Vial Cleaning System Manual
Contents
1. LIMITED WARRANTY Savillex Corporation Savillex warrants its products against defects in materials and workmanship for 90 days from the time of shipment Savillex makes no warranty express or implied with respect to any components products information or services provided by any third party Upon Savillex s confirmation of defects Buyer s EXCLUSIVE REMEDY shall be for Savillex at Savillex s option and subject to return of the defective product to repair or replace the defective product or to refund the price paid by Buyer for such product Warranty coverage excludes product damage which Savillex determines is due to accident misuse or lack of reasonable care Buyer s warranty rights are subject to Savillex being promptly notified in writing upon discovery of a warranty claim with a detailed explanation of the defect and the claimed defective product being received by Savillex freight prepaid within 30 days after expiration of the warranty period EXCEPT AS STATED IN THIS DOCUMENT NO OTHER WARRANTY EXPRESS OR IMPLIED IS GIVEN OR AUTHORIZED BY SAVILLEX IMPLIED WARRANTIES OF MERCHANTABILITY AND FITNESS FOR A PARTICULAR PURPOSE ARE EXPRESSLY DISCLAIMED LIMITATION OF LIABILITY SAVILLEX DISCLAIMS AND IS NOT LIABLE FOR ANY SPECIAL INDIRECT INCIDENTAL OR CONSEQUENTIAL DAMAGES OF ANY NATURE OR TYPE WHETHER ARISING OUT OF WARRANTY OR OTHER CONTRACT NEGLIGENCE OR OTHER TORT OR OTHERWISE INCLUDING WITHOUT LIMITATION FORESEEABLE LOS2. Measurement Vial Cleaning System Diameter with lid 185 mm 7 28 in Spare Parts Sold Separately Vial Cleaning System Height with pour spout 400 mm 15 75 in Vial Cleaning System Empty Weight with pour spout 2 100 g 4 63 Ibs 3 4 Vent Nut Assembly 1 4 vent nut 9 mm PTFE membrane PTFE retaining ring Description Part Number 3 8 Knurled Ferrule Cap Nut 750 FP6 Used to close pour spout assembly Yo Ferrule Nut Cleaning Container 550 740 400835 Used to attach pour spout assembiy to cleaning container lid 2 3 Brim Capacity 4 500 mL 1 2 gal Maximum Temperature Rating hotplate setting 450 F 230 C Pressure Rating iP Slat 755025 Guidelines for Use Opening the Vial Cleaning System 1 Place the silicone grip mat on a flat rigid surface 2 Place the closed sealed cleaning container on the silicone grip mat 3 Place both hands on the sealing ring and press downwards 4 Turn the sealing ring in a counter clockwise direction until removed Closing the Vial Cleaning System 1 Place the silicone grip mat on a flat rigid surface 2 Place the cleaning container on the silicone grip mat Place the cleaning container lid on top of the cleaning container 4 Thread the sealing ring onto the cleaning container in a clockwise direc tion until the sealing ring makes face contact with the cleaning container lid 5 Place both hands on the sealing ring press dovvnvvards and turn clock vvise unti
3. with a thermocouple to prevent overheating and damaging the vial cleaning system 5 Due to the thermal insulation properties of PFA the hotplate temperature setting will need to be higher than the desired internal liquid temperature in order to obtain the desired internal liquid temperature WARNING Do not use the vial cleaning system on a hotplate surface above 450 F 230 C Exceeding this temperature may cause irreversible damage to the vial cleaning system 6 Atthe end of the desired heating time remove the vial cleaning system from the hotplate and allow the contents to cool to room temperature DANGER The vial cleaning system will be hot to the touch Wear appropriate personal protective equipment when handling NOTE The vent nut assembly while allowing gas to escape will retain acid vapors inside the vial cleaning system The vial cleaning system can be heated for several days without losing a significant amount of liquid volume to evaporation WARNING Do not attempt to remove the threaded sealing ring or cleaning container lid while heating or when hot Although the container vents through the vent nut assembly a small amount of pressure and acid vapor may build up inside the vial cleaning system Emptying the Vial Cleaning System DANGER Take appropriate precautions during filling with and dispensing of acid Always wear recommended safety apparel when handling or working with acids In case of contact flush with c
4. S LOST PROFITS AND RELIANCE DAMAGES IN NO EVENT SHALL SAVILLEX S LIABILITY UNDER ANY CAUSE OF ACTION RELATING TO A PRODUCT EXCEED THE PURCHASE PRICE OF THE PRODUCT Visit www savillex com for complete sales terms and conditions Savillex Your Fluoropolymer Solutions Partner Savillex Corporation 10321 West 70th St Eden Prairie MN 55344 3446 USA Phone 952 935 4100 Fax 952 936 2292 Email info Savillex com www savillex com SMO02 020515
5. Savillex Y Fluoropolymer Soluti Part Vial Cleaning System User s Manual The vial cleaning system provides the safest and most efficient method for Materials of Construction heated soaking and cleaning PFA vials and labware It is designed to be a direct ECTFE sealing ring replacement for glass beakers used by many labs for this process PTEE filter membrane and retaining ring in 4 vent nut assembly PFA all other parts Liability Disclaimer Every effort has been made in the preparation of this publication to provide Unpacking and Inspection the user with the most current correct and clearly expressed information Open the shipping carton and remove the and instructions required for use and operation of the vial cleaning system vial cleaning system Note that some parts Savillex Corporation assumes no liability or responsibility for damages resulting are inside the cleaning container Check from errors omissions and accuracy of the information in this manual The all of the components against the below information included has been compiled from a variety of sources and is subject packing list and inspect for shipping to change vvithout notification Savillex Corporation makes no vvarranties damage such as cracks scratches dents or representations regarding the quality content completeness suitability etc Should any components be missing adequacy sequence accuracy or timeliness of such information If you discove
6. eet MSDS for safe handling instructions 1 Place both hands around the middle of the sealed cleaning container 2 Slide both hands upward until you contact the external flange ring 3 Securely grasp the cleaning container with hands at this location and lift to transfer Heating the Vial Cleaning System The vial cleaning system should ONLY be operated under an acid fume hood Although the liquid will remain fully contained within the cleaning container some acidic vapors will be released through the vent opening in the cleaning container lid WARNING Do not use the vial cleaning system on a hotplate surface above 450 F 230 C Exceeding this temperature may cause irreversible damage to the vial cleaning system 1 Securely transfer the filled and sealed vial cleaning system to the hotplate 2 Make sure that the vent nut assembly is installed and secured Never plug the vent port while heating 3 Use the recommended hotplate temperature settings below to achieve your desired internal liquid temperature NOTE Internal liquid temperature may vary depending on the liquid used for cleaning i e acid concentration Hotplate Temperature Approx Internal Liquid Approx Time to Reach Setting Temperature Internal Liquid Temperature 392 F 200 C 194 212 F 90 100 C 320 F 160 C 158 176 F 70 80 C 4 Because of the possible variability of hotplate surface temperature we recommend that you verify the surface temperature
7. l you cannot rotate the sealing ring any further approximately Va turn more z Filling the Vial Cleaning System DANGERI Take appropriate precautions during filling vvith and dispensing of acid Alvvays wear recommended safety apparel when handling or working with acids In case of contact flush with copious quantities of water See reagent manufacturer s material safety data sheet MSDS for safe handling instructions 1 Place items to be cleaned inside the cleaning container 2 Place the cleaning container on the silicone grip mat 3 Fill the cleaning container with cleaning solution to a level not to exceed the external flange ring 4 Place the cleaning container lid on top of the cleaning container 5 Follow the previously prescribed closing instructions to seal the vial cleaning system 6 Make sure that the 72 cap nut and 1 4 vent nut assembly are securely tightened NOTE Alternatively you may install the pour spout instead of the Y cap nut and use the 3 8 cap nut on the pour spout to close seal the vial cleaning system Refer to the section on emptying the cleaning container for installing the pour spout assembly Handling the Filled Vial Cleaning System DANGER Take appropriate precautions during filling and dispensing of acid Always wear recommended safety apparel when handling or working with acids In case of contact flush with copious quantities of water See reagent manufacturer s material safety data sh
8. opious quantities of water See reagent manufacturer s material safety data sheet MSDS for safe handling instructions 1 Allow the vial cleaning system and contents to reach room temperature 2 If the pour spout assembly was not previously installed remove the 12 cap nut from the lid and attach the pour spout assembly Slide Y2 fitting onto tube past groove Insert grooved tube end into port fitting until it bottoms out Thread ferrule nut to port fitting and hand tighten Pull on tubing SLOWLY until you feel the ferrule catch on the grooved edge Re tighten the fitting hand tight 3 Remove the 3 8 knurled ferrule cap nut from the end of the pour spout assembly 4 Securely grasp the cleaning container with both hands as previously described and tilt to pour into an approved collection vessel Loosening the vent nut assembly will allow the contents to empty faster It is not necessary to remove the vent nut assembly completely as the holes in the side of the nut allow air to enter the vial cleaning system 5 Open the vial cleaning system as previously described and carefully remove the contents Service and Maintenance The vent nut assembly P N 550 740 300731 is the only part that requires any maintenance The complete vent nut assembly is easily removed and should be replaced periodically as determined by the cleanliness of your application Do not allow the vent nut assembly to become dirty or clogged Warranty and Liability
9. r or damaged contact your local distributor any errors or omissions we encourage you to contact Savillex immediately or Savillex Danger Categories and Signal Words Signal words described below are highlighted in boldface and used in connection with warnings throughout this manual For your own safety and to avoid property damage please observe these warnings System Components Included DANGER Denotes most severe hazards Failure to follow safety instructions is likely to cause severe personal injury death or severe property damage Description WARNING Denotes less severe hazards Failure to follow safety instructions may li cause severe personal iniury death or severe property damage 1 Pour Spout Assembly 1 2 ferrule nut 3 8 cap nut pour spout Oualified Users 2 Sealing Ring This product is intended as an experimental tool for research and development in the laboratory by gualified analytical chemists Only those individuals that have adequate technical training knowledge and demonstrated expertise should use it Observe all safety procedures and best laboratory practices to 4 Cleaning Container assure safe operation As in all laboratory operations the user must assure that 5 Silicone Grip Mat O adeguate safety procedures are established to protect all personnel from the potential hazards in the use of this product Ki 550 740 400817 Specifications 7 Y Cap Nut Cleaning Container 550 740 600586 Description
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