Operating Manual.
Contents
1. X06L LAM 06 LLM 06 HAM eX06LLINM LXZ9ELHM IXZ9 LHM LXZ9ELHM LXZ9ELHM SS3NHVH 30v4H31NI AH0SS329V LLHM e CX968NM CX968NM CX968INM CX968INM SS3NHVH H313W 7V9 6HM IXL6LLHM 5 IXL6LLHM SSINYYH 8HM 61XHM 61XHM 61XHM 61XHM SS3NHVH AVidSIQ ZHM 9X06LLHM 9X06LLHM 9X06LLHM 9X06 LLHM SS3NHVH QHVOS YJLIW SHM SX06LLHM SX06LLHM SX06LLHM SX06 553 MS 3HfSS3Hd SHM VXO6LLHM VX06LLHM YX06LLHM vX06LLHM SS3NHVH QHVO8 Ivo PHM e X06LLHM X06LLHM X06LLHM X06 LLHM SS3NHVH H3MOd DV EHM ZXOGLLHM ZXOGLLHM SS3NuvH YIMOd 20 ZHM 1X06LLHM 1X06LLHM LXO6LLHM 1X06LLHM SSINYVH LHM Q QION310S AVM E YOS X06L1AH X06LLAH X06LLAH X06LLAH QION310S HSN 08 EZZXIS EZZXIS EZZXIS EZZXIS 195 2X06 5 TXOGLLMS 2X06 LIMS TXOGLLMS HOLIMS 25 1X06LLMS 1X06LLMS 1X06LLMS 1X06LLMS HOLIMS 353451 5 9LIXNL 9LIXNL 9LIXNL 9LIXNL AlddfiS 154 c IXO6HNd 1 1 IXOS HNA dWnd ind IXLGLLIS cmi 116105 a 15 4009 LIINI NAHM G3L93NNO9 149 NO Z SNId ALON 2x9680d 2x9680d 2x9680d 2x9680d 0 wala 0d 06124 TXOGLL2. 13 1 Section 14 Replacement Parts 14 1 Ordering Proced res te 72 condat avt hatte tk the osa 14 3 Flow CATE Buca CARN SCs Reid dap t eae 14 4 Witing Diagrami Ses i I ote a Y sce as ge 14 5 vi Nanopure Analytical Thermo Scientific Section 1 Safety Information Your Thermo Scientific Nanopure Analytical Ultrapure Water System has been designed with function reliability and safety in mind It is the user s responsibility to install it in conformance with local electrical codes This manual contains important operating and safety information The user must carefully read and understand the contents of this manual prior to the use of this equipment For safe operation pay attention to Notes Cautions and Warnings throughout the manual Water purification technology employs one or more of the following chemicals electrical devices mercury vapor lamps steam and heated vessels Care should be taken when installing operating or servicing Thermo Scientific products The specific safety notes pertinent to this product are listed below Warnings To avoid electrical shock always 1 Use a properly grounded electrical outlet of correct voltage and current handling capacity 2 Do not mount your Nanopure Analytical directly over equipment that requires electrical service Routine maintenance of this unit may
3. Tank u 08964 H Float Switch Z Ed 2 D2706 Pressure Switch Figure 8 1 Feedwater Float Pressure Switch Feedwater Float or Accessories D8964 float switch and D2706 pressure switch are designed Pressure Switch o protect the Nanopure Analytical pump by alerting the system of an inadequate feed water condition so that the pump can be shut down If an inadequate feed water condition exists and the pump is shut down due to this condition the display will read Check Inlet Follow the proceeding instructions for installation 1 Disconnect the unit from the electrical power 2 If using the D8964 float switch follow the installation instructions included with the float switch for installation into a tank 3 If using the D2706 low pressure switch install the PVC tee supplied with D2706 in the incoming water line Screw the switch into the top of the tee then connect the inlet tubing of the Nanopure Analytical into the remaining opening of the PVC tee 4 Route the cable from the float or low pressure switch to the top left of the Nanopure Analytical Thermo Scientific Nanopure Analytical 10 1 Section 10 Accessories Feedwater Float or Pressure Sw cont Dispense Overflow Cutoff Float 10 2 Nanopure Analytical 5 Remove the jumper plug from the back upper left portion of the unit and save for future use 6 Plug the cable
4. 1 up or down enter key keys pressed l pressed a oh la 3 Change Units ee dispense key pressed ee ee a Compensation Temperature System flush Auto Dispense Menu Arrow Legend gt Keypress Options ve Automatic Entry YY Menu Wrap around Operational Overview 14 4 Nanopure Analytical Flow Chart up or down enterkey oe keys pressed ka pressed 7 Sanitize Unit Air Purge Depressurize NIST calibrate Reset Timers Advanced menu Optional Printer M Remote Gun Date Format Set Date Set Time Set Cell Constant Set Display Brightness Diagnostics menu Thermo Scientific Section 14 Replacement Parts
5. lt 70 ppm Siea eh a ata aire lt 1 ppm DIE eS vaca NC EP VR RR ES 596 SDI Product Water Water Quality Resistivity gt 18 2 Pyrogen TOC uiuo beer NE VIS wem Pride 5 10 ppb Bacterian cC 0 01 CFU ml Flow Rate Up to 2 L min maximum at minimum inlet feed water pressure 10 PSIG with a new final filter Volumetric Dispense Seuls Listo Du Mice AM La rods t 590 Repeatability xoi on gr aate dines i 396 Nanopure Analytical 3 1 Section 3 General Specifications Electrical Requirements The Nanopure Analytical is equipped with 2 power cords to be plugged into an electrical outlet of the appropriate voltage U K customers use cord CRX100 and fuses for 240V installation Model D11901 100 240 VAC 100 watts 47 63 Hz 1 phase Environmental Conditions Operating 4 C 40 C 20 to 80 RH non condensing Installation Category II over voltage in accordance with IEC 664 Pollution Degree 2 in accordance with IEC 664 Altitude limit 3 500 meters Storage 25 C to 65 C 10 to 85 relative humidity RH Declaration of Conformity We hereby declare under our sole responsibility that this product conforms with the technical requirements of the following standards EMC EN 61000 3 2 Limits for Harmonic Current Emissions EN 61000 3 3 Limits for Voltage Fluctuations and Flicker EN 61326 1 Electrical Equipment
6. 7 Press ENTER 8 Proceed through the options by pressing ENTER until Set Cell Constant is displayed 9 Press the UP or DOWN arrow to select Yes 10 Press ENTER 11 Note that the digits are entered from left to right 12 Press the UP or DOWN arrow to change the blinking digit Once the digit is correct press ENTER to advance to the next digit 13 After all digits have been entered line 2 of the display will read NO Finished 14 If the cell constants displayed on line 1 of the display are correct press the UP or DOWN arrow to select Yes 15 Press ENTER 16 Press BACK twice to return to the Idle mode Nanopure Analytical 9 3 Section 9 User Settings Use of Standby Mode 9 4 Selecting the Set Nanopure Analytical Point At the end of the work day place the Nanopure Analytical in Standby mode for the night To place the unit in Standby mode 1 From the Idle mode when display reads Nanopure Idle xx xx xx xx xx xx press STANDBY OR 2 From the xx x or x xx uS cm operational display Press STANDBY After STANDBY is pressed the display will read Standby and the green LED will slowly blink For 10 minutes of every hour while the pump is energized the display will read Standby Recirculating xx minutes Press START STOP to return to the recirculating mode Note When in Standby mode press START STOP to continue nor
7. missing from post each of the 4 posts must contain an o ring Disconnect inlet water and depressurize system Next disconnect the manifold and verify replace missing o ring Reinstall cartridge pack as indicated in Cartridge Pack Replacement Water is leaking at atmos Tubing not fully inserted Insert tubing into connection until it bottoms out pheric drain connection 13 2 Nanopure Analytical Thermo Scientific Thermo Scientific Section 14 Replacement Parts Consumables Consumable parts are those required to support the day to day operation of this equipment We establish two types of consumables those items that must periodically be replaced to maintain performance filters resin cartridges etc and other items of limited life indicator lights fuses etc that you can expect to replace on a more or less random basis Where practical we recommend the frequency of replacement or provides information on life expectancy from which you may calculate a replacement interval compatible with your usage pattern The replacement of consumable parts is discussed in the Maintenance and Servicing section to assist you in accomplishing your own service Consumables may be ordered separately and in some cases as an expendables kit Check with your Technical Services representative for additional information on the expendables kit Recommended Quantity Dlamond Kit Organic Free R O amp Distilled Feed
8. During normal Recirculation the printer prints date time purity and temperature readings once every minute Make sure the printer and Nanopure are turned OFF Connect the Nanopure to the printer via the RS232 port Use the tan printer cable included with the Epson printer Plug the printer power cord into an electrical outlet Turn the Nanopure ON Turn the printer ON From the Idle display press the UP or DOWN arrow until display reads Advanced Menu Press ENTER From the Printer Attached display press the Up or DOWN arrow for YES Press ENTER Press BACK twice to return to the Idle mode During normal Recirculation mode a purity and temperature reading will be printed once every 12 minutes Located on the front of the printer AY1137X1 this switch turns power to the printer ON and OFE The POWER light will illuminate when the printer is ON For additional setup and operation refer to the instruction manual included with the printer Nanopure Analytical 11 3 Thermo Scientific Cell Cleaning Section 12 Maintenance and Servicing Disconnect electrical service to the unit Wipe exterior surfaces with lightly dampened cloth containing mild soap solution Warning Avoid splashing detergent or acid on clothing or skin A e Ensure all piping connections are tight to avoid chemical leakage e Carefully follow manufacturer s safety instructions on labels of chemical containers and material sa
9. LHM QN9 SISSYHI Sq S3snd 9 J ir 7 HOLIMS 3InGOW AYINI YIMOd EHM 154 Fal n 14 5 Nanopure Analytical Thermo Scientific Thermo Scientific 401 Millcreek Road Marietta Ohio 45750 United States www thermofisher com ThermoFisher SCIENTIFIC
10. Setting Timed Dispensing Performing a System Flush 9 6 Nanopure Analytical UP arrow 0 25 up to 1 L then 5 L then incremental by 5 L DOWN arrow Decrement 1 L until 1 L then 0 251 Maximum 60 L Minimum 0 25 L me From the normal recirculating mode when the display is showing purity press the UP or DOWN arrow until the display reads Auto Dispense Menu Press ENTER Display will read Dispense Method Press the UP or DOWN arrow to select TIME Press ENTER Display will read Time Setting xx Minutes Press the UP or DOWN arrows to set the desired time value Press ENTER UP arrow 1 up to 5 min then increments by 5 minutes DOWN arrow Decrement by 1 minute Maximum 40 minutes Minimum 1 minute me From the normal recirculating mode when the display is showing purity press the UP or DOWN arrow until the display reads System Flush Press ENTER Press the UP or DOWN arrow to select Short Flush or Extended Flush Press ENTER Display will read System Flushing xxx Seconds or xxx Minutes Remaining Note Press the STOP STOP switch to cancel the flush A Thermo Scientific Changing Purity Units Thermo Scientific Temperature Compensation Auto Standby Section 9 User Settings The units are factory set to mQ cm 1 From the normal recirculating mode when the display is showing purity press the Up or DOWN arrow until display will rea
11. pull forward and remove The control panel fits tightly in the unit so it may be difficult to remove Note The removable control panel was not designed to be repeatedly removed from the unit therefore you may experience difficulty when attempting to remove it It is therefore recommended that the control panel be permanently mounted in a remote location or remain intact with the unit A 3 Replace the control panel with the blank panel provided with the unit to protect the electrical connector Note The blank protective cover on the rear side panel display connector should remain in place when the display is not remotely located Nanopure Analytical 5 3 Section 5 Installation in Remote Loc cont 5 4 Install Control Panel Nanopure Analytical 4 Using the wall bracket as a template locate and drill the mounting holes in the wall A minimum of two customer supplied fasteners will be required Attach the wall bracket to the wall using the customer supplied fasteners 5 Locate the 25 pin connector on the back top right of the unit Remove the protective black cover and store it for future use if the control panel is returned to the top cover 6 Locate the 10 ft 3 1 m 25 pin M F cable included with the unit attach the female end to the 25 pin connector on the back top right of the unit and the other end to the connector on the bottom of the control panel 7 Tighten the cable screws on each end to s
12. DOWN arrow until the desired time is displayed for the unit to automatically enter Standby 7 Press ENTER 8 Press BACK until you return to the Idle display Note If set to YES unit will automatically enter Standby Mode only once per day If the unit mode is later changed from Standby the unit will not again automatically enter Standby until the preset Auto Standby time is again reached Unit Under Counter auto dispense lock out is factory set to NO This option will lock out any type of automatic dispense out of the unit Accudispense accessory D13661 will still operate normally This will prevent accidental dispensing from the unit if it is located under a counter or similar area such that the unit dispenser is not in sight of the user but the display is i e remote mounted display Note When UNIT UNDER COUNTER is set to YES Auto Dispense will not be available from the main unit dispenser 1 From Nanopure Idle xx xx xx xx xx xx press the UP or DOWN arrow until display reads Advanced Menu 2 Press ENTER 3 Press ENTER to proceed through the options until UNIT UNDER COUNTER is displayed 4 Press the UP or DOWN arrow to choose YES 5 Press ENTER 6 Press BACK until you return to the Idle display Thermo Scientific Section 10 Accessories
13. arrange for the unit to be repaired at our expense and to your satisfaction Regardless of your needs our professional telephone technicians are available to assist you Monday through Friday from 8 00 a m to 6 00 p m Eastern Time Please contact us by telephone or fax If you wish to write our mailing address is Thermo Fisher Scientific 401 Millcreek Road Box 649 Marietta OH 45750 International customers please contact your local Thermo Scientific distributor iv Nanopure Analytical Thermo Scientific Section 1 Section 2 Section 3 Section 4 Section 5 Section 6 Section 7 Section 8 Thermo Scientific Table of Contents Safety Information 1 1 2 1 General Pu E RE 2 1 General 3 1 Unpacking E 4 1 a 5 1 too ate af te Pacta dod 5 2 Bench Mounting tao 5 2 Accessories ato e Nu aeg aan 2 5 2 Install Control Panel in a Remote Location 5 3 Water Connections odit diserti heb ais 5 5 Atmospheric Drain Connection 5 6 Feed Water Connection cire te Pott 5 6 Tubins Installation Det trat
14. cartridge pack out 7 Install new cartridge pack rinse and clean according to the instructions in the Initial Operation section 0 2 Micron Filter Replace the 0 2 micron final filter whenever any of the following Replaceme Nt conditions occur the product water flow rate is reduced or bacteria break through Caution Do not overtighten the 0 2 micron filter or use excessive force in seating it Filter can be damaged by overtightening or excessive force A Note If a newly installed 0 2 micron filter clogs rapidly after installation the Nanopure Analytical may need to be cleaned to remove bacterial contaminants See System Cleaning 0 2 Micron Filter Figure 12 2 Replacing 0 2 Micron Final Filter Thermo Scientific Nanopure Analytical 12 5 Section 12 Maintenance and Servicing 12 6 0 2 Micron Filter Replacement cont Fuse Replacement Shutdown Nanopure Analytical To replace the 0 2 micron filter assembly 1 Remove the old 0 2 micron filter assembly by turning it counterclockwise until it is free from the dispense arm manifold Remove the new 0 2 micron filter assembly from the bag and insert it into the dispense arm manifold Gently turn it clockwise until it is fully seated Remove the protective cap from the filter bell Rinse 1 2 liters of water through the filter to drain prior to using the product water Tu
15. into the jumper plug outlet 7 Reconnect the electrical power Accessory AY1367X1 overflow float with 6 ft 2 83 meter cable is designed as a user option to ensure automatic dispensers time or volumetric do not overflow carboy style containers This accessory can be especially helpful if the actual volume of a container is unknown It can also protect against overflows if the entered stored volume of a previous container has not been changed and is set for a volume greater than the carboy being filled Finally the accessory can be useful for automatic time dispenses as it is usually difficult to ensure the set time will equal a specific volume of water 1 Prior to initialing an automatic dispense time or volumetric plug AY1367X1 into connector on back right side of Nanopure See Figure 10 2 4 Ps f ul zz Se at L i N 2 PA d X 9 cpu p mnt J j U d p NI x Figure 10 2 Dispense Overflow Cutoff Float 2 Position carboy to be filled and place float assembly on open neck of carboy Position float assembly such that it will not interfere with product water stream being dispensed into carboy Thermo Sc
16. involve water spillage and subsequent electrical shock hazard if improperly located 3 Replace fuses with those of the same type and rating 4 Disconnect from the power supply prior to maintenance and servicing Thermo Scientific Nanopure Analytical 1 1 Section 1 Safety Information 1 2 Nanopure Analytical To avoid personal injury Do not use in the presence of flammable or combustible materials fire or explosion may result This device contains components which may ignite such materials This device is to be used with water feeds only Cleaning agents must be used in compliance with instructions in this manual Failure to comply with the above could result in explosion and personal injury Avoid splashing cleaning solutions on clothing or skin Ensure all piping connections are tight to avoid chemical leakage Ensure adequate ventilation Carefully follow manufacturer s safety instructions on labels of chemical containers and material safety data sheets Depressurize system prior to removing the cartridge pack Refer servicing to qualified personnel A full cartridge pack may weigh about 20 lbs Thermo Scientific General Usage Thermo Scientific Section 2 Introduction Congratulations on your purchase of a Thermo Scientific Nanopure Analytical ultrapure water system This water purification system is designed to provide high resistivity reagent grade water that exceeds ASTM Type I ISO 3696 and CLS
17. or DOWN arrow until you reach the desired year Press ENTER 9 When prompted with Set Time press the UP or DOWN arrow to choose Yes then press ENTER This is to set the time of day 10 Press the UP or DOWN arrow until you reach the desired hour value Press ENTER 11 Press the UP or DOWN arrow until you reach the desired minute value Press ENTER 12 Press BACK twice to return to the Idle mode Note Time values are displayed in 24 hr military time For example 6 00p m 18 00 00 hr min sec 9 2 Nanopure Analytical Thermo Scientific Setting the Call Thermo Scientific Constant Section 9 User Settings The actual temperature and cell constants are attached to the cell cable internal to the Nanopure unit This data helps ensure that the purity displayed is as accurate as possible The only time the user would need to enter this data is if the cell or main board is being replaced and or updated 1 Shut power OFF to the unit and disconnect the power cord 2 Unlatch and open the right side door 3 Find and copy down the two cell constants attached to the gray cable leaving the electronics board mounted on the inside of the right side door 4 Close and latch the right side door 5 Reconnect the power cord and turn unit ON 6 From the Idle mode when the display reads Nanopure Idle xx xx xx press the UP or DOWN arrow until the display reads Advanced Menu
18. panel display which allows the system to be mounted almost anywhere within the laboratory Use the wall bracket for wall mounted systems as a template to drill mounting holes The Nanopure Analytical does not include screws and fasteners for mounting Please refer to the General Specifications section for clearance requirements Note The outlet of a gravity feed storage reservoir must be above or at the same level as the inlet of the Nanopure Analytical Caution Wall composition condition and construction as well as fastener type must be considered when mounting this unit The mounting surface and fasteners selected must be capable of supporting a minimum of 150 Ibs 68kg Inadequate support and or fasteners may result in damage to mounting surface and or equipment If you are unsure of mounting surface composition condition and construction or correct fasteners consult your building maintenance group or contractor A Warning Do not locate the Nanopure Analytical directly over equipment that requires electrical service Routine maintenance of this unit may involve water spillage and subsequent electrical shock hazard if improperly located Warning Do not use in the presence of flammable materials fire or explosion may result This device contains components which may ignite such materials A Nanopure Analytical 5 1 Section 5 Installation 5 2 Other Accessories Bench Mounting Wall Mounting Nanopure Analyt
19. that the membrane is functioning Poor quality feed water properly If a Still is the feed water source ensure that the distillate temperature to the NANOpure does not exceed 40 C 104 F If feed water is from a central water purification system verify water quality and proper functioning of the system See General Specifications Dispense more water through the Nanopure to purge air from the unit Purity display continuously Bad Gellibenaeton Check the connection of the cell as it attaches to the meter circuit board OVERRANGE mounted the inside of the right door If you have N I S T module perform a 1 5 calibration Incorrect 1 5 calibration offset If you do not have a N I S T module perform the calibration function WITHOUT the calibration module as if you had it answer YES to prompt The display will read Calibration failed but this will clear any incorrect offset to zero E 0 2 micron filter clogged Replace final filter as indicated in 0 2 Micron Filter Replacement PC board communication error Turn the Nanopure OFF 1 0 Switch and restart the unit Display reads Meter Board Problem System electronics failure Replace the resistivity meter board mounted on the inside of the right door Wing head screws are not tight enough Tighten wing head screws on unit manifold Water is leaking between the manifold and the cartridge jack New cartridge pack o ring
20. D50280 Diamond Kit Organic Free Deionized Feed 050281 Final Filter D3750 Description Catalog No Main Fuse 120 Volt Slow Blow 1 6 Amp 250V Nanopure Analytical 14 1 Section 14 Replacement Parts 14 2 Nanopure Analytical General Maintenance Parts General maintenance parts are defined as laboratory level repair parts which do not require great expertise or special tools for installation We recommend that you stock the general maintenance parts as an aid to ensuring the continued operation of this equipment Catalog No Recommended Quantity Quick Disconnect Inlet CUX11 Quick Disconnect Insert 3 8 tube CUX9 Cartridge Pack O Rings GSX68 Safety Stock For critical applications where performance with minimum downtime is required we recommend that you maintain a local stock of those parts listed in the General Maintenance Parts and Safety Stock sections External Display Cable remote display use 1 C11 Main PC Board Recirculation Pump amp Motor Pressure Regulator Resistivity Cell 1 Power Supply PC Board 116 1 Calibration PC Board Resistivity Meter PC Board PC896X2 14 Check Valve Flow Sensor Flush Solenoid Cartridge Pack Manifold Dispenser Manifold W Solenoid Dispense Switch Cell O ring Thermo Scientific Ordering Procedures Thermo Scientific Section 14 Replacement Parts Optional Accessory Ordering Information Description Catalog No rs nean N I S T Calibrat
21. Drain Connection Tubing Installation Nanopure Analytical 1 Locate the length of 3 8 O D tubing provided with the unit with a quick disconnect insert on one end and a 3 8 95 cm O D X 1 4 64 cm NPT tubing adapter on the other 2 Install the tubing adapter onto your incoming water line We recommend a customer supplied shut off valve be installed in your feed water line Do not connect the feed water to your Nanopure Analytical You will connect the feedwater during the Initial Cleaning procedure explained later in this manual Note The cartridge pack must be installed before connecting water line 3 Ifa pressure switch is to be used see the Installing a Float or Pressure Switch section for more information When the Nanopure Analytical flushes its membrane the water used is sent to drain through this connection To install 1 Locate the drain water tubing This is the 1 4 64 cm O D tubing that is approximately 6 ft 1 9 m long The atmospheric drain fitting is located on the lower left side of the Nanopure Analytical 2 Route the other end of the drain water tubing to an atmospherically vented drain and make a connection Ensure there are no kinks in the tubing and that it proceeds on a downward plane Proceed to Initial Operation To make tubing connections refer to Figures 5 4 and 5 5 1 Make sure the tubing is cut off reasonably square and that no plastic burrs or ridges are pres
22. I CLRW Type I standards It uses a four stage deionization process combined with a 0 2 micron filter to polish suitable feed water distilled deionized or reverse osmosis of up to 18 2 megohm cm Water resistivity is continuously monitored by a resistivity cell and displayed on a digital display The electronics can be verified and calibrated utilizing a N I S T Traceable Calibration module See accessory ordering information Please read the instructions carefully to ensure that you receive maximum benefit from the Nanopure Analytical Also please fill out and return the enclosed warranty registration card as it will help us assure you of proper warranty coverage Do not use this product for anything other than its intended purpose Nanopure Analytical 2 1 Thermo Scientific Section 3 General Specifications Dimensions 13 5 W x 19 5 H x 17 0 D 34 3 x 49 5 x 43 2 cm Clearance Requirements Sides 9 22 9 cm minimum for servicing Above 3 7 6 cm minimum for removal of the top cover 4 75 12 1 cm minimum for opening the front door Feed Water Requirements Types iie ee gts vet eae RO DI distilled t het ore Less than 1 0 ppm Turbidity 1 0 N T U maximum Pressure Range Gravity feed to 20 psig 1 38bar 1 41 kg cm max Temperature Range 4 C 40 C 40 104 F 5
23. Id TXO6LLId 2 061199 29 t9680 HOLIMS LVO1d IXE6LLId IXZ6LLId IXL6L Id vX06L TOHINOD NIYIN inen IXWT n 90 20 HOLIMS SHNSS3Hd 1X06113A 1X06 13A 1X06113N YOSNISMOH 154 SX9683 SX9683 SX9683 SX9683 31000W LSIN a vX9683 vX9683 VX9683 vX9683 T39 ALIALLONGNOD oma yaar 7X96839 7X96839 7X96839 7X96839 90 1831NI 1490 ONIMOTIOS JHL 40 803 LNIOd NOLLO3NNOO She Sehen AIO MUGUMU ES Hera 6 5 ON 38 m Ajuo n ym S ON 1uvd uno ON 1300 20d 9d 5 104 1SM LN3NOdIAOO WYY9Y10 8 e r o SH bx m CEN 6HM 1HM od a 199 elu 00000000000 y D d 9HM LXZ9 LAV 30VJU31NI 1Y074 55990900669 bd bg bodd 33010 MO 383A0 3534510 er ezr ar 5 8HM gt me AB VA L J 199210 3 9 9 39vui31NI esuedsiq NOV o LHM AWD vir er 9 195 ag 3 Wr ii e ar op sir 945 d 88888 ood 3328832383808 bod a delete T 000000000000 Sela 5 YOLOINNOD LOWY Loo d T 9La JN DE D THM 18 tos gos ann Cj gl OO I 1 OO LN 154 Y Y
24. Nanopure Analytical Ultrapure Water System Series 1367 Operating Manual and Parts List LT1367X1 Rev 0 Part of Thermo Fisher Scientific Models covered in this manual Model number Voltage D11901 7143 100V 240V MANUAL NUMBER LT1367X1 7007143 0 6 9 10 Transfer to Marietta was LT1367X1 3 4 10 CCS REV ECR ECN DATE DESCRIPTION By Thermo Scientific Nanopure Analytical i CAUTION Contains Parts and Assemblies Susceptible to Damage by Electrostatic Discharge ESD Important Read this instruction manual Failure to read understand and follow the instructions in this manual may result in damage to the unit injury to operating personnel and poor equipment performance Caution All internal adjustments and maintenance must be performed by qualified service personnel Material in this manual is for information purposes only The contents and the product it describes are subject to change without notice Thermo Fisher Scientific makes no representations or warranties with respect to this manual In no event shall Thermo be held liable for any damages direct or incidental arising out of or related to the use of this manual 2010 Thermo Fisher Scientific All rights reserved Nanopure Analytical Thermo Scientific Important operating and or maintenance instructions Read the accompanying text carefully gt gt
25. Potential electrical hazards Only qualified persons should perform procedures associated with this symbol re T Equipment being maintained or serviced must be turned off and locked off to prevent possible injury Hot surface s present which may cause burns to unprotected skin or to materials which may be damaged by elevated temperatures Marking of electrical and electronic equipment which applies to electrical and electronic equipment falling under the Directive 2002 96 EC WEEE and the equipment that has been put on the market after 13 August 2005 24 mee This product is required to comply with the European Union s Waste Electrical amp Electronic Equipment WEEE Directive 2002 96 EC It is marked with the WEEE symbol Thermo Fisher Scientific has contracted with one or more recycling disposal companies in each EU Member State European Country and this product should be disposed of or recycled through them Further information on Thermo compliance with this directive the recyclers in your country and information on Thermo products will be available at www thermofisher com v Always use the proper protective equipment clothing gloves goggles etc VY Always dissipate extreme cold or heat and wear protective clothing v Always follow good hygiene practices v Each individual is responsible for his or her own safety Thermo Scientific Nanopure Analytical iii Do You Need Information or Assistance
26. R 8 Display will show Calibration Module Installed Press the UP or DOWN arrow to select YES 9 Press ENTER Thermo Scientific Nanopure Analytical 10 3 Section 10 Accessories Electronic Cal w 10 Display will read Calibration In Progress When the calibration is i complete the display will read Calibration passed failed for 4 Opti Cal Mod cont seconds and then return to the N I S T Calibrate display Note Calibration in progress may take up to two minutes to complete A 11 Press BACK to return to the Idle mode 12 Turn the main power switch to the OFF O position Unplug the unit 13 Remove the calibration module and reconnect the cell 14 Reattach the cover plate and close and latch the door 15 Reconnect the power cord The calibration procedure is complete Remote Volumetric Refer to the Operating Instructions for your manual or Accudispense Dispenser volumetric remote dispenser LT1366X11 10 4 Nanopure Analytical Thermo Scientific Connect Communicate through RS 232 Port Thermo Scientific Hyperterminal Section 11 Computer Printer Set Up Note Due to character set differences hyperterminal may display the symbol as Also the symbol may be displayed as o The procedure for the connection of the Nanopure to a computer and communication through the RS 232 port using the hyperterminal follows 1 Connect the 9 pin serial cable part
27. TER Display will show System Flushing and the time remaining as the system depressurizes The frequency with which you will need to clean your unit and replace your cartridge pack is dependent on your feed water s characteristics your purity requirements and your usage Clean your Nanopure Analytical and replace the cartridge pack when the product water purity drops below acceptable levels of resistivity when organic levels become too high or if a new 0 2 micron filter clogs rapidly after installation even though the cartridge pack was thoroughly rinsed before the 0 2 micron filter was installed The simple to use cleaning syringe is available Catalog Number CMX25 This is used to effect a complete cleaning Warning Depressurize system prior to removing cartridge pack Warning A full cartridge pack may weigh about 20 lbs 9 kg Figure 12 1 Cartridge Pack Replacement Thermo Scientific Section 12 Maintenance and Servicing Cartridge Pack Replacement Remove the feed water line by depressing the stainless steel thumb pad Depressurize the system according to System Depressurization under the Maintenance and Servicing section 3 Shut power OFF to the unit and disconnect the electrical service to the unit 4 Open the front left side door 5 Loosen the wing head screws on the cartridge manifold 6 Remove the exhausted cartridge pack by lifting the unit manifold and pulling the
28. VARTE RGR 9 7 Temperature Compensation 9 7 Changing Purity Units 9 7 Unit Under Counter 9 8 Section 10 Accessories 10 1 Feedwater Float or Pressure 10 1 Dispense Overflow Cutoff 10 2 Electronic Calibration w Optional Cal 10 3 Remote Volumetric Dispenser 10 4 Section11 Computer Printer Set Up 11 1 Connect Communicate through RS 232 Port 11 1 Hyperterminal ora eS Bee TELLE ep a 11 1 Priocomim ete SSSR SPERA A DRE 11 2 Connecting and Starting th Printer 11 3 Section12 Maintenance and Servicing 12 1 Cell e lt oe 12 1 Systemi Cleaning ede vp Eee v deus 12 2 Cartridge Pack Replacement 12 4 System Depressurization v4 00 yo PRR Pace en Y aec 12 4 0 2 Micron Filter 12 5 SHUGOWI P eddie 12 6 Fuse Replacements naa dob mur a EEES RR 12 6 Section 13
29. WHX18 from the Nanopure RS 232 port to COM2 port or COMI port on back of computer 2 From the Idle display press the UP or DOWN arrow until display reads Advanced Menu 3 Press ENTER 4 From the Printer Attached display press the Up or DOWN arrow for NO 5 Press ENTER 6 Now during the normal Recirculation mode date time purity and temperature readings will be sent to the computer once per minute 7 Run your Microsoft Windows program Open Hyperterminal located in the accessories directory give your setting a name and choose a symbol 8 In the Connect Using box select direct to COM2 or COMI as port depending on your computer and click OK 9 Using the selection boxes in the next screen configure the options as 9600 baud 8 bit No parity 1 stop bit Flow Control None 10 To receive data to a file select Transfer and capture text Accepting default will put the file which you name in the c windows directory called capture txt and the file will be an ASCII text file 11 You should see the data on the computer screen Nanopure Analytical 11 1 Section 11 Computer Printer Set Up Hyperterminal continued 11 2 Procomm Nanopure Analytical 12 When you are finished storing data from the Nanopure save your file You can exit Hyperterminal or set up a new experiment 13 Hyperterminal data can be manipulated and graphed in Excel software T
30. an e D Rd s 5 6 Electrica Connections oues fits oar dies 5 7 Wi EM Pr 6 1 Control Panel sutor VAL ATRAS EACH IR RUD TOC Kate Ce 6 1 Main Power Switch 52 ARA ACRES 6 1 Qu MEET PEUT 6 2 Initial 7 1 Cartridge 7 1 lima iO DT UR A PDA 7 2 System Cleaning Procedure 7 3 Normal Operation 8 1 Automatic Dispensing 8 2 Dispensing Water s seda ute siete Seat ETA EA AS 8 2 Nanopure Analytical V Table of Contents Section9 User Settings 9 1 Setting the Displayed Language 9 1 Adjusting Display Brightness 9 1 Setting the Date and 9 2 Setting the Call Constant ei keer ei ekks 9 3 Selecting the Set Point 9 4 User Standby Modein ies opinari VE Gerd tg eho Gees 9 4 Setting Volumetric Dispensing 9 5 Resetting the Cleaning 9 5 Setting Timed Dispensing 9 6 Performing a System 5 9 6 Auto Standby 265 Pues a udo AAE AEREE
31. anual Warning Disconnect from the power supply prior to maintenance and servicing Warning Refer servicing to qualified personnel Warning Avoid splashing cleaning solution on clothing or skin Ensure all piping connections are tight to avoid leakage Ensure adequate ventilation Carefully follow manufacturer s safety instructions and material safety data sheets This device to be used with water feeds only Cleaning agents must be used in compliance with instructions in this manual Failure to comply could result in explosion and personal injury A It is best to perform cleaning procedures early in the afternoon After cleaning is complete approximately 3 5 hours place the unit into its normal recirculation mode to allow the system to recirculate overnight after cleaning 1 If you have installed an Accudispense volumetric remote dispenser place it in Manual mode From the Idle mode press the UP or DOWN arrow until the display reads Clean Unit 2 Press ENTER 3 Display will prompt Disconnected Inlet Water NO 4 Disconnect feed water supply at the quick disconnect inlet valve Thermo Scientific Section 12 Maintenance and Servicing System Cleaning Press the UP or DOWN ARROW to select YES and then press c ontinu ed ENTER Display will now prompt Injected Cleaner NO 6 Remove solution syringe from wrapper 7 Open front left side door Remove luer cap on system i
32. ctronics will initialize and check its calibration All units have been factory calibrated If calibration is Ok the display will show Calibration passed The display will next read Self Test in progress Self Test Passed Finally the display will read 10 0 2 This is a reading of the calibration reference value 4 From an Idle display press the START STOP switch on the control panel to enter the normal recirculating mode The unit s pump will begin to run 5 The display will then begin reading resistivity of the product water Initially it will read MO cm until the air is bled from the system Note On initial start up the purity meter may display or uS cm This is caused by air in the cell and should be replaced by a resistivity reading almost immediately If the dots aren t replaced by a value after one minute refer to the Troubleshooting section of this manual A 6 Allow the water s resistivity to rise to the desired purity before drawing off water 7 The system should left On or in Standby during the work day See Use of Standby Mode Note Do not turn off the Nanopure Analytical during non work hours Doing so will allow bacterial growth and other contamination of the water in the system As a result the system will require a rinse up period at the beginning of the work day to achieve high quality product water We recommend using the Standby Mode A No
33. ds Change Units Press ENTER 2 Press the UP or DOWN arrow to select or uS cm Press ENTER 3 Press BACK to return to the normal recirculating mode Note Purity displayed will have an asterisk the the left of the reading xx x or x xx uS cm to inform the user that uncompensated purity is being displayed Temperature Compensation is factory set to ON From the normal recirculating mode when the display is showing purity press the Up or DOWN arrow until the display reads Temperature Compensation Press ENTER 2 Press the UP or DOWN arrow to select OFF or ON Press ENTER 3 Press BACK to return to the normal recirculating mode Auto Standby is factory set to NO This option allows for a convenient method for the user to ensure that the Nanopure Analytical unit will be placed in Standby at a predetermined time each day This is especially convenient to ensure the unit is placed in Standby during weekends 1 From the Nanopure Idle xx xx xx xx xx xx press the UP or DOWN arrow until display reads Advanced Menu 2 Press ENTER 3 Press ENTER to proceed through the options until AUTO STANDBY START is displayed Nanopure Analytical 9 7 Section 9 User Settings 9 8 Auto Standby continued Unit Under Counter Nanopure Analytical 4 Press the UP or DOWN arrow to choose YES Press ENTER 6 Press the UP or
34. ds Nanopure Idle xx xx xx press the UP or DOWN arrow until the display reads Reset Timers 2 Press ENTER 3 Display will read Reset Cleaning Timer and show on the right side of the second line when the user will start receiving Clean Unit reminders 4 Press the UP or DOWN arrow to select Yes 5 Press ENTER and the timer will be reset This will reset the cleaning timer for approximately six months calendar time Note Volumetric dispensing is based upon total fluid volume entering the Nanopure Analytical Point of drawoff accuracy will be compromised if you are dispensing water volumetrically while simultaneously drawing water manually through the remote dispenser accessory Note Once Volumetric or Timed Dispensing values are set they will remain in memory until changed by the user To turn the dispense method OFF select OFF in the Dispense Method menu 1 From the normal recirculating mode when the display is showing purity press the UP or DOWN arrow until the display reads Auto Dispense Menu 2 Press ENTER 3 Display will read Dispense Method Press the UP or DOWN arrow to select VOLUMETRIC 4 Press ENTER Display will read Unit Volume Setting xx Liters 5 Press the UP or DOWN arrow to set the desired volume value Press ENTER Nanopure Analytical 9 5 Section 9 User Settings Setting Volumetric Dispensing cont
35. e the locking screws Note Please refer to the General Specifications section for clearance requirements Thermo Scientific Wall Mounting continued Install Control Panel in a Remote Location Thermo Scientific Section 5 Installation Warning Do not locate the Nanopure Analytical directly over equipment that requires electrical service Routine maintenance of this unit may involve water spillage and subsequent electrical shock hazard if improperly located Note The outlet of a gravity feed storage reservoir must be above or at the same level as the inlet of the Nanopure Analytical Caution Wall composition condition and construction as well as fastener type must be considered when mounting this unit The mounting surface and fasteners selected must be capable of supporting a minimum of 150 Ibs 68kg Inadequate support and or fasteners may result in damage to mounting surface and or equipment If you are unsure of mounting surface composition condition and construction or correct fasteners consult your building maintenance group or contractor A For your convenience the control panel can be removed from the unit and mounted at a convenient location within 10 ft 3 1 m of the unit To remove the control panel from the unit 1 Turn the unit OFF and disconnect it from the power supply 2 Slide the control panel upward about 1 4 64 cm to 3 8 95 cm just enough to clear connector on top cover
36. ecure the cable to the unit and control panel 8 The control panel may now be mounted on the wall Caution Repeated removal and replacement of the control panel from the top cover may eventually cause it to become damaged Note A bracket is available that will allow you to mount the control panel on the bench If bench mounting is desired order bracket AY1367X2 Blank panel Wall Mount Bracket Figure 5 1 Control Panel Wall Mounting Thermo Scientific Section 5 Installation Water Connections Caution Do not connect feed water until directed to do so during Initial Cleaning Note To prevent leaking push the tubing into the atmospheric drain connection until it bottoms out Accudispense A 1 control cable LI Remote 1 Remote 2 Feed s Water Inlet G NY Atmospheric er Drain m 31 Figure 5 2 Water Connections Left Side of Unit Overflow Float 5 Connection dip Figure 5 3 Water Connections Right Side of Unit Thermo Scientific Nanopure Analytical 5 5 Section 5 Installation 5 6 Feed Water Connection Atmospheric
37. ent 2 Mark from end of tube the length of insertion Tube size Insertion length 1 4 O D 1 75 cm 11 16 3 8 O D 1 9 cm 3 4 3 Wet the tube end with water and insert tube straight into fitting until it bottoms out on interior shoulder and insertion mark is no longer visible 4 remove tubing push collet toward fitting body and pull on tubing To reuse fitting begin assembly at Step 1 Thermo Scientific Section 5 Installation COLLET TYPICAL Figure 5 4 Mark Tubing Insertion Length Figure 5 5 Push Collet Back to Remove Electrical The Nanopure comes with a 120V power cord with 2 1 6 amp fuses and Connections 240V power cords with 2 0 63 amp fuses The Nanopure is not shipped with fuses installed in the fuse draw of the power module Before connecting the power cord to the power module install the proper fuses in the fuse holder Refer to Figure 5 6 Fuse Holder Power Switch Power Cord Figure 5 6 Electrical Connections Thermo Scientific Nanopure Analytical 5 7 Main Power Switch Thermo Scientific Control Panel Section6 Controls LED NANOpure Diamond DISPENSE Figure 6 1 Control Panel The main power switch on the Nanopure Analytical is located on the lower back right side of the unit as you face the front of the unit directly above the power cord receptacle The Nanopure Analytical is contro
38. fety data sheets Caution Feed water must be disconnected and the system must be depressurized before performing the cell cleaning procedure A 1 Disconnect inlet water and depressurize See System Depressurization section 2 Turn unit OFE Open right side door and remove PC board cover 3 Disconnect cable from J2 and snip plastic cable tie located on the inside top of unit Unscrew and remove the cell by turning the gray bushing counterclockwise Carefully remove O ring to clean the cell 5 Wash the cell in a mild detergent solution or a 1096 inorganic acid solution follow acid manufacturers recommended handling procedure This may be done in an ultrasonic cleaner or with a soft brush 6 Thoroughly rinse the cell in deionized or distilled water following the detergent or acid cleaning 7 After cleaning check the o ring replace if necessary 8 Reinstall the cell into the cell well and hand tighten 9 Reroute the cable and reconnect to J2 on circuit board Nanopure Analytical 12 1 Section 12 Maintenance and Servicing 12 2 Cell Cleaning continued System Cleaning Nanopure Analytical 10 Replace PC board cover and close door 11 Reconnect water and turn unit ON Note The cleaning timer will display after six months reminding you to clean the unit Complete the system cleaning procedure and reset the cleaning timer according to the Resetting the Cleaning Timer section in this m
39. filter and bell assembly at this time Caution Do not allow the Nanopure Analytical to operate unless water is available to the unit 1 Attach the feed water line to the unit by snapping the quick disconnect coupling into the quick disconnect body in the lower left back of the unit 2 Attach an atmospheric drain line 1 4 0 64 cm tubing by pushing into the quick connect fitting on the lower left back of unit See layout connection under the Water Connections section 3 Check to ensure the dispense knob is in the OFF middle position 4 Select the appropriate power cord remove and install the two fuses into the fuse draw in the power entry module U K customers use cord CRX100 and fuses for 240V installation Warning Use a properly grounded electrical outlet of correct voltage and current handling capacity 5 Connect attach to proper electrical outlet and the unit 6 Turn the unit on by turning the main power switch to the I ON position 7 The system greeting will display the type of unit you own This greeting is Base 8 The system electronics will initialize and check its calibration All units have been factory calibrated If calibration is Ok the display will show Calibration passed The display will next read Self Test in progress Self Test Passed Finally the display will read 10 0 2 MQ cm This is a reading of the calibration reference value 9 From t
40. for Measurement Control and Laboratory Use Part I General Requirements Safety EN 61010 1 Safety Requirements for Electrical Equipment for Measurement Control and Laboratory Use Part I General Requirements per the provisions of the Electromagnetic Compatibility Directive 2004 108 EC and per the provisions of the Low Voltage Directive 2006 95 EC Copies of the Declaration of Conformity are available upon request 3 2 Nanopure Analytical Thermo Scientific Section 4 Unpacking 1 Remove the unit from its shipping container Remove all contents carefully Ensure that the feed and drain tubing cleaning cartridge wall bracket accessory parts bag and power cords see list below are removed from the packaging materials before discarding Put the Nanopure Analytical on a bench Cleaning Cartridge CMX25 Wall Bracket Unit BC1190X12 Wall Bracket Remote Display BC1190X10 Accessory Parts Bag includes Feed Water Tube 3 8 O D TU1119X7 Drain Tube O D TU1190X12 Display Cable WHX20 Blank Display DL1190X18 Plug Adapter 42 Power Cords Also required for installation Customer Supplied Fasteners to mount unit and remote display Thermo Scientific Nanopure Analytical 4 1 Thermo Scientific Section5 Installation The Nanopure Analytical features a removable control
41. he Idle mode when the display reads Nanopure Idle xx xx xx press ENTER to run an air purge Thermo Scientific Initial Rinse continued System Cleaning Thermo Scientific Procedure Section 7 Initial Operation 10 Unit will display Air Purge Press ENTER 11 Upon completion of the air purge complete the System Cleaning Procedure Caution Never dispense water without first installing hose barb provided in parts bag or final filter supplied with cartridge pack A Your Nanopure Analytical has been shipped with a cleaning syringe Cat No CMX25 When the system is new or whenever a new cartridge pack is installed the system should be cleaned It is best to perform cleaning procedures when the system or water is not required The entire cleaning procedure will take approximately 3 5 hours to complete Clean your Nanopure as follows 1 Ifyou have installed an Accudispense volumetric remote dispenser place it in Manual Mode From the Idle display press the UP or DOWN arrow until display reads Clean Unit 2 Press ENTER 3 Unit display will ask if you have Disconnected Inlet Water NO 4 Disconnect feed water supply at the quick disconnect inlet valve on left side of unit 5 Press the UP or DOWN ARROW to select YES and then press ENTER Display will now read Injected Cleaner NO Injection Port 6 Open front left side door to expose cartridge
42. he procedure for the connection of the Nanopure to a computer and communication through the RS 232 port using Procomm follows 1 Connect the 9 pin serial cable from the Nanopure RS 232 port to 2 port or COMI port on back of computer 2 From the Idle display press the UP or DOWN arrow until the display reads Advanced Menu 3 Press ENTER 4 From the Printer Attached display Press the Up or DOWN arrow for NO 5 Press ENTER 6 The unit will now during the normal Recirculation mode send a purity and temperature reading to the computer once per minute 7 Open DOS window and change directory to procomm directory 8 Open procomm executable 9 Press ALT F10 for configuration screen 10 Enter into Line Settings screen by typing ALT P 11 Type in 11 Enter sets parameters as 9600 8 N 1 12 Type in 21 Enter sets to COM2 or in 20 Enter sets to COM I depending on your computer 13 Type in 24 Enter saves settings 14 Type ESC to exit setup menu 15 Procomm is now ready to accept input from the Nanopure Thermo Scientific Procomm continued Connecting and Starting Thermo Scientific the Printer Printer Set Up Section 11 Computer Printer Set Up 16 To begin downloading a file Type ALT F1 and give the file an 10 appropriate name when prompted The optional printer part no AY1137X1 provides a paper tape record for future reference
43. ical Optional accessories for this unit include a float switch low pressure switch N I S T Traceable Calibration Module standard remote dispenser Accudispense volumetric remote dispenser dispense overflow cutoff float and printer If you purchased a float switch or low pressure switch refer to the Accessories section of this manual If you purchased a standard or Accudispense volumetric remote dispenser refer to their respective operators manuals for installation instructions 1 Place the Nanopure Analytical on a bench top that is accessible to pretreated water electricity and an atmospherically vented drain Install the Nanopure Analytical on a wall in a convenient location that is accessible to water an atmospherically vented drain and electricity 1 Locate the wall bracket packed separately from the unit 2 Using the wall bracket as a template locate and drill the mounting holes in the wall A minimum of four customer supplied fasteners will be required two on the top and two on the bottom 3 Attach the wall bracket to the wall using the customer supplied fasteners 4 Remove the locking screws on each side of the wall bracket 5 Pull the two locking slides on each side of the wall bracket out as far as they will go 6 Hang the unit on the wall bracket by sliding the mounting pins into the wall bracket slots 7 Push the locking slides on each side of the wall bracket in as far as they will go 8 Replac
44. ientific Section 10 Accessories Dispense Overflow 3 Initiate Auto Dispense as described in the Automatic Dispensing Cutoff Float c ont section of this manual If during the auto dispense the float is lifted by the rising water the auto dispense will immediately be stopped and an error message will be displayed momentarily Caution This accessory is not intended for use with small containers as its weight could cause small lightweight containers to tip over Note If an auto dispense is stopped by the AY1367X1 the Nanopure will change modes to normal recirculation Electronic Calibration you purchased the optional N I S T calibration module Catalog No w Option al Cal Mod 825 you can perform a calibration of the Nanopure purity sensing electronics traceable to N I S T standards 1 Disconnect power cord from the unit 2 Unlatch and open the right door Remove the 2 screws and remove the cover plate over the PC boards 3 Locate the outlet cell connection on the circuit board and remove the outlet cell connection at J2 4 Connect the N LS T calibration module to the connection point 2 Outlet Cell on the calibration board PC1190X2 5 Close and latch door 6 Reconnect the power cord and turn Figure 10 3 PC Board the unit on by depressing the main power switch 7 From the Idle mode Press the UP or DOWN arrow until the display reads N LS T Calibrate Press ENTE
45. ight side of the unit as you face the unit is ON the switches on the control panel function as follows START STOP allows you to alternate the unit between the normal recir culation mode when the display is showing purity and the Idle mode STANDBY allows you to put the unit into standby recirculating water for 10 minutes hour The display will read Standby during periods of inac tivity and Recirculating and the time remaining during the 10 minute recirculation DISPENSE allows you automatically deliver water from the unit Please refer to Automatic Dispensing in the User Settings section of this manual for information UP and DOWN arrows allow you to scroll between menu options items and values BACK allows you to return to the previous menu option item Please note that use of the BACK switch from a selection screen will return you to the previous menu option item while maintaining the selection s value upon entry ENTER allows you to activate a selected menu option item and also func tions as Yes whenever an option with a question mark appears DISPENSE KNOB when the unit is in the recirculation mode push to the right to deliver water continuously until pushed back to the middle Push to the left to deliver water manually until button is released Note The unit MUST be in the normal recirculating mode when the display is showing purity in order to dispense water 6 2 Nanopure Anal
46. ion Module Low Pressure Switch Float Switch Remote Dispenser Manual Accudispense Volumetric Remote Dispenser Serial Cable for Communication with Computer Printer 120 240 VAC system AY1137X1 Printer Replacement Paper Roll AY669X4 Dispense Overflow Cutoff Float AY1367X1 Bench Top Display Holder AY1367X2 Refer to the Specification Plate for the complete model number serial number and series number when requesting service replacement parts or in any correspondence concerning this unit All parts listed herein may be ordered from the Thermo Scientific dealer from whom you purchased this unit or can be obtained promptly from the factory When service or replacement parts are needed check first with your dealer If the dealer cannot process your request then contact our Technical Services Department Prior to returning any materials contact our Technical Services Department for a Return Materials Authorization number RMA Material returned without an RMA number will be refused Nanopure Analytical 14 3 Section 14 Replacement Parts power switch turned on Barnstead Thermolyne Vx xx Style English Unit Initialization amp Meter Calibration Check NANOpure Dlamond Idle XX RK xx xx xx i standby S start_stop back key key pressed 2 key pressed M pressed Language back key pressed force print line ani mmc
47. lled through a panel which incorporates switches to control its functions START STOP STANDBY DISPENSE DOWN ENTER and BACK This control panel utilizes a digital display to show system information and the purity of the product water The intensity brightness of the display may be adjusted according to user preference See Adjusting Display Brightness in User Settings of this manual A single LED located on the top of the control panel will illuminate to inform you of the system status as follows LED is not illuminated System is OFF or in Idle mode Solid Green LED System is recirculating and operating normally e Blinking Green LED System is in Standby mode Red LED System is alerting user to an operational error or maintenance issue Nanopure Analytical 6 1 Section 6 Controls Control Panel The control panel can be removed from the unit and remotely mounted continu ed Please refer to Installing the Control Panel ina Remote Location in the Installation section of this manual for more information about how to remove the control panel from the unit Note The removable control panel was not designed to be repeatedly removed from the unit therefore you may experience difficulty when attempting to remove it It is therefore recommended that the control panel be permanently mounted in a remote location or remain intact with the unit Switches When the main power switch on the lower back r
48. mal operation A Note Refer to Auto Standby section to have the unit automatically enter Standby Mode each day at a predetermined time chosen by the user A Note If you have installed an Accudispense volumetric remote dispenser its Purity Above Setpoint LED will slowly blink when the water system is in Standby Mode A The Nanopure Analytical electronics include a user programmable set point which alerts you when water quality falls below the programmed set point The set point is user selectable from 1 18 factory set at 10 MQ cm 1 From the Idle mode when display reads Nanopure Idle xx xx xx xx xx xx press the UP or DOWN arrow until display reads Advanced 2 Press ENTER 3 Proceed through the options by pressing ENTER until Adjust Set Point is displayed 4 Press the UP or DOWN arrow to choose Yes 5 Press ENTER 6 Press the UP or DOWN arrow until the desired value is displayed 7 Press ENTER Thermo Scientific Selecting the Set Point continued Cleaning Timer Resetting the Setting Volumetric Thermo Scientific Dispensing Section 9 User Settings 8 Press BACK to return to the Idle mode The second line of the display will show a Below Set point message once every 8 to 10 seconds when the measurement is below the set point The set point indication is set at the factory at 10 MQ cm From the Idle mode when the display rea
49. njection port located on the right side of the cartridge pack manifold by turning counterclockwise 8 Remove the syringe luer cap and attach the syringe to the system luer fitting 9 Slowly inject the solution into the system and remove syringe Avoid injecting air into system 10 Replace luer cap on injection port Close door 11 Press the UP or DOWN arrow to select YES and then press ENTER Display will now read Reconnected Water NO 12 Attach feed water supply removed in Step 4 13 Press the UP or DOWN arrow to select YES and press ENTER Display will now read Unit Cleaning 14 Unit may now be left unattended until the display reads Cleaning Complete Press ENTER 15 After cleaning is complete and the user presses ENTER the unit will return to the Idle mode 16 Press the START STOP switch to return the unit to the normal recirculating mode Thermo Scientific Nanopure Analytical 12 3 Section 12 Maintenance and Servicing 12 4 System Depressurization Cartridge Pack Replacement Nanopure Analytical This should be done prior to removing a cartridge pack The unit needs to be plugged in and operating to correctly perform this depressurization step Important Disconnect inlet water from the left back of unit 1 From the Idle display press ENTER 2 From Air Purge press the UP arrow 3 From Depressurize press the UP arrow to select YES 4 Press EN
50. on Thermo Scientific Products If you do please contact us 8 00 a m to 6 00 p m Eastern Time at 1 740 373 4763 Direct 1 800 438 4851 Toll Free U S and Canada 1 877 213 8051 FAX http www thermoscientific com Internet Worldwide Web Home Page service led marietta thermofisher com Service E Mail Address Our Sales Support staff can provide information on pricing and give you quotations We can take your order and provide delivery information on major equipment items or make arrangements to have your local sales representative contact you Our products are listed on the Internet and we can be contacted through our Internet home page Our Service Support staff can supply technical information about proper setup operation or troubleshooting of your equipment We can fill your needs for spare or replacement parts or provide you with on site service We can also provide you with a quotation on our Extended Warranty for your Thermo Scientific products Whatever Thermo Scientific products you need or use we will be happy to discuss your applications If you are experiencing technical problems working together we will help you locate the problem and chances are correct it yourself over the telephone without a service call When more extensive service is necessary we will assist you with direct factory trained technicians or a qualified service organization for on the spot repair If your service need is covered by the warranty we will
51. pack Remove solution syringe from wrapper 7 Remove luer cap on system injection port located on the right side of the cartridge pack manifold by turning counterclockwise 8 Remove syringe luer cap and attach syringe to the system luer fitting Figure 7 2 Injecting Cleaning Solution Nanopure Analytical 7 3 Section 7 Initial Operation 7 4 System Cleaning Procedure cont Nanopure Analytical 9 Slowly inject solution into system and remove syringe Avoid injecting air into the system 10 Replace luer cap on injection port and close door 11 Press the UP or DOWN arrow to select YES and then press ENTER Display will now read Reconnected Water 12 Attach feed water supply removed in Step 4 Warning Avoid splashing cleaning solution on clothing or skin Ensure all piping connections are tight to avoid leakage Ensure adequate ventilation Carefully follow manufacturer s safety instructions and material safety data sheets This device to be used with water feeds only Cleaning agents must be used in compliance with instructions in this manual Failure to comply could result in explosion and personal injury Note After cleaning is complete the cleaning timer will need to be reset refer to Resetting the Cleaning Timer for another six month timing sequence 13 Press the UP or DOWN arrow to select YES and press ENTER Display will now read Unit Cleaning 14 Uni
52. r no product flow from 0 2 micron filter clogged the dispense arm or remote dis penser if attached Feed water not connected Reconnect feed water Pump protector in reservoir feed water line pressure switch or Connect the pump protector jumper plug or pressure switch cord to jumper plug not connected to pump the receptacle located on the upper left hand section of the Nanopure Display reads Check Inlet and pump does not run Open feed water line shut off connect feed water line to Nanopure and ensure sufficient pressure or sufficient water level in the feed water reservoir Air in cell If you just started your Nanopure wait 1 minute to see if it corrects Display reads MQ cm for itself more than 10 seconds Bad cell connection Check connection of the cell as it attaches to the circuit board Recirculated water will not rinse up to desired purity level Insufficient feed water pressure or volume to satisfy the Nanopure Exhausted cartridge pack Replace cartridge pack as indicated in Cartridge Pack Replacement Check the expiration date Cartridge packs begin to lose capacity after being stored for 2 years from the date of manufacture Replace the cartridge pack with an unexpired one Cartridge pack is beyond expiration Short cartridge pack life date Thermo Scientific Nanopure Analytical 13 1 Section 13 Troubleshooting If a ROpure is the feed water source check
53. rn off the Nanopure Analytical and disconnect it from the power supply by removing the power cord directly below the main power switch on right side of unit Locate the fuse drawer above the power cord receptacle Pull out the fuse drawer located in the power entry module Remove old fuses and replace with fuses of the same type and rating See Replacement Parts Replace fuse drawer Reattach the power cord Operate normally Warning Replace fuses with those of the same type and rating If the Nanopure Analytical is to be shut down for an extended period of time the unit should be completely drained and the cartridge pack removed to prevent the growth of bacteria If the system has remained inactive and full of water for more than 96 hours the unit should be drained cleaned and new cartridge pack installed prior to use Thermo Scientific Section 13 Troubleshooting Ensure Nanopure power cord is connected to a live power source and No electrical power to Nanopure completely plugged into electrical outlet as well as power entry mod ule on the unit Make sure on off switch is in the I on position Main fuse s blown Replace the main fuse s as indicated in Fuse Replacement Power supply fuse blown i Technical Services concerning power supply fuse replace Replace final filter as indicated in 0 2 Micron Filter Replacement section Nanopure completely inactive pump and display not operating Reduced o
54. s ENTER 3 Press ENTER to proceed through the options until Set Display Brightness is displayed 4 Press the UP or DOWN arrow to choose Yes 5 Press ENTER 6 Press the UP or DOWN arrow until the desired value 100 75 50 or 25 is displayed 7 Press ENTER 8 Press BACK until you return to the Idle display Setting the Displayed From the Idle mode when display reads Nanopure Idle xx xx xx Langu age xx xx xx press the BACK switch until the display reads LANGUAGE 2 The currently selected language is displayed on line 2 of the display 3 Press the UP or DOWN arrow to select the language desired 4 Press ENTER Thermo Scientific Nanopure Analytical 9 1 Section 9 User Settings Setting the Date and 1 From the Idle mode when the display reads Nanopure Idle Time xx xx xx press the UP or DOWN arrow until display reads Advanced 2 Press ENTER 3 Press ENTER when the unit displays Printer Attached 4 When prompted with Date Format press the UP or DOWN arrow to show the date format desired Press ENTER to select the desired format and continue 5 When prompted with Set Date press the UP or DOWN arrow to choose Yes then press ENTER 6 Press the UP or DOWN arrow until you reach the desired month Press ENTER 7 Press the UP or DOWN arrow until you reach the desired day Press ENTER 8 Press the UP
55. t may now be left unattended until display reads Cleaning Complete Press ENTER 15 After cleaning is complete the unit will return to the Idle mode 16 Press the START STOP switch to return the unit to the normal recirculation mode 17 Remove the new 0 2 micron filter and bell assembly Figure 7 3 from the bag and insert it into the dispenser arm manifold Gently turn it clockwise until it is fully seated Thermo Scientific Section 7 Initial Operation System Cleaning 18 Remove the protective cap from the filter bell Turn the dispense knob Procedure cont to the left or right and flush 1 2 liters of water through the 0 2 micron filter The product water is now ready for use Note For more demanding applications where low TOC water is required a rinse of 15 20 liters through the cartridges and 0 2 micron filter may be necessary Caution Never dispense water without first installing hose barb provided in parts bag or final filter supplied with cartridge pack He 0 2 Micron Filter Figure 7 3 Installing 0 2 Micron Filter Thermo Scientific Nanopure Analytical 7 5 Thermo Scientific Section 8 Normal Operation 1 Turn the system power ON by depressing the main power switch to the I position 2 The system greeting display indicates the type of unit you own This greeting is Base 3 The system ele
56. te From the normal recirculating mode when the display is showing purity press ENTER to show the current temperature The temperature will display for about 5 seconds before returning to the normal recirculating mode A Nanopure Analytical 8 1 Section 8 Normal Operation Dispensing Water Use the dispense knob for manual dispensing or use the Dispense switch for volumetric or timed dispensing See User Settings Automatic Dispe nsing This feature Factory set to OFE is accessible only from the normal recirculating mode when the display is showing purity 1 Place a container under the dispenser 2 Press DISPENSE Water will start dispensing immediately Display will read xx MO cm xx Liters Remaining or xx Seconds Remaining or AUTO DISPENSE lt OFF gt depending on which dispensing method was last chosen in the auto dispense menu Note Press any switch except ENTER to stop dispensing Display will read Auto Dispense Interrupted by User Note If the Nanopure Auto Dispense feature is set to TIME a connected Accudispense accessory if applicable will not automatically dispense 8 2 Nanopure Analytical Thermo Scientific Section 9 User Settings Adjusting Display From the Idle mode when the display reads Nanopure Idle Brightn ess xx xx xx press the UP or DOWN arrow until display reads Advanced Menu 2 Pres
57. ytical Thermo Scientific Section7 Initial Operation Cartridge packs will come bagged with four manifold connection caps Part Application Diamond Kit Organic Free R O amp Distilled Feed D50280 Ultra Low Organics Type 1 Water Reverse Osmosis or Distilled Water Feed Diamond Kit Organic Free Deionized Feed 050281 Ultra Low Organics Type 1 Water Deionized Water Feed Diamond Kit 1 R O amp Distilled Feed D50282 Low Organics Type 1 Water Reverse Osmosis or Distilled Water Feed Diamond Kit Type 1 Deionized Feed D50283 Low Organics Type 1 Water DI Water Feed Each cartridge pack includes one 0 2 micron absolute final filter Cartridge Pack Warning Depressurize system prior to removing cartridge pack Installation Manifold 1 Open front left side door Turn the cartridge pack so the caps are facing you Remove the caps 2 Verify that each of the four posts on the cartridge pack has an o ring 3 Lift unit manifold upwards insert cartridge pack and align the pack so that it mates with the unit manifold 4 Lower unit manifold until it is flush with the top of the al cartridge pack Figure 7 1 Cartridge Pack Installation Thermo Scientific Nanopure Analytical 7 1 Section 7 Initial Operation Cartridge Pack Install 7 2 continued Initial Rinse Nanopure Analytical 5 Hand tighten wing head screws securely 6 Close door Note Do not install the 0 2 micron
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