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ORBISPHERE Model 6110 Total Package Analyzer

1. System initialization End application rda Installation Maintenance em Anti loam bag replacement EC sensor maintenance Goretex filter replacement Needle tip and seal replacement This section describes the maintenance options that are available directly from the instrument e Digital input verification e Actuator verification e Analog value monitoring e Global system view e System initialization e End application e Wizards e Sensor services 17 Maintenance 9 8 1 Digital input verification The goal of this menu is to check all devices that provide digital inputs to the instrument microprocessor A black dot in the circle to the right of each option signifies that the specific sensor has been activated Digital impul xerific ation gp Inputs Emergency stop pushed Axis reference position actieated End of trien upper bound activated End of travel lover bound actreated Fret door Closed Prolectech n cover opened Lis Sound error Lowy level of ant foam Foam detection actrated Botte ren detection acinabed 9000090000 e Emergency stop pushed Activated when the emergency stop button is pushed The ultra sound option will also have a black dot as the power supply of the sonotrode is deactivated at the same time e Axis reference position activated The black dot indicates that the piercing device is positioned in the reference home location e End of travel upper bound a
2. Document Number DG6110 C ORBISPHERE Model 6110 Total Package Analyzer USER MANUAL oeptember 2009 Revision A CF LANGE Table of Contents Section 1 General Information Nuria 5 O A N 5 EE Tale tel Le EE 5 V V Ussesi hazala normales E 5 1252 ENEE EE o e A 5 1 2 3 Instrument switches and buttons nenne nennen nnne nnn nn 5 1 24 Precautionary Ee ii tient ia Ro Gee nas data ides ec arte enclave tee a ipaa Du 6 INST CEN OI T D M m 6 1220 Be le Aoi iN ETT T ai 6 1 21 MUSSO RANIA Midas 7 ko Product recycling form ALON EE 7 124 WEE dISDOSS ee 9 1 5 Restriction of hazardous substances RoHS 10 Seclion 2 Specifications ii Ai 11 2 1 Technical SPCCHICATONS E 11 2 2 Model le le d Mee E iios ooi ett a iia 12 2 9 INSTUMENtAIMENSIONS TTE INIT 13 2 4 Main instrument components nennen nne nnne nen snas rna aes ss sse re ssa senis 14 CNN onmi ER PEO ROO TT 14 22 2 NST SIS EE 15 2A Ne ale TEE 16 2 WEE Lee De e 17 SeCHOITS Installall R EE 19 eth MID 6 iso oT T TM TM 19 9 2 MAIN elle el EEN 19 E ROS ne le te tod se ne 20 nn e a 20 99 NS Tee AI mM I ELI MM I M LE 21 9 0 PurgeandTorcng gas SUD EE 21 3 7 Antifoam cartridge preparation and installatiOn ooccconcconcconcconnconcocnncancconnonnnnnnnonnnonnnos 22 3 1 1 Antifoam cartridge preparation EE 22 3 122 Antitoam cartridge Installation 24 3 8 Oxygen sensor preparation and installatiON occcoococccnoco
3. 3 9 Prime the antifoam tubing 1 Anantifoam priming tool is available from the spares kit delivered with the instrument Place this on the ultrasonic base of the instrument using the lasers to center it illustrated below left and lower the plastic front door illustrated below right 2 Activate the motor to lower the instrument head allowing the needle to penetrate approximately to the center of the priming tool illustrated below If using the wizard simply press the Do It key on screen If not using the wizard refer to Manual displacement on page 80 for details on lowering the instrument head 3 Start the antifoam pump to prime the tubes and continue until the white antifoam liquid starts to appear from the needle If using the wizard use the on screen Start and Stop buttons to control this If not using the wizard refer to Antifoam system on page 81 for details and press the Start injection button to control the liquid output 4 Raise the instrument head to its home position Do It key with the wizard or Manual displacement on page 80 otherwise Remove the priming tool and rinse well with water otore with the syringe and antifoam container for next usage 27 Installation 3 10 Run instrument auto check 28 If using the installation wizard an instrument auto check is run automatically on completion of the installation steps If not using the wizard select the System initialization option in the Maintenan
4. 6 Manually raise the piercing device back to its upmost home position Refer to Home position on page 79 if you are unsure how to do this T The antifoam tubing needs to be primed to ensure they are full of the new antifoam For instructions on doing this refer to Prime the antifoam tubing on page 27 73 Maintenance 9 5 Oxygen sensor maintenance Wear on the membrane and chemical reactions within the gas sensor requires that the oxygen sensor be serviced regularly to restore its original sensitivity A clear sign that a sensor maintenance is required is when measurements are noticeably less stable than usual and when a calibration does not improve the situation 74 1 Lower the piercing device to its lowest point it will stop automatically once this point is reached If using the wizard simply press the Do It key on screen If not using the wizard refer to Manual displacement on page 80 for details Remove the plastic front protection door by carefully raising it up on its rollers and over the top of the instrument to give access to the antifoam cartridge location Unscrew the two screws No 1 in the diagram locking the small sensor access panel and remove it to reveal the sensor No 2 in the diagram Disconnect the sensor cable then unscrew the sensor collar and remove both the collar and sensor from its location Once the sensor has been removed it can be easily serviced For full details on servicing
5. Name Solubility Temp normalization Formula 1 5 Name Comment Brimful vol Height Tilt position Package backstop Package type Name TPO2 02 Lig 02 HS CO2 Total CO2 Liq CO2 HS CO2 PT HS Volume Liquid vol D 02 D CO2 Formula 1 5 Name First name ID Password Security level Start time Frequency pattern Configuration This section describes the sequence of actions required to configure the instrument The following configuration options are available from the main screen e Units and resolutions e Package parameters e Instrument parameters e Security and user management e Communication e Sensor configuration 5 2 Units and resolutions 5 2 1 Units Letz and resolu dior configuration Units Resolution Concentration 07 concentration pph CO2 concentration f Length nm EJ Temperature ke D Volume mi K Pressure mbar Cluarncties nia CH This option allows you to assign units to all values displayed by the instrument e For each value listed a rolling list will be displayed giving the units valid for that particular parameter Select the required unit from the list and press Ok to continue When all units have been assigned press Ok on the main screen to save these values and continue 5 2 2 Resolutions 36 Lits anc meselutiane configuration Units resolutions Concentration OF Concentration CU concertrabon Length Temper
6. 1 pressure pressure is too high the input reference gas The measured package height is HExoo2 Unmatched package different from the value defined in neck the Package size 2 the package definition Check the black seal on the piercing unit The measurement pressure is Check the purge gas pressure the Check the purge gas pressure gas pressure W4 Measurement stopped lower than 9 9 bar Check the forcing gas pressure HEX004 The needle pressure is too g gas p 4 low Check the Gore Tex filter Check the airtightness of the gas Gas path not airtight path between the piercing unit and the measurement chamber Check the black seal on the piercing unit Check the airtightness of the gas HEX008 W8 Headspace pressure not leak has been detected path between the piercing unit stable between the cap and the seal and the measurement chamber Check the forcing gas pressure Check the Gore Tex filter the Gore Tex filter W20 Measurement process The pressure in the package is HEX020 incomplete Insufficient initial too low to continue with a package pressure measurement spontaneous degassing is HEX040 din BR Deus detected at the end of the first degassing expansion W80 Measurement process Check foam intrusion in the gas incomplete Insufficient The measured pressure is too path HEX080 low to compute the second phase ackage pressure durin Ee stage i of the measurement Check Gore Tex fi
7. 69 Analysis 8 3 Table settings This options allows you to define up to 10 data elements that the instrument will display for each measurement More data is recorded but only 10 values can be displayed on screen Table Settings Column 1 at Column B oan im Column 2 Column 7 T lig Colmn3 Package narne Column B hg A Coburn Corus Column HR Operator name Column 5 Cr Tatal Gomm 10 e Column 1 10 Define for each column the data to view from the drop down list of available data elements Select Validation to accept and save the selected data elements 70 Section 9 Maintenance 9 1 Maintenance schedule This following table shows the recommended maintenance schedule for an average of 500 package analyses per week This proposed schedule should be modified according to operating conditions Interval Clean front protection door Gore Tex filter replacement There are 4 maintenance wizards available from the maintenance menu that give on screen instructions on the following maintenance subjects These functions are also described in detail in this section of the manual e Antifoam cartridge replacement see Replacing the antifoam cartridge on page 72 e EC sensor maintenance see Oxygen sensor maintenance on page 74 e Gore Tex filter replacement see Gore Tex filter replacement on page 75 e Piercing gasket and tip replacement see Replacing the piercing gasket and tip on page 76 9 2 Instrumen
8. Anb taar lower level Foam detection 4 Press the Start injection button and you should hear the injector working You should hear as many clicks as you have defined for the injection number In addition the liquid should be seen exiting from the tip of the needle 5 On completion of the test raise the instrument head to its home position Remove the priming tool and rinse well with water Store with the syringe and antifoam container for next usage 9 8 3 Analog value monitoring This screen shows all the main analog signals related to the main components of the instrument Select this option to view the analog and actual values for e Temperature e Pressure e CO concentration e Flow e Current e Temperature sensor anio vale monitevirgg Analogue values Temperature value 0 570 Wok 24 TYE SC Pressure value D 3n Vor E 1131 mbar LO concentration HS Dr Vor n DU ar Fira value 0 8 38 val 0 000 mis Current value 15 220 HA p 769 DEn EC sensor lemperabure 0 450 von ET E 82 Maintenance 9 8 4 Global system view This option allows you check various components of the instrument e O2calibration valve e Gas calibration valve e Reference volume valve e Main purge valve e Needle purge valve e On off valves function e Regulating valves function e Ultrasound e Flow regulation e Manual displacement e Proportional valve O2 Calib nz teg B LAA Prop Valve Gas Calb Pr
9. CAUTION When the instrument is ON purge gas must be supplied at all times to avoid damage to the sensors A single user supplied source of CO can be used to supply the main forcing and purge gas by fitting a two way divider supplied to the end of the gas supply tubing Install the gas connections as follows referring to Figure 4 on page 16 for the gas input and output connection placements 1 Insert the forcing gas tubing into Gas Input 1 The recommended input pressure is 5 bar maximum of 7 bar of CO N or compressed air Insert the purge gas tubing into Gas Input 2 The recommended input pressure is 5 bar maximum of 7 bar of CO This pressure should be higher than the package pressure so for some beverages e g soft drinks it may be necessary to increase the input pressure Insert the calibration gas tubing into Gas Input 3 The recommended input pressure is 2 bar maximum of 7 bar of 95 pure CO If required insert a reference pressure controller into Gas Output to control the output pressure level Note To make the instrument operational only the forcing gas and purge gas are mandatory The calibration gas and reference pressure controller are optional 21 Installation 3 Antifoam cartridge preparation and installation An empty 280mL volume antifoam cartridge is delivered as part of the installation kit A recharge bottle of antifoam is part of the package along with the necessary tools to transfe
10. Check that the cover is correctly in place and fixed with screws Check that the position detector is in place in the back of the analyzer STE The emergency stop button is in the activated This can happen during transportation Release the i uud position pushed in button to its normal position by turning it clockwise 10 1 4 Measurement problems Cover is not on the analyzer or is badly Protection Cover positioned Cover detection sensor failure Observation Explanation Negative TPO results CO purge gas is not of the required purity of gt 99 5 The instrument never reaches the threshold value CO purge gas is not of the required purity of gt 99 5 Stop the analysis by pressing the emergency button and remove the bottle Check that the piercing spike is in place and not unscrewed Pull the emergency button to his initial position and restart the The bottle goes up with the piercing head instrument Open the front door to stop the process Remove the bottle and check that the piercing spike is in place and is not unscrewed Close the front door and press the Abort button on the screen 90 Section 11 Spare Parts and Accessories Antifoam cartridge empty for 6110 Power Cord Japanese Plug Total O2 CO2 package analyzer DG6110 MAN F 6110 Manual in French DG6110 MAN J 6110 Manual in Japanese DG6110 SYS Total O2 CO2 package analyzer DGA1100 MAN D A1100 Manual in German DGA1100 MAN E A1100 Manual in Engl
11. Seal to package Thermistor assembly w o ring Solenoid valve 2 2 NC w o ring Power supply cable 6110 instrument user manual A1100 sensor user manual The following must be provided locally by the user Calibration and purge gas for O and CO sensor CO5 4 to 7 bar 58 to 102 psia purity gt 99 5 Forcing gas for piercing device air CO or No 2 to 7 bar 29 to 102 psia purity 99 596 Second calibration gas for CO sensor optional 4 to 7 bar 58 to 102 psia purity 70 19 Installation 3 3 Positioning CAUTION The instrument is heavy 55 kg so extreme care must be taken when handling to avoid damaging the instrument or inflicting personal injury Hach Lange recommends installing the instrument on a sturdy laboratory table that can more than support the 55kg weight Place it on a clean flat surface and convenient to the power source The display screen should be at head height for easy viewing and operation 3 4 Installation steps 20 Important Note The instrument can be easily installed by following the installation wizard embedded in the instrument software This wizard will start automatically once power is connected to the instrument for the first time It is recommended to use this wizard for the first time installation If further information or clarification is required refer to the corresponding installation steps in this manual If not using the wizard you will need to have access to the m
12. 540 x 942 mm 21 1 x 21 3 x 37 1 ins 55 kg 121 Ibs IP20 100 240 VAC 10 50 60 Hz Max 250 VA Purge gas CO with purity gt 99 9 at 4 to 7 bar 58 to 102 psia Forcing gas Air N or CO at 2 to 7 bar 29 to 102 psia Power requirements Power consumption Compliance Low voltage 2006 95 EC EMC 2004 108 EC Electromagnetic compatibility standards EN 61326 2006 IEC UL CSA 61010 1 IEC UL CSA 60825 1 European directives Laser product safety Digital display TFT VGA 640 x 480 color display touch screen with backlight Operating system Windows CE 4 2 Languages English Digital connections 1 x USB client 2 x USB host 1 x Ethernet 1 x RS485 Specifications 2 2 Model identification system The instrument identification number and the instrument serial number are located on the label on the back panel and can be found on order confirmation and invoice papers The different models available are described in the following matrix A Oxygen EC Sensor D Carbon Dioxide TC Sensor T Table 1 100 240 VAC 0 English language sp ajo 6 H Example 6110 AD T1000000 e Total Package Analyzer model 6110 e With an Oxygen EC sensor and a Carbon Dioxide TC sensor e able mounted version e 100 240 VAC e English language software 12 Specifications 2 3 Instrument dimensions Figure 1 Instrument dimensions Specifications 2 4 Main instrument components 2 4 1 Front view Figure 2 Instrument
13. China Se ASE SMM mM 15 unen c A mE E AAA AA BP PFE RL Backlit display Ultrasound head Brass spacers o RAMA BEEF at ATE no Ps e E FE ril SE Xx ATESA Ub rem r shes Ear e re FR GIE 10 Seclion2 Specifications 2 1 Technical specifications opecifications are subject to change without notice Analysis 1 ppb 20 ppm O5 0 75 5 VN or 1 5 10 g kg Total Package Oxygen 5 ug L 10 whichever is the greater Repeatability r95 at 20 C 5 C CO 0 05 V V or 0 10 g kg 2 whichever is the greater 2 ppb 10 whichever is the greater Measurement range NO lt 1 ppb 0 01 V V or 0 02 g kg N IN Detection limits Q O N Typical analysis time About 4 minutes Sample throughput 12 samples per hour Antifoam cartridge refill Approximately every 2 000 measurements ppb or ppm V V g kg g L or W bar mbar psia C F or K mg mL mg L mL L or ug L O concentration CO concentration Display units Pressure Temperature Package quantities Package temperature 2 to 30 C 28 to 86 F 1 4 to 6 8 bar 20 to 73 psia 0 to 40 C 32 to 104 F Up to 8096 Maximum package height 340 mm 13 39 ins Package pressure Operating limits Ambient temperature Relative humidity Minimum package height 90 mm 3 54 ins 150 ml Metallic or PET Package setu g P Minimum volume Enclosure types Dimensions L x W x H Weight Enclosure protection 537 x
14. Mas checks 20 03 2009 045331 Masal diaplaceemese SS Ol BES E SS ss Se Se EON reen m re Then selected a location on your PC to store the file The files and filenames are the text files that are listed in Data download configuration on page 46 49 Configuration 5 7 Sensor configuration This option defines the sensor service and calibration schedule for all the sensors installed on the instrument Depending on the sensor selected it is also possible to define automatic calibration and verification frequencies Select from the following sensors O2 sensor CO2 sensor Pressure sensor Temperature sensor Flow sensor Barometric pressure sensor The following example is for the O sensor which illustrates all the available settings DEE management Mest saraca date Dr TOF A8 Calbration management Net cabeamon date Domen AE Puto cabra ke Auto cakbration frequency Frequency selection Heft auto calibraci n dato Terr CE Auto yenficabon Met auto ventication date TELHA UE Check the activation flags as required Service frequency When set the system will inform you when a sensor service is required by setting the LED indicator on the top right of the header banner to yellow Calibration frequency When set the system will inform you when a sensor calibration is required by setting the LED indicator on the top right of the header banner to yellow Auto calibration When set the system wi
15. Security management Pacman flags ke Access nght enabled Auto kapott ke Audit trail Logout timer E min This option configures parameters related to confidentiality Check the activation flags as required Access rights enabled When checked recommended it is required to log on as a registered user to access the menus When disabled default all menus are access free and there will be no name recorded against any actions in the log file To set up valid users refer to User management on the next page Auto logoff When checked the user is logged out automatically when the set delay for inactivity Logout timer is reached and the instrument goes on standby When in standby mode the instrument will trigger any outstanding automatic actions that have been set e g sensor calibration verification etc See Sensor configuration on page 50 for additional details Audit trail When checked every action from a user is recorded in an audit file for traceability These actions cover the configuration calibration and maintenance options Each record holds the date and time of the action the action ID and description and the operator name and ID The audit file is a rolling buffer recording the last 1000 actions Logout timer Enter a maximum time of inactivity in minutes for all users Users are logged out automatically when the period of inactivity exceeds this value provided the Auto log off feature is enabled Clear
16. audit trail file This option deletes the audit file When all details have been entered select Ok to confirm 43 Configuration 5 5 2 User management 44 When selected the list of registered users for this instrument are displayed re came pu Que T om meme You can then e Add New users e Delete existing users e Edit existing users Note To have the Delete and Edit options available select one of the existing users first To add a new user all of the following fields must be completed Br a rg opt ri Marne Fraser Security level Operator e Name Enter the user surname 3 15 characters e First Name Enter the user first name 3 15 characters e ID Enter an alphanumeric ID 1 10 characters e Password Enter an alphanumeric password 3 15 characters e Security level Select the security level from the drop down list For a list of options available at each level refer to the following table Configuration Available options Measurement and Analysis Calibration Measurement Analysis and Maintenance Configuration Calibration Measurement Analysis and Maintenance Administrator Configuration Calibration Measurement Analysis and Maintenance When all details have been entered select Ok to add the new user To remove or modify an existing user select the user in the user management screen and select Edit or Delete as appropriate To save all changes press on the Ok b
17. but can be reactivated by tapping it Once reactivated you will need to enter a valid user ID and password combination if this has been set up e For detailed information on the other options refer to e Configuration Configuration on page 35 e Calibration Calibration on page 53 e Measurement Measurement on page 63 e Analysis Analysis on page 69 e Maintenance Maintenance on page 71 4 2 2 Touch screen The user interface on the front panel is a TFT VGA 640x480 color display with touch screen To make navigation user friendly the interface software is Windows CE based providing easy selection through menus 4 2 3 Virtual keyboard When a text box alphanumeric field is selected for data entry a virtual keyboard appears on screen as illustrated below This is used in a similar way to a standard PC keyboard IL number Once values have been entered press the J Enter key on the right of the keyboard to confirm input and exit the virtual keyboard During editing the edited field name is displayed along with units where applicable Note Use the Cap key at the bottom left of the keyboard to switch between upper and lower case characters This is important for case sensitive information such as passwords 31 User Interface and Startup 4 2 4 User identification and access level If access rights have been enabled it will be necessary to log on as an authorized user to
18. calibration time is 20 30 minutes New calibration 1 Start a new calibration by pressing the New calibration button A calibration screen is displayed a veer Calibration Mie Serie values Slope coeffcient 75 320 bar Ratio ldeal membrane 7061 b Rabo last calbrabon Moo D Stability ina y Current 14 483 TI Temperature ECS C Bar melint pressure 543 3 miar Calbratian riormaton Liser rame omes User ID 4 S Cakbranon cate 28 D3 2008 07 15 10 Caleraton Statue Ratio within range 59 Calibration 2 he value Ratio ideal membrane is a percentage of the current against the ideal current for the membrane being used If this percentage is not within the accepted range an error message is displayed and the calibration process fails A warning message will be displayed when this value is close to the boundaries but when calibration can be accepted 3 he value Ratio last calibration shows the percentage of this measurement and the last sensor calibration measurement The Stability field shows the stability of the measurements 4 The Calibration Status box at the bottom of the screen shows whether the calibration is valid or not Only if valid and with stable measurements will the Validation button be displayed Pressing this button will allow you to accept the calibration store the new values and write the details to the calibration report file Note Remember it is recommended to
19. components front view Specifications 2 4 2 Left side view 2 3 1 Power socket 5 USB A connector for mass storage device 2 Power ON OFF rocker switch 6 RS485 9 pin connector 3 USB A connector for mass storage device 7 Ethernet connection Figure 3 Instrument components left side view 15 Specifications 2 4 3 Right side view 2 3 1 Emergency STOP button 4 Gas connection No 3 IN Calibration gas CO only 2 Gas connection No 1 IN Forcing gas air CO or No 5 Gas connection No 4 OUT Pressure sensor calibration 3 Gas connection No 2 IN Purge gas CO only Figure 4 Instrument components right side view Specifications 2 5 Operation overview 1 Piercing The reference volume is filled with the purge gas and the whole of the gas sampling path is fully purged The purge stops when the rubber seal of the piercing device contacts the top of the package Once the package is pierced a pump injects an antifoam solution into the headspace 2 Oxygen in headspace The regulating valve is opened and the gas contained in the headspace flows on the O sensor at a given rate The quantity of O in the headspace is obtained by integrating the volumes of O leaving the package per unit of time 3 Liquid analysis CO and O3 The gas flow is stopped and the ultrasonic sonotrode is activated The equilibration pressure and the temperature are measured and a P T CO value is calculated The
20. fabricante o proveedor de los equipos para solicitar instrucciones sobre c mo devolver los equipos obsoletos para su correcto reciclado NEDERLANDS Elektrische apparatuur die is voorzien van dit symbool mag na 12 augustus 2005 niet meer worden afgevoerd naar Europese openbare afvalsystemen Conform Europese lokale en nationale wetgegeving EU richtlijn 2002 96 EC dienen gebruikers van elektrische apparaten voortaan hun oude of afgedankte apparatuur kosteloos voor recycling of vernietiging naar de producent terug te brengen Nota Als u apparatuur voor recycling terugbrengt moet u contact opnemen met de producent of leverancier voor instructies voor het terugbrengen van de afgedankte apparatuur voor een juiste verwerking POLSKI Sprz t elektryczny oznaczony takim symbolem nie moze by likwidowany w europejskich systemach utylizacji po dniu 12 sierpnia 2005 Zgodnie z europejskimi lokalnymi i pa stwowymi przepisami prawa Dyrektywa Unii Europejskiej 2002 96 EC u ytkownicy sprz tu elektrycznego w Europie musz obecie przekazywa Producentowi stary sprz t lub sprz t po okresie u ytkowania do bezp atnej utylizacji Uwaga Aby przekaza sprz t do recyklingu nale y zwr ci si do producenta lub dostawcy sprz tu w celu uzyskania instrukcji dotycz cych procedur przekazywania do utylizacji sprz tu po okresie u ytkownia PORTUGUES Qualquer equipamento el ctrico que ostente este s mbolo n o poder ser eliminado
21. instrument s automatic calibration feature based on an average of 500 package analyses per week This proposed schedule can be modified according to operating conditions Barometric pressure sensor 6 months 53 Calibration 6 4 Barometric pressure sensor After selecting this option the details of the last barometric pressure sensor calibration are displayed This shows the values recorded and information about who performed the last calibration and when The due date of the next calibration is also shown determined by the parameters entered in Sensor configuration on page 50 There is the option of starting a new calibration or viewing the last 10 barometric pressure sensor calibration reports see Calibration reports on page 62 Rae pressure Sore oe Current value Disel eoelhement Deviation last calibration mien ns l emperature User Nam Joras User ID 100 Calibration date 17 04 09 Da 35 D AM Calbrab n due date Anm DEB 1 Start a new calibration by pressing the New calibration button A calibration screen is displayed with the top box showing the current barometric pressure as measured by the instrument Ew onec pru SLT ee C abhiration Measured values Current barometric pressure 5798 Deviation last calibiration DOT Stability Temperature New barometnc value Calbrabon mlarrmalion Lisor narrse ines Usar ID 1004 Calibration date 17 04 9009 0 591 DIRE AM 2 Using a p
22. is disabled 7 1 2 Package ID Define the package to be measured The package details must have already been entered into the system see Package parameters on page 37 for details Pgh aci EE Ts E index 0 Selected Package Package Package 4 Canned wg beer Es KR Pe Select the package from the list provided and press Ok If necessary you can change the package details using the Edit button For details on editing a package refer to Package parameters on page 37 64 Measurement 7 1 3 Start analysis Important Note Once a sample has completed the measurement process it will contain a small amount of antifoam Therefore after measurement ensure the sample is disposed of in a sink or similar to avoid any risk of ingestion Once the Start Analysis option is selected the instrument will display any operator instructions and progress throughout the duration of the measurement process Note If the Diagnostic measurement view and the Display diagnostics results boxes have been checked during configuration see Measurement output on page 41 then the screens will differ see examples in Diagnostic measurement and results views on page 68 but the process is the same Select this option to start the measurement process Each screen will give information regarding the measurement step being taken and will give instructions on any user involvement required Note It is advisable to cover the bas
23. min manng Transhening Cab TemgprTable ba Free space 359 60 MB Used space 4 L3 Do nob remige LIBE m rronyl On completion a pop up window will inform you the process completed successfully and you can remove the device Remove the device and press YES in the pop up window to continue followed by EXIT in the main window to complete the process Next insert the device into an available USB port on your computer and download the data to an appropriate folder using standard computer software The text files with a txt file extension are in a readable format on a PC and most document editors MS Word Notepad etc can be used to open these files as well as spreadsheet and other reporting tools e g MS Excel The following is an example of the instrument configuration report Configuration txt as viewed using the Notepad utility Configuration txt Notepad File Edit Format View Help TPA Configuration Units and resolutions Volume 2 ml Quantity 1 ma Time O Second Threshalds Delta P2 n 02 Delta P 2 00 Delta D 0 04d Delta PF O 03 Min o2 Threshold o 00 Max 02 Step 0 0 00 standby flow val 0 25 Flow val in system flush 47 Configuration 5 6 2 Web browser configuration I RITE DTE condis ation Enable browser access Device name nua amp 1n Obtain an IP address automatically Your dict can mE address assigned autorncatic al if your network support the capabilbe
24. oxygen sensor calibration are displayed This shows the values recorded and information about who performed the last calibration and when The due date of the next calibration is also shown determined by the parameters entered in Sensor configuration on page 50 There is the option of starting a new calibration or viewing the last 10 oxygen calibration reports see Calibration reports on page 62 Important Note This procedure uses information from the barometric pressure sensor Be sure that this parameter is reliable i e a recent barometric pressure sensor calibration has been performed see Barometric pressure sensor on page 54 Oo enon Last calbration value Calbration coeficient 111 824 Ratio deal meriang EM 791 kann last calibration Ed rH Stability 0 25 Temperature 28 17 Barometric pressure 361 55 User name Jones User IC 1004 Calibration date 74 14 09 01 74 00 PMH Calibration due date ZA ZU The O sensor should be calibrated after each sensor service or when the calibration due date parameter has been passed After a sensor service wait at least 30 minutes after mounting a new membrane before calibrating Note For full details on sensor servicing please refer to the A1100 Sensor Installation and Maintenance Manual that was delivered with the instrument The Os sensor is calibrated in situ with an air pump providing a continuous flow of fresh air in front of the sensor head The recommended minimum
25. process 2 more times until the antifoam cartridge is full 8 On completion rinse out the syringe and all tubing with water Screw the cap back onto the antifoam container and store the tools and container in a cool dry place Note One antifoam recharge bottle should be enough to fill the cartridge at least 3 times 23 Installation 3 7 2 Antifoam cartridge installation Install the cartridge as follows 1 Lower the piercing device to its lowest point it will stop automatically once this point is reached If using the wizard simply press the Do It key on screen If not using the wizard refer to Manual displacement on page 80 for details 2 Remove the plastic front protection door by carefully raising it up on its rollers and over the top of the instrument to give access to the antifoam cartridge location 3 Open and remove the small front door No 1 in the diagram for easy access to the antifoam cartridge chamber Fit the cartridge in place by lining up the two fluid connectors chamber connector shown as No 2 in the diagram cartridge connector as No 3 4 Press down gently and twist slightly if necessary until the cartridge clicks into place No 4 in the diagram with the two connectors located towards the back 5 Attach the two connectors No 5 in the diagram to the pump leads inside the chamber no specific polarity 6 Return the small door to its original location and close to secure t
26. that can be used are listed down the left side of the screen and the operators and operands are listed down the top right In the bottom right of the screen are a number of screen navigation options to assist in editing The colored indicator in the top right corner shows the validity of the formula as it is being created It is initially colored yellow but will turn red if the formula is invalid and green when valid When the indicator is red the Ok button will be unavailable Use the Select button to select an existing formula to include in the new formula The list of existing formulae is displayed as a rolling list When a valid formula has been entered press the Ok button to continue You are then requested to assign a name to the new formula after which an information box is displayed showing the name of the user who created the formula and the date and time it was created If required add any free format alphanumeric text to identify the formula and press Ok to continue User name ones Date 17 04 2008 Time Edit or delete a formula To edit or delete a formula first select the formula from the list displayed and then press either Edit or Delete as appropriate If delete was selected you will be asked to confirm deletion before the formula is deleted from the list If edit was selected the formula editor screen is displayed to allow you to change the definition of the formula 40 Configuration 5 4 In
27. this option the details of the last temperature sensor calibration are displayed This shows the values recorded and information about who performed the last calibration and when The due date of the next calibration is also shown determined by the parameters entered in Sensor configuration on page 50 There is the option of starting a new calibration or viewing the last 10 temperature sensor calibration reports see Calibration reports on page 62 The temperature calibration is made using an accurate internal resistor Temaer ELUTTEET 1701 Last calibration value Offset coefficient SHOE coefficient Resistance 1 temperature Stabilty Resistance 2 temperature stabile Wiser name User ID Calibration date 20 04 08 07 24 00 FM Calibration due date ANA 1 Start a new calibration by pressing the New calibration button A calibration screen is displayed LUTTE STAT TORTE don Cobb alem Measured values Temperature 1 Stability lemperabure 2 stability Calibraman mforrnati n User name User ILI C alibratian date 2 The instrument measures two temperature values and checks the stability of the measurements Provided the measurements are stable you can choose to accept or reject the new values Press Validation to store the new setting 3 Once the calibration is completed a calibration report is created 58 Calibration 6 8 Oxygen sensor After selecting this option the details of the last
28. 04 7009 i j Cimri Hum 1 fo 000 i i hum 2 n 0000 Cmnt 1 O2 Total O2HS Dis CO2 Cmnt 2 0 0 0 0 5 21 Cmnt 3 Cin 4 Cmnt 5 The three measurements are displayed graphically and are color coded Those in green show that the measurements are within the defined limits for this package Those in red signify that the measurements are outside the defined limits These limits have been previously defined in the alarms section of Package parameters on page 37 It is possible to add 2 numerical values and 5 comments to these results by entering them in the text boxes displayed down the left Press the Continue button to return to the main measurement screen or press the Info button to display more detailed results again color coded in a tabular format Ma Le cem vy ales i For additional information on viewing the full set of measurement results see the section entitled Open data on page 69 67 Measurement 7 2 Diagnostic measurement and results views These views are essentially used for troubleshooting purposes by Hach Lange service technicians therefore no detailed explanation of the data displayed is given in this manual 7 2 4 Measurement view As the measurement process executes the measurement details are displayed down the left side of the screen The first line of the display shows the current stage in the process The right side of the screen gives additional textual information Gar
29. 7 7T Runan instrument auto check see Run instrument auto check on page 28 Note At this point the physical installation has been completed 8 Set the security levels user ID s and passwords see Security and user management on page 43 Note To commission the instrument so that it is ready for use follow the next steps to configure the instrument and calibrate the sensors 9 Configure the instrument parameters see Configuration on page 35 10 Perform a barometric sensor calibration see Barometric pressure sensor on page 54 11 Perform an oxygen sensor calibration see Oxygen sensor on page 59 Wait until the residual value of the sensor is low enough controlled automatically by the analyzer This operation may take around 2 hours depending on storage conditions The instrument should now be ready for use If a problem should arise please refer initially to Maintenance on page 71 If the problem cannot be overcome please contact your Hach Lange representative who will be happy to assist you Installation 3 9 Power supply CAUTION Check voltage requirement sticker on the rear panel of the instrument before connecting Connect the power cable supplied with the instrument to the socket at the rear of the instrument left in diagram for AC power connection To switch the instrument on and off press the rocker switch right in the diagram I for On and O for Off 3 6 Purge and forcing gas supply
30. FRANCAIS A partir du 12 ao t 2005 il est interdit de mettre au rebut le mat riel lectrique marqu de ce symbole par les voies habituelles de d chetterie publique Conform ment la r glementation europ enne directive UE 2002 96 EC les utilisateurs de mat riel lectrique en Europe doivent d sormais retourner le mat riel us ou p rim au fabricant pour limination sans frais pour l utilisateur Remarque Veuillez vous adresser au fabricant ou au fournisseur du mat riel pour les instructions de retour du mat riel us ou p rim aux fins d limination conforme ITALIANO Le apparecchiature elettriche con apposto questo simbolo non possono essere smaltite nelle discariche pubbliche europee successivamente al 12 agosto 2005 In conformit alle normative europee locali e nazionali Direttiva UE 2002 96 EC gli utilizzatori europei di apparecchiature elettriche devono restituire al produttore le apparecchiature vecchie o a fine vita per lo smaltimento senza alcun costo a carico dell utilizzatore Nota Per conoscere le modalit di restituzione delle apparecchiature a fine vita da riciclare contattare il produttore o il fornitore dell apparecchiatura per un corretto smaltimento DANSK Elektriske apparater der er maerket med dette symbol m ikke bortskaffes i europaeiske offentlige affaldssystemer efter den 12 august 2005 henhold til europaeiske lokale og nationale regler EU direktiv 2002 96 EF skal europaeiske
31. ON 6 Cali FA e EE 53 6 1 Calibration MEn oVerviGW s uto dor p doas mae du te es tubae itus ee 53 6 2 otandards redulrermefilS EEN 53 0 9 Calibration eine TE 53 6 4 Barometric pressure Sensor iia 54 670 Pressure Senso MUNERE TE 55 SAP MI A 57 6 7 Temperature iia Kee 58 6 9 OVEN SENSO EE 59 6 9 CaroOn GlOXIGe Senso di cid 60 6 10 leie FOR NE DOMS mati a a aa 62 Section 7 Measurement EE 63 TIMOR SCIE a de enr cn Tot 64 ee VE Oper EE 64 AZ i re icona P Tr 64 e e a EE 65 7 2 Diagnostic measurement and results views 68 LL Measurement EE 68 JM RU tu 68 S cHon s AnalySiS i oot eid a Nena oM ecd tres rese etd cpi ume ada d 69 9 1 JAnalyze MENU Ee NEE 69 A A a A 69 99 Table SENOS eut a Ee 70 Section 9 Maintenance racion aia 71 G WE le Ei eer Ee ET 71 97 TAS dl ME TET TT TET cer 71 OS Purge ya d Bie EE 11 9 4 Replacing the antifoam camada cat 12 9 4 1 Antifoam cartridge removal ccccccceccceececeeeeceeeceneesseeeueeseeeeseeseneeseeessueesegeesaeeteeeeneeees 72 9 4 2 Antifoam cartridge renlensbment ss 12 943 Anttoam cartridge installallOh oua ores toa eoa tur oves liada 13 9 5 Oxygen sensor maten ande te da O 14 9 6 Gore Tex filter replacement iii iiiisieeeieeeceeeeeeeeenn 15 9 7 Replacing the piercing gasket and tip RL 76 9 8 Maintenance menu OVGrvVleuw een ket eene nennen nnne nnne RTE E EET saei se isses asa LEE ktr sae rns 77 9 9 Di
32. One and first point calibration starts automatically By default the first point calibration option uses the Barometric connection button highlighted at top right of the screen This can be switched to Forcing gas connection if required by pressing on the highlighted button 2 When the measurement stabilizes the Validation button is highlighted Press this to accept the measurement or override the current value by entering a value into the Measured pressure box and press Validation Prune A d r At First Fle SL miu Ermeni Curent read pressure 1058 07 mbar Garomeinc pressure f B2 97 miar TR Stability fon Measured pressure a 5 Van Calbrabon dor bon Ulver neri nes Licor IC TUL Calibration date En 494 2009 10 17 18 AM One and fret point calibration 7 Second point for ten points calibrabon 55 Calibration 56 3 A second Validation button will be highlighted at the bottom left of the screen If only a one point calibration is required press this second Validation button to accept the calibration and complete the process If a two point calibration is required select the Second Point for two points calibration button at the bottom of the screen Brace carn cabhiratinn Second pressure measurement Currerm read pressure 15131 HU rri Barometnic pressure 969 od riae Stability 0 00 MES ME User ID TU Calbrabon date 20 054 2008 10 77 10 AM Measur
33. Warning messages on page 88 The Column selection defines the three measurements to display on the measurement results screen after the measurement process has completed see screen example on page 67 e Column 1 3 For each of the three columns define the measurement to display from the drop down list When all details have been entered select Ok to confirm 41 Configuration 5 4 2 Time and date Use this option to set the system date and time parameters and the display format Timn Date configuration Tire M AAA Hour Format Mute Ee HK C 24H Second Format mm de yyyy da rmevyyy ve men dd When all details have been entered select Ok to confirm 5 4 3 System information Use this option to display the system information about the currently configured boards Mam hard CE version Board sii 0013640001457 TRA sofware version EC board SO Are versian Control board Solana versn ALIO board Solana versn Select Exit to exit the screen 42 Configuration 5 5 Security and user management Note When the instrument is started for the first time security is disabled by default To avoid any unauthorized access it is highly recommended that each user be entered into the system and given appropriate access rights as soon as possible Details are provided in this section Select from security management User management Audit trail 5 5 1 Security management
34. ZATION Sensitization Will not occur To the best of our knowledge the chemical physical and SIGNS AND SYMPTOMS OF EXPOSURE toxicological properties have not been thoroughly investigated ROUTE OF EXPOSURE Skin Contact May cause skin irritation Skin Absorption May be harmful if absorbed through the skin EyeContact Contact May cause eye irritation gt Material may be irritating to mucous membranes and upper respiratory tract May be harmful if inhaled May be harmful if swallowed 94 Material Safety Data Sheets MSDS ECOLOGICAL INFORMATION Test Type LCO Fish Species Brachydanio rerio Time 96 h Value 180 mg l Test Type LC50 Fish Species Brachydanio rerio Time 96 h Value 250 mg l Test Type LC100 Fish Species Brachydanio rerio Time 96 h Value 350 mg l DISPOSAL CONSIDERATIONS Incinerate in a furnace providing environmental regulations permit Observe all federal state and local environmental regulations TRANSPORT INFORMATION RID ADR Non hazardous for road transport IMDG Non hazardous for sea transport IATA Non hazardous for air transport REGULATORY INFORMATION Not hazardous according to Directive 67 548 EEC Caution Substance not yet fully tested EU COUNTRY SPECIFIC INFORMATION Germany WGK 1 Self Classification OTHER INFORMATION WARRANTY The above information is believed to be correct but does not purport to be all inclusive and shall be used only as a guide The informati
35. aburie Vokumme Pressure CIS ries Fonmula Configuration Touch the Resolutions tab on the screen to define the display resolution for all values displayed by the instrument e For each parameter listed a rolling list will be displayed giving the available display resolutions A maximum of 4 digits and a decimal point can be displayed Decimals can be limited to O 1 2 or 3 for easier reading This does not affect the actual resolution of data measured and stored only the data displayed on screen Select the required resolution from the list and press Ok to continue When all display resolutions have been defined press Ok on the main screen to save these values and continue Note The instrument performance and specifically the sensitivity and accuracy of each measured parameter is not affected by the choice of resolution This is purely for screen display purposes Refer to Technical specifications on page 11 to view the accuracy of each measured parameter 5 3 Package parameters Select from e Package management e Formula management 5 3 1 Package management This option allows you to add new package definitions up to a maximum of 100 and edit or delete existing definitions When selected a screen is displayed listing all existing packages Selected package Package Package 1 Bottled bght beer Press the New button to create a new package The new package will be created using the default package parameter
36. ach a supply of known CO gas to the instrument as indicated by Gas connection IN 3 in Figure 4 on page 16 Enter the known concentration value in the Gas purity box Press the Validation button at the bottom of the screen to accept the new calibration 61 Calibration OG tar Cala bon TC second calibramon gas Gas read purty as Tie Stability Las purity i ablbrabion morrai User narra User ID Calibrabon date 29 04 2009 07 23 42 O Main gaz Second calibrabon gaz 5 Press the Validation button to accept the calibration store the new values and write the details to the calibration report file If the calibration cannot be performed an error message will be displayed giving the reason Verification 1 The process is exactly the same as for a new calibration but once the details have been displayed on screen press the Cancel button to complete the process No report is produced 6 10 Calibration reports OF pre calibration Report recom sf 4 Calibrabon coeficient 9 614 Fate deal menbrane 15511 Rato last membrane 20 199 Stability 0 32 Temperature 32 5B Sarme pressure 0 55 User name Jones Licor Ej 1004 Calbration date 79 04 09 01 74 00 PH Calbration due date DE ATL A j tae Lei Details of the last 10 calibrations of the selected sensor are displayed on screen Use the First Previous Next and Last buttons to scroll through all existing reports Note The calibration reports can b
37. aintenance menu in order to complete the installation Make sure you have read the section entitled User Interface and Startup on page 29 so you are aware of startup and data entry procedures including the default username and passwords before starting the installation Also ensure you have suitable standards available before performing any calibration See standards requirements on page 53 for calibrating the instrument sensors 1 Connect the instrument to a power source see Power supply on page 21 2 Turn the instrument ON An instrument auto check routine will start automatically As this is the first time the instrument will have been turned on a number of red LEDS will appear but at this stage these should be ignored as the instrument is not yet fully operational Note The following steps 3 to 7 can be completed by following the on screen instructions and diagrams shown on the instrument by the installation wizard Where processes are unclear from the wizard please refer to the corresponding step in these more detailed installation instructions 3 Connect the purge and forcing gas to the instrument see Purge and forcing gas supply on page 21 4 Prepare and install the antifoam cartridge see Antifoam cartridge preparation and installation on page 22 5 Prepare and install the oxygen sensor see Oxygen sensor preparation and installation on page 25 6 Prime the antifoam tubes see Prime the antifoam tubing on page 2
38. and over the top of the instrument to give access to the antifoam cartridge location Locate the red nut under the measurement column No 1 in the diagram and unscrew it by turning it clockwise 4 Remove and discard the old filter No 2 in the diagram and replace it with a new one No 3 in the diagram Screw the red nut back in position finger tight 5 The plastic front protection door can now be put back in place by lowering it down over the instrument ensuring the rollers are correctly located inside the slots on each side CAUTION Ensure the rollers are correctly positioned inside the slots before slowly and carefully lowering the door Incorrect positioning and or forcing the door down could easily damage the exterior housing of the instrument 6 Manually raise the piercing device back to its upmost home position Refer to Home position on page 79 if you are unsure how to do this 75 Maintenance 9 7 Replacing the piercing gasket and tip 76 1 CAUTION A The piercing tip is very sharp Take extreme care during this process Lower the piercing device to its lowest point it will stop automatically once this point is reached If using the wizard simply press the Do It key on screen If not using the wizard refer to Manual displacement on page 80 for details The illustration below left shows the position of the black rubber gasket Carefully twist and remove the gasket to reveal the piercing head
39. as been completed the color will change to green provided it was the only sensor awaiting a service Observation Explanation Negative TPO results CO purge gas is not of the required purity of gt 99 5 The instrument never reaches the threshold value CO purge gas is not of the required purity of gt 99 5 Stop the analysis by pressing the emergency button and remove the bottle Check that the piercing spike is in place and not unscrewed Pull the emergency button to his initial position and restart the The bottle goes up with the piercing head instrument Open the front door to stop the process Remove the bottle and check that the piercing spike is in place and is not unscrewed Close the front door and press the Abort button on the screen 85 Maintenance 86 Section 10 Troubleshooting 10 1 Error and warning messages Note If any error or warning persists please contact your Hach Lange representative for assistance 10 1 1 Error messages Release emergency stop button HEX001 E1 E Stop E top butt hed The measuring head has missed an obstacle HEX002 E2 Motor error Initialize the motor Emergency stop button pushed if the motor is moving E4 The front door has been The front door has been opened before d HEX004 opened The measurement the end of the measurement process process has been stopped The front door is not closed properly Control the front door mechanism There is a probl
40. atrav s dos sistemas p blicos europeus de tratamento de res duos s lidos a partir de 12 de Agosto de 2005 De acordo com as normas locais e europeias Directiva Europeia 2002 96 EC os utilizadores europeus de equipamentos el ctricos dever o agora devolver os seus equipamentos velhos ou em fim de vida ao produtor para o respectivo tratamento sem quaisquer custos para o utilizador Nota No que toca devolu o para reciclagem por favor contacte o produtor ou fornecedor do equipamento para instru es de devolu o de equipamento em fim de vida para a sua correcta elimina o General Information 1 4 Product disposal Note The following only applies to European customers Hach Lange is committed to ensuring that the risk of any environmental damage or pollution caused by any of its products is minimized as far as possible The European Waste Electrical and Electronic Equipment WEEE Directive 2002 96 EC that came into force on August 13 2005 aims to reduce the waste arising from electrical and electronic equipment and improve the environmental performance of all those involved in the life cycle of electrical and electronic equipment In conformity with European local and national regulations EU Directive 2002 96 EC stated above electrical equipment marked with the above symbol may not be disposed of in European public disposal systems after 12 August 2005 Hach Lange will offer to take back free of charge to the cu
41. b s whenever and wherever yog need it Hadh m a eh cured subdiary of Darahar Corporation a lorbara DOO ampar EDI pn reen rwmabrlimm ad spero only Ha reasdi 11 E E und he You will be required to enter a valid username and password combination as defined in User management on page 44 48 Configuration The initial screen will then be displayed You can then click on Expand All to see all the available options Then click on the report you wish to view as in Audit trail below Audit trail report 18 30 af 29 50 04 2009 eat Econo calce xng ee 20 03 2000 attigi t Brom valet s iran Wisel sheds Se ET DA T 04058 n 10 03 2009 sn 20 03 2009 oe 303 2009 eus 20 03 2009 SC L 643118 19 01 2049 5m Depending on the option selected you will have the possibility to browse through all pages of the reports by clicking on the First Previous Next and Last buttons at the bottom Click on Exit to select another report or click directly on the list of reports on the left To download the data for your selected option right click on Import top right of the screen and select Save Target As Audit trail report 21012009 ap0 2009 21 81 2008 Cirer ine Larsen 55 Rocca TOF Zei ine Fare So pour FL E pem Elect valve ver rr mor Meses Checho Gud umm vea 20 03 2009 Ejermo vae veriicanon
42. ber of instrument parameters are also displayed down the left side of the screen indicating the current software and board versions installed Please wait Instrument auto check ae Boards OE OF sensor OK Li sensor resxhual 000817 mirar WTO sensor KO Temperature sensor Ok e Flow sensor OK ma e Pressure sensor OE Be Right Antioam level Empty e Foin detezctor OK Total Pa ckage Analyzer a Electro valves OK Model 6110 Main board OUT ADS f coag wil D Operabnig system 0 06 EC board siniss7 Motor mi amp alzation In progress irasod Orc e Protecbon cover L Emergency stop 4 07 ALIO based sii vi 06 Control board ein vit OF Skip Ship all ERE _ The right side of the screen lists each of the instrument components that are checked and a colored indicator to the left of each component shows the current status e A green indicator means that the component is installed and working correctly e Ared indicator means that there is a problem with that particular component e A yellow indicator means that the component is in the process of being checked e A blue indicator means that the component has not yet been checked A colored LED indicator on the top right of the header banner will indicate the current status of the instrument with regards to the sensor and hardware configuration e A green indicator means that no problems have been encountered e A yellow indicator m
43. bration and verification options in addition to the date parameters you will also need to define an idle time in minutes The operation will then only start when the instrument has been idle for that period of time 51 Configuration 52 Section 6 Calibration 6 1 Calibration menu overview Barometric pressure sensor New barometric value Pressure sensor Measured pressure Flow sensor H Measured flow Temperature sensor Q2 sensor This section describes the sequence of actions required to calibrate the sensors and flow meter on the instrument e Barometric pressure sensor e Pressure sensor e Flow sensor e Temperature sensor e O2 sensor e CO2 sensor 6 2 Standards requirements Although the instrument includes reliable and accurate automatic sensor calibration and verification routines refer to Sensor configuration on page 50 it is recommended that once a year calibrations should be made with external certified standards The instrument will provide accurate results provided accurate reference standards are used The following table shows the maximum ranges for the standards These ranges should not be exceeded CO at 99 9 purity at 0 1 which is the purge gas for the normal operation CO sensor CO at 80 95 purity at 0 1 CO at 80 20 N purity at 0 1 for nitrogenated beer analysis 6 3 Calibration schedule This following table shows the recommended sensor calibration intervals using the
44. brugere af elektriske apparater nu returnere gamle eller udtjente apparater til producenten med henblik p bortskaffelse uden omkostninger for brugeren Bemaerk forbindelse med returnering til genbrug skal du kontakte producenten eller leverandgren af apparatet for at fa instruktioner om hvordan udtjente apparater bortskaffes korrekt General Information SVENSKA Elektronikutrustning som ar markt med denna symbol kanske inte kan lamnas in pa europeiska offentliga sopstationer efter 2005 08 12 Enligt europeiska lokala och nationella f reskrifter EU direktiv 2002 96 EC m ste anv ndare av elektronikutrustning i Europa nu aterlamna gammal eller utrangerad utrustning till tillverkaren for kassering utan kostnad for anvandaren Obs Om du ska aterlamna utrustning for tervinning ska du kontakta tillverkaren av utrustningen eller terf rs ljaren for att fa anvisningar om hur du aterlamnar kasserad utrustning for att den ska bortskaffas pa ratt s tt ESPANOL A partir del 12 de agosto de 2005 los equipos el ctricos que lleven este s mbolo no deber n ser desechados en los puntos limpios europeos De conformidad con las normativas europeas locales y nacionales Directiva de la UE 2002 96 EC a partir de esa fecha los usuarios europeos de equipos el ctricos deber n devolver los equipos usados u obsoletos al fabricante de los mismos para su reciclado sin coste alguno para el usuario Nota S rvase ponerse en contacto con el
45. ce Menu to perform a standard system startup see System initialization on page 83 Verify the results of the auto check See Instrument startup on page 29 for a more detailed explanation of the auto check process and results Section 4 User Interface and Startup 4 1 User interface 4 1 1 Instrument The instrument front panel is comprised of a touch screen acting as display touch pad and keyboard Turning the instrument ON and OFF Note It is recommended to keep power supplied to the instrument at all times unless the instrument is to be moved to another location if it will not be used for a long period of time e g vacation period or if maintenance procedures need to be carried out inside the instrument The instrument has a power switch located on the left side of the base A LED on the instrument measurement start button No 5 in Figure 2 on page 14 indicates when the instrument is powered on 4 2 Instrument startup When the instrument is powered ON an initial splash screen is displayed showing the company logo and instrument model number The instrument then goes through a number of startup procedures to check all components are installed and functioning correctly Important Note Once the instrument is switched on you will need to wait until the O2 sensor residual value reaches the threshold of 0 1 mbar This operation can take up to two hours depending on the instrument and sensor conditions prior to startup A num
46. ctivated The upper bound limit is located higher than the reference position If this button is activated it means that the system is in an abnormal state of operation and you should call your local Hach Lange representative e End of travel lower bound activated Activated when the piercing device is in its lowest position e Front door closed Activated when the front door is closed e Protection cover opened Activated when the top protection cover is not in place e Ultra sound error Activated when the sonotrode is not working correctly Low level of antifoam Activated when the antifoam cartridge is nearly empty e Foam detection activated Activated when foam or liquid has ingressed into the gas sampling tube e Bottle rim detection activated Activated when a package is detected by the optical barrier For control purposes this can be activated by passing the hand between both optical detectors 78 Maintenance 9 8 2 Actuator verification This menu allows you to manually move the piercing device and to effect a number of other controls Select from e Home position e Manual displacement e Ultrasound ON OFF e Lasers ON OFF e Antifoam system 9 8 2 1 Home position select the operation you would lke pe n Infermmalibenis Zog reference position End af travel upper bound End of travel lover bound Select from e Initialization to return the piercing device assembly back to its home top pos
47. de analysis in progress Liquid anaysis 0 ei ru The preoure rg stabe 00 014 moar 84 51 b End of the desd volume nnsmag Presoure X549 HT Temp N Z position PF Barom 7 2 2 Results view The following screen is displayed on completion of the measurement process Hor Te POLA Head pace volume neferenmeca Head pace ONE Edd d Q2 mi head space C2 in Liquid Total O2 a LZ Phase 1 U2 Phase AB ep d a PIT CO True GU Total OO d E Ce ON SINE measured sensor values Note If the Stored measured sensor values box at the bottom of the screen is checked the values are recorded in the results file and as raw data but with pre defined units These units cannot be changed by the user 68 Sections Analysis 8 1 Analyze menu overview This section describes the options available for viewing the measurement data on the instrument e Open data e Table settings 8 2 Open data This option allows you to view the measurement data from the last 1000 measurements TER ET TE EL DE Aus A DEUS ZA Lai Jd D The data elements displayed are those defined in Table settings on page 70 Use the Previous and Next buttons to scroll through the data Use the Exit button to return to the main analyze menu Select one of the lines of data and the Info button will be made available Press the Info button to see more details of the measurement in a new screen
48. e and adjusting its position to that defined for this package Lock it in place by turning the locking wheel clockwise finger tight Once the package is secure against the backstop and the piercing position aligned with the two red laser beams close the front door Start the measurement process by pressing the START button on the right side of the instrument base Initialization Package menie aon Package 1 it poston Pont n adputimera Operas xnon Please wt Elapsed tere 25 Lets than SUE A progress bar is displayed at the bottom of the screen showing the elapsed time to date and the estimated time for measurement completion This bar is updated on an on going basis No intervention or action from the user is required until the measurement process has completed However you do have the option to Abort the process at any point The measurement goes through four main stages during which time a number of measurements are taken and calculated e The piercing arm is lowered and the package is pierced e The head space is analyzed e The liquid is analyzed Measurement e The measurement completes and the piercing arm is raised to its home position Once measurement is complete the results are displayed The three columns of data displayed are those that were previously defined in Measurement output on page 41 Operator Jonas Package Package gt CO CO campi Standard beer 11 47 37 30
49. e easily transferred to a PC or USB storage device see details in the section entitled Communication on page 46 62 Section 7 Measurement The following flow chart shows an overview of the measurement process The actions listed on the left are performed by the user and those on the right by the instrument Enter operator 1D and password required D T Select package and adjust tik and Close analyzer front door Y Press analyzer START button Laser pointer activated Measure reference volume pressure t id Pierce the package D Laser pointer deactivated gt Y Measure H5 P T Y HS expansion anc determine O Enable ultrasound Measure new HS PIT T T New HS expansiomand determine O and CO purity Arlean d ean T Lift piercing device T Display measured values 63 Measurement 7 1 Main screen The initial screen displays standard information about the package to measure Ki Lise d Package lderficatien Package Tit open 1 0 Package backstop 2 0 amp atan Spaas Shand by Cosfigqurablo Calibration TTE Malalenancs Qo e mm You have the option to change the details displayed or to start the measurement process e Operator e Package ID e Start analysis 7 1 1 Operator Provided access to the instrument is by a valid ID and password combination the operator name will be displayed This will be blank if security access
50. e of the circular package holder with water for better energy transmission of ultrasound waves to the package content The first screen gives details of the package being analyzed and gives the user information on what action to take Sample analysis in progress Package identficabon Package 1 Iit pasion Pont n adustment Operators action Open the front door and place the package for analyzing As instructed raise the transparent front door in order to place the package in the measuring chamber As soon as the door is raised the initialization screen is displayed with the next set of instructions Compe analis in progress Initialization Package ibentific aigi Package 1 TR pasion Potion adpuistment Operations action Put the package to analyze in place Pay amnerton to the piercing Poston tenant wath me aser Cros Close the Front door Push the Button t stat Pa measurement As instructed place the package to be analyzed on the circular platform and set the tilt position as defined for this package by turning the black knob on the front Two red laser beams are activated as the front door is raised Position the package so that the centre of the package is where the two red beams intersect This is the place where the package will be pierced 65 Measurement 66 Make sure that the package is also hard up against the backstop This may require realigning the backstop by turning the locking wheel counter clockwis
51. eans that a sensor service or calibration is required or that an automatic planned task e g sensor calibration or verification is required and which will be activated the next time the instrument is in standby mode e Ared indicator means that there is a problem with the sensor or hardware configuration or that the instrument is not ready e g oxygen level is too high 29 User Interface and Startup For detailed information on the sensor configuration options refer to Sensor configuration on page 50 If the LED indicator is not green then pressing on this will display a list of configuration errors or warnings as in the example below Gener configuration status Sensor conhgutabon status Firm detectar anno test is Fail LC sensor auta calbrabon is pending LO senor auto verificatian rs pending Temperature Sensor senacing ls pending It is advisable to correct all of the errors listed before continuing to ensure the instrument is working correctly It is not recommended to continue if the LED is showing red see Red LED s on startup screen on page 89 for assistance Note On instrument startup for the first time the O2 sensor residual and the Antifoam level LEDS will always be red This is normal as the system has not yet been fully commissioned and these red LEDS can be ignored at this stage On completion of all startup checks you may be required to enter a valid identification number and password as described in User
52. ed Erg RE rro Calbrati n information User rame O One and first pont calibraban Second point for mo ponts calbeatian By default the second point calibration option uses the Forcing gas connection button highlighted at top right of the screen When the measurement stabilizes the Validation button is highlighted Attach a certified precision barometer to the gas outlet tube on the lower right side of the instrument as indicated by Gas connection OUT in Figure 4 on page 16 and take the pressure reading If this value is different from the measurement displayed on screen enter this pressure reading in the Measured pressure box and press Validation or if the values are the same just press Validation Finally press the Validation button at the bottom of the screen to accept the new calibration and complete the process Once the calibration is completed a calibration report is created Calibration 6 6 Flow sensor After selecting this option the details of the last flow sensor calibration are displayed This shows the values recorded and information about who performed the last calibration and when The due date of the next calibration is also shown determined by the parameters entered in Sensor configuration on page 50 There is the option of starting a new calibration verifying the flow sensor or viewing the last 10 flow sensor calibration reports see Calibration reports on page 62 Important Note This p
53. em with the antifoam Moe Try another measurement Injection E10 Foam has been Incorrect tilt of the sonotrode Check the tilt of the sonotrode HEX010 detected in the gas path The Check the antifoam level and refill if measurement process is There is no more antifoam necessary canceled Prime the anti foam pump The pressure in the package is greater Increase the purge gas pressure than the purge gas pressure E20 Not enough pressure in Problem of flow regulation during the Check the purge gas pressure HExo20 the system The measurement Change the Gore Tex filter measurement process is i canceled Wee patnis Palen oF totaly Control the antifoam injection HEX040 E40 Check gas SE Before filling the reference volume the Check the purge gas pressure current pressure XXXXX pressure is lower than 1 5 bar The ultrasound power supply is OFF Check the ultrasound power supply The emergency stop button is not HEX100 E100 Ultrasound error EEN i a There is too much water in the Remove any excess water ultrasound generator i The motor is above the reference HEX200 E200 Motor error High position Go to the maintenance menu move limit the motor down and initialize it An upper or lower limit is ON 87 Troubleshooting 10 1 2 Warning messages Warnin Code in 9 Displayed message Probable cause results code file W1 Unstable reference The variation of reference Check the pressure stability of HEX001
54. eplacement e EC sensor maintenance e Gore Tex filter replacement e Needle tip and seal replacement These options are also described at the front of this section see Replacing the piercing gasket and tip on page 76 Oxygen sensor maintenance on page 74 Gore Tex filter replacement on page 75 and Replacing the piercing gasket and tip on page 76 for more detailed explanations of these procedures 84 9 8 8 Sensor services Maintenance This option lists the service due date for each sensor These are user defined in Sensor configuration on page 50 As each service due date is passed the Service done button will be made available as with the Barometric pressure sensor in the example below DOTADO Sb vircs O2 Sensor Semice due date CO Sensor serie due dale Pressure Sensor Serice due date H TALA ESTIS Temperature sensor Serio due date Ek sernai serie due date Barometric pressure sensor Senece due date 01042010 DILL ALIS 21 04 2008 21 04 2009 01042009 17 03 2008 Press the Service done button provided the service has been performed on the sensor This will then reset the service due date based on how the sensor service has been configured Note Pressing the Service done button may also have an effect on the colored LED indicator on the top right of the header banner For example if this showed yellow indicating a sensor service was required then by letting the system know the service h
55. essure Temp 41378 2h qn mbar c Ref Val Mam Purge Meedle Purge mmy Check a component by pressing on the button schematic which will turn to green and observe the values being displayed Note If the gas flow rate is manually changed be aware that the automatic purge procedure every 5 minutes will reset the gas flow rate back to 0 25 mL s which will have an impact on the values being observed 9 8 5 System initialization Selecting this option initiates the standard system startup process without having to power off and on the instrument See Instrument startup on page 29 for more information on system startup 9 8 6 End application Select this option to perform an orderly shut down of the instrument On completion the instrument can be powered OFF 83 Maintenance 9 8 7 Wizards This option gives a visual guide on a number of standard procedures to perform on the instrument There are currently two groups of wizards available for e Installation e Maintenance be Slip installation wizard on device startup The installation wizard will be invoked automatically the first time the instrument is switched on to help you complete the installation of the instrument Once the instrument has been successfully installed the Skip installation wizard on device startup checkbox should be checked to ensure a normal startup from there onwards The maintenance wizard gives you four options e Antifoam bag r
56. get access to the instrument functionalities and settings see Security and user management on page 43 to set these up By default three levels of user have been defined for the instrument and will be required on first access to the instrument me CR Ion Administrator Administrator 09 123 Administrator After setting up your own user list these three default entries should be removed First press Login at the bottom of the screen to access the full login screen Please cr er your SET MATE and passer Ligaen nari First naenie ienticalon number User access ngit IL riurntier Passer aur Ne mma Enter your identification and password in the boxes provided and press Ok to continue Your details will be displayed at the top left corner of the screen Then press the Ok button at the bottom left of the screen to gain access to the main menu There are three user access levels Level Available options Administrator Configuration Calibration Measurement Analysis and Maintenance Manager Configuration Measurement Analysis and Maintenance Operator Measurement and Analysis For security purposes when the session inactivity delay period has expired adjustable using the option Security management on page 43 the user is logged off automatically 32 User Interface and Startup 4 2 5 Rolling list For convenience selection through a possible large list of items has been designed with a rolling li
57. gital elef tere WEE 78 9 0 2 JACIUAtOF Ve MIG allis ere ee Ee Gees 79 9 9 9 Analog value MONIOTINO EE 82 Table of Contents 9 58 Global system LEE 83 GE ESS aa E NEN 83 GR heen e io 9 Reese er Eon eee mere Oe wn ea ES 83 96 0 NWIZ ANOS mH EN 84 E Tee e 85 Section 10 TroubleShoollfg n ttp retten diia 87 10 1 Error and warning messages TT I TU ETE 87 10 171 Eror THeSSQOBS cedet ee EE 87 IA a E a 88 IOMA medqbED sS onstartup SCI EE 89 10 154 MEASUTEMENE proble has EE 90 Section 11 Spare Parts and Accessories nnns 91 Section 12 Material Safety Data Sheets MSDS 93 12 7 mcon antiiOaMm part DniumDber39150 uote nr Mn dr ui en Hb due Ba uc 93 Table of Contents Section 1 General Information 1 1 About this manual The information in this manual has been carefully checked and is believed to be accurate However Hach Lange assumes no responsibility for any inaccuracies that may be contained in this manual In no event will Hach Lange be liable for direct indirect special incidental or consequential damages resulting from any defect or omission in this manual even if advised of the possibility of such damages In the interest of continued product development Hach Lange reserves the right to make improvements in this manual and the products it describes at any time without notice or obligation Copyright 2009 by Hach Lange All right
58. he chamber 24 Installation 3 8 Oxygen sensor preparation and installation 3 8 1 Oxygen sensor preparation Your A1100 electrochemical sensor has been thoroughly cleaned and tested at the factory before shipment It has been shipped with a cartridge containing a membrane and electrolyte pre installed to protect the sensor head This cartridge must be removed see Oxygen sensor removal process below and replaced with a new one prior to first use to make it fully operational The new cartridge is included in the sensor recharge kit supplied with the instrument The sensor recharge kit also contains two protection caps one with a grille Cy and one without Ensure you use the protection cap with a grille illustrated o right for this instrument The sensor should be made operational before being installed in the instrument To do this follow the detailed instructions in Section 4 1 Sensor preparation of the ORBISPHERE Model A1100 User Manual supplied with the instrument Should you have any questions your Hach Lange representative will be pleased to help 3 8 2 Oxygen sensor removal To remove the oxygen sensor following these simple steps 1 With the plastic front door still removed and the measurement head at its lowest position unscrew the two screws No 1 in the diagram below holding the small sensor access panel and remove it to reveal the sensor i H A D AS AT Eh wae ni Gei 25 I
59. identification and access level on page 32 to continue Provided all startup checks were successful the measurement screen will be displayed If there are errors encountered on startup that mean the instrument cannot function correctly a warning screen will be displayed indicating the next course of action Please wait Instrument auto check Boards CH 07 sensor Sensor aut he system iz not funcional Plrase fix the problern and initialize he irrsIruenerm Main board rl Press Shp al to go to Maintenance menu Operabig 5 EL board gt Val Control board sink 40 08 i Skip all al zl AT H KR In the above example the recommended action is to press the Skip all button which will then take you to the maintenance screen so the problem s can be diagnosed and corrected You may be required to enter a valid identification number and password to access the maintenance screen 30 User Interface and Startup 4 2 1 Instrument options A footer banner will be displayed on each screen showing the options available Press the Standby button to leave the instrument in operational mode if there is a long time delay between measurements In this mode and if automatic operation settings have been configured see Sensor configuration on page 50 the system performs verification processes in order to guarantee the instrument status and therefore the quality of the package analysis The screen will go blank
60. illustrated below right Carefully clean the head with a damp tissue to remove all traces of grease and liquid residue Place a new gasket on the piercing head Shut off the forcing gas to allow easier manipulation of the needle assembly Next slide the piston up illustrated below left to reveal the needle assembly and piercing tip illustrated below right side CAUTION A The piercing tip is very sharp Do not push from underneath but hold the piston from the 6 Unscrew the piercing tip at the bottom of the needle assembly and replace it with a new one The new tip should be screwed in finger tight then using a piece of tissue paper to protect the tip tighten with a pair of small pliers olide the piston back down to hide the needle Turn the forcing gas back on and raise the piercing device back to its upmost home position Refer to Home position on page 79 if you are unsure how to do this Maintenance 9 8 Maintenance menu overview Digital input verification Actuator verification Home position Manual displacement Ultrasound ON OFF Lasers ON OFF Anti foam system Activation time zi Injection number Analog value monitoring M Temperature Pressure GOZ concentration Flow Current Temperature sensor Global system view O2 calibration valve Gas calibration valve Reference volume valve Main purge valve Needle purge valve Ultrasound Flow regulation Manual displacement Proportional valve
61. iring the instrument in contravention of these principles could cause damage to the instrument and corporal injury to the person carrying out the repair It renders the warranty null and void and could compromise the correct working of the instrument and the electrical integrity or the CE compliance of the instrument If you have any problems with installation starting or using the instrument please contact the company that sold it to you If this is not possible or if the results of this approach are not satisfactory please contact the manufacturer s Customer Service 1 2 3 Instrument switches and buttons The mains power switch is located at the rear left of the instrument No 2 in Figure 3 on page 15 To switch the instrument on and off press the rocker switch to the required position O for Off and I for On The measurement button is located at the front right of the instrument No 5 in Figure 2 on page 14 Press this button to start a package measurement General Information 1 2 4 Precautionary labels Read all labels and tags attached to the instrument Personal injury or damage to the instrument could occur if not observed This symbol when noted on a product indicates a potential hazard which could cause serious personal injury and or death The user should reference this instruction manual for operation and or safety information This symbol when noted on a product enclosure or barrier indicates that a ri
62. ish DGA1100 MAN F A1100 Manual in French DGA1100 MAN J A1100 Manual in Japanese 91 Spare Parts and Accessories 92 Section 12 Material Safety Data Sheets MSDS 12 1 Silicon antifoam part number 33156 PRODUCT AND COMPANY IDENTIFICATION PRODUCT NAME Silicon antifoam emulsion 3096 in water Hach Lange SA 6 Route de Compois COMPANY Case Postale 212 CH 1222 V senaz Switzerland PHONE NO 0041 22 594 64 00 COMPOSITION INFORMATION ABOUT THE COMPONENTS INGREDIENT CAS NO PERCENT HAZARDOUS Silicone antifoam emulsion N A 70 No Water 7732 18 5 30 No IDENTIFICATION OF HAZARDS SPECIAL INDICATION OF HAZARDS TO HUMANS AND THE ENVIRONMENT Not hazardous according to Directive 67 548 EEC FIRST AID INHALATION If inhaled remove to fresh air If breathing becomes difficult call a physician INGESTION If swallowed wash out mouth with water provided person is conscious Call a physician In case of contact immediately wash skin with soap and copious amounts of water OVERVIEW SKIN CONTACT In case of contact with eyes flush with copious amounts of EYE CONTACT water for at least 15 minutes Assure adequate flushing by separating the eyelids with fingers Call a physician FIRE FIGHTING MEASURES FIRE EXTINGUISHING MEDIA Suitable Water spray Carbon dioxide dry chemical powder or appropriate foam SPECIAL INFORMATION Wear self contained breathing apparatus and protective clothing to preven
63. ition This can be useful if for some reason the piercing device has not returned its home position e Freeze will stop the piercing device if the initialization button has been pressed 79 Maintenance 9 8 2 2 Manual displacement This option allows you to test the movement of the piercing assembly LX UM Select the operation you wl Io to perform Informations Current posan Zog reference position End af travel upper bound End of travel lover bound Select from e UP e DOWN e Speed Press on the UP button to move the piercing assembly up or on the DOWN button to move it down The current position is displayed as the assembly moves up or down Note The longer you press on the button the further the piercing assembly will move in the requested direction Pressing continuously on the UP button will take the assembly to its home top position and pressing continuously on the DOWN button will take it to its lowest position It is advisable to check the process using the three different speed settings low medium and high by toggling the speed with the Speed button 9 8 2 3 Ultrasound ON OFF owitch between having the ultrasound system on or off Important Note Before turning ON remove any pierced packages from the package holder to avoid any liquid spillage With some water in the base of the package holder test the system is working by moving your finger across the base of the package holder and toggling
64. kage by selecting the box at the top of the screen and entering a free format alphanumeric package description e Comment Enter a free format alphanumeric text This text will appear against the package description in the main package management screen e Brimful volume Enter the volume of the package when full to overflowing e Height Enter the overall height of the package This information is used if you activate the Package size check option in Measurement output on page 41 e Tilt position Enter the tilt position of the package holder optional e Peck backstop Position of the package backstop optional The backstop is calibrated on a scale of zero to seven e Package type Select from a scrolling list of images the one that most resembles the type of package being measured bottle can etc Note The above reference values are displayed at the start of the measurement process once a package has been selected so the operator can adjust the instrument accordingly tilt position etc 38 Configuration Alarms tab Index D Mame Package 1 Product Package Alarms Min Max LI POI 00 100 mg O Liquid vol Doug foo 00 my noc bom 2000 100 my 70 002 jCO2Twa o0 100 mg C Formato O 02 Lig 00 in mg O Formula 2 peoks o0 00 mg Formulas 1co2PT 000 000 yg O Formula HS Valume nn aon mi C Formula 5 e Name Change the name of the package by selecting the box at the top of the
65. leave the calibration running for 20 30 minutes before accepting the calibration 5 If the calibration cannot be performed an error message will be displayed giving the reason Verification 1 The process is exactly the same as for a new calibration but once the details have been displayed on screen press the Cancel button to complete the process No report is produced 6 9 Carbon dioxide sensor 60 After selecting this option the details of the last carbon dioxide sensor calibration are displayed This shows the values recorded and information about who performed the last calibration and when The due date of the next calibration is also shown determined by the parameters entered in Sensor configuration on page 50 There is the option of starting a new calibration or viewing the last 10 carbon dioxide calibration reports see Calibration reports on page 62 e Last calibration value set cnetticienit oe Coefficient Calibration que 1 puny Calibrabi n gas 2 puriby ge Measurement ztshlty Gas 2 Measurement stability F Ene lemperature Liser nam Jones User IL 1004 Calibration date 24 04 09 01 74 00 FM Calibration due date Amm Ag The CO sensor needs to be calibrated approximately once every 3 months and is calibrated using near pure CO purity gt 99 5 which may already be supplied as the forcing and purge gas You can also perform a two point calibration using a second supply of gas that has a known bu
66. ll automatically perform a sensor calibration on the defined date and time see also note below The LED indicator on the top right of the header banner will turn red if the calibration failed for any reason Auto verification When set the system will automatically perform a sensor verification on the defined date and time see also note below The LED indicator on the top right of the header banner will turn red if the verification failed for any reason Important Note Both the auto calibration and auto verification processes will only be started when the system is in standby mode Standby mode can be triggered manually by the user or after an automated system log off 50 Configuration Press the Frequency selection button to set the desired frequency Stat tme When Idle far f mim Frisquency pater O Weed D gb Monthly every of every um month O Yearhy amp every ist sl Sunday sl of every le month e Choose between Weekly Monthly or Yearly by pressing the appropriate radio button e With the Weekly option define the day of the week when the operation will take place e With the Monthly option define e The date and monthly interval e g every 15th day every 3 months or e The day and monthly interval e g every 1st Sunday every 2 months e With the Yearly option define e The date and month e g every 1st February or e The day and month e g every 2nd Saturday of July Note With the automatic cali
67. lter 88 Troubleshooting 10 1 3 Red LED s on startup screen Switch analyzer off wait 10 seconds and switch back on If the LED is still red contact your Hach Lange representative O sensor No communication between sensor and board Check connection of the oxygen sensor Check gas purity and gas connections Check sensor protection cap positioning Wait until a residual 0 1 mbar is reached Bad communication between boards This may Boards happen when switching the analyzer on Monitor the sensor behavior in the Global System View screen see Global system view on page 83 Oz sensor residual O2 concentration is not below residual threshold perform a sensor maintenance necessary for the too high 0 1 mbar initial start up Note A high residual value will also affect the TC sensor readings and may cause them to go out of bounds The problem with the TC sensor readings will self correct as the residual value returns to normal Check sensor voltage on the analog value monitoring screen see Analog value monitoring on No communication between sensor and board page 82 Sensor damaged Perform a calibration Check validity of the calibration standard Replace sensor if values are out of range TC sensor Check sensor voltage on the analog value monitoring screen see Analog value monitoring on No communication between sensor and board page 82 Sensor damaged Perform a calibration Check
68. ng and rotating it until it is free from its location 9 4 2 Antifoam cartridge replenishment 72 A replacement cartridge can be used or the existing cartridge refilled with antifoam If refilling the existing cartridge follow the instructions given in Antifoam cartridge preparation on page 22 Important Note To ensure the performance and reliability of the instrument it is strongly recommended to only use the silicon antifoam supplied by Hach Lange part number 33156 Maintenance 9 4 3 Antifoam cartridge installation 1 Fitthe cartridge back in place by lining up the two fluid connectors chamber connector shown as No 1 in the diagram cartridge connector as No 2 2 Press down gently and twist slightly if necessary until the cartridge clicks into place No 3 in the diagram with the two connectors located towards the back 3 Attach the two connectors No 4 in the diagram to the pump leads inside the chamber no specific polarity 4 Return the small door to its original location and close to secure the chamber The plastic front protection door can now be put back in place by lowering it down over the instrument ensuring the rollers are correctly located inside the slots on each side CAUTION Ensure the rollers are correctly positioned inside the slots before slowly and carefully lowering the door Incorrect positioning and or forcing the door down could easily damage the exterior housing of the instrument
69. nnconcnonnnoconononnnoncnonnnnonononannnnnnos 25 3 8 1 Oxygen sensor Dreparaion enne nnn ktr ke sne nsn nnne nne ana nn 25 302 OXYden Sensor Te mov alcaldia 25 3 8 3 Oxygen KEE Ee n EE en BEE 26 3 9 Prime the antfoam TUBING EE 27 SO RUMMNSTUMENCAUOCNECK aren a a 28 Section 4 User Interface and Startup oooococcoocccccococcnoconononoconoonnonccononnnccononcnnnononnnnnnonnnos 29 T USER ne er EE 29 SEH MAS UMTS ergeet EE 29 EZ ANS TUNEL Stan idea 29 EZ Instrument ODUOFIS Ee dE 31 422 TOUS TCO E mmm 31 4 2 9 NAMA ICV DOAN A A A A 31 4 2 4 User identification and access level ooccocccocnconncocicocnnornnornnocnoncnonnnnnnoconocarnnnronarnnnnnnns 32 Se le el 33 A20 WANNA ei le elle i r DIEI EE 33 4 5 Mena Structure OVOVIEW eege d REI E Ra E un 34 E le er ui Le TC Te WEE 35 D Gontigurauor MeN e EE 35 32 IMUSIC Be UNO EE 36 SLM O EUER SNL UU EUER 36 LAL Miele cai 36 Table of Contents 5 9 PACKAGE parameter A 37 9 9 1 Package EE EE 37 9 9 2 FO MUI Mana EE 39 D at dg ewe E E EE 41 94 1 Measurement er E E 41 942 le Ee Ko EE 42 ES A 42 5 5 Security arid user management iii A A A A ies 43 5 5 1 ele e En ER 43 9072 User un El Ee E EE 44 Pss fae 210 To sc eet od 45 2 06 COMMUNICATOR MR aen rese eee m E 46 9 6 1 Data download Keele tel Een EE 46 5 6 2 Web browser copnfguraton nennen nennen nnne nnne nsn rns snas 48 9 Senso COMMU AO gue s cod tue atl chalet elena Me a ee cn le net 50 SECTI
70. nstallation 2 Disconnect the sensor cable standard LEMO 10 plug in connection at the top of the sensor No 2 in the diagram and unscrew the sensor locking nut No 3 in the diagram below The sensor can now be removed from its position 3 8 3 Oxygen sensor installation Once the sensor is operational it must then be re installed in the instrument 1 With the plastic front door and the sensor access panel still removed and the measurement head at its lowest position insert the sensor into the sensor socket No 1 in the diagram below and screw the locking nut No 2 in the diagram below finger tight to hold the sensor firmly in place Connect the sensor cable to the top of the sensor No 3 in the diagram below using the standard LEMO 10 plug in connection and hand tighten the cable collar 2 Replace the sensor access panel and secure in place with the two screws 3 The plastic front protection door can now be put back in place by lowering it down over the instrument ensuring the rollers are correctly located inside the slots on each side 26 Installation CAUTION Ensure the rollers are correctly positioned inside the slots before slowly and carefully lowering the door Incorrect positioning and or forcing the door down could easily damage the exterior housing of the instrument 4 Manually raise the piercing device back to its upmost home position Refer to Home position on page 79 if you are unsure how to do this
71. on in this document is based on the present state of our knowledge and is applicable to the product with regard to appropriate safety precautions It does not represent any guarantee of the properties of the product PRODUCT USE For laboratory use only Not for drug household or other uses The information in this sheet is believed to be correct at the time of printing The details should be reviewed periodically and should be checked for special uses 95 Material Safety Data Sheets MSDS 96 97 GI LANGE UNITED FOR WATER QUALITY
72. r the liquid to the cartridge 100mL volume syringe tubing and connectors Important Note To ensure the performance and reliability of the instrument it is strongly recommended to only use the silicon antifoam supplied by Hach Lange part number 33156 3 7 1 Antifoam cartridge preparation To fill the cartridge proceed as follows numbers in the boxes correspond to the steps 1 Connect the syringe to the tubing with the quick connector 2 Unscrew the cap from the antifoam recharge bottle and put the tubing in making sure it goes as near to the bottom of the liquid as possible Pull on the syringe to extract the liquid until the syringe is full Remove the syringe and tubing from the recharge bottle 5 Attach the end of the tubing from the syringe to the other piece of tubing using the quick fit connector 6 Remove any trapped air in the system by applying a small amount of pressure to the end of the connector with a small screwdriver or similar to open the valve Push slightly on the end of the syringe until antifoam can be seen dripping out of the end of the connector Remove the screwdriver 22 Installation T Attach the end of the second piece of tubing to the antifoam cartridge by pressing until the connector clicks into place on the inlet valve Then push on the end of the syringe to empty the contents into the cartridge The syringe has a volume of 100mL and the cartridge a volume of 280mL so repeat the
73. raban HO YES Formula HO YES Faer dala NEC YES E IE Emu Scroll through the list of available data files using the up down arrow keys on the right and select if the file to be exported is in data or text format By default the text format is set to YES and the data format to NO Set both formats to NO if you do not require the file downloaded Use the Invert Selection button under each column to toggle between YES and NO Note It is recommended to set the files to text format for easy loading into standard software applications on the PC such as Microsoft Excel or similar The data format is only required for Hach Lange service and support personnel When the data formats have been configured select Ok to confirm The following files can be transferred e Audit trail Audit trail txt e Calibration files Calib Barometer txt Calib CO2 txt Calib Flow txt Calib O2 txt Calib Pressure txt and Calib Temperature txt e Liquid Liquid txt e Package Package txt e Result Result txt e Configuration Configuration txt e Formula Formula txt e Raw data Raw data txt Configuration To transfer the data files plug an external mass storage device such as a USB memory stick into one of the two USB A ports at the rear left of the instrument The instrument will recognize the presence of the device and the following screen will be displayed as the files are automatically copied USB data oem USB dece found Progress Less than a
74. recision certified barometer measure the barometric pressure in the location where the instrument is used and compare the values If values are the same press Cancel otherwise enter the new barometric value in the lower box and press Validation to store the new setting 3 Once the calibration is completed a calibration report is created 54 Calibration 6 5 Pressure sensor After selecting this option the details of the last pressure sensor calibration are displayed This shows the values recorded and information about who performed the last calibration and when The due date of the next calibration is also shown determined by the parameters entered in Sensor configuration on page 50 There is the option of starting a new calibration or viewing the last 10 pressure sensor calibration reports see Calibration reports on page 62 Important Note This procedure uses information from the barometric pressure sensor Be sure that this parameter is reliable i e a recent barometric pressure sensor calibration has been performed see Barometric pressure sensor on page 54 Ing Sese Last Cai bration value cope rrib an volt L tzet mbar Pressure 1 mbar otablity meas 1 7h Pressure 7 l rritar otabdity meas 2 Te Liser name Jomes User IL TUH Calibration date 20 04 09 10 15 00 AM Calibration due date 00 00 00 1 Start a new calibration by pressing the New calibration button A calibration screen is displayed and the
75. regulating valve is then opened and the gas escaping the liquid mixes with the gas of the headspace The O signal is an exponential function to which coefficients can be included and the total O5 contained in the bottle is calculated by integrating this function 4 Headspace volume At the end of the run the gas flow is stopped and the valve is opened The gas of the reference volume expands in the headspace and the pressure reaches a new value The headspace volume is calculated with the ideal gas law principle 5 End of measurement The piercing head assembly is lifted out of the package A short burst of gas purges the gas sampling path to flush out any residual liquid or foam The system returns to the standby mode where the sensors are kept under a slight purge gas flow 17 Specifications 18 Section 3 A Installation WARNING This section provides necessary information to install and connect the instrument The installation of the instrument should be performed in accordance with relevant local regulations Disconnect the power supply of the instrument before carrying out any work inside the instrument Any work inside the instrument should be performed exclusively by personnel specialized and authorized to work on electrical installations In addition and in accordance with safety standards it must be possible to disconnect the power supply of the instrument in its immediate vicinity CAUTION Proper ESD electros
76. rocedure uses information from the pressure sensor Be sure that this parameter is reliable i e a recent pressure sensor calibration has been performed see Pressure sensor on page 55 Last calibration value Coefficnt A 1043 CGoslhecent E Ab Coatmcsant C 057 Measurement E stabikty D OD Measurernent Z statt DUR Measurement 3 stabikby D OD User name Jones User IL 1004 Calbrabon date 20 04 08 1101500 AM Calibrati n due g 00 00 00 New calibration 1 Start a new calibration by pressing the New calibration button A calibration screen is displayed 2 The instrument will then compute the measured flow in four steps at 0 200 ml s 0 400 ml s 0 800 ml s and at 0 000 ml s The results are displayed on screen Current va Pressure mbar Elasped time Second Temperature Le Measured values Deta P mbar Detat Second lic mas step 4200 mis Step 7 400 mis Step 3 0 3900 mis step 4 0 000 mibg 3 After a few minutes when the process is complete the Validation button is highlighted Press this button to accept the calibration you will need to confirm acceptance 4 Once the calibration has completed a calibration report is created Verification 1 The process is exactly the same as for a new calibration but once the details have been displayed on screen press the Cancel button to complete the process No report is produced 57 Calibration 6 7 Temperature sensor After selecting
77. s You will then need to select the new package and edit these default parameters to define the new package parameters To edit or delete a package first select the package from the list displayed by touching the package name on the screen and then press either Edit or Delete as appropriate lf Delete was selected confirm the deletion to delete the package from the list lf Edit was selected a new screen is displayed to allow you to change the definition of the package Select each tab in turn to define the package definitions 37 Configuration Product tab Package Product Package arme Solubiity Water Formula selecbon Formula 1 Temp average Formula 7 Mong m F rrraula 3 None T Formula 4 None T F rrrula 5 Hone e Name Change the name of the package by selecting the box at the top of the screen and entering a free format alphanumeric package description e Solubility Enter the type of beverage in the package e Formula Define up to five different formulae to apply to a measurement for computing a new parameter The formula definitions must have been first entered into the system see Formula management on page 39 for details Package tab Edit package Index D Package 1 Product Package Alarme Comment ied light bgt Package type kern 3 Brimful val 330 00 mi Hewght 18000 mm Tilt position Pck backstop e Name Change the name of the pac
78. s grise you need ask your network administrator for appropriate IP settings Use these IP setings IP address Subnet mask Deiaut gateway This option allows you to set up an Ethernet connection to download data or system configuration details from the instrument directly to a web page that can be accessed from a PC To be able to use this option the instrument must be connected to the network Access the information by launching an internet browser on your PC and typing http followed by the device name assigned to the instrument see screen above The home page will then be displayed sh LR D Windies Interest Ietkre p uude dj wl St 8 chi D LECT ei A dg Mach pride being ana avsilzurmntaton for mde rage ol ullra pure eter and utra pure ar pt Siten n tha deveria Dectrensct imbustital ite Scweveg add Poser Cans tem ir Ag d trusbed partner sw earn the total confidence of Dur customers Dy prowiding them posce of mad trough mue arca Bol onm and proc Hort perform accurately and aad A commitment to research and reat ees us be hen Gu Ani mess Te gien anil cpimrm ugly engin Meee FE eit Excellence in Process Analytics Hach o 5 49d m dele erg Ue bei sole squat momstarew and preci abria workin CHE riberas and coupl ef Gobel pernos acpurtie for beverage aectrinea etai Me cana ke pime parra don AED abona rh loca offica amd authored Genter opsr kw e mona cha Di coute around the work eur Got a a ada
79. s reserved No part of the contents of this manual may be reproduced or transmitted in any form or by any means without the written permission of Hach Lange 1 2 Safety information Please read the entire manual before unpacking setting up or operating this instrument Pay particular attention to all warning and caution statements Failure to do so could result in serious injury to the operator or damage to the equipment To ensure the protection provided by this equipment is not impaired do not use or install this equipment in any manner other than that which is specified in this manual 1 2 1 Use of hazard information WARNING A warning is used to indicate a condition which if not met could cause serious personal injury and or death Do not move beyond a warning until all conditions have been met CAUTION A caution is used to indicate a condition which if not met could cause minor or moderate personal injury and or damage to the equipment Do not move beyond a caution until all conditions have been met Note A note is used to indicate important information or instructions that should be considered before operating the equipment 1 2 2 Service and repairs None of the instrument s components can be serviced by the user Only personnel from Hach Lange or its approved representative s is are authorized to attempt repairs to the system and only components formally approved by the manufacturer should be used Any attempt at repa
80. screen and entering a free format alphanumeric package description e Alarm parameters Select the parameter for which you want to change the alarm settings and enter the minimum and maximum values allowable for each parameter listed When the measurement value falls below the minimum level and or exceeds the maximum level for any parameter listed an alarm will be triggered 5 3 2 Formula management This option allows you to add new formula definitions up to a maximum of 40 and edit or delete existing definitions You can use up to 14 variables pre defined by the instrument and 2 user defined numerical variables that can be set up manually at the end of each measurement These values can be entered into the Num 1 and Num 2 fields of the comments section on the measurement results screen see example measurement screen on page 67 When the option is selected a screen will be displayed listing all existing formulae Fonmula management Hp Formula name F Temp average Temperature liquid Temperature ECHO 2 ero Or 02 be qu total The Info button can be used to display information about the selected formula such as the operator who created it the date and time of creation or the last edit and any comments associated with it 39 Configuration New formula Press the New button to create a new formula The formula editor screen is displayed Use the editor to define a formula The measurement values
81. sk of electrical shock and or electrocution exists and indicates that only individuals qualified to work with hazardous voltages should open the enclosure or remove the barrier This symbol when noted on the product indicates that the marked item can be hot and should not be touched without care This symbol when noted on the product indicates the presence of devices sensitive to electrostatic discharge and indicates that care must be taken to prevent damage to them This symbol when noted on the product identifies a risk of chemical harm and indicates that only individuals qualified and trained to work with chemicals should handle chemicals or perform maintenance on chemical delivery systems associated with the equipment This symbol when noted on the product indicates a laser device is used in the equipment This symbol if noted on the product indicates the need for protective eye wear This symbol when noted on the product identifies the location of the connection for protective earth ground Electrical equipment marked with this symbol may not be disposed of in European public disposal systems In conformity with European local and national regulations European electrical equipment users must now return old or end of life equipment to the manufacturer for disposal at no charge to the user Products marked with this symbol indicates that the product contains toxic or hazardous substances or elements The number inside the s
82. st as in the example below Use the up and down arrows at the side to navigate or select one item directly and press Ok Formula 2 Formula 3 Pressure calibration with two paints o ra ees SES We ege PET Store mew Calibration parameters Mom en eA i At various stages a warning message may be displayed to request confirmation from the operator that his last action s must be applied or that there is a problem that did not enable the requested action to be performed Note Warning messages can be suppressed by unchecking the Warning messages parameter in Measurement output on page 41 For a full list of all possible warning and error messages and the recommended action to take please refer to the section entitled Troubleshooting on page 87 33 4 3 Menu structure overview User Interface and Startup JOSUOS aunssaud augeuogeg LOPES PGA om JOSUOS majd weped Auenbaly LONE eS ony Josuss DNI L awn mies Josuas ansia 108008 709 105008 ZO Geng info Josuos uonginBijuoa 19844010 OM y VOpembyuos peojusop eeg puowossejdas 205 pue dy pos UAW Epa Jayy 010105 Baoaueuajuieul JO SUS 73 HAS Juge juawose des Beg ueoj nuyr gen Hp SpAJEZIAM juauuaDeugu Aaen uogeardde pug uonezieniu ums s BAJEA jeuorradodsg juswosejdsip enuey uonejnBal mold juoweGeuew yansos quauraBeueu ssn pue yunoas punosen aas aBund appaay BAJEA Bund upep aapea QUINOA 220242494 SAJEA UO EIQIIES SEE BAJRA
83. stomer any old unserviceable or redundant instruments and systems which carry the above symbol and which were originally supplied by Hach Lange Hach Lange will then be responsible for the disposal of this equipment In addition Hach Lange will offer to take back at cost to the customer any old unserviceable or redundant instruments and systems which do not carry the above symbol but which were originally supplied by Hach Lange Hach Lange will then be responsible for the disposal of this equipment Should you wish to arrange for the disposal of any piece of equipment originally supplied by Hach Lange please contact your supplier or our After Sales Service department in Geneva for instructions on how to return this equipment for proper disposal General Information 1 5 Restriction of hazardous substances RoHS The European Union RoHS Directive and subsequent regulations introduced in member states and other countries limits the use of six hazardous substances used in the manufacturing of electrical and electronic equipment Currently monitoring and control instruments do not fall within the scope of the RoHS Directive however Hach Lange has taken the decision to adopt the recommendations in the Directive as the target for all future product design and component purchasing This product is compliant with the European Union RoHS Directive Note The following only applies to exports of this product into the People s Republic of
84. strument parameters select from e Measurement output e Time Date e System information 5 4 1 Measurement output Define the parameters shown on the screen after and during the measurement process Ci Sipps m Prae SAH a vates Display diagnostic result Package se check Warming messages Column selector oke 1 voi HE Come 2 E Total Column 3 e Diagnostic measurement view Use this option to troubleshoot measurement problems If this box is checked then instead of the standard measurement progress screens being displayed during the measurement process the measurement values are displayed instead see example in Measurement view on page 68 e Display diagnostic results Use this option to troubleshoot measurement problems If this box is checked then instead of the standard measurement results screen being displayed at the end of the measurement process more detailed measurement values are displayed instead see example in Results view on page 68 e Package size check If checked the instrument will verify that the package size is the same as that defined in the height parameter for the package being measured If different a warning message will be displayed The height detection resolution is 1 mm e Warning messages If checked any warning messages will be displayed during the package measurement process If left unchecked all warnings will be suppressed For a full listing of possible warnings refer to
85. t Wipe down the instrument with a damp cloth to keep the exterior clean and also paying particular attention to the inside of the transparent front door 9 3 Purge gas cylinder Check the purge gas cylinder daily to ensure there is an adequate supply of gas On no account should the cylinder become empty while the instrument is switched on 71 Maintenance 9 4 Replacing the antifoam cartridge 9 4 1 Antifoam cartridge removal The antifoam cartridge is located inside the measurement head It will need replacing about once every six months but you can check the level by using the option Antifoam system on page 81 part of the Actuator verification menu on page 79 If the lower level button is highlighted replace the cartridge as follows 1 Lower the piercing device to its lowest point it will stop automatically once this point is reached If using the wizard simply press the Do It key on screen If not using the wizard refer to Manual displacement on page 80 for details 2 Remove the plastic front protection door by carefully raising it up on its rollers and over the top of the instrument to give access to the antifoam cartridge location 3 Open and remove the small front door No 1 in the diagram for easy access to the antifoam cartridge chamber Disconnect the two pump leads No 2 in the diagram 4 With a pen or similar push in the latch to release the cartridge No 3 in the diagram Remove the cartridge by raisi
86. t lower concentration of CO e g purity of 9596 Perform the calibration as follows Calibration One point calibration 1 Start a new calibration by pressing the New calibration button A calibration screen is displayed showing the latest gas purity data of the main gas The Main gas radio button will be highlighted at the bottom of the screen CO tir Cab atb TC first calibration da Gas read purty as Tiv Stability 535 purity Calbrabon mnfarmaban User name User IL Calibration date 39 04 2009 OF 23 47 a Main gaz O Second calibraban gaz 2 Ifthe value of the gas purity for the main gas is incorrect enter the correct value in the Gas purity box 3 Press the Validation button A message will be displayed warning you that this is a one point calibration CO tena calibration IC first Calibration gas Gas read purity Bo 3 in Gas flaw ho UE Stability poa y JN One value cakbration enabled Gas purity Calibration information User name User IC Calibration date 28 04 2008 07 23 42 a Main gas O Second calibration as 4 Press the Validation button at the bottom of the screen to accept the new calibration Once the calibration has completed a calibration report is created Two point calibration 1 Proceed as for a one point calibration steps 1 to 3 above 2 Do not press the Validation button at the bottom of the screen but select the Second calibration gas radio button and att
87. t contact with skin and eyes MEASURES IN CASE OF SPILLAGE Wash spill site with soap solution Flush spill area with copious amounts of water Absorb on sand or vermiculite and place in closed containers for disposal HANDLING AND STORAGE Directions for Safe Handling Avoid inhalation Avoid contact with eyes skin and clothing Avoid prolonged or repeated exposure Conditions of Storage Keep tightly closed EXPOSURE CONTROLS INDIVIDUAL PROTECTION ENGINEERING CONTROLS Safety shower and eye bath Mechanical exhaust required GENERAL HYGIENE MEASURES Wash thoroughly after handling PERSONAL PROTECTIVE EQUIPMENT Eye Protection Chemical safety goggles Material Safety Data Sheets MSDS PHYSICAL AND CHEMICAL PROPERTIES APPEARANCE Color White Form Turbid viscous liquid BEEN m At temperature or pressure 6 5 7 5 A range 100 C 760 mmHg MP MP range 1 0 C Flash point N A Flammability N A Autoignition temp N A Oxidizing properties N A Explosive properties N A Explosion limits N A Vapor pressure N A SG density 0 999 g cm Partition coefficient N A Viscosity N A Vapor density N A Saturated vapor conc N A Evaporation rate N A Bulk density N A Decomposition temp N A Solvent content N A Water content N A Surface tension N A Conductivity N A Miscellaneous data N A Solubility N A TOXICOLOGICAL INFORMATION ACUTE TOXICITY e Oral Rat gt 5 000 mg kg LD50 Skin Rat gt 2 000 mg kg SENSITI
88. tatic discharge protocols must be followed to prevent damage to the product when working with the electronic boards 3 1 Unpacking CAUTION The instrument is heavy 55 kg so extreme care must be taken with handling to avoid damaging the instrument or inflicting personal injury It is highly recommended to have two people remove the instrument from the box In addition the instrument should always be moved and stored in a vertical position Carefully remove the instrument and its accessories from the box and packing material referring to the packing list included to confirm that everything has been delivered Please visually inspect the instrument for shipping damage If anything is missing or damaged contact the manufacturer or your dealer immediately You may want to retain the box and other packing material in case you later need to ship the instrument Please dispose safely and ecologically of the box and packing material if not stored for future use Please read through this manual thoroughly before carrying out the installation 3 2 Main components Your 6110 Total Package Analyzer is shipped with the following components Equipment included 6110 instrument O EC sensor pre installed Antifoam cartridge empty Antifoam recharge bottle 1L Syringe for anti foam cartridge Anti foam priming vessel Kit of 4 pre filled cartridges with premounted 2956A membranes for O sensors Filter with Gore Tex membrane Piercing tip
89. the EC sensor please refer to the accompanying ORBISPHERE Model A1100 User Manual After servicing insert the sensor back into the sensor socket and secure with the sensor collar finger tight to hold it firmly in place Connect the sensor cable to the top of the sensor using the standard LEMO 10 plug in connection and hand tighten the cable collar Replace the sensor access panel and secure back in place with the two screws The plastic front protection door can now be put back in place by lowering it down over the instrument ensuring the rollers are correctly located inside the slots on each side CAUTION Ensure the rollers are correctly positioned inside the slots before slowly and carefully lowering the door Incorrect positioning and or forcing the door down could easily damage the exterior housing of the instrument 9 Manually raise the piercing device back to its upmost home position Refer to Home position on page 79 if you are unsure how to do this Maintenance 9 6 Gore Tex filter replacement The Gore Tex filter is located under the measurement column and should be replaced every three months 1 Lower the piercing device to its lowest point it will stop automatically once this point is reached If using the wizard simply press the Do It key on screen If not using the wizard refer to Manual displacement on page 80 for details Remove the plastic front protection door by carefully raising it up on its rollers
90. the switch between ON and OFF You should sense a noticeable difference 9 8 2 4 Laser ON OFF owitch between having the laser lights on or off Test the system is working by toggling the switch to ON and you should see the two red laser beams intersecting on the package holder Toggle the switch back to OFF and the laser beams should disappear 80 Maintenance 9 8 2 5 Antifoam system Use this option to test that the antifoam injector system is working to purge the system before an extended stand by several weeks or when performing start up procedures Follow these instructions 1 Anantifoam priming tool is available from the spares kit delivered with the instrument Place this on the ultrasonic base of the instrument using the lasers to center it illustrated below left and lower the plastic front door illustrated below right 2 Activate the motor to lower the instrument head allowing the needle to penetrate approximately to the center of the priming tool illustrated below Refer to Manual displacement on page 80 for details on lowering the instrument head 81 Maintenance 3 Select the Antifoam system option from the Actuator verification screen and enter e Activation time Enter the activation time in milliseconds e Injection number Enter the number of injections Antitcam pump system Push the button to inject antifaor constantly Antifaarm pump parameters ACEN tme Ijecbon number informations
91. unt of antifoam After measurement ensure the sample is disposed of in a sink or similar to avoid any risk of ingestion Refer also to the material safety datasheet MSDS Silicon antifoam part number 33156 on page 93 for additional antifoam safety information 1 3 Product recycling information ENGLISH Electrical equipment marked with this symbol may not be disposed of in European public disposal systems after 12 August 2005 In conformity with European local and national regulations EU Directive 2002 96 EC European electrical equipment users must now return old or end of life equipment to the manufacturer for disposal at no charge to the user Note For return for recycling please contact the equipment manufacturer or supplier for instructions on how to return end of life equipment for proper disposal DEUTSCH Elektrogerate die mit diesem Symbol gekennzeichnet sind d rfen in Europa nach dem 12 August 2005 nicht mehr ber die ffentliche Abfallentsorgung entsorgt werden In bereinstimmung mit lokalen und nationalen europ ischen Bestimmungen EU Richtlinie 2002 96 EC m ssen Benutzer von Elektrogeraten in Europa ab diesem Zeitpunkt alte bzw zu verschrottende Gerate zur Entsorgung kostenfrei an den Hersteller zur ckgeben Hinweis Bitte wenden Sie sich an den Hersteller bzw an den Handler von dem Sie das Ger t bezogen haben um Informationen zur R ckgabe des Altger ts zur ordnungsgem en Entsorgung zu erhalten
92. uomneJqies zo mara WNAE jeqoio VO ELO waag Guvoyuow an ea Goyeuy Joquinu ose awn VONLANIY indino juswaunseoy SI0J0wEeJed uewungsu Vogt L n sojenja vogue induy e 610 UMUS EUEU E MIO y sumas age Cep uad sJajaugjed aDgyagg ua uaBieguegu abeyoeg 3080608 Z0 Josuas anjgjadura y JOSIE MO aoupgua gunssasd pansew JOSLIOS GJITSSOJg REIR uongajuaauo2 ZO 00 0309 pue sy 306008 euns saJd AUOT an EA saweg MIN 34 Section 5 Configuration 5 1 Configuration menu overview O2 concentration CO2 concentration Length Temperature Volume Pressure Quantities Formula resolutions only Units and resolutions Package manageme Package parameters Package Formula management New Edit Delete Instrument parameters Measurement output Diag measurement view Display diag results Package size check Warning messages Column selection Time Date System information Security and user management p Security management Access rights enabled Auto logoff Audit trail Logout timer Clear audit trail file User management Audit trail Communication Data Text format Data download configuration Web browser configuration Device name IP Settings O2 sensor CO2 sensor Pressure sensor Temperature sensor Sensor configuration Service frequency Calibration frequency Auto calibration Flow sensor Auto verification Barometric pressure sensor
93. utton you will be required to confirm the changes or press the Exit button to exit the screen without making any changes Note The maximum number of permitted users is 99 5 5 3 Audit trail This option allows you to view the list of user actions performed on the instrument Audit trod report 1 13 of 28 KSC SE TE 13 0 AM 71 04 2008 08 13 08 S ms 17 04 2008 08 05 03 AM 1552 fR d 17 04 2009 MESS OTe baaa 07 55 44 P 17 04 3009 07 54 08 AM 61715 Prag CR a EE Note The actions are listed chronologically with the latest action always at the top of the list When the maximum of 1 000 recorded actions is reached the oldest is deleted and replaced with the latest Scroll through the audit trail screens using the First Previous Next and Last buttons or select the Exit button to leave this option Note To clear the audit trail file use the option available on the main security screen see Security management on page 43 45 Configuration 5 6 Communication This option sets the parameters required for exporting instrument data files to your PC or USB storage device Select from e Data download configuration e Web browser configuration 5 6 1 Data download configuration 46 UER Data downoad configuration Configure dara download options of fie in sclecti n File name Data format Test format Calbrabon fies HO YES A Liquid HA YES Package Me YES te sul NO YES Conhgu
94. validity of the calibration standard Replace sensor if values are out of range Temperature sensor Check sensor voltage on the analog value monitoring screen see Analog value monitoring on No communication between sensor and board page 82 Sensor damaged Perform a calibration Check validity of the calibration standard Replace sensor if values are out of range Flow sensor Check sensor voltage on the analog value monitoring screen see Analog value monitoring on No communication between sensor and board page 82 Pressure sensor Sensor damaged Perform a calibration Check validity of the calibration standard Replace sensor if values are out of range Cartridge empty Check that both connectors on the bottom of the Anti foam level Level connectors not connected or badly cartridge are firmly in place connected Refill the cartridge if empty Foam detector Ingress of foam or liquid in the sampling tube Activate needle purge in the Global System View screen see Global system view on page 83 Check device function in the Digital Input Verification screen see Digital input verification on page 78 Electrovalves TET Initialize motor position in the Actuator Verification Motor Bad initialization or communication Do screen see Actuator verification on page 79 Check iet function in the Global System View Ultrasound Sonotrode failure screen see Global system view on page 83 89 Troubleshooting
95. ymbol indicates the environmental protection use period in years 1 2 5 Class 1 LASER A Class 1 LASER is installed in this instrument Class 1 LASERS are products where the radiant power of the LASER beam accessible the accessible emission is always below the Maximum Permissible Exposure value Therefore for Class 1 LASERS the output power is below the level at which it is believed eye damage will occur Exposure to the beam of a Class 1 LASER will not result in eye injury Class 1 LASERS may therefore be considered safe However Class 1 LASER products may contain LASER systems of a higher Class but there are adequate engineering control measures to ensure that access to the beam is not reasonably likely This Class 1 Laser product complies with 21 CFR Chapter 1 subchapter J It is evaluated and tested in accordance with EN 61010 1 Safety Requirements for Electrical Equipment for Measurement and Control and Laboratory Use and IEC EN 60825 1 Safety of Laser Products 1 2 6 CFL backlight The CFL compact florescent light used for backlighting the screen display contains a small anount of mercury Please dispose of any used CFL s in accordance with local state or federal laws concerning the disposal of products containing mercury General Information 1 2 7 Use of antifoam Antifoam is injected into the sample as part of the measurement process Once a sample has completed the measurement process it will therefore contain a small amo

ORBISPHERE Model 6110 Total Package Analyzer

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