated with the results page of any pre programmed sample This associated page is selected during Samples edition see section 4 5 Samples edition page Il 70 Flash result specification page editing consists of entering 2 results values upper and lower limits When a test run is performed using a pre programmed sample the result observed corrected or rounded depending on the test configuration is compared with the upper and lower limits If the result is within the specifications in spec for the results page then it is recorded in this page If a result of a pre programmed sample is
36. 105 PROM 114 RAM 114 Safe memory 114 Fault No test flame 114 Fault Glow plug current failure 114 Fault Sample probe 115 Fault Abnormal heating rate 115 Fault Flash detection failure 115 Fault Program checksum error 115 Fault Abnormal flash detection 115 Fault Abnormal atmospheric pressure 115 Fault Motor board link 115 Fault Test system 115 Fault Motor board link 115 Fault Heating 116 Fault Test flame abnormally lit 116 Fault Test start refused on SC6 Sample Changer connected 116 Fault No cup detected on Sample Changer 116 Final Phase Test parameters I 67 Fire detection I 27 Fire detection Replacing thermofuse III 106 Flags Input Circuit Signals I 74 Flame Test I 47 Flash on first flame test 117 Flash point I 18 Flash point detection Threshold adjusting III 104 Flash point test Preparation and procedure I 41 Flash Safety Alarm at EFP Page 111 138 FP92 5G2 User and Maintenance Manual Test parameters I 67 FP92 5G2 I 19 Function keys I 37 Fuses Main III 106 G General II 55 General scope I 19 Go No Go II 67 Test parameters I 67 H Hardware Flow control RS 232 II 82 Heating Diagnostics I 75 Heating rate Possible combinations II 66 Heating rate Test parameters II 65 I Igniter Diagnostics Il 75 Ignition Source I 24 ISL 4 ISL FP92 5G2 Software Protection 4 K Keypad 1 37
37. 2 ISL has once again developed a user friendly and ergonomically attractive petroleum product Analyzer Our regular customers will recognize the ISL experience and reliability combined with the now established mark of the new generation of ISL Analyzers The Analyzer you have just acquired has been born of a combination of customer feedback and over 20 years of experience in the design and manufacturing of petroleum products Analyzers The ISL FP92 5G2 automated Analyzer has been designed for the determination of the Cleveland Open Cup Flash and Fire Points for all petroleum products except fuel oils and those having an open cup flash point below 79 C 175 F The flash point of a material is used to define flammable and combustible materials Flash point can indicate the possible presence of highly volatile and flammable materials in a relatively non volatile or non flammable material The Fire Point measures the characteristics of the sample to support combustion see ASTM definition further on The ISL FP92 5G2 Analyzer can be used to perform Flash point and Fire point tests according to the ASTM D92 IP 36 IP 403 ISO 2592 EN 22592 NF T60 118 and JIS K2265 standard methods use The user of the ISL FP92 5G2 should establish the appropriate safety and health A These standards do not address all the safety concerns if any associated with their practices before using the Analyzer Summary of ASTM Test Method The test cup is filled to
38. 7A001 F DL Run environment definition the Runs environment menu P a 4 2 2 Fast Phase Do not confuse this phase with the preheating phase This phase is optional and provided for those operators who wish to start the test rapidly and or who wish to apply the ignition source before the temperature EFP 28 C for ASTM D92 specified in the standard method It is particularly interesting for heating samples that have a high EFP It can also be used to rapidly determine an approximate EFP for a sample This phase can be disabled by selecting none for the heating rate The 2 heating phases can have same heating rate high high or standard standard In this way a uniform heating rate will be kept for the 2 phases but the frequency of the E igniter presentation may be different The minimum limit value for the end of the fast phase before the first presentation is thus disregarded The fast phase igniter presentations continue until the temperature of the start of the standard phase Heating rate 3 possibilities exist None disables the fast phase Standard 5 5 C min 10 F min et High 15 5 C min 27 5 F min Selection during test creation Flip flop type Test Every Interval in C F between igniter applications The minimum value for a high heating rate is 6 C 12 F and maximum value is 100 C 200 F For the standard heating rate the test frequency can be from 1 to 100 C 2 to 200
39. C or F corrected or not by barometric correction depending on the product programmed Appendix B 126 Manuel d utilisation FP92 5G2 DOCV207A001 F DOCV207A001 F Transmitted data z Meaning of result message fields under ticket form from left to right Result message R Identification Analyzer No Type of message identifier Test name Sample No Test No Cup No Temperature Unit Expected flash point Flash point Flash point at first application Corrected flash point Fire point Corrected fire point Type of test stop Calibration indicator 5 3 The run context message Number characters 2 2 12 12 2 2 D JAJA anlan aoan of Description R for result 1 to 20 1 to 6 always 99 when the sample changer is not connected C or F always 999 9 always 999 9 10 11 or12 After flash flash and fire detection or flash and fire safety detection indicates that next calibration date has passed or that the temperature measurement values were adjusted manually is sent in all other cases The run context message is transmitted in only one message C Example elr CNCC 02 10 2001 AAO SOT SS 75 Meaning of run context message fields from left to right Message C Identification Analyzer number Type of message identifier Operator name In spec page no Out of spec page no In spec indicator Atmospheric pressure Pressure unit Type of igniter Glo
40. D risk of electrostatic discharge 5 5 Installation of the SC6 Sample Changer Refer to the documentation provided with the Sample Changer Page 1 34 FP92 5G2 User and Maintenance Manual DOCV207A001 F L Specifications installation and switching on 5 6 Switching on 1 Before plugging in the Analyzer and the printer to the mains supply make sure that the mains supply matches the specifications on their identification plates Serious A damage may result from using an incorrect voltage supply 2 Analyzer peripherals for example the printer and the external link should only be connected while the Analyzer and the peripheral equipment are switched off Switch on the main ON OFF switch see Figure l 5 page 1 31 at the rear of the Control Unit The screen lights up If it doesn t first check backlight and contrast settings see Figure 1 9 page I 37 5 6 1 Switch on display At switch on the display becomes a Had ISL FP92 5G2 Groupe ISL Z l Verson wwwisl France com 14790 VERSON Tel 33 2 31 26 43 00 France Fax 33 2 31 26 62 93 lt Espagnol gt lt Frangais gt lt Deutsh gt lt English gt Screen 1 Switch on display Press the key corresponding to the desired language The Run test display appears DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 1 35 FP92 5G2 Sample ID Sample No EFP C Fire point N Test 1 ASTM D92 C C Operator KExit gt
41. E PRINTING submenu 1 of 3 settings are possible for the Regulation check parameter in SERVICE PRINTING e 0 No regulation check printout The default value on switching on is 0 e 1 Regulation check printing on connected and On line printer The third is reserved for ISL 5 3 4 Printer reset To command a printer reset select Printer reset of SERVICE PRINTING DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 11 77 ae DL 6 Configuration Analyzer setup menu Ex Page 11 78 About ISL FP92 5G2 KExit gt ANALYZER SETUP Printer setup Run default values Ext link setup Lab manager setup Technical setup Real time clock ISL setup Sample changer setup Screen 36 6 1 Printer setup Accessing to the printer setup needs the access level 1 e Select Analyzer setup in the main menu e Select Printer setup in the ANALYZER SETUP menu PRINTER SETUP Paper width Red ink code End of printout line feeds 5 Light format for result printing O N Automatic results printing O N Degree symbol ASCII code 248 KExit gt Screen 37 Paper width flip flop 40 80 Red ink code Ref Printer doc Automatic results printing flip flop Y N Degree ASCII code Ref Printer doc Printer line feed 5 for example Light format for result printing flip flop Y N printer User Manual FP92 5G2 User a
42. ELECTION screen appears Cup Sample ID 1 Sample No 5 6 lt Exit gt Flash Fire C lt Print list gt Screen 7 Cup selection e Select the cup 1 to 6 The screen becomes CUP DATA ENTRY Sample ID Sample No EFP C Fire point Y Test Operator lt Cancel gt N Delete contents Stop after run N lt OK gt Screen 8 Cup data entry e Enter the test start parameters The contents of an already programmed cup can be deleted by selecting Delete contents Deletion of the contents can be cancelled by selecting lt Cancel gt It is possible to program the sample changer to stop after a test run by selecting Stop after run In this way the temperature probe and flash detector can be cleaned before the next programmed cup When ready the sample changer should be rotated manually using the optical sensor on the SC6 control panel Select lt OK to start a test as programmed After selecting lt OK gt the first programmed cup will start automatically DOCV207A001 F FP92 5G2 User and Maintenance Manual Page l 45 DL FP92 5G2 8 3 1 Programming further cups If you want to program a test for another cup select it from the list and repeat the above operation The cup already under test is not available for renewed programming until the test in hand has finished and the Time under choker has been completed The corresponding line is blanked
43. ERS EEE TEE ee ets ee a eae Sates A ns ne ne es 126 5 1 Message format 126 5 2 The result message 126 5 3 The run context message 127 5 4 The test program message 128 5 5 RS232 link test message 128 6 External link testes sovctie ch enr intended Po HATA RE 128 Page 12 FP92 5G2 User and Maintenance Manual DOCV207A001 F 7 Example of the use of RS 232C Tink with a PC ere 129 7 1 Analyzer configuration 129 7 2 PC Software configuration 129 7 2 1 Menu Port Settings 129 7 2 2 Start and end of record 129 7 2 3 Input record structure 129 7 2 4 Input record definition 130 APPENDIX C MASTER PASSWORDS nnnsnnennnnnnnsennenenennnensnensenneennenneenneenneesnenee 131 INDEX e E se nstsans osunsoasaese oo docsuastbedestaessussosens suiecavanns estocenadssd ovevussadensddaves ssncvesdssvovevessass 135 LON ae seis cic ce ca tee ese ea ak tea scat wien cng RCE te ated SR Hts CoE ig ae 137 DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 13 z FP92 5G2 Page intentionally blank Page 14 FP92 5G2 User and Maintenance Manual DOCV207A001 F Part I Using the FP92 5G2 z FP92 5G2 Page intentionally blank Page l 16 FP92 5G2 User and Maintenance Manual DOCV207A001 F 2 General DOL 1 General 1 1 ISL Company Profile We would like to take this opportunity to thank you for choosing ISL product We are confident that you will be completely satisfied with your new Analyzer and we ho
44. F The operator should enter a value for the 2 categories of EFP EFP lt 110 C 230 F EFP gt 110 C 230 F N B It is possible to enable the fast phase without entering Test every program parameters the result is no igniter presentations until the start of the standard phase It is possible to proceed to a safety test at the beginning of the tests by setting this parameter to 999 9 C Test every Tests start at 0 C a flame application is done at test starting the next one will be done in standard phase Start test at If the fast phase is enabled then the operator can enter here the temperature for the first application of the igniter End of fast phase The temperature at which the fast phase ends should be such that the next phase the Standard Phase begins correctly i e in accordance with the conditions outlined in the standard method being used The value of this program parameter depends on the heating rate combination used for the test The minimum limit values for this program parameter are given in the table further on If the value is less than the minimum limit value in the table then the limit value indicated will be used as the default value and this non conformity will be signaled as a warning alarm The operator should add the start test at value entered for the standard phase to the corresponding limit value A correct value must be entered so as to obtain the correct heating rate
45. L Lab manager Setup I 83 Laboratory Setup I 83 Last run result Validation I 93 M Maintenance 11 103 Manual stop Test I 47 Measurements checks I 40 Measures Display Il 74 Measures Atmospheric pressure I 40 Modification of an already existing test II 70 N No test flame 114 Numerical pad I 37 O Operators Display Il 72 DOCV207A001 F Operators name Edition I 72 P Passwords I 28 PC link Alan RS485 link I 33 Loading Unloading data I 34 RS 232C 1 34 Service port I 34 Power consuming devices I 20 Power On Parameters Setup II 87 Preheating time Test parameters II 64 Pre safety Alarm at EFP Test parameters II 67 Presentation The Cleveland elements I 24 Presentation ISL FP92 5G2 I 20 Printer Diagnostics 11 75 Reset I 77 I 94 Printer Setup II 78 Printer Link test II 95 Printing One Sample Contents I 94 One spec page II 95 One test contents I 95 Regulation check I 77 Results II 96 Run environment I 94 Service III 103 Printing list Samples I 94 Tests II 94 Printing list Operators II 94 Printing list Results pages II 94 Probe Correction I 40 II 60 Correction table II 60 Replacing III 104 Response Time Correction I 40 Probe and flash detector Diagnostics I 75 Program Checksum Error 115 PROM Fault 114 Protocol of communication 123 Q Quality I 56 R RAM Fault 114
46. MAXIMUM TIME Entries possible for the latter parameter are 1 900s Refer to the chapter 6 Configuration Analyzer setup menu section 6 4 Run default values page 11 87 5 2 17 Low battery This failure is tested for permanently If this failure is signaled e Do not switch off the Analyzer data stored could be lost e Perform Service Parameters uploading making sure to use a new file name e g use the date in the file name SPDDMMYY NVM Refer to the chapter 6 Configuration Analyzer setup menu section 6 3 4 Upload Download page II 84 In this way the last internal parameters version will be saved in a file e f necessary replace the Analyzer battery the battery life is 7 to 8 years refer to the Part III chapter 3 Internal operations section 3 2 Battery troubles replacing the battery page IlI 105 Regular uploading should be performed as part of the maintenance schedule of the Analyzer 5 2 18 Test flame abnormally lit This failure is tested for in standby If it is signaled the operator should check that the flame is in fact lit If it is not the detection ignition device may be at failure If it is have a qualified technician engineer check the ignition system In the latter case e Switch off the gas supply source e Switch off the Analyzer 5 2 19 Test start refused on SC6 Sample Changer connected In standby if the Sample Changer is connected the system checks that the e Test s
47. Make sure that the Analyzer is supported on a level steady surface e Thoroughly clean and dry all parts of the cup and its accessories before starting the test Any deposits of carbon on the cup should be removed with steel wool Flush the cup with cold water and then dry it using an appropriate method for a few minutes to remove the last traces of cleaning solvent and water Take particular care to avoid the presence of cleaning agents solvents used after a previous test Cool the cup to at least 56 C 100 F below the expected flash point before using e Carry out the regular checks as described in the previous chapter chapter 7 Measurements checks page I 40 of the current part If calibration is necessary refer to the chapter 3 Calibration the Quality menu page II 56 LU For other preparation procedures consult the standard method CN The section Preparation and procedure contains extracts from the ASTM D92 Standard Method DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 1 41 ae DL FP92 5G2 8 2 Test procedure 1 Fill the test cup with the test specimen so that the top of the meniscus is exactly at the filling line inside the test cup If too much specimen has been added use a medicine dropper or similar device to remove the excess If there is any sample on the outside of the cup empty clean and refill it Eliminate any air bubbles or foam on the surface of the liquid while maintaining the prop
48. R Reserved for public relations department IN ss covsawesd P E REPORT Date ceecesscesseeeseenee PURPOSE wish to Report an error Submit a suggestion a comment Get more information In the area of Hardware Software Manual ANALYZER ENVIRONMENT please be complete e HARDWARE Type of analyzer iecere Seral NY 5e hunter nn ns Options Parallel printer Graphic printer Plotter RS232C interface Alan c e SOFTWARE Version 22 41 unten ATTACHED SHEETS Listing Diskette Drawing Text Other PROBLEM DESCRIPTION COMMENTS SUBMITTED BY Name Company Address Phone Fax Date Send this report to your local Sales office or to Groupe ISL Service Clients BP 70285 14653 CARPIQUET CEDEX FRANCE Tel 33 2 31 26 43 00 Monday through Friday from 9 00 a m to 5 00 p m French Time Fax 33 2 31 26 62 93 E mail service paclp fr Web www isl france com DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 5 z FP92 5G2 Page intentionally blank Page 6 FP92 5G2 User and Maintenance Manual DOCV207A001 F ey DL Caution This ISL Analyzer has been carefully designed manufactured and inspected for quality It has been equipped with a number of safety features However the use of this Analyzer may involve the handling of solvents chemicals and other potentially dangerous flammable toxic etc materials Please exercise
49. S485 link setup connection to the Alan Part Il 6 2 network Part Il 6 4 Deletion of the Sample changer setup menu from the run default values Part Il 6 4 2 Adding of the safety parameter Probe missing safety Part Il 6 7 Adding of the parameter Time between two cups Part II 11 3 Detection principle adding of ei abnormal detection before this Adding of the alarm review RS RS 4 Modification of the setting of conditions of the Check probe position alarm Er B Detailed explanation on the RS 232C communication protocol Deletion of the spare part list consult the DOCV207X200file of the spare part list Deletion of the spare part list consult the DOCV207X200 file the DOCV207X200 file Displaying of the Sample N in the test starting screen of the sample Part 8 3 changer key lt Cups Data gt 08 18 06 DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 3 DL FP92 5G2 ISL C copyright The ISL FP92 5G2 Analyzer and this manual are protected by copyright Reproduction of the unit will result in prosecution All rights to the manual are reserved Reproduction in any form including in the form of excerpts shall require written permission from the copyright holder ISL FP92 5G2 Software 2000 ISL This software is owned by ISL and is registered under the registration number IDDN FR 001 110042 00 R P 2000 000 30000 at the Agence pour la Protection des Programm
50. Sample Changer Width 365 mm 365mm Depth 360 mm 690mm Height 520 mm 520mm Weight 27 kg around 41 kg Conforms to Standard Methods e ASTM D 92 e IP 36 and IP 403 e EN 22592 and NF T60 118 e ISO 2592 e JIS K2265 Environmental Characteristics e Storage Temperature 20 to 50 C e Operating Temperature 10 a 40 C e Recommended Operating Temperature 15 35 C Power Supply e 100 120V and 200 240V at 50 or 60Hz e Power Consumption 700 W max e Safe Memory Non volatile RAM NVRAM backup battery life 7 to 8 years Heating e Low Voltage Heating Element 24 Volts limited at 550 Watts Igniter Standard Analyzer equipped with a gas flame igniter Gas Supply e Gas SV Inlet Tube O D 10 mm e Gas admission pressure standard gas cylinder pressure security maximum 1 bar e Test unit silicon gas tubing to igniter nozzle D3 5 D1 5 mm External Link e Standard Centronics parallel interface for printer e ALAN Interface e Service Port e RS 232C Serial Link with or without protocol signals and codes CTS ENQ ACK XON XOFF on 9 pin output male connector Fire Detection e On fire detection an audio alarm is triggered and the Analyzer switches to standby e A safety relay is provided for connection of a fire extinguishing system and or an external alarm See the relevant section of the manual 3 Part e Thermofuse mounted on the test arm 157 C 250 V AC 10 A Temperature Measurement e Measuring instr
51. Specifications installation and switching on page I 29 In the displayed screen select Main menu and then Full mode run access level 1 The full mode run must be exited to allow a normal mode run FULL MODE RUN Prepare the run Ready for run End of full mode run lt Exit gt Screen 50 This mode allow to create a new test from an existing one the current test or any pre saved one This can be done at a time if values are known or by a experimental approach based on successive tests The resulting test can be saved and reloaded if it s needed 8 1 Using current test program If the operator decides to use the current test program in the memory he should select Ready for run and start the program using the same principle refer to the Part chapter 8 Flash point test page I 41 DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 11 91 ae DL FP92 5G2 8 2 With modified current test program or another program If the operator wants to modify the current program before starting the test or if he wants to load another test program he should select Prepare the run PREPARING A FULL MODE RUN Load a test Edit loaded current test Save the current test Print the current test KExit gt Screen 51 The operator can now e Modify the current program e Load another program e Save a modified program e Print the current test e Select Ready for run an
52. The number of results in that page selected items e The number of In spec and Out spec items e The maximum and minimum result values e The average result value e The standard deviation or the mean square deviation The mean square deviation is calculated by the formula xj All results 2 De x Xa mean or average result Drs N N sample number Dms standard deviation Once the operator has made his item choice see above he can select lt Print gt to print out the statistics or the statistics and the selected items collectively To do so select e Statistics only or e Statistics and selected items Printout with all the results provides all results on the page For page 21 the statistics zone at the beginning of the printout will be blank DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 11 97 ae DL FP92 5G2 11 3 Results Display Printing and transmitting To displa rint or transmit results e Select Result memory in the main menu e Select One result display print transmit e Select Show list e Select a result page from the list press lt Down gt for the 2nd page of the list to be visualized Having selected a page the previous display reappears with the Selected Page indicated e Select lt Show results gt and the last result recorded on that page is displayed e The information on the results displayed can be divided in 5 parts 1 Number of the result
53. To check that the igniter is operating correctly e Select Igniter in the DIAGNOSTICS screen to display the IGNITER DIAGNOSTICS screen 5 2 6 1 Test flame igniter If you want to light the test flame the gas supply source must be connected at the rear of the Analyzer and switched on e Select Flame Gas SV as to display ON The test flame must light e Select Main Gas SV to display ON The solenoid valve emits a clicking sound when opened DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 11 75 DL FP92 5G2 e Select Glow plug to display ON so as to light the test flame Once the pilot flame has been lit Set at OFF as to extinguish the igniter If you have just switched on the gas supply you may have to be patient and wait for a the gas to arrive 5 2 6 2 Presentation of lighted igniter Having lit the installed igniter using the IGNITER DIAGNOSTICS screen it can then be presented e Select lt Exit gt to return to the DIAGNOSTICS screen and then select Flame test The lighted igniter is presented as already explained above 5 2 7 Sample Changer SC 6 e Select SC 6 Rotation to rotate sample changer by one cup position 5 3 Service printing internal parameters It is always useful to have printout recordings of the Service Parameters and Measures The SERVICE PRINTING menu is called up by e Selecting Service in the main menu and then selecting Service printing
54. a specified level with the sample and put in position The temperature probe and the flash detector are automatically positioned at the beginning of the test The temperature of the sample is increased rapidly at first 14 to 17 C 25 to 30 F min and then at a slow constant rate 5 to 6 C 9 to 11 F min as the flash point is approached Starting at least 28 C 50 F below the expected flash point and at each successive 2 C 5 F a small test flame is passed across the center of the cup The presentation of the igniter whether test flame or electrical igniter is performed automatically by displacement of the igniter arm at the specified intervals The lowest temperature at which the application of the test flame causes the vapors above the surface of the liquid to ignite is taken as the flash point To determine the fire point the test is continued until the application of the test flame causes the oil to ignite and burn for at least 5 seconds The operator can also run a non standard Flash point Fire point test on the FP92 5G2 Analyzer DEFINITIONS The Flash Point is the lowest temperature corrected to a barometer pressure of 101 3 kPa 760 mmHg at which the application of an ignition source causes the vapors of a specimen of a sample to ignite under specified The Fire Point is the lowest temperature at which a specimen will sustain burning for 5 seconds EFP Expected Flash Point The material is deemed to have flashed when a
55. able _ ENQ No result ACK gt If the analyzer has results it starts their transmission On receiving the message the host computer must check it checksum and must reply ACK O6H or NAK 15H depending on whether the message was correct or not If there are several fruitless communications the host computer may decide to abort transmission by sending an EOT 04H character ANALYZER HOST COMPUTER Successfull transmissions ENQ 1 result message XXXXX p ACK 4 ENQ Next result YYYYY gt s ACK ENQ No more result ACK gt ANALYZER HOST COMPUTER Result sent faulty reception ENQ 1 result message XXXXX gt not properly received NAK 4 ENQ Same message XXXXXX gt not properly received lt lt NAK ENQ Same message XXXXXX gt not properly received Host ends the communication EOT Abort DOCV207A001 F Manuel d utilisation FP92 5G2 Appendix B 125 ae DL FP92 5G2 5 Transmitted data Example 1 R ACTIVA 3000 120796 1 6 99 C 208 0 209 0 209 5 999 9 999 9 10 0B 1 C LG 4 21 0 100 6 1 E 7 0 12 07 96 0 11 29 3 1 T D92B FAST O 1 1 2 2 0 999 158 1 2 0 191 0 N 228 238 999 6C The data that can be transmitted are divided in 3 groups Result See messages R below See messages C below If defined in the RS232 link setup Test product See message T below If define
56. ain When the Analyzer is switched off during downloading on switching on again it will detect a transfer requirement and will signal this requirement to a connected PC on which the transfer program is running 6 3 4 1 Principle of transfer procedure The Analyzer goes into transfer mode either by automatic detection or by operator request it waits for transmission from the PC Once the PC transfer program is loaded it sends a message to the Analyzer The Analyzer indicates the type of transfer required After a safety protection exchange between the PC and the Analyzer the PC sends the required information to the Analyzer which treats this information The PC confirms the termination of the transfer 6 3 4 2 Installation and starting the transfer program Follow the instructions of Read me file 6 3 4 3 Transfer requested by the operator Preparation e Switch off the host PC and the Analyzer and connect the external link cable between the serial link connector at the rear of the Analyzer and the host PC Switch on the PC and Analyzer e Note the names of the HEX and NVM files in the C ISL MEMPROG sub directory On the Analyzer e Select Upload downloaa in the TECHNICAL SETUP submenu UPLOAD DOWNLOAD Internal parameters upload Internal parameters download Program download Text download Warning Reset required to terminate lt Exit gt Screen 46 e Select the required command The Analyzer di
57. ar corner of the control unit housing e From the rear slid the cover to the rear so as to disengage the positioning tabs in the rear of the LCD screen housing Remove the cover to the rear A Always replace the housing cover before switching on the Analyzer Reassembling of the cover is done as following e Fit the cover from the rear First engage the positioning tabs on the bottom of the cover Then put the rear corner test unit side of the cover in place Next engage the positioning tabs of the front of the cover in the holes provided in the rear of the screen housing Make sure that the positioning tabs are opposite these holes before pushing the cover forward into place e Replace the 3 screws 2 in the bottom corners and 1 in the top rear corner test unit side of the control unit chassis 3 2 Battery troubles replacing the battery If a low battery problem is signaled when the Analyzer is switched on proceed as explained in the section 5 2 17 Low battery page 116 If battery replacement is necessary proceed as follows Before handling the processor board or any other electronic components touch a CS grounded metallic element to discharge yourself 1 Switch the Analyzer off 2 Remove the Analyzer cover housing as explained in section 3 1 1 page Ill 105 of the current part 3 Locate the processor board see the figure below 4 The battery is the very small black box on the screen side of the processor boar
58. at the first presentation In any case if the fast phase is too long the system will be automatically regulated so as to respect the heating rate of the Standard Phase the mini limit value given the table below being substituted for the erroneous parameter value If the operator is not sure of the value to be entered it is best to leave it blank and the value will be calculated automatically See also the graphs below DOCV207A001 F FP92 5G2 User and Maintenance Manual Page II 65 FP92 5G2 Register End of fast phase Fast End of EFP 28 phase fast phase Temperature Time Heating rate Time 250 12 200 gt 10 s Y 150 S8 nm 100 se 6 S amp 4 Be P o i EFP 17 EFP F i 3 De 3 Fast End Standard EFP phase Time phase of fast phase Time phase Curve 1 Curve 2 Fast Phase None Standard None lev e High High Standard Standard Phase Standard High Standard X minimum values 28 C 0 C 0 C End of fast phase values if the tests start at EFP 28 C Tableau 1 Heating rate combinations possible and fast phase limit values 4 2 3 Standard Phase This phase sets the parameters heating rate interval between igniter applications temperature of first application of the igniter in accordance with the standard method being used Heating rate possible combinations and fast phase limit values Heating rate 2 possibilities exist Standard 5 5 C min 10 F in or High 15 5
59. ation 4 1 Failures and alarms 4 1 1 Fire detection 4 1 2 Failures switching the Analyzer to standby 4 1 3 Failures refusing a test start and stopping a test run 4 1 4 Report alarms 4 1 5 Warning alarms for non conformity correction 4 2 Passwords 5 1 Technical specifications 5 2 After unpacking 5 3 Connections 5 3 1 Gas supply connection 5 3 2 Connecting the relight glow plug 5 3 3 Assembling the flash point detector and the temperature probe 5 3 4 Connecting printer 5 3 5 FP92 5G2 PC link 5 4 Handling precautions for LCD devices LCDs 5 5 Installation of the SC6 Sample Changer 5 6 Switching on 5 6 1 Switch on display 5 6 2 Auto test The Analyzer interlace seirinin e a e era rare ara aetna 6 1 Keypad 6 2 Display 6 3 Text editing 6 4 Entering a numeric value 6 5 Flip flop entries 7 1 Temperature measurement 7 1 1 Temperature probe reading 7 1 2 Response time correction 7 2 Atmospheric pressure measurement DOCV207A001 F FP92 5G2 User and Maintenance Manual DL FP92 5G2 STE LGSWPOUMELESE ETES MANN RE ANR E ee ee dR Balt ins ON ne nr nr 1 41 8 1 Preparation and procedure I 41 8 1 1 Sampling 1 41 8 1 2 Preparation 1 41 8 2 Test procedure I 42 8 2 1 Selecting a test procedure 1 42 8 2 2 Test starting 1 43 8 3 Test starting on the Sample Changer I 45 8 3 1 Programming further cups 1 46 8 3 2 Programmed cup 1 46 8 3 3 Cup selection screen 1 46 8 3 4 Sample Changer control panel 1 46 8 4 Test
60. ator can enter 1 to 255 minutes If the preheating is enabled the heating power is applied until the bottom of the cup reaches a temperature of approximately 400 C after about 2 min At this point the preheating count commences The preheating continues for the duration programmed for this program parameter 1 to 255 min When entering this parameter keep in mind that the probe will be positioned in the cup 2 minutes before the end of preheating If the preheating time is 1 minute the probe will be positioned at the beginning of the preheating count N B It is possible modify the preheating time during a test using the lt Control gt function of the Run Start screen Barometric correction It is possible to automatically correct the thermometer readings for the calculation of results 3 possibilities exist e 1 ASTM According to the barometric correction indicated in the ASTM D92 01 standard method e 2 ISO According to the barometric correction indicated in the standard method ISO 2592 00 e None no barometric correction Selection during test creation Flip flop Rounded 2 possibilities Y or N If Y is selected the result will be rounded off after the barometric correction to the nearest test usually every 2 C E g For a test every 2 C Flash detected 187 C Corrected flash 188 1 C Flash corrected and rounded 189 C Page II 64 FP92 5G2 User and Maintenance Manual DOCV20
61. ce Line status in standby 12 V MARK Input signals used CTS RTS DOCV207A001 F Manuel d utilisation FP92 5G2 Appendix B 123 ae DL FP92 5G2 3 Communication protocols Flow control Protocol can be gt None gt RTS CTS gt Xon Xoff gt ENQ ACK Powe Type Gammon i Xon Xoff ENQ ACK Appendix B 124 Transmitted messages are sent without any way to stop them from the host computer However a special parameter Time between two messages in the ISL analyzers allows to define a pause between to successive message from 0 0 s to 10 0 s by step of 0 1 s Note This time is applied between 2 entire messages not between characters Existing signals defined in the RS232C interface standard are used to control the transmission Connect the host computer serial RTS signal to the analyzer CTS signal When the input buffer of the host computer is full the RTS signal changes its state Seeing its CTS signal changing the analyzer stops transmission until CTS changes again Note This hardware handshake is controlled by the communication hardware analyzers and can stop restart transmission between any characters This well known handshake is qualified as software protocol because it is controlled by the host computer reception software to control the data flow If the software needs time to process the last incoming message it can send the Xoff character to the analyzer which imm
62. ce Manual DOCV207A001 F Configuration Analyzer setup menu DL 6 7 Sample changer setup e Select ANALYZER SETUP in the main menu refer to the Screen 10 page II 55 e Select SAMPLE CHANGER SETUP in the ANALYZER SETUP menu refer to the Screen 36 page Il 78 There are 4 parameters e The Sample changer on line menu permits to a FP92 5G2 Analyzer which has a Sample Changer connected to be operated as a single post without disconnecting the Sample Changer this parameter should be set at N selected by flip flop This may be necessary if the sample changer is out of order If the Changer on line parameter is N at power on and a sample changer is connected the operator is warned by display Likewise if this parameter is Y at power on and the sample changer is not connected the operator is warned by display The status of this parameter is indicated on the initial display see Part chapter 5 Specifications installation and switching on page 1 27 e The Time between two cups menu is used for setting the minimum time between two tests so that exhaust evacuation is enabled programmable from 15 to 999s e The Time under damper after flash fire parameters are used for setting the minimum time under the damper dampers the damper zone is comprised of 3 cup positions There are 2 parameters one for test runs ended by flash point detection and one for tests ended by fire point detection If another tes
63. conds Flame test lighting which continues until the test flame is lit respecting the limits imposed by the No test flame fault alarm Preheating Preheating phase of program for solid or viscous samples gt Tests The phase before the temperature the first presentation of the igniter Tests The temperature for the first presentation of the igniter has been reached Presentation Automatic presentation of the igniter Applications the number of applications of the igniter lt Flame Test gt to present the igniter at any time during a test run lt Fin gt back to test run screen The date the time and the intensity of the glow plug current During the igniter application the great size temperature display is locked The displays will be unlocked only if the flash point has not been detected Thus if the flash point is detected the detection temperature will still displayed after the test automatic stop 8 4 1 Igniter check after pressing RUN START If a test flame is being used as igniter check its diameter To adjust the test flame to a diameter of 3 2 to 4 8 mm 5 32 according to standards If necessary use the setting knob in the front side of the control unit Figure 1 3 page I 25 8 4 2 Manual test stop The test can be stopped manually at any time during a test run 1 Press the keypad STOP key 2 Confirm the current test stop by selecting Ok at screen 8 5 Standard test stop trigger
64. configured N for no then the operator must manually validate the last run result before it will be transmitted on the external link If another result is recorded before validation for transmission the result will be lost LN See the chapters 9 Result of the last test run the Last run result page Il 93 and chapter 10 Printings the Printing menu page II 94for more information c End of transmission EOT character e Select End of transmission character EOT type in the numerical value and confirm with ENT The EOT character falls into 2 categories 0 or gt 0 1 99 EOT Character 0 There is no EOT character at the end of transmission EOT Character gt 0 The last character sent is the EOT character 6 2 1 4 Data flow control e Select Data flow control in the RS 232 LINK SETUP submenu The display becomes RS 232 FLOW CONTROL Hardware flow control RTS CTS N Software flow control XON XOFF N ENQ ACK protocol N Time between two successive messages If no protocol used 0 0 s lt Exit gt Screen 42 The first 3 parameters keys for protocol selection are Flip flop with Y N as choices Only one of them can be configured Y e Select the desired configuration which is automatically taken into account on selection a Transmission without protocol The last parameter can be used when no protocol is used i e when all of the RS 232 Flow control protoc
65. corresponding cup amp A test has been programmed on the cup but the cup is waiting to be tested ongoing test on another cup The test having stopped the delay programmed by the Sample changer setup parameter Time under damper after flash fire has not yet been completed For further information on the Time under damper after flash fire parameter see the relevant section in the chapter 6 Configuration Analyzer setup menu section 6 7 Sample changer setup page II 89 If the sample changer is disconnected the Changer on line parameter should be set to N If not a message will be displayed on switching on the Analyzer SC6 off line cE and parameter ON An alarm Changer motor failure will also be signaled Update this parameter the Analyzer must be switched off and on again Page l 46 FP92 5G2 User and Maintenance Manual DOCV207A001 F 2 Flash point test DL 8 4 Test running The test running screen gathers the following information EFP Expected Flash Point The EFP may be modified during a test Screen 2 page I 36 or during a test in the test running screen Screen 6 page l 44 Status Current status of the Analyzer Here is a table with the significance of the Status field Field value Significance Idle The apparatus is in standby Rotation The sample changer is being positioned only when the accessory is installed Ignition Glow plug ignition for about 15 se
66. d 5 Unclip the battery carefully using a small flat tipped screwdriver if necessary 6 Insert the new battery being careful orientation it correctly 7 Reassemble the Analyzer cover see the section 3 1 1 page IIl 105 of the current part before switching on the Analyzer DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 111 105 DL FP92 5G2 Battery Processor board Figure III 4 Internal view of the Analyzer 3 3 Fire detection thermofuse replacing If an external fire extinguishing system has been connected by the user disconnect it before the following verification To test the Fire Detection alarm switch off the Analyzer and remove the thermofuse by unplugging it Switch on the Analyzer without the thermofuse The Fire Detection alarm should be triggered To stop the audio alarm switch off the Analyzer To replace the thermofuse proceed as follows 1 Switch off the Analyzer 2 Unplug the defective thermofuse 3 Replace with a new thermofuse 3 4 Fuses Switch off the Analyzer and disconnect it from the mains before removing any fuses For continued protection against risk of fire replace only with a fuse of the specified type and current rating as indicated in the Spare Parts list at the end of this manual appendix e There are 2 mains fuses at the rear of the Analyzer located below the mains supply socket see in Part e To remove the mains fuses e Use a screwdriver to open t
67. d ISO 9001 certification in 1995 Though best known for distillation viscosity testing cold behavior instrumentation flash point evaporation loss oxidation and asphalt testing equipment ISL s contributions to automated petroleum testing continue to grow With more than 10 patents to date ISL s constant research into new technologies buttresses our precedent for ultimate precision performance and safety The company now offers over 20 Automatic Analyzers for different applications giving incontestable benefits to its users in increasing of test precision by elimination of operator subjectivity and human errors while increasing productivity and reduce operator time with highest level of safety A worldwide distribution network supports our customers with quick efficient service and our highly knowledgeable service staff buttresses this relationship providing solutions to product or application challenges Please visit our web site for more information www islfrance com DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 1 17 iSL FP92 5G2 1 2 Symbols and typographical conventions The symbols and the typographical conventions used in this manual are the following Conventions Meaning Bold Italic Menus or submenus to selected in the LCD screen Bold CAPITALS Menu up screen indications Bold CAPITALS Keys on the front panel of the device ae Note Important comment AN Attention Call for particular care
68. d by Stop after cup or anomalies After this alarm the cup under test stays in position Restarting can be performed by e A RUN START of the cup in position for example by re entering the EFP e Rotation of the SC6 to the correct position using the photosensor Push button when another cup has been programmed The STOP key unlocks the cup under test Page A 118 FP92 5G2 User and Maintenance Manual DOCV207A001 F ay DL Warning alarms 7 Warning alarms An intermittent audio alarm is triggered and the red indicator on the keypad is illuminated The active pulse is always half that programmed for the Error Report alarms Acknowledgement of the alarm extinguishes the indicator On displaying the origin of the alarm Warning alarms are indicated by a number WARNING No NN The list of single warnings and the corresponding warning numbers are given in the table below How to use the following table for multiple warnings If the warning number displayed is not in the table below then a multiple warning has been signaled If 2 or more warnings are signaled the warning number displayed is the sum of the individual warning numbers For example if the safety alarm temperature is too high 2 and the fast heating phase is too long 8 the warning number displayed will be the sum 2 8 therefore 10 Warning No Description of problem 1 Frequency of flame presentation i e the parameter Test Every is no
69. d in the RS232 link setup To be transmitted a result must be validated by A manual validation that must be performed at the analyzer level refer to the section 9 2 page 11 93 The transmission is only possible after the validation An automatic validation that can be set in the RS232 link setup refer to the section 6 2 1 3 page II 80 5 1 Message format Messages are in ASCII code Character strings are enclosed within double quotes They start with an opening bracket They finish with a closing bracket 2 characters CK and the characters CR LF and EOT CK 2 characters checksum the 2 least significant digits expressed in ASCII of the result of the hexadecimal sum of all the preceding characters including the brackets CR 1 non printable character Carriage Return ODh LF 1 non printable character Line Feed OAh EOT 1 non printable character End Of Transmission character programmable in the RS232 setup menu If 0 there is no end of transmission character Ee The value 999 indicates that the field is not being used reserved for a future use 5 2 The result message As indicated above if the transmission of data on the RS 232C link has been validated automatic or manual validation the result message is systematically transmitted under the form 1 R ACTIVA 3000 120796 1 6 99 C 208 0 209 0 209 5 999 9 999 9 10 0B Temperatures are expressed in
70. d start the program using the same principle as for a normal test It is also possible to print the current program In Full mode the operator can view all the details of the test program by selecting lt Down gt in the test start display 8 3 Exiting Full mode To run a test after a Full mode run select End of full mode run lf the current test program has been created and not saved it will be lost on quitting Full mode when the operator confirms by lt OK gt The context of the program will be also lost on quitting If the operator wishes to conserve the exact program created in Full mode he must select Save the current test of Prepare the run before exiting Full mode The default program on switching on is reselected as current program on quitting Full mode Page 11 92 FP92 5G2 User and Maintenance Manual DOCV207A001 F Result of the last test run the Last run result DL 9 Result of the last test run the Last run result The Last run result menu of the main menu is provided for displaying printing and validation for transmission on the external link of the result of the last run e Select Last run result in the main menu e To print the last run result select Print e To display the last run result select Display After having checked the last run result e Select Validate external link transmission in LAST RUN RESULT display e lf Automatic Validation of Results is configured N
71. displayed over the number of results stored in memory n N and item on the page 2 Conditions of the test amp Sample ID sample no operator name test no test name and atmospheric pressure amp The EFP the observed Flash Point result the corrected Flash Point result amp rounded Some events are interpreted as a detection ex a bubble touching the flash detection ring and the analyzer can not know if it is really the flash point yet a flash point can not be detected while the test arm is at rest Test flame passing Detection If the analyzer registers one or several detections near the flash point but out off the flame presentation phase the flash point detected is uncertain Test flame passing Detection So the analyzer registers detections occurred between the three last phases of the test If it is the case the system indicates the result obtained is uncertain with an asterisk in front of the flash result Flash 150 0 C the message Abnormal detection before this flash will be printed on the last line of the result ticket 3 In spec information Yes No or Safety _ for page 21 and an indicator if amp The probe temperature measurement values were manually adjusted i e without using the automatic calibration function of the system refer to the section 6 3 3 page Il 84 amp The next
72. e II 84 Specification pages iSL FP92 5G2 Display I 71 Specification pages Edition and display I 71 Standard Phase Test parameters II 66 Start test at Test parameters I 65 Starting Flash point test 1 43 Statistics I 97 Symbols and typographical conventions I 18 T Temperature measurement Checks I 40 Temperature unit Test parameters II 64 Test Parameters I 62 Principle I 62 Test Every Test parameters II 65 II 66 Test flame Adjusting I 25 Test flame and pilot light I 24 Test flame igniter Diagnostics I 75 Test name Test parameters II 64 Test procedure I 42 Test running I 47 Test start II 66 Test starting on the Sample Changer I 45 Test unit I 23 View I 23 Text Editing I 39 Thermofuse Remplacement III 106 Transmission with protocol RS 232C II 82 Transmission without protocol RS 232C II 81 Transmitted data RS 232 1 79 V Validation Automatic of results II 81 Manual of results I 81 Results II 81 View Test unit I 23 W Warning Alarms 1 27 Page 111 140 FP92 5G2 User and Maintenance Manual DOCV207A001 F
73. e Analyzer and the PC e Switch them both on again e Start up the transfer program as before and the Analyzer may request a transfer in the same way as explained above in section 6 3 4 2 page II 85 If a down load is necessary the Analyzer detects this automatically this need When the Analyzer is waiting for a download the red LED will flash every second e A downloading in progress is indicated by rapid flashing which is related to the rate of data transfer Page II 86 FP92 5G2 User and Maintenance Manual DOCV207A001 F Configuration Analyzer setup menu 6 4 Run default values The access to this menu needs the level 1 access password e Select Analyzer setup in the main menu e Select Run default values in the ANALYZER SETUP menu RUN DEFAULT VALUES Power on parameters Safety parameters lt Exit gt Screen 47 6 4 1 Power on parameters e Select Power on parameters in the RUN DEFAULT VALUES submenu e Select Atmospheric pressure unit It can be mmHg or kPa Selection is by flip flop e Select Default test and select a test from the resulting lists e Select Screen saver after _ min Enter a time in minutes before the backlight is switched off standby mode The duration before the screen standby mode is activated can be set from 1 to 99 minutes If it is set to 99 minutes the backlight remains switched on This function is not active during flash point tests The standby
74. e Manual Page A 113 ae DL FP92 5G2 5 2 Summary of some failures 5 2 1 Fire detection The system tests for this failure from auto test until switch off If the failure is detected the system always switches to standby The Analyzer must be switched off to stop the audio alarm Once verifications and reparations have been carried out replace the thermofuse 5 2 2 Signal conditioning failure This failure is detected when a dialogue absence between the Central Unit and the digitizer is detected 5 2 3 Memory failures After the Analyzer switching on the content of the different memories is regularly checked by the microprocessor If an error exists it will be detected by calculation and comparison of a checksum control PROM If a PROM failure is signaled switch off and on the Analyzer If the failure still exists contact the ISL Service Department RAM If this failure is signaled switch off and on the Analyzer If the failure still exists contact the ISL Service Department Safe Memory Non volatile RAM NVRAM The life duration of the NVRAM memory battery is approximately 7 to 8 years This alarm may be due to a faulty battery The content of the non volatile memory where the Service Parameters are stored is checked by the microprocessor If an error exists the Analyzer automatically goes into download mode to restore the back up memory content by loading a backup file from a PC For this a diskette con
75. e Save memory to a host computer e An external link cable for uploading downloading e An ALAN RS232 C adapter Page 1 26 FP92 5G2 User and Maintenance Manual DOCV207A001 F ay DL Analyzer system safeties 4 Analyzer system safeties All parts of the Analyzer that may come in contact with the operator are not exposed to voltages exceeding 24 volts EN 61010 1 The provision of handles permits the test cup and the heating plate to be removed in complete security Any malfunctioning will be signaled by an audio alarm The origin of failure error and report alarms may be displayed 4 1 Failures and alarms 4 1 1 Fire detection The system is equipped with a fire detector On detection of fire the system switches the Analyzer to standby A continuous audio alarm is triggered and remains active until the Analyzer is switched off A continuous audio alarm is triggered and the type of alarm can be checked by pressing ALARM STOP Any external alarm fire extinguishing system connected by the customer will be triggered by the fire detection fault e Commanding of the gas supply SV and the igniter is disabled To stop the alarm the Analyzer must be switched off e The user can connect an external alarm device see in Part Ill section 3 5 Connecting an external alarm device page lll 107 The user can also connect his own fire extinguisher device to the system security relay In this case those devices are also set off 4 1 2 Failures s
76. e and the temperature probe with a suitable cleaning agent In general all dirty accessories including the test flame nozzle that might affect the test run result should be cleaned Depending on the state of the different accessories for example the choker they may be disassembled for a thorough cleaning The use of knurled screws make the assembling disassembling procedures more easier no particular tools are needed see the figures Figure l 10 and Figure l 11 below VAN Do not use cleaning solvents near a flame DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 1 49 DL FP92 5G2 Damper fixation Knurled bolt Damper Figure 1 10 Temperature probe fixation knurled Screw Flash point fixation knurled screw Figure 1 11 Page 1 50 FP92 5G2 User and Maintenance Manual DOCV207A001 F L Regular maintenance 9 Regular maintenance Specific time intervals are not given for these checks In fact the ideal time intervals depend on the Analyzer environment frequency of use and the customer s Quality Assurance needs The following conditions should be taken into consideration when deciding the regular maintenance time intervals e Ambient temperature above 25 C 77 F e A number of different Analyzer operators e Dirty or dusty ambient air e The Analyzer is operated during multiple shifts each day The optimal time interval will only come from experience Here is a list of checks and possible maintenance
77. e operator can setup the analyzer to sent the Conditions of run and the Test contents Refer to the Appendix B section 5 page 126 for the description of the messages sent through the RS 232C link 6 2 1 2 Hardware setup Communication parameters e Select Hardware setup in the RS 232 LINK SETUP submenu to display RS 232 HARDWARE SETUP Baud rate 9600 baud Data bits 8 Stop bits si Parity None KExit gt Screen 40 e All the parameter keys are of the flip flop type with 2 or more possibilities taken into account on selection refer to the Appendix B section 1 page 123 6 2 1 3 Software setup e Select Software setup in the RS 232 LINK SETUP submenu The display becomes RS 232 SOFTWARE SETUP Analyzer ID 0 99 1 Automatic validation of results N End of transmission character 0 KExit gt Screen 41 a Analyzer ID number e Select Analyzer ID and type in and confirm with ENT the Analyzer ID number 0 99 This number is sent with each result message Page II 80 FP92 5G2 User and Maintenance Manual DOCV207A001 F DL Configuration Analyzer setup menu b Automatic validation of results Use the Flip flop key Automatic validation of results to display Y or N elf Automatic validation of results is set at Y for yes then the result is automatically transmitted when the test run is terminated e lf Manual validation of results is
78. ed 0 to 365 days If the CS calibration frequency is not respected the operator is warned on starting a test It is also possible to disable test starting if the calibration frequency is not respected 7 1 1 Temperature probe reading A temperature probe correction function is available This correction is performed using a temperature table from 0 to 400 C 32 752 F at intervals of 20 C 36 F Refer to the chapter 3 Calibration the Quality menu page Il 56 7 1 2 Response time correction There is also a function which permits the correction of the temperature probe response time so that it equivalent to an ASTM D92 thermometer for the Cleveland Flash and Fire point test This correction only applies during test runs 7 2 Atmospheric pressure measurement For this check the operator must use a reference barometer 1 Select Service in the main menu 2 Select Measures display to display the current measures of the Analyzer 3 Check that the Atmospheric pressure reading on the display is the same as the reference barometer reading If calibration is necessary refer to the chapter 3 Calibration the Quality menu page II 56 Page 1 40 FP92 5G2 User and Maintenance Manual DOCV207A001 F 2 Flash point test DL 8 Flash point test 8 1 Preparation and procedure 8 1 1 Sampling The operator should be familiar with the applicable sampling standards given in the standard method In particular do
79. ed by automatic detection As already indicated the EFP flash pt can be modified until the first automatic application of the igniter The EFP at this point is memorized and will be displayed on the Flash point result line after flash point detection e If the fire point has not been requested an intermittent audio alarm is triggered when the Flash Point is detected If the fire point has been requested the result is recorded and the test continues After flash point detection and before fire point detection 1 The current sample temperature is displayed On the first line below the large Sample temperature display are displayed 2 the EFP at the first automatic igniter presentation 3 the number of igniter applications until the flash point 4 the FLASH point detected and 5 a result indicator for the In spec test see the chapter 10 Printings the Printing menu page Il 94 The result information is also available at the bottom of the Test start screen DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 1 47 DL FP92 5G2 If the Fire Point was requested the EFP memorized at the first fire pt application is displayed on the 2nd line below the large Sample temperature display The number of igniter applications A for the fire point is also displayed on this line The first fire point application is counted from the first application after flash point detection If no fire point was requested this
80. ed with the pre programmed sample The upper and lower result limits are entered during Specification pages editing described in section 4 6 Specification pages editing and display page 11 71 When a test run is performed using a pre programmed sample the result observed corrected or corrected amp rounded depending on the configuration during Test Customizing is compared with the results specifications mini and maxi If the result is within the specifications In spec it is recorded in the In spec page specified for the pre programmed sample see section 4 5 Samples edition and display page II 70 If the result is not In spec it is recorded in the Out of spec page of the pre programmed sample The Out spec page may be the same as the In spec page or it may be the page 21 All the results that are not from pre programmed samples will be recorded in page 21 The storage of the results in all the pages functions on a FIFO first in first out basis When the maximum number of results that can be saved on a page is greater than 5 the First In First Out system processes the results in blocks of 5 results This means that when the maximum number of results plus one are recorded the first block of 5 results is displaced and lost When the maximum number of results for a page is 5 CS only one result is lost when the 6th result is recorded There is no warning when a result or a block of results is displaced from a r
81. ediately stops the transmission until it receives from the host computer the Xon character This is a full protocol It allows flow control and data acknowledgment The transmission is fully controlled by the host computer which must send an ENQ enquiry character Any message must be acknowledged by the host computer by sending a ACK character Note There is no need to define a time between messages because the message sequencing keeps pace with the ENQs sent by the host computer Manuel d utilisation FP92 5G2 Xon 11H Xoff 13H Developed by ISL this protocol is detailed below DOCV207A001 F ay ENQ ACK protocol details DL 4 ENQ ACK protocol details The host computer must acknowledge all messages from the analyzer Should communication fail only the host computer can decide whether or not to abort transmission Analyzer response time on receiving ENQ lt 100 ms Waiting time for message acknowledqment 2 sec Results transfer delay after end of test delay for ENQ not limited Number of transmission of the same result message on not limited end with ACK or EOT receiving NAK reception Request reception and acknowledgement of results The host computer uses the ENQ code 05H to ask the analyzer if any results are ready to be sent If the analyzer has no results to send it replies ACK 06H The host computer does not have to reply to this ACK ANALYZER HOST COMPUTER No result avail
82. er level of liquid in the cup 2 Correctly place the heating plate the insulating sheet and the test cup 3 Make sure that the sample temperature probe is correctly connected and that the probe is correctly mounted in its holder on the flash detector temperature probe arm 4 Put the anti draught shield in position accessory 5 Igniter check after pressing RUN START Check that the test flame diameter If necessary use the valve setting knob see Figure l 3 page I 25 to adjust the test flame to a diameter of 3 2 to 4 8 mm 5 32 according to the standard The test start procedure used depends on the customer s needs A number of procedures are indicated in the next section Ce A fire point measurement can be requested in the TEST START screen 8 2 1 Selecting a test procedure Several test procedures are possible The user can proceed very quickly by entering only the EFP or eventually by calling back the previous one This kind of procedure assume minimal prior run environment definition default values pressure unit and the test No Refer to the section 6 4 Run default values page II 87 The user can also give more or less information about the test run environment by entering or selecting the right elements in the given lists operator or test names This other kind of procedure need a prior complete environment definition Refer to the Part Il chapter 4 Run environment definition the Runs environmen
83. es 249 rue de Crim e 75019 Paris It is protected in France by the Code de Propri t Intellectuelle laws and internationally by international treaty provisions and all other applicable national laws It must not be copied reproduced adapted translated rented or disassembled This also applies to the accompanying manuals INFORMATION Information in this document is subject to change without notice and does not represent a commitment on the part of ISL ISL provides this document as is without warranty of any kind either expressed or implied including but not limited to the particular purpose ISL may make improvements and or changes in this manual or in the product s and or the program s described in this manual at any time This product could include technical inaccuracies or typographical errors Changes are periodically made to the information herein these changes may be incorporated in new editions of the publication Reproduction of any part of this manual without express written permission is forbidden Translation in foreign local language other than French or English Translation in other language than French and English have no contractual value and have been performed under responsibility of the local distributor In any case the reference of the present literature will be the French and or English release provided under ISL copyright Page 4 FP92 5G2 User and Maintenance Manual DOCV207A001 F CUSTOME
84. esults page Also no recording will be made of test runs which do not result in Flash Point detection except tests stopped on Safety e A maximum of 550 results can be recorded in all the pages taken together e Memory space for 50 results is reserved for page 21 e The pages 1 to 20 can be configured during specification pages editing for from between 5 to 50 results in steps of 5 i e 10 15 20 45 50 respecting the total number 500 of results permitted Page 11 96 FP92 5G2 User and Maintenance Manual DOCV207A001 F Results and printing the Results memory menu 11 2 Statistics Select Result memory in the main menu e Select Statistics e Select Selected page to choose the results page e Select the results page from the list of 20 pages ae Statistics are not available for the Fire Point or for page 21 e Use Selected item to select by flip flop for the page displayed one of the following 1 All the results 2 Inspec results only 3 Out of spec results only Having made your item choice press lt Display gt to display the statistics page STATISTICS Page _ Items All results Selected items _ In spec 8 Out ofspec 0 Result min 62 0 Result max 64 0 Average 63 00 Deviation 0 71 lt Exit gt Screen 53 The above display indicates the page selected and the type of selection for the Selected page e g All results Also indicated are e
85. for no in the RS 232C SOFTWARE SETUP then the operator must manually validate the last run result before it will be transmitted on the external link Ez If another result is recorded before validation for transmission the result will be lost 9 1 Displaying the last run result The display LAST RUN RESULT DISPLAY indicates e The date and the time e The sample ID the sample no the operator the test no the test name and the atmospheric pressure e The observed and the corrected or the corrected amp rounded Flash Point result e An indicator if The probe temperature measurement values were manually adjusted i e without using the automatic calibration function of the system see section 6 3 3 Modification of the sample temperature calibration values page II 84 or e The next calibration date has passed e The observed and the corrected or the corrected amp rounded Fire point result To print the result from this display press lt Print gt 9 2 External link transmission validation e After having checked the last run result e Select Validate external link transmission in Last run result display e Select lt OK gt to validate DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 11 93 ae DL FP92 5G2 10 Printings the Printing menu The Analyzer is equipped with a standard Centronics parallel printer interface including a standard 25 pin PC connector A 40 column or an 80 co
86. gt Screen 12 For calibration of the sample temperature measurement the sample temperature probe must be disconnected and replaced by an ISL probe simulator PS 400 Disconnect the temperature probe see in Part chapter 5 Specifications installation and switching on page I 29 and connect probe simulator e Select Temperature measure calibration of TEMPERATURE MEASUREMENT screen TEMPERATURE MEASUREMENT CALIBRATION Operator OP1 Calibration reference REF Use 0 400 C probe simulator Use resistance values lt Exit gt Screen 13 e Enter the operator name and the calibration reference If the probe simulator has not been guaranteed 0 C 400 C then its resistance values should be guaranteed and their exact values must first be entered Resistance values can be guaranteed by ISL or another authorized company Resistance Values Guaranteed Entry of exact values e Select Use resistance values DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 11 57 DL FP92 5G2 TEMPERATURE MEASUREMENT CALIBRATION Resistance on position 0 100 00 Ohms Resistance on position 400 247 06 Ohms KExit gt Screen 14 Enter the exact resistance values to 2 decimal digits opposite O C and 400 C Typical ISL probe simulator values are indicated in the above display e Press lt OK gt to confirm Continue as described for Probe simulator guaranteed below Probe S
87. gt and the test is displayed Modification and saving of the existing test are performed in the same way as program creation described in section 4 3 Customizing a test entering parameters page II 67 It may be saved under the same test no using Save or a new test no using Save As 4 5 Samples edition and display The raison d tre of sample families has been evoked in section 4 1 The ISL FP92 5G2 test principle page II 62 To create or edit a sample the operator laboratory manager access level 1 selects the Samples edit function of RUNS ENVIRONMENT He may immediately use the lt Show List gt function to display the list of sample numbers from 1 to 20 He may at this point select the sample number an already existing one or a free one From the Samples edit display e Select the lt Edit gt function to switch the system to Edit mode e Enter the ID and the EFP 20 350 C 70 660 F If you wish to continue the test until the fire point is detected display Y N to disable fire point detection The temperature unit C F displayed is selected during test program creation e Enter the In spec and Out spec pages The Out spec page may be the same page as the In spec or it may be the page 21 The user must now save the sample he has just edited The principle is the same as that described in section 4 3 above for saving a test program Just as it is possible to display a test it is also possible
88. haracter on the display or select directly the line concerned by pressing the corresponding left selection key then use the arrow keys LEFT RIGHT The number keyboarding is directly done on the numeric keypad e Press the ENT key the selected letter is displayed in the Sample ID box e Use the arrow keys again to select the 2nd letter in the Sample ID box e Etc To delete a character in the edit box use the BACKSPACE key or the arrow keys to select the character and then select lt Del gt To insert a character select lt nser gt The Alpha Edit key allows to activate one or the other one of the two cursors In this way confirm each character of the desired text The complete text will be displayed in the Edit box e Press ENT again to confirm the displayed text collectively e The previous display reappears with the text displayed on the initially selected line e g Sample ID e Press the RESET key to abandon editing e When the cursor is positioned in the Sample ID edit box digits are entered directly from the keypad 6 4 Entering a numeric value e Using the corresponding function key to the side of the screen select the line directly on the screen e g EFP The cursor is placed for data entry e Use the LEFT RIGHT arrow keys for digit position selection and the UP DOWN arrow keys to select the digit value The BACKSPACE key is also available or enter the digits directly from the keypad e Di
89. he flap and remove the fuse holders e Replace with a new fuse 6 3A 230V 10A 115V Page 111 106 FP92 5G2 User and Maintenance Manual DOCV207A001 F L Internal operations 3 5 Connecting an external alarm device It is possible to connect an external alarm device onto the Analyzer The connector provided for the connection of the user s external alarm device functions as an ON OFF switch for the user s device The user must provide the power supply for his alarm device This connector has 3 connection positions 1 2 and 3 such that e Thermofuse OK and in place 2 3 closed 1 2 open e Thermofuse blown or removed 2 3 open 1 2 closed VAN To stop the alarm the Analyzer must be switched off To connect an external alarm device the main Analyzer housing cover must be removed as described in the section 3 1 1 page 111 105 of this chapter At the rear of the Analyzer e Locate the grommet to the left of the fan at the rear of the control unit e Pass the wiring of the external alarm device through this opening e Connect the wiring of the external alarm to J1 on the post management board the connector located near the ventilator connection made by screw of the Igniter board in accordance with the requirements of the external alarm device and using the operation details given at the beginning of this section e Reassemble the housing cover not forgetting to respect the warnings indicated in section 3 1 1
90. he sample temperature probe to the corresponding connector of the connection panel see Figure I 8 page I 32 Figure 1 6 The test arm Figure 1 8 Assembling the sample temperature probe 5 3 4 Connecting printer Connect the printer to the parallel printer connector see Figure l 5 page 1 31 at the rear of the Analyzer before switching on the Analyzer or the printer Once the Analyzer and the printer have been switched on carry out a link check as described in the chapter 5 Diagnostics and measures the Service menu page II 73 For printer setup see section 6 1 Printer setup page II 78 Page 1 32 FP92 5G2 User and Maintenance Manual DOCV207A001 F DL Specifications installation and switching on 5 3 5 FP92 5G2 PC link The FP92 5G2 analyzer is fitted as standard with an RS 232C interface and an RS485 interface 5 3 5 1 RS485 serial link Connection to the ALAN Network The FP92 5G2 has been designed to run under the Alan management software developed by ISL itready RETR The Alan software Automatic Laboratory Analyzer Network is a multitasking software running under Windows and allowing up to 31 ISL analyzers to be connected to the same PC computer see the illustration below It allows data coming from different ISL analyzers to be collected and stored Besides multi analyzers results database management and control according to the analyzer type run control alarms displaying in
91. his field Field Input Filter Length Note 1 Ignore this field 1 2 None 3 3 None 5 4 None 15 5 None 15 6 None 3 7 None 3 8 None 4 9 None 6 10 None 6 11 None 6 12 None 6 13 None 6 14 None 3 15 None 3 16 Ignore this field 6 Field Postamble Keystroke virgule 17 None 3 18 None 5 19 None 15 20 None 3 21 None 3 22 None 4 23 None 6 24 None 4 25 None 6 27 None 13 28 None 3 29 None 8 30 Ignore this field 3 31 None 2 32 Ignore this field 1 Appendix B 130 Manuel d utilisation FP92 5G2 DOCV207A001 F Appendix C Master passwords z FP92 5G2 Page intentionally blank Appendix C 132 Manuel d utilisation FP92 5G2 DOCV207A001 F Example of the use of RS 232C link with a PC DL Factory Set Passwords are the following e The Laboratory password level 1 is 0 The master password is 3174 e The Service password level 2 is 0 The master password is 6216 To modify the factory set passwords refer to the sections listed below 1 For Laboratory password Access level 1 modification refer to the Part Il chapter 6 Configuration Analyzer setup menu section 6 5 Laboratory setup page II 88 2 For Service password Access level 2 modification refer to the Part II chapter 6 Configuration Analyzer setup menu section 6 3 Service service parameters page II 83 DOCV207A001 F Manuel d utilisation FP92 5G2 Appendix C 133 z FP92 5G2 Page intentionally blank Appendix C 134
92. ics and measures the Service menu sense 11 73 5 1 Diagnostics and measures displays 11 73 5 1 1 Diagnostics display 11 73 5 1 2 Measures display I 74 5 2 Different diagnostics II 75 5 2 1 Heating 11 75 5 2 2 Probe and flash detector 11 75 5 2 3 Printer 11 75 5 24 RS 232C External link 11 75 5 2 5 Damper 11 75 5 2 6 Igniter 11 75 5 2 7 Sample Changer SC 6 11 76 5 3 Service printing internal parameters 11 76 5 3 1 Service parameters list printing II 76 5 3 2 Measures printing 11 77 5 3 3 Regulation check 11 77 5 3 4 Printer reset 11 77 Page 10 FP92 5G2 User and Maintenance Manual DOCV207A001 F 6 Configuration Analyzer setup Menu eee II 78 6 1 Printer setup I 78 6 2 External link setup 11 79 6 2 1 RS 232C link setup 11 79 6 2 2 RS 485 link setup connection to the Alan network I 82 6 3 Service service parameters II 83 6 3 1 Regulation parameters I 84 6 3 2 Buzzer pulse width I 84 6 3 3 Modification of the sample temperature calibration values I 84 6 3 4 Upload Download I 84 6 4 Run default values Il 87 6 4 1 Power on parameters 11 87 6 4 2 Safety parameters I 87 6 5 Laboratory setup I 88 6 6 Real time clock Il 88 6 7 Sample changer setup I 89 7 Access levels and passwords the Access menu sense 11 90 7 1 Selection of the access level 11 90 7 2 Modifying passwords 11 90 8 Full mode run the Full mode run menu ses 11 91 8 1 Using current test program I 91 8 2 Wi
93. imulator Guaranteed the ISL PS 400 is guaranteed 0 and 400 C e Select Use 0 400 C probe simulator TEMPERATURE MEASUREMENT CALIBRATION 0 C 400 C KExit gt Screen 15 Page 11 58 FP92 5G2 User and Maintenance Manual DOCV207A001 F ay Calibration the Quality menu DL e Position probe simulator rotary switch on 0 C 32 F TEMPERATURE MEASUREMENT CALIBRATION Position probe simulator rotary switch on 0 C 32 F Temperature 0 X AID CCCCC lt OK gt when reading in stable Screen 16 e Position the rotary switch on 0 C and wait until the Temperature and A D readings are stable e Once the readings are stable press lt OK gt The previous display reappears This time select 400 C and the display becomes TEMPERATURE MEASUREMENT CALIBRATION Position probe simulator rotary switch on 400 C 752 F Temperature XXX X A D CCCCC lt OK gt when reading is stable Screen 17 e Position the rotary switch on 400 C and wait until the Temperature and A D readings are stable e Once the readings are stable press lt OK gt 3 2 Periodicity and test start refusal e Select Calibration frequency and enter the periodicity for the performance of calibrations in days 0 to 365 0 means that there is no periodicity programmed e Use the Start test refusal key to select Y for yes or N for no If thi
94. in the Cup selection screen The cup under test is indicated in the top right of the Test run screen activated by pressing lt Display gt 8 3 2 Programmed cup When a cup is programmed the corresponding red LED on the front of the Sample Changer lights up The LED will go out when the test has finished and the set time under the damper has passed indicating that the cup is ready for a new program 8 3 3 Cup selection screen Once a cup has been programmed it remains displayed on the cup selection screen after test stop until another test is selected for the cup or until the Analyzer is switched off If the Analyzer is switched off before a programmed cup led illuminated has gone into test then the programmed data remain in memory and on the Cup selection screen after switching on again The test will not however be started automatically it must be restarted by the operator To do so he must reselect the cup number in the Cup selection screen and then press lt OK in the Cup data entry screen 8 3 4 Sample Changer control panel 1 The ON OFF led on the right 2 An optical sensor for sample changer rotation Block it once just like touching a push button to rotate the sample changer by one cup position 3 Six cup LEDs When a LED is not illuminated it means that the corresponding cup is available for programming a test An illuminated led means one of the following conditions amp There is a test in progress on the
95. indicator is extinguished 1 3 Warning alarm A warning alarm indicates that the test started correctly but that the system had to intervene to correct a non conformity This alarm may be signaled during test starting or during a test run when an EFP modification provokes a warning The conformity of the test is guaranteed in its standard phase An intermittent audio alarm is triggered and the red indicator on the keypad is illuminated The active pulse of the audio alarm is always half that of the error report alarm Once acknowledged the indicator is extinguished A warning number is displayed on pressing ALARM STOP Warning no NN A table at the end of this chapter lists the warning numbers and the corresponding warnings see the Tableau 2 page 119 DOCV207A001 F FP92 5G2 User and Maintenance Manual Page A 111 DL FP92 5G2 2 Displaying alarm cause stopping audio alarm e When an audio alarm is triggered press the ALARM STOP key to discover the origin of the alarm refer to the section 6 1 page I 37 In the case of Fault Error and Report alarms the exact cause of the alarm is displayed Examples FAULTS AND ALARMS lt Review gt Fire detection Flash on first flame test End of test flash amp fire lt Exit gt lt Acquit gt Screen 55 In the case of warning alarms a warning number is displayed e Select lt Acquit gt to stop the audio alarm and return to the previous display
96. ine e Analyzer setup e Service setups e Quality calibrations e ISL configuration ce Only service parameters accessible by level 1 and 2 are treated in this manual DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 11 83 DL FP92 5G2 6 3 1 Regulation parameters The PID regulation parameters can be set manually by the Service engineer e Select Regulation parameters REGULATION PARAMETERS Kp pp Ti ili s Td ds Delta t xx s KExit gt Screen 45 Normally these values are not modified However it is possible to disable a parameter by entering 0 The delta is for information It cannot be modified by the operator 6 3 2 Buzzer pulse width This parameter is used to set the active pulse of the intermittent Error and Report alarms The active pulse of the Warning alarms is half the value set for the Error and Report alarms e Select Buzzer pulse width and type in a value between 0 and 100 ms Confirm by ENT 6 3 3 Modification of the sample temperature calibration values The low and high reference resistance values and the corresponding A D conversion counts relate to the temperature probe calibration They are set by automatic calibration and are not normally modified afterwards If they are manually adjusted using this function then an indicator will signal this on the results display and printout Refer to the chapters 9 Result of the last test run the Last run re
97. ing decided to display one of these items he may disable enable modification of the display item e Select the Customizing run mode screen of the RUNS ENVIRONMENT menu e Enable or disable the display item by selecting Y for yes or N for no Selection is by flip flop choice The configurable display items are e Sample ID display e Sample No display e Test ID display e Operator name display e Second screen display selected using the lt Down gt key in Run mode Run Start screen For the display items that have been selected for display the Modify keys on the right of the screen can then be used to enable disable Y N modification of the first 4 display items on the list above Page 11 72 FP92 5G2 User and Maintenance Manual DOCV207A001 F DL Diagnostics and measures the Service menu m 5 Diagnostics and measures the Service menu This chapter describes how the Diagnostics submenu is used to check the operation of the different elements of the Analyzer Diagnostics cannot be performed when in test running mode Likewise a test cannot Ce be started when the Analyzer is in diagnostic mode e Select Service in the main menu e Select Diagnostics in the SERVICE menu Once the DIAGNOSTICS display appears the Analyzer is in diagnostic mode and it remains in diagnostic mode until the lt Exit gt key is selected in this display 5 1 Diagnostics and measures displays DIAGNOSTICS
98. ing to be modified use the Show tests list command to select the test number then press on Edit selected test DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 11 67 iSL e Select New one and the first page for parameter entry appears CUSTOMIZING A TEST Name Temperature unit C Preheating time Barometric correction Y Rounded N lt Down gt Screen 27 FP92 5G2 Enter the test program parameters as explained in Part section 6 3 Text editing page I 39 See chapter 4 2 Test parameters page II 62 above for definitions of the various test program parameters 3 more pages of entries are made in the same way either by editing text or numeric values or by using flip flop type keys The 4 displays correspond with the 4 parts described in section 4 2 Test parameters page II 62 e To abandon test creation press RESET When all entries have been made and with the FINAL PHASE displayed Page II 68 FINAL PHASE lt Up gt Go No Go N Test at EFP only Pre safety a TP C Safety TP C Fire safety at EFP ZZ C lt Cancel gt lt Down gt Screen 28 FP92 5G2 User and Maintenance Manual DOCV207A001 F DL Run environment definition the Runs environment menu SS e Press lt Ok gt and the display becomes CUSTOMIZING A TEST Save Save as lt Exit gt Screen 29 e Select SAVE AS and the list of
99. is installed and switched on e Next No increment the sample number e Previous EFP for using the previous test EFP e The RUN START function is used to start the test selected on the screen If no igniting device is connected the field between brackets still blank FP92 5G2 User and Maintenance Manual Page 1 43 DL FP92 5G2 e lt Control gt This function allows 1 the access to the diagnostics of the damper the probe the igniter the test and the igniter arms 2 To the modification during the test of the preheating remaining time by entering a new value New time e The lt Display gt see Screen 6 below function switches the Analyzer to the 4 digit sample temperature TEST RUN display This TEST RUN screen is automatically activated at test start The temperature display can be read at a distance of 5 meters The expected flash point the Analyzer status e g Test the date the time and the glow plug current when it is used are also displayed e The lt Down gt key allows the operator to display the page numbers allocated to the results ln Spec and Out spec e The temperature T and the no of igniter applications A are displayed at the bottom of the screen These values evolve during a test The run mode screen can be set to display and give access only to certain functions CS Refer to the chapter 4 Run environment definition the Runs environment menu sec
100. is refused If a checksum error is detected print the program and check it for errors If no errors are found modify a parameter and save the program so as to force the calculation of the checksum 5 2 10 Abnormal flash detection This failure is tested for during a test run The test is not stopped It is signaled if e A flash point is detected before the igniter presentation phase and between actual presentations of the igniter e On lowering the flash detector probe arm a flash point is detected This is probably due to the cup being badly positioned resulting in the flash detector touching the cup The failure is not triggered by manual presentation commanded during the CS presentation phase a manual presentation is commanded by selecting lt Flame test gt of the test run Screen refer to the Part I 5 2 11 Abnormal atmospheric pressure This failure is tested for permanently A test cannot be started but a test run in progress is not stopped It is signaled if the pressure reading P is abnormal 590 mmHg gt P gt 830 mmHg 78 kPa and 111 kPa 5 2 12 Motor board link failure This failure is tested for permanently If it is signaled a test run cannot be started and a run in progress is stopped It is signaled when there is a dialogue problem between the central unit microprocessor and the keyboard microcontroller Switch off the Analyzer and then on again Have connections checked If the failure still exists c
101. isplay gt lt Down gt Tmp 22 1 App 0 Screen 5 Test run screen This screen contains following elements e Sample ID sample identifier ID e Sample No Sample number e EFP expected flash point if not entered via a pre programmed sample the EFP is entered directly See 6 4 Entering a numeric value page I 39 e Fire point a fire point measurement can be requested e Test Type of test for example ASTM D92 A IP 36 The Analyzer complies with the ASTM D 92 IP 36 IP 403 ISO 2592 EN 22592 NF T60 118 and JIS K2269 standard methods see in Part chapter 2 General scope page I 19 e Operator Operator s name e lt Exit gt to main menu The sample ID the type of test and the operator name can be pre programmed On ae selecting one of these functions the operator is presented with a list He should select one item from the displayed list Cup data DOCV207A001 F e Cup under test indicate the number of cups of the SC6 sample changer in test position 1 Nul the sample changer is not connected or is not switched on 2 0 No cup has been detected in test position or the sample changer has not been turned during its switch on or no cup has been found in test position after this rotation 3 1 6 indicate the detected cup in test position e lt Cups data gt the access to this function is authorized only if the sample changer
102. isplay the Output page in the memory e Select lt Show List gt and then select a specification page from the resulting lists e Select lt Print gt in the resulting OUTPUT PAGES DISPLAY 10 2 3 One test contents e Select One test contents of ENVIRONMENT PRINTING e Select Show tests list and select a test from the resulting lists e Select lt Display gt to display the test just selected The 4 screen pages of the test are also displayed in the same way e Select lt Print gt to obtain a printout of the selected test 10 3 Printer link test Refer to the chapter 5 Diagnostics and measures the Service menu page 11 73 section 5 Diagnostics and measures the Service menu page 11 73 of the current part DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 11 95 ae DL FP92 5G2 11 Results and printing the Results memory menu 11 1 Results pages Result pages from 1 to 20 are reserved for the pre programmed samples Flash point result specifications can be entered for these pages A result page 21 also exists but upper and lower results specifications cannot be entered for this page there are no specifications for the fire point results During samples editing described in chapter 4 Run environment definition the Runs environment menu section 4 5 Samples edition and display page II 70 the laboratory manager selects the results pages In spec and Out spec to be associat
103. istic printout and possibly transmission On the other hand they allow programs to be configured and the Analyzer to be set according to the needs of the user Moreover it is controlled to avoid any mistake The access to these functions presupposes that the user is familiar with the techniques of plugging tests The FP92 5G2 settings are accessible from the main menu see following sections 2 The main menu The main menu can be acceded from the initial screen select lt Exit gt from the test run screen MAIN MENU Quality Full mode run Runs environment Last run result Service Printing Analyzer setup Results memory lt Access gt lt Exit gt Screen 10 Main menu This menu gives access to the following functions Functions Content Access level Quality Temperature measurement calibration Run environment Service Analyzer setup lt Access gt Full mode run Last run result Printing Results memory DOCV207A001 F Next calibration date Probe correction table Atmospheric pressure calibration Programs samples operators and result pages edition Program sample operator and result lists display Customizing run mode screen Current measures and diagnostics Configuration Printer External link ALAN or RS232C Service Level 2 access password Regulation parameters Buzzer pulse width Upload Download ISL settings access level 3 Default values Laboratory setup Real time clock Entering password f
104. lating plates Asensor to detect the presence of a cup Amobile damper which is automatically presented at the end of the test to open the cup A fixed two cup safety damper which can be disassembled for cleaning A draught protector for the SC 6 Sample changer The control panel DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 1 21 en DL FP92 5G2 3 1 The FP92 5G2 Analyzer The ISL FP92 5G2 Analyzer is compact and self contained It can be globally divided into 2 parts the control unit and the test unit Test unit FP92 5G2 Figure 1 1 FP92 5G2 Analyzer 3 1 1 The control unit The Control Unit on the left includes In the front side The screen The keypad Contrast and brightness adjusting knobs Test flame and pilot light adjusting knobs In the back side The external link connectors Printer RS 232C ALAN The mains connector and the ON OFF switch Gas alimentation nozzle In the lateral right side or Connection panel The connectors of the sample temperature probe and of the flash detection device test flame relit the fire detection thermofuse the heating red indicator and the flash point red indicator and finally the flash point detection adjustment screw see Figure l 4 Connection panel connectors page 1 31 Page I 22 FP92 5G2 User and Maintenance Manual DOCV207A001 F Presentation of the FP92 5G2 DL 3 1 2 The test unit The Test Unit on the right
105. lifetime the screen automatically goes into standby mode after a period of inactivity the length of which can be programmed It is equally easy for the operator to set up the desired test the necessary information sample name and type of test can be taken from the lists of suggestions i e lists of sample names and names of tests relating to the standards listed in the previous section It should be noted that sample names can be associated with particular tests again for the sake of simplicity and speed If these are not the user s priority it is of course possible to fine tune the test parameters see in Part Il chapter 4 Run environment definition the Runs environment menu page II 62 Quite how finely the parameters are set depends of course on the access authorizations granted there are three levels of access A continuous audible alarm is triggered if a fault prevents the test starting or a current test proceeding The reasons for the alarms can be displayed see in Appendix A Alarms page 109 When atest is started all the incompatibilities that are not serious enough to warrant stopping the test are reported as warnings by an audible alarm and a Warning no XXX A list of the numbers of all the possible warnings is given in the Fault and warning alarms appendix At the end of the test an intermittent audible alarm sounds The test results are arranged in pages according to specification intervals With the necessary
106. line is not displayed After fire point detection the 2nd line displays 1 the EFP at the first fire point application 2 the no of applications until fire point detection and 3 the actual fire point detected If there is a fire safety alarm triggered the fire point displayed is 999 9 Fire xxx x Safety With xxx x Sample temperature at safety The operator can press ALARM STOP on the keypad to display End of test flash amp fire To stop the audio alarm select lt Acquit gt 1st flash point EFP flash Flash pt Fire pt application value detected detected EFP modification EFP modification allowed 1st fire test EFP fire for result line memorized EFP flash for result line memorized Once the test is stopped e The igniter arm returns to its standby position e The flash detector temperature probe arm is withdrawn to its standby position e The choker arm returns to its connection panel housing The flash and fire point temperature still displayed when the test is stopped The result observed corrected rounded depending on the program is displayed to the nearest first decimal digit The current sample temperature takes the place of the displayed detection temperature Ez in the following cases At the beginning of a new test by pressing the STOP key by selecting Sample ID Sample No or menu lt START RUN gt by selecting Prepare the ru
107. lt Measures gt Damper Printer Probe RS 232 link A Flame test Ignitor Heating Off Heating 0 SC6 rotation Test flame device lt Exit gt Screen 33 5 1 1 Diagnostics display Once the operator has activated a command he can use lt Measures gt to check the device in question In general the procedure is 1 Activate the command 2 Check the corresponding measures display reading e g Heating and or check directly the device e g igniter printout external link output When diagnostics are activated for any of the devices concerning heating and ignition heating element gas SV gas igniter and glow plug they remain active for 4 min DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 11 73 DL FP92 5G2 5 1 2 Measures display From the DIAGNOSTICS display press lt Measures gt MEASURES Cup under test Sample tmp 23 8 C Block tmp A D 27970 R 109 26 AID Heating 0 0 V Corr Rate 0 0 C min AID Atm prs 101 8 KPa Glow plug 0 1 A A D 19974 AID 150 Flash A D Flags HGFEDCBA PONMLKII KExit gt lt Print gt Screen 34 The MEASURES display can be used to check the current readings and the corresponding Analog Digital conversion counts This permits identification of abnormal readings and can aid you in identifying possible faulty components e Press lt Exit gt to return to the diagnostics display Flags or Status of Input Circuit Signals The Flags
108. lumn EPSON compatible printer can be used e ISL can deliver such a printer as an accessory e All printouts are in text mode e All print functions can be accessed from the Printing menu of the main menu e Select Printing of the main menu Results get in SECURITY can be displayed or printed See section 4 5 Samples Ce edition and display page 11 70 of the chapter 4 Run environment definition the Runs environment menu current part 10 1 Printer reset Resetting the printer has the effect of reprogramming the printer hardware and its interface e Select Printer reset in the Printing menu 10 2 Environment printing e Select Environment printing in the PRINTING menu The following lists can be printed immediately e Samples list e Operators list e Test results pages list e Tests list ENVIRONMENT PRINTING Samples list One sample contents Pages list One page contents Tests list One test contents Operators list KExit gt Screen 52 10 2 1 One sample contents e Select One sample contents and the Sample display in the memory appears e Select lt Show List gt and select a sample from the resulting display e Select lt Print gt to start printing of the displayed sample Page II 94 FP92 5G2 User and Maintenance Manual DOCV207A001 F ay DL Printings the Printing menu 10 2 2 One spec page contents e Select One page contents of ENVIRONMENT PRINTING to d
109. matically enabling to the test flame to be relit even if the pilot light is on The alarm is triggered if the glow plug current is outside the specified limits e lt 5A et gt 15A if the plug is lit e gt 1A if the plug is not lit The test that is running is not aborted Page A 114 FP92 5G2 User and Maintenance Manual DOCV207A001 F amp Fault alarms DOL 5 2 6 Sample temperature failure This failure is tested for during test running It is triggered if an abnormal temperature reading T is measured 100 C gt T gt 410 C 148 F and 770 F If detected the test is stopped Check the connection of the probe 5 2 7 Abnormal heating rate During the test this failure is triggered if the heating rate is greater than the setpoint this value can be set between 10 and 150 Vc of the heating rate setpoint The test is not stopped if the sample temperature is less than the EFP but if the temperature is greater than the EFP the system stops the test if the Stop if heat rate alarm amp tmp gt EFP is set on Yes refer to the section 6 4 2 Safety parameters page Il 87 5 2 8 Flash detection failure This failure is tested for at run start and during a run If it is signaled a test cannot be started and a run in progress is stopped This failure is signaled if the flash detector ring is not connected Check the connection 5 2 9 Program checksum error This failure is tested for at run start up Test start up
110. meter temperature is approaching 6 1 2 Flash on first flame test Except for a Go No Go run this error alarm is signaled if the flash point is detected on the first flame test of a normal flash point test The run is therefore terminated 6 1 3 Result out of spec Signaled when the flash point result is not within the specification limits entered This error alarm is detected if e The sample has been pre programmed e An associated In spec page has been designated during Sample editing eA Spec Mini and a Spec Maxi have been entered for the flash point result during Specification pages editing of the associated In spec page There are no specifications for the fire point results Refer to the section 4 2 Test parameters page II 62 6 1 4 End of flash test Signals normal flash point detection when the Fire Point has not been requested 6 1 5 End of test flash and fire For tests for which the Fire Point has been requested this alarm signals the normal Fire Point detection after Flash Point detection If the Flash Point is detected normally in such a test but the Fire Point is not detected then the test will be stopped by an End of test fire safety temperature alarm DOCV207A001 F FP92 5G2 User and Maintenance Manual Page A 117 DL FP92 5G2 6 1 6 End of test no flash e GO NO GO must be programmed Y in the FINAL PHASE of the test program refer to the section 4 2 Test pa
111. mode is signaled by a slow flashing of the green LED on the Analyzer front panel By pressing any key the screen display is reactivated e Select Language 0 to configure the language choice at the Analyzer power on the value 0 allows the operator to choose another value will lock the Analyzer on the chosen language 6 4 2 Safety parameters e Select Safety parameters in the RUN DEFAULT VALUES submenu e Select Heating power upper limit and then enter the value as a percentage of the maximum power 550W Values allowed 1 100 e Select the Upper limit maximum time This is the maximum duration in seconds for the previous parameter i e the maximum time at the maxi entered e Select Alarm if heating rate diff gt 100 from 10 to 150 This parameter determines the admissible difference between the programmed heating rate and the observed heating rate e Select Stop if heat rate alarm amp tmp gt EFP N Y N e Select Probe missing safety from 1 min to 15 min This parameter determines the duration after the test starting from which the heating rate of the sample is verified It is factory set to 4 min that is convenient for most of tested products If this duration is modified to start a test with a warmed sample gt 100 C enter again the It could be dangerous to increase the duration before the heating rate verifying factory set value after the test is completed DOCV207A001 F FP92 5G2
112. n An intermittent audio alarm is triggered and the warning number can be displayed by pressing ALARM STOP The list of warning numbers is given in the Alarms Appendix see in Appendix A section 2 page 112 DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 1 27 ae DL FP92 5G2 4 2 Passwords There are 3 access levels level 1 and level 2 require passwords Level 0 O level for laboratory Operator Data information and basic functions are accessible without entering a password Level 1 M level for laboratory Manager Data information and functions concerning the calibration report quality and operator configuration accessible in access level 1 Level 2 S level for Service Data information service functions and technical configuration of the Analyzer accessible in access level 2 Level 3 ISL only access level The selection of access levels is treated in the Access levels and passwords The Access menu Part II Once an access level has been confirmed by entering the correct password it remains available until the system is explicitly requested to return to an inferior access level On switching on the Analyzer access level 0 is selected by default Page 1 28 FP92 5G2 User and Maintenance Manual DOCV207A001 F Specifications installation and switching on DL 5 Specifications installation and switching on 5 1 Technical specifications Physical Dimensions and Weight Single post With
113. n or End of full mode run Page I 48 FP92 5G2 User and Maintenance Manual DOCV207A001 F Flash point test 2 6 C EFP 50 0 C App 10 FLASH 27 6 Spec In spec Status Idle lt Flame test gt lt Exit gt 17 04 2000 17 31 0 1A Screen 9 End of test screen 8 5 1 Flash on first flame test If a flash point is detected on the first application of the igniter when the test is not programmed GO NO GO see the chapter 4 Run environment definition the Runs environment menu section 4 1 The ISL FP92 5G2 test principle page II 62 an alarm is triggered and the test is stopped On displaying the origin of the alarm the operator will know that a Flash on first flame test has been detected In this way the operator may repeat the test with a fresh specimen of the sample using the erroneous flash point temperature as the EFP The first application for the repeated test will thus be 17 C 30 F below the erroneous flash point 8 5 2 Detection before the standard phase If the flash point is detected before the standard phase the current test is stopped and the abnormal flash test detection alarm is triggered 8 6 Cleaning the test set CE The recommended safe handling temperature is below 55 C 130 F 1 Select lt Damper gt in the current test run screen to drive back the damper to its place 2 Carefully remove the cup and its contents 3 Clean the cup the flash detection prob
114. nd Maintenance Manual FP92 5G2 Values indicated are given for printers supplied by ISL For other printers refer to the DOCV207A001 F DL Configuration Analyzer setup menu 6 2 External link setup 6 2 1 RS 232C link setup The access to the external link setup is possible with the access level 1 e Select Analyzer setup in the main menu e Select Ext link setup in the ANALYZER SETUP menu e Select RS 232 link setup to display the submenu of the same name RS 232 LINK SETUP Transmitted data Hardware setup Software setup Data flow control Computer on line N lt Exit gt Screen 38 The ALAN RS 232C adapter must be connected to allow the access to the RS 232 LINK Se SETUP menu refer to the section 5 3 5 2 page I 34 Referral Refer to the Appendix B page 121 for the RS 232C link characteristics the description of the communication protocol and the content of the messages sent LU The different commands displayed in this way are treated in the following sections 6 2 1 1 Transmitted data e Select Transmitted data of the RS 232 LINK SETUP menu The display becomes RS 232 TRANSMITTED DATA Conditions of run N Test contents N lt Exit gt Screen 39 All the selections are in Flip flop mode and the possibilities are Y N yes or no DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 11 79 DL FP92 5G2 As well as the result message th
115. not use samples from leaky containers or from plastic containers having walls that are porous for volatile material and eliminate any air bubbles or foam collected on the surface of the specimen so as to avoid erroneous flash points Samples containing dissolved or free water may be dehydrated with calcium chloride or by filtering with qualitative filter paper or with a loose plug of dry cotton ASTM D92 standard Solid or viscous samples bitumen asphalt which must be heated until they are fluid enough for testing should not be heated to a temperature exceeding 56 C 100 F below the EFP U For other sampling practices see the relevant standard method DE AE 8 1 2 Preparation The operator should be familiar with the dangers associated with Flash Point tests AN Some of these dangers are indicated in the standard methods Dispose of solvents and waste material in accordance with local regulations Detection of the presence of the test flame is by ionization detection The automatic CS relighting of the test flame is performed by a low voltage heating resistor e Tests should be performed in a draught free location If the Analyzer is equipped with the anti draught shield accessory put it in place before starting the test Particular care must be taken during the last 17 C 30 F rise in temperature prior to the flash point so as to avoid disturbance of the vapors in the test cup by careless movements or breathing near the cup e
116. nterface Function keys STOP Alarm stop stop printing and Reset keys Running test and standby green LED and alarm red LED Numerical pad Arrow keys Brightness adjusting knob Contrast adjusting knob Figure l 9 Analyzer interface 6 1 Keypad The universal type keypad no particular language has been kept simple It has no alphabetic keys and no double function keys It includes It includes a AN UY Numerical keys Backspace DELETE Deleting characters Point Dash ooje Function keys RESET Abandons all data entry or quits sample creation display page creation display and program creation display PRINT STOP Stops printing ALARM STOP Displays the triggered alarm The audio alarm can be stopped except for fire detection in this display STOP Abandons test running started using RUN START No effect on character entry ILE CENT D ENT Confirmation of entry a letter text collectively a value DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 1 37 iSL FP92 5G2 Two built in indicators Test green led continuous Test running intermittent Screen in standby mode Alarm red led fault error or report alarms continuous audio alarm Selection keys on either side of the LCD screen lt gt C gt _ Direct on screen selection of the displayed menus Arrow keys UP DOWN LEFT RIGHT arrow keys selection of let
117. ol parameters are configured N e Select the 4th parameter key and enter the value in seconds see Screen 42 above The time between each message will be as configured It is not possible to request a second transmission of any message DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 11 81 DL FP92 5G2 b Transmission with protocol If a communication protocol parameter is configured Y for yes then a dialogue protocol will be necessary between the analyzer and the external computer e The Analyzer must be authorized to transfer results e It is the external computer that controls the message transfer rate The operator can choose from 3 types of protocols Hardware flow control Refer to the RS 232C appendix hardware characteristics of the link Software flow control If the Software Flow Control protocol is used then transmission is started automatically by default on switching on and continues until the analyzer receives the XOFF code which instructs it to stop sending data The analyzer will only resume sending data when it has received the XON code The values of the character codes are 11H for XON and 13H for XOFF c ENO ACK protocol All messages from the analyzer must be acknowledged by the external computer transmission confirmed as security precaution 6 2 1 5 Computer on line For the external link to be operational the Computer on line parameter of the RS 232 LINK SETUP menu must be set at Y U
118. onnected on the igniter arm Gas supply is controlled by a solenoid valve and the operator may adjust the test flame by means of a valve screw knob on the Analyzer front side Figure l 3 page 1 25 At test start the system will attempt to light the test flame during 10 minutes If after this delay it is still not lit the test is stopped During testing if the test flame is absent for 1 minutes or if itis absent at the moment of test flame presentation the test is stopped e Gas used Propane or Butane e Inlet pressure 40 mbar maxi e Inlet operating pressure Butane 28 mbar e Inlet operating pressure Propane 37 mbar e The gas solenoid valve and the gas flame igniter can be manually commanded for diagnostics The igniter arm can also be commanded by lt Control gt of the RUN START screen Use the Flame test command Page 1 24 FP92 5G2 User and Maintenance Manual DOCV207A001 F Presentation of the FP92 5G2 DL 3 2 2 2 Adjusting the test flame Two knobs in the Analyzer front panel enable the test flame of the test arm and the pilot light to be adjusted Test flame adjusting knob Pilot light adjusting knob FP93 5G Figure 1 3 Test flame and pilot light adjusting knobs 3 2 3 The flash detector The flash detector is mounted on the same arm as the temperature probe It is connected directly on the Igniter board It is automatically positioned at the beginning of the test On flash point detection
119. ontact the ISL Service Department 5 2 13 Check test device positioning Checked continuously This failure is signaled by the motor board when the test arm is stuck or unable to move If this failure is signaled the system prevents the test starting or stops the current test 5 2 14 SC6 Motor board link failure This failure is tested for permanently If it is signaled a test run cannot be started but a run in progress is not stopped It is signaled when there is a dialogue problem between the central unit board microprocessor and the SC6 motor microcontroller Switch off the Analyzer and then on again Have connections checked If the failure still exists contact the ISL Service Department DOCV207A001 F FP92 5G2 User and Maintenance Manual Page A 115 DL FP92 5G2 5 2 15 SC6 Motor failure This failure is tested for permanently If it is signaled a test run cannot be started but a run in progress will not be stopped It is signaled when a fault is detected for example a mechanical gag on the sample changer connected Have connections checked Check there is no mechanical gag between parts Check there is a cup and control the four optical detectors of cup position 5 2 16 Heating failure This failure is tested for during test running If it is signaled the test run is stopped It is signaled if the heating power upper limit has been active for a duration above that set for the safety parameter UPPER LIMIT
120. or a given access level Preparing exiting the full mode run Displaying printing and transferring the last test result Initializing the printer Service printings Internal parameters Statistics Displaying printing and transferring a result Displaying the result pages allocation Pages cleanup FP92 5G2 User and Maintenance Manual Page 11 55 ae DL FP92 5G2 3 Calibration the Quality menu To ensure the reliability of the test results it is possible to quickly verify the measures of the Analyzer refer to the relevant section of Part I Those checks must be done at regular time intervals If a calibration is needed a PS 400 Probe simulator is necessary To achieve those operations follow the instructions of following sections First select Quality in the main menu The following display appears QUALITY Temperature measurement calibration Next calibration date JJ MM AA Probe correction table Atmospheric pressure calibration KExit gt Screen 11 cE Calibrations cannot be performed during test running Page II 56 FP92 5G2 User and Maintenance Manual DOCV207A001 F ay Calibration the Quality menu DL 3 1 Sample temperature measurement calibration e Select Sample probe calibration in the Quality display TEMPERATURE MEASUREMENT Temperature measure calibration Calibration frequency 30 days Next calibration date JJ MM AA Start test refusal N lt Exit
121. or board link failure 115 5 2 13 Check test device positioning 115 5 2 14 SC6 Motor board link failure 115 5 2 15 SC6 Motor failure 116 5 2 16 Heating failure 116 5 2 17 Low battery 116 5 2 18 Test flame abnormally lit 116 5 2 19 Test start refused on SC6 Sample Changer connected 116 5 2 20 No cup detected on SC6 Sample Changer 116 5 2 21 Check probe position 117 O72 RODOFEGIGLINS Rs ot ARIA a E El eee Al no eas el eo ee eda A ata 117 6 1 Report alarms summery 117 6 1 1 Pre safety temperature reached flash and fire 117 6 1 2 Flash on first flame test 117 6 1 3 Result out of spec 117 6 1 4 End of flash test 117 6 1 5 End of test flash and fire 117 6 1 6 End of test no flash 118 6 1 7 End of test flash safety temperature 118 6 1 8 End of test fire safety temperature 118 6 1 9 Sample changer stop after cup or anomalies alarm 118 Warning ald MS sers mana rer entente ne enr tente Cdt talent dre tete 119 APPENDIX B RS232 LINK FEATURE G scscsssssscesccssscesccesssscesccesssscesccesssssesceessseceescessscessceessessesceeeess 121 J dnterface features inde rene RS RP IA eh rte RES See tay Sense AR ENA A cai 123 D Oiitlet Conn ctor broaching resserre ddr taie et ee one E eee le dd eu 123 3 Communication PLOLOCOIS serment rire ee et arr ne edit te aride entire 124 4 2 ENO JACK protocol d tails issu dense dant elas ae sheet ddl eh Sandee vole ns reset de 125 Ste LFANSMIER ALAS cies E
122. other side an RS 232C connector to be connected to the PC Note The ISL analyzers allow transmitting data according to specific customized criteria Ee and a user defined protocol The RS 232C communication interface has to be parameterized Refer to the section 6 2 page II 79 5 3 5 3 The SERVICE port The FP92 5G2 has a serial SERVICE port as a standard fitting with which with the help of the ISL UDS service software supplied software updates can be downloaded via a PC and the contents of the memory such as the internal parameters and results can be saved for subsequent reloading refer to the section 6 3 4 page II 84 for transfer commands 5 4 Handling precautions for LCD devices LCDs Easily scratched The LCD is easily scratched If rubbed by hard objects the LCD may be damaged Handle the LCD with care so as not to scratch it Moisture Water Electricity fed to an LCD with moisture on its surface may damage it Gently wipe off any moisture or let it dry before using the LCD Dirt The LCD can be stained by fingerprints saliva starch oil and fat If it is stained gently wipe it with a soft cloth High temperature and humidity The LCD dislikes high temperature and high humidity Ensure that the storage and operating temperatures indicated in the 5 1 Technical specifications page I 29 of the current part Vacuum Cleaners If the work room is cleaned using a vacuum cleaner keep it away from the LC
123. own gt key DOCV207A001 F STANDARD PHASE Heating rate Standard Test every 2 0 C if EFP lt 110 0 C Test every 2 0 C if EFP gt 110 0 C Start of test at EFP XX C if EFP lt 110 C Start of test at EFP XX C if EFP gt 110 C lt Up gt lt Down gt Screen 24 FP92 5G2 User and Maintenance Manual Page II 63 DL FP92 5G2 e Press the lt Down gt key FINAL PHASE lt Up gt Go No Go N Pre safety at TP XX C Flash safety at EFP YY C Fire safety at EFP 22 C lt Cancel gt Screen 25 As can be seen on displaying this pre programmed test a test program can be divided into 4 parts corresponding with the 4 displays above Except for the fast phase all program parameters must be entered during test program creation 4 2 1 Identification and definition parameters Test Name It is used for identification purposes A maximum of 12 characters alphanumeric may be used Temperature Unit The temperature is selected depending on whether the operator wishes to use C or F Selection during test creation Flip flop Preheating time A preliminary heating phase is possible for solid or viscous samples bitumen asphalt which must be heated until they are fluid enough for testing N B The temperature during preheating should not exceed 56 C 100 F below the expected flash point 0 disables the preheating If preheating is necessary the oper
124. pe that you continue to call on us for all of your laboratory s petroleum testing needs Before you begin we ask you to take a few minutes to become acquainted with ISL and its history ISL s beginnings go back to 1975 when a group of engineers and scientists from the heart of the Northern France s petrochemical industry began seeking ways to automate petroleum testing The neighboring industry served as an excellent research and development proving ground for their new equipment By the end of 70 s several quality instruments had been developed and were being marketed in Europe under ATPEM Trademark The most famous of these new instruments was the CPP 97 Automatic Cloud and Pour Point Analyzer Introduced in the early 1980 s its successor the CPP97 6 revolutionized cold flow testing enabling up to six tests automatically and simultaneously Adding new automatic instruments each year ATPEM soon became a worldwide leader in automatic petroleum test instrumentation In 1986 they expanded operations reorganizing into the company now knows as ISL Striving to maintain close contact with customers in over 75 countries ISL has since grown founded sales amp service branches on each continent With design marketing service and support operating together under the ISL roof the company reached a new dimension in 1993 by obtaining ISO 9002 certification from the BVQI Working hard to extend our quality assurance programme we receive
125. rameters page II 62 In this case if the flash point is not detected at the unique presentation of the ignition source allowed this error alarm is triggered The test run is terminated 6 1 7 End of test flash safety temperature eA Flash safety at efp is programmed in the Final phase of the test program refer to the section 4 2 Test parameters page II 62 An alarm is triggered on reaching this temperature It is entered as a temperature value above EFP EFP T C F 6 1 8 End of test fire safety temperature eA Fire safety at EFP is programmed in the Final phase of the test program refer to the section 4 2 Test parameters page II 62 An alarm is triggered on reaching this temperature It is entered as a temperature value above EFP EFP T C F If the Fire EFP is modified during the test this parameter will be correspondingly modified ee 6 1 9 Sample changer stop after cup or anomalies alarm When using the Sample Changer if the parameter SC6 in standby after anomalies is set at Y any one of a number of alarms switches the Sample Changer to standby once the test in progress stops These alarms are e Flash safety temperature reached e Fire safety temperature reached e Flash on first flame test e Result out of spec e Abnormal flash detection e This alarm is also signaled if the cup test is programmed to Stop after run The SC6 switches to standby They are both signale
126. s parameter is set at Y then a test cannot be started unless sample probe calibration is performed within the period defined for Calibration frequency DOCV207A001 F FP92 5G2 User and Maintenance Manual Page II 59 ae DL FP92 5G2 3 3 Probe correction table e Select Quality in the main menu and then select Probe correction table PROBE CORRECTION TABLE Title Temp unit T Correction Reference Probe value Please respect temperature unit lt Edit table gt KExit gt Screen 18 Note the reminder on the display indicating that the probe correction is calculated by ce Reference Thermometer Reading Sample Temperature Probe Reading e Select Title and enter a title for identification purposes If the temperature unit needs to be modified use the Temp unit flip flop key to select the correct unit e Select lt Edit Table gt There are 21 probe correction values between 0 C 32 F and 400 C 752 F inclusive in steps of 20 C 36 F They are displayed on 2 pages press the lt Down gt key for the second page The corrections can be positive or negative Negative ones must be signed All can be entered to the nearest 0 1 of a degree A linear correction will be made for values falling between the 21 correction values For example e Probe correction at 80 C 0 1 C e Probe correction at 100 C 0 e Probe correction at 120 C 0 2 C At
127. safety parameter is entered by the system Its value differs from the fire safety parameter by the same value as the flash pre safety temperature differs from the flash safety temperature All the safety temperature parameter values can be displayed in full mode once the EFP has been entered To do so select lt Down gt to activate the TEST DETAILS screen Flash Safety Alarm at EFP An alarm can be set which will trigger an intermittent audio alarm and switch the system to standby at a given temperature above EFP pre safety to EFP 50 C 90 F See in Part chapter 4 Analyzer system safeties page l 27 of the manual for the actions triggered on switching to standby The red fault alarm indicator is illuminated Fire Safety Alarm at EFP An alarm can be set which will trigger an intermittent audio alarm and switch the system to standby at a given temperature above EFP flash safety to EFP 100 C 180 F See in Part chapter 4 Analyzer system safeties page l 27 for the actions triggered on switching to standby The red fault alarm indicator is illuminated 4 3 Customizing a test entering parameters Creating a new program needs the level 1access password e Select Runs environment in the Main Menu e Select the submenu Customize a test The display becomes CUSTOMIZE A TEST Selected test 1 Show tests list New one lt Edit selected test gt lt Exit gt Screen 26 For a test runn
128. se the Flip flop selection key to set the parameter 6 2 2 RS 485 link setup connection to the Alan network e Select PC LINK SETUP Analyzer PC ID ISL FP92 5G2 Analyzer network address 1 PC on line Y Interface status 0 0 correct KExit gt lt Init gt Screen 43 e Select Analyzer network address keyboard the analyzer identifying number on the network then press the Exit key Page II 82 FP92 5G2 User and Maintenance Manual DOCV207A001 F DL Configuration Analyzer setup menu 6 3 Service service parameters This chapter deals with service parameter configuration and service parameter functions that are specific to access level 2 Service level Operator and Laboratory Manager configuration access level 0 and 1 is treated in chapter 6 The Analyzer interface section 6 4 Run default values page II 87 If access is denied to a function the system indicates the access level necessary One of the first service operations should be to print out the Service Parameters list Ce See the section 5 3 1 page 11 76 e Select Analyzer setup of the main menu to display the ANALYZER SETUP menu e Select the Technical setup submenu TECHNICAL SETUP Service password PPPPP Regulation parameters Buzzer pulse width WWW Sample temperature calibration values Upload Download lt Exit gt Screen 44 The service parameters are stored in non volatile memory They def
129. splay indicates the type of transfer expected cE The reset referred to will be performed automatically at the end of the transfer DOCV207A001 F FP92 5G2 User and Maintenance Manual Page II 85 DL FP92 5G2 On the PC e Start the transfer program on the PC as explained in the read me file e Enter the communications serial port as requested 1 or 2 Confirm by ENT Analyzer Program and Texts Software Downloading e Type in the name and extension of the information file named ISL FP92 Vxx xx being the software version and confirm by ENT Service Parameters Uploading Downloading e Input the file name requested and press ENT to confirm the name and extension must be given A The PC screen informs the operator of the function in progress On the Analyzer The Analyzer screen informs the operator of the function in progress During uploading of service parameters to the PC do not use the original filename A name containing the date could be used for example SPDDMMYY NVM End of transfer If transfer has been completed successfully e The Analyzer is reset automatically 6 3 4 4 Unsuccessful transfer to Analyzer or no display on switching on If the transfer which has begun has not been successful the Analyzer should restart the process Also if there is no display on switching on this method may also be used and a transfer requirement should be signaled on the PC For this e Switch off th
130. splay the desired value Press the ENT key to confirm the value 6 5 Flip flop entries This is the simplest form of parameter setting It is used in all cases where a limited number of choices are possible Examples include Y N C F The operator need only press the key until the desired parameter is displayed DOCV207A001 F FP92 5G2 User and Maintenance Manual Page I 39 ae DL FP92 5G2 7 Measurements checks To ensure that the FP92 5G2 results are reliable the operator may quickly check the various readings These readings should be checked at regular intervals in conformity with the quality assurance needs of the customer 7 1 Temperature measurement For this operation the operator needs an ISL probe simulator PS 400 The Analyzer should not be in running mode 1 Disconnect the temperature probe from its connector see Figure l 4 page I 31 and connect the ISL PS 400 in its place 2 From the run test screen see Screen 2 page 1 36 select lt Display gt 3 Set the PS 400 rotary switch on 0 C 32 F 4 Once the temperature display has stabilized make sure that the temperature reading is 0 C 32 F 5 Now position the PS 400 rotary switch on 400 C 752 F and once the reading on the display has stabilized make sure that it is 400 C 752 F If calibration is necessary consult the chapter 3 Calibration the Quality menu page II 56 The sample probe calibration frequency can be programm
131. sult page ll 93 and chapter 11 Results and printing the Results memory menu page II 96 6 3 4 Upload Download A PC program is provided with the standard FP92 5G2 Analyzer for uploading and downloading of the Service parameters to and from a host computer using the Service port It is also possible to upgrade the Analyzer program and texts software in the same way In the latter case an upgrading diskette is used An external link cable is provided for connection to the PC Modem signals are not provided during downloading If necessary transfer by modem should be carried out in 2 steps 1 Transfer between 2 PCs by modem 2 Local transfer between PC and Analyzer without modem signals The transfer mode Uploading Downloading is a specific Analyzer mode The Analyzer switches to this mode e Either by automatic detection of a transfer requirement signaled on the PC screen e Or on request by the operator from the Analyzer keypad In the former case the Analyzer cannot leave transfer mode until it has succeeded in linking with the host PC Page II 84 FP92 5G2 User and Maintenance Manual DOCV207A001 F DL Configuration Analyzer setup menu In the latter case it is best not to try to quit the transfer mode If the downloading process has begun then some of the memory has probably been deleted If an error has been made the best method is to let the transfer continue its course and start the transfer over ag
132. t menu section 4 5 Samples edition and display page Il 70 4 6 Specification pages editing and display page 11 71 4 7 Operators name edition and display page ll 72 The user can create customized tests responding special needs Refer to the chapter 4 Run environment definition the Runs environment menu section 4 3 Customizing a test entering parameters page II 67 and section 4 4 Modification of an already existing test page Il 70 The user can otherwise enter the Full Mode Run This mode gives the opportunity of editing or creating a customized test by proceeding with an experimental approach i e test sessions followed if necessary by fine adjustments The resulting program can be saved and called back for subsequent tests Refer to the chapter 8 Full mode run the Full mode run menu page II 91 The functional flexibility of the FP92 5G2 Analyzer offers many tests procedures the user has to choose the one which corresponds to his needs The on part of this manual allows for this purpose an exhaustive Analyzer setup information Page l 42 FP92 5G2 User and Maintenance Manual DOCV207A001 F Flash point test 8 2 2 Test starting Select lt Run menu gt from initial screen see Screen 3 pagel 36 Sample ID Sample No EFP C Fire point N Test 1 C Operator lt Exit gt Cup under test lt Cups data gt Next No Previous EFP lt RUN START G gt lt Control gt lt D
133. t compatible with the heating rate 2 Flash safety alarm temperature too high 4 Flash pre safety alarm temperature too high 8 Fast heating phase too long would result in an incorrect heating rate during igniter presentation of the standard phase 16 Fire safety alarm temperature too high Tableau 2 Warning numbers DOCV207A001 F FP92 5G2 User and Maintenance Manual Page A 119 z FP92 5G2 Page intentionally blank Page A 120 FP92 5G2 User and Maintenance Manual DOCV207A001 F Appendix B RS232 Link features z FP92 5G2 Page intentionally blank Appendix B 122 Manuel d utilisation FP92 5G2 DOCV207A001 F DL Interface features In this document analyzer is used for the ISL FP92 5G2 while host computer designates the computer to which the ISL FP92 5G2 is connected 1 Interface features EIA RS 232C serial link Rate 300 to 19200 BPS Data bits 7 8 Stop bits 1 2 Parity none odd even Switchable on line off line state Pre defined message transmission available for test Possibility to define an identifier number for the analyzer Possibility to activate result auto validation Automatic detection of the RS 232C interface cable adapter 2 Outlet connector broaching The RS 232C connector of the adapter is a 9 pin connector The pin configuration is as shown below TxD RxD SIGNAL 2 _ OND ee 5 E 9 a 7 6 EIA RS 232C interfa
134. t entailing rotation of the previous test cup outside of the damper zone is programmed or requested within this time limit then the sample changer will wait the end of the time limit before rotating If he wishes the operator can manually rotate the SC6 using the photosensor push button at any time e SC6 in standby after anomalies lf this parameter is set at Y any of a number of alarms switches the Sample Changer to standby once the test in progress stops These report alarms are amp Flash safety temperature reached amp Fire safety temperature reached amp Flash on first flame test amp Result out of spec Abnormal flash detection These alarms are signaled by the error alarm Stop after cup or anomalies If the Stop after run parameter is set at Yes the Stop after cup or anomalies alarm is signaled once the test stops and the SC6 switches to standby To continue the tests on another programmed cup the SC6 should be rotated manually using the photosensor push button DOCV207A001 F FP92 5G2 User and Maintenance Manual Page II 89 ae DL FP92 5G2 7 Access levels and passwords the Access menu The menus and the functions have been sorted according to access levels The first level level 0 is accessible to all operators The other levels levels 1 and 2 are only accessible after entering the corresponding password If the operator tries to use a function in an access level for which the pass
135. taining the service parameters configuration and an upload download PC programme is provided with the standard FP92 5G2 Analyzer Please refer to the chapter 6 Configuration Analyzer setup menu page Il 78 Note So as to have an updated version of the service parameters configuration the Ee maintenance schedule of the Analyzer should include uploading of the service parameters When uploading the service parameters configuration do not use the same file name as the file on the diskette delivered with the Analyzer 5 2 4 No test flame gas igniter This failure is tested for when gas test flame ignition kit is being used and therefore connected At test start the system tests for the presence of the test flame If the flame is not present the system tries to light it for a maximum of 10 minutes If the flame is still not present this alarm is triggered During the test in the case of an unexpected loss of test flame the system tries to relight the test flame for 1 minute After that duration if a test flame is not detected the system stops the test and the system goes into standby Check the connection and position of the flame detection ignition device 5 2 5 Glow plug current failure gas igniter The glow plug is first used to light the test flame and the pilot light at the beginning of the test During applications the igniter arm returns from over the cup with the test flame extinguished The glow plug lights syste
136. tart refused on changer alarm is disabled e Time under the damper for the previous cup is correct Assuming that these conditions are fulfilled and a test cup has been programmed for the sample changer further cup entry is disabled and the usual test start checks are performed If as a result of these checks a test run cannot be started then the Test start refused on SC6 alarm is signaled This alarm may be due to a number of reasons The operator must check for the exact origin of the alarm It may be due to e A failure signaled e No EFP entered e Incoherent test program parameters e A program checksum error e The calibration date having passed If on pressing the ALARM STOP key no other alarm is displayed the operator can carry out rapid diagnostics by trying a single post test start using RUN START 5 2 20 No cup detected on SC6 Sample Changer This alarm is triggered when a cup in programmed and no cup is detected during the Sample Changer rotation Page A 116 FP92 5G2 User and Maintenance Manual DOCV207A001 F 2 Report alarms DOL 5 2 21 Check probe position At test start the analyzer waits for the measurement to be stabilized about 1 min then the heating is switched on After a predefined duration programmable with a level 2 access refer to the section 6 4 2 page Il 87 parameter Probe missing safety the system verifies the probe presence by verifying that the heating rate of the sample is
137. ter see LCD handling precautions further on Page 1 30 FP92 5G2 User and Maintenance Manual DOCV207A001 F z Specifications installation and switching on 5 3 Connections Adjustment of the flash point detection threshold for the ring shaped electrode of ionization Red LED Heating control Red LED Temperature probe connector Flash point detection Green LED Test flame detection Glow plug connector Green LED Non used oS j Figure l 4 Connection panel connectors ALAN network Inlet Outlet ports Service port Printer port Logic board Ventilator General fuses Gas supply nozzle Analyzer ON OFF switch Heating block cooler Power supply plug Figure l 5 Analyzer rear view 5 3 1 Gas supply connection e Connect the gas supply to the adapter hose nipple N at the rear of the Analyzer see Figure l 5 above 5 3 2 Connecting the relight glow plug e Connect if necessary the relight glow plug to the connection panel see Figure l 4 above DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 1 31 iSL FP92 5G2 5 3 3 Assembling the flash point detector and the temperature probe e Assemble the flash point detector over the test arm like it s indicated in Figure l 7 below and tighten it with the knurled screw e Assemble the sample temperature probe over the test arm like it s indicated in Figure l 8 below and tighten it with the knurled screw e Connect t
138. ternal parameters management the ISL Alan software allows transmitting results directly to a LIMS or ever information system Note The Alan Kit is optional hardware and software package Refer to the Alan Installation and Getting Started Manual Each analyzer connects to the Alan network via the RS485 serial interface through two ports input output located on the rear panel see Figure l 5 page I 31 Example of an ISL analyzers network Converter RS232 RS485 FP92 5G 5G2 and FP93 5G 5G2 AD86 5G and AD86 5G2 PMD100 and ii PMD110 FZP 5G 5Gs and FZP 5G2s FPP 5G 5Gs FP170 5G 5G2 Note The RS485 communication interface has to be parameterized Refer to the section 6 2 2 RS 485 link setup connection to the Alan network page Il 82 DOCV207A001 F FP92 5G2 User and Maintenance Manual Page 1 33 DL FP92 5G2 5 3 5 2 RS 232C serial link The network input output ports of the analyzer link interface with the Alan network may be connected via a special adapter supplied with the analyzer to form an RS 232C serial link enabling results to be collected on a PC and for transmission to a LIMS refer to the Appendix B page 121 for the meaning of the messages Use the adapter supplied with the analyzer see the Packing List it has two RS485 connectors on one side which have to be connected simultaneously to the analyzer s Alan input and output ports and on the
139. ters of alphabet in A 7 editor mode UP DOWN Also used for incrementation decrementation of digits during Aw numeric entry LEFT RIGHT Also used for selection of digit position during numeric entry The keypad is rendered watertight by a polyester film Text entries sample ID operator are selected from the display When an entry requires text the alphabet and 6 other characters are displayed Text is then edited as explained in section 6 3 Text editing page I 39 of the current part 6 2 Display The keypad has a built in LCD graphic screen In that way the displayed functions can be directly selected using the function keys on either side of the screen see Figure l 9 page I 37 and Screen 4 above Le In this manual select means pressing the relevant key of the indicated function C gt Sample ID D Sample No CP EFP D Fire point N P Test gt Operator CP lt Exit gt Tmp TTT T Cup under test lt Cups data gt Next No Previous EFP lt RUN START G gt lt Control gt lt Display gt lt Down gt App 0 HHOHOOE Screen 4 The example of the run test screen Page 1 38 FP92 5G2 User and Maintenance Manual DOCV207A001 F 2 The Analyzer interface DL 6 3 Text editing e Select the line directly on the screen for example Sample ID followed by lt Other gt The alphabet is displayed e Use the arrow keys LEFT RIGHT UP DOWN to select the letter or c
140. th modified current test program or another program I 92 8 3 Exiting Full mode 11 92 9 Result of the last test run the Last run result inner 11 93 9 1 Displaying the last run result 11 93 9 2 External link transmission validation 11 93 10 Printings th Printing Menuisier drrtirne nn de E AN EE EEEE NARE EAA E sd 11 94 10 1 Printer reset 11 94 10 2 Environment printing I 94 10 2 1 One sample contents 11 94 10 2 2 One spec page contents IL 95 10 2 3 One test contents 11 95 10 3 Printer link test I 95 11 Results and printing the Results memory menu ses 11 96 11 1 Results pages 11 96 11 2 Statistics 11 97 11 3 Results Display Printing and transmitting I 98 11 4 Results pages allocation I 98 11 5 Page cleanup I 99 11 5 1 One page contents cleanup 11 99 11 5 2 Delete page name and contents II 99 PART III FP92 5G2 MAINTENANCE sscsscssssscvsrcsssesoscssencsssesesssssncssssnersesssesessssssessssnersesessnersesssesosees IH 101 TL GEnera l tras AR RS iene ed RE Ben dein Ne de LR nd Le LS RS Nee telah eine 111 103 2 External operations aeaii ni Batak Asia anesaih dieses Ain der Me ne ate sees 111 104 2 1 Replacing the sample temperature probe III 104 2 2 Replacing the flash point detector III 104 2 3 Adjusting the flash point detection threshold III 104 3 1nternal Operations sieste nn ce avd babs nee ne tr cbg bat Cis cD Me re M cee eects 11 105 3 1 Analyzer dismantling assembling for maintenance
141. this way when the sample ID is selected the associated test will then be summoned Edition of samples is treated further on 4 2 Test parameters Before using the function Customize a test of Runs Environment for test program creation let us first display a pre programmed test to discover the parameters and information contained in a Test e Select Display a test in the RUNS ENVIRONMENT submenu CUSTOMIZE A TEST Selected test _ Show tests list New one lt Edit selected test gt KExit gt Screen 21 e Select Show tests list and the list of existing tests are displayed 1 to 20 Select one of the pre programmed tests for example T01 D92 C The above display returns The Selected test entry reads 1 Page 11 62 FP92 5G2 User and Maintenance Manual DOCV207A001 F Run environment definition the Runs environment menu L e Now select the lt Edit Selected Test gt function and the display becomes for example CUSTOMIZING A TEST Name D92 C Temperature unit C Preheating time Omin Barometric correction 1 Rounded Yes lt Down gt Screen 22 e Press the lt Down gt key to display the next page FAST PHASE Heating rate Standard Test every 10 0 C if ERP lt 110 0 C Test every 10 0 C if ERP gt 110 0 C Start of test at XX YY C End of fast phase at ERP YY C lt Up gt lt Down gt Screen 23 e Press the lt D
142. tion 4 8 Customizing run mode screen page 11 72 A number of Entry options are available using the function keys on the side of the screen 1 Select Sample ID and then select one of the pre programmed sample names proposed 2 Select Operator and then select one of the pre programmed operator names proposed 3 Select Test and then one of the pre programmed tests proposed 4 Select Sample No Enter the sample number as explained in Entering text and numeric values of this chapter It is possible to use the Next No function so as to increment the sample no used for the previous test 5 Select EFP and enter the Expected Flash Point as explained in the Entering a numeric value section of this chapter Press ENT It is also possible to use the Previous EFP function so as to reselect the EFP for the previous test run If the apparatus has been correctly prepared you are now ready to start a test run A RUN START function is provided for this purpose When the RUN START function is selected the following 2 6 C EFP C Applications 0 Status Idle lt Flame test gt KExit gt 17 31 lt Damper gt 17 04 2000 Screen 6 Test run screen Page l 44 FP92 5G2 User and Maintenance Manual DOCV207A001 F Flash point test 8 3 Test starting on the Sample Changer The procedure for programming a test on a cup or cups is as follows e Select lt Cups Data gt in the TEST START screen The CUP S
143. ument Pt 100 probe e Range 100 to 400 C 148 to 752 F same probe as the AD86 5G e Correction available in steps of 20 C 36 F e Response time equivalent to ASTM Thermometer for Specification E1 DOCV207A001 F FP92 5G2 User and Maintenance Manual Page I 29 DL FP92 5G2 LCD Monochrome Graphic Display e Backlight Cold cathode fluorescent e Resolution 320 240 pixels 15 lines of 40 characters e Viewing area 120 99 mm approx e Pixel size 0 33 0 33 e Contrast and backlight adjustable e Backlight standby mode adjustable Clavier Tactile type keys The screen and keypad are resistant to most chemicals met in the petrochemical industries Autonomy Operated as a stand alone apparatus with standard external link for transmission of results to a host computer 5 2 After unpacking Once the Analyzer has been unpacked it is best to leave it idle in the laboratory for a few hours especially if it has been stored at low temperatures e The recommended laboratory temperature is between 15 and 35 C 59 to 95 F e The Analyzer should be placed on a steady horizontal bench top and preferably in a fume cupboard e In any case the Analyzer location should be draught free with also the possibility of darkening so that if necessary the flash point can be easily observed e Allow a minimum clearance of 100 mm at the rear and sides of the Analyzer e Protect the Analyzer from all projections of wa
144. urn to their housings in the central unit at the end of the test and when the Analyzer switches to safety mode as a result the cup can be handled Not only is the FP92 5G2 simple to use it is also very safe All parts of the Analyzer that may come in contact with the operator are protected from voltages exceeding 24 volts Handles are provided on the cup for safe removal while they are still hot Any malfunctioning will be signaled by an audio alarm the origin can be displayed Certain failures switch the Analyzer to safety state see next chapter for consequences of safety state status The system is equipped with a fire detection system that triggers a continuous alarm The Analyzer switches to safety state disabling commanding of all power consuming units for example cutting off the gas supply The customer may use the safety relay provided to connect his own fire alarm and or extinguishing accessory to the system Page 1 20 FP92 5G2 User and Maintenance Manual DOCV207A001 F ay Presentation of the FP92 5G2 DL The term power consuming devices is used in this manual for electrical and EE electromechanical devices that have their own power supply This term is not used for devices that are purely electronic for example integrated circuits LED s The FP92 5G2 can be equipped with an optional SC6 Sample changer to the right of the testing unit This comprises A six place carousel equipped with heating plates and insu
145. w plug current The date in the format configured on the Analyzer Format of the date Time of the end of the test run Number of characters Manuel d utilisation FP92 5G2 Description C for contents Y N or yes no or not requested 0 or 1 mmHg ou kPa G gas amperes for example JJ MM YY 0 1 2 or 3 JU MM YY MM JJ YY JJ MM YYYY MM JJ YYYY for example HH MM Page appendix B 127 ae DL FP92 5G2 5 4 The test program message The test product message is transmitted in only one message T Example LED S R rd Dang S 0 40 01 0 35 2 2 1 29 Meaning of product message fields from left to right Message T Identification Humber ot Description characters Analyzer number 2 Type of message identifier 2 T for test Program name 12 Barometric correction 1 O or N Rounded 2 0 1 2 None ASTM D92 or ISO NF EN Preheating 2 0 99 min If gt 99 99 is displayed Heating rate fast phase 2 0 1 or 2 high standard or none Test every of fast phase 5 Start test temperature of fast phase 3 Temperature of end of fast phase 3 the real temperature value is sent Heating rate standard phase 2 0 or 1 standard or high Test every of standard phase 5 Start test temperature of standard phase 5 the real temperature value is sent Go No Go 1 Y or N Pre safety alarm Pre safety alarm temperature 3 Pre safety alarm flash point 3 Pre safety alarm fire
146. which the test cup is placed The metal plate is equipped with an extension at the front for the attachable handle The handle supplied has a safety locking catch The positioning tabs on the top of the heating block should be engaged in the holes of the corners of the heating plate e An insulating sheet which covers the metal plate except over the area of plane depression in which the test cup is placed The test cup is placed from the front with its handle to the front of the Analyzer Heating can be controlled through diagnostic mode The connection panel red indicator Figure l 4 page I 31 lights up 3 2 2 The ignition source The igniter is mounted on the igniter arm The system detects the presence of the igniter system and displays G after lt RUN START on the RUN START screen The operator may use the Flame test of the lt Control gt menu to present the igniter arm 3 2 2 1 Test flame and pilot light The Test Flame kit is equipped with a flame detection and ignition device This detection ignition device is connected on the connection panel of the test unit connector and is mounted on its holder on the connection panel see Figure l 4 page I 31 When a gas flame igniter is installed the igniter arm carries out a to and fro movement over the cup thus returning to the flame detection ignition device position after each igniter application The test flame is extinguished during the return voyage The gas inlet tube is c
147. witching the Analyzer to standby Failures presenting a certain risk switch the Analyzer to standby in this case the power consuming units are switched to standby The power supply and the gas alimentation are turned off the power consuming units to standby the operator must switch off the Analyzer and A If the detection of those failures see Alarm list in the Alarm appendix do not switch unplug the power supply 4 1 3 Failures refusing a test start and stopping a test run These failures trigger a continuous audio alarm Press ALARM STOP to display the type of alarm see in Appendix A section 2 page 112 4 1 4 Report alarms e A report alarm signals an abnormal event e g Flash on first flame test during the test or in the results A continuous audio alarm signal is triggered e A report alarm signals a normal event e g End of test flash A discontinuous audio alarm signal is triggered the active pulse of the discontinuous audio alarm can be set see in the chapter 6 Configuration Analyzer setup menu section 6 3 2 Buzzer pulse width page Il 84 In both cases a red indicator on the keypad is illuminated see section 6 1 Keypad page 1 37 When the alarm is acknowledged the indicator is extinguished 4 1 5 Warning alarms for non conformity correction This means that the system has had to correct an abnormality in the test run However the conformity of the run is guaranteed after the correctio
148. word has not been given a message informs him that the PASSWORD WAS NOT GIVEN and access is refused These level are explained in Part chapter 4 Analyzer system safeties section 4 2 Passwords page I 28 7 1 Selection of the access level To check the current access level select lt Access gt in the main menu The following screen in displayed ACCESS CONTROL Current access level is _ 0 Level 1 Lab manager access _ Level 2 Service access _ lt Back to level 0 gt KExit gt Screen 49 e Select the access level required and enter the corresponding password e Confirm by ENT e The Current access level should now indicate the new access level e When the Analyzer is switched on the default access level is 0 7 2 Modifying passwords Factory Set Passwords are the following e The Laboratory password level 1 is 0 Modification of Laboratory password is described in chapter 6 Configuration Analyzer setup menu section 6 5 Laboratory setup page II 88 e The Service password level 2 is 0 Modification of Service password is described in chapter 6 Configuration Analyzer setup menu section 6 3 Service service parameters page II 83 Page II 90 FP92 5G2 User and Maintenance Manual DOCV207A001 F Full mode run the Full mode run menu DL 8 Full mode run the Full mode run menu Select lt Exit gt from initial menu see in Part chapter 5

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