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1. 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH TUVRheinland 8 Luftreinhaltung z Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 1 9 Oder Annex 5 Measured values from field test sites related to actual conditions Page 5 of 22 Manufacturer Thermo Fisher Scientific Suspended particulate matter PM10 Type of instrument TEOM 1405 F Measured values in yg m ACT Serial No SN 20006 amp SN 20107 No Date Ref 1 Ref 2 Ref 1 Ref 2 Ratio SN 20006 SN 20107 Remark Test site PM2 5 PM2 5 PM10 PM10 PM2 5 PM10 PM10 PM10 ug m ug m ug m ug m ug m ug m 121 5 31 2010 13 2 13 0 62 8 20 0 SN 20006 noisy signal Teddington 122 6 1 2010 15 2 15 5 76 0 20 7 SN 20006 noisy signal Summer 123 6 2 2010 12 4 11 9 69 5 19 7 SN 20006 noisy signal 124 6 3 2010 9 0 8 8 57 1 15 8 SN 20006 noisy signal 125 6 4 2010 17 8 17 9 67 9 29 8 SN 20006 noisy signal 126 6 5 2010 17 3 16 4 70 1 29 1 SN 20006 noisy signal 127 6 6 2010 7 3 6 4 59 8 15 2 SN 20006 noisy signal 128 6 7 2010 4 0 3 7 51 9 8 2 SN 20006 noisy signal 129 6 8 2010 4 5 4 4 46 5 10 7 SN 20006 noisy signal 130 6 9 2010 11 3 9 8 66 9 15 3 SN 20006 noisy signal 131 6 10 2010 7 8 7 6 73 1 12 6 SN 20006 noisy s
2. 0 10 20 30 40 50 60 70 80 90 100 Reference yg m Figure 36 Reference equivalence function SN 20006 test site Teddington Summer Reference vs SN 20107 Teddington Summer 100 Measured values 90 80 Regression line 70 E so L p y Z freee Acceptance range gt according to EN 12341 g 50 y x 40 amp 30 oO 10 0 10 20 30 40 50 60 70 80 90 100 Reference yg m Figure 37 Reference equivalence function SN 20107 test site Teddington Summer 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Fr Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page liner 42s Reference vs SN 20006 Cologne Winter 100 Measured values 90 80 Regression line 7 Bose a ee oe ts al Fes eeee Acceptance range gt according to EN 12341 g 50 y x 40 S 30 j Eee 20 10 0 10 20 30 40 50 60 70 80 90 100 Reference yg m Figure 38 Reference equivalence function SN 20006 test site Cologne parking lot Ref
3. 740300_2011_936_21209885B_eng doc TUVRheinland Precisely Right TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 195 of 422 Annex 5 PM10 measured values from field test sites related to standard conditions EN 12431 Page 21 of 22 Manufacturer Thermo Fisher Scientific Suspended particulate matter PM10 Auf enluft Type of instrument TEOM 1405 F Measured values in g m STD Serial No SN 20006 amp SN 20107 No Date Ref 1 Ref 2 Ref 1 Ref 2 Ratio SN 20006 SN 20107 Remark Test site PM2 5 PM2 5 PM10 PM10_ PM2 5 PM1q PM10 PM10 ugm pg m ug Nm yg Nm ug Nm ug Nm 271 8 10 2011 12 8 13 6 14 9 14 3 Bornheim 272 8 11 2011 12 2 12 1 10 3 11 9 Summer 273 8 12 2011 6 9 7 6 5 9 9 1 274 8 13 2011 11 1 9 0 275 8 14 2011 7 5 7 2 4 6 8 8 276 8 15 2011 14 3 14 9 15 4 16 4 277 8 16 2011 14 5 13 8 15 4 16 9 278 8 17 2011 27 8 27 2 28 8 30 2 279 8 18 2011 18 2 17 4 23 4 23 1 280 8 19 2011 14 1 13 6 15 9 17 1 281 8 20 2011 19 2 17 4 282 8 21 2011 18 4 18 7 21 9 21 3 283 8 22 2011 21 1 20 8 23 7 26 0 284 8 23 2011 32 4 32 9 36 6 39 0 285 8 24 2011 1
4. 100 Measured values 90 80 Regression line 70 jy SE ie a en ae E eal essere Acceptance range gt according to EN 12341 g 50 y x 40 S 30 j Pa 20 10 0 10 20 30 40 50 60 70 80 90 100 Reference yg m Figure 34 Reference equivalence function SN 20006 test site Teddington Winter Reference vs SN 20107 Teddington Winter 100 Measured values 90 80 Regression line 70 go __ ee frre Acceptance range a according to EN 12341 2 50 y x 3 40 ao S 30 oO 20 10 0 10 20 30 40 50 60 70 80 90 100 Reference yg m Figure 35 Reference equivalence function SN 20107 test site Teddington Winter 740300_2011_936_21209885B_eng doc a T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 118 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Reference vs SN 20006 Teddington Summer 100 Measured values 90 80 Regression line 70 so __ y ee i o Acceptance range 2 according to EN 12341 g 50 y x 40 3 S 30 2 oe 20 10
5. O 10 20 30 40 50 60 70 80 90 100 110 120 130 Candidate 1 yg m Figure 60 Results of the parallel measurements with the candidates SN 20006 SN 20107 measured component PM all test sites values 2 30 g m 1405 F SN20006 SN20107 Alle Standorte lt 30 yg m Rohwerte 130 120 110 100 Messwerte 90 Regressionskurve 80 seeeecs y x 70 60 Pr fling 2 yg m 50 40 30 20 10 0 10 20 30 40 50 60 70 80 90 100 110 120 130 Pr fling 1 yg m Figure 61 Results of the parallel measurements with the candidates SN 20006 SN 20107 measured component PM o all test sites values lt 30 g m 740300_2011_936_21209885B_eng doc a s T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 148 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 1 5 4 10 Calculation of the expanded uncertainty of the instruments For the test of PM25 measuring systems the equivalency with the reference method shall be demonstrated according to chapter 9 5 2 2 to chapter 9 5 4 of the guidance document Demonstration of Equivalence of Ambient Air Monitoring Methods in the field test at least at
6. 17 5 17 0 16 5 16 0 15 0 17 01 2011 16 02 2011 18 03 2011 17 04 2011 17 05 2011 Figure 51 Total flow rate at candidate SN 20006 Cologne Winter PM10 20107 6 min Col W 2011 200 PM10 20107tmoTEOMAMC_0 tmoTEOMAFilterLoad_0 180 160 140 120 100 80 60 40 20 0 17 01 2011 16 02 2011 18 03 2011 17 04 2011 17 05 2011 16 06 2011 Figure 52 Course of time of the PM concentration ug m and the filter load Candidate SN 20107 Cologne Winter 740300_2011_936_21209885B_eng doc A TUVRheinland Precisely Right Page 138 of 422 TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 3 3 3 2 3 1 3 0 2 9 2 8 17 01 2011 16 02 2011 18 03 2011 17 04 2011 17 05 2011 16 06 2011 PM10 20107 6 min Col W 2011 tmoTEOMAFlowMass_0 Limit TEOM Flow Figure 53 PM flow rate at candidate SN 20107 Cologne Winter 18 0 17 5 17 0 16 5 16 0 15 5 15 0 17 01 2011 16 02 2011 18 03 2011 17 04 2011 17 05 2011 PM10 20107 6 min Col W 2011 Total flow Limit Total Flow Figure 54 Total flo
7. O 10 20 30 40 50 60 70 80 90 100 Candidate 1 yg m Figure 45 Result of the parallel measurements with the candidates SN 20006 SN 20107 test site Teddington Summer 100 SN 20006 vs SN 20107 Cologne Winter 90 80 70 60 50 40 Measured values Regression line Acceptance range according to EN 12341 y x 30 20 10 Candidate 2 yg m O 10 20 30 40 50 60 70 80 90 100 Candidate 1 yg m Figure 46 Result of the parallel measurements with the candidates SN 20006 SN 20107 test site Cologne parking lot 740300_2011_936_21209885B_eng doc A TUVRheinland Precisely Right Page 126 of 422 TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 100 SN 20006 vs SN 20107 Bornheim Summer Measured values 90 80 Regression line 70 Acceptance range 60 according to EN 12341 50 40 y x 30 Candidate 2 ug m 20 10 40 50 60 70 80 90 100 Candidate 1 yg m Figure 47 Result of the parallel measurements with the can
8. 0 09240 TM1 0 09220 a TM2 0 09200 TM3 gt 0 09180 x Mean TM1 0 09160 Se E ENE S a o Mean TM2 0 09140 e Mean TM3 0 09120 oe 2 0 09100 S 5 10 15 20 25 No of weighing Figure 76 Stability of the control filters 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH M Luftreinhaltung A TUVRheinland Genau Richtig Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 213 01424 Table 36 Stability of the control filters Control filter No Weighing No TM1 TM2 TM3 1 0 09257 0 09155 0 09110 2 0 09258 0 09155 0 09113 3 0 09260 0 09155 0 09115 4 0 09260 0 09157 0 09116 5 0 09262 0 09156 0 09117 6 0 09264 0 09157 0 09116 7 0 09262 0 09154 0 09114 8 0 09260 0 09156 0 09116 9 0 09262 0 09156 0 09113 10 0 09263 0 09160 0 09117 11 0 09263 0 09158 0 09118 12 0 09263 0 09158 0 09117 13 0 09267 0 09160 0 09118 14 0 09265 0 09157 0 09116 15 0 09266 0 09159 0 09119 16 0 09269 0 09162 0 09122 17 0 09268 0 09162 0 09121 18 0 09267 0 09161 0 09121 19 0 09266 0 09161 0 09118 20 0 09268 0 09160 0 09120 21 0 09264 0 09161 0 09117 22 0 09264 0 09159 0 09116 Average 0 09264 0 09158 0 09117 Standard de viation 3 2911
9. Hd JUslquy luloq maq juaIquy ainsseld juaiquy ainjesodway juaiquy SUOH IPUOD JUuaIquy 4 A 9 4 suopuog juawnij su igure F Screens accessible through the Instrument Conditions screen S QeIIBAe JOU UBYM u pp y aie YyoIyM SUOIdOC raaijoe pue pakejdsip sAemje suondo pusabe 4 4 11 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 4 SCREENS AND SETTINGS Ambient Conditions Screen Figure 4 10 Ambient Conditions screen 4 12 Operatine Guine TEOM 1405 F The Ambient Conditions screen Figure 4 10 shows the current ambient conditions for the monitor TEOM 1405 F SElEHTIFIC Instrument Conditiong cmbient Cadilions OF EWS 1 En Gad The Ambient Conditions screen contains the following information e Ambient Temperature This field contains the current ambient tempera ture C at the site This value cannot be edited and will be correct only when the ambient temperature humidity sensor is properly installed e Ambient Pressure This field contains the current ambient pressure atm at the site This value cannot be edited e Ambient Dew Point This field contains the current ambient dew point C at the site This value cannot be edited and will be correct only when the ambient temperature humidity sensor is properly installed e Ambient Relative Humidity This field contains the current ambient pressure atm
10. Cologne 88 31 2 32 0 31 6 1 00 1 987 1 99 20 Winter c SN 20006 Concentration averages device SN 20006 e c SN 20107 Concentration averages device SN 20107 Case Concentration averages of the devices SN 20006 amp SN 20107 Single values can be taken from the annex 5 of the appendix 740300_2011_936_21209885B_eng doc a s T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 102 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 1 5 3 12 Long term drift The long term drift at zero point and reference point shall not exceed the requirements of Table 2 in the field test A value ct at 70 to 80 of the upper limit of the certification range Shall be used as reference point Note This test point is not evaluable for particulate measuring devices on the basis of currently val id Standard versions of the Standard VDI 4202 Part 1 September 2010 and VDI 4203 Part 3 September 2010 due to a lack of defined minimum requirements According to the deci sion of the competent authorities in Germany see Module 5 3 1 alternatively the following specifications of the previous version of Standard VDI 4202 Part 1 June 2002 are referred to The temporal change of the zero point measured value shall no
11. Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 109101482 6 1 5 3 14 Response time The response time rise of the measuring system shall not exceed 180 s The response time fall of the measuring system shall not exceed 180 s The difference between the response time rise and response time fall of the measuring system shall not exceed 10 of response time rise or 10 s whatever value is larger Note This point is not relevant for particulate measuring devices 6 2 Equipment Not applicable 6 3 Performance of test Not applicable 6 4 Evaluation Not applicable 6 5 Assessment Not applicable Minimum requirement fulfilled 6 6 Detailed representation of the test results Not applicable 740300_2011_936_21209885B_eng doc m T V Rheinland Energie und Umwelt GmbH TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 110 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 1 5 3 15 Difference between sample and calibration port The difference between the measured values obtained by feeding gas at the sample and c
12. Select Download Setup in the Commands window of the ePort Main screen The Download Setup Wizard will display Figure 3 29 Select the Next gt button The Select Data screen will display Select the data to download either all data on the instrument or the data since the last download Select the Next gt button The Select Location screen will display Use the Browse button to select a location for the data file downloaded by the software Select the Next gt button The Download Type screen will display Select automatic downloads Select the Next gt button Operatine Guine TEOM 1405 F 3 27 Section 3 Basic OPERATION 7 The Download Schedule screen will display Figure 3 30 Select a starting date and time and a download frequency daily weekly hourly Select the Next gt button Figure 3 30 Download Setup Wizard E gt Download Setup Wizard Download Schedule Setup Schedule for Automated Downloads Frequency Starting 11 16 2006 10 49AM Y once a day Once a week Every 12 hour s 8 The Completing the Download Setup Wizard screen will display Select the Finish button 3 28 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 3 Basic OPERATION Performing a To download data Data Download Figure 3 31 ePort Main screen Pis irent Hp 3 2 Geet Pe oe AET 145A 200080605 PAi aaoo cece EAD ES 105A 2007 20606 g 115A S065 THERMO F
13. 0 10 20 30 40 50 60 70 80 90 100 PM Reference pg m A TUVRheinland Precisely Right Page 157 of 422 Figure 68 Reference vs candidate SN 20107 measured component PM19 Teddington Summer 100 90 4 80 60 50 4 40 PM 1405F FDMS pg m 30 20 4 SN 20006 Cologne Winter 4 10 20 30 40 50 60 70 80 90 100 PM Reference pg m Figure 69 Reference vs candidate SN 20006 measured component PM19 Cologne Winter 740300_2011_936_21209885B_eng doc a s T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 158 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 100 90 a SN 20107 Cologne Winter 80 70 4 60 50 40 PM 1405F FDMS pg m 20 0 10 20 30 40 50 60 70 80 90 100 PM Reference pg m Figure 70 Reference vs candidate SN 20107 measured component PM Cologne Winter 100 90 a SN 20006 Bornheim Summer Z 80 a 70 60 4 50 PM 1405F FDMS pg m 40 50 60 70 80 90 100 PM Reference yg m Figure 71 Reference vs candidate SN 20006 measured component PM1o Bornheim Summer 740300_2011_936_21209885B_eng doc TUV Rh
14. Figure 7 Vacuum pump p n 10 011413 740300_2011_936_21209885B_eng doc ss TUV Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 36 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B The measuring device is operated via touch screen at the front of the device The user can retrieve data and instrument information change parameters as well as perform tests and controls of the functionality of the measuring device TEOM 1405 F SCIENTIFIC TEOM Data MC pg ms 30 Min MC pig ms 1 Hr MC pig ms 8 Hr MC g m 12 Hr MC pg m 24 Hr MC pg m Filter loading 26 14 Frequency 254 7451 Hz Noise 0 002 ug Fully operational Normat status 09 28 2011 12 58 Figure 8 amp Main window of the user display On the first level the main window of the user display is located here the current time the current date the instrument status normal warning the current operational condition e g fully operational stabilizing the mass concentration values MC moving hourly mean every 6 minutes updated 30 min presently not implemented 1h 8h 12h and 24h averages the vibration frequency the noise of the mass measuring and the loading of the TEOM filter are displayed
15. RS Para 3 13010 Optional Up to 3 ASCII codes can be added to response from the instrument In this case lt CR gt and lt LF gt ASCII codes 013 and 010 are appended to the response Enter 0 if nothing is to be appended COCO nome ever temion ERE nse P raat Rom em DEEE 2 digit Channel Number as defined Number of current status conditions of current status conditions E DEAC o e e aa afe Up to 3 digits appended to the end of New location of the Storage Marker TEN the response transmission according to B move to beginning of storage the entry for RS Para 3 buffer E move to end of storage as 250 to move forward by 250 SA as 1000 to move backwards by iaa 1000 records Do not right fill D 0 a Rs 8 a a a ee Oe es o THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F B 9 Appennix B SERIAL COMMUNICATION AK Protocol Response if Command Addressed to Instrument is Unrecognizable COM 2 WAY SETTINGS ASCII code for the 1 digit Station Number for example 4 052 The Station Number is always 1 digit in length ASCII code representation of the 2 digit Channel Number for example KO 075 048 The Channel Number is always 2 digits in length RS Para 3 13010 Optional Up to 3 ASCII codes can be added to response from the instrument In this case lt CR gt and lt LF gt ASCII codes 013 and 010 are appended to the response Enter 0 if nothing is to be appended Transmission to Instrumen
16. Field test days with a relative humidity gt 70 Deviation to average reference Deviation in of average reference Deviation in of ALV Single values can be taken from annex 5 and 6 in the appendix The presentation and the assessment of the measuring uncertainties Wc at the days with a relative humidity gt 70 is made in Table 24 and in Table 25 Single values can be taken from annex 5 and 6 in the appendix 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH F Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 131 01482 Table 24 Comparison candidate 20006 with reference device rel humidity gt 70 all test sites measured component PM Comparison candidate with reference according to Guide Demonstration of Equivalence Of Ambient Air Monitoring Methods January 2010 Candidate 1405 F SN SN 20006 Test site All test sites rH gt 70 Limit value 50 Status of measured values Raw data Allowed uncertainty 25 Results of regression analysis Slope b 1 01 not significant Uncertainty of b 0 02 Ordinate intercept a 0 90 significant Uncertainty of a 0 41 Results of the equivalence test Deviation at limit value 0 53 g m Uncertainty Uc s at limit
17. On 28 05 2010 it was detected that the output measured values have been very noisy after the zero filter operation The problem was a leaking switching valve which was not changed until 11 06 2011 due to communication problems All measured values between 28 05 2011 and 11 06 2011 were rejected SN 20107 On 28 09 2011 the device had to be stopped in order to fix a leak No further malfunctions of the devices have been observed The regular cleaning of the sampling inlets in the maintenance interval the change of the TEOM filter the 47 mm filter approx every 4 weeks and the regular check of the flow rates respectively of the tightness can lead to outages of more than 2h per device especially when all is done on one day The affected daily averages in this case have been rejected 740300_2011_936_21209885B_eng doc a s T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 82 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 5 Assessment The availability was 94 5 for SN 20006 98 6 for SN 20107 without outages due to test conditions or 88 6 for SN 20006 and 92 1 for SN 20107 including outages due to test conditions The high amount of downtime days 15d for SN 20006 caused by the leak switching v
18. The TEOM Data screen includes menu buttons allowing users to access the other main screens The status bar at the bottom of the screen displays operating information including the current operating mode lock mode and date and time as well as the current status Normal or Warning s Note Upon initial instrument start up the values in the mass concentration fields are the running averages that are accumulated until a 1 hour time period has passed The values are visible to provide the user with an indication that the instrument is functioning after instrument power up or reset These raw values are used for internal calculations only amp 4 2 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC THERMO FISHER SCIENTIFIC Section 4 SCREENS AND SETTINGS The TEOM Data screen contains the following information MC ug m This field contains the mass concentration value The unit calculates the mass concentration MC value by subtracting the Ref MC from the Base MC This is a one hour average updated every 6 minutes This value cannot be changed by the user 01 Hr MC ug m This field contains the 1 hour mass concentration average This is a sliding average that is updated every 60 minutes on the hour This value cannot be changed by the user 08 Hr MC ug m This field contains the XX hour mass concentration average The user may set value to any whole number greater than 1 This is a sliding average tha
19. Z 6 Loosen the sample tube fitting on the top plate of the 1405 F tower then push the dryer back while lifting the switching valve slightly then partially remove it from the tower It will still be connected by the tubes leading to the cooler Select the Next gt button 7 The Clean Valve screen will display Clean the chamber of the switching valve with the cleaning brush do not use a cleaning solution provided with the system Figure 5 46 Select the Next gt button Figure 5 46 Cleaning the valve with the valve brush 5 36 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 8 The Reinstall screen will display Set the switching valve back into the system ensuring that the empty quick connect fitting is located on the top of the switching valve 9 Tighten the two Swagelok connections Tighten them finger tight at first then turn them 1 1 4 turns with the wrench 10 Reinstall the tubing into the quick connect fitting on the top of the switching valve 11 Reinstall the cover of the unit and tighten the sample tube fitting at the top of the unit Select the Next gt button 12 The wizard will display a message showing the procedure is complete Figure 5 47 Select the Finish button to exit the wizard and return to the Maintenance screen or select the lt Back button to move backward one step in the procedure Figure 5 47 Completing the Valve Complet
20. 10 Perform a leak check refer to the following section for leak check information Install a TEOM filter into the mass transducer Section 5 Install a 47 mm filter into the FDMS tower Section 5 When in the System Status screen ensure that the serial number listed for the instrument matches the serial number on the back of the unit When in the Instrument Conditions screen select the Flows button to display the Flows screen Select the Flow Rates button to select the desired flow rates for the Main and Bypass flow channels Select the Flow Control button to select the desired flow control Active or Passive and the desired standard and average temperatures and pressures Refer to Section 4 for more information on screens and settings When in the Settings screen select the System button then the Set Time button to set the current date and time Refer to Section 4 for more information on screens and settings When in the Settings screen select the Advanced button then the Mass Transducer KO Constant button to confirm the current KO setting for the TEOM The number programmed into the unit must match the KO constant on the label near the mass transducer Refer to Section 4 for more information on screens and settings When in the Settings screen select the Data Storage button to display the Data Storage screen Confirm the desired data is selected to be logged by the instrument Refer to Storing Data
21. Instrument conditions the user may control and modify different settings of the instrument regarding temperature and flow rates as well as inform him about ambient condi tions of the instrument 740300_2011_936_21209885B_eng doc A T VRheinland T V Rheinland Energie und Umwelt GmbH Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 40 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B TEOM 1405 F SCIENTIFIC amp yer womans a on 128 Figure 12 Menu Settings In the menu Settings the user has access to system data and advanced settings At this point e g date time can be set the password protection can be activated analogue and digi tal output can be parameterized or the calibration constant Ko can be displayed 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 P 41 of 422 Report No 936 21209885 B ORE BAR TEOM 1405 F SCIENTIFIC C Figure 13 Menu Service In the menu Service all implemented procedures for the instrument main
22. Section 4 SCREENS AND SETTINGS Operating Mode 4 6 Operatinc Guine TEOM 1405 F The TEOM 1405 Monitor displays its current operating mode in the lower left hand corner of TEOM Data screen Figure 4 2 and most of the other instrument screens The unit s operating modes Figure 4 2 are defined as follows Stabilizing This operating mode indicates that the unit has not begun to compute mass values because the monitor s temperatures and flow rates are stabilizing The temperatures and flow rates must remain within a very narrow range of values for 30 minutes before the instrument enters the next operating mode The monitor always starts in Stabilizing Mode when it is turned on or reset Collecting Data This operating mode indicates that the unit has begun to collect data records but the monitor has not yet computed its first mass concentration value Computing Data This operating mode indicates that the unit has computed the first mass concentration value Fully operational This operating mode indicates that the unit is fully operational The monitor normally resides in this mode All mass values are being computed by the instrument Setup Mode When the unit is in this operating mode it continues to draw a sample flow and maintain operational temperatures but it does not collect any data Certain operating parameters such as temperatures and flow rates can be changed only in this mode because doing so during data coll
23. T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 16 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Thermo Fisher Scientific has commissioned TUV Rheinland Energie und Umwelt GmbH with the performance of a suitability testing of TEOM 1405 F Ambient Particulate Monitor for the component PM10 The suitability testing of the measuring system was carried out applying the following standards and requirements e Standard VDI 4202 Part 1 Minimum requirements for suitability tests of automatic ambient air measuring systems Point related measurement methods of gaseous and particulate pollutants September 2010 or June 2002 e Standard VDI 4203 Part 3 Testing of automatic measuring systems Test proce dures for point related ambient air quality measuring systems of gaseous and particu late pollutants September 2010 or August 2004 e Standard EN 12341 Ambient air quality determination of the PM fraction of sus pended particulate matter Reference method and field test procedure to demon strate reference equivalence of measurement methods German version EN 12341 1998 e Guide Demonstration of Equivalence of Ambient Air Monitoring Methods English version of January 2010 The m
24. The competent German body agreed with the proposed procedure by decision of 27 June 2011 respectively 07 October 2011 6 5 Assessment The test was done based on the minimum requirements stated in Standard VDI 4202 Part 1 September 2010 The test points 5 3 2 5 3 7 5 3 8 5 3 11 and 5 3 12 are evaluated as be fore based on the minimum requirements stated in Standard VDI 4202 Part 1 from 2002 i e using the reference values Bo B and B2 The testing of the test points 5 3 3 5 3 4 5 3 13 and 5 3 18 is waived as they are not relevant for particulate measuring devices Minimum requirement fulfilled yes Detailed representation of the test results Not required for this minimum requirement 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH F Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B a 6 1 5 3 2 Repeated standard deviation at zero point The repeatability standard deviation at zero point shall not exceed the requirements of Table 2 in the certification range according to Table 1 of Standard VDI 4202 Part 1 September 2010 In case of deviating certification ranges the repeatability standard deviation at zero point shall not exceed 2 of the upper limit of this cer
25. nal value The criteria for passing the tightness check implemented by the manufac turer a deviation of the flow values at a blocked inlet of no more than 0 15 l min from zero flow at the PM10 path and no more 0 60 l min from ze ro flow at the bypass path were ap proved as appropriate parameters for the monitoring of the device tightness The tightness check may only be per formed using the tightness check as sistant to avoid damages of the in strument 129 132 139 TUV Rheinland Energie und Umwelt GmbH w Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Specification Test result Page filled 5 4 9 Determination of For the test of PM2 5 measur The in between uncertainty between uncertainty be ing systems the uncertainty be the candidates ubs is with a maximum tween systems tween the systems under test of 1 35 g m for PM10 below the re under test ubs shall be determined according quired value of 2 5 yg m to chapter 9 5 2 1 of the guid ance document Demonstration of Equivalence of Ambient Air Page 27 of 422 Monitoring Methods in the field test at least at four sampling test sites representative of the future application 5 4 10 Calculation
26. ug Nm yg Nm ug Nm ug Nm 301 9 9 2011 13 0 12 7 10 5 11 9 Bornheim 302 9 10 2011 14 1 14 3 Summer 303 9 11 2011 10 0 10 0 8 5 10 5 304 9 12 2011 12 4 12 6 9 9 11 6 305 9 13 2011 17 3 17 9 13 4 15 8 306 9 14 2011 16 0 16 5 12 3 13 5 307 9 15 2011 25 3 26 2 23 9 24 2 308 9 16 2011 24 4 26 9 Inlet gt Zero filter 309 9 17 2011 Zero filter 310 9 18 2011 7 4 7 5 Zero filter 311 9 19 2011 13 0 12 3 11 9 11 3 312 9 20 2011 13 0 13 0 13 9 13 3 313 9 21 2011 13 0 13 1 11 1 12 1 314 9 22 2011 20 1 20 0 16 6 16 2 315 9 23 2011 27 3 27 6 25 9 24 6 316 9 24 2011 23 6 21 8 317 9 25 2011 22 5 23 1 23 0 22 5 318 9 26 2011 19 9 22 0 Audits 319 9 27 2011 40 2 42 2 42 0 39 5 320 9 28 2011 27 2 27 2 29 5 SN 20107 leak repairs 321 9 29 2011 27 0 27 0 28 1 31 1 322 9 30 2011 24 6 26 0 24 4 27 2 323 10 1 2011 21 8 24 3 324 10 2 2011 39 8 42 9 325 10 3 2011 22 9 22 9 29 2 32 3 326 10 4 2011 15 9 18 9 327 10 5 2011 6 8 7 2 328 10 6 2011 9 6 11 4 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Sci
27. 3 0 4 0 7 9 7 1 9 2 8 1 7 2 8 5 6 4 6 6 A TUVRheinland Precisely Right Page 203 of 422 Page 7 of 11 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Page 204 of 422 Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Annex 6 Ambient conditions at the field test sites Page 8 of 11 No Date Test site Amb temperature avg Amb temperature max Amb pressure Rel humidity Wind velocity Wind direction Precipitation C C hPa m s 7 mm 211 3 26 2011 Cologne 7 7 11 6 1010 64 8 1 5 105 0 0 212 3 27 2011 Winter 9 3 16 3 1006 60 9 1 1 196 0 0 213 3 28 2011 7 2 13 7 1009 60 2 1 9 172 0 0 214 3 29 2011 9 6 18 5 1007 62 1 1 1 168 0 0 215 3 30 2011 12 6 15 9 1008 66 7 2 4 170 0 0 216 3 31 2011 13 8 15 6 1011 78 2 3 7 230 6 5 217 4 1 2011 13 9 18 8 1014 78 1 2 3 175 0 0 218 4 2 2011 17 6 24 3 1006 62 2 2 6 159 0 0 219 4 3 2011 10 9 15 8 1009 85 3 2 0 251 8 7 220 4 4 2011 10 0 15 0 1017 65 3 2 7 214 0 0 221 4 5 2011 11 8 15 1 1020 71 9 2 1 173 0 9 222 4 6 2011 16 2 23 0 1019 73 9 1 8 196 0 0 223 4 7 2011 13 8 21 6 1019 67 2 3 0 245 0 0 224 4 8 2011 12 9 18 2 1018 64 7 2 9 255 0 0 225 4 9 2011 11 3 18 9 1018 59 8 1 3 183 0
28. Ambient conditions Temperature 8 25 C Humidity Non condensing Sampling flow rate Inlet 16 67 l min 1 m h Flow rate PM Path 3 l min Flow rate Bypass 13 67 l min Filter material TEOM Pallflex TX40 Mass measured values MC moving 1h average updated every 6 minutes 1 Hr MC moving 1h average updated every 60 minutes on the full hour 8 Hr MC moving 8h average updated every 60 minutes on the full hour 12 Hr MC moving 12h average updated every 60 minutes on the full hour 24 Hr MC moving 24h average updated every 60 minutes on the full hour Detector Mass transducer Checks Cont Noise lt 0 1 ug Frequency in the range 150 400 Hz Discont Check of the calibration constant Ko Parameter instrument temperatures 740300_2011_936_21209885B_eng doc aT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 46 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Nominal value for the following instru ment temperatures Mass transducer cap 30 C Mass transducer case 30 C PM air tube 30 C Parameter FDMS Dryer type NAFION Dryer Type C Temperature dryer normal conditions 4 C Dew point of the air flows normal con ditio
29. Department of Environmental Protection kt ie Lt LS Karsten Pletscher Dr Peter Wilbring Cologne November 25 2011 936 21209885 B 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page Welt 422 8 Literature 1 Standard VDI 4202 Part 1 Minimum requirements for suitability tests of automated ambient air quality measuring systems Point related measurement methods of gase ous and particulate pollutants June 2002 amp September 2010 2 Standard VDI 4203 Part 3 Testing of automated measuring systems Test proce dures for point related ambient air quality measuring systems of gaseous and particu late pollutants August 2004 amp September 2010 3 Standard EN 12341 Ambient air quality determination of the PMyo fraction of sus pended particulate matter Reference method and field test procedure to demonstrate reference equivalence of measurement methods German version EN 12341 1998 4 Guide Demonstration of Equivalence of Ambient Air Monitoring Methods English version of January 2010 5 Operating manual 42 0109785 Revision A 000 Sep 22 2009 6 Operating manual LVS3 Statu
30. Measured values in g m STD Serial No SN 20006 amp SN 20107 No Date Ref 1 Ref 2 Ref 1 Ref 2 Ratio SN 20006 SN 20107 Remark Test site PM2 5 PM2 5 PM10 PM10 PM2 5 PM1 PM10 PM10 g m yg m ug Nm _ ug Nm ug Nm ug Nm 121 5 31 2010 21 4 22 1 20 9 SN 20006 noisy signal Teddington 122 6 1 2010 20 7 21 4 21 6 SN 20006 noisy signal Summer 123 6 2 2010 18 5 18 3 20 8 SN 20006 noisy signal 124 6 3 2010 16 3 16 6 16 7 SN 20006 noisy signal 125 6 4 2010 27 6 28 4 31 8 SN 20006 noisy signal 126 6 5 2010 25 5 26 2 31 4 SN 20006 noisy signal 127 6 6 2010 12 3 12 0 16 3 SN 20006 noisy signal 128 6 7 2010 8 2 7 7 8 8 SN 20006 noisy signal 129 6 8 2010 9 8 10 6 11 4 SN 20006 noisy signal 130 6 9 2010 16 6 17 2 16 3 SN 20006 noisy signal 131 6 10 2010 10 9 11 4 13 5 SN 20006 noisy signal 132 6 11 2010 11 1 12 5 r 13 3 Noer measurement Ve Repair leaking switching valve 133 6 12 2010 14 0 14 2 12 7 14 9 134 6 13 2010 18 4 18 8 17 7 19 2 135 6 14 2010 13 9 13 2 13 7 15 5 136 6 15 2010 10 5 10 2 10 1 12 4 137 6 16 2010 11 2 10 8 11 8 13 7 138 6 17 2010 7 4 8 3 10 9 10 8 139 6 18 2010 14 2 15 1 140 6 19 2010 9 4 9 7 9 5 12 3 141 6 20 2010 16 1 16 0 16 9 18 5 142 6 21 2010 21 8 20 0 PM10 Grubbs outlier 143 6 22 2010 13 9 14 7 21 0 17 9 144 6 23 2010 16 2 16 6 21 7 20 3 145 6 24 2010 12
31. Rel humidity A TUVRheinland Precisely Right Wind velocity m s Page 207 of 422 Page 11 of 11 Wind direction Precipitation mm 9 9 2011 9 10 2011 9 11 2011 9 12 2011 9 13 2011 9 14 2011 9 15 2011 9 16 2011 9 17 2011 9 18 2011 9 19 2011 9 20 2011 9 21 2011 9 22 2011 9 23 2011 9 24 2011 9 25 2011 9 26 2011 9 27 2011 9 28 2011 9 29 2011 9 30 2011 10 1 2011 10 2 2011 10 3 2011 10 4 2011 10 5 2011 10 6 2011 Bornheim Summer 19 0 23 8 16 2 19 4 16 7 15 2 14 1 17 1 16 8 13 3 13 6 15 6 16 9 15 2 Outage of weather station 0 4 1 5 0 7 1 7 1 6 1 5 0 6 1 4 1 0 1 0 1 4 0 5 0 8 1 2 167 155 165 204 219 224 207 145 207 200 231 196 204 231 0 0 0 0 16 2 0 0 0 0 0 0 0 0 0 0 3 6 4 5 0 9 0 0 0 0 0 0 740300_2011_936_21209885B_eng doc TUVRheinland TUV Energie und Umwelt GmbH Precisely Right Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Seite 208 von 422 Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Appendix 2 Filter weighing procedure A German test sites Cologne and Bornheim A 1 Carrying out the weighing All weightings are done in an air conditioned weighing room Ambient conditions are 20 C 1 C and 50 5 relative humidity which confor
32. Section 4 SCREENS AND SETTINGS Flow Rates Screen Figure 4 12 Flow Rate screen 4 14 Operatine Guine TEOM 1405 F Select the Flow Rates button in the Flows screen to display the Flow Rates screen Figure 4 12 This screen allows users to adjust the flow rates for the main and bypass flow channels TEOM 1405 F Instrument Conditiong Flaws gt Flow Fale The Flow Rates screen contains the following controls buttons e Main flow rate This field contains the current value of the main path flow rate l min The default setting is 3 1 min To view or adjust the setpoint select the button to display the keypad Figure 4 3 The current value can not be edited e Bypass flow rate This field contains the current value of the bypass flow rate The default setting is 13 67 1 min To view or adjust the setpoint select the button to display the keypad Figure 4 3 The current value can not be edited e Total flow This field contains the current value of the total flow rate of the instrument l min The current value can not be edited THERMO FISHER SCIENTIFIC Flow Control Screen Figure 4 13 Flow Control screen THERMO FISHER SCIENTIFIC Section 4 SCREENS AND SETTINGS Select the Flow Control button in the Flows screen to display the Flow Control screen Figure 4 13 This screen allows users to adjust the flow control method TEOM 1405 F In irument Conditighn amp Flows gt F lew Goniral Volume
33. Section 6 6 of this test point shows the evaluated results A linear correlation y a bx is assumed between the results of both methods in order to evaluate the comparability of the candidates y and the reference procedure x The correlation between the average values of the reference devices and the candidates is established by orthogonal regression Regression is calculated for e All test sites e Each test site separately e 1 data set with measured values PM 2 30 ug m Basis average value of reference measurement For further evaluation the results of the uncertainty uc s of the candidates compared with the reference method are described with the following equation which describes Ucr as a func tion of the PM concentration x 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 14301482 RSS Ee x a b 1 x Usr Yi With RSS Sum of the relative residuals from orthogonal regression u x random uncertainty of the reference procedure if value Ups which is calcu lated for using the candidates can be used in this test refer to point 6 1 5 4 9 Determination of uncertainty between systems under
34. a7 606 12 2002o Aa J OTA BT fsiorzon og os og fz o6 P06 06 03 2011 0 4 00 07 03 2011 05 09 zonm 05 ar os f 08 mon o0 os 01 f o4 s0920 o1 or of 06 measured on 11 01 2010 SN 20006 on 07 03 2010 and SN 20107 on 06 02 2010 and 07 02 2010 TEOM filter not installed correctly strong noise not possible to evaluate SN 20006 on 26 05 2010 strong noise due to a leak at the switching valve measured value rejected 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 10501484 TESNE E PEDE Zero point drift SN20006 6 0 4 0 2 0 0 0 2 0 4 0 Measured value ug m 6 0 Figure 30 Zero point drift SN 20006 measured component PM ee eee Zero point drift SN20107 6 0 4 0 2 0 0 0 2 0 4 0 6 0 Measured value yg m SN N N S S 2 o S O K S N N S O SS o o o O O O NA Na N2 NA V Na V V X No NA a Av we IN oss yw Time Figure 31 Zero point drift SN 20107 measured component PM 740300_2011_936_21209885B_eng doc a s T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinh
35. after the initialization process Figure 4 1 Title screen TEOM 1405 F 1 01 Ambient Particulate Monitor with FDMS Cepit i 11 7 Therm Finke Sarii inc alleys rear Tha popan u priii bp cop pighi fe atd nieromcral Juba This curred LAE by SOL Daima Saren Cisia 2 168 TH Fre tia Fiaa We A eee hee Cia od 8 Seto ohh et dae ory Embi Theta iat Feud Saeed Pat ee Hera The Title screen includes the instrument model and the firmware version of the instrument THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 4 1 Section 4 SCREENS AND SETTINGS TEO M Data Screen After the Title screen the TEOM Data screen will automatically display Figure 4 2 The TEOM Data screen shows the basic operating information as well as status conditions and the instrument operating mode The TEOM Data screen can be displayed by selecting the TEOM Data button in any of the other four main screens System Status Instrument Conditions Settings Service Figure 4 2 TEOM Data screen with menu buttons status and operating and lock modes highlighted r MENU BAR gt System Status S ee MENU BUTTONS 1 Hr ME ugima l B Howur value pgm iE Instrureent 12 Hr ME pigeon Conditions Ba He ME fugim Filter boating Settings Peas Hoke SCREEN INFO aj Fuly opertnesl torza status Ful WATT 1153 STATUS BAR Instrument mode Lock mode Status conditions Current date time warning s
36. atm respectively For the instrument to report mass concentrations according to this EPA standard the user must ensure that the standard temperature Std Temp and standard pressure Std Pres entered in the instrument equal 25 C and 1 Atmosphere Section 4 These are the default values for the instrument Std Temp 273 15 latm Flow_Rate Flow_Rate x ms ae 273 15 Std Pres The flow rates referenced internally by the instrument to 0 C are converted to EPA standard conditions Note When reporting concentrations to actual conditions the system must be set for Active flow control Section 4 This will ensure that the monitor uses the current actual values for temperature and pressure in the equation above a Operatine Guine TEOM 1405 F 1 11 Section 1 INTRODUCTION 1 12 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section2 Setup and Installation This section describes the setup and installation of the TEOM 1405 F including the pump flow splitter tripod sample tube and sample inlet After you have set up the system you must perform a leak check on the monitor Section 3 and install a TEOM filter Section 5 in the mass transducer before starting a sample run If you want to install the monitor in an outdoor location consult Thermo Fisher Scientific for specific site recommendations Figure 2 1 TEOM 1405 Monitor Inlet Flow splitter Tripod TEOM 1405
37. select the Service button to display the Service screen then select the Calibration button to display the Calibration screen Figure 5 48 Select the Mass Transducer KO Verification button to start the KO Verification Wizard Figure 5 79 Select the Next gt button to begin the procedure Welcome to the KO Verification Wizard This wizard helps you verity the callbration constant KO on the TEOM umbient Particulate Monitar The instrument will be pul in Setup mode for RO verification Te continue press Neri Operatine Guine TEOM 1405 F 5 63 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 6 The Install Pre Filter screen will display Figure 5 80 Remove the inlet and install the flow audit adapter onto the flow splitter then install the pre filter assembly the filter and short length of silicone tubing onto the flow audit adapter Figure 5 81 Select the Next gt button Figure 5 80 install Pre Filter A pre lilter fow audit adapter and shori length of scone tubing are supplied wilh the instrument Install Pre Filter screen 5 64 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Figure 5 81 Series 1405 inlet assembly Flow splitter THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 65 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Figure 5 82 Stabilizing screen 5 66 Operatine Guine TEOM 1405 F 7 The Remove Sample
38. 0 12 5 8 2 7 3 23 9 11 2 11 7 12 5 16 1 15 0 20 6 SN 20107 Remark Test site PM10 ug Nm Teddington Winter PM10 Grubbs outlier Device not yet in operation Zero filter PM10 Grubbs outlier PM2 5 Grubbs outlier TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B TUVRheinland Precisely Right Page 187 of 422 Annex 5 PM10 measured values from field test sites related to standard conditions EN 12431 Page 13 of 22 Manufacturer Thermo Fisher Scientific Suspended particulate matter PM10 Auf enluft Type of instrument TEOM 1405 F Measured values in g m STD Serial No SN 20006 amp SN 20107 No Date Ref 1 Ref 2 Ref 1 Ref 2 Ratio SN 20006 SN 20107 Remark Test site PM2 5 PM2 5 PM10 PM10 PM2 5 PM1d PM10 PM10 ugima pg m ugNm3 yg Nm y ug Nm ug Nm 31 1 8 2010 17 9 18 2 16 2 Devi i Teddington evice not yet in 32 1 9 2010 14 5 14 8 13 2 operation Winter 33 1 10 2010 19 4 19 3 17 3 34 1 11 2010 51 5 51 5 48 7 SN 20107 Zero filter 35 1 12 2010 48 5 48 9 48 3 48 0 36 1 13 2010 54 0 54 1 52 3 53 9 37 1 14 2010 16 2 16 6 17 3 17 8 38 1 15 2010 27 2 27 7 19 6 2
39. 0 226 4 10 2011 14 0 23 1 1016 60 2 1 1 191 0 0 227 4 11 2011 16 0 25 0 1012 58 8 3 9 244 2 7 228 4 12 2011 7 7 12 4 1018 66 7 4 1 257 0 9 229 4 13 2011 10 1 14 3 1013 57 1 2 0 203 0 0 230 4 14 2011 8 0 14 2 1013 65 4 0 6 159 0 0 231 4 15 2011 10 4 17 0 1014 53 6 1 2 169 0 0 232 4 16 2011 11 9 16 9 1017 51 7 0 9 166 0 0 233 4 17 2011 11 4 19 2 1017 53 7 1 2 139 0 0 234 4 18 2011 14 3 21 2 1011 48 6 1 9 149 0 0 235 4 19 2011 15 5 25 5 1009 52 4 1 2 146 0 0 236 4 20 2011 16 6 25 7 1008 51 3 1 1 154 0 0 237 4 21 2011 17 8 26 3 1006 54 1 0 7 180 0 0 238 4 22 2011 20 0 27 8 1003 51 8 1 3 146 8 3 239 4 23 2011 18 0 28 9 1005 58 0 0 7 152 0 0 240 4 24 2011 18 1 28 0 1011 51 7 1 0 172 0 0 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Annex 6 Date Test site 4 25 2011 4 26 2011 4 27 2011 4 28 2011 4 29 2011 4 30 2011 5 1 2011 5 2 2011 5 3 2011 5 4 2011 5 5 2011 5 6 2011 5 7 2011 5 8 2011 7 25 2011 7 26 2011 7 27 2011 7 28 2011 7 29 2011 7 30 2011 7 31 2011 8 1 2011 8 2 2011 8 3 2011 8 4 2011 8 5 2011 8 6 2011 8 7 2011 8 8 2011 8 9 2011 Cologne Winter Bornheim Summer Ambient conditions at the field test sit
40. 11 Next look at the status code table to decipher the status code In the 1 000 s place of the table there are three status codes that when added together will total 11 H 1000 Serial Port Problem H 2000 Line Printer Problem and H 8000 Leak on Loop B These are three more of the status codes that the unit is displaying in its status code e In the 10 000 s place of the status code there are no 0 status codes displayed e In the 100 000 s place of the status code 800000 a status code of 800000 is displayed which matches H 800000 Sensor Comm Prob lem e In the 1 000 000 s place of the status code there are no 0 status codes displayed Therefore the downloaded status code 8433666 H 80B002 breaks down into the following status codes according to the example status code table H 2 Power Switch TPIC H 1000 Serial Port Problem H 2000 Line Printer Problem H 8000 Leak on Loop B H 800000 Sensor Comm Problem THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F A 5 Appenpix A TROUBLESHOOTING Notes A 6 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC AK Protocol THERMO FISHER SCIENTIFIC Appendix B Serial Communication The TEOM 1405 Monitor supports AK Protocol This protocol permits a locally or remotely located computer to obtain information electronically from the unit These protocols a
41. 20006 measured component PM19 Teddington Winter 740300_2011_936_21209885B_eng doc a s T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 156 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 100 90 a SN 20107 Teddington Winter ra 80 4 A 70 Pail 60 F 50 v a 2 30 Pa PM 1405F FDMS pg m 0 10 20 30 40 50 60 70 80 90 100 PM Reference ug m Figure 66 Reference vs candidate SN 20107 measured component PM19 Teddington Winter 100 90 a SN 20006 Teddington Summer 80 70 60 50 40 PM 1405F FDMS pg m3 30 20 a4 10 4 4 0 10 20 30 40 50 60 70 80 90 100 PM Reference pg m Figure 67 Reference vs candidate SN 20006 measured component PM19 Teddington Summer 740300_2011_936_21209885B_eng doc TUV Rheinlan d Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 100 90 80 70 60 PM 1405F FDMS pg m a SN 20107 Teddington Summer
42. 2010 17 6 17 7 17 8 18 1 104 5 14 2010 19 7 19 6 19 9 19 9 105 5 15 2010 13 1 13 3 14 3 13 4 106 5 16 2010 9 8 9 9 11 9 11 8 107 5 17 2010 16 6 17 1 18 7 17 8 108 5 18 2010 22 0 22 3 22 2 23 7 109 5 19 2010 20 7 20 2 22 3 22 7 110 5 20 2010 19 5 19 9 25 1 24 2 111 5 21 2010 18 7 19 5 21 6 22 7 112 5 22 2010 9 4 9 4 11 1 12 7 113 5 23 2010 9 9 10 2 13 7 13 3 114 5 24 2010 18 7 18 9 20 8 21 2 115 5 25 2010 16 4 16 0 17 9 18 9 116 5 26 2010 20 0 20 0 Zero filter 117 5 27 2010 8 4 8 3 Zero filter gt Inlet 118 5 28 2010 15 1 14 6 15 7 SN 20006 noisy signal 119 5 29 2010 11 1 11 4 11 9 SN 20006 noisy signal 120 5 30 2010 8 6 8 4 10 2 SN 20006 noisy signal 740300_2011_936_21209885B_eng doc A TUVRheinland Precisely Right Page 190 of 422 Annex 5 TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B PM10 measured values from field test sites related to standard conditions EN 12431 Page 16 of 22 Manufacturer Thermo Fisher Scientific Type of instrument TEOM 1405 F Suspended particulate matter PM10 Auf enluft
43. 20107 No Date Ref 1 Ref 2 Ref 1 Ref 2 Ratio SN 20006 SN 20107 Remark Test site PM2 5 PM2 5 PM10 PM10 PM2 5 PM10 PM10 PM10 ugm pg m ugNm3 yg Nm y ug Nm ug Nm 241 4 25 2011 28 9 29 1 31 9 34 0 Cologne 242 4 26 2011 32 7 33 3 35 0 41 6 Winter 243 4 27 2011 45 9 47 1 48 1 50 5 No ref measurement PM2 5 244 4 28 2011 29 4 29 7 33 0 34 5 245 4 29 2011 27 6 29 3 32 5 32 1 246 4 30 2011 22 4 23 6 24 2 25 7 247 5 1 2011 13 7 13 7 15 1 16 6 248 5 2 2011 16 8 15 7 18 0 18 7 249 5 3 2011 16 4 15 8 17 5 18 7 250 5 4 2011 21 0 20 9 22 5 22 5 251 5 5 2011 20 9 20 5 22 5 23 3 PM2 5 Grubbs outlier 252 5 6 2011 32 5 33 2 31 0 31 8 253 5 7 2011 49 3 51 3 45 8 48 1 254 5 8 2011 25 0 24 8 23 6 24 6 255 7 25 2011 19 0 19 2 21 7 20 3 Bornheim 256 7 26 2011 20 8 20 4 21 5 24 1 Summer 257 7 27 2011 22 8 22 4 24 0 25 2 258 7 28 2011 28 0 26 9 31 1 28 4 259 7 29 2011 17 7 17 7 21 2 19 9 260 7 30 2011 11 8 12 0 261 7 31 2011 13 9 15 0 14 8 15 4 262 8 1 2011 19 2 20 8 20 8 22 9 263 8 2 2011 20 6 22 0 20 6 22 0 264 8 3 2011 26 1 28 2 26 9 28 3 265 8 4 2011 14 9 16 1 18 5 21 7 266 8 5 2011 18 4 19 5 18 2 21 5 267 8 6 2011 12 2 14 7 268 8 7 2011 6 0 6 9 6 0 6 7 269 8 8 2011 8 3 8 0 6 1 8 1 270 8 9 2011 11 2 11 8 Audit flow rate
44. 20107 all test sites 740300_2011_936_21209885B_eng doc a s T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 122 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 1 5 4 3 Reproducibility of the sampling systems The PM sampling systems of two identical systems under test shall be reproducible among themselves according to EN 12341 This shall be demonstrated in the field test 6 2 Equipment Not necessary for this minimum requirement 6 3 Performance of test The test was performed at different test sites during field test In doing so the different sea sons and different levels of PM19 concentrations were taken into account At each test site at least 15 valid data pairs were determined 6 4 Evaluation The two sided confidence interval Clos calculated from the concentration averages measured with the candidates shall not exceed a value of 5 g m for concentration averages of 100 ug m or less and of 0 05 for concentration averages of more than 100 ug m The demonstration of comparability of the candidates is focused on the differences D of the concentration values Y Ideally both candidates are equal and thus sample the same sus pended particulate matter fraction implying D 0 The procedur
45. 28 ug m3 Teddington Summer 0 895 1 112 0 057 0 055 0 883 SN 20006 Dataset Cologne Winter 0 987 0 992 0 013 0 327 0 461 Individual Datasets Bornheim Summer 0 931 1 134 0 041 2 097 0 750 Teddington Winter 0 987 0 959 0 014 1 549 0 337 lt 30 ug m3 186 0 860 1 069 0 029 1 377 0 528 12 26 2 2 Combined Datasets gt 30 ug m3 0 966 0 986 0 026 0 104 1 147 9 36 100 0 All Data 237 0 970 0 994 0 011 0 170 0 294 9 01 23 2 Orthogonal Regression Limit Value of 50 ug m3 eee Slope b up Intercept a ua Wem gt 28 ug m3 Teddington Summer 0 927 1 065 0 039 0 807 0 605 SN 20107 Dataset Cologne Winter 0 978 1 005 0 017 0 710 0 609 Individual Datasets Bornheim Summer 0 906 1 112 0 047 0 860 0 859 Teddington Winter 0 983 0 934 0 019 0 108 0 455 lt 30 ug m3 184 0 886 1 052 0 026 0 062 0 467 13 06 2 2 Combined Datasets gt 30 ug m3 46 0 949 1 010 0 034 0 139 1 526 11 60 100 0 All Data 230 0 970 0 996 0 011 0 795 0 292 9 07 21 7 740300_2011_936_21209885B_eng doc A TUVRheinland Precisely Right Page 154 of 422 PM 1405F FDMS pg m TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fishe
46. 3 Basic OPERATION 3 The Select Data screen will display Figure 3 34 Select the From the beginning button to download all the data on the instrument Select the From last download button to download only the data stored since the last data download Select the OK button Figure 3 34 Select Data screen Select Data Downiads Gan contain al the dala from in hrumment s database or only he dala oolected since the lasi download Download data we A Ew 4 The instrument will display a downloading data message and begin transferring data to the USB drive Note Do not remove the USB drive from the instrument while the data is downloading a 5 When the data download is complete the instrument will display a Download complete message and display the file name as it is stored on the USB flash drive The file name format is the instrument serial number followed by a date time stamp Remove the USB flash drive and select the OK button to continue 3 32 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 3 Basic OPERATION Viewing Data files are downloaded and saved as csv files txt files through USB Downloaded Data at can be opened and viewed with Microsoft Excel The file name format is the instrument serial number followed by a date time stamp The data files will be saved to the folder selected using the Download Setup Wizard Refer to the Setting Up for a Data Download section fo
47. 3 Teddington Winter 05 01 2010 20 1 18 7 Teddington Summer 21 06 2010 14 1 15 7 Teddington Summer 28 06 2010 17 9 19 4 Cologne Winter 04 03 2011 83 3 87 5 70 Not Outlier Outlier Deleted 60 Outlier Not Deleted 1 to 1 Line Z aouaIajay iW 0 10 20 30 40 50 60 70 PM Reference 1 Figure 23 Grubbs test results for the PM reference method Teddington Winter 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B A TUVRheinland Precisely Right Page 57 of 422 70 Not Outlier Outlier Deleted 60 Outlier Not Deleted 1 to 1 Line Z aouaIIjay Wd 0 10 20 30 40 50 PM Reference 1 60 70 Figure 24 Grubbs test results for the PM reference method Teddington Summer 100 Not Outlier 90 Outlier Deleted Outlier Not Deleted 80 1 to 1 Line z aouaIajay Wd 0 10 20 30 40 50 60 70 PM Reference 1 80 90 100 Figure 25 Grubbs test results for the PM reference method Cologne Winter 740300_2011_936_21209885B_eng doc A TUVRheinland Precisely Right Page 58 of 422 TUV Rheinland Energie und Umwelt
48. 3 11 8 18 0 17 6 146 6 25 2010 24 6 25 4 29 0 28 0 147 6 26 2010 31 0 31 2 37 7 37 8 148 6 27 2010 21 4 19 7 149 6 28 2010 23 6 23 0 PM10 Grubbs outlier 150 6 29 2010 9 5 9 7 11 9 11 6 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B TUVRheinland Precisely Right Page 191 of 422 Annex 5 PM10 measured values from field test sites related to standard conditions EN 12431 Page 17 of 22 Manufacturer Thermo Fisher Scientific Suspended particulate matter PM10 Auf enluft Type of instrument TEOM 1405 F Measured values in g m STD Serial No SN 20006 amp SN 20107 No Date Ref 1 Ref 2 Ref 1 Ref 2 Ratio SN 20006 SN 20107 Remark Test site PM2 5 PM2 5 PM10 PM10 PM2 5 PM1q PM10 PM10 ugm pg m ugNm3 yg Nm y ug Nm ug Nm 151 6 30 2010 10 2 10 1 12 9 13 6 Teddington 152 7 1 2010 11 8 12 5 15 3 14 9 Summer 153 1 27 2011 12 7 13 3 Audits Cologne 154 1 28 2011 35 7 36 4 Audits Winter 155 1 29 2011 Zero filter 156 1 30 2011 80 9 82 5 Zero filter 157 1 31 2011 93 1 92 6 Zero filter 158 2
49. 3 14 2 70 4 14 1 14 7 262 8 1 2011 12 7 11 4 18 0 19 2 64 8 19 4 21 4 263 8 2 2011 10 3 10 1 19 0 20 1 52 1 19 0 20 2 264 8 3 2011 17 0 16 6 24 4 26 1 66 5 25 0 26 3 265 8 4 2011 8 7 8 4 13 8 14 7 60 2 17 0 19 9 266 8 5 2011 8 6 10 6 17 1 18 0 54 7 16 8 19 8 267 8 6 2011 11 2 13 5 268 8 7 2011 2 8 3 1 5 6 6 4 49 5 5 6 6 3 269 8 8 2011 2 8 4 0 7 9 7 5 44 1 5 8 7 6 270 8 9 2011 2 7 3 2 10 8 11 2 27 1 Audit flow rate 740300_2011_936_21209885B_eng doc y T V Rheinland Energie und Umwelt GmbH TUV Rheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Page 184 of 422 Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Annex 5 Measured values from field test sites related to actual conditions Page 10 of 22 Manufacturer Thermo Fisher Scientific Suspended particulate matter PM10 Type of instrument TEOM 1405 F Measured values in yg m ACT Serial No SN 20006 amp SN 20107 No Date Ref 1 Ref 2 Ref 1 Ref 2 Ratio SN 20006 SN 20107 Remark Test site PM2 5 PM2 5 PM10 PM10 PM2 5 PM10 PM10 PM10 ug m ug m yg m ug m ug m ug m 271 8 10 2011 5 3 6 4 47 0 14 0 13 4 Bornheim 272 8 11 2011 5 5 5 2 47 3 9 5 11 0 Summer 273 8 12 2011 3 0 3 8 50 2 5 5 8 5 274 8 13 2011 10 2 8 3 275 8 14 2011 26 3 6 4
50. 3 17 Section 3 Basic OPERATION 10 When the installation is complete the Setup Complete screen will display Figure 3 20 Select the Finish button to complete the ePort and Microsoft INET Framework installation Figure 3 20 Microsoft NET Framework Setup Complete screen I Microsoft NET Framework 2 0 Setup Setup Complete Microsoft NET Framework 2 0 has been successfully installed It is highly recommended that you download and install the latest service packs and security updates for this product For more information visit the following Web site 3 18 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 3 Basic OPERATION Connecting to the when the ePort software is installed and the TEOM 1405 unit and the PC Series 1405 F Unit ate connected to the same network the software can connect to the instrument and download data Additional Technical Notes regarding information on connecting to instruments over the network are offered in the library on our website at www thermo com aqi Once you have connected to an instrument or instruments and saved a configuration file select Open Saved Configuration in the ePort Open screen to open that configuration and automatically connect to all the instruments that were saved in that configuration To connect to the instrument 1 Ensure that the PC and the instrument ate connected to the same network using the Ethernet connection on the back of
51. 37 2 36 2 179 2 22 2011 36 5 37 9 43 3 43 8 85 4 45 1 46 2 180 2 23 2011 38 0 37 9 45 7 45 7 83 0 47 1 48 3 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH TUVRheinland 8 Luftreinhaltung z Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 181 0f422 Annex 5 Measured values from field test sites related to actual conditions Page 7 of 22 Manufacturer Thermo Fisher Scientific Suspended particulate matter PM10 Type of instrument TEOM 1405 F Measured values in yg m ACT Serial No SN 20006 amp SN 20107 No Date Ref 1 Ref 2 Ref 1 Ref 2 Ratio SN 20006 SN 20107 Remark Test site PM2 5 PM2 5 PM10 PM10 PM2 5 PM10 PM10 PM10 ug m ug m ug m yg m ug m ug m 181 2 24 2011 30 3 31 4 85 9 37 7 38 9 Cologne 182 2 25 2011 26 4 26 7 88 6 31 2 30 1 Winter 183 2 26 2011 18 9 18 8 184 2 27 2011 13 5 13 3 88 5 15 7 16 0 185 2 28 2011 36 7 36 0 82 3 42 9 43 7 186 3 1 2011 66 6 66 0 88 2 72 6 76 5 187 3 2 2011 49 4 49 7 83 1 59 2 60 9 188 3 3 2011 39 4 37 5 77 1 48 3 49 5 189 3 4 2011 76 3 76 5 PM10 Grubbs outlier Inlet gt Zero filter 190 3 5 2011 Zero filter 191 3 6 2011 8 9 9 2 65 1 Zero filter 192 3 7 2011 8 3 9 0 66 2 Zero f
52. 4 1 4 Set up times and warm up times The set up times and warm up times shall be specified in the instruction manual 6 2 Equipment A clock was required for this test 6 3 Performance of test The AMS were started up according to the description given by the manufacturer Necessary setup and warm up times were recorded separately Necessary constructional works prior to the measurement such as the installation of an inlet through the cabinet roof were not included in this test 6 4 Evaluation The setup time comprises the time needed for all necessary works from system installation to start up The measuring system must be protected from weather inconsistencies e g in an acclimated measuring cabinet Extensive construction work is required in order to lead the sample tube through the roof of a measuring cabinet A non stationary application is therefore only as sumed together with the belonging peripheral devices The following steps are generally necessary for the installation of the measuring device Unpacking and installation of the measuring system in a rack or on a table Connection of the sampling tube flow splitter tripod and PM1o sampling inlet Connection of the pump Mounting of ambient air sensor nearby the sampling inlet Connection of all connecting and control lines Connection of power supply Switch on of the measuring system Performance of the leak test Installation of the TEOM filter as well as the two 47 mm
53. 5 MAINTENANCE AND CALIBRATION PROCEDURES 6 The Disconnect Vacuum Line screen will display Remove the main line from the bottom of the T connection of the dryer vacuum line Figures 5 38 and 5 39 Select the Next gt button Figure 5 38 Main dryer vacuum line T fitting Main dryer vacuum line Figure 5 39 Main dryer vacuum line removed from T fitting 5 30 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 7 The Connect the Vacuum Line screen will display Install the piece of tubing with the orifice fitting provided in the instrument package into the top quick connect fitting of the cooler assembly Figure 5 40 Figure 5 40 Y adapters installed Orifice Adapter for vacuug 8 Install the main dryer vacuum line removed in step 6 into the bottom of the other adapter Figure 5 40 and install the piece of tubing into the bottom quick connect fitting of the cooler assemby Select the Next gt button Note Ensure that you use the adapter with the orifice provided with the unit It restricts the flow through the cooler to the proper rate A THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 31 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 9 The system will automatically begin heating the cooler to 50 C to clean the cooler The wizard will display a timer screen to show how much time is left to complete the cleaning Figure 5 41
54. 62 0 0 4 189 0 0 109 5 19 2010 16 0 23 3 1025 68 8 0 1 235 0 0 110 5 20 2010 18 1 24 4 1026 72 3 0 1 247 0 0 111 5 21 2010 18 9 25 5 1024 62 4 1 2 111 0 0 112 5 22 2010 18 2 24 6 1022 60 0 1 2 131 0 0 113 5 23 2010 21 7 31 1 1014 51 3 0 3 213 0 0 114 5 24 2010 20 5 30 8 1007 54 6 1 4 158 0 0 115 5 25 2010 15 0 20 2 1006 54 5 2 3 91 0 0 116 5 26 2010 13 2 18 2 1005 66 0 1 0 140 1 5 117 5 27 2010 13 3 19 4 1006 58 9 0 4 241 0 3 118 5 28 2010 15 2 21 8 1010 59 6 0 6 209 0 0 119 5 29 2010 14 1 16 7 1003 82 5 1 0 209 1 0 120 5 30 2010 14 6 21 0 1010 52 9 1 6 263 0 0 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Annex 6 Date Test site Amb temperature avg Amb temperature max Amb pressure Rel humidity Wind velocity Wind direction C C hPa m s 7 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 5 31 2010 6 1 2010 6 2 2010 6 3 2010 6 4 2010 6 5 2010 6 6 2010 6 7 2010 6 8 2010 6 9 2010 6 10 2010 6 11 2010 6 12 2010 6 13 2010 6 14 2010 6 15 2010 6 16 2010 6 17 2010 6 18 2010 6 19 2010
55. 740300_2011_936_21209885B_eng doc T V Rheinland Energie und Umwelt GmbH TUV Rheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Page 202 of 422 Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Annex 6 Ambient conditions at the field test sites Page 6 of 11 No Date Test site Amb temperature avg Amb temperature max Amb pressure Rel humidity Wind velocity Wind direction Precipitation C C hPa m s 7 mm 151 6 30 2010 Teddington 7 1 2010 Summer 153 1 27 2011 Cologne 0 2 3 2 1015 72 1 1 6 49 0 0 154 1 28 2011 Winter 1 8 3 4 1015 77 0 1 3 98 0 0 155 1 29 2011 2 1 4 7 1013 77 0 0 9 157 0 0 156 1 30 2011 3 4 1 8 1015 83 9 0 7 168 0 0 157 1 31 2011 3 8 2 2 1020 86 9 1 3 127 0 0 158 2 1 2011 2 3 0 4 1022 88 2 2 1 172 0 0 159 2 2 2011 0 8 2 5 1021 88 6 3 1 144 8 7 160 2 3 2011 4 3 7 6 1018 83 0 2 9 193 0 3 161 2 4 2011 9 9 10 7 1014 72 4 6 9 239 0 3 162 2 5 2011 11 0 12 0 1017 71 2 7 1 241 0 0 163 2 6 2011 8 2 10 6 1018 69 5 3 9 224 0 0 164 2 7 2011 9 8 15 5 1011 60 9 3 6 212 0 6 165 2 8 2011 3 2 10 3 1017 77 0 1 1 166 0 0 166 2 9 2011 6 1 10 9 1014 67 6 3 2 120 0 0 167 2 10 2011 8 7 11 0 1007 84 2 3 2 185 14 0 168 2 11 2011 8 9 11 2 1007 93 5 2 0 193 33 0 169 2 12 2011 6 0 7 8 1007 89 8 2 7 130 3 0 170 2 13 2011 6 3
56. 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Ty Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 37 of422 EEk TEOM 1405 F SCIENTIFIC System Status Operating mode Fully operational RS232 mode AK protocol Vacuum pump pressure 0 28 atm Protection level Unlocked IP address 10 175 240 169 Serial number 1234567890 Instrument firmware version 1 51 E Fy perona omasa a eeen 57 Figure 9 Menu System status here software version 1 51 In the menu System Status status information of the instrument can be looked at At this place also the current software version can be looked at Note The testing was performed with software version 1 51 2009 During the testing the software was constantly developed and optimized up to the version 1 55 During the development problems with the touch screen display were resolved e g there have been problems with the button reboot during a possible system crash No influence on the instrument performance is to be expected due to the realised changes up to the version 1 55 740300_2011_936_21209885B_eng doc ss TUV Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisel
57. 89 4 29 2010 20 2 20 4 22 3 22 0 90 4 30 2010 12 0 12 5 13 0 13 8 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH TUVRheinland 8 Luftreinhaltung z Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 189 of 422 Annex 5 PM10 measured values from field test sites related to standard conditions EN 12431 Page 15 of 22 Manufacturer Thermo Fisher Scientific Suspended particulate matter PM10 Au Benluft Type of instrument TEOM 1405 F Measured values in g m STD Serial No SN 20006 amp SN 20107 No Date Ref 1 Ref 2 Ref 1 Ref 2 Ratio SN 20006 SN 20107 Remark Test site PM2 5 PM2 5 PM10 PM10 PM2 5 PM1q PM10 PM10 yg m g m ug Nm ug Nm yg Nm ug Nm 91 5 1 2010 12 6 12 0 Teddington 92 5 2 2010 8 8 9 0 Summer 93 5 3 2010 13 8 12 9 94 5 4 2010 15 2 15 3 15 2 15 1 95 5 5 2010 19 4 20 5 20 8 20 7 96 5 6 2010 16 8 17 4 17 3 16 9 97 5 7 2010 13 3 13 7 15 0 14 2 98 5 8 2010 9 1 9 3 10 2 10 3 99 5 9 2010 14 5 14 6 15 1 14 3 100 5 10 2010 10 5 10 1 12 2 13 0 101 5 11 2010 10 8 10 0 12 5 12 3 102 5 12 2010 12 5 12 9 13 9 13 2 103 5 13
58. 9 1 1002 81 1 4 2 106 0 0 171 2 14 2011 6 0 8 7 998 87 5 2 5 143 5 1 172 2 15 2011 5 4 8 2 992 86 9 3 5 110 1 8 173 2 16 2011 4 0 9 8 994 86 7 1 4 125 0 0 174 2 17 2011 4 1 10 2 1002 76 8 1 7 124 0 0 175 2 18 2011 2 7 3 6 1009 78 4 1 5 104 0 0 176 2 19 2011 2 7 5 3 1010 73 6 4 5 95 0 0 177 2 20 2011 0 5 2 9 1011 67 1 4 1 77 0 0 178 2 21 2011 2 7 0 9 1011 65 5 3 1 94 0 0 179 2 22 2011 1 6 4 2 1015 56 2 3 0 124 0 0 180 2 23 2011 1 2 3 6 1016 59 6 5 0 132 0 0 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Annex 6 Date Test site Amb temp Cologne Winter 2 24 2011 2 25 2011 2 26 2011 2 27 2011 2 28 2011 3 1 2011 3 2 2011 3 3 2011 3 4 2011 3 5 2011 3 6 2011 3 7 2011 3 8 2011 3 9 2011 3 10 2011 3 11 2011 3 12 2011 3 13 2011 3 14 2011 3 15 2011 3 16 2011 3 17 2011 3 18 2011 3 19 2011 3 20 2011 3 21 2011 3 22 2011 3 23 2011 3 24 2011 3 25 2011 Ambient conditions at the field test sites Amb pressure Rel humidity Wind velocity Wind direction Precipitation hPa m s mm erature avg Amb temperature max C C 2 2 3 8 5 3 6 3 4 2 3 8 5 2 4 8 3 7 3 4 2 7
59. C 20 8 8 20 20 25 25 20 The respective results of the 3 single measurements can be taken from annex 2 and 3 in the appendix 740300_2011_936_21209885B_eng doc aT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 96 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 1 5 3 8 Sensitivity coefficient of the electric voltage The sensitivity coefficient of supply voltage shall not exceed the requirements of Table 2 A value ct at 70 to 80 of the upper limit of the certification range shall be used as refer ence point Note This test point is not evaluable for particulate measuring devices on the basis of the currently valid version of Standard VDI 4202 Part 1 September 2010 and VDI 4203 Part 3 Septem ber 2010 due no non defined minimum requirements According to the decision of the com petent German body see module 5 3 1 reference is made alternatively to following previ ous version of Standard VDI 4202 Part 1 June 2002 The changes of the measured value for the reference value B caused by the voltage chang es typical for an electrical grid within the interval 230 15 20 V shall not exceed Bo 6 2 Equipment Adjustable isolating transformer Ko tes
60. Cologne Bornheim winter summer parking lot motorway parking winter lot summer Time period 12 2009 03 2010 04 2010 07 2010 01 2011 05 2011 07 2011 10 2011 No of paired values Candidates 46 49 88 68 Characteristics Urban background Urban background Urban background Rural structure mo torway Rank of pollution Average Average Average to high Low to average The complete test was performed within the scope of the test program Combined MCERTS and T V PM Equivalence Testing Programme In the context of European harmonization the test program was developed by British and German test institutes Bureau Veritas UK Limited National Physical Laboratory NPL and TUV Rheinland and comprises the testing of the latest series of suspended particle measuring systems by different manufacturers in the laboratory and at field test sites in the UK and in Germany The minimum requirements were fulfilled during suitability testing TUV Rheinland Energie und Umwelt GmbH therefore suggests publication as a suitability tested measuring system for continuous monitoring of suspended particulate matter PM9 in ambient air 740300_2011_936_21209885B_eng doc a s T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separat
61. Combined Datasets gt 30 ug m3 0 966 0 986 0 026 0 499 1 147 10 09 100 0 All Data 237 0 970 0 994 0 011 0 565 0 294 9 55 23 2 Orthogonal Regression Limit Value of 50 ug m3 SN 20107 Dataset Slope b up Intercept a ua Wem gt 28 ug m3 Teddington Summer 57 0 927 1 065 0 039 0 412 0 605 Cologne Winter 74 0 978 1 005 0 017 0 315 0 609 Individual Datasets Bornheim Summer 54 0 906 1 112 0 047 1 255 0 859 Teddington Winter 45 0 983 0 934 0 019 0 287 0 455 lt 30 ug m3 184 0 886 1 052 0 026 0 457 0 467 11 92 2 2 Combined Datasets gt 30 ug m3 46 0 949 1 010 0 034 0 534 1 526 11 58 100 0 All Data 230 0 970 0 996 0 011 0 400 0 292 8 86 21 7 740300_2011_936_21209885B_eng doc aT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 166 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 1 5 5 Requirements on multiple component measuring systems Multiple component measuring systems shall comply with the requirements set for each component also in the case of simultaneous operation of all measuring channels 6 2 Equipment Not applicable 6 3 Performance of test Not applicable 6 4 Evaluation
62. F THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 2 1 Section 2 SETUP AND INSTALLATION Installation Considerations 2 2 Operatine Guine TEOM 1405 F The TEOM 1405 F may be located in any convenient indoor location which is maintained between 8 and 25 C 46 to 77 F The user must run a sampling tube through the roof of the monitoring site refer to the inlet installation instructions later in this section The entrance to the sample inlet must be 1 8 to 2 1 m 70 to 82 inches above the roof based on U S EPA requirements Refer to local regulations for the actual inlet height requirements Although the TEOM monitor is inherently rugged it is a precision instrument The user will obtain the best operating conditions and longest instrument life when the unit is not exposed to extremes of weather Filter exchange in particular may be best accomplished by a technician operating in an indoor environment where there is no possibility of rain or snow contaminating the filter Be sure to install the ambient temperature humidity sensor If you do not install the ambient temperature humidity sensor you must set the instrument to Passive flow control Section 4 or the mass flow controller will attempt to control the sample flow as if the ambient temperature is absolute zero The sample line for the main channel should proceed in a straight vertical line from the PM 10 inlet and to the inlet of the unit To achie
63. Filter screen will display Open the mass transducer and remove the standard TEOM filter from the mass transducer Refer to the section on installing removing TEOM filter for assistance on removing the filter Close the mass transducer without installing another filter Select the Next gt button Note DO NOT use the calibration filter exchange tool for installing or removing ANY filter other than the pre weighed calibration filter a The Stabilizing screen will display Figure 5 82 While the instrument waits to mesaure the frequency of the system with no TEOM filter installed a countdown timer on the screen will show the progress of the stabilization step When the stabilization Complete message displays select the Next gt button Stabilizing Wail for ing inumedt to siabaine THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 9 The Enter Filter Weight screen will display Figure 5 83 Select the Filter Weight button The keypad will display Enter the weight of the pre weighed filter into the system and press the Enter button to save the value and exit the keypad Select the Next gt button Figure 5 83 Enter Filter Weight 4 pre weighed lilier is part of he mass calibration verification Kil Enter Filter Weight screen THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 67 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 10 The Install Calibration Filter screen
64. Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 4 SCREENS AND SETTINGS Whenever a status warning is displayed select the System Status button to display the System Status screen Figure 4 6 The System status screen provides basic operating information and access to the list of the current active status warnings Figure 4 6 System Status screen System Status System Status Operating mode Stabilizing Seo mode Hone Vacuum pump PEST oun im Encho sure te mperatume Ou Inshore Probection level Liniei ed Conditions address 182 188 199 125 Serial number 120587890 fasbrument firterare version DAZ Settings Semice ab Maii Farei me OR 1147 To view the current status warnings select the View Warnings button or touch the warning triangle or the title bar when it is visible in any screen The Warnings screen will display Figure 4 7 Select the lt Previous Warning and Next Warning gt buttons to view the status warnings Figure 4 7 Warnings screen SCIEMTIFIC Syebem Salle 4 arnings Flare warning The clantent Tow diryiabes wara Chars 10 Troa Het H pni x Back a menna wort ah DINERO TEE THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 4 9 Section 4 SCREENS AND SETTINGS Instrument The Instrument Conditions button displays the Instrument Conditions Conditions Screen screen Figure 4 8 and provides access to several temperature and flow settings
65. Hex type in the hexadecimal number then select Dec a To properly use the hexadecimal numbers converted from the decimal data download separate the converted number and the status codes on the table into place holders the one s ten s 100 s 1 000 s 10 000 s and 100 000 s and the 1 000 000 s place Each place in the converted code will have a hexadecimal digit Each hexadecimal digit 0 F in each place will have a unique status code or set of status codes that go with it Ce poc unnar eoio foum arcae C eee ee C CC C CC C CO Cc C CC C CC C CC C CC CC CC eooo po po C CCC C CC Operatine Guine TEOM 1405 F A 3 Appenpix A TROUBLESHOOTING D ecli p h e ring When the unit shows more than one status code it adds the codes together Status C od es and displays them as a decimal sum For example if the unit displays a Memory status code listed as hexadecimal number H 1 on the instrument s specific status code table and a Valve A status code listed as hexadecimal number H 4 on the instrument s specific status code table at the same time the two status codes when downloaded would be displayed as the decimal number 5 The decimal number 5 must then be converted back to hexadecimal in this case also 5 to match the status code table Only two status codes would add up to a value of 5 Table A 2 By looking at instrument s sp
66. January 2010 requires that when operating in networks a candidate method needs to be tested annually at a number of sites corresponding to the highest expanded uncertainty found during equivalence testing These criteria are banded in 5 steps Guide 4 point 9 9 2 table 6 We have to bear in mind that the highest determined expanded uncertainty lays before the correction of the intercept for SN 20107 in Bornheim Summer in the range 20 to 25 and after the correction of the intercept SN 20107 in Bornheim Summer in the range 15 to 20 The application of a correction factor for the TEOM 1405 F Ambient Particulate Monitor for PM therefore slightly improves the expanded measuring uncertainties but does not bring a decisive advantage The demonstration of equivalence of the TEOM 1405 F Ambient Par ticulate Monitor for PM can also be shown without the application of correction factors and terms The respective realization of the above mentioned requirement on ongoing QA QC in net works is the responsibility of the network operator or of the responsible authority of the mem ber state However TUV Rheinland and their UK partners recommend that the expanded uncertainty for the full data set is referred to for this namely 8 4 uncorrected dataset re spectively 8 5 dataset after offset correction which again would require an annual test at two measurement sites 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umw
67. Minimum value Alem value i amem af Operatine Guine TEOM 1405 F 4 27 Section 4 SCREENS AND SETTINGS ContactClosureScreen Select the Contact Closure button to display the Contact Closure screen Figure 4 22 When in the Contact Closure screen use the buttons to select a variable operator and compare value for the desired contact closure channel 1 2 Figure 4 22 Contact Closure screen TEOM 1405 F Setlings gt oulpul gt Contwe Closure inahrument Wariabbe Compare Operator Campane Value af Mnong Heraa siaus ai ERIRE 1E 4 28 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 4 SCREENS AND SETTINGS RS232 Screen Select the RS232 button to display the RS232 screen Figure 4 23 The RS232 screen allows users to set up the serial port for communication with the RP Comm software or AK protocol Figure 4 23 RS232 screen TEOM 71405 F Settings Analog amp Digital Oulputs A3232 OK Cancel af Mdn Heraa siaus we zanr 1257 THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 4 29 Section 4 SCREENS AND SETTINGS Settings Advanced Screen Figure 4 24 Advanced Screen 4 30 Operatine Guine TEOM 1405 F Select the Advanced button to display the Advanced screen Figure 4 24 which allows users to adjust the advanced settings of the unit TEOM 1405 F Selmar draad a Pely operational Hiema sates E OWE2 200F DEIF When in the Advanced screen
68. PM10 Report No 936 21209885 B Page eer aee 6 1 5 3 3 Repeated standard deviation at reference point The repeatability standard deviation at reference point shall not exceed the requirements of Table 2 in the certification range according to Table 1 of Standard VDI 4202 Part 1 Septem ber 2010 The limit value or the alert threshold shall be used as reference point In case of deviating certification ranges the repeatability standard deviation at reference point shall not exceed 2 of the upper limit of this certification range In this case a value ct at 70 to 80 of the upper limit of this certification range shall be used as reference point Note According to the decision of the competent German body see module 5 3 1 this test point is not relevant for particulate measuring devices 6 2 Equipment Not applicable 6 3 Performance of test Not applicable 6 4 Evaluation Not applicable 6 5 Assessment Not applicable Minimum requirement fulfilled 6 6 Detailed representation of the test results Not applicable 740300_2011_936_21209885B_eng doc aT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 90 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 1 5 3 4 Linearity La
69. PROCEDURES 13 When the final verification has been performed the Completing the KO Verification Wizard screen will display The screen will display either a pass Figure 5 86 or a fail Figure 5 87 message for each KO number Select the Finish button Note If one or both of the KO verifications fail repeat the procedure for that KO number If the verification fails again contact Thermo Scientific a Figure 5 86 Completing to KO Verification Wizard screen with a pass message Completing the KO Verification Wizard The KO Veritication Wizard has completed sucessfully The instrument will be put in Run moete when ihis wisard is finished KD 1000 giat Audit K 1000 00 Perceni difference 0 0 Te close this wizard press Finish Figure 5 87 Completing the KO Verification Wizard screen with a fail message Completing the KO Verification Wizard The KO Verification Wizard has completed wunsucesstully The Instuanent wil be put in Fun mode when this wizard is finished KO 1000 0000ta Audit KO 0 0 Percent ditference 100 0 To close this witard press Finish 5 70 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC THERMO FISHER SCIENTIFIC AppendixA Troubleshooting The current status condition is located in the status bar at the bottom of the TEOM Data screen Section 4 and most other instrument screens In data files however status codes are reported as decimal hexadecimal nu
70. Pan aiji c d 1 x f u a aay n 2 with u a uncertainty of the original intercept a the value of which has been used to obtain Yi corr Algorithms for the calculation of intercepts as well as slopes and their variances by orthogo nal regression are described in detail in annex B of 6 RSS is determined analogue to the calculation in module 9 5 2 2 9 5 6 With respect to b The value of the slope b may be used as a factor to correct all input values y according to the following equation Xi Y icom b The resulting values of Yi cor may then be used to calculate the following new terms by linear regression Y i corr C dx and UE Viar O f dF xut 2 ie with u b uncertainty of the original slope b the value of which has been used to obtain Yi corr Algorithms for the calculation of intercepts as well as slopes and their variances by orthogo nal regression are described in detail in annex B of 4 RSS is determined analogue to the calculation in module 9 5 2 2 9 5 6 With respect to c The values of the slope b and of the intercept a may be used as correction terms to correct all input values y according to the following equation y 7a Y izor b 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH F Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Parti
71. Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 99 0f4a2 6 1 5 3 10 Averaging effect For gaseous components the measuring system shall allow the formation of hourly averages The averaging effect shall not exceed the requirements of Table 2 of Standard VDI 4202 Part 1 September 2010 Note This point is not relevant for particulate measurements 6 2 Equipment Not applicable 6 3 Performance of test Not applicable 6 4 Evaluation Not applicable 6 5 Assessment Not applicable Minimum requirement fulfilled 6 6 Detailed representation of the test results Not applicable 740300_2011_936_21209885B_eng doc a s T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 100 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 1 5 3 11 Standard deviation from paired measurements The standard deviation from paired measurements under field conditions shall be determined with two identical measuring systems by paired measuremen
72. SN 20006 amp SN 20107 No Date Ref 1 Ref 2 Ref 1 Ref 2 Ratio SN 20006 SN 20107 Remark Test site PM2 5 PM2 5 PM10 PM10 PM2 5 PM10 PM10 PM10 yg m yg m yg m yg m yg m ug m 1 12 9 2009 11 3 11 6 27 5 27 5 41 6 23 8 Teddington 2 12 10 2009 16 4 16 2 25 4 25 4 64 2 22 2 Winter 3 12 11 2009 11 8 14 7 20 3 20 2 57 9 16 0 4 12 12 2009 6 4 6 5 13 5 13 6 47 6 11 5 5 12 13 2009 8 6 9 1 13 4 13 9 65 1 11 5 6 12 14 2009 27 9 28 3 35 3 35 3 79 6 30 8 7 12 15 2009 39 8 38 8 47 6 47 4 82 8 45 2 8 12 16 2009 24 9 24 5 30 0 30 3 82 0 28 0 9 12 17 2009 5 7 5 6 10 2 10 1 55 7 8 7 10 12 18 2009 11 6 11 9 16 9 17 0 69 3 14 2 11 12 19 2009 10 3 11 0 15 4 14 9 70 4 14 3 12 12 20 2009 6 2 6 4 iti 11 0 56 9 9 3 13 12 21 2009 17 7 17 7 20 2 20 4 87 2 19 0 14 12 22 2009 29 4 28 9 32 9 PM10 Grubbs outlier 15 12 23 2009 17 8 Device not yet in 16 12 24 2009 18 3 operation 17 12 25 2009 12 2 18 12 26 2009 8 0 19 12 27 2009 7 2 20 12 28 2009 23 3 21 12 29 2009 10 8 22 12 30 2009 11 3 23 12 31 2009 6 0 6 5 12 2 24 1 1 2010 16 1 25 1 2 2010 15 0 26 1 3 2010 20 9 27 1 4 2010 Zero filter 28 1 5 2010 15 6 15 5 18 4 PM10 Grubbs outlier 29 1 6 2010 16 9 PM2 5 Grubbs outlier 30 1 7 2010 15 3 15 7 17 4 740300_2011_936_21209885B_eng doc y T V Rheinland Energie und Umwelt GmbH TUV Rheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality mea
73. TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 9 97422 6 1 5 2 6 Switch over Switch over between measurement and functional check and or calibration shall be possible telemetrically by computer control or manual intervention 6 2 Equipment Not required for this minimum requirement 6 3 Performance of test The AMS can be monitored and partly controlled by a user directly at the instrument or via telemetric remote control Some functions as for example the performance of the Ko test can only be done directly at the instrument 6 4 Evaluation All operating procedures that do not require practical work on test site can be monitored by a user directly at the instrument as well as by telemetric remote control 6 5 Assessment Generally all necessary operations for functional check can be monitored directly at the de vice or via telemetric remote control Minimum requirement fulfilled yes 6 6 Detailed representation of the test results Not required for this minimum requirement 740300_2011_936_21209885B_eng doc aT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 80 of 422 company Thermo Fisher Scientific for the comp
74. TEOM 1405 F THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES b To calibrate the bypass flow channel remove the bypass line from the flow splitter and connect the 3 8 inch flow adapter to the green tubing of the bypass line Figure 5 66 Connect the flow meter adapter to the flow audit adapter When the flow audit device is attached to the correct channel select the Next gt button Figure 5 66 Bypass connection Bypass line THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 53 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Figure 5 67 Flow Calibration screen 5 54 Operatine Guine TEOM 1405 F 6 The wizard will display a screen that shows the current low setpoint flow rate as measured by the instrument in the TEOM flow rate button Figure 5 67 Allow the flow to stabilize Select the TEOM flow rate button and enter the current flow rate to two decimal places as measured by the flow meter into the number pad and select the Enter button The newly entered flow rate will display in the TEOM flow rate button Select the Next gt button Flow Calibration Click the bulion to enter ihe flow rate measured by the llow device Main TEOM flow rate 24 lpm x Back Mex gt Cancel 7 The wizard will display a screen that shows the current high setpoint flow rate as measured by the instrument in the TEOM flow rate button Allow the flow to stabilize Select the TEOM
75. TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B PM10 measured values from field test sites related to standard conditions EN 12431 Page 12 of 22 Manufacturer Serial No Thermo Fisher Scientific Type of instrument TEOM 1405 F SN 20006 amp SN 20107 Suspended particulate matter PM10 Auf enluft Measured values in g m STD No ANOOAARWD WNNNNNNNNNNSBBZSBZBBBBABZO COONODANABWNHHRTOOANDAKRWNH O 740300_2011_936_21209885B_eng doc Date 12 10 2009 12 11 2009 12 12 2009 12 13 2009 12 14 2009 12 15 2009 12 16 2009 12 17 2009 12 18 2009 12 19 2009 12 20 2009 12 21 2009 12 22 2009 12 23 2009 12 24 2009 12 25 2009 12 26 2009 12 27 2009 12 28 2009 12 29 2009 12 30 2009 12 31 2009 1 1 2010 1 2 2010 1 3 2010 1 4 2010 1 5 2010 1 6 2010 1 7 2010 12 9 2009 Ref 1 PM10 yg Nm 28 0 25 1 20 2 13 5 13 4 35 2 46 9 30 1 10 2 16 7 15 5 11 2 20 7 15 4 Ref 2 PM10 ug Nm 28 3 25 4 20 3 13 7 14 0 35 6 47 2 30 7 10 3 17 0 15 1 11 2 21 1 14 3 Ratio PM2 5 PM10 SN 20006 PM10 ug Nm 24 5 22 0 16 1 11 6 11 5 30 9 44 9 28 2 8 8 14 2 14 4 9 5 19 7 33 3 18 3 19
76. USER ANALOG OUTPUT GROUND USER ANALOG OUTPUT 3 USER ANALOG OUTPUT GROUND USER ANALOG OUTPUT 4 USER ANALOG OUTPUT 5 USER ANALOG OUTPUT GROUND USER ANALOG OUTPUT 6 USER ANALOG OUTPUT 7 USER ANALOG OUTPUT GROUND USER ANALOG OUTPUT 8 USER ANALOG INPUT 1 USER ANALOG INPUT GROUND USER ANALOG INPUT 2 USER ANALOG INPUT GROUND USER ANALOG INPUT 3 USER ANALOG INPUT GROUND 3 USER ANALOG INPUT 4 USER ANALOG INPUT GROUND Je O O 0 0 Q elelelele ol USER DIGITAL OUTPUT 1 USER DIGITAL OUTPUT 1 USER DIGITAL OUTPUT 2 USER DIGITAL OUTPUT 2 9 90 0 0 90 ie Table 3 1 1405 USER 1 0 pin Channel Pin Channel Pin assignments Analog output 1 1 Analog output 1 ground 14 Analog output 2 2 Analog output 2 ground 15 Analog output 3 Analog output 3 ground 16 gt J w Analog output 4 Analog output 4 ground 16 N Analog output 5 Analog output 5 ground Analog output 6 18 Analog output 6 ground Analog output 7 6 Analog output 7 ground 19 Analog output 8 7 Analog output 8 ground 19 Analog input 1 20 Analog input 1 ground 8 Analog input 2 21 Analog input 2 ground g Analog input 3 22 Analog input 3 ground 10 Analog input 4 23 Analog input 4 ground 11 Digital 1 0 1 24 Digital 1 0 1 12 Digital 1 0 2 25 Digital 1 0 2 13 THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 3 35 Section 3 Basic OPERATI
77. always 2 digits in length RS Para 3 13010 Optional Up to 3 ASCII codes can be added to response from the instrument In this case lt CR gt and lt LF gt ASCII codes 013 and 010 are appended to the response Enter 0 if nothing is to be appended COCO fe veer erm oewmion EECA treme 2 fiasco OE EBES a a Ask Storage command 2 digit Channel Number as defined Number of current status conditions of current status conditions re Fan t paapaa fae au storage This can be smaller than The number of records to be requested number due to end of file downloaded from the instrument s Storage Marker moved to after last storage Downloading begins at the A ee record transmitted Not right filled storage marker which can be set Up to 3 digits appended to the end of the response transmission according to the entry for RS Para 3 The instrument then transmits the number of storage records shown in response bytes10 through 12 above Each record is followed by lt CR gt lt LF gt B 8 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Appennix B SERIAL COMMUNICATION AK Protocol Set Storage Marker Command SSTO COM 2 WAY SETTINGS RS Para 1 ASCII code for the 1 digit Station Number for example 4 052 The Station Number is always 1 digit in length RS Para 2 75048 ASCII code representation of the 2 digit Channel Number for example K0 075 048 The Channel Number is always 2 digits in length
78. and lightly tighten the knob to ensure the flow splitter stays in place Figure 2 10 Figure 2 10 Bottom of the flow splitter 4 Flow splitter Sample tube 2 10 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 2 SETUP AND INSTALLATION 3 Measure and mark a spot in the roof directly above the 1 2 inch sample line on the top of the instrument Note In this example a 4 inch hole was cut in the roof to accommodate a 4 inch PVC pipe and seal The cap of the PVC pipe was then drilled to accommodate the sample line a 4 Drill the hole in the roof for the 1 2 inch sample line and another hole for the 3 8 inch bypass line tubing The bypass tubing may also be run through a window or other opening 5 Set the tripod on the roof above the 1405 unit and adjust the legs so the top of the tripod is above the roof opening Figure 2 11 Installing the sample tubes and bypass line through the roof Flow splitter with bypass Sample tube extensions 1 3 4 inch centers THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 2 11 Section 2 SETUP AND INSTALLATION 6 Install the slow splitter in the tripod and install the inlet assembly on top of the flow splitter Adjust the tripod so the entrance to the sample inlet is 1 8 to 2 1 m 70 to 82 inches above the roof Figure 2 12 Note This measurement may vary based on the inlet height required by the local regulatory agency Verify height requirement pr
79. and the current ambient air conditions for the instrument Figure 4 8 Instrument Conditions screen TEOM 1405 F System Status Instuanent Conditions Settings Service Fs sort Worst sats _ ETO When in the Instrument Conditions screen select the Ambient Conditions Instrument Temperatures Flows FDMS Module or Analog Inputs buttons to reach the desired screens Figure 4 9 4 10 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 4 SCREENS AND SETTINGS julod jas julod jas ainssalg Bay upg aINSsald PIS HPA 19S dwe pls pa julod t SUOIIPUOD p4epues 10 jen oy 0 yod y N Y 10 BAISSEd 101 Uu09 MO 4 julod S MOJ UIEN HPF A julod jas ssed q ypa A molj aye1 MmOl ssedig ayes MOJ s ey MOl4 elol ule zx julod jas dw 191009 p3 sBunjes jauueyo ndu Bojeue ypa uoisod anen Juan dw 4 19 009 julod map 198A1q dwa 1afq p jauueYo ndui Hojeuy OW eseg ulw o g g JauueYd ndu Hojyeuy OW 40H z euueyo ndu Bojeuy JauueYyo ndu Bojyeuy jndu Bojeuy 4 julod jas julod julod jas dwa eqn se ypa yes dwa deo ypa dwa eseo ypa n e1 d w eqn uy ainjesodwoa deg nyes dw j aseg sainjesoadway uawni su
80. business and that you require it to deliver timely and reliable data We are dedicated to helping you realize a maximum value in your technology investment by providing a high level of personal attention premium technical assistance and fast reliable response Thermo Scientific offers a full suite of warranty and service contract programs designed to meet your specific support needs and keep your instrumentation operating at peak performance As Thermo Fisher Scientific s instrumentation changes so do our operating manuals However these changes may affect only one aspect of an instrument while leaving the instrument as a whole unchanged To explain these individual changes to our customers Thermo Fisher Scientific will update only those sections of its operating manuals that are affected by the instrument updates or improvements To help our customers keep track of the changes to the TEOM 1405 sampler and its operating guide following is a list of the sections with their respective revision numbers Section Number and Description Revision Number Section 1 Introduction A 000 Section 2 Setup and Installation A 000 Section 3 Basic Operation A 000 Section 4 Screens and Settings A 000 Section 5 Maintenance and Calibration Procedures A 000 Appendix A Troubleshooting A 000 Appendix B Serial Communication A 000 THERMO FISHER SCIENTIFIC Preface Table of Contents Section1 Section 1 Introduction i sdisiciascuvcvsiciadsvattvsver
81. dryers to remove moisture from the sample gases is insufficient resulting is a high sample dewpoint High ambient temperature humidity or both may cause this condition to occur If the high ambient temperature or humidity exists such that the dewpoint of the sample gases may exceed 0 C Thermo Fisher Scientific recommends the cooler temperatures be adjusted to a 10 C set point for the operating period where the high ambient temperature or humidity exists This is accomplished by setting the cooler temperature to 10 C at the beginning of the typical calendar period when these conditions exist and resetting the cooler temperature to 4 C at the end of the calendar period When changing the cooler temperature from 4 C to 10 C follow these steps 1 Remove the TEOM sample filters 2 Perform the Cooler Cleaning as instructed in Secion 5 3 Change the Cooler temperature from 4 C to 10 C 4 Install new TEOM Sample filters The instrument is now ready to sample at the new FDMS cooler temperature When changing the cooler temperature setting from 10 C to 4 C these steps are not necessary Operatine Guine TEOM 1405 F 4 21 Section 4 SCREENS AND SETTINGS Settings Screen Figure 4 17 Settings screen 4 22 Operatine Guine TEOM 1405 F The Settings button displays the Settings screen Figure 4 17 and provides access to system data and advanced settings for the instrument TEOM 1405 F System Sia
82. filter Check of the instrument setting regarding die regulation of the flow rate here Ac tive Actual date and time and the parameterization of the proper calibration constant Ko e Check of the sensors for ambient temperature and pressure and the flow rate e Optional connection of peripheral recording and control systems data logger PC with ePort RPComm and HyperTerminal to the respective interfaces 740300_2011_936_21209885B_eng doc a s T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 68 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B The performance of these actions and therewith the set up time takes approx 2 hours The warm up time contains the time need between the start of operation of the measuring system and the readiness for measurement After switching on the system the system is in the stabilizing phase stabilizing until reach ing the stabilized condition regarding the instrument temperature The duration of the stabiliz ing phase is dependent of the ambient temperature at the installation place and of the ther mic instrument condition when switched on In the scope of the suitability test the stabilizing times where between 30 min and 90 min After reaching a stabilized cond
83. four sampling test sites representative of the future application The maximum expanded un certainty of the systems under test shall be compared with data quality objectives according to Annex A of Standard VDI 4202 Part 1 September 2010 The tests are performed as well for the components PM 6 2 Equipment For this test point additionally the devices according to chapter 5 of this report were used 6 3 Performance of test The test was carried out at four different sites during field test Different seasons and varying concentrations for PM19 were taken into consideration Of the complete data set at least 20 of the concentration values determined with the ref erence method shall be greater than the upper assessment threshold according to 2008 50 EC 7 For PM the upper assessment threshold is at 28 pg m At each test site at least 40 valid data pairs were determined Of the complete data set 4 test sites 237 valid data pairs for SN 20006 230 valid data pairs for SN 20107 in total 23 3 of the measured values are above the upper assessment threshold of 28 yg m for PM o The measured concentrations were referred to ambient conditions 6 4 Evaluation Point 9 5 2 2 The calculation of the in between instrument uncertainty Uert of the reference devices is carried out prior to the calculation of the expanded uncertainty of the candidates The in between instrument uncertainty Uret of the reference devices shall be lt 2 ug m
84. in order to minimize relative mass changes caused by the weighing room conditions Equation Dust MF post Mrara X MKonpost MKONpre F1 MKoOnpre average mass of the 3 control filters after 48 h and 72 h pre weighing MKonpost average mass of the 3 control filters after 48 h and 72 h post weighing Mrara average mass of the filter after 48 h and 72 h pre weighing MF post average mass of the loaded filter after 48 h and 72 h post weighing Dust corrected dust mass of the filter This shows that the method becomes independent from weighing room conditions due to the corrective calculation Influence due to the water content of the filter mass between virgin and loaded filter can be controlled and do not change the dust content of sampled filters Hence Point EN 14907 9 3 2 5 is fulfilled The below example of the standard weight between November 2008 and February 2009 shows that the allowed deviation of not more than 20 ug on the previous measurement is not exceeded Stability of standard weight between Nov 08 and Feb 09 0 20010 0 20005 2 oo of i 0 0 0000 0 0 Standard weight lt 0 20000 D e Mean standard weight 0 19995 0 19990 0 5 10 15 20 25 No of weighing Figure 75 Stability of standard weight 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH W Luftreinhaltung A TUVRheinland Genau Richt
85. is related to a defined and actively regulated sampling volume and thereby the particulate concentration is determined 6 5 Assessment The test took place according to the minimum requirement stated in Table 5 of Standard VDI 4202 Part 1 September 2010 The measuring unit TEOM 1405 F Ambient Particle Monitor is a gravimetric measuring de vice which determines the mass depotest sited on a filter via oscillating micro weighing The determined mass is related to a defined and actively regulated sampling volume and thereby the particulate concentration is determined Minimum requirement fulfilled yes 6 6 Detailed representation of the test results Not necessary for this minimum requirement 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH F Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 11501422 6 1 5 4 2 Equivalency of the sampling system The equivalency between the PM sampling system and the reference method according to EN 12341 T5 shall be demonstrated 6 2 Equipment For this test point additional equipment was used according to point 5 of this report 6 3 Performance of test The test was performed at different test sites during field test according t
86. it is secure and free from blockages Figure 5 27 Figure 5 27 Rain jar cover 5 20 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC THERMO FISHER SCIENTIFIC 12 13 14 15 16 17 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Apply a light coating of silicone grease to the O rings Figure 5 26 to ensure that a seal is made when they are reinstalled on the flow splitter Clean the lower collector assembly s threads to ensure a tight seal when the two halves are reassembled Reassemble the top and bottom inlet assemblies until the threads tighten Hand tighten only Reinstall the insect screen and align the top plate markings with the lower plate markings Install the top plate onto the lower plate and tighten the four pan head screws Place a light coating of silicone grease on the gasket inside the cap of the rain jar This will ensure a leak free fit Reinstall the rain jar Place the inlet on the flow splitter Take care not to damage the internal O rings For information on cleaning the cyclone refer to the supplemental cyclone operating manual Operatine Guine TEOM 1405 F 5 21 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Exchanging In Line Filters Figure 5 28 Back of 1405 unit 5 22 Operatine Guine TEOM 1405 F The main flow in line filter 57 010745 and the large bypass flow filter 57 010755 should be changed every 6 months or as necessary They are locat
87. measuring device and approximately 550 600 W for the pump During a 24 h test these specifications were checked At no time the mentioned value was exceeded during these investigations 6 5 Assessment The instrument design specifications listed in the operating manual are complete and correct Minimum requirement fulfilled yes 6 6 Detailed representation of the test results Not required for this minimum requirement 740300_2011_936_21209885B_eng doc a s T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 70 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 1 4 1 6 Unintended adjustment It shall be possible to secure the adjustment of the measuring system against illicit or unin tended adjustment during operation 6 2 Equipment No additional equipment required 6 3 Performance of test The operation of the measuring device is carried out via a touch screen display at the front panel or via the RS232 or Ethernet interfaces from an external computer A change of the parameters or the adjustment of sensors is only possible via several key se quences The measuring device has the following level of password protection Low Lock Mode In this mode the user can see all instrument views and can
88. of 422 Report No 936 21209885 B filled 5 3 4 Linearity Lack of fit 5 3 5 Sensitivity coeffi cient of the sam ple gas pressure Sensitivity coeffi cient of the sam ple gas tempera ture Sensitivity coeffi cient of the sur rounding tem perature 5 3 8 Sensitivity coeffi cient of the elec tric voltage The analytical function describ ing the relationship between the output signal and the value of the air quality characteristic shall be linear The Sensitivity coefficient of the sample gas pressure at reference point shall not ex ceed the specifications of Ta ble 2 of Standard VDI 4202 Part 1 September 2010 The Sensitivity coefficient of the sample gas temperature at reference point shall not ex ceed the specifications of Ta ble 2 of Standard VDI 4202 Part 1 September 2010 The sensitivity coefficient of the surrounding temperature at ze ro and reference point shall not exceed the specifications of Table 2 of Standard VDI 4202 Part 1 September 2010 For PM Zero point value for ATu of 15 K between 5 C and 20 C or 20 K between 20 C and 40 C shall not exceed Bo The measurement value in the range of B shall not exceed 5 for ATu of 15 K between 5 C and 20 C or for 20 K between 20 C and 40 C The sensitivity coefficient of the electric voltage at reference point shall not exceed the specifications made in Table 2 of Standard VDI 4202 Part 1 Septe
89. of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 69 0f422 6 1 4 1 5 Instrument design The instruction manual shall include specifications of the manufacturer regarding the design of the measuring system The main elements are e Instrument shape e g bench mounting rack mounting free mounting Mounting position e g horizontal or vertical mounting Safety requirements Dimensions Weight Power consumption 6 2 Equipment A measuring device for power consumption measurement and a scale were used for this test 6 3 Performance of test The installation of the delivered instruments was compared with the description given in the manuals The specified power consumption was continuously tested for 24 h under standard operation conditions during field test 6 4 Evaluation The measuring system has to be installed in horizontal mounting position e g on a table or a rack independent from atmospheric conditions The temperature at the installation test site shall be within the range of 8 C to 25 C with a relatively low amount of temperature fluctua tion maximum 2 C per hour no direct sun no direct exposure to heater or air conditioner The dimensions and the weights of the measuring system are in compliance with the specifi cations in the manual The power consumption of the measuring system with the used pump is specified by the manufacturer with at maximum 100 130 W for the
90. recommends the following regular maintenance Maintenance procedures for the TEOM 1405 F Replace Refurbish the dryer Replace Refurbish the FDMS dryer once Replace the TEOM filter Replace the 47 mm filter Clean the sample inlet Replace the in line filters Clean the cooler Clean the switching valve Clean the air inlet system Rebuild the sample pump a year or as necessary See page 5 3 Replace the TEOM filter when the filter loading percentage displayed in the Main screen nears 100 or every 30 days Replace the 47 mm filter every time you replace the TEOM filter every 30 days Clean the sample inlet that is mounted on the tripod each time that you replace a TEOM filter every 30 days Replace the main flow in line filter and the bypass in line filter every 6 months or as necessary Clean the cooler once a year or as necessary Clean the switching valve once a year or as necessary Clean the air inlet system inside the mass transducer once a year or as necessary Rebuild the sample pump once every 18 months or as necessary The pump rebuild kit 59 008630 contains instructions for rebuilding the pump These maintenance intervals are guidelines Requirements for routine maintenance are site specific and may vary from one location to another THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 1 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Maintenance Wizards he T
91. selected contains the average pressure atm setting for passive flow control The default setting is 1 atm To adjust the setpoint select the button to display the keypad Figure 4 3 The instrument is delivered with the following temperature and pressure settings Standard temperature 25 C Standard pressure 1 atmosphere atm Average temperature 25 C Average pressute 1 atmosphere atm The user must choose how they want the monitor to control the volumetric flow actively or passively e Active Flow Control uses actual ambient pressure and ambient temperature from instrument sensors to set the flow rates e Passive Flow Control uses operator input ambient temperature and ambient pressure to control flow At their discretion operators can input seasonal average temperature and pressure To select active flow control select the Active flow control button Figure 4 13 To use the actual temperature and pressure to control the volumetric flow you must install the ambient temperature humidity sensor The instrument s mass flow controllers measure flow on a mass basis All of the size selective inlets including the PM 10 inlet operate on a constant volumetric flow basis If the user chooses to use passive flow control they must select the Passive flow control button Figure 4 13 The average temperature and average pressure used by the instrument may vary with season and altitude If the user wants the unit to use the averag
92. separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Standards Dev yg m Dev ug m Page 1 of 1 ZP Measured value with zero filter Measured value ug m TUV Rheinland Energie und Umwelt GmbH A TUVRheinland 8 Luftreinhaltung z Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 173 of 422 Annex 3 Dependence of measured value on ambient temperature Page 1 of 1 Manufacturer Thermo Fisher Scientific Standards RP Ko Test Type 1405F Serial No SN 20006 SN 20107 Cycle 1 Temperature Measured value Ko Dev Cycle 2 Measured value Ko Cycle 3 Dev Measured value Ko SN 20006 Dev 15066 2 15068 0 15057 7 15058 9 15062 0 15088 2 15088 8 15106 4 15102 6 15086 2 SN 20107 aac Measured value Ko Measured value Ko Dev Measured value Ko x cl a 6 17345 5 17417 1 17363 4 17409 0 17352 6 17421 3 17388 7 i 17436 6 17397 2 17442 3 740300_2011_936_21209885B_eng doc TUVRheinland Precisely Right Page 174 of 422 Annex 4 Manufacturer Thermo Fisher Scientific Type 1405F Serial No SN 20006 SN 20107 Cycle 1 Dependence of measured value on main
93. system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Schematic set up of the MASS transducer cccccceceaeeeeseeeeeeeeecaeseeseeeeeesaees 29 Overview of complete system TEOM 1405 F Ambient Particulate Monitor 32 American PM sampling inlet Original style p n 57 000596 0001 for TEOM 1405 F Ambient Particulate Monitor 0 eeeeeeeeeeeeeeeeeeeeees 33 FIOW SDPIIMEST see ieniet dette tou estes ahs ii E E ie eA 33 Measuring device TEOM 1405 F Ambient Particulate Monitor 265 34 Measuring device TEOM 1405 F Ambient Particulate Monitor 2 system from left in measuring Station ccccccccesccessseseeseeceseceseseeeeeeeeeeees 34 Vacuum pump p n 10 011413 00 eeeesseeeseeeceeeeeeeaeeeaeeeaaeaeeeaaeaeaeeeaaaeaaeeaaaeaes 35 Main window of the user display cce ccccecectenee ee eeeeeeeeeeeeeeeeeeeeeseeeeneeeeeeeneee 36 Menu System status here software version 1 51 cccecceecceeeeeeeeeeeeeeeeeeeeees 37 Warning messages display triangular warning symbol button View WamningS cuxsasscsconieretediareetacniccarcetanadm E an a anaE Na AAA AAAA EEEa 38 Menu Instrument conditions cece cece eee cece eect eect eee e cece eeeeeeeeeeeeeteeeteeeeeeeeeees 39 Men TNC oi ceca nied Sameera ace etbaht dade dit aaia 40 Men SEVICE niiss iinet la eed a
94. systems under test uss The graphical representation is done in Figure 55 to Figure 61 Table 30 Uncertainty between systems under test Ups for the candidates SN 20006 and SN 20107 measured component PM19 Candidate Test site No of Uncertainty ups values 20006 20107 All test sites 251 Single test sites 20006 20107 Teddington Winter 1 10 20006 20107 Teddington Summer 0 78 20006 20107 Cologne Winter 1 15 20006 20107 Bornheim Summer 1 20 Classification via reference value 20006 20107 Values gt 30ygim 46 1 35 20006 20107 Values lt 30 g m 1 03 1405 F SN20006 SN20107 All Test Sites Raw data Measured values Regression line PN y x Candidate 2 ug m 0 10 20 30 40 50 60 70 80 90 100 110 120 130 Candidate 1 ug m Figure 55 Results of the parallel measurements with the candidates SN 20006 SN 20107 measured component PM39 all test sites 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH F Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 14501482 1405 F SN20006 SN20107 Teddington Winter Raw
95. the candidates SN 20006 SN 20107 measured component PM o all test sites values 2 30 g m 147 Figure 61 Results of the parallel measurements with the candidates SN 20006 SN 20107 measured component PM o all test sites values lt 30 pg m 147 Figure 62 Reference vs candidate SN 20006 amp SN 20107 measured component PM o all test sites 5 Aten ek ect oeiete sohbet bbs oe heehee decent ANENA AENEAN NANAK NAANA ENAN 154 Figure 63 Reference vs candidate SN 20006 measured component PM All test SIGS vaviissuccovec caseevacecdaavecvaexeveduveanvecsavesvansy ean ea EESE TOE EEEa E tt 154 Figure 64 Reference vs candidate SN 20107 measured component PM AI TEST SITS S EEES TE S S ET T E ETTE 155 Figure 65 Reference vs candidate SN 20006 measured component PM Teddington WINterjnenoinrurni t oaia EE aN ESE 155 Figure 66 Reference vs candidate SN 20107 measured component PM Teddington WIMEN ica secedsaiaconiccatercannnmintenatabeens wasnueounbindeaecntee vantcceouecianantanicaeds 156 Figure 67 Reference vs candidate SN 20006 measured component PM Teddington SUNIMET i cicealidhncunctcentiiansiiccdudinialdusasectoamibcbs Mearahassl giwebinekedapidnent 156 740300_2011_936_21209885B_eng doc aT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Page 12 of 422 Figure 68 Figure 69 Figure 70 Figure 71 Figure 72 Figure 73 Figure 74 Figur
96. the component PM10 Report No 936 21209885 B Page 11301422 6 1 5 3 18 Overall uncertainty The expanded uncertainty of the measuring system shall be determined The value deter mined shall not exceed the corresponding data quality objectives in the applicable EU Direc tives on air quality listed in Annex A Table A1 of Standard VDI 4202 Part 1 September 2010 Note According to the decision of the competent German body see module 5 3 1 this test point is not relevant for particulate measuring devices Reference is made to module 5 4 10 6 2 Equipment According to the decision of the competent German body see module 5 3 1 this test point is not relevant for particulate measuring devices Reference is made to module 5 4 10 6 3 Performance of test According to the decision of the competent German body see module 5 3 1 this test point is not relevant for particulate measuring devices Reference is made to module 5 4 10 6 4 Evaluation According to the decision of the competent German body see module 5 3 1 this test point is not relevant for particulate measuring devices Reference is made to module 5 4 10 Assessment According to the decision of the competent German body see module 5 3 1 this test point is not relevant for particulate measuring devices Reference is made to module 5 4 10 Minimum requirement fulfilled 6 6 Detailed representation of the test results According to the decision of the competent Germ
97. tion of thermal mance due to in tube and valve fitting stress in the creased operating fitting material reliability The change was made after the performance of the two field test sites in England In the fol lowing lab test and the two field test campaigns in Germany no negative influence on the in strument performance could be observed 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH F Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 4501422 Table 3 contains a list of the most important device related characteristics of the particulate ambient air measuring device TEOM 1405 F Ambient Particulate Monitor Table 3 Device related characteristics TEOM 1405 F Ambient Particulate Monitor manufactur er information Dimensions Weight TEOM 1405 F Ambient Particulate Moni tor Measuring device 432 x 483 x 1400 mm 33 kg without pump Sampling tube approx 0 3 m between Inlet and Flow Splitter 1m between Flow Splitter and inlet of central unit Sampling inlet US Original Style Energy supply 100 115 230 V 50 60 Hz Power input Approx 100 130 W normal operation central unit Approx 550 600 W normal operation pump
98. to EN 12341 2 50 y x 40 S 30 2 r 20 10 0 10 20 30 40 50 60 70 80 90 100 Reference yg m Figure 41 Reference equivalence function SN 20107 test site Bornheim Summer 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH F Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 121 01484 Reference vs SN 20006 All test sites 100 Measured values 90 80 Regression line 7 Bose a ee oe al Pes eeee Acceptance range gt according to EN 12341 g 50 y x 40 S 30 j Co 20 10 0 10 20 30 40 50 60 70 80 90 100 Reference yg m Figure 42 Reference equivalence function SN 20006 all test sites Reference vs SN 20107 All test sites 100 Measured values 90 80 Regression line 70 so h p g Z J wee Acceptance range gt according to EN 12341 g 50 y x 40 S 30 ae el 20 10 0 10 20 30 40 50 60 70 80 90 100 Reference yg m Figure 43 Reference equivalence function SN
99. two sided 95 confidence interval of the Student t distribution with f lt n lt 2 degrees of free dom is used The two sided confidence interval Clos for the average concentration values gt 100 ug m is then calculated as follows Clos S gt te 0 975 During the field tests no concentration values gt 100 ug m were measured A statistical eval uation of these concentration ranges is for this reason not possible Therefore the assess ment according to b is not applicable 6 5 Assessment The two sided confidence interval Clos is with a maximum of 2 57 g m beneath the de manded value of 5 ug m for all test sites Minimum requirement fulfilled yes 6 6 Detailed representation of the test results Table 21 shows the calculated values for the standard deviation Sa and the two sided confi dence interval Clos The graphical representation follows in Figure 44 to Figure 48 The dia grams contain besides the regression line of both candidates determined via linear regres sion analysis the curve y x which is seen as the ideal case and the two sided acceptance range All single values for the candidate can be looked up in annex 5 740300_2011_936_21209885B_eng doc WT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Pag
100. volatile PM components The TEOM 1405 F Monitor is composed of two major components Figure 1 1 the sample inlet assembly and the TEOM 1405 F unit with FDMS system The user enters the system parameters into the TEOM 1405 F unit using a color touch screen that is located on the front of the unit The instrument s internal storage buffer can store a large amount of data for later viewing or downloading over a network connection A USB connection allows easy downloads to a portable USB flash drive Additionally the system is furnished with software for personal computers to allow the user to download data and update instrument firmware The instrument does not require a dedicated computer to function in the field Analog outputs are available to transmit the measurements to a user s data acquisition system Ethernet and RS232 ports allow for communication over a network or serial communications THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 1 1 Figure 1 1 Schematic of typical installation Inlet Flow splitter Tripod TEOM 1405 F THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 1 2 THERMO FISHER SCIENTIFIC Section 1 INTRODUCTION The sensor unit contains a mass measurement hardware system that monitors particles that continuously accumulate on the system s exchangeable TEOM filters By maintaining a flow rate of 3 1 min through the sample channel and measuring the total mass accumul
101. when shutting off the measuring device These works come up every 6 or 12 months In the remaining time maintenance works are limited to the check of contaminations plausibility checks and eventual status error messages Minimum requirement fulfilled yes 6 6 Detailed representation of the test results The maintenance works were carried out during the test in accordance with the instructions given in the manual No problems were noticed while following the described procedures All maintenance works could be done with customary tools without taking much time and effort 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH F Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page ea odes 6 1 4 1 3 Functional test If the operation or the functional check of the measuring system requires particular instru ments they shall be considered as part of the measuring system and be applied in the corre sponding sub tests and included in the assessment Test gas units included in the measuring system shall indicate their operational readiness to the measuring system by a status signal and shall provide direct as well as remote control via the measuring system 6 2 Equipment Manual zero
102. while picking it up with the filter exchange tool a 10 Hold the filter exchange tool in line with the tapered element Figures 5 8 and 5 9 and lightly place the hub of the filter onto the tip of the tapered element Select the Next gt button Figure 5 8 Placing the filter on the tapered element 5 8 OperaTING Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 11 The Seat Filter screen will display Gently press down on the TEOM filter to ensure that it is seated properly Figure 5 9 12 Remove the filter exchange tool by slowly retracting it until it clears the filter Figure 5 9 Do not disturb the filter 13 Place the bottom of the filter exchange tool on top of the TEOM filter Figures 5 9 and apply downward pressure approximately 0 5 kg or 1 Ib to seat the filter firmly in place Figure 5 9 Placing the filter on the tapered element 14 The Precondition Filter screen will display Place a new TEOM filter on the empty conditioning post on the mass transducer Refer to the next section for more information on conditioning filters Select the Next gt button 15 The Close Instrument screen will display Raise the mass transducer to the closed position and fasten the holding rod onto the latch plate 16 Close and latch the door to the sensor unit Keep the door open for as short a time as possible to minimize the temperature change in the system Select th
103. with PM10 pre separator of the Page 72 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 6 Detailed representation of the test results Figure 28 shows a view of the rear side of the instrument with the respective measured value outputs Figure 28 View on rear of the device TEOM 1405 F Ambient Particulate Monitor 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 13 onde 6 1 5 1 General The manufacturer s specifications in the instruction manual shall be by no means better than the results of the performance test Deviating specifications shall be corrected in the instruc tion manual by the manufacturer before declaration of suitability 6 2 Equipment Not necessary for this minimum requirement 6 3 Performance of test The test results are compared with the specifications given in the manual 6 4 Evaluation Found deviations between the first draft of the manual and the actual design were resolved 6 5 Assessment Differences between the instrument design and the descriptions given in the manual could not be detected Minimum requirement fulfilled yes 6 6 Detailed rep
104. 0 2 5 4 30 2010 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Page 200 of 422 Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Annex 6 Ambient conditions at the field test sites Page 4 of 11 No Date Test site Amb temperature avg Amb temperature max Amb pressure Rel humidity Wind velocity Wind direction Precipitation C C hPa m s CI mm 91 5 1 2010 Teddington 12 4 18 2 1004 75 3 0 5 184 9 4 92 5 2 2010 Summer 7 4 9 5 1012 76 5 1 8 233 4 8 93 5 3 2010 7 7 12 2 1021 60 1 1 7 240 0 5 94 5 4 2010 7 9 13 4 1021 66 2 0 8 226 0 0 95 5 5 2010 12 1 16 7 1012 64 2 0 8 209 0 0 96 5 6 2010 10 9 17 3 1007 59 1 1 2 175 0 0 97 5 7 2010 9 9 14 2 1007 64 5 1 4 181 0 8 98 5 8 2010 8 6 10 5 1009 78 3 1 1 213 0 0 99 5 9 2010 9 2 12 2 1008 69 6 1 0 153 0 0 100 5 10 2010 9 5 14 3 1008 56 5 1 4 173 0 0 101 5 11 2010 6 7 11 1 1009 66 1 0 6 196 0 0 102 5 12 2010 8 1 13 4 1011 61 1 0 6 220 0 0 103 5 13 2010 9 7 15 0 1009 59 8 0 3 212 0 0 104 5 14 2010 12 0 16 3 1008 58 0 0 4 213 0 0 105 5 15 2010 12 5 19 2 1011 60 3 0 4 260 0 0 106 5 16 2010 11 3 17 2 1014 82 3 0 2 219 4 8 107 5 17 2010 12 8 19 8 1021 63 0 0 4 266 0 0 108 5 18 2010 14 1 20 5 1024
105. 0 3 39 1 16 2010 13 8 14 0 11 0 11 8 40 1 17 2010 20 6 20 8 17 5 18 1 41 1 18 2010 27 1 27 3 25 2 25 9 42 1 19 2010 26 9 27 2 Power supply interrupted 43 1 20 2010 32 1 32 4 28 6 29 8 44 1 21 2010 27 7 28 4 24 2 24 1 45 1 22 2010 9 9 10 1 9 4 10 3 46 1 23 2010 25 8 25 3 23 2 23 6 47 1 24 2010 20 6 20 4 18 6 18 5 48 1 25 2010 41 3 42 1 39 3 49 1 26 2010 58 5 59 1 54 4 55 4 50 1 27 2010 39 0 39 6 34 1 33 4 51 1 28 2010 14 2 14 6 13 0 14 1 52 1 29 2010 9 6 9 8 9 4 9 6 53 1 30 2010 17 6 17 8 15 7 16 3 54 1 31 2010 17 3 17 0 15 2 16 0 55 2 1 2010 14 7 14 6 14 2 14 3 56 2 2 2010 12 3 12 1 11 9 11 6 57 2 3 2010 19 6 19 8 16 4 16 6 58 2 4 2010 20 3 20 6 18 7 19 3 59 2 5 2010 Inlet gt Zero filter 60 2 6 2010 Zero filter 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Page 188 of 422 Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Annex 5 PM10 measured values from field test sites related to standard conditions EN 12431 Page 14 of 22 Manufact
106. 0_2011_936_21209885B_eng doc TUVR h T V Rheinland Energie und Umwelt GmbH ein and Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 78 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 1 5 2 5 Operating states The measuring system shall allow the control of important operating states by telemetrically transmitted status signals 6 2 Equipment PC for data acquisition 6 3 Performance of test A PC was connected locally via Ethernet to the AMS and data transfer incl instrument status tested Furthermore it is possible to control the instrument via serial interface AK Protocol With a respective router or modem the remote control is possible 6 4 Evaluation The measuring device enables a complete telemetric control of the AMS through a choice of different possibilities Ethernet RS232 6 5 Assessment The measuring devices can be extensively monitored and controlled by an external PC via modem or router Minimum requirement fulfilled yes 6 6 Detailed representation of the test results Not necessary for this minimum requirement 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system
107. 1 33 6 32 4 32 4 29 9 209 3 24 2011 34 1 33 8 34 8 33 9 210 3 25 2011 38 5 39 1 39 3 40 8 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B TUVRheinland Precisely Right Page 193 of 422 Annex 5 PM10 measured values from field test sites related to standard conditions EN 12431 Page 19 of 22 Manufacturer Thermo Fisher Scientific Suspended particulate matter PM10 Type of instrument TEOM 1405 F Measured values in g m STD Serial No SN 20006 amp SN 20107 No Date Ref 1 Ref 2 Ref 1 Ref 2 Ratio SN 20006 SN 20107 Remark Test site PM2 5 PM2 5 PM10 PM10 PM2 5 PM1q PM10 PM10 ugima pg m ug Nm _ ug Nm ug Nm ug Nm 211 3 26 2011 18 1 19 8 Cologne 212 3 27 2011 36 8 37 0 36 1 38 2 Winter 213 3 28 2011 33 1 32 9 32 2 33 8 214 3 29 2011 67 7 68 4 66 6 69 1 215 3 30 2011 25 1 24 6 25 0 25 8 216 3 31 2011 10 9 9 7 10 1 a li a 217 4 1 2011 13 8 13 7 13 3 12 7 218 4 2 2011 34 8 33 4 219 4 3 2011 22 9 23 4 21 6 21 0 220 4 4 2011 18 3 17 1 17 2 18 2 221 4 5 2011 19 7 19 7 19 4 20
108. 1 2011 73 4 72 7 73 9 74 8 159 2 2 2011 24 8 24 6 22 5 25 0 160 2 3 2011 20 2 20 7 19 0 19 8 161 2 4 2011 11 3 11 8 10 7 11 0 162 2 5 2011 8 9 9 5 163 2 6 2011 15 0 15 3 14 4 16 4 164 2 7 2011 18 0 19 5 19 1 19 9 165 2 8 2011 30 5 31 5 28 7 30 4 166 2 9 2011 30 0 31 3 28 6 31 3 167 2 10 2011 25 7 27 7 26 6 27 8 168 2 11 2011 13 6 14 6 13 2 15 2 169 2 12 2011 18 8 19 4 170 2 13 2011 17 6 19 0 17 1 17 2 171 2 14 2011 24 5 25 2 24 7 26 3 172 2 15 2011 19 7 20 5 21 5 20 4 173 2 16 2011 34 8 35 4 36 1 34 4 174 2 17 2011 43 1 43 3 45 2 45 4 175 2 18 2011 43 6 44 2 46 1 47 9 176 2 19 2011 56 7 56 2 177 2 20 2011 29 3 29 9 30 7 28 9 178 2 21 2011 36 1 36 1 36 8 35 9 179 2 22 2011 42 6 43 6 44 7 45 8 180 2 23 2011 45 4 45 9 47 0 48 4 740300_2011_936_21209885B_eng doc TUVRheinland Precisely Right Page 192 of 422 TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Annex 5 PM10 measured values from field test sites related to standard conditions EN 12431 Page 18 of 22 Manufacturer Thermo Fi
109. 12 6 13 7 52 1 29 2010 5 7 6 0 61 5 9 2 9 4 53 1 30 2010 12 4 12 5 70 7 15 6 16 2 54 1 31 2010 12 2 13 0 73 5 15 1 15 9 55 2 1 2010 8 4 8 3 57 5 14 1 14 2 56 2 2 2010 8 3 8 3 70 0 11 6 11 2 57 2 3 2010 9 4 9 3 48 6 15 9 16 1 58 2 4 2010 12 0 12 4 61 7 18 0 18 6 59 2 5 2010 Inlet gt Zero filter 60 2 6 2010 Zero filter 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B TUVRheinland Precisely Right Page 177 of 422 Annex 5 Measured values from field test sites related to actual conditions Page 3 of 22 Manufacturer Thermo Fisher Scientific Suspended particulate matter PM10 Type of instrument TEOM 1405 F Measured values in yg m ACT Serial No SN 20006 amp SN 20107 No Date Ref 1 Ref 2 Ref 1 Ref 2 Ratio SN 20006 SN 20107 Remark Test site PM2 5 PM2 5 PM10 PM10 _ PM2 5 PM10 PM10 PM10 ug m yg m ug m yg m ug m ug m 61 27210 es Zero filter Teddington 62 2 8 2010 19 9 SN 20006 Zero filter gt Inlet Winter 63 2 9 2010 6 3 6 3 53 8 10 8 11 8 64 2 10 2010 5 8 5 6 46 6 10 9 13 2 65 2 11 2010 12 4 12 0 60 5 16 3 18 8 66 2 12 2010 6 7 6 5 52 7 10 1 12 5 67 2 13 2010 8 8 8 8
110. 14405 0323 0 0 285 S0B675 25 510075 250 4390046 250 4 30 64206 1820 19918428F 1406 25579 o o 7255 98975 235510115 250 440046 204 21 6S206 1020 ISAT 14405 2323 o 0 25 00075 265 510115 20 431846 20 4 6S2006 1820 IISA 14E o o 25 98975 25 510143 250 440046 204 23 65206 18 20 15a AHF 1440520323 0 0 25 SOGEIS 265 510178 250 44346 20 4 24 650006 1820 19918487F 1406 25579 o o 255 98575 25 510187 250 440046 204 25652006 1021 1670 4697 14405 0323 0 0 205 S0BE75 265 510184 20 44346 w04 25 S520006 1821 1a IME o o 7265 98975 265 510158 250 440046 204 27 662008 1021 Imad 1440520323 0 0 205 OBES 265 510152 250 430046 20 4 23 62006 18 21 IIB 4eSF 14406 269g o o 7265 98975 725 510081 250 440046 20 4 23 662008 1021 150A ARF 144050323 0 0 25 0005 25 51005 250 480046 20 4 30 60006 18 21 Sissy 14406 27a o o 25 8575 255 AIS 250 440046 204 GS2006 1022 ISNA 14405 2033 0 0 205 S0BE75 285 808605 250 4390046 20 4 6S 2006 18 22 1ISSI8 42eSF 14406 267g o o 7265 98975 265 682 250 440046 204 33 65206 1022 157GA 144050323 0 0 205 OBES 265 508692 250 490046 20 4 341650006 1822 15991848F 1406 25979 o o 7255 98575 765 B559 250 440046 20 4 35 65206 18 22 189G AR 144050323 0 0 25 OBES 265 808383 250 480046 20 4 35 65206 1822 19918487F 14406 255979 o o 265 98575 265 987273 250 440046 204 37 65206 1023 SEAR 14405 0323 Lt 0 205 SORES 265 500103 250 4390046 0 4 38 S520066 1823 ISB 42a 14406 26g o o 25 98375 265 5089 250 440046 204 33 65
111. 1_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 910f422 6 1 5 3 5 Sensitivity coefficient of the sample gas pressure The sensitivity coefficient of sample gas pressure at reference point shall not exceed the re quirements of Table 2 of Standard VDI 4202 Part 1 September 2010 A value ct at 70 to 80 of the upper limit of the certification range shall be used as reference point Note This point is not relevant for particulate measuring devices 6 2 Equipment Not applicable 6 3 Performance of test Not applicable 6 4 Evaluation Not applicable 6 5 Assessment Not applicable Minimum requirement fulfilled 6 6 Detailed representation of the test results Not applicable 740300_2011_936_21209885B_eng doc aT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 92 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 1 5 3 6 Sensitivity coefficient of the sample gas temperature T
112. 2 karsten pletscher de tuv com Scope of report Report 170 Pages Annex Page 171 Manual Page 218 Manual of 204 Pages Total 422 Pages 740300_2011_936_21209885B_eng doc r T V Rheinland Energie und Umwelt GmbH TUV Rheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the P 4 of 422 company Thermo Fisher Scientific for the component PM10 AUR Report No 936 21209885 B Blank Page 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Ty 7 Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 5 01422 Content 1 SUMMARY AND PROPOSAL FOR DECLARATION OF SUITABILITY eeeee 13 141 SUMMATY ie sticrcerccedncubaacktn tenes nn a anal asians anienmeceedguat abs sbetaniced Ea NaRa AE EEEa Eia 13 1 2 Proposal of declaration of suitability ccccccessseeeeseneceeeeeeeeeeneeceeeeeeeeeesesseeeeeeeeeeeeeeeegs 18 1 3 Summary of test TESUNS cicceiseescucnorseefateain sateteastesiecebeetenaasinuceiesdetalsetbe nacabuncsnastebeusonnuleenste 19 2 TASK DEFINIT TION Reeeepeer eee e errr ren een entre reenter tern ter meyer errerte rena rrer
113. 2 1 2 turns a 4 Open the mass transducer refer to the Replacing the TEOM Filter section earlier in this chapter for instructions on opening the mass transducer 5 26 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC THERMO FISHER SCIENTIFIC Figure 5 35 Air inlets Nozzle Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 5 Place a piece of plastic or another protective material over the exposed TEOM filters 6 Using a soapy water alcohol or freon solution clean the left side of the ait inlet Figure 5 35 A soft brush may be used to remove particulate matter on the insides of the walls o 7 Allow the air inlet to dry 8 Remove the protective material from the exposed TEOM filters 9 Close the mass transducer and latch the latch 10 Install the air thermistors into the cap of the mass transducer assembly and tighten lightly with the wrench 11 Close and latch the door to the unit Keep the door open for as short a time as possible to minimize the temperature change in the system 12 Turn on the TEOM 1405 unit Operatine Guine TEOM 1405 F 5 27 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Cleaning the Coolers The cooler should be cleaned once per year or as necessary The Cooler Cleaning Wizard describes all the steps necessary to clean the cooler Some additional information is included below Follow these steps to clean the coolers 1 In the 1405 TEOM Data screen select the Servic
114. 206 1023 16A AHF 14405 0323 0 0 205 SORES 265 08719 250 430046 20 4 4 65206 1823 1918487 614406 254979 o o 255 8575 765 98518 250 440046 20 4 187A TGR RO Tne ee a n S RNOETE WERNI ENANAR na mer 4 1405A200010605_2006 6 6_13 47 5 lt a pe Peachy n THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 3 33 Section 3 Basic OPERATION User O The TEOM 1405 allows users additional analog input and analog and Co nne cti ons digital output capabilities using the 25 pin USER I O connector on the back of the instrument The female 25 pin USER I O connector Figures 3 36 has connections for eight analog output four analog input and two digital output contact closure connections Figure 3 36 USER 1 0 connector Thermo Fisher Scientific offers a 25 pin male connector manufactured by Phoenix Contact that can be wited to match to the USER I O connector on the back of the instrument Figure 3 37 Figure 3 37 25 pin connector 3 34 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 3 Basic OPERATION USER I O Wire the desired analog input analog output or digital output connections Pin Assignments to the Phoenix Contact 25 pin male connector according to the manufacturer s instructions and the pin assignments of the TEOM 1405 Figure 3 38and Table 3 1 Figure 3 38 1405 USER 1 0 pin assignments User I O USER ANALOG OUTPUT 1 USER ANALOG OUTPUT GROUND USER ANALOG OUTPUT 2 15
115. 3 Criterion 4 Criterion 5 C a L Other Combined Datasets gt 30 ug m3 51 0 966 0 986 0 026 0 104 1 147 9 36 100 0 All Data 237 0 970 0 994 0 011 0 170 0 294 9 01 23 2 Orthogonal Regression Limit Value of 50 ug m3 nc s r2 Slope b ub Intercept a ua WCM gt 28 ug m3 SN 20107 Dataset Teddington Summer Cologne Winter Individual Datasets Bornheim Summer Teddington Winter 57 0 927 1 065 74 0 978 1 005 54 0 906 1 112 45 0 983 0 934 0 807 0 710 0 860 0 108 1 8 55 4 3 7 lt 30 ug m3 184 0 886 1 052 0 062 ed as follows Combined Datasets gt 30 ug m3 46 0 949 1 010 All Data 230 0 970 0 996 The check of the five criteria from chapter 6 1 Methodology of the equivalence check result Criterion 1 Greater than 20 of the data are greater than 28 g m Criterion 2 The intra instrument uncertainty of the candidates is smaller than 2 5 g m Criterion 3 The intra instrument uncertainty of the reference is smaller than 2 0 ug m Criterion 4 All of the expanded uncertainties are below 25 Criterion 5 The slope and the intercept are not significant for the All data comparison for SN 20006 The intercept for SN 20107 is significantly greater than allowed Other The evaluation of the All data set for both candidates together shows that the AMS demonstrates a very good correlation with t
116. 3 0 3 60 2 6 2010 5 1 7 8 1017 89 7 0 6 227 0 0 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B A TUVRheinland Precisely Right Page 199 of 422 Annex 6 Ambient conditions at the field test sites Page 3 of 11 C C hPa m s El mm 2 7 2010 Teddington 3 8 5 6 85 1 0 8 201 0 0 62 2 8 2010 Winter 82 1 2 0 137 0 5 63 2 9 2010 77 7 1 3 233 0 0 64 2 10 2010 70 1 1 8 215 0 0 65 2 11 2010 74 1 1 1 233 1 0 66 2 12 2010 76 5 1 1 167 0 5 67 2 13 2010 82 4 0 5 254 0 0 68 2 14 2010 91 8 0 1 241 0 3 69 2 15 2010 89 7 0 1 203 7 9 70 2 16 2010 94 6 0 1 186 23 1 71 2 17 2010 78 8 0 3 139 1 0 72 2 18 2010 92 6 0 7 216 4 6 73 2 19 2010 87 5 0 2 238 0 3 74 2 20 2010 87 9 0 2 216 3 3 75 2 21 2010 92 2 0 5 150 14 7 76 2 22 2010 88 2 1 4 140 2 8 77 2 23 2010 92 2 0 8 127 3 6 78 2 24 2010 91 6 0 5 188 2 8 79 2 25 2010 88 1 1 0 174 8 6 80 2 26 2010 77 0 0 7 208 1 3 81 2 27 2010 88 4 0 7 181 17 5 82 2 28 2010 88 5 0 5 258 4 3 83 3 1 2010 78 0 0 2 236 0 0 84 3 2 2010 62 9 0 9 101 0 0 85 3 3 2010 71 6 2 5 85 0 0 86 3 4 2010 72 0 1 0 196 0 0 4 27 2010 Teddington 0 0 4 28 2010 Summer 0 0 4 29 201
117. 5 222 4 6 2011 24 7 25 1 25 0 26 6 223 4 7 2011 24 1 25 3 24 8 25 9 224 4 8 2011 36 2 36 3 Inlet gt Zero filter 225 4 9 2011 Zero filter 226 4 10 2011 24 3 23 5 Zero filter 227 4 11 2011 31 8 32 3 34 8 35 8 228 4 12 2011 18 9 18 1 18 2 20 7 229 4 13 2011 25 1 24 1 26 1 27 9 230 4 14 2011 32 7 32 5 34 0 36 0 231 4 15 2011 32 9 33 2 27 9 27 4 232 4 16 2011 35 8 34 3 233 4 17 2011 22 5 22 0 234 4 18 2011 27 6 28 1 29 7 31 8 235 4 19 2011 31 9 32 6 34 8 36 5 236 4 20 2011 35 8 36 4 39 3 40 9 237 4 21 2011 36 9 39 3 238 4 22 2011 32 6 33 7 239 4 23 2011 43 5 45 5 240 4 24 2011 33 3 35 6 740300_2011_936_21209885B_eng doc y T V Rheinland Energie und Umwelt GmbH TUV Rheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Page 194 of 422 Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Annex 5 PM10 measured values from field test sites related to standard conditions EN 12431 Page 20 of 22 Manufacturer Thermo Fisher Scientific Suspended particulate matter PM10 Au Benluft Type of instrument TEOM 1405 F Measured values in g m STD Serial No SN 20006 amp SN
118. 5 2 7 Maintenance in terval TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B filled Performance requirements The manufacturer s specifica tions in the instruction manual shall be by no means better than the results of the perfor mance test Deviating specifi cations shall be corrected in the instruction manual by the manufacturer before declara tion of suitability General requirements on measuring systems Have to comply with the re quirements of Table 1 of the Standard VDI 4202 Part 1 The upper limit of measure ment of the measuring systems shall be greater or equal to the upper limit of the certification range Negative output signals or measured values may not be suppressed life zero Uncontrolled emission of oper ation and calibration gas shall be avoided The instrument pa rameters shall be secured by buffering against loss caused by failure in the mains voltage When mains voltage returns the instrument shall automati cally reach the operation mode and start the measurement ac cording to the operating in structions The measuring system shall al low the control of important op erating states by telemetrically transmitted status signals Switch over
119. 5 36 TEOM 1405 F CIENTIFIC Service Calibration Ambien Caleation Click the button bo enter the cusrent actual aeblent bemperabure of pressure EAN Ee m a Mabidn Harea chiles a ATHE 1E 3 Determine the current temperature C at the ambient temperature sensor using an external thermometer C 5 9 x F 32 4 If the measured value is within 2 C of the temperature displayed in the Ambient Temperature field of the button no further action is necessary Select the lt Back button to return to the Calibration screen If the value is not within 2 C of the temperature displayed in the Ambient Temperature field of the button select the Ambient Temperature button A keypad will display Enter the actual temperature as measured by the external thermometer and press the Enter button The Ambient Temperature Calibration screen will display with the new entered value Select the lt Back button to return to the Calibration screen THERMO FISHER SCIENTIFIC Calibrating the Ambient Pressure Figure 5 53 Ambient Calibration screen THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Perform the ambient air temperature calibration pressure calibration and leak check Section 3 before executing the flow calibration procedure To calibrate the ambient pressure 1 In the TEOM Data screen select the Service button to display the Service screen then select t
120. 5 5 4 3 8 3 276 8 15 2011 6 0 5 4 41 7 14 5 15 3 277 8 16 2011 6 0 6 0 45 1 14 5 15 9 278 8 17 2011 14 7 14 0 56 3 26 6 28 0 279 8 18 2011 9 0 8 7 54 1 21 5 21 2 280 8 19 2011 6 6 6 2 48 8 15 0 16 2 281 8 20 2011 17 9 16 2 282 8 21 2011 10 4 10 3 60 4 20 3 19 6 283 8 22 2011 10 9 10 8 55 8 22 0 24 2 284 8 23 2011 19 2 19 1 63 7 33 6 35 8 285 8 24 2011 6 7 7 4 41 9 15 3 18 8 286 8 25 2011 11 5 12 1 63 4 19 5 19 8 287 8 26 2011 4 9 5 5 48 8 12 5 12 4 288 8 27 2011 5 3 5 9 289 8 28 2011 1 8 1 8 24 1 7 8 7 3 290 8 29 2011 5 9 6 2 53 0 11 2 11 6 291 8 30 2011 9 1 8 1 51 1 16 0 17 2 292 8 31 2011 14 5 13 9 57 2 24 3 26 0 293 9 1 2011 17 7 18 2 66 9 27 9 28 9 294 9 2 2011 14 9 15 0 60 6 24 1 24 0 295 9 3 2011 26 4 25 7 296 9 4 2011 8 2 8 0 65 3 13 1 11 8 297 9 5 2011 4 8 5 0 53 8 7 6 7 6 298 9 6 2011 5 2 5 6 49 8 10 4 10 2 299 9 7 2011 6 1 5 8 46 1 11 0 11 6 300 9 8 2011 8 0 7 8 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B TUVRheinland Precisely Right Page 185 of 422 Annex 5 Measured values from field test sites related to actual conditions Page 11 of 22 Manufacturer Thermo Fisher Scientific Suspe
121. 57 6 11 2 13 2 68 2 14 2010 13 9 13 4 84 8 12 6 16 3 69 2 15 2010 12 5 12 8 79 2 13 5 15 2 70 2 16 2010 14 9 15 9 83 9 15 4 17 0 71 2 17 2010 44 8 45 2 86 3 47 4 48 4 72 2 18 2010 13 1 12 3 85 9 12 2 16 2 73 2 19 2010 18 3 18 5 84 6 18 7 20 9 74 2 20 2010 16 5 16 6 85 2 17 3 19 8 75 2 21 2010 7 4 7 3 71 7 8 2 10 0 76 2 22 2010 9 9 10 3 61 1 13 4 14 9 77 2 23 2010 14 5 14 4 64 9 17 6 19 8 78 2 24 2010 9 2 9 1 51 6 14 7 15 9 79 2 25 2010 5 9 4 8 57 2 8 6 9 7 80 2 26 2010 4 4 4 3 38 8 10 4 11 2 81 2 27 2010 11 8 TIEZ 61 6 18 1 17 5 82 2 28 2010 5 0 5 2 53 5 7 0 9 7 83 3 1 2010 26 2 26 8 84 3 2 2010 12 7 13 1 60 4 18 6 20 5 85 3 3 2010 7 9 8 7 39 3 17 8 19 7 86 3 4 2010 9 3 8 7 54 2 15 2 16 6 87 4 27 2010 12 1 11 2 56 7 21 2 20 6 Teddington 88 4 28 2010 16 0 16 7 64 3 26 8 26 0 Summer 89 4 29 2010 11 3 11 4 58 9 21 1 20 7 90 4 30 2010 5 4 5 4 45 9 12 4 13 1 740300_2011_936_21209885B_eng doc y T V Rheinland Energie und Umwelt GmbH TUV Rheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Page 178 of 422 Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Annex 5 Measured values from field test sites related to actual conditions Page 4 of 22 Manufacturer Thermo Fisher Scientific Suspended particulate
122. 6 20 2010 6 21 2010 6 22 2010 6 23 2010 6 24 2010 6 25 2010 6 26 2010 6 27 2010 6 28 2010 6 29 2010 Ambient conditions at the field test sites Teddington 14 3 Summer 13 0 17 4 17 5 20 3 22 1 18 2 15 8 15 7 17 8 15 2 15 5 15 6 16 9 14 6 14 4 15 2 17 6 14 5 12 5 15 6 19 8 21 5 21 8 21 3 21 9 21 1 22 8 23 2 21 5 16 7 16 7 24 5 22 7 29 6 28 4 24 7 22 7 20 9 22 2 19 4 21 7 21 5 21 7 20 6 19 3 21 0 24 3 21 1 16 2 22 1 27 5 29 5 30 0 27 7 28 3 27 1 30 8 31 0 30 0 1014 1013 1017 1016 1014 1008 1006 1002 997 1000 1002 1006 1012 1007 1017 1022 1018 1015 1014 1014 1017 1017 1017 1014 1012 1011 1011 1013 1013 1013 72 1 86 7 55 2 51 8 55 5 60 2 68 1 73 9 81 3 72 1 83 2 68 2 63 0 65 8 70 4 56 1 57 8 58 5 69 7 55 8 55 8 55 1 50 1 52 4 54 7 56 1 63 2 50 3 43 9 70 2 A TUVRheinland 0 6 0 4 0 7 1 6 0 5 0 4 0 6 0 5 0 5 1 1 1 8 0 5 0 7 0 7 1 5 1 8 1 9 1 6 1 1 1 5 0 7 0 4 0 3 0 3 0 4 1 0 0 9 0 3 0 3 0 2 203 176 152 91 179 185 262 154 193 154 211 243 201 192 163 171 164 142 216 253 240 194 238 226 261 130 146 203 218 210 Precisely Right Page 201 of 422 Page 5 of 11 Precipitation mm 0 0 2 8 0 0 0 0 0 0 0 0 0 0 7 9 2 3 0 0 0 3 0 0 0 0 0 3 1 8 0 0 0 0 0 0 0 8 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 2 8 0 0
123. 6 Detailed representation of the test results Not required 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Pade 13301422 6 1 5 4 7 Constancy of sample volumetric flow The sample volumetric flow averaged over the sampling time shall be constant within 3 of the rated value All instantaneous values of the sample volumetric flow shall be within a range of 5 of the rated value during sampling 6 2 Equipment For the test additionally a flow meter according to point 4 was provided 6 3 Performance of test The sample volumetric flow was calibrated before the first field sampling test site and tested for its correctness before each field sampling test site using a dry gas meter or a mass flow meter and readjusted if necessary For the measuring device TEOM 1405 F Ambient Particulate Monitor a total flow rate of 16 67 l min at the inlet is split in two sub flows the PM path with 3 l min and the Bypass with 13 67 l min To determine the constancy of the relevant sample volumetric flow a flow rate for PM10 and a total flow rate for the test site Cologne Winter which partly was characterized by high concentrations and fi
124. 74 20 9 280 8 19 2011 16 8 21 2 1011 80 0 1 5 235 3 3 281 8 20 2011 20 7 28 1 1011 66 6 0 8 157 0 0 282 8 21 2011 23 2 31 4 1007 74 8 1 0 184 0 3 283 8 22 2011 20 4 24 4 1009 76 5 1 2 253 0 0 284 8 23 2011 22 6 27 8 1005 78 4 0 9 206 0 0 285 8 24 2011 20 1 27 2 1007 76 6 0 7 192 0 6 286 8 25 2011 20 8 27 6 1003 83 4 1 0 176 2 1 287 8 26 2011 19 4 30 2 999 83 7 1 5 195 29 1 288 8 27 2011 15 3 20 0 1007 77 0 1 1 207 0 3 289 8 28 2011 15 6 19 7 1009 69 2 1 3 212 0 0 290 8 29 2011 14 5 18 4 1008 66 7 2 0 243 0 0 291 8 30 2011 13 6 18 4 1008 73 6 0 8 236 0 0 292 8 31 2011 14 8 21 4 1007 72 0 0 7 225 0 0 293 9 1 2011 16 4 23 4 1006 71 6 0 6 182 0 0 294 9 2 2011 21 2 29 4 1004 72 2 0 8 160 0 0 295 9 3 2011 24 5 30 9 1002 67 0 1 3 132 3 6 296 9 4 2011 20 2 27 4 1002 79 5 1 1 223 0 6 297 9 5 2011 16 6 21 4 1009 62 9 1 9 217 0 0 298 9 6 2011 17 4 20 6 1005 66 8 2 6 219 4 8 299 9 7 2011 14 9 18 1 1004 73 1 2 2 246 5 7 300 9 8 2011 14 7 16 2 1003 84 7 1 1 209 3 3 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Annex 6 Date Test site Ambient conditions at the field test sites Amb temperature avg C Amb temperature max Amb pressure
125. 8 1 18 1 16 6 20 3 286 8 25 2011 20 2 20 2 21 1 21 4 287 8 26 2011 11 5 11 6 13 7 13 6 288 8 27 2011 5 7 6 2 289 8 28 2011 8 1 8 1 8 2 7 7 290 8 29 2011 12 0 12 2 11 8 12 2 291 8 30 2011 17 9 17 5 16 8 18 1 292 8 31 2011 27 3 25 1 25 7 27 4 293 9 1 2011 29 1 27 9 29 7 30 8 294 9 2 2011 27 0 26 2 26 1 26 0 295 9 3 2011 28 9 28 1 296 9 4 2011 13 7 13 1 14 2 12 8 297 9 5 2011 9 7 9 7 8 1 8 1 298 9 6 2011 11 8 11 4 11 2 10 9 299 9 7 2011 13 2 14 1 11 7 12 3 300 9 8 2011 8 5 8 3 740300_2011_936_21209885B_eng doc y T V Rheinland Energie und Umwelt GmbH TUV Rheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Page 196 of 422 Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Annex 5 PM10 measured values from field test sites related to standard conditions EN 12431 Page 22 of 22 Manufacturer Thermo Fisher Scientific Suspended particulate matter PM10 Aufenluft Type of instrument TEOM 1405 F Measured values in g m STD Serial No SN 20006 amp SN 20107 No Date Ref 1 Ref 2 Ref 1 Ref 2 Ratio SN 20006 SN 20107 Remark Test site PM2 5 PM2 5 PM10 PM10 PM2 5 PM10 PM10 PM10 yg m ug m
126. Ambient Particulate Monitor with PM10 pre separator of the Page 2 of 422 company Thermo Fisher Scientific for the component PM10 s Report No 936 21209885 B Acknowledgement T V Rheinland Energie und Umwelt GmbH would like to acknowledge the involvement of Bureau Veritas and the National Physical Laboratory as our UK partners in this pro ject for their involvement in collecting the UK field data project management and data processing NPL National Physical Laboratory 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 3 0f422 DAkks Deutsche Akkreditierungsstelle D PL 11120 02 00 Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Device tested TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator Manufacturer Thermo Fisher Scientific 27 Forge Parkway Franklin Ma 02038 USA Test period December 2009 to October 2011 Date of report November 25 2011 Report Number 936 21209885 B Editor Dipl Ing Karsten Pletscher Tel 49 221 806 259
127. CE REPAIR SERVICE RELOCATION OR ALTERATION TO OR OF OR OTHER TAMPERING WITH THE PRODUCTS PERFORMED BY ANY PERSON OR ENTITY OTHER THAN SELLER WITHOUT SELLER S PRIOR WRITTEN APPROVAL OR ANY USE OF REPLACEMENT PARTS NOT SUPPLIED BY SELLER SHALL IMMEDIATELY VOID AND CANCEL ALL WARRANTIES WITH RESPECT TO THE AFFECTED PRODUCTS THE OBLIGATIONS CREATED BY THIS SECTION TO REPAIR OR REPLACE A DEFECTIVE PRODUCT SHALL BE THE SOLE REMEDY OF BUYER IN THE EVENT OF A DEFECTIVE PRODUCT EXCEPT AS EXPRESSLY PROVIDED IN THIS SECTION 9 SELLER DISCLAIMS ALL WARRANTIES WHETHER EXPRESS OR IMPLIED ORAL OR WRITTEN WITH RESPECT TO THE PRODUCTS INCLUDING WITHOUT LIMITATION ALL IMPLIED WARRANTIES OF MERCHANTABILITY OR FITNESS FOR ANY PARTICULAR PURPOSE SELLER DOES NOT WARRANT THAT THE PRODUCTS ARE ERROR FREE OR WILL ACCOMPLISH ANY PARTICULAR RESULT Safety Notice Repair of instrumentation manufactured by Thermo Scientific should only be attempted by properly trained service personnel and should only be conducted in accordance with the Thermo Scientific system documentation Do not tamper with this hardware High voltages may be present in all instrument enclosures Use established safety precautions when working with this instrument The seller cannot foresee all possible modes of operation in which the user may attempt to use this instrumentation The user assumes all liability associated with the use of this instrumentation The seller further disclaims any re
128. CEDURES Advanced Filter Change For experienced users who ate comfortable with the filter change operation the monitor offers an advanced filter change mode When the users selects the advanced mode in the TEOM Filter Replacement starting screen Figure 5 5 the system automatically stops the TEOM filter and displays a screen to prompt the filter change operation Figure 5 15 Replace Filter Open the mass tranmducer and replace filter Figure 5 15 Advanced filter change screen How teat the meirant ie iy sebup ode and lek TEOM it shopped you say Shange the filter lt Back Peri 2 Cancel When the screen displays change the filters and select the Next gt button The finished screen will display Figure 5 16 Figure 5 16 Wizard complete message Seren Ron lbeanant Wizard Filter You have sucessiuly completed the TEGH Filter Replacement Wizard THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 13 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Note The advanced filter wizard DOES NOT automatically check the frequency Users MUST ensure that the frequency is stable in order to ensure valid test data Look at the change in the TE s oscillating frequency on the TEOM Data screen Figure 5 17 The last two digits of the reading will fluctuate due to noise and the rest will remain steady If more than the last two digits fluctuate in this reading this indicates that the TEOM filter is loose Re seat t
129. D CALIBRATION PROCEDURES 5 Clean the internal wall surface of the acceleration assembly Figure 5 24 Note Ensure the acceleration nozzle is clean If not use a cotton swab and cleaner to remove any contamination A Figure 5 24 Interior wall of inlet 6 Inspect the large diameter impactor nozzle O ring for damage or wear Figure 5 20 Replace it if necessary Apply a thin film of silicone grease to the O ring Also apply a light coating of silicone grease to the aluminum threads of the upper acceleration assembly 7 Using a general purpose cleaner with a paper towel clean the collector assembly walls and plate Figure 5 25 Note Most of the contamination in the inlet is usually found on the collector plate a Figure 5 25 Inside of inlet collector assembly Collector plate THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 19 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 8 Clean the three vent tubes Figure 5 25 You may need to use a cotton swab to clean these vent tubes 9 Clean the bottom side of the collector assembly Figure 5 26 Inspect the two inlet tube sealing O rings for damage or wear If necessary replace the O rings Figure 5 26 Bottom of collector assembly with O rings 10 Clean the weep hole in the collector plate where the moisture runs out to the moisture trap Figure 5 25 11 Clean the rain jar Inspect the rain jar cover s brass nipple fitting to ensure that
130. E 05 2 4937E 05 2 8558E 05 rel standard de viation 0 036 0 027 0 031 Median 0 09264 0 09158 0 09117 lowest value 0 09257 0 09154 0 09110 highest value 0 09269 0 09162 0 09122 Highlighted yellow average value Highlighted green lowest value Highlighted blue highest value 740300_2011_936_21209885B_eng doc TUVRheinland TUV Energie und Umwelt GmbH Precisely Right Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Seite 214 von 422 Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B B UK test site Teddington B 1 Implementation of Weighing Protocols NPL National Physical Laboratory were subcontracted to weigh filters manually for the field study In line with EN14907 filters were kept in the weighing room for less than 28 days the glove box used for weighing was maintained at 20 1 C and 50 5 and filters were weighed twice before and after sampling Table 37 summarizes the conditioning and weigh ing timescales utilised Table 37 conditioning and weighing timescales Pre Sampling Post Sampling Condition minimum of 48 hours Condition 48 hours Weigh Filters Weigh Filters Condition 24 hours Condition 24 hours Weigh Filters Weigh Filters At the start of each weighing session the balance was exercised to remove mechanic
131. EOM 1405 software allows users to step through the periodic maintenance procedures Select the Service button to display the Service screen When in the Service screen select the Maintenance button to display the Maintenance screen Figure 5 1 TEOM Data screen TEOM Data TEOM 1405 F TEOM Data System Status MC pgm E 3 38 mihi MAC gen 4 50 1 Hr bet jugi 3 45 B Hour valwe pgi jc 0 00 Instrtenant 12 Hr bat ugm o 00 Conditions 2Hr MC gee O00 Filbew kpadang 1225 t Settings Froger 2427055 Hz Hoi aii jeg Figure 5 2 1405 Service screen System States instament Conditions Settings assert Worst _ ETT 5 2 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Figure 5 3 1405 Maintenance screen TEOM 1405 F Service gt Maintenance 1 FDMS Dryer Thermo Fisher Scientific recommends an annual dryer replacement Replacement refurbishment for the FDMS dryers installed in the 1405 F TEOM Series This refurbishment 75 010965 is to minimize sampling artifacts that could effect the measurement of total mass concentration over time The refurbishment consists of cleaning and any necessary replacement of parts Contact Thermo Fisher Scientific s Service Department Refurbishment THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 3 Section 5 MAINTENANCE AND CALIBRATION PROCED
132. EOM filter 1 Ensure that the filter exchange tool is clean and free of any contamination that might be transferred to the TEOM filter 2 In the 1405 TEOM Data screen select the Service button to display the Service screen then select the Maintenance button to display the Maintenance screen Figure 5 3 3 Select the Replace TEOM Filter button to start the TEOM Filter Replacement Wizard Figure 5 5 Select the Next gt button to begin the procedure Note If you are an experienced user and comfortable with changing TEOM filters select the Advanced User Mode button to stop the movement of the mass transducer and proceed with a quick exchange procedure Refer to the next section for a complete explanation of the Advanced User Mode for filter changes a Figure 5 5 TEOM Filter Replacement Wizard starting screen Welcome to the TEOM Filter Replacement Wizard This wizard heips you replace TEOM filters on the TEOM Ambient Particulate Monitor The instrument will be put in Setup mode tor tilter replacement i Ensure that the titer exchange tool is Ay clean and tree of any contamination that might be trnstened to the TEOM fter Ad anced User Mode To continue press Newt Next gt Cancel 5 6 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 4 The Open Mass Transducer screen will display Open the door of the sampler 5 Pull the TEOM latc
133. FDMS unit shall be changed or refur bished For the monitoring securing of a proper dryer performance the manufacturer recommends to monitor a pump vacuum nominal gt 510 mm Hg and a dew point of the air flow nominal lt 2 C at 4 C cooler temperature as well as to carry out period ical at least once a year zero point checks running of the measuring device with ze ro filter at the inlet 12 Every 18 months or if necessary the sampler pump shall be maintained or renewed To carry out the maintenance works the instruction of the manual chapter 5 are to be taken into account All works can usually be carried out with commonly available tools 740300_2011_936_21209885B_eng doc aT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 64 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 5 Assessment Maintenance works can be carried out with commonly available tools taking reasonable time and effort For the maintenance works as per points 3 4 6 and 10 the device is switched to setup mode The restart of the normal measuring process occurs after one hour after having finished the check and after having left the setup mode The maintenance works as per points 8 9 11 and 12 can only be done
134. Figure 5 41 Cleaning channel Cleaning channels screen 10 When the procedure is finished select the Next gt button 11 The Close Unit screen will display Disconnect the adapters and reinstall the tubing into the cooler assembly as described by the wizard 12 Reinstall the 47 mm filter cassette with new filter installed into the unit Refer to the Replacing the 47 mm Filters section earlier in this chapter for more information on removing the filter cassettes 13 Reinstall the tower cover 5 32 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 14 Select the Next gt button The wizard will display a message showing the procedure is complete Figure 5 42 Select the Finish button to exit the wizard and return to the Maintenance screen or select the lt Back button to move backward one step in the procedure Figure 5 42 Complete screen Completing the Cooler Cleaning Wizard The Cooler Cleaning Wizard has completed sucess tulby The iestrument will be put in Run mede when this wizard is finished Toe close thie witard prese Finish THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 33 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Cleaning the The switching valve should be cleaned once a year or as necessary Switching Valve Follow these steps to clean the switching valve 1 In the 1405 TEOM Data screen select the Service
135. GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Z aouaIay We 70 Not Outlier Outlier Deleted 60 4 Outlier Not Deleted 1 to 1 Line 0 10 20 30 40 50 60 70 PM Reference 1 Figure 26 Grubbs test results for the PM reference method Bornheim Summer 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 5901422 Filter handling Mass determination The following filters were used for the suitability testing Table 8 Used filter materials Measuring device Filter material type Manufacturer Reference value Emfab 47 mm Pall LVS3 The filter material EMFAB Teflon coated glass fibre filters was used in the scope of the Combined MCERTS and T V PM Equivalence Testing program by special request of our British partners because according to 8 they consider it most appropriate for the test pur pose The filter handling is according to the re
136. ISHER SCIENTIFIC Ensure that the PC and the instrument ate connected to the same network using the Ethernet connection on the back of the instrument Refer to the Connecting to the TEOM 1405 Unit section for information on connecting the instrument to a network Use the ePort PC software to connect to the instrument and display the ePort Main screen Figure 3 31 Refer to the Connecting to the TEOM 1405 Unit section for information on connecting to the instrument Note Once you have connected to an instrument or instruments and saved a configuration file select Open Saved Configuration in the ePort Open screen to open that configuration and automatically connect to all the instruments that were saved in that configuration a 1405200100605 DichotFDMS Serial Nemden 14064309100505 IP Address 10 210 96 145 States the Commands An Connicad Duta al Remote heat ae Deolyy ge Ponh Inatrurert irera af Cceriked Sanu Download Details Decanload folder Location C Progran Mia tharrelaPeet Last download Pectomabed deemioads Cesbbed re a Last noad or Stlected Date and Tine Next downloud wil start with dete after 2i Dor lt 2007 0 220 ex Operatine Guine TEOM 1405 F 3 29 Section 3 Basic OPERATION 3 Select Download Data in the Commands window of the ePort Main screen The Download Data screen will display Figure 3 32 Figure 3 32 Download Data screen Download Data To download data
137. MS Serial umber 12456799 DP Adcirees 110 210 9524 Status Adja Corrmaanejs D Conrinad Date ID Rewete bhatace Oits p Upgrade hutrurart Frrrawe Fi Door Seseching fse Insirumenis C Operatine Guine TEOM 1405 F 3 23 Section 3 Basic OPERATION 3 All instruments located on the local network will be displayed in the Instrument frame on the left side of the Main screen To edit a displayed instrument or delete an instrument from the list right click on the instrument and select Edit Instrument or Delete Instrument Figure 3 27 Note To add an instrument from another network connected to the local network select Instrument then New Instrument from the menu bar Refer to the previous section for more information on manually adding an instrument to the configuration a Figure 3 27 Adding or deleting an ap ePort instrument from the list File Instrument Help E kd Group ww 14054200090602 ew 14054200090604 ep 14054200090605 14054200 aaae ror e 14054200 Delete Instrument 4 To save this list as a configuration select File then Save from the menu bar at the top of the Main screen The Save As screen will display Type in the desired name for the configuration and select Save Note Once you have connected to an instrument or instruments and saved a configuration file select Open Saved Configuration in the ePort Open screen to open that configuration and automatically connect to all the
138. Minimum requirement fulfilled yes 6 6 Detailed representation of the test results Not required for this minimum requirement 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH F Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 101422 6 1 5 2 4 Failure in the mains voltage In case of malfunction of the measuring system or failure in the mains voltage for a period of up to 72 h uncontrolled emission of operation and calibration gas shall be avoided The in strument parameters shall be secured by buffering against loss caused by failure in the mains voltage When mains voltage returns the instrument shall automatically reach the op eration mode and start the measurement according to the operating instructions 6 2 Equipment Not required for this minimum requirement 6 3 Performance of test A failure in the mains voltage was simulated and it was tested if the instrument remains un damaged and ready for measurement after restart of the power supply 6 4 Evaluation Since the measuring devices need neither operational nor calibration gases for operating an uncontrolled escape of gases is not possible In the case of a failure in the mains voltage the measuring device
139. Not applicable 6 5 Assessment Not applicable Minimum requirement fulfilled 6 6 Detailed representation of the test results Not applicable 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Report on the suitability test of the ambient air quality measuring system Precisely Right TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 7 Page 167 of 422 Recommendations for practical use Works in the maintenance interval 4 weeks The following procedures are required to be undertaken at regular intervals Regular visual inspection telemetric monitoring Check if device status is o k Check if there are no error messages Check if there are no contaminations Check of the instrument functions according to the instructions of the manufacturer Maintenance of the sampling inlet according to the instructions of the manufacturer Monthly change of the TEOM filters or in case the filter load gt 90 is reached Simultaneously with the change of the TEOM filters the cooled 47 mm filter of the FDMS unit have to be changed Every 4 weeks plausibility check of temperature pressure sensors if necessary re calibration Every 4 weeks leak check Every 4 weeks check of the flow rate if necessary re calibration Apart from that follow the manufacturer s d
140. O audit Figure 5 87 a 5 68 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 12 The Replace Sample Filter screen will display Figure 5 85 Remove the calibration filter with the calibration filter removal tool Correctly install and properly seat a new TEOM filter onto the mass transducer using the regular filter exchange tool Follow the instructions for changing a filter earlier in this section Select the Next gt button Note DO NOT use the calibration filter exchange tool for installing or removing ANY filter other than the pre weighed calibration filter a Note If the frequency doesn t stabilize the wizard will display a screen with instructions to re seat the filter Re seat the filter and select the Next gt button The Stabilizing screen will display If the unit is unable find a stable frequency the second time the unit will fail the KO audit Figure 5 87 a Figure 5 85 Replace Sample Filter Replace Sample Filter screen Do mot use the calibration filler exchange tool te installing or removing any filter oiher than the calibration filter Dpen he ie Irument door amd mass transducer Correctly install and properly geal a mew regular TEOM filter onto the mase transducer Close the mass transducer and instrument door x Back Peri gt Cancel THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 69 Section 5 MAINTENANCE AND CALIBRATION
141. OM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Description of the test SiteS 2 0 0 0 ce eee ce ccc ceeecee cece cence eens eeeeeeeeeeeeeeeeeeeneeeeeeeeeeeereeess 17 Instrument modifications after field test site Teddington Summer 44 Device related characteristics TEOM 1405 F Ambient Particulate Monitor manufacturer information wiocacsndsascuetnccetcanee eel sacteste des stueesascostedectanmncaeessdnetdenstine 45 Field test Sites cienne i ie ee a eee 49 Ambient conditions at the field test sites expressed as daily averages 54 Results Grubbs outlier test Reference PMo cceeceeeeeeeeeeeeeeennneeeeeeeeeeeennees 55 Removed data pairs reference PM1o according to Grubbs n 56 Used filter materials ccccccceeeeeeeeeeeeeeeeeeeeeeeeeceeeceeeeeeeceeeeeeeeeeeeeeeeeeeeeeeeeeeeeees 59 Certification ranges GR set uieeeaccesiecierceecidecteescrraneedidsaaatieie E EEG 74 Determination of availability without test related outages eceeeeeeeeeeeeeeee 82 Determination of availability including test related Outages cece 82 Detection limit PM cccecceeccceeccsceccsueceeueeseueeseeueeesuaeeeuaaeeuuaseuuaeeeuaueeuaeeeuaaeeuaaeess 88 Dependence of the zero point on the surrounding temperature deviation in ug m average for 3 MEASUFEMENMS 0 cee e
142. ON 3 36 Operatine Guine TEOM 1405 F When the 25 pin Phoenix Contact connector is attached to the unit with the wired digital or analog device connections the inputs outputs must be set up using the TEOM 1405 software screens When in the Instrument Conditions screen select the Analog Inputs button to set up the analog inputs 1 4 and convert the incoming voltage to the desired scale The analog inputs are self calibrating When in the Settings screen select the Analog amp Digital Outputs screen to set up the analog outputs 1 8 and digital outputs contact closures 1 2 e When in the Analog amp Digital Outputs screen select the Analog Outputs button to seta minimum and maximum value for the output for the desired output channel Refer to Section 5 for information on calibrating the analog outputs e When in the Analog amp Digital Outputs screen select the Contact Closure 8 8 P button to select a variable operator and compare value for the desired contact closure channel 1 2 Refer to Section 4 for complete information on setting the inputs outputs in the Analog Inputs and Analog amp Digital Outputs screens THERMO FISHER SCIENTIFIC Section4 Screens and Settings This section describes the screens shown in the instrument software and the system s operating modes as well as how to change instrument settings When the instrument is started it will display the Title screen for a few seconds Figure 4 1
143. Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 81 01422 6 1 5 2 8 Availability The availability of the measuring system shall be determined during the field test and shall be at least 95 6 2 Equipment Not required for this minimum requirement 6 3 Performance of test Start time and end time of the availability tests were defined by the start and end of the field tests at each test site All measurement interruptions e g due to system outage or mainte nance works were considered for this test 6 4 Evaluation Table 10 and Table 11 show a compilation of the operation maintenance and malfunction times The measuring systems have been operated over a time period of 328 measuring days SN 20006 and 294 measuring days SN 20107 during field test This time period in cludes 14 days of zero filter operation for SN 20006 and 13 days of zero filter operation for SN 20107 refer to Annex 5 Data loss caused by external influences which cannot be attributed to the devices them selves have been recorded on 19 01 2010 10 03 2011 and 14 03 2011 power outage Therefore the total operating time is reduced to 325 SN 20006 and 291 SN 20107 meas uring days The following malfunctions of the devices have been observed SN 20006
144. Setup Mode Refer to the beginning of this section for more information on operating modes e Stop This button manually puts the instrument in Stop All Mode Refer to the beginning of this section for more information on operating modes e Reboot This button IMMEDIATELY restarts the instrument Pressing the button returns the unit to Stabilizing Mode and will require the full warm up period before restarting data collection THERMO FISHER SCIENTIFIC Section 4 SCREENS AND SETTINGS Service Advanced Select the Advanced button to display the Advanced screen Figure 4 28 Screen The Advanced screen allows users to manually adjust the status temperatures or flows of several instrument components Figure 4 28 Advanced screen TEOM 1405 F Service Advanced we ozr 1253 ai Habing Heey sialup Only qualified service personnel should attempt to adjust these settings Contact Thermo Scientific before adjusting any of these settings THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 4 35 Section 4 SCREENS AND SETTINGS Installing New Firmware Figure 4 29 System Status screen IP address 4 36 Operatine Guine TEOM 1405 F If the instrument needs new firmware there are two methods that can be used to update the instrument using the ePort software or by using a USB flash drive Refer to Section 3 for information on installing and starting the ePort software New versions of the TEOM 1405 instrument software ar
145. System screen Figure 4 19 allows users to set the basic configuration Figure 4 19 System screen 4 24 Operatine Guine TEOM 1405 F of the unit TEOM 1405 F Seliinge gt Sysiem cme oe tit EA Bat omer eS ED Slopped Moma sates ae AORTAE 1207 When in the System screen e Set Time Select the Set Time button to enter the current time and date e Password Protection Select the Password Protection button to initiate High Lock or Low Lock mode In Low Lock mode the user can view all instrument screens and can change the operating mode to perform filter changes High Lock mode means the user cannot view any screens other than the TEOM Data screen The user can also set the password using this button Network Configuration Select the Network Configuration button to determine whether the unit s Internet Protocol IP address will be selected automatically or entered manually If the user wishes to specify an IP address the user must enter both the correct IP address and the Subnet mask for the system e Display Select the Display button to choose the preferred viewing mode of the instrument screen white background with black text or black background with white text THERMO FISHER SCIENTIFIC THERMO FISHER SCIENTIFIC Section 4 SCREENS AND SETTINGS Decimal Symbol Select the Decimal Symbol button to choose whether to separate decimal numbers with a period or a comma
146. TUV RHEINLAND ENERGIE UND UMWELT GMBH DAkks Deutsche Akkreditierungsstelle D PL 11120 02 00 Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM pre separator of the company Thermo Fisher Scientific for the compo nent PM1 TUV Report 936 21209885 B Cologne November 25 2011 www umwelt tuv de luft de tuv com TUV Rheinland Energie und Umwelt GmbH is accredited for the following work areas Determination of emissions and ambient airs of air pollution and odor substances Inspection of correct installation function and calibration of continuously running emission measuring devices including systems for data evaluation and remote monitoring of emissions Suitability testing of measuring systems for continuous monitoring of emissions and ambient airs and of electronic systems for data evaluation and remote monitoring of emissions according to EN ISO IEC 17025 The accreditation is valid up to 31 01 2013 DAkkS register number D PL 11120 02 00 Reproduction of extracts from this test report is subject to written consent TUV Rheinland Energie und Umwelt GmbH D 51105 K ln Am Grauen Stein Tel 0221 806 2756 Fax 0221 806 1349 740300_2011_936_21209885B_eng doc i i TUV Rheinland Energie und Umwelt GmbH TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F
147. The unit must be restarted for this change to take effect Date Format Select the Date Format button to choose whether to display the date in the Month Day Year or the Day Month Year format The unit must be restarted for this change to take effect Operatine Guine TEOM 1405 F 4 25 Section 4 SCREENS AND SETTINGS Analog amp Digital The Analog amp Digital Outputs screen Figure 4 20 allows users to set the Outputs Screen basic parameters of the unit Figure 4 20 Analog amp Digital Outputs screen TEOM 1405 F Sellings Aralag amp Digital Outputs a Sifting Mereal chiles a TUR PONE 1 When in the Analog amp Digital Outputs screen select the Analog Outputs or Contact Closure buttons to set up the analog output and contact closure functions Select the RS232 button to set up the unit for serial connections using RPComm or other programs using AK protocol 4 26 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Analog Outputs Screen Figure 4 21 Analog Outputs screen THERMO FISHER SCIENTIFIC Section 4 SCREENS AND SETTINGS Select the Analog Outputs button to display the Analog Outputs screen Figure 4 21 In the Analog Outputs screen use the buttons to select a variable and set a minimum and maximum value for the output for the desired output channel 1 8 Refer to Section 5 for information on calibrating the analog outputs Settings output pAnaleg Outputs Instrument Variable
148. URES TEOM Filter Replacement Filter Loading Figure 5 4 TEOM Data screen 5 4 Operatine Guine TEOM 1405 F The Series 1405 TEOM filter needs to be changed periodically before filter loading can affect the flow or at least every 30 days Note Change the filter at least every 30 days a The filter loading percentage value indicates the percentage of the TEOM filter s total capacity that has been used You can check the TEOM filter loading percentage on the monitor s TEOM Data screen Figure 5 4 Because this value is determined by the pressure drop of the main sample flow line the instrument always shows a non zero value even if no TEOM filter is mounted in the mass transducer New TEOM filters generally exhibit filter loading percentages of 15 to 30 at a main flow rate of 3 1 min and less at lower flow rates TEOM 1405 F i li Teh Hata System Status MC pgm E hin hC dugim 1 Hr hat pgm Hour wvalwe gim jc Instrument 12 Hr bat pgm Conditions 2 H ME ugh Filter bowing Fregainibey Settings E Meine Harm plats OFF T13 TEOM filters must be replaced before the filter loading percentage reaches 100 to ensure the quality of the data generated by the instrument At some point above 100 the main flow drops below its set point If the filter loading percentage is higher than 30 at a main flow rate of 3 l min when a new TEOM filter is placed on the mass transducer or if the l
149. a E sacar Ea aad aaa a aeaa ar A oe ude cateagacd 79 5 2 7 Maintenance interval sseeesseseseessesseoosorssssrsnrnrrorirnnnnnnnnnonnnnunnunnunntteenanneeesceeeone 80 5 2 8AValla Dil Yass een a Er eee sericea 81 5 2 9 Instrument software siasseelivececanttnilenntoenstsaustladdiuntentnd daahigaciendieeetendenl datecant ecebstens 83 93 Generalsin i E e ene mre en AEAEE re 85 5 3 2 Repeated standard deviation at Zero point sessrersrrrrrrrrrrrrrrrrrrrrrnrrrrrrrenn 87 5 3 3 Repeated standard deviation at reference poOint ccccccccccceeeeeeeeeeeeeeeeeees 89 5 3 4 Linearity Lack of fit cssteccnccansarsinseaastntdatantasaeaunicectecentedeansecdntncesnexsanseuonariormuases 90 5 3 5 Sensitivity coefficient of the sample gas PreSSUre ccccccccccceeeeeeeeteeeeeeees 91 5 3 6 Sensitivity coefficient of the sample gas temperature ccccccceeeeeeeeeeeees 92 5 3 7 Sensitivity coefficient of the surrounding temperature ccccccccecceeeeeeeees 93 5 3 8 Sensitivity coefficient of the electric voltage o oo eeeeeneee terre eeeeennaeeeeeeeeeeee 96 9 3 9 OSS SESW rusi onra naenin S ai aiaa paa Ea EI AiE eaae niae 98 5 3 10 Averaging CEC cscissscccttiecateenansecsctpeastetantecdaualdotestesteauanusscnumeetansasatuconerannevende 99 5 3 11 Standard deviation from paired measurements ccccccccceeeceeeeeeeeeeeeeees 100 5 3 12 L ng term drifters eissidein niin an iaa adaa Eaa aa Ra iadaaa n
150. a arr O o Qoo0oo0oo0oo0oo0ooO0oO0OO0OO0OO0OO0O000O000O00O0O0O0O0O fc SON DDrKEONTAYAN T GHTNMTNORDAHDONS B NAC FP Foto E O E o n Te NN amp toro Y Y oOo 00 00000 E T E eE e aaa Se ee oO oO dqa y se id TH KH ooo0oo0oo0oo0oo0o0o0o yr PL eS eSeeLle L SooSoDRKR OHTA ARS SE ES a T a LOR 6 Ore te aes oO oa O Kt Streubreite ug 740300_2011_936_21209885B_eng doc TUVRheinland Precisely Right Seite 218 von 422 740300_2011_936_21209885B_eng doc TUV Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Appendix 3 Manuals TEOM 1405 F Ambient Particulate Monitor with FDMS Option 42 010978 Revision A 000 22Sep2009 This documentation contains trade secrets and confidential information proprietary to Thermo Fisher Scientific The software supplied with the instrumentation documentation and any information contained therein may not be used duplicated or disclosed to anyone in whole or in part other than as authorized in a fully executed Thermo Fisher Scientific End User License Agreement or with the express written permission of Thermo Fisher Scientific 2007 Thermo Fisher Scientific All rights reserved TEOM is a registered trademark of Thermo Fisher Scientif
151. a nasa eee cdc gest aida Se ties ead E E E ai 65 6 1 4 1 5 Instrument design acter ate bectae tee dat satestedctdedgaddoeadteeididincnaitnet ad duoantalennebinasiadledens 69 6 1 4 1 6 Unintended AC USIMGME c2c cnccasasesseutarndoecteceiansvascitondaeeinaicasadueoeccoanddeasabboseBbesnds 70 6 1 4 1 7 Data OulpUt atin nieiieis nee Mn Aine iil Glen niah wis 71 6 1 5l Genera lsrs aE a a a a a eaea 73 6 1 5 2 1 Certification rangEeSiisiciisriisc isse ninn bent sSeadelassacdieGtdndutantatcuoideestdemnandedtiaeatieeciins 74 6 1 5 2 2 Meas ning rangE marsis oeno a aie i NE E ETa A ERE EANES 75 740300_2011_936_21209885B_eng doc aT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 6 of 422 company Thermo Fisher Scientific for the component PM10 6 1 6 1 6 1 6 1 6 1 6 1 6 1 6 1 6 1 6 1 6 1 6 1 6 1 6 1 6 1 6 1 6 1 6 1 6 1 6 1 6 1 6 1 6 1 6 1 6 1 6 1 6 1 Report No 936 21209885 B 5 2 3 Negative output signals Jiecnccatecsnssddneciccetacdsi sada gacdiieedaauddesadenesdeeetadeaseedernecadeeaiens 76 5 2 4 Failure in the mains VON G vices ste cscticcncensdoeslsacesh clean tageahebetedensnaheedeeeddenes une 77 5 2 5 Operating Sle WS Sanici aaisa 78 5 2 0 OWC OVOP cata cates scarce T
152. ab filters of A Pre spread weighed relative to the check weight and B Post spread weighed relative to the check weight 217 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH F Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 1997422 1 Summary and proposal for declaration of suitability 1 1 Summary According to Directive 2008 50 EC of 21 May 2008 on Air quality and cleaner air for Europe replaces Council Directive of 27 September 1996 on ambient air quality assessment and management including its daughter directives 1999 30 EC 2000 69 EC 2002 3 EC and the Council Decision 97 101 EC the methods described in Standard EN12341 Air quality De termination of the PM1o fraction of suspended particulate matter Reference method and field test procedure to demonstrate reference equivalence of measurement methods and Stand ard EN14907 Ambient air quality Standard gravimetric measurement method for the de termination of the PM25 mass fraction of suspended particulate matter serve as reference methods for suspended particle measurement of the respective mass fraction However EC member states are free to use any other method in the case of particulate ma
153. aie aian 102 5 3 13 Short time drift ereere eee a a Paia 108 5 3 14 RESPONSE Mencari euie an AREE EAEE REEE EE EEE FAAEA A FERAE NERENS 109 5 3 15 Difference between sample and calibration port ccccccccceeseeeeeeeeeeees 110 5 3 16 Converter efficiency seccccccccanksnssactesnctdantcnatevanuabcottisentednataunctbnestageanaxacanareotuntens 111 5 3 17 Increase of NO concentration due to residence in the measuring system 112 5 3 18 Overall uncertainty ssseeeesseseeseessesoreossssrsranrrornrnnnnnnnnrrnnnnnnnennntetenannneeeeeeeos 113 5 4 1 Generalerna akoiete En aE 114 5 4 2 Equivalency of the sampling system c ceeceeeeeeeeeeennneeeeeeeteeeeeeeneeeeeeeeeees 115 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH 7 7 Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Pagemondee 6 1 5 4 3 Reproducibility of the sampling systems ccceeeeeeeeeeneeeeeeeeeteteeeeeeeeeeeeees 122 6 1 ee CAINS AUION occas eceess cates iise e Ee aea aa AEE E EANA NEEE 127 6 1 54 5 CIOS aS N SII VILY hasiaci aaan 129 6 1 5 4 6 Averaging SSC ces cs sencgevececcatvauslncancan tne sceasieedaacnesateeyaMeaaaeeinaectenntansutiessSaacseress 132 6 1 5 4 7 Constancy of sample
154. al ibration port shall not exceed the requirements of Table 2 of Standard VDI 4202 Part 1 Sep tember 2010 A value ct at 70 to 80 of the upper limit of the certification range shall be used as reference point Note This point is not relevant for particulate measuring devices 6 2 Equipment Not applicable 6 3 Performance of test Not applicable 6 4 Evaluation Not applicable 6 5 Assessment Not applicable Minimum requirement fulfilled 6 6 Detailed representation of the test results Not applicable 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page titer 422 6 1 5 3 16 Converter efficiency In the case of measuring systems with a converter the efficiency of the converter shall be at least 98 Note This point is not relevant for particulate measuring devices 6 2 Equipment Not applicable 6 3 Performance of test Not applicable 6 4 Evaluation Not applicable 6 5 Assessment Not applicable Minimum requirement fulfilled 6 6 Detailed representation of the test results Not applicable 740300_2011_936_21209885B_eng doc aT T V Rheinland Energie und Umwelt GmbH A TUVR
155. al stiff ness and then calibrated At the start and end of each batch of filters a 50 and 200 mg check weight were weighed In line with the recommendations of the UK PM Equivalence Report filters were weighed relative to a 100 mg check weight and not a tare filter as the latter was shown to lose mass over time Four filters were weighed between check weights as the balance drift over time had been shown to be small 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung N TUVRheinland Genau Richtig Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 21501424 The Check weight Mass CM of the filter was calculated for each weighing session using E A 1 below CM eee E A1 Where Mcheck bef Mass of check weight weighed immediately prior to sample filter Mcheck att Mass of check weight weighed immediately after sample filter The Relative Mass RM of the filter was calculated for each weighing session using E A 2 below RM 1 jue CM E A 2 Where Miter Mass of sample filter Particulate Mass PM is calculated using the following equation in accordance with EN14907 PM Plas ERM inn Rian ey E A3 2 2 Where Pre1 denotes weighing session 1 prior to sampling Pre2 denotes weig
156. altung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 106 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Table 18 Sensitivity drift SN 20006 amp SN 20107 Date SN 20006 SN 20107 Measured Deviation Deviation Measured Deviation Deviation value form previ form start value form previ form start ous value value ous value value Ko Ko CS ee ae ee Ec ae 05 03 2010 149292 07 07 17098 0 09 29 __ 27 01 2011 149848 01 03 f 174129 08 09 12 05 2011 149126 0 5 08 f 172017 12 03 19 07 2011 151065 13 05 174066 12 09 26 09 2011 149814 08 03 173308 04 04 measured on 05 02 2010 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 107 of4aa Reference point drift SN 20006 t Dev K0 value permissible dev Deviation from previous value Figure 32 Drift of the measured value SN 20006 measured component PM 19 Refere
157. alve cannot be fully shuffled off onto the AMS itself since a prompt repair was not possible due to communication problems Minimum requirement fulfilled yes 6 6 Detailed representation of the test results Table 10 Determination of availability without test related outages Device 1 SN 20008 Device 2 SN 20107 Operating time od 325 291 Maintenance Actual operating time Availability Table 11 Determination of availability including test related outages fF Device 1 SN 20008 Device 2 SN 20107 Operating time od 325 291 Actual operating time d 288 268 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH w Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 83 01422 6 1 5 2 9 Instrument software The version of the instrument software to be tested shall be displayed during switch on of the measuring system The test institute shall be informed on changes in the instrument soft ware which have influence on the performance of the measuring system 6 2 Equipment Not required for this minimum requirement 6 3 Performance of test It was tested if the instrument software can be displayed at the instrument The manufactur er
158. an body see module 5 3 1 this test point is not relevant for particulate measuring devices Reference is made to module 5 4 10 740300_2011_936_21209885B_eng doc a s T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 114 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 1 5 4 1 General Test for particulate measuring units according to the minimum requirement stated in Table 5 of Standard VDI 4202 Part 1 Furthermore the particle mass concentration shall be related to a defined volume The rela tion to volume with respect to pressure and temperature shall be comprehensively described 6 2 Equipment Not necessary for this minimum requirement 6 3 Performance of test The test took place according to the minimum requirement stated in Table 5 of Standard VDI 4202 Part 1 It was tested if the measured particulate mass concentrations are referred to a defined vol ume 6 4 Evaluation The test took place according to the minimum requirement stated in Table 5 of Standard VDI 4202 Part 1 September 2010 The measuring unit TEOM 1405 F Ambient Particle Monitor is a gravimetric measuring de vice which determines the mass depotest sited on a filter via oscillating micro weighing The determined mass
159. and Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 f 422 Report No 936 21209885 B Page 336 Figure 3 American PM o sampling inlet Original style p n 57 000596 0001 for TEOM 1405 F Ambient Particulate Monitor 4 Flow splitter t Bypass tube t 1 2 inch sample tube nut Sample tube aam Figure 4 Flow splitter 740300_2011_936_21209885B_eng doc n TUV Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 34 of 422 company Thermo Fisher Scientific for the component PM10 g Report No 936 21209885 B Figure 5 Measuring device TEOM 1405 F Ambient Particulate Monitor Figure 6 Measuring device TEOM 1405 F Ambient Particulate Monitor 1 system from left in measuring station 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B A TUVRheinland Precisely Right Page 35 of 422
160. and Canadian safety standards UL Standard 61010 1 2004 2nd Edition CAN CSA C22 2 No 1010 1 2004 2nd Edition Thermo Fisher Scientific certifies that this product operates in compliance with the EC Directive 89 336 EEC in reference to electrical emissions and immunity Specifically the equipment meets the requirements of EN 61326 1 1998 for Immunity and Emissions In addition the hardware has been tested for personal or fire safety hazards in accordance with EN61010 1 2001 Safety in fulfillment of EC Directive 73 23 EEC This product is required to comply with the European Union s Waste Electrical amp Electronic Equipment WEEE Directive 2002 96 EC It is marked with the WEEE symbol Thermo Fisher Scientific has contracted with one or more recycling disposal companies in each EU Member State and this product should be disposed of or recycled through them Further information on Thermo Fisher Scientific s compliance with these Directives the recyclers in your country and information on Thermo Fisher Scientific products which may assist the detection of substances subject to the RoHS Directive are available at www thermo com WEEEROHS Operatine Guipe TEOM1405 F VIII Preface Service Information Section Revision List VIII Operatine Guine TEOM 1405 F When you purchase Thermo Fisher Scientific products you can depend on quality products and expert service We know that your product s performance is critical to your
161. and is 1 month Page 73 74 75 76 77 78 79 80 TUV Rheinland Energie und Umwelt GmbH w Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Specification Test result 5 2 8 Availability Minimum 95 The availability was 94 5 for SN 20006 98 6 for SN 20107 without outages due to test conditions or 88 6 for SN 20006 and 92 1 for SN 20107 including outages due to test conditions The high amount of downtime days 15 d for SN 20006 caused by the leak switching valve cannot be fully shuffled off onto the AMS itself since a prompt repair was not possible due to communication problems 5 2 9 Instrument soft The version of the instrument The version of the instrument soft ware software to be tested shall be ware is shown on the display The displayed during switch on of test institute is informed on changes the measuring system The test in the instrument software institute shall be informed on changes in the instrument software which have influence on the performance of the measuring system Page 21 of 422 5 3 Requirements on measuring systems for gaseous air pollutants 5 3 1 General Minimum requirement accord The test was done based on the min i
162. ange All sin gle values for the candidates and the reference device separated according to test site can be taken from annex 5 of the appendix Table 19 Results of the linear regression analysis of the measurements with both candidates SN 20006 and SN 20107 at the four test sites SN 20006 No of paired Slope m Ordinate R values N intercept b Teddington W 66 0 954 1 401 0 99 Teddington S 42 1 057 0 952 0 90 Cologne W 74 0 984 0 598 0 99 Bornheim S 55 1 095 1 504 0 93 SN 20107 No of paired Slope m Ordinate R values N intercept b Teddington W 45 0 928 0 299 0 98 Teddington S 57 1 034 1 398 0 93 Cologne W 74 0 997 1 127 0 98 Bornheim S 54 1 060 0 032 0 91 Table 20 Results of the linear regression analysis of the measurements with both candidates SN 20006 and SN 20107 total Device No of paired Slope m Ordinate R values N intercept b SN 20006 237 0 981 0 160 0 97 SN 20107 230 0 986 1 148 0 97 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH F Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 117 of422 Reference vs SN 20006 Teddington Winter
163. ant Ko no con centration values could be simulated an assessment in the range B was not possible for this reason 6 5 Assessment The permitted surrounding temperature at the test site of the measuring device pursuant to the manufacturer is 8 C to 25 C When observing the values output by the device a maxi mum influence of the surrounding temperature on the zero point of 2 3 g m in the range 8 C to 25 C could be detected At reference point no deviation gt 0 4 to the default value at 20 C could be observed Minimum requirement fulfilled yes 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung TS l Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page aa onde 6 6 Detailed representation of the test results Table 13 Dependence of the zero point on the surrounding temperature deviation in ug m average for 3 measurements Temperature Deviation End temperature SN 20006 SN 20107 a S E E Oe t o f o g Cao s o o Os o o o Table 14 Dependence of sensitivity calibration constant Ko on the surrounding temperature deviation in average for 3 measurements Temperature Deviations SN 20006 SN 20107 Start temperature End temperature C
164. ark Test site PM2 5 PM2 5 PM10 PM10 PM2 5 PM10 PM10 PM10 yg m ug m yg m yg m ug m ug m 211 326201 CY 176 191 f Cologne 212 3 27 2011 24 6 24 8 69 5 34 8 36 7 Winter 213 3 28 2011 20 5 20 7 64 2 31 3 32 7 214 3 29 2011 44 7 44 2 67 8 64 3 66 5 215 3 30 2011 15 6 15 6 65 8 23 8 24 5 216 3 31 2011 6 0 5 1 56 2 9 7 10 6 217 4 1 2011 8 5 7 7 61 7 12 7 12 1 218 4 2 2011 32 5 31 1 219 4 3 2011 14 6 13 7 63 6 20 8 20 1 220 4 4 2011 8 8 9 0 51 6 16 7 17 6 221 4 5 2011 11 0 11 4 58 7 18 8 19 8 222 4 6 2011 13 0 12 9 54 6 23 9 25 2 223 4 7 2011 13 7 13 1 56 7 23 7 24 8 224 4 8 2011 19 0 19 8 55 7 Inlet gt Zero filter 225 4 9 2011 Zero filter 226 4 10 2011 11 1 11 8 50 1 Zero filter 227 4 11 2011 15 2 15 1 48 2 32 7 33 6 228 4 12 2011 9 0 8 2 49 0 17 8 20 2 229 4 13 2011 12 5 12 2 51 9 25 3 26 9 230 4 14 2011 19 6 19 4 61 5 33 2 35 0 231 4 15 2011 13 3 11 4 38 8 27 0 26 5 232 4 16 2011 34 3 32 8 233 4 17 2011 21 8 21 2 234 4 18 2011 17 0 17 2 64 6 28 3 30 2 235 4 19 2011 17 5 17 9 58 0 33 0 34 4 236 4 20 2011 20 0 20 8 59 8 37 0 38 4 237 4 21 2011 34 5 36 7 238 4 22 2011 30 2 31 1 239 4 23 2011 40 8 42 6 240 4 24 2011 31 1 33 1 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH TUVRheinland 8 Luftreinhaltung z Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particul
165. artment behind the water trap filter Figure 2 23 Place the 1405 unit into the enclosure install the other end of the 5m tubing that is connected to the bulkhead into the quick connect elbow fitting for the pump connection on the back of the 1405 unit Figure 2 21 THERMO FISHER SCIENTIFIC Figure 2 24 left Sample connections inside enclosure Figure 2 25 right Sample connections on top of Sample tube Bypass tubing THERMO FISHER SCIENTIFIC the enclosure Section 2 SETUP AND INSTALLATION 7 Select a location on the pump tubing to install the vacuum gauge It should allow the gauge to be easily monitored Thermo Scientific suggests a location about half a meter from where the tubing is installed in the pump connection on the back of the unit Cut the tubing and install the two ends into the quick connect fittings on the vacuum gauge 8 From the 10m length of tubing for the bypass line cut a piece of tubing long enough to reach from the water trap filter to the bypass filter on the back of the 1405 unit Figure 2 21 and 2 23 Install the tubing into the quick connect fittings on the water trap filter and bypass filter Note The bypass tubing will be connected to the bypass connection on the flow splitter and to the water trap when you assemble and install the sample inlet on top of the enclosure later in this section A 9 Ensure that the sample tube is properly installed in the flow splitter refer
166. at the site This value cannot be edited and will be correct only when the ambient temperature humidity sensor is properly installed THERMO FISHER SCIENTIFIC Section 4 SCREENS AND SETTINGS Flows Screen The Flows screen Figure 4 11 offers access to the flow rates and flow controls of the unit Figure 4 11 Flows screen TEOM 1405 F In iruenent Conditigng Flows ENTIFIC Back ai Tabia Mere sialur m CEG 1a Select the Flow Rates button to view or adjust the instrument s flow rates Select the Flow Control button to view or adjust the units standard temperature and pressure settings or select active or passive flow control The TEOM 1405 Monitor uses mass flow controllers to ensure a constant and precise flow through the instrument The mass flow controllers use the actual active volumetric flow control setting or average passive volumetric flow control setting temperature and pressure values to regulate the volumetric flow through the system The active volumetric flow control setting directs the unit to use the actual ambient temperature and pressure to regulate the volumetric flow through the system The passive volumetric flow control setting directs the unit to use the average temperature and pressure values to regulate the volumetric flow through the system Refer to the following sections for information on setting flow rates and flow controls THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 4 13
167. ate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 183 of 422 Annex 5 Measured values from field test sites related to actual conditions Page 9 of 22 Manufacturer Thermo Fisher Scientific Suspended particulate matter PM10 Type of instrument TEOM 1405 F Measured values in yg m ACT Serial No SN 20006 amp SN 20107 No Date Ref 1 Ref 2 Ref 1 Ref 2 Ratio SN 20006 SN 20107 Remark Test site PM2 5 PM2 5 PM10 PM10 PM2 5 PM10 PM10 PM10 ug m ug m yg m ug m ug m ug m 241 4 25 2011 19 6 20 7 73 6 30 2 32 1 Cologne 242 4 26 2011 17 0 17 6 55 7 33 0 38 9 Winter 243 4 27 2011 46 3 48 4 No ref measurement PM2 5 244 4 28 2011 16 2 17 8 60 8 31 2 32 6 245 4 29 2011 19 0 19 3 72 0 30 2 29 8 246 4 30 2011 12 9 13 3 61 0 22 4 23 8 247 5 1 2011 6 7 7 0 52 9 14 1 15 4 248 5 2 2011 9 3 9 2 59 8 17 1 17 7 249 5 3 2011 9 0 9 3 59 2 16 8 18 0 250 5 4 2011 11 4 11 5 56 1 21 9 21 8 251 5 5 2011 21 4 22 1 PM2 5 Grubbs outlier 252 5 6 2011 13 7 13 6 44 2 29 0 29 7 253 5 7 2011 19 1 17 6 39 2 42 0 43 9 254 5 8 2011 12 3 12 2 53 0 21 8 22 7 255 7 25 2011 12 1 11 2 17 8 17 8 65 4 20 3 19 0 Bornheim 256 7 26 2011 11 8 11 8 19 6 19 1 61 2 20 2 22 5 Summer 257 7 27 2011 14 3 13 7 21 5 20 9 65 9 22 5 23 7 258 7 28 2011 17 5 19 0 26 5 25 2 70 6 29 3 26 7 259 7 29 2011 10 2 7 9 16 8 16 6 54 2 20 0 18 8 260 7 30 2011 11 2 11 4 261 7 31 2011 9 8 9 5 13
168. ated on the TEOM filter the device can calculate the mass concentration in near real time In addition the TEOM 1405 F monitor is equipped with the FDMS System The FDMS system is composed of the following components e air chiller filter dryer and a switching valve that is used to direct the sample flows through system The FDMS Filter Dynamics Measurement System provides a representative determination of the particulate matter PM mass concentration as it exists in the ambient air The FDMS unit automatically generates mass concentration measurements ug m that account for both nonvolatile and volatile PM components Operatine Guine TEOM 1405 F 1 3 Section 1 INTRODUCTION Overview of Manual This manual describes the installation and operation of the TEOM 1405 F 1 4 Operatine Guine TEOM 1405 F Monitor Follow the setup instructions contained in Section 2 and 3 before attempting to operate the unit This manual is divided into five sections Sections 1 and 2 explain the system s hardware while later sections describe the system s software and the setup and operation of the monitor The following list provides an overview of the topics handled in each section of the manual Section 1 Introduction This section provides an overview of the TEOM 1405 Monitor as well as the theory of operation of the instrument s mass transducer Section 2 Setup and Installation This section describes how to set up and install
169. ature range from 20 C to 50 C accuracy better than 1 C e Adjustable isolating transformer e Zero filter for external zero point check e Ko check kit The measured values were recorded in the devices The stored measured values were read out via Data download via USB Section 6 describes the laboratory tests and the results 740300_2011_936_21209885B_eng doc a s T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 48 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 4 3 Field test The field test was carried out with two identical systems with the serial numbers Device 1 SN 20006 Device 2 SN 20107 The following test program was specified for the field test e Determination of the comparability of the candidates according to the Guide Demon stration of Equivalence of Ambient Air Monitoring Methods e Determination of the comparability of the candidates and the reference methods ac cording to the Guide Demonstration of Equivalence of Ambient Air Monitoring Meth ods Sampling flow stability check Determination of the calibration ability and set up of analysis function Determination of field reproducibility Determination of drift behaviour of zero point and sensitivity Inves
170. ban background summer 3 Cologne parking 01 2011 05 2011 Urban background lot winter 4 Bornheim motor 07 2011 10 2011 Rural structure traffic way parking lot influence summer 740300_2011_936_21209885B_eng doc WT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 50 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Figure 16 to Figure 19 show the course of time of the PM o concentrations at the field test sites which were recorded with the reference measuring device 100 90 oO 80 D 70 s _ 60 50 i 40 a Ss 30 c e o 20 10 0 Q Q Q Q oO oO oO oO oO oO oO oO oO O t t p oO oO oO O O p O oO N N N N N N N N N N N N N R Z R Z A g 2L ss A o oO N N N kaa N N N Figure 16 Course of time of the PM concentrations Reference at the test site Teddington winter 100 Conc PM10 Ref in pg m a oO 10 0 oO oO oO i oO oO oO oO oO oO oO oO oO N N N N N N N N N N SS s s tied S i ES N SN N vy c Ke ie 1O N Q N lo N N N
171. bes were char acterized by the following dimension e Height cabinet roof 2 50 m e Height of the sampling for the Candidate 1 10 m 0 51 m above the cabinet roof e Reference device 3 61 3 01 m above ground e Height of the wind vane 4 5 m above ground The following Table 5 contains therefore not only an overview on the most important meteor ological data of the four test sites but also an overview on the PM conditions during the test Refer to section 5 and 6 for detailed results 740300_2011_936_21209885B_eng doc A TUVRheinland Precisely Right Page 54 of 422 Table 5 Ambient conditions at the field test sites expressed as daily averages TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Teddington Uk Teddington UK Cologne Bornheim winter summer parking lot motorway parking winter lot summer No of paired values 67 59 83 59 reference Ratio PM2 5 PM10 Range 38 8 90 6 30 2 92 3 38 8 93 5 24 1 70 6 Average 67 7 59 2 67 7 54 1 Ambient temperature C Range 3 7 9 8 6 7 23 2 3 8 22 1 13 2 24 5 Average 3 1 15 4 8 8 17 9 Ambient pressure kPa Range 97 9 103 7 99 7 102 6 99 2 103 1 99 6 101 8 Ave
172. between meas urement and functional check and or calibration shall be pos sible telemetrically by computer control or manual intervention If possible 3 months minimum 2 weeks 740300_2011_936_21209885B_eng doc Differences between the instrument design and the descriptions given in the manual could not be detected The assessment of the measuring device in the range of the relevant limit values is possible A measuring range of 0 1 000 g m is set by default Other measuring ranges up to a maximum of 0 1 000 000 g m are possible The measuring range value of the measuring device is higher than the respective upper limit of the certifica tion range Negative measuring signals are dis played directly and are output correct ly via the respective measured value outputs by the measuring system All instrument parameters are pro tected against loss through buffering After the power supply has returned the measuring device goes back into a failure free operational condition and continues independently the measuring operation after achieving the instrument status fully operation al The measuring devices can be exten sively monitored and controlled by an external PC via modem or router Generally all necessary operations for functional check can be monitored di rectly at the device or via telemetric remote control The maintenance interval is defined by necessary maintenance proce dures
173. button to display the Service screen then select the Maintenance button to display the Maintenance screen Figure 5 3 2 Select the Clean the Switching Valve button to start the Valve Cleaning Wizard Figure 5 43 Select the Next gt button to begin the procedure Figure 5 43 Valve Cleaning Wizard Welcome screen Welcome to the Valve Cleaning Wizard This wizard hos you clean the switching vahe on the TEGA Dichol sunbient Partioulate Monitar The insirumemi will be put in Setup mode tor caraiion T continue prese Next 5 34 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 3 The Remove Front Cover screen will display Remove the front cover from the unit and locate the switching valve fittings and tubing connections Figure 5 44 4 Remove the tubing from the top quick connect fitting on the switching valve Select the Next gt button Figure 5 44 Interior of 1405 tower Switching valve 1 fas Tubing bi Fitting THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 35 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 5 The Remove Valve screen will display Using a 1 inch wrench or an adjustable wrench completely loosen the Swagelok fitting on the top of the switching valve and the Swagelok fitting on the bottom of the switching valve Figures 5 44 and 5 45 Figure 5 45 Removing a valve Swagelok fitting j
174. cale Select the Analog Input 1 Analog Input 2 Analog Input 3 or Analog Input 4 buttons to convert the analog input to a desired scale Figure 4 15 Analog Inputs screen TEOM 1405 F x Back ab Siting Heres etates a CHORE 1s THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 4 19 Section 4 SCREENS AND SETTINGS FDMS Module Screen Figure 4 16 FDMS Module Screen 4 20 Operatine Guine TEOM 1405 F The FDMS Module screen Figure 4 16 allows users to access the values used by the Filter Dynamics Measurement System to generate the mass concentration measurements TEOM 1405 F Ingtrument Conditiong gt FOMS Module SCIENTIFIC Base ME SVE ppa Aateranice MC 19 55 jie 30 minute base ME FiS pee 30 minute eetereer ME iia ppw Dryer temperat itir OC Dryer dgw poini 11 51 T Deyer phatio bumii izid Gurren valve poaitiom The FDMS Module screen contains the following information Base MC This field contains the mass concentration value recorded by the TEOM filter while the FDMS system draws dried ambient air base flow through the sample flow lines This value is a rolling 1 hour average updated every 6 minutes Reference MC This field contains the mass concentration value recorded by the TEOM filter while the FDMS system draws dried filtered and cooled ambient air reference flow through the sample flow lines This value is a rolling 1 hour average updated every 6 minutes 30
175. ce 8 192 0x00001000 Head 1 4 096 0x00000800 Head 0 2 048 0x00000400 MFC 1 Device 1 024 0x00000200 MFC 0 Device 512 0x000001 00 System Bus 256 0x00000080 Vacuum Pressure 128 Ambient Vac lt 0 1 atm 0x00000040 Case or Cap Heater 64 gt 2 deviation 0x00000020 FDMS Valve 32 0x00000010 Bypass Flow 16 gt 10 deviation 0x00000008 Ambient RH amp Temp Sensor 8 Ambient RH amp temp sensor disconnected 0x00000004 Database 4 Unable to log to the database 0x00000002 Enclosure Temp 2 temperature exceeds 60 C 0x00000001 Power Failure 1 Operating Guide TEOM 1405 F Thermo Fisher Scientific Converting Decimal Hexadecimal Numbers Table A 2 Hex digits and status codes THERMO FISHER SCIENTIFIC APPENDIX A TROUBLESHOOTING The easiest way to convert the decimal numbers reported by the unit is to use the calculator on a Windows based PC To convert a decimal status code to a hexadecimal number 1 Open the Windows calculator it s located in Accessories under All Programs in the Start menu 2 Select View then Scientific to open the scientific style calculator 3 Select Dec to choose the decimal calculator option and then enter the decimal status number into the calculator 4 Select Hex to choose the hexadecimal calculator option The new number displayed in the calculator is the hexadecimal number you will use to decipher the status code list Note To convert a hexadecimal to a decimal number select
176. change the operation mode in or der to perform a filter change High Lock Mode In this mode the user can only see the TEOM Data Because an installation of the measuring device outdoors is not possible an additional pro tection is granted by installing it at test sites where no unauthorised people can go to e g locked measuring cabinet 6 4 Evaluation Unintended adjustment of instrument parameters is avoided by the password protection The adjustment of sensors and a change of the parameters can only be done via several key se quences Moreover there is an additional protection against unauthorized intervention by the installation in a locked measurement cabinet 6 5 Assessment The AMS is protected against unauthorized and unintended adjustment In addition the AMS shall be locked in a measuring cabinet Minimum requirement fulfilled yes 6 6 Detailed representation of the test results Not required for this minimum requirement 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH w Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 104a 6 1 4 1 7 Data output The output signals shall be provided digitally e g RS 232 and or as analogue signals e g 4
177. chotFOMS Serial men 1406430109505 IP Address 10 210 96 145 States Ative Cormaands Domnined Dut ls Aes Dain Decenboad folder Location C Frogran Piesi TharnolaPorti Last domsload Artamated domsloads Cased ID Rewete Interface Deor gt Upgrade hutrurar Frrrasre I Cored sop an biad ba Lest Downhaad or Saated Date and Tine Meat dosmboad wil start with dete alter 31 Jen 2007 06 2620 ex Note Data will not be collected during the upload procedure and the instrument will be restarted a THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 4 37 Section 4 SCREENS AND SETTINGS 6 The Thermo 1405 Installer Wizard screen will display Figure 4 31 Select the Next gt button Figure 4 31 FRE aT bd Thermo 1405 Installer screen Welcome to the Thermo 1405 Installer 1405 This wizard will guide you through the process of installing Installer new software on your Thermo instrument All configuration data will be restored All other stored data will be erased Note This application calls 7 Zip an archive utility licensed under the GNU LGPL The source code for 7 Zip can be SCIENTIFIC downloaded from www 7 zip org Thermo Hectron Corporation 7 The Software File screen will display Select the Browse button to locate and select the file from the CD or the file that was downloaded from the company website For firmware updates using ePort the file is named etx dichotFDMS_ePort
178. cientific for the component PM10 Report No 936 21209885 B Page 49 er aee The impaction plates of the PM 9 sampling inlets of the reference devices were cleaned ap prox every 2 weeks and lubricated with silicone grease in order to guarantee a safe separa tion and secretion of the particulate The PM sampling inlets of the candidates were cleaned approx every 4 weeks In general the sampling inlet shall be cleaned according to the manufacturer s instructions while taking into account the local suspended particulate mat ter concentrations The flow rate was tested on each candidate and each reference device prior to and after each change of location with a dry gas meter respectively a mass flow meter which could be connected to the air inlet of the systems via a hose assembly Measurement test sites and test site of the measuring devices The measuring devices have been installed in the field test in such a way that only the sam pling inlets and the flow splitter are located above the roof of the measurement cabinet The central units of both candidate systems as well as the central units of the reference systems LVS3 were installed inside the climate controlled measurement cabinet The field test was carried out at the following test sites Table 4 Field test sites No Measuring test Period Characterization site 1 Teddington UK 12 2009 03 2010 Urban background winter 2 Teddington UK 04 2010 07 2010 Ur
179. ck of fit The analytical function describing the relationship between the output signal and the value of the air quality characteristic shall be linear The linearity is considered as secured when the deviation of the group averages of the measured values of the calibration function in the certification range meet the specifications stated in Table 2 of Standard VDI 4202 Part 1 September 2010 For other certification ranges the deviation of the group average of the measured values of the calibration function shall not exceed 5 of the upper limit of the respective certification range Note According to the decision of the competent German body see module 5 3 1 this test point is not relevant for particulate measuring devices For particulate measuring devices for PM o this test shall be performed according to mini mum requirement 5 4 2 Equivalency of the sampling system 6 2 Equipment See module 5 4 2 PMio 6 3 Performance of test For particulate measuring devices for PM o this test shall be performed according to mini mum requirement 5 4 2 Equivalency of the sampling system 6 4 Evaluation See module 5 4 2 PMio 6 5 Assessment For particulate measuring devices for PM o this test shall be performed according to mini mum requirement 5 4 2 Equivalency of the sampling system Minimum requirement fulfilled 6 6 Detailed representation of the test results See module 5 4 2 PM10 740300_201
180. continue on the instrument SC LEN TEP TC Thermo Hectron Corporation i Cancel Note The instrument will restart automatically after the firmware is uploaded A 4 40 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC THERMO FISHER SCIENTIFIC Section 4 SCREENS AND SETTINGS To install new firmware using a USB Flash Drive Note In order to update the instrument firmware via the USB port Current instrument firmware version 1 51 or later is required to be installed on the monitor Contact Thermo Fisher Scientific for further information if an earlier version is installed If updating the firmware using ePort this limitation does not apply a To perform a firmware upgrade using the USB port first copy the firmware upgrade files to the root folder of a standard USB flash drive The required files are etx_singleFDMS tar etx_singleFDMS kernel etx_singleFDMS_USB rc 1 Record all important configuration information from the instrument This includes KO values instrument serial number data storage settings etc 2 Turn off the instrument 3 Open the front panel that contains the instrument display 4 Compare the inside of the instrument to the following figure If the instrument interface board matches the figure proceed to step 4 If the unit is an updated version close the front panel and continue with step 6 An updated interface board includes the text Thermo Fisher Scientific along the front e
181. ct a qualified electrician if there is doubt as to whether the power service for the instrument is adequate a Operatine Guine TEOM 1405 F 2 15 Section 2 SETUP AND INSTALLATION Figure 2 17 Power switch 2 16 Operatine Guine TEOM 1405 F 3 Press the POWER switch on the front panel of the control unit Figure 2 17 The unit will begin its startup routine After a few moments the Title screen will appear on the control unit s display and then the TEOM Data Main screen Refer to Sections 3 and 4 for information on the instrument s software screens 4 Plug the pump into an appropriate power source to draw a sample stream through the system Power switch The TEOM Data screen will show a warning message Section 4 because the flow rates and temperatures are outside of tolerance ranges The warning may remain active during the first 30 minutes after the power switch is pressed while the monitor warms up The status warning icon automatically disappears after all flow rates and temperatures reach tolerance ranges The monitor waits until the flow rates and temperatures stabilize within a narrow range before starting data collection This ensures the validity of all data points computed by the system Note Upon initial instrument start up the values in the mass concentration fields are the running averages that are accumulated until a 1 hour time period has passed The values are visible to provide the user with an in
182. ction 5 MAINTENANCE AND CALIBRATION PROCEDURES 3 Locate the analog outputs jumpers and test points located at the front of the board and ensure that the jumper for the channel you are calibrating is set to the correct voltage limit Figures 5 70 and 5 71 Note Set the jumper on the right and middle posts pictured for 0 1 VDC and over the middle and left posts for 0 5 VDC a Figure 5 70 Front of interface board with jumpers and testpoints highlighted J6 T vok Jo s Volts E324 Jumper Test point Label Ground test point Close up of aoe cade D 7h SUTE j JUMPERS f Setting guide 1 T i e r voit _ 5 Volts S24 REA JP304 JP3 5 DAs DAS t THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 57 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 4 In the 1405 Data screen select the Service button to display the Service screen then select the Calibration button to display the Calibration screen Figure 5 48 5 Select the Analog Output Calibration button to start the Analog Output Calibration Wizard Figure 5 72 Select the Next gt button to begin the procedure Figure 5 72 Welcome to the Analog Output Welcome to the Analog Calibration Wizard screen Output Calibration Wizard This wizard eins you parton analog ouipul calbration on ihe TEOM Bicheat Ambient Particulate Monitor To continue press Next 6 The Select Channel to Calibrate screen will display F
183. ctive candidate 1 X th 1 0 95 Sxo where S o aor te X i 1 n Reference value Bo 2 ug m 740300_2011_936_21209885B_eng doc A TUVRheinland Precisely Right TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 88 of 422 company Thermo Fisher Scientific for the component PM10 6 5 Assessment Report No 936 21209885 B The detection limit was determined from investigations on 0 82 ug m for device 1 SN 20006 and 0 82 yg m for device 2 SN 20107 Minimum requirement fulfilled yes 6 6 Detailed representation of the test results Table 12 Detection limit PM1 Device SN 20006 Device SN 20107 Amount of values n 15 15 Average of the zero values x g m 0 96 1 28 Standard deviation of the values s g m 0 38 0 38 Student Factor th 1 0 95 2 14 2 14 Detection limit X g m 0 82 0 82 Single values from the determination of the detection limit can be looked up in annex 1 in the annex 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH w Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component
184. culate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 163101422 The resulting values of Yi cor may then be used to calculate the following new terms by linear regression Vicor C dx and us s Views u x c d 1 x f xru b u a a n 2 with u b uncertainty of the original slope b the value of which has been used to obtain Yicorr and with u a uncertainty of the original intercept a the value of which has been used to obtain Yi corr Algorithms for the calculation of intercepts as well as slopes and their variances by orthogo nal regression are described in detail in annex B of 4 RSS is determined analogue to the calculation in module 9 5 2 2 9 5 6 The values for Uc scor are used for the calculation of the combined relative uncertainty of the candidate systems after correction according to the following equation us s corr y W oMcor y Ty For the corrected data set uncertainty is calculated at the daily limit value Wecmcorr by taking as yi the concentration at the limit value The expanded relative uncertainty Wem corr is calculated according to the following equation Wom corr k i W cmcorr In practice k 2 for large number of available experimental results The highest resulting uncertainty Wcm is compared and assessed with the requirements on data quality of ambient air measurements accordin
185. d 5 46 Operatine Guine TEOM 1405 F 5 The Connect Flow Audit Device screen will display Attach a flow meter to the appropriate flow channel a To audit the main flow channel remove the inlet and attach the 1 1 4 inch flow adapter meter to the top of the flow splitter Figure 5 56 Disconnect the bypass line from the side of the flow splitter don t let it fall to the ground and cap the bypass fitting with the 3 8 inch Swagelok cap provided with the system Figure 5 57 Flow meter adapter Bypass cap THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES b To audit the bypass flow channel remove the bypass line from the flow splitter and connect the 3 8 inch flow adapter to the green tubing of the bypass line Figure 5 58 Connect the flow meter adapter to the flow audit adapter When the flow meter is attached select the Next gt button Figure 5 58 Bypass connection Bypass line THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 47 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 6 The Measure Flow screen will display Allow the flow to stabilize When the flow is stable press the flow button and enter the reading from the flow device Select the Next gt button 7 The Flow Audit Results screen will display the difference between the flow rate of the instrument and the flow rate on the measurement device Figure 5 59 If the difference is less than 10 percent yo
186. data 130 120 110 100 Measured values 90 Regression line 80 EE y x 70 60 50 Candidate 2 ug m 40 30 20 10 0 10 20 30 40 50 60 70 80 90 100 110 120 130 Candidate 1 ug m Figure 56 Results of the parallel measurements with the candidates SN 20006 SN 20107 measured component PM o test site Teddington Winter 1405 F SN20006 SN20107 Teddington Summer Raw data 130 120 110 100 Measured values 90 Regression line 80 bnaaai y x 70 60 50 Candidate 2 ug m 40 30 20 10 0 10 20 30 40 50 60 70 80 90 100 110 120 130 Candidate 1 ug m Figure 57 Results of the parallel measurements with the candidates SN 20006 SN 20107 measured component PM test site Teddington Summer 740300_2011_936_21209885B_eng doc a TUV Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 146 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 1405 F SN20006 SN20107 Cologne Winter Raw data 130 120 110 100 Measured values 90 Regression line 80 mahaa y
187. determined Annual limit value PM 40 ug m 10 of ALV 4 ug m Further investigations were made to determine whether the comparability of the candidate systems with the reference method according to Guide Demonstration of Equivalence of Ambient Air Monitoring Methods 4 is also given at days of more than 70 relative humidi ty 740300_2011_936_21209885B_eng doc a s T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 130 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 5 Assessment No interference caused by moisture in the sample gt 1 9 ug m deviation from nominal value for PM could be observed During the field test no negative influence on the measured values could be noted at chang ing relative humidities The comparability of the candidates with the reference method ac cording to Guide Demonstration of Equivalence of Ambient Air Monitoring Methods 4 also is given for the days with a relative humidity gt 70 Minimum requirement fulfilled yes 6 6 Detailed representation of the test results Table 23 shows a summarizing presentation Table 23 Deviation between reference measurement and candidates at the days with a rela tive humidity gt 70 measured component PM
188. dge of the board 5 Locate the Module power Jumper on the interface board as indicated in Figure 4 34 and install a jumper across the pins One of the analog input jumpers may be temporarily used for this purpose 6 Insert the USB Flash Drive and turn on the instrument power 7 The instrument will automatically locate and install the necessary files from the USB flash drive and update the instrument firmware 8 At the end of the update process the instrument will pause for 20 seconds before a blank white screen appears Remove the USB Flash Drive The instrument will reboot automatically to complete the installation of the firmware 9 If you installed a jumper in step 4 above turn off the instrument power and remove the jumper If one of the analog input jumpers was used replace it in the original location Close the instrument front panel and turn on the instrument power Operatine Guine TEOM 1405 F 4 4 Section 4 SCREENS AND SETTINGS 10 Verify the instrument settings were retained including serial number and KO Re enter these values if necessary 11 Thermo Fisher Scientific recommends performing a calibration of the instrument temperatures pressure and flows after a firmware update Refer to Section 5 for calibration instructions Figure 4 34 Interface Board 4 42 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section5 Maintenance and Calibration Procedures P e riod i c Thermo Fisher Scientific
189. dication that the instrument is functioning after instrument power up or reset These raw values are used for internal calculations only THERMO FISHER SCIENTIFIC Section 2 SETUP AND INSTALLATION Turnin g Off the 1f the instrument needs to be turned off turn the power switch on the front nstrument of the unit to off 0 Note Wait at least 1 minute after shutdown before reapplying power to the unit The instrument may also be restarted without turning it off Restarting the To restart the instrument Instrument 1 In the Service screen Section 4 select the Instrument Control button to display the Instrument Control screen Figure 2 18 2 Select the Reboot button Figure 2 18 Instrument Control screen SElEHTIFIC THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 2 17 Section 2 SETUP AND INSTALLATION Using the Thermo Fisher Scientific offers an outdoor shelter for the 1405 unit The 0 utdoor Shelter shelter is fully climate controlled and includes space for the 1405 unit pump and accessories such as a data logger or additional monitoring devices It is available in both 120V and 240V version o I y a 2 a Figure 2 19 1405 unit in the outdoor enclosure 2 18 Operatinc Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 2 SETUP AND INSTALLATION To install the 1405 unit in an outdoor shelter 1 Before placi
190. didates SN 20006 SN 20107 test site Bornheim 100 SN 20006 vs SN 20107 All test sites Measured values 90 80 Regression line 70 Acceptance range 60 according to EN 12341 50 y x 40 30 Candidate 2 yg m 20 10 40 50 60 70 80 90 100 Candidate 1 yg m Figure 48 Result of the parallel measurements with the candidates SN 20006 SN 20107 all test sites 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B pager 127 01422 6 1 5 4 4 Calibration The systems under test shall be calibrated in the field test by comparison measurements with the reference method according to EN 12341 Here the relationship between the output sig nal and the gravimetrically determined reference concentration shall the determined as a steady function 6 2 Equipment See module 5 4 2 6 3 Performance of test For PM o The comparability of the measuring systems was demonstrated within the scope of the test ing see module 5 4 2 For the determination of the calibration and the analysis function the compl
191. doc a T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the P 136 of 422 company Thermo Fisher Scientific for the component PM10 Secor Report No 936 21209885 B PM10 20006 6 min Col W 2011 200 PM10 20006 tmoTEOMAMC_0O tmoTEOMAFilterLoad_0O 180 160 140 120 100 80 60 40 20 0 17 01 2011 16 02 2011 18 03 2011 17 04 2011 17 05 2011 16 06 2011 Figure 49 Course of time of the PM concentration ug m and the filter load Candidate SN 20006 Cologne Winter PM10 20006 6 min Col W 2011 3 3 tmoTEOMAFlowVass_0 Limit TEOM Flow 3 2 3 1 3 0 29 28 17 01 2011 16 02 2011 18 03 2011 17 04 2011 17 05 2011 16 06 2011 Figure 50 PM flow rate at candidate SN 20006 Cologne Winter 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 422 Report No 936 21209885 B Page 13r of PM10 20006 6 min Col W 2011 18 0 Total flow LimitTotal Flow
192. e Finish button to exit the wizard and return to the Calibration screen or select the lt Back button to move backward one step in the procedure Note If you want to audit the total flow rate following the calibration procedure see Figure 5 62 a Figure 5 68 Completing the Flow Calibration Completing the Flow Wizard screen Calibration Wizard To complete the calibration remove the Flew Audit Derice The inesirumeni will tee Putin Run mede when this wizard bs finished T close this wizard press Finish THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 55 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Calibrating the The Analog Output Calibration Wizard allows users to calibrate the eight Analog Outputs analog output channels to either 0 1 VDC or 0 5 VDC Note Always wear appropriate anti static devices when working with the system electronics a To calibrate the analog outputs 1 Attach an antistatic wrist strap to your wrist Attach the other end of the wrist strap to the chassis of the control unit to discharge any static electricity while working on the unit Note Always wear appropriate anti static devices when working with the system electronics a 2 Open the door to the unit Figure 5 69 and locate the interface board mounted to the bottom of the unit Figure 5 69 1405 DF unit with left door open Interface board 5 56 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Se
193. e periodically made available either on computer CD or in the online library on the company website at www thermo com aqdi The next section provides instructions on installing new firmware via ePort Refer to the following section for installing software via USB To install new firmware using ePort 1 Download the new firmware file onto a personal computer PC from the company website or locate the updated version on the software CD Note the file name 2 Ensure that the PC and the instrument ate connected to the same network using the Ethernet connection on the back of the instrument Refer to Section 3 for information on connecting the instrument to a network 3 In the System Status screen of the machine you want to update locate and record the IP address Figure 4 29 TEOM Data TEOM 1405 F System Stats Sysiem Status Operating mode Stabilizing ASz37 mode flome Veum PLD persue io zim Enchosure tempersiure Oh Instr Probection level LUinioried F address 182 188 193 129 Serial number 123458730 instrument rmeare version 0 82 Settings Service a Sahig Homa state a eean es THERMO FISHER SCIENTIFIC Section 4 SCREENS AND SETTINGS 4 Use the ePort PC software to connect to the instrument refer to Section 3 for information on connection to the instrument 5 In the ePort Main screen Figure 4 30 select Upgrade Instrument Figure 4 30 Software ePort Main screen 14054200100605 Di
194. e 124 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Table 21 Two sided 95 confidence interval Clos for the candidates SN 20006 and SN 20107 Candidate Test site No of Standard Student Confidence values deviation s factor t interval Clos a oe o 20006 20107 Teddington W 2 015 20006 20107 Teddington S 2 012 20006 20107 Cologne W 1 988 SN 20006 vs SN 20107 Teddington Winter Measured values Regression line Acceptance range according to EN 12341 y x Candidate 2 ug m O 10 20 30 40 50 60 70 80 90 100 Candidate 1 yg m Figure 44 Result of the parallel measurements with the candidates SN 20006 SN 20107 test site Teddington Winter 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B A TUVRheinland Precisely Right Page 125 of 422 SN 20006 vs SN 20107 Teddington Summer 100 90 80 70 60 50 40 Measured values Regression line Acceptance range according to EN 12341 y x 30 20 10 Candidate 2 ug m
195. e 3 29 Download Setup Wizard SA Download Setup Wizard l Welcome to the Download Setup Wizard This wizard helps you setup downloads from the instrument in easy steps 4 The Select Data screen will display Select the data to download either all data on the instrument or the data since the last download Select the Next gt button 5 The Select Location screen will display Use the Browse button to select a location for the data file downloaded by the software Select the Next gt button 6 The Download Type screen will display Select manual downloads Select the Next gt button 7 The Completing the Download Setup Wizard screen will display Select the Finish button 3 26 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 3 Basic OPERATION Setting Up for Users can set up automatic downloads for the TEOM 1405 monitor using Automatic Data THERMO FISHER SCIENTIFIC Downloads the ePort software To set up the software to automatically download data 1 Ensure that the PC and the instrument are connected to the same network using the Ethernet connection on the back of the instrument Refer to the previous section for information on connecting the instrument to a network Use the ePort PC software to connect to the instrument and display the ePort Main screen Figure 3 28 Refer to the previous sections for information on connecting to the instrument or instruments
196. e 75 Figure 76 Figure 77 Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Reference vs candidate SN 20107 measured component PM o Teddington SUMIME occ ciscshcczccccsapeieStnnesziequscdhanastt ctectacdbiseeintdtagtcbacedeadueracganets 157 Reference vs candidate SN 20006 measured component PM o Cologne CVV INGE recreire i aeea a a E A R E iEnd 157 Reference vs candidate SN 20107 measured component PM30 Cologne Winter caccccicusuasestesnsckacaveatentennicosseecaran cantvesteveadpeadeaeadtertoetavnersndstnetens 158 Reference vs candidate SN 20006 measured component PM3o Bornheim Summer 22 32 2cecceceatsansd cuts ieaptaduslactduahe inte catndsaaienSideeesaaabinacdcssectletes 158 Reference vs candidate SN 20107 measured component PM o Bornheim SUmmMer resien aae r e En A EE e tence 159 Reference vs candidate SN 20006 measured component PM3o VAISS gt 30 PHOT sranane E E EE A ENAA ERRET 159 Reference vs candidate SN 20107 measured component PM3o values S 30MM eirinn ei hoia RARER SETE EERTE 160 Stability Of standard WEIOM sacisiccadsivivncchcreseeraaasraterercemiaaniesvedheactanaradenrunanent 210 Stability of the control TINGS cesta iesas Hove tivan Hecgnohuivns mee secmaahudeaaueinceieddadadbelbasouna 212 Distribution for Emf
197. e By 40 ug m for PM10 e Sp Standard deviation from repeat determinations e n No of parallel measurements e tno95 Student factor for 95 certainty e x Measuring signal of device 1 e g SN 20006 at i concentration e Xz Measuring signal of device 2 e g SN 20107 at i concentration 6 5 Assessment The reproducibility Rp for PM was 23 during field test for the complete data set Minimum requirement fulfilled yes 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 101 of 422 6 6 Detailed representation of the test results The test results are summarized in Table 16 The graphical representation for PM is shown from Figure 55 to Figure 59 Note The determined uncertainties are applied to the reference value B for each test site Table 16 Concentration averages standard deviation uncertainty range and reproducibility in the field measured component PM Test site Amount C C Cyes t U SN 20006 SN 20107 O f Tom iom ome oe foe Teddington 46 18 8 20 0 19 4 0 26 2 013 0 53 75 Winter Teddington 49 16 4 16 4 16 4 0 49 2 010 0 98 41 Summer Bornheim 16 7 17 5 17 1 1 10 1 996 2 19 18 Summer
198. e Next gt button THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 9 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 17 The system will automatically test the newly installed TEOM filter to ensure it is firmly seated The system will display a screen with the wait time Figure 5 10 Figure 5 10 Stabilizing Wait for ineirumment lo siaidine Stabilizing screen 18 If the system is unable to obtain a stable frequency for the filter it will display a screen stating the filter needs to be re seated Figure 5 11 Otherwise the filter change is complete go to step 21 Figure 5 11 e seat Filter Re seat Filters Screen Fatera need lo be re seated after they have experienced an in tease i bemperaiure 5 10 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 19 If the filter needs to be re seated open the door to the sampler and the mass transducer and press straight down on the TEOM filter with the bottom of the filter exchange tool Figure 5 9 This ensures that the filter is properly seated Close the mass transducer and sensor unit door Select the Next gt button 20 The system will again display the waiting screen while it is testing for a stable frequency If it still cannot obtain a frequency for the filter it will prompt the user to re seat the filter a second time If it still cannot obtain a stable frequency the procedure will prompt to re
199. e TEOM 1405 F unit before running the 47 mm Filter first sample run and every time that you install a new TEOM filter into the unit To install the 47 mm filter 1 Locate the small door on the left side of the TEOM 1405 F unit Open the small filter door Figures 5 19 Figure 5 19 Filter door open Notch Locking disk 2 Turn the filter holder counterclockwise until the notches line up with the locking disk Figure 5 20 and then pull outward to remove the holder from the unit Figure 5 20 Removing the 47 mm filter Filter Blue filter cassette 5 16 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 3 Locate blue filter cassette and remove the used 47 mm filter 4 Insert a new 47 mm filter into the cassette Be sure to install the 47 mm filter into the cassette with the face of the filter paper facing the top of the cassette The top of the cassette fits nzo the bottom of the cassette Figure 5 21 Figure 5 21 7 47 mm filter cassette O Pme with filter and screen Filter Screen Bottom gt 5 Close the filter cassette Figure 5 22 Figure 5 22 Closing the filter cassette 6 Install the filter into the filter holder with the top of the cassette and filter surface facing out 7 Line up the notches with the locking disks and install the filter holder into unit Turn the holder clockwise to lock it
200. e button to display the Service screen then select the Maintenance button to display the Maintenance screen Figure 5 3 2 Select the Clean Coolers button to start the Cooler Cleaning Wizard Figure 5 36 Select the Next gt button to begin the procedure Figure 5 36 Cooler Cleaning Wizard Welcome to the Cooler Welcome screen Cleaning Wizard This wizard eins you purge the coolers pi semi yelatile particies thal have and accumulated on ihe inside Sete The instrument will be putin Setup mode for cleaning To continue press Next PIERI gt Cancel 3 The Remove Filter Cassettes screen will display Open the compartment door on the side of the unit and remove the 47 mm filter cassette and filter Refer to the Replacing the 47 mm Filters section earlier in this chapter for more information on removing the filter cassettes Select the Next gt button 5 28 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 4 The Open Unit screen will display Remove the front cover from the unit tower and locate the cooler assembly the switching valve and the dryer vacuum connection Figure 5 37 Figure 5 37 Interior of 1405 tower Cooler assembly 5 Remove the tubing from both the top and bottom quick connect fittings on the cooler Figure 5 37 Select the Next gt button THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 29 Section
201. e ee eee eee eee 3 11 Downloading Data i cnidinitncnsaianidinbnzet tteneast lated tates unnnsanchseai anionatand 3 13 Tast line e Poft a AAA S 3 14 Connecting to the Series 1403 F UNIE ssssissiisvssnscsisneevenvssvsvvevionssavesncnvbes 3 19 Finding Instruments On a Netwofk os cesessacsedecnsdsuadesotsnasatdsevessneqnetdoeanaries 3 23 Setting Up for Manual Data Downloads ss ssssssssssssssssrresrrsssrsssresreseresees 3 25 Setting Up for Automatic Data Downloads sicticssicssasessscssvedseatenssieareans 3 27 Petforming a Data Download sssini 3 29 Downloading Data To a Flash Dive ssiasirvicivcenscasnsinansenitetavatestonustetbaasees 3 31 Viewing Downloaded Data iuscrassiaceiamraisncancemciactinentaittnsiehtanaancas 3 33 User I O Connections vicccecccccssssscsscssssssscescescsscescesssesscescessssesscessesseeeeees 3 34 USER I O Pin Assignments ss sssssesssesressseseessssetsssereeesssreeesrtessrereresssrreese 3 35 Section4 Screens and SettingS csccscscscssssesssesesseeessssesessceeseseeaseessseeeaears 4 1 TROM Data Screenreaders 4 2 Operating NUS isin csinsaaniiuanilnsace snes dub naoa EENet 4 6 System Status ETECI sea vsce eracqensatns ecuenscuuusussseensveunausernaanotnnerrinuenceuaruetane 4 8 Instrument Conditions Screett cacisisssaisassessesastuatrsocseaiaesiaodvinessantevees 4 10 Ambient Conditions Sereen es ceshssuedsireqnecseaesdincanstorgsoeesesnareiGoqnrtadeigreas 4 12 Pees SORE CH risia e A A AN 4 13 Flow Rates SHOE siiis 4 14 F
202. e eeeeeeeeeeeee tees teeeeeeeteeeteeeeseeeeeeeeees 95 Dependence of sensitivity calibration constant Ko on the surrounding temperature deviation in average for 3 measurements eeeerereeeees 95 Dependence of the measured value of the mains voltage deviation in 97 Concentration averages standard deviation uncertainty range and reproducibility in the field measured component PMo ceeeeeeeeeeeeeeeeeees 101 Zero point drift SN 20006 amp SN 20107 with zero filter 00 cceeeeeeeeeeeeeees 104 Sensitivity drift SN 20006 amp SN 20107 ii cssccciccssacetesinneaeenscbncstsnseceertsianensdestaane 106 Results of the linear regression analysis of the measurements with both candidates SN 20006 and SN 20107 at the four test sites 00 0 0 116 Results of the linear regression analysis of the measurements with both candidates SN 20006 and SN 20107 total 0 eee eeeeeeeeeeeeeeeeeeeeeeees 116 Two sided 95 confidence interval Clos for the candidates SN 20006 and SN 20107 i aE E EA dondedastieedadcaa duane mune rena ntanans 124 Results of the calibration and analysis function measured component PM 127 Deviation between reference measurement and candidates at the days with a relative humidity gt 70 measured component PM3 seeseeeeeeereee 130 Comparison candidate 20006 with reference device rel humidity gt 70 all test sites measured component PMjo ccccccceccaesesesece
203. e external zero point check of the measuring system and for the check of the calibra tion constant Ko a zero filter is installed at the instrument inlet The use of this filter enables the provision of particulate free air Figure 14 Zero filter during field test 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland TSI DONS Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 P 43 of 422 Report No 936 21209885 B age 430 By means of the available shut off valve a leak test of the measuring system according to chap ter 3 of the manual can also be performed with the zero filter To check the calibration constant Ky a special filter kit with pre weighed TEOM filters is used Figure 15 Set of filters for the check of the calibration constant Ko 740300_2011_936_21209885B_eng doc A TUVRheinland Precisely Right Page 44 of 422 TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Within the scope of the testing after the test site Teddington Summer a mod
204. e filter mount for the bypass flow channel 8 Slide the large filter cartridge off the mount and install a new cartridge onto the mount Figure 5 33 Figure 5 33 Bypass filter mount with clean and dirty filter cartridges Clean filter cartridge Dirty filter cartridge j 9 Install the mount into the unit then install the cover for the bypass flow 10 Plug in the sample pump and return to normal operation THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 25 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Cleaning the Air Inlet You must clean the heated air inlet in the TEOM 1405 once a year to remove the buildup of particulate matter on its inner walls You can order a tapered bristle brush that is appropriate for cleaning the air inlet system from Thermo Scientific You will need a piece of plastic or another protective material soapy water alcohol or freon solution a 1 2 inch or adjustable wrench and a soft brush to clean the air inlet Follow these steps to clean the air inlet system 1 Turn off the TEOM 1405 unit 2 Open the door of the unit Figure5 34 and locate the thermistor in the top of the mass transducer assembly Figure 5 34 Thermistor on top of mass transducer Thermistors 3 Using the 1 2 inch wrench remove the thermistor from the top of the mass transducer assembly Note The thermistor has a short thread depth Installation removal should take 1 1 2 to
205. e is as follows The average concentrations Y of the i th parallel measurement of the candidate samplers are calculated followed by dividing the average concentrations Y into two separated data sets a Data set with Y lt 100 g m with number of paired values n lt and b Data set with Y gt 100 g m with number of paired values n gt Re a The absolute standard deviation sa is calculated from the paired values of the data set with Yi lt 100 pg m Sa D7 2n The corresponding Student factor ty_ 9975 is used defined as the 0 975 quintile of the two sided 95 confidence interval of the Student t distribution with f lt n lt 2 degrees of free dom The two sided confidence interval Clos for the average concentration values lt 100 ug m is then calculated as follows Clos Sa ti o975 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 123 01484 Re b The relative standard deviation s is calculated from the paired values of the data set with Y gt 100 ug m as follows s A X D Y 2n Once again the corresponding Student factor t _ o975 defined as the 0 975 quintile of the
206. e temperature and pressure to control the volumetric flow they should manually adjust the average temperature and average pressure settings as climatic conditions change The user usually has to adjust the average pressure only once for the average barometric pressure at the sampling site i e station pressure not adjusted to sea level However the user generally must adjust the average temperature periodically often 4 times per year in accordance with changing average ambient temperatures 4 16 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC THERMO FISHER SCIENTIFIC Section 4 SCREENS AND SETTINGS The mass concentration is reported based on the volume sampled through the TEOM inlet It can be reported in terms of the mass collected per actual volume sampled through the inlet or reported in terms of mass collected per standard volume sampled through the inlet If the user chooses to set the unit to report the mass concentration levels to Actual conditions they must select the Active flow control button Figure 4 13 This will cause the monitor to use the actual ambient temperature and ambient pressure in its flow rate calculations If the user chooses to set the unit to report the mass concentration levels to Standard conditions they must set the standard temperatures and pressures to the appropriate standard regulatory values Operatine Guine TEOM 1405 F 4 17 Section 4 SCREENS AND SETTINGS Instrument The Instr
207. e to the tare filter and check weight are shown in Figure 77 If filters lose relative mass between weightings then the distribution will be shifted to the right whereas if there is a gain in the relative mass the distribution will shift to the left EN14907 states that unsampled filters should be rejected if the difference between the masses of the two pre weightings is greater than 40 ug Similar ly EN14907 states that sampled filters should be rejected if the difference between the masses of the two post weightings is greater than 60 ug Filters were not rejected based on these criteria The observed distributions of repeat mass measurements are considered un likely to have had a significant effect on the results 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Genau Richtig Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 211101424 Figure 77 Distribution for Emfab filters of A Pre spread weighed relative to the check weight and B Post spread weighed relative to the check weight A 250 D gt 200 5 5 150 2 100 D c 50 0 _ ll il B 250 200 150 gt D 5 gt 100 2 50 j 0 rrr
208. easuring system TEOM 1405 F Ambient Particulate Monitor determines the particulate concentration by an oscillating microbalance measuring principle TEOM Tapered Element Oscillating Microbalance With the aid of a pump ambient air is sucked at 16 7 l min via a PM 9 sampling inlet The dust laden sampling air is collected and quantified on a TEOM filter By securing a constant flow rate of 3 l min and by a continuous determination of the collected mass on the TEOM filter the PM1o concentration can nearly be determined in real time The measuring system TEOM 1405 F Ambient Particulate Monitor is equipped with a so called FDMS system Filter Dynamics Measurement System By using a FDMS system non volatile as well as the volatile particulate matter is taken into account while determining the concentration of the particulate matter The tests took place in the laboratory and for several months in the field The following test sites were chosen for the field test according to Table 1 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Table 1 Description of the test sites A TUVRheinland Precisely Right Page 17 of 422 Teddington UK Teddington Uk
209. ecific table and breaking down the downloaded status codes you will be able to decipher which status codes the unit has displayed Repeat the operation for each place in the hexadecimal code 10 s 100 s etc Example For example decipher the following decimal status code 8433666 for an instrument with the given example status code table Table A 3 First convert the decimal status code downloaded from the monitor to a hexadecimal number using the Windows or another scientific calculator 8433666 H 80B002 Table A 3 Example status code table pans wwe rng A 4 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC APPENDIX A TROUBLESHOOTING be In the one s place of the status code a status code of 2 is displayed In the one s place of the status code table the 2 status code matches the H 2 Power Switch PIC status code This is one of the status codes that the unit is displaying in its status code e In the ten s place of the status code there are no 0 status codes displayed e In the 100 s place of the status code there are no 0 status codes displayed In the 1 000 s place of the status code a status code of B is displayed Because there are no status codes in the status code table that match this number the numbers needs to be broken down further Convert B to a decimal number using Table A 2 which converts B to
210. ection would adversely affect the quality of the data The instrument will automatically prompt the user to enter the Setup Mode when changing a temperature flow or other adjustable value After the new value is entered and saved it will automatically return to one of the four regular operating modes above If several parameters need to be changed the user can enter the Setup Mode manually avoiding the warning prompts when changing each variable To manually enter the Setup Mode select the Instrument Control button in the Service screen page 4 30 In the Instrument Control screen page 4 32 press the Setup button When the unit is in the Setup Mode the user can change all of the system s parameters To manually leave the Setup Mode and start data collection when in the Instrument Control screen select the Run button THERMO FISHER SCIENTIFIC THERMO FISHER SCIENTIFIC Section 4 SCREENS AND SETTINGS Stop All Mode Certain situations may arise in which the user may want to turn off all temperatures and flows in the instrument To enter the Stop All Mode select the Instrument Control button in the Service screen page 4 30 In the Instrument Control screen select the Stop button page 4 32 When the unit is in this operating mode it suspends operation of the instrument In this mode data collection ceases flow rates in the system drop to zero and the output to the temperature circuits is turned off Also the monitor will reset i
211. ed on the back of the unit Figure 5 28 These filters prevent contamination from reaching the flow controller For convenience replace the large in line filters immediately following one of the regularly scheduled TEOM filter exchanges This allows you to exchange the in line filters during the 30 minute flow and temperature stabilization period Bypass filter Main flow filter THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES To exchange the in line filters 1 Unplug the sample pump 2 Unscrew and remove the small filter cover for the main flow channel on the back of the unit Figure 5 29 Figure 5 29 Removing the filter cover 3 Unscrew the filter mount for main flow channel Figure 5 30 Figure 5 30 Removing the filter mount THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 23 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 4 Slide the filter cartridges off the mount and install a new cartridge onto the mount Figure 5 31 Figure 5 31 Filter cartridge and mount Filter cartridge Mount T 5 Install the mount into the unit then install the cover 6 Unscrew and remove the large filter cover from the bypass flow channel on the back of the unit Figure 5 32 Figure 5 32 Bypass in line filter Large filter cover 5 24 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 7 Unscrew th
212. edure has been carried out at the beginning of each field test site It is recommended to check the tightness of the AMS once a month using the described pro cedure 6 4 Evaluation The tightness check via the tightness check assistant was done at the beginning of each field test site The criteria for approving the tightness check implemented by the manufacturer a deviation of the flow values at a blocked inlet of no more than 0 15 I min from zero flow at the PM4o path and no more 0 60 l min from zero flow at the bypass path were approved as appropri ate parameters for the monitoring of the device tightness The tightness check may only be performed using the tightness check assistant to avoid damages of the instrument 740300_2011_936_21209885B_eng doc TUVRh T V Rheinland Energie und Umwelt GmbH ein and Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 140 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 5 Assessment The criteria for passing the tightness check implemented by the manufacturer a deviation of the flow values at a blocked inlet of no more than 0 15 I min from zero flow at the PMio path and no more 0 60 I min from zero flow at the bypass path were approved as appropri ate parameters for the monitoring of the dev
213. eeesecseeeeeseceeeeseesaeaeeess 131 Comparison candidate 20107 with reference device rel humidity gt 70 all test sites measured component PM jo ccccccceccaeeesesececeeeecceeeeeseceeeeseesaeaeesns 131 Results control flow rate ccessscinlactoceccenreuas iececcetee dens Neeste ett aaeteadaigaiuansateecemeateonays 134 Parameter for the total flow measurement 24h average Cologne Winter SN 20006 ee Rare re ep nen On eet ee ne er Cer eee ene cer nr een eee 135 Parameter for the total flow measurement 24h average Cologne Winter SIN ZO 107 siciscvcnatentans E E Sutua rns eoetecxaattatebaveua guste tavnaetnecanscans 135 Results of the tightness check during field teSt cc eeeeeeeeentteeeeeeeeeeeeeeeee 140 Uncertainty between systems under test Ups for the candidates SN 20006 and SN 20107 measured component PM1o ccccccceeessecceeeeeesaseeeeeeeeceeeeeaaes 144 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 9 01422 Table 31 Overview equivalence test TEOM 1405 F Ambient Particulate Monitor for PM gy e ea a ar a EE E EE E E E T E SaR 151 Table 32 In between instrument uncertainty Uret of the
214. einland Energie und Umwelt GmbH Wi Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 15901482 100 90 a SN 20107 Bornheim Summer A 80 Fa 70 wa i J 50 pa 40 4 A 30 4 ti PM 1405F FDMS pg m 0 r 7 T 7 T T 0 10 20 30 40 50 60 70 80 90 100 PM Reference ug m Figure 72 Reference vs candidate SN 20107 measured component PM19 Bornheim Summer 100 90 a SN 20006 80 70 4 60 50 40 PM 1405F FDMS pg m3 30 20 0 T T r T 0 10 20 30 40 50 60 70 80 90 100 PM Reference pg m Figure 73 Reference vs candidate SN 20006 measured component PMj9 values 2 30 g m 740300_2011_936_21209885B_eng doc a s T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 160 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 100 90 f a SN20107 Fa i A 3 60 4 a 50 ha A 40 a 20 YK 0 10 20 30 40 50 60 70 80 90 100 PM Refe
215. electronic measuring equipment of the LVS3 small filter device displays the incoming sampling air volume in standard or operating m as soon as the sampling is complete To determine the PM10 concentration the laboratory performed a gravimetric determination of the amount of suspended particulate matter on the respective filters The obtained result was then divided by the respective volume of sampling air in operating m or standard m accord ing to EN 12341 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 61 0f422 6 Test results 6 1 4 1 1 Measured value display The measuring system shall be fitted with a measured value display 6 2 Equipment No additional devices are needed 6 3 Performance of test It was checked whether the measuring device has a display for measured values 6 4 Evaluation The measuring device has a display for measured values The following values are dis played MC Mass concentration moving 1h average updated every 6 minutes 30 Min MC not working at the moment 1 Hr MC moving 1h average updated every 60 minutes every full hour 8 Hr MC moving 8h average updated every 60 minutes every fu
216. elt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 16501484 6 6 Detailed representation of the test results Table 34 shows the results of the evaluations of the equivalence check after the application of the correction factor for the intercept on the complete data set Table 34 Summary of the results of the equivalence check SN 20006 amp SN 20107 after in tercept correction 23 25 3 gt 28 ums gt 28 25 3 gt 28 ums m3 Orthogonal Regression Betw een Instrument Uncertainties PM10 1405F FOMS Wem Slope b up Intercept a ua Reference Candidate All Data 215 0 973 0 994 0 011 0 000 0 291 lt 30 ug m3 169 0 882 1 055 0 028 0 962 0 501 gt 30 ug m3 i 46 0 963 0 992 0 029 0 177 1 274 Orthogonal Regression Limit Value of 50 ug m 3 Slope b up Intercept a ua Wem gt 28 ug m3 Teddington Summer 42 0 895 1 112 0 057 0 340 0 883 SN 20006 Cologne Winter 74 0 987 0 992 0 013 0 068 0 461 Individual Datasets Bornheim Summer 55 0 931 1 134 0 041 2 492 0 750 Teddington Winter 66 0 987 0 959 0 014 1 944 0 337 lt 30 ug m3 186 0 860 1 069 0 029 1 772 0 528 11 31 2 2
217. ely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 143 01482 Furthermore the evaluation of the following data sets is done e Each test site individually e 1 Data set with measured values lt 30 ug m for PMio Basis averages of reference measurement The in between instrument uncertainty Ups is calculated from the differences of all 24 hour results of the simultaneously operated candidate systems according to the following equa tion Vis Yiz u2 ee bs Qn with Yi1 and yi2 results of the parallel measurements of individual 24h values i n No of 24h values 6 5 Assessment The in between uncertainty between the candidates ups is with a maximum of 1 35 ug m for PM below the required value of 2 5 ug m Minimum requirement fulfilled yes 740300_2011_936_21209885B_eng doc aT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 144 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 6 Detailed representation of the test results Table 30 shows the calculated values for the uncertainty between
218. ements no minimum requirement defined 6 1 5 3 12 Long term drift no minimum requirement defined 6 1 5 3 13 Short time drift not relevant for particulate devices 6 1 5 3 18 Overall uncertainty not relevant for particulate devices For this reason an official request to the competent German body was made to define a co ordinated procedure for dealing with inconsistencies in the Standard 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH 7 Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Pade 19 0142 The following procedure was suggested The test points 5 3 2 5 3 7 5 3 8 5 3 11 and 5 3 12 are evaluated as before based on the minimum requirements stated in VDI 4202 Part 1 from 2002 i e using the reference values Bo B4 and B2 The testing of the test points 5 3 3 5 3 4 5 3 13 and 5 3 18 is waived as they are not rele vant for particulate measuring devices The competent German body agreed with the proposed procedure by decision of 27 June 2011 respectively 07 October 2011 According to the applied standards the following reference values have been agreed upon PMio Bo 2 ug m B 40 g m B2 200 ug m 740300_2011_936_21209885B_eng doc a s
219. enclosure about 4 to 6 inches Connect the coiled tubing from the water trap filter to the bypass line near the top of the shelter with the quick connect fitting Ensure that the coiled water trap tubing is vertical Figure 2 19 Figure 2 27 Virtual impactor temperature humidity sensor and sample tubes Temperature humidity sensor Flow splitter Bypass connection THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 2 23 Section 2 SETUP AND INSTALLATION 13 Locate the ambient temperature and humidity sensor Connect the sensor to the flow splitter using the U bolt provided with the 1405 unit Figure 2 27 14 Attach the sensor cable to the sensor and run the sensor cable to the instrument through the opening in the back of the enclosure Figure 2 28 Attach the sensor to the sensor connection on the back of the TEOM 1405 unit Figure 2 29 Note The opening in the back of the enclosure can also be used for other connections such as Ethernet connections a Figure 2 28 aed gt Temperature humidity sensor cable entering the outdoor enclosure Sensor cable Figure 2 29 Temperature humidity sensor connection of the back of the TEOM 1405 F unit Temperature humidity cable connection 2 24 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 2 SETUP AND INSTALLATION 15 Install the inlet Figure 2 30 Note Drain the water trap as needed a Note Thermo Scientific strongly recom
220. eng doc a T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 52 of 422 company Thermo Fisher Scientific for the component PM10 g Report No 936 21209885 B The following figures show the measuring cabinet at the field test sites Teddington Cologne parking lot and Bornheim motorway parking lot Figure 21 Field test site Cologne parking lot 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Ty Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 P f 422 Report No 936 21209885 B age 33 0 Figure 22 Field test site Bornheim motorway parking lot Besides the measuring device for the determination of particulate ambient air a device for the determination of meteorological characteristics was installed at the cabinet measuring test site A continuous determination of ambient temperature ambient pressure relative hu midity wind velocity wind direction and the amount of precipitation was made The 30 min averages were recorded The installation of the cabinet itself and the arrangement of the sampling pro
221. entific for the component PM10 Report No 936 21209885 B Annex 6 Date Test site Amb temperature avg Amb temperature max Amb pressure Rel humidity Wind velocity Wind direction Precipitation C C hPa m s 7 mm 9 8 Teddington Winter 12 9 2009 12 10 2009 12 11 2009 12 12 2009 12 13 2009 12 14 2009 12 15 2009 12 16 2009 12 17 2009 12 18 2009 12 19 2009 12 20 2009 12 21 2009 42 22 2009 12 23 2009 12 24 2009 12 25 2009 12 26 2009 12 27 2009 12 28 2009 12 29 2009 12 30 2009 12 31 2009 1 1 2010 1 2 2010 1 3 2010 1 4 2010 1 5 2010 1 6 2010 1 7 2010 Ambient conditions at the field test sites 3 9 5 7 5 8 4 2 3 4 0 6 1 5 1 3 0 8 0 9 1 1 2 1 2 8 4 1 4 1 5 9 2 4 3 7 4 8 4 3 2 3 1 6 1 6 3 7 0 8 2 3 1 2 A TUVRheinland Precisely Right Page 197 of 422 Page 1 of 11 0 3 0 3 0 0 0 0 0 3 0 0 0 3 2 8 1 3 0 0 1 8 0 0 8 6 0 3 7 1 0 5 2 5 0 8 0 0 1 8 11 7 5 6 0 0 0 0 0 0 0 0 0 0 4 8 1 8 0 0 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Page 198 of 422 Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Annex 6 Ambient conditions a
222. er so that the top of the installed sample tube or flow adapter is approximately 15 5 cm 6 from the top of the flow splitter it must be between 5 75 and 6 25 inches from the top of the flow splitter Figure 2 7 3 Tighten the 1 2 inch sample tube nut Ensure that the top of the flow adapter remains between 5 75 and 6 25 inches from the top of the flow splitter Figure 2 7 Figure 2 6 Flow splitter Bottom of the flow splitter i Bypass tube 1 2 inch sample tube nut ooo i Sample tube Figure 2 7 Measuring the distance from the top of the sample tube to the top of the flow splitter THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 2 7 Section 2 SETUP AND INSTALLATION Assembling the Tripod Figure 2 8 Placing the metal bracket on the tripod foot 2 8 Operatinc Guipe TEOM 1405 F An optional tripod is available for installation on the roof of a sampling building To assemble the tripod 1 Locate a tripod foot and remove the rubber leg holder if one is attached Place one leg of the tripod onto the tripod foot Place a metal bracket over the rubber base of the tripod leg and into the two slots on the tripod foot Figure 2 8 Ensure that the bracket is placed over the rubber base on the end of the tripod leg Insert a plain washer then a lock washer onto each threaded end of the bracket then install the nuts on the threaded ends of the bracket and tighten them with a 3 8 o
223. erence vs SN 20107 Cologne Winter 100 Measured values 90 80 Regression line 70 go __ 1 l y g Z Acceptance range 5 according to EN 12341 g 50 y x 40 ao S 30 i Leer al 20 10 0 10 20 30 40 50 60 70 80 90 100 Reference yg m Figure 39 Reference equivalence function SN 20107 test site Cologne parking lot 740300_2011_936_21209885B_eng doc a T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 120 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Reference vs SN 20006 Bornheim Summer 100 Measured values 90 80 Regression line 70 6g SE Pa a el 8 ees ail Peseeee Acceptance range gt according to EN 12341 g 50 y x 40 S 30 j C radl 20 10 0 10 20 30 40 50 60 70 80 90 100 Reference yg m Figure 40 Reference equivalence function SN 20006 test site Bornheim Summer Reference vs SN 20107 Bornheim Summer 100 Measured values 90 80 Regression line 70 B si de 7 ee a e Acceptance range according
224. ertainty of the candidates w cm is calculated for each data set by combining the contributions from 9 5 2 1 and 9 5 2 2 according to the following equation 2 u i W ou a For each dataset the uncertainty W cm is calculated at the level of y 50 ug m for PM4o Point 9 5 4 The expanded relative uncertainty of the results of the candidates is calculated for each data set by multiplication of Wo cm with a coverage factor k according to the following equation Wem K Wen In practice k 2 for large n Point 9 6 The highest resulting uncertainty Wcm is compared and assessed with the re quirements on data quality of ambient air measurements according to EU Standard 7 Two results are possible 1 Wem Waqo gt Candidate method is accepted as equivalent to the standard method 2 Wem gt Waqo gt Candidate method is not accepted as equivalent to the standard method The specified expanded relative uncertainty Waqo for particulate matter is 25 7 6 5 Assessment The determined uncertainties Wey without application of correction factors lay for all ob served data sets beneath the defined expanded relative uncertainty Wago of 25 for particu late Minimum requirement fulfilled yes The following Table 31 shows an overview of the results of the equivalence check for the candidate TEOM 1405 F Ambient Particulate Monitor for PMj9 For the case that a criterion is fulfilled or not the text is represented in gree
225. ervice screen select the Verification or Calibration buttons to display the Verification and Calibration screens Figure 5 48 and 5 49 Figure 5 48 Calibration screen TEOM 1405 F Service gt Calbration ef abion Meresdl elatus oe EOE 1218 Figure 5 49 Verification screen TEOM 1405 F Service gt Verihecalion x Back ai Seong Heey sialug m TETE 11 THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 39 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Figure 5 50 Number entry keypad 5 40 Operatine Guine TEOM 1405 F Users enter values into the calibration screens using a number keypad Figure 5 50 Whenever the user is prompted to enter a value such as an externally measured temperature pressure or flow rate the calibration wizard will automatically display a keypad Enter the value into the keypad as instructed by the wizard then select the Enter button to set the value or press the Cancel button to exit the keypad screen and return to the wizard Ambient temperature THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Auditing the System Users can instantly audit all of the instruments functions through a single software screen When in the Verification screen select the Instrument Audit button to display the Instrument Audit screen Figure 5 51 The Instrument Audit screen shows the temperature flow and other values that can be audited by the use
226. es Amb pressure Rel humidity Wind velocity Wind direction hPa m s Amb temperature avg C Amb temperature max C A TUVRheinland Precisely Right Page 205 of 422 Page 9 of 11 Precipitation mm 0 0 2 1 8 9 0 3 3 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1 2 0 0 51 7 5 9 0 0 0 0 0 0 0 0 0 0 5 4 3 6 0 6 7 7 1 8 6 2 14 8 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Page 206 of 422 Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Annex 6 Ambient conditions at the field test sites Page 10 of 11 No Date Test site Amb temperature avg Amb temperature max Amb pressure Rel humidity Wind velocity Wind direction Precipitation C C hPa m s 0 mm 271 8 10 2011 Bornheim 18 0 22 4 1013 57 5 1 3 224 0 0 272 8 11 2011 Summer 20 9 25 5 1004 53 8 1 2 220 0 3 273 8 12 2011 18 5 21 7 1003 78 9 1 1 228 2 1 274 8 13 2011 20 1 23 7 1001 77 0 0 7 185 0 0 275 8 14 2011 17 4 19 9 1000 86 2 1 1 219 17 4 276 8 15 2011 17 9 22 4 1009 71 8 1 2 230 0 0 277 8 16 2011 19 1 23 9 1010 69 0 0 7 190 0 6 278 8 17 2011 21 1 27 8 1007 73 8 0 7 206 4 7 279 8 18 2011 22 5 31 3 1004 76 6 1 2 1
227. es included in the assessment Test gas units included in the measuring system shall indi cate their operational readiness to the measuring system by a status signal and shall provide direct as well as remote control via the measuring system 4 1 4 Set up times and The set up times and warm up The setup and warm up times were 67 warm up times times shall be specified in the determined instruction manual 4 1 5 Instrument de The instruction manual shall The instrument design specifications 69 sign include specifications of the listed in the operating manual are manufacturer regarding the de complete and correct sign of the measuring system 4 1 6 Unintended ad It shall be possible to secure The AMS is protected against unau 70 justment the adjustment of the measur thorized and unintended adjustment ing system against illicit or un In addition the AMS shall be locked intended adjustment during in a measuring cabinet operation 4 1 7 Data output The output signals shall be Measured signals are offered ana 71 provided digitally and or as an alogue signals logue 0 1 or 5 V and digital via Ethernet RS 232 UBS 740300_2011_936_21209885B_eng doc A TUVRheinland Precisely Right Page 20 of 422 5 1 General 5 2 5 2 1 Certification ranges 5 2 2 Measuring range 5 2 3 Negative output signals 5 2 4 Failure in the mains voltage 5 2 5 Operating states 5 2 6 Switch over
228. es obtained by feeding gas at the sample and calibration port shall not ex ceed the requirements of Table 2 of Standard VDI 4202 Part 1 September 2010 In the case of measuring sys tems with a converter the effi ciency of the converter shall be at least 98 In case of NO measuring sys tems the increase of NO2 con centration due to residence in the measuring system shall not exceed the requirements of Table 2 of Standard VDI 4202 Part 1 September 2010 The expanded uncertainty of the measuring system shall be determined The value deter mined shall not exceed the cor responding data quality objec tives in the applicable EU Di rectives on air quality listed in Annex A Table A1 of Standard VDI 4202 Part 1 September 2010 740300_2011_936_21209885B_eng doc Not applicable Not applicable Not applicable Not applicable According to the decision of the com petent German body see module 5 3 1 this test point is not relevant for particulate measuring devices Refer ence is made to module 5 4 10 110 111 112 113 TUV Rheinland Energie und Umwelt GmbH w Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Specification Test result Page filled Re
229. es obtained for slope and or intercept of all paired instruments to gether The fulfillment of the 5 criteria is checked in the following chapters In chapter 6 1 5 4 9 Determination of uncertainty between systems under test u s criteria 1 and 2 will be checked In chapter 6 1 5 4 10 Calculation of the expanded uncertainty of the instruments criteria 3 4 and 5 will be checked In chapter 6 1 5 4 11 Application of correction factors and terms there is an exemplary evaluation for the case that criterio 5 cannot be fulfilled without the application of correction factors or terms 740300_2011_936_21209885B_eng doc TUVRh T V Rheinland Energie und Umwelt GmbH ein and Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 142 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 1 5 4 9 Determination of uncertainty between systems under test Ups For the test of PM2 5 measuring systems the uncertainty between the systems under test shall be determined according to chapter 9 5 2 1 of the guidance document Demonstration of Equivalence of Ambient Air Monitoring Methods in the field test at least at four sampling test sites representative of the future application The tests are performed as well for the component PM 6 2 Equipment Not required for this m
230. ete data set is used 237 valid measured value pairs for SN 20006 230 valid measured value pairs for SN 20107 The parameters of the calibration function y m x b were determined by linear regression The analysis function is the reversal of the calibration function It reads x 1 m y b m The slope m of the regression line characterized the sensitivity of the measuring device the ordinate intercept b characterized the zero point The values result as shown in Table 22 Table 22 Results of the calibration and analysis function measured component PM Device Nr Calibration function Analysis function Y m x b x 1 m y b m Device 1 SN 20006 0 981 1 019 0 163 Device 2 SN 20107 0 986 1 014 1 164 m 740300_2011_936_21209885B_eng doc aT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 128 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 5 Assessment A statistically secured relation between the reference measuring procedure and the instru ment display could be demonstrated Minimum requirement fulfilled yes 6 6 Detailed representation of the test results See module 5 4 2 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH w Luft
231. filter Ko check kit 6 3 Performance of test The device status is constantly monitored and problems are indicated by a series of different warning messages Important parameters for a proper performance e g noise of the mass measurement flow rates pump vacuum dew point of the air sample moreover can be looked up at the device itself or while recording the data Furthermore there is also the possibility to check the zero point of the measuring device ex ternally For this a zero filter is installed at the device inlet The use of this filter allows the provision of particle free air Within the scope of the test work a determination of the zero point by using the zero filter was also performed approx every 4 weeks Moreover there is the possibility to check the calibration constant of the mass measurement externally For this the calibration constant is determined using the Ko check kit and after wards compared with the nominal value stored within the device Within the scope of the check the calibration constant was determined at the beginning and the end of each test site 6 4 Evaluation All instrument functions which are listed in the manual are available and can be activated The current status of the system is monitored continuously and problems are indicated by a series of different warning messages An external check of the zero point by using the zero filter is possible at any time An exter nal check of the mass measu
232. flow rate button and enter the current flow rate to two decimal places as measured by the flow meter into the number pad and select the Enter button The newly entered flow rate will display in the TEOM flow rate button Select the Next gt button 8 The wizard will display a screen that shows the current setpoint flow rate as measured by the instrument in the TEOM flow rate button Allow the flow to stabilize Select the TEOM flow rate button and enter the current flow rate to two decimal places as measured by the flow meter into the number pad and select the Enter button The newly entered flow rate will display in the TEOM flow rate button Select the Next gt button THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 9 After the third flow value has been entered the Select Flow to Calibrate screen will display again The flow channel that was just calibrated will be grayed out on the screen to show it was calibrated during this calibration session If you want to calibrate another flow channel select another channel and follow steps 4 9 and the wizard to complete additional flow channels Otherwise ensure that no flow channel buttons are selected and select the Next gt button 10 The Completing the Flow Calibration Wizard screen will display Figure 5 68 Remove the flow meter and flow adapter s and install the inlet Ensure all lines including the bypass are reconnected Select th
233. from PL 1405 click Begin Download Begin Download 4 Select the Begin Download button The ePort software will download data based on the settings created in the Download Setup wizard Refer to the previous section for information on setting up downloads The message window will display a Downloading Data message while the software is downloading data from the instrument When the download is complete it will display a Download Complete message Select the Done button to exit the Download Data screen 3 30 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 3 Basic OPERATION Downloading Data The TEOM 1405 also supports data downloads using the USB connection To a Flash Drive on the front of the instrument and a USB flash drive Note Due to the size of the storage buffer downloading all stored data may take 30 minutes or more a To download data using the USB connection 1 Plug a flash drive into the USB connection on the front of the instrument The Download Data to USB Flash Drive screen will display Figure 3 33 Figure 3 33 Download Data to USB TEOM 1405 F Flash Drive screen y Download Data to USB Flash Drive Sd A USB flash drive is detected Are you sure you want to download the data 2 To continue with the download select the Yes button To cancel select the No button then remove the USB drive THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 3 31 Section
234. g to EU Standard 7 Two results are possible 1 Wem S Waqo gt Candidate method is accepted as equivalent to the standard method 2 Wom gt Waqo Candidate method is not accepted as equivalent to the standard method The specified expanded relative uncertainty Wago for particulate matter is 25 7 6 5 Assessment The candidate systems fulfil the requirements on the data quality of ambient air quality measurements during the test already without application of correction factors Minimum requirement fulfilled yes The evaluation of the All data comparison for both candidate nevertheless delivers a signifi cant intercept for SN 20107 see Table 31 The intercept for the All data comparison is 0 395 For this reason an intercept correction for the All data comparison was performed and all data sets re evaluated with the corrected values All data sets comply with the speci fications on the data quality after the correction The improvement of the expanded measur ing uncertainty is only relatively marginal 740300_2011_936_21209885B_eng doc aT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 164 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B The version of the Guide of
235. ge 23 of 422 Not applicable 5 3 10 Averaging effect For gaseous components the measuring system shall allow the formation of hourly averag es The averaging effect shall not exceed the requirements of Table 2 of Standard VDI 4202 Part 1 September 2010 5 3 11 Standard devia tion from paired measurements The standard deviation from parallel determinations shall be done with two identical meas uring devices during field test It shall not exceed the specifi cations stated in Table 2 of Standard VDI 4202 Part 1 September 2010 For PM RD gt 10 referring to B4 5 3 12 Long term drift The long term drift at zero point and reference point shall not exceed the requirements of Table 2 in the field test A value ct at 70 to 80 of the upper limit of the certification range shall be used as reference point For PM Zero point within 24 h and within the maintenance interval a maximum of BO As reference point within 24 h and within the maintenance in terval a maximum 5 of B1 5 3 13 Short time drift The short term drift at zero point and reference point shall not exceed the requirements of Table 2 of Standard VDI 4202 Part 1 September 2010 within 12 h for benzene 24 h in the laboratory test and within 24 h in the field test A value ct at 70 to 80 of the upper limit of the certification range shall be used as reference point Not applicable 99 The reproducibility RD for PM10 wa
236. h toward you to open the transducer latch 6 With the mass transducer unlatched swing the bottom of the mass transducer downward exposing the tapered element TE Figure 5 6 Select the Next gt button Figure 5 6 Opening the mass transducer TEOM filter Conditioned TEOM filters 7 The Remove Old Filter screen will display Carefully insert the lower fork of the filter exchange tool under the used TEOM filter so that the filter disk is between the fork and the upper tab of the filter exchange tool Figure 5 7 The tines of the fork should straddle the hub of the filter base Figure 5 7 Opening the mass transducer 8 Gently pull straight up lifting the TEOM filter from the tapered element TE Do not twist or tilt the filter exchange tool from side to side while removing the filter from the TE This will damage the TE THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 7 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 9 The Replace Filter screen will display Pick up a new conditioned TEOM filter from one of the filter holders with the filter exchange tool so that the filter disk lies between the fork and the upper tab of the tool and the hub of the filter lies between the tines of the fork Figures 5 8 and 5 9 Note TEOM filters must be preconditioned to avoid excessive moisture buildup prior to their use in the system Refer to the next section A Note Do not touch the filter with your fingers
237. he Calibration button to display the Calibration screen Figure 5 48 2 Select the Ambient Calibration button to display the Ambient Calibration screen Figure 5 53 TEOM 1405 F Service Calibration gt Ambient Calibration Click the button to enter the coment actual smijeni bempersbure or pressure ieee lal linet ell con ef Tabinng Harmas status F TADS e006 VIC 3 Determine the current ambient pressure in atmospheres absolute pressure not corrected to sea level 4 If the measured value is within 0 01 atm of the pressure displayed in the Ambient Pressure field of the button no further action is necessary Select the lt Back button to return to the Calibration screen If the value is not within 0 01 atm of the pressure displayed in the Ambient Pressure field of the button select the Ambient Pressure button A keypad will display Enter the actual pressure as measured by the external device and press the Enter button The Ambient Pressure Calibration screen will display with the new entered value Select the lt Back button to return to the Calibration screen Operatine Guine TEOM 1405 F 5 43 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Auditing the To auditthe main or bypass flow Flow Rates In the TEOM Data screen select the Service button to display the Service screen then select the Verification button to display the Verification screen Figure 5 49 2 Select the Flow Audit butt
238. he back of the TEOM 1405 unit Figure 2 15 11 Fasten the tripod feet to the roof The length and type of fasteners depends on the type of roof surface The tripod feet also may be attached to a pallet or 3 4 marine plywood with the pallet or plywood secured by concrete blocks or sand bags Figure 2 14 Temperature humidity sensor installed on flow splitter Flow splitter Temperature humidity sensor U bolt Figure 2 15 Temperature humidity sensor connection of the back of the Series 1405 unit Temperature humidity cable connection 2 14 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Applying Power to the Instrument Figure 2 16 Power connection on back of unit THERMO FISHER SCIENTIFIC Section 2 SETUP AND INSTALLATION The TEOM 1405 F unit accepts all voltage inputs between 85 and 240 volts AC The unit should be connected to an appropriate code approved electrical outlet for the sampler location Contact a qualified electrician if there is doubt as to whether the power service for the instrument is adequate To turn on the monitor 1 Install an appropriate power cord into the universal power connection on the back of the instrument at the appropriate voltage Note DO NOT attempt to bypass the grounding requirements for the unit a ey 2 Install the other end of the power cord into an appropriate easily accesible grounded code approved electrical outlet Note Conta
239. he filter and check the frequency again Figure 5 17 TEOM Data screen System Status insinuant Conditions Settings 5 14 Operatine Guine TEOM 1405 F TEOM 1405 F TEOM Data MAE i pgm E Bhn hE dugim 1 Hr Mee pgm B Hour value pgm iE 12 Hr h t ugm 2 H MC ugm Filter boadtirny Frequency Nokee a Fiy operational Harasa status al net i53 THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Conditioning the TEOM Filters TEOM filters must be preconditioned to avoid excessive moisture buildup prior to their use in the system The TEOM 1405 has two posts for pre conditioning filters To precondition a TEOM filter 1 Place two TEOM filters on the TEOM filter holders of the mass transducer Figure 5 18 to condition the filters 2 When it is time to install a new TEOM filter use a conditioned filter from one of the filter holders 3 Replace the conditioned TEOM filter that was on the filter holder with a new filter Figure 5 18 Conditioned TEOM Filters Conditioned filter Conditioned filter Note Extra filters should be stored inside the carrier box in the interior of the unit near the mass transducer to ensure they are at or near the appropriate temperature and humidity level for sampling a THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 15 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Replacing the Install a new 47 mm filter into th
240. he flow splitter when you assemble and install the sample inlet following section a Note Thermo Scientific strongly recommends that you use the vacuum pump provided with the unit If you choose to install a different pump it must be oil free and able to maintain a 21 Hg vacuum at a flow of 16 67 min a THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 2 5 Section 2 SETUP AND INSTALLATION Adjusting the An isokinetic flow splitter Figures 2 5 and 2 6 is used in combination Flow Splitter with an automatic flow controller to divide the main bypass flow into two components after the air stream passes through the size selective inlet The two sample flow components are the main flow 3 1 min that flows to the TEOM mass transducer and the bypass flow 12 1 min Figure 2 5 Flow splitter in about 15 cm i Sample tube 1 2 sample tube fastener nut __ Sample tube Even though the flow splitter and sample tube are pre assembled verify the assembly position prior to use Should it need to be re assembled refer to the instructions that follow 2 6 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 2 SETUP AND INSTALLATION The tubing package is designed to use the short sample tube in the flow splitter To set up the flow splitter assembly 1 Locate the flow splitter Figures 2 5 and 2 6 2 Loosen the 1 2 inch sample tube fastener nut and slide the sample tube down into the flow splitt
241. he reference method with a slope of 0 994 and an intercept of 0 395 at an expended total uncertainty of 8 4 The January 2010 version of The Guidance is ambiguous with respect to which slope and in tercept should be used to correct a candidate should it fail the test for equivalence After communication with the convenor of the EC working group which is responsible for setting up the Guide Mr Theo Hafkenscheid it was decided that the requirement of the November 2005 version of the Guidance are still valid and that the slope and intercept from the orthog onal regression of all the paired data should be used These are shaded gold and marked other in the key on the above Table 31 740300_2011_936_21209885B_eng doc a s T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 152 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B The 2006 UK Equivalence Report 8 highlighted that this was a flaw in the mathematics re quired for equivalence as per the November 2005 version of The Guidance as it penalised instruments that were more accurate Appendix E Section 4 2 therein This same flaw is copied in the July 2009 version It is the opinion of TUV Rheinland and their UK partners that the TEOM 1405 F Ambient Par
242. he sensitivity coefficient of sample gas temperature at reference point shall not exceed the requirements of Table 2 A value ct at 70 to 80 of the upper limit of the certification range shall be used as reference point Note This point is not relevant for particulate measuring devices 6 2 Equipment Not applicable 6 3 Performance of test Not applicable 6 4 Evaluation Not applicable 6 5 Assessment Not applicable Minimum requirement fulfilled 6 6 Detailed representation of the test results Not applicable 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH F Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 9301422 6 1 5 3 7 Sensitivity coefficient of the surrounding temperature The sensitivity coefficient of surrounding temperature at zero and reference point shall not exceed the requirements of Table 2 A value ct at 70 to 80 of the upper limit of the certi fication range shall be used as reference point Note This test point is not evaluable for particulate measuring devices on the basis of the currently valid version of Standard VDI 4202 Part 1 September 2010 and VDI 4203 Part 3 Septem ber 2010 due no non defined minimum requirement
243. he touch screen display were resolved e g there have been problems with the button reboot during a possible system crash No influences on the system performance are expected from the changes which were made on the firmware up to version 1 55 The laboratory tests for the determination of system characteristics were followed by a field test of several months at different test sites All concentrations determined under operational conditions are presented in g m opera tional conditions Additionally according to Standard EN 12341 the PM1o concentrations are presented in normal conditions in g m 273 K 101 3 kPa for the evaluation The following report comprises a description of each minimum requirement according to standards 1 2 3 4 in number and wording 4 2 Laboratory test The laboratory test was carried out with two identical devices of TEOM 1405 F Ambient Par ticulate Monitor measuring system with the serial numbers SN 20006 und SN 20107 Accord ing to the Standards 1 2 the following test program was specified for the laboratory test Description of system functions Determination of detection limits Determination of the dependence of zero point sensitivity on ambient temperature Determination of the dependence of zero point sensitivity on the mains voltage Sampling flow stability check The following devices were used to determine the system characteristics during laboratory test e Climate chamber temper
244. he vacuum disconnected and flow through the instrument with the inlet blocked which should also be zero The leak check passes if the main flow is within 0 15 l min and the bypass flow is within 0 60 l min of their zero value with the vacuum disconnected In order to ensure proper performance of the instrument and ensure no leaks the instrument prompts the operator to perform a leak check with the FDMS valves in both the base and reference positions Note The Leak Check Wizard automatically disables the switching valve during a leak check Performing a leak check without the wizard can damage the switching valve a To perform a leak check 1 In the 1405 TEOM Data screen select the Service button to display the Service screen then select the Verification button to display the Verification screen 2 Select the Leak Check button to display the Leak Check Wizard screen Figure 3 2 Select the Next gt button Figure 3 2 Leak Check Wizard start screen Welcome to the Leak Chack Wizard This wizard belies you pertonm a leak check on the Series 1405 Ambient Particulate hionitor The insirumeni wili be put in Setup mode for calbrailon To continue prese Mexi 3 4 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 3 Basic OPERATION 3 The Select Valve Position screen will display The current valve position is displayed on the screen To start the leak check select the current valve position leak c
245. heck button Figure 3 3 Select the Next gt button Note If trying to isolate a leak with the valve in a specific position select the specific valve position desired and proceed a Figure 3 3 e Leak Check Wizard screen M ole with current valve position see eee select The wizard will verify each TEOM independently 4 The Remove the TEOM filter screen will display Remove the TEOM filter from the transducer to ensure it isn t damaged during the leak check procedure Select the Next gt button 5 The Disconnect Vacuum Line screen will display Remove the main vacuum line pump connected to the pump from the back of the unit Figure 3 4 Select the Next gt button THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 3 5 Section 3 Basic OPERATION Figure 3 4 Back of TEOM 1405 unit Pump connection 6 The Stabilizing screen will display Allow 1 minute for the flows to stabilize then select the Next gt button 7 The Reconnect Vacuum Line screen will display Reinstall the pump vacuum tubing into the back of the unit Select the Next gt button 8 The Remove Inlet screen will display Remove the inlet Figure 3 5 Select the Next gt button 3 6 Operatinc Guipe TEOM 1405 F THERMO FISHER SCIENTIFIC Section 3 Basic OPERATION Figure 3 5 Inlet assembly Inlet Figure 3 6 Leak check adapter Flow splitter Leak adapter 9 The Attach Audit Adapter screen will di
246. heinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 112 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 1 5 3 17 Increase of NO concentration due to residence in the measuring system In case of NO measuring systems the increase of NO concentration due to residence in the measuring system shall not exceed the requirements of Table 2 of Standard VDI 4202 Part 1 September 2010 The requirements of Table 2 Standard VDI 4202 Part 1 September 2010 apply to certifica tion ranges according to Table 1 of Standard VDI 4202 Part 1 September 2010 For deviat ing certification ranges the requirements shall be proportionally converted Note This point is not relevant for particulate measuring devices 6 2 Equipment Not applicable 6 3 Performance of test Not applicable 6 4 Evaluation Not applicable 6 5 Assessment Not applicable Minimum requirement fulfilled 6 6 Detailed representation of the test results Not applicable 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH w Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for
247. hing session 2 prior to sampling Post1 denotes weighing session 1 after sampling Post2 denotes weighing session 2 after sampling 740300_2011_936_21209885B_eng doc TUVRheinland TUV Energie und Umwelt GmbH Precisely Right Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Seite 216 von 422 Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Pre Spread Spe Post Spread Spost and Blank Spread Spiank were calculated using the following equations Spre RM anpi RM gap E A 4 S Post RM Endi RM End2 E A 5 Soig Men CM rena Me CM anfi E A6 2 2 As with the UK PM Equivalence Report 11 it was not possible to weigh all filters within the 15 day timeframe suggested in EN14907 However as filters were removed immediately from the reference samplers and placed in the refrigerator it was not necessary to determine if T Ambient exceeded 23 C It is felt that as 15 days was impractical for a relatively small scale field study it is less likely to be attainable if this methodology were adopted by a National or Regional network and as such the methodology employed herein is representative of how the reference samplers would be operated in practice A 2 Analysis of Protocols Employed The distributions of pre and post weight for all Emfab filters weighed relativ
248. ic Other trademarks are the property of their respective holders Mention of specific product names other than Thermo Fisher Scientific products in this manual does not constitute an endorsement or recommendation by Thermo Fisher Scientific of that equipment Warranty Seller warrants that the Products will operate substantially in conformance with Seller s published specifications when subjected to normal proper and intended usage by properly trained personnel for 12 months from date of installation or 13 months from date of shipment whichever is less the Warranty Period Seller agrees during the Warranty Period provided it is promptly notified in writing upon the discovery of any defect and further provided that all costs of returning the defective Products to Seller are pre paid by Buyer to repair or replace at Seller s option defective Products so as to cause the same to operate in substantial conformance with said specifications Replacement parts may be new or refurbished at the election of Seller All replaced parts shall become the property of Seller Shipment to Buyer of repaired or replacement Products shall be made in accordance with the provisions of Section 5 of the Terms and Conditions of Sale agreement Lamps fuses bulbs and other expendable items are expressly excluded from the warranty under Section 9 of the Terms and Conditions of Sale agreement Seller s sole liability with respect to equipment materials pa
249. ice tightness The tightness check may only be performed using the tightness check assistant to avoid damages of the instrument Minimum requirement fulfilled yes 6 6 Detailed representation of the test results Table 29 contains the determined values from the tightness check Table 29 Results of the tightness check during field test SN 20006 SN 20107 Limit Basis Refer Limit Basis Refer ence ence l min l min l min l min l min l min Teddington PMio 0 15 0 01 0 01 0 15 0 06 0 06 Winter Bypass 0 60 0 0 0 0 060 016 0 19 Teddington PMio 0 15 0 0 0 0 0 15 0 04 0 04 Summer Bypass 0 60 0 14 0 14 060 0 07 0 07 Cologne PMio 0 15 0 06 0 06 0 15 0 04 0 04 winter Bypass 0 60 0 11 0 11 0 60 0 0 0 0 Bornheim PMio 0 15 0 05 0 05 0 15 0 06 0 06 Summer Bypass 0 60 0 07 0 08 0 60 0 0 0 0 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH WT Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 141 01482 6 1 Methodology of the equivalence check modules 5 4 9 5 4 11 According to the version of the Guide from January 2010 4 the following 5 criteria must be f
250. ifetime of consecutive TEOM filters becomes noticeably shorter you may need to replace the in line filter Refer to Exchanging the In Line Filters later in this section THERMO FISHER SCIENTIFIC THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Filters should be stored inside the unit for easy access and to keep them dry and warm TEOM filter life depends upon the nature and concentration of the particulate matter sampled as well as the flow rate settings TEOM filters must be replaced when the filter loading value approaches 100 This generally corresponds to a total mass accumulation on the filter of approximately 3 5 mg TEOM filter life at a main flow rate of 3 l min is generally 21 days at an average PM 10 concentration of 50 ug m TEOM filter life is longer at lower flow rates because the particulate matter accumulation on the TEOM filter is slower TEOM filters must be replaced before the filter loading percentage on the status line of the Main screen reaches 100 When the filter loading percentage is greater than 90 the unit will trigger a status condition You must replace the 47 mm filter every time that you replace a TEOM filter Note Do not handle new TEOM filters with your fingers Use the filter exchange tool provided with the instrument to replace filters a Operatine Guine TEOM 1405 F 5 5 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Changing the TEOM Filters To install a T
251. ification of the measuring system from configuration C to D was made In doing so the following compo nents were changed Table 2 Instrument modifications after field test site Teddington Summer No Component Configuration C Configuration D Reason Assessment 1 Mass Transducer Hinge Belville washer Coil compression Simplification of No influence on the spring with ma spring the manufactur instrument perfor chined hinge ing mance blocks 2 Mass Transducer Latch High force Consistent force Simplification of No influence on the screw latch hook latch the operability instrument perfor mance 3 Mass Transducer Ship Not available Removable plate For the protec No influence on the ping Bracket couples mass tion of the de instrument perfor transducer to en vice during mance closure transport 4 Air Tube Tower top in Rubber isola Direct connection Simplification of No influence on the terface tors between using bulkhead fit the manufactur instrument perfor bulkhead fitting ting ing mance and cover 5 Diverter valve shipping Not available Bracket coupling For the protec No influence on the bracket valve to tower tion of the de instrument perfor vice during mance transport 6 Air tube Valve coupler Direct connec Sorbothane isolator Higher flexibil Improvement of the tion between between weldment ity compensa instrument perfor weldment air air tube and valve
252. ig Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 P 211 of 422 Report No 936 21209885 B eee Table 35 Stability standard weight Difference to Weighing Standard the previous Date No weight weighing g ug 12 11 2008 1 0 20002 13 11 2008 2 0 20001 10 10 12 2008 3 0 20002 10 11 12 2008 4 0 20002 0 17 12 2008 5 0 20003 10 18 12 2008 6 0 20002 10 07 01 2009 7 10 08 01 2009 8 0 14 01 2009 9 0 20000 10 15 01 2009 10 10 21 01 2009 11 0 22 01 2009 12 0 29 01 2009 13 1 0 30 01 2009 14 0 20000 10 04 02 2008 15 10 05 02 2009 16 0 11 02 2009 17 0 12 02 2009 18 0 20000 10 18 02 2009 19 0 20000 0 19 02 2009 20 0 20000 0 26 02 2009 21 0 20000 0 27 02 2009 22 0 19999 10 Highlighted yellow average value Highlighted green lowest value Highlighted blue highest value 740300_2011_936_21209885B_eng doc A TUVRheinland Precisely Right Seite 212 von 422 TUV Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 0 09280 Stability control filter Emfab 0 09260 XEVEuseyussate cLRLSR oe
253. ignal 132 6 11 2010 12 5 No ref measurement PM2 5 Repair leaking switching valve 133 6 12 2010 6 6 6 6 48 8 12 1 14 1 134 6 13 2010 9 7 9 9 55 8 16 7 18 1 135 6 14 2010 7 2 6 2 51 4 13 1 14 8 136 6 15 2010 2 9 3 1 30 2 9 7 11 9 137 6 16 2010 5 0 4 6 45 4 11 3 13 1 138 6 17 2010 4 1 4 5 57 6 10 3 10 1 139 6 18 2010 13 6 14 4 140 6 19 2010 3 7 3 4 38 1 9 1 11 8 141 6 20 2010 9 1 8 9 58 4 16 2 17 7 142 6 21 2010 7 5 7 3 20 6 18 8 PM10 Grubbs outlier 143 6 22 2010 4 9 6 3 41 9 19 7 16 8 144 6 23 2010 8 1 8 0 52 0 20 3 18 9 145 6 24 2010 6 9 6 3 58 5 16 8 16 4 146 6 25 2010 14 6 15 4 64 0 27 1 26 1 147 6 26 2010 20 9 20 1 70 1 35 3 35 2 148 6 27 2010 19 8 18 2 149 6 28 2010 10 4 9 3 22 0 21 4 PM10 Grubbs outlier 150 6 29 2010 4 9 4 7 53 3 11 1 10 9 740300_2011_936_21209885B_eng doc y T V Rheinland Energie und Umwelt GmbH TUV Rheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Page 180 of 422 Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Annex 5 Measured values from field test sites related to actual conditions Page 6 of 22 Manufacturer Thermo Fisher Scientific Suspended particulate matter PM10 Type of instrument TEOM 1405 F Measured values in yg m ACT Serial No SN 20006 am
254. igure 5 73 Select which analog output channel you want to calibrate Select the Next gt button Figure 5 73 Select Channel to Calibrate Select Channel to Calibrate screen Select the analog output channel you wish fo calibrate To complete ihe wizard make sure no channels are selected and click Hex Analog Cutput Channel 1 Analog Cutpat Channel 2 Analog Clana Channel 3 Analog Output Channel 4 Analog Output Channel 7 nalog Output Channel amp Analog Output Channel 7 Analog Output Channel E 5 58 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 7 The Select Analog Output Range screen will display Figure 5 74 Set the voltage range for the analog output Select the Next gt button Note Ensure that the voltage range selected for the analog output channel matches the jumper voltage setting for the analog output channel step 3 a Figure 5 74 select Analog Output Ran Select Analog Output B up Range screen 8 The Connect Meter screen will display Figure 5 75 Locate the test point Figure 5 70 for the analog output being calibrated and attach a voltmeter set to VDC to the test point and to the ground test point on the board Select the Next gt button Figure 5 75 Connect Meter Connect Meter screen THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 59 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 9 The Meas
255. ilter 193 3 8 2011 31 1 31 8 71 7 42 5 41 9 194 3 9 2011 19 1 18 8 63 9 28 6 28 9 195 3 10 2011 Power cut complete 196 3 11 2011 16 7 16 1 49 2 29 9 31 5 197 3 12 2011 30 6 33 0 198 3 13 2011 13 3 13 1 83 0 15 0 15 4 199 3 14 2011 18 2 20 0 71 5 Power cut only Thermo 200 3 15 2011 37 4 37 8 86 3 44 1 44 8 201 3 16 2011 66 2 68 1 PM2 5 Grubbs outlier 202 3 17 2011 50 7 49 6 74 1 67 1 68 4 203 3 18 2011 28 4 28 1 73 5 37 3 38 3 204 3 19 2011 18 4 19 1 205 3 20 2011 20 4 20 3 72 0 27 3 28 7 206 3 21 2011 22 4 22 3 64 8 34 3 31 4 207 3 22 2011 41 7 41 6 75 4 54 7 50 3 208 3 23 2011 20 3 20 4 63 0 31 8 29 3 209 3 24 2011 18 6 20 2 58 7 33 9 32 9 210 3 25 2011 27 6 27 5 74 2 37 5 38 8 740300_2011_936_21209885B_eng doc y T V Rheinland Energie und Umwelt GmbH TUV Rheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Page 182 of 422 Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Annex 5 Measured values from field test sites related to actual conditions Page 8 of 22 Manufacturer Thermo Fisher Scientific Suspended particulate matter PM10 Type of instrument TEOM 1405 F Measured values in yg m ACT Serial No SN 20006 amp SN 20107 No Date Ref 1 Ref 2 Ref 1 Ref 2 Ratio SN 20006 SN 20107 Rem
256. imum requirement fulfilled yes 6 6 Detailed representation of the test results Table 17 contains the determined values for the zero point and the calculated deviation refer ring to the previous value and the start value in ug m Figure 30 to Figure 31 show the graphical representation of the zero point drift over the test period In Table 18 the deviations of the measured values are shown in of the respective previous value Figure 32 and Figure 33 show the graphical representation of the drift of the meas ured values referring to the previous value 740300_2011_936_21209885B_eng doc a s T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 104 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Table 17 Zero point drift SN 20006 amp SN 20107 with zero filter o SN 20006 SN 20107 Measured Deviation Deviation Measured Deviation Deviation value from from start value from from start previous value previous value value value Not yet oper 06 12 2009 ating Not yet oper 07 12 2009 1 4 1 4 1 4 ang ewan or os 07 3 mon or ot o a 07 03 2010 47 18 12 12 26 04 2010 01 o6 01 14 7 05 Rejected due orano os os o o e o fo oos 2901 2011 15 10 15
257. in place Note Do not overtighten the filter holder The O ring creates the seal not the force of the turn a 8 Close the small filter door THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 17 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Cleaning the The PM 10 inlet should be cleaned every time the TEOM filter is changed PM 10 Inlet oras necessary To clean the unit you will need an ammonia based general purpose cleaner cotton swabs a small soft bristle brush paper towels distilled water silicone based stopcock grease a small screwdriver a small adjustable wrench and a pocket knife To clean maintain the PM 10 inlet 1 Remove rain jar from the inlet and the inlet from the sample tube Unscrew the top acceleration assembly from the lower collector assembly Figure 5 23 Figure 5 23 Top of inlet assembly Top plate Lower plate O ring Nozzle 2 Mark the top plate deflector cone and lower plate with a pencil to facilitate proper orientation when reassembling then use a Phillips screwdriver to remove the four pan head screws from the top of the top plate Figure 5 23 Lift the top plate off the four threaded spacer standoffs and set aside 3 Clean the insect screen with brush or water then dry 4 Using a general purpose cleaner and paper towel clean the deflector cone on the inside of the top plate 5 18 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AN
258. ing the Valve Cleaning Wizard screen Cleaning Wizard The Vale Cleaning Wizard has completed sucematulhy The iestrument will be put in Run mede when this wizard bs finished T close this wizard prese Finish THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 37 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Aud it Calibration Thermo Fisher Scientific recommends the following regular maintenance Procedures ptocederes for the TEOM 1405 F 5 38 Operatine Guine TEOM 1405 F Ambient temperature Audit calibrate the ambient air temperature Ambient pressure Flow Leak check Analog outputs Mass transducer measurement once per month The temperature must be calibrated before a flow calibration Audit calibrate the ambient pressure measurement once per month The pressure must be calibrated before a flow calibration Audit calibrate the main and bypass flows once a month Perform a leak check once a month or as necessary refer to Section 3 for leak check instructions Calibrate the analog output channels once a year or as necessary for example any time the voltage range setting is changed Audit the calibration of the mass transducer once a yeat THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES The TEOM 1405 software allows users to step through the standard calibration and audit procedures Select the Service button to display the Service screen When in the S
259. ing to the general relation y m x b with i candidate 1405 F 6 5 Assessment The reference equivalence functions lay within the limits of the respective acceptance range Furthermore the variation coefficient R of the calculated reference equivalence functions in the relevant concentration range for the data sets All data set Teddington Winter and Cologne Winter is 2 0 95 For the data sets Teddington Summer and Bornheim Sum mer the variation coefficient is lt 0 95 Both test sites are characterized by a low variation of 740300_2011_936_21209885B_eng doc a s T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 116 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B the particulate concentrations The equivalence test according to 6 1 5 4 10 Calculation of the expanded uncertainty of the instruments is fulfilled nevertheless for all test sites Minimum requirement fulfilled no Detailed representation of the test results The results of the regression analysis are summarized from Table 19 to Table 20 The graph ical representations are shown from Figure 34 to Figure 43 Next to the regression line the diagrams show an image of the ideal curve y x and the two sided acceptance r
260. inimum requirement 6 3 Performance of test The test was carried out at four different sites during field test Different seasons and varying concentrations for PM19 were taken into consideration Of the complete data set at least 20 of the concentration values determined with the ref erence method shall be greater than the upper assessment threshold according to 2008 50 EC 7 For PM the upper assessment threshold is at 28 pg m At each test site at least 40 valid data pairs were determined Of the complete data set 4 test sites 237 valid data pairs for SN 20006 230 valid data pairs for SN 20107 in total 23 3 of the measured values are above the upper assessment threshold of 28 g m for PM1o The measured concentrations were referred to ambient conditions 6 4 Evaluation According to Point 9 5 2 1 of the Guide Demonstration of Equivalence of Ambient Air Moni toring Methods applies The uncertainty between the candidates up must be lt 2 5 ug m An uncertainty of more than 2 5 ug m between the two candidates is an indication that the performance of one or both systems is not sufficient and the equivalence cannot be declared The uncertainty is determined for e All test sites together complete data set e 1 data set with measured values 2 30 ug m for PM Basis averages reference measurement 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precis
261. instruments that were saved in that configuration a 3 24 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 3 Basic OPERATION Setting Up for Data can be manually downloaded from the TEOM 1405 monitor through Manual Data Downloads the built in Ethernet connection using the ePort software To set up the software to manually download data 1 Ensure that the PC and the instrument are connected to the same network using the Ethernet connection on the back of the instrument Refer to the previous section for information on connecting the instrument to a network 2 Use the ePort PC software to connect to the instrument and display the ePort Main screen Figure 3 28 Refer to the previous two sections for information on connecting to the instrument or instruments Figure 3 28 ePort Main screen 1405200100605 DichotFDMS Serial Herbert 14064200100605 IP Address 10 210 96 145 States Ative Cormmaancs Downined Detade Ay Dorica Date s L Last download 2 Rewate reat ace Deor gt Upgrade uetrumert Proeaee Ag Coemioad Sonu oee ee Lest Downiosd of Selected Date and Tine Next desendowd will start with dete alter 3i Jon 207 Ce 2 20 ear THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 3 25 Section 3 Basic OPERATION 3 Select Download Setup in the Commands window of the ePort Main screen The Download Setup Wizard will display Figure 3 29 Select the Next gt button Figur
262. ion of the 2 digit Channel Number for example K0 075 048 The Channel Number is always 2 digits in length Ro Fates codes 013 and 010 are appended to the response Enter 0 if nothing is to be appended COCO fe veer erm bemmion e Set Function command where xx represents a 2 digit code between 00 and 32 These codes are defined below 13010 Optional Up to 3 ASCII codes can be added to response from the instrument In this case lt CR gt and lt LF gt ASCII 4 digit Set Function command with the 2 digit xx code corresponding to the function that was set 2 digit Channel Number as defined Number of current status conditions of current status conditions e C Upto 3 digits appended to the end of the response transmission according to the entry for RS Para 3 LISTING OF FUNCTION CODES xx lt Run gt lt Data Stop gt lt F1 gt lt F5 gt lt Stop All gt Ensure that the instrument is in the Stop Mode Set Time Transmit the proper values in PRCs 2 through 6 Execute the SF26 command THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F B 7 Appenpix B SERIAL COMMUNICATION AK Protocol Ask Storage Command ASTO COM 2 WAY SETTINGS RS Para 1 ASCII code for the 1 digit Station Number for example 4 052 The Station Number is always 1 digit in length RS Para 2 75048 ASCII code representation of the 2 digit Channel Number for example K0 075 048 The Channel Number is
263. ior to installation Figure shows PM 10 inlet only Height of PM 10 inlet is the same for PM 2 5 and PM 1 a Figure 2 12 Inlet installed Inlet entrance 1 8 to 2 1 m above the roof Inlet Flow splitter 7 Center the tripod over the roof hole Measure and cut the sample tube extensions from the top of the instrument through the roof and connect to the flow splitter sample tube Make sure to clean and deburr the cut ends of the sample tube extensions 2 12 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 2 SETUP AND INSTALLATION 8 Connect the green bypass tubing the other end is attached to the coiled tubing of the water trap filter to the bypass fitting on the flow splitter using the 3 8 inch Swagelok fitting Figure 2 13 Note Ensure that the coiled tubing connected to the water trap filter is mounted vertically so condensed water will drip into the water trap filter a Figure 2 13 Bypass tubing and sample tubes installed Bypass connection Flow splitter extension tube THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 2 13 Section 2 SETUP AND INSTALLATION 9 Locate the ambient temperature and humidity sensor Connect the sensor to the flow splitter using the U bolt provided with the system Figure 2 14 10 Attach the sensor cable to the sensor and run the sensor cable to the instrument through an opening in the roof or through a window Attach the sensor to the sensor connection on t
264. irections and recommendations 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 168 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Further maintenance works The following works are necessary in addition to the regular works in the maintenance inter val Every 6 months or when necessary the Inline filter for PM1o and Bypass path shall be changed to avoid a contamination of the flow rate regulator Once a year or when necessary the cooler the switching valve and the air inlet system are to be cleaned Once a year the calibration of the mass measuring transducer is to be checked us ing the Ko test kit The dryer inside the FDMS unit has to be change or refurbished once a year or when necessary For the monitoring securing of a correct dryer performance the manufacturer recommends to observe the pump vacuum nominal gt 510 mm Hg and the dew point of the air flow nominal lt 2 C at 4 C cooler temperature and periodically perform a zero point test operation of the measuring device with zero filter at the entrance Every 18 months or when necessary the sampling pump must be maintained or renewed Further details are provided in the user manual
265. irement fulfilled yes 6 6 Detailed representation of the test results Table 15 shows the summarized representation of the test results Table 15 Dependence of the measured value of the mains voltage deviation in Mains voltage Deviation SN 20006 SN 20107 Ko Start voltage End voltage Ko The single values can be taken from annex 4 of the appendix 740300_2011_936_21209885B_eng doc TUVR h T V Rheinland Energie und Umwelt GmbH ein and Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 98 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 1 5 3 9 Cross sensitivity The change in the measured value caused by interfering components in the sample gas shall not exceed the requirements of Table 2 of Standard VDI 4202 Part 1 September 2010 at zero and reference point Note This point is not relevant for particulate measuring devices The minimum requirement 5 4 5 is valid Therefore the results of this test can be found in module 5 4 5 6 2 Equipment Not applicable 6 3 Performance of test Not applicable 6 4 Evaluation Not applicable 6 5 Assessment Not applicable Minimum requirement fulfilled 6 6 Detailed representation of the test results Not applicable 740300_2011_936_21209885B_eng doc TUV
266. is averaging time 6 2 Equipment For the test a clock was provided 6 3 Performance of test It was tested if the AMS allows the formation of daily averages 6 4 Evaluation The FDMS unit of the AMS switches alternately every 6 minutes between the operating modi base mode and reference mode to take into account the amount of semi volatile particle matter see as well point 3 2 On the basis of the determined mass concentration in the base mode and the respective following reference mode the expended mass concentration is determined Example The device collects for 6 minutes in the base mode and determines a base mass concen tration of 5 ug m Afterwards the device collects for 6 minutes in the reference mode and determines a reference mass concentration of 1 ug m The expended mass concentration amounts therefore to 5 g m 1 ug m 6 ug m The actual available sampling time base mode per measuring cycle therefore is exactly 50 of the total cycle The results of the field tests according to 6 1 5 4 10 Calculation of the expanded uncertainty of the instruments in this report show that for this instrument configuration a comparability of the candidates could be demonstrated securely with the ref erence method and the formation of daily averages therefore is possible securely 6 5 Assessment The formation of valid daily averages is possible Minimum requirement fulfilled yes 6
267. ition the instrument starts collecting first data Collecting Data This data is not yet used to determine mass concentration The collecting of first data is followed by first data computation Computing Data Afterwards the instrument is fully operational Fully operational The intermediate steps Collecting Data and Computing Data take one hour After that the instrument deliv ers the moving 1h average values of the mass concentration which are updated every 6 minutes If required possible changes of the basic parameterization of the measuring system can likewise be performed within few minutes by personal familiar with the devices However the measuring operation is for this purpose interrupted and the instrument switched in setup mode 6 5 Assessment The setup and warm up times were determined The measuring system can be operated at different measurement test sites with manageable effort The set up time is approximately 2 hours and the warm up time is depending on the necessary stabilizing time 1 5 to 2 5 hours Minimum requirement fulfilled yes 6 6 Detailed representation of the test results Not required for this test 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH F Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator
268. l settings It calculates mass concentration mass rate and the total mass accumulation on the TEOM filter under the following conditions Flow rate through sample inlet 16 7 1 min 1 m hr Main sample flow rate 3 l min Temperature of sample stream 30 C Particulate matter mass concentration less than 5 ug m to several g m Operatine Guine TEOM 1405 F 1 5 Section 1 INTRODUCTION Theory of Operation 1 6 Operatine Guine TEOM 1405 F The TEOM 1405 F Monitor is a true gravimetric instrument that draws ambient air through a sample filter at constant flow rate continuously weighing the filter and calculates the near real time mass concentration of the collected particulate matter In addition the instrument computes the 1 hour 8 hour 12 hour and 24 hour averages of the mass concentration Utilizing the FMDS allows the TEOM 1405 F to provide representative measurement of the particulate matter PM mass concentration as it exists in the ambient air The FDMS unit automatically generates mass concentration measurement ug m that account for both nonvolatile and volatile PM components To accomplish this the FDMS unit constantly samples ambient air and using a switching valve to change the path of the sample flow automatically compensates for the semi volatile faction of the collected sample Every six minutes the switching valve alternates the sample flows between the base and reference sample periods During the ba
269. later in this section for more information on selecting storage variables If you will be setting up the unit to receive an analog input to transmit analog outputs or setting up the unit s contact closure circuits refer to Section 4 for information on the screens and settings used for these parameters If you will be using the password function to control access to the unit s operation refer to Section 4 for information on setting up the password function THERMO FISHER SCIENTIFIC Section 3 Basic OPERATION 11 Select the TEOM Data button to display the TEOM Data screen The instrument will begin collecting data when the mode status window displays a Fully operational message Note Upon initial instrument start up the values in the mass concentration fields are the running averages that are accumulated until a 1 hour time period has passed The values are visible to provide the user with an indication that the instrument is functioning after instrument power up or reset These raw values are used for internal calculations only a THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 3 3 Section 3 Basic OPERATION Perfo rming The TEOM 1405 F should be leak checked once a month or as needed Leak Check The system comes with flow audit leak check adapter for the 1 1 4 inch flow splitter and the 3 8 inch bypass line The Leak Check Wizard compares the measured difference between the units zero flow with t
270. lect the Finish button to exit the wizard and return to the Verification screen or select the lt Back button to move backward one step in the procedure Figure 5 60 Finish screen with flow audit Completing the Flow Audit results Wizard To complete the audit remove the Flew Audit Device Main Gow percent error 5 Bypass flow percent error Ei The instrument will be putin Run mede when this wizard is finished To close thie witard press Finish lt x Back Finish Figure 5 61 Finish screen with a failed audit Completing the Flow Audit Wizard The Flee Audit Wizard was wrsuecesstul because one or more of the threes drifted by more than 10 percent simce the lat calibration Please consult the service manual ter froublesheeoting Instrections Te comete the audit remove the Flow Audit Device Moin Bys percent eror 176Z Bypass flow peroen error 35E T close this wizard prese Finish THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 49 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Calibrating the Perform the ambient air temperature calibration pressure calibration and Flow Rates leak check Section 3 before executing the flow calibration procedure To calibrate or audit the main and bypass flows you will need a 1 1 4 inch flow adapter a 3 8 inch Swagelok flow adapter and a flow measutement device The reference flow meter such as a bubble meter dry gas meter or mass flow meter should ha
271. leting the Analog Output Calibration Wizard screen will display Figure 5 78 Select the Finish button to exit the wizard and return to the Verification amp Calibration screen or select the lt Back button to move backward one step in the procedure Completing the Analog Output Calibration Wizard The Analog Guiput Wizard has completed sucessfully When the wizard is finished the results of ihe calbrailon will be applied Toe close this wizard press Finish Operatine Guine TEOM 1405 F 5 61 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Verifying the Calibration Constant 5 62 Operatine Guine TEOM 1405 F The calibration of the mass transducer in the TEOM 1405 Monitor is determined by the mass transducer s physical mechanical properties Under normal circumstances the calibration does not change materially over the life of the instrument Contact Thermo Scientific if the results of the verification procedure fails You can locate the original calibration constant on the Instrument Checkout Record or the Final Test Record documents that are shipped from the factory with the instrument Before the TEOM 1405 is shipped to the customer it is calibrated with a new pre weighed TEOM filter installed in its mass transducer as a calibration weight Because the mass of the filter cartridge with particulate matter differs from the mass of a new filter cartridge by only a small fraction calibrating the system with a calib
272. ll hour 12 Hr MC moving 12h average updated every 60 minutes every full hour 24 Hr MC moving 24h average updated every 60 minutes every full hour 6 5 Assessment The measuring device comprises a measured value display Minimum requirement fulfilled yes 740300_2011_936_21209885B_eng doc ss TUV Rheinland Energie und Umwelt GmbH TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 62 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 6 Detailed representation of the test results Figure 27 shows the user s display with the current measured concentration values Figure 27 Display of the measured concentration value 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 63 0f422 6 1 4 1 2 Easy maintenance Necessary maintenance for the measuring systems should be possible without larger effort if possible from outside 6 2 Equipment No additional equipment required 6 3 Performance of test Necessary regular maintenance
273. logne Winter 57 Grubbs test results for the PM reference method Bornheim Summer 58 Display of the measured concentration value eeseeseseeeeeeeeseseerrrrresssrrrrenn 62 View on rear of the device TEOM 1405 F Ambient Particulate Monitor 72 Display of the software version here 1 51 in the menu System Status 84 Zero point drift SN 20006 measured Component PMig cccceeceeseeeeeeeeeeeeees 105 Zero point drift SN 20107 measured component PM o ccceeeeeeeeeeeeeees 105 Drift of the measured value SN 20006 measured component PM p 0 107 Drift of the measured value SN 20107 measured component PM p 6 107 Reference equivalence function SN 20006 test site Teddington Winter 117 Reference equivalence function SN 20107 test site Teddington Winter 117 Reference equivalence function SN 20006 test site Teddington Summer 118 Reference equivalence function SN 20107 test site Teddington Summer 118 Reference equivalence function SN 20006 test site Cologne parking lot 119 Reference equivalence function SN 20107 test site Cologne parking lot 119 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH F Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the com
274. low Control Scree innne aea Eaa dar aT TREE E 4 15 Instrument Temperatures Seretse siiin irinn 4 18 Arialog Tnputs Gi i ns fas ccs Sata tas cntedeckevddnncavscunevade estenaattatevesteeserceoeaneees 4 19 THERMO FISHER SCIENTIFIC Operatinc Guipe TEOM1405 F IX Preface FDMS Module Sereen sivacinivawessnisntesaivensniseavodavcastn intssacn casassanduiancvanesoveninias 4 20 FDMS Cooler Temperature Semin oasis sssssciniesisavnstancsvantaaesescanieieaaanisns 4 21 DRUGS SOLE aiiiar nenies aieeaii aiSia 4 22 Syster Vag crete scng set na vgtinu sect tvaasine needs neat vedina oa SEAE o ES TONE REN Srana 4 24 Analog amp Digital Outputs Screen cssssssssscastensavsssrasesnsenavenvesinsstenrevestoens 4 26 Analog COMES Serei sasscavesacacsdsanscedevedusnnesseseuadeacdoraneanasinslnsanetiasuaaonnten 4 27 C ntact Clos te SCrECN rrean ar n aae T aE 4 28 KEPAN a T seisnen aieaddeentsedtceatocusubisuancnive 4 29 Settings Adyanced DORE sun tucrnenlatarstunrneiuienihsaantinndansatenaieaiiasitexapnaaasis 4 30 Seryice SGr fi senemi ia a E TES 4 32 Tnstument Control SLCC isendi saesae er ii ori diniin 4 34 Service Advanced Sree sisscsesraisssisvcrsssaiventsocesatitneseaoconnansesniaecnnanranereantvned 4 35 Tastalling New FiItNWATE isiin nran 4 36 Section5 Maintenance and Calibration Procedures ssssssssssssssesseesseens 5 1 FST VRS th CB niisiis sssrini pate napanarens avnesvaueevacteavesaeonepmaeaaraes 5 1 M int nance Wizards sicciss assitranes
275. lter loads up to gt 50 were recorded in the candidates and the flow rates were evaluated on a 24 h basis 6 4 Evaluation From the determined average for the flow rate average standard deviation and maximum and minimum value were defined 740300_2011_936_21209885B_eng doc a s T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 134 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 5 Assessment The results from the performed flow rate checks before each field test site are represented in Table 26 Table 26 Results control flow rate Flow rate check before SN 20006 SN 20107 l min Deviation l min Deviation Test site from nominal from nominal value value Teddington Winter PM 3 02 0 67 3 02 0 67 Total 16 61 0 36 16 77 0 60 Teddington Summer PM 3 14 4 66 3 07 2 33 Total 17 35 4 08 16 96 1 74 Cologne Winter PM 2 96 1 33 3 05 1 67 Total 16 40 1 62 16 22 2 70 Bornheim Summer PM 3 08 2 67 2 80 6 67 Total 16 73 0 36 16 73 0 36 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring sy
276. mA to 20 mA 6 2 Equipment PC with software ePort 6 3 Performance of test The test was carried out using a PC with the software ePort via Ethernet The AMS was connected to a PC via Ethernet and the data were downloaded As usual the data was in parallel downloaded to an USB stick via USB interface The test was performed by comparing both data The AMS has the possibility to offer analogue signals maximum 8 analogue exits as well as to offer measuring signals communication via serial interface RS 232 AK protocol software e g RPComm or HyperTerminal 6 4 Evaluation The measured signals are offered at the rear side of the instrument in the following way Analogue 0 1 resp 5 V concentration range selectable Digital Ethernet with Software ePort RS 232 interface AK protocol USB The transmitted measured values via Ethernet comply with the data downloaded via USB interface 6 5 Assessment Measured signals are offered analogue 0 1 or 5 V and digital via Ethernet RS 232 UBS The connection of additional measuring and peripheral devices to the respective ports of the devices is possible e g analogue entrances Minimum requirement fulfilled yes 740300_2011_936_21209885B_eng doc n TUV Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor
277. mass system if additional mass is added the frequency of the oscillation decreases This can be seen by observing the frequency on the display of the TEOM 1405 unit Section 4 and operating the monitor both with and without a filter in place In a spring mass system the frequency follows the equation f K 7 M where f frequency K spring rate M mass K and M are in consistent units The relationship between mass and change in frequency can be expressed as where 1 1 dm K 3 T f fo dm change in mass K spring constant including mass conversions i initial frequency Hz f final frequency Hz THERMO FISHER SCIENTIFIC THERMO FISHER SCIENTIFIC Section 1 INTRODUCTION When this equation is rearranged you can solve for the spring constant K dm K _ ft i Thus K the calibration constant for the instrument can be easily determined by measuring the frequencies with and without a known mass pre weighed TEOM filter cartridge Operatine Guine TEOM 1405 F 1 9 Section 1 INTRODUCTION Mass Flow Controllers 1 10 Operatine Guine TEOM 1405 F The mass flow controllers MFCs in the TEOM 1405 Monitor are internally calibrated for a standard temperature and pressure of 25 C and 1 Atmosphere 1013 2 millibars or 760 mm Hg The system can operate on Active or Passive flow to maintain constant volumetric flow at sample inlet For passive flow control the user must en
278. matter PM10 Type of instrument TEOM 1405 F Measured values in yg m ACT Serial No SN 20006 amp SN 20107 No Date Ref 1 Ref 2 Ref 1 Ref 2 Ratio SN 20006 SN 20107 Remark Test site PM2 5 PM2 5 PM10 PM10 PM2 5 PM10 PM10 PM10 ug m ug m ug m yg m ug m ug m 9 57200 es i 1424 15 Teddington 92 5 2 2010 8 6 8 7 Summer 93 5 3 2010 13 6 12 7 94 5 4 2010 8 5 8 6 56 7 15 0 14 8 95 5 5 2010 14 0 13 9 72 5 20 0 19 9 96 5 6 2010 9 8 9 2 58 0 16 6 16 2 97 5 7 2010 7 8 7 7 59 8 14 4 13 6 98 5 8 2010 4 5 4 2 48 5 9 9 10 0 99 5 9 2010 6 5 7 6 50 4 14 6 13 8 100 5 10 2010 4 9 5 1 49 7 11 8 12 5 101 5 11 2010 6 2 6 0 60 1 12 2 12 0 102 5 12 2010 8 4 8 3 67 5 13 6 12 9 103 5 13 2010 13 4 13 2 77 7 17 3 17 5 104 5 14 2010 12 7 13 7 69 9 19 2 19 1 105 5 15 2010 7 0 6 7 54 0 13 8 12 9 106 5 16 2010 5 6 5 2 56 4 11 4 11 3 107 5 17 2010 10 2 10 3 62 5 18 2 17 3 108 5 18 2010 12 7 13 4 60 8 21 4 22 8 109 5 19 2010 14 0 15 2 74 2 21 5 21 8 110 5 20 2010 13 9 14 7 75 9 24 0 23 1 111 5 21 2010 14 3 15 5 81 7 20 7 21 6 112 5 22 2010 6 4 6 2 70 3 10 5 12 1 113 5 23 2010 5 6 5 7 60 0 12 8 12 5 114 5 24 2010 12 0 12 4 69 7 19 5 19 7 115 5 25 2010 6 1 6 9 42 4 16 9 17 8 116 5 26 2010 9 7 9 2 49 8 Zero filter 117 5 27 2010 7 3 7 3 92 3 Zero filter gt Inlet 118 5 28 2010 8 2 8 2 57 7 15 0 SN 20006 noisy signal 119 5 29 2010 5 0 4 9 46 1 11 2 SN 20006 noisy signal 120 5 30 2010 4 0 3 9 48 9 9 7 SN 20006 noisy signal
279. may be precut The typical setup has 5m of tubing for the pump and 10m for the bypass line 2 Locate the sample pump in a location to minimize vibrations effecting the instrument Push the one end of the 5m pump tubing into the fitting on the vacuum pump Figure 2 2 Figure 2 2 Vacuum pump 3 Push the other end of the 5m length of pump tubing into the pump connection on the back of the TEOM 1405 unit Figure 2 3 Figure 2 3 Back of TEOM 1405 unit To water trap filter Pump connection Bypass filter 2 4 Operatine Guipe TEOM 1405 F THERMO FISHER SCIENTIFIC Section 2 SETUP AND INSTALLATION 4 Mount the water trap filter assembly near the 1405 unit Figure 2 4 The water trap should be mounted at the low point of the tubing to the instrument Figure 2 4 Water trap filter assembly Quick connect fitting Water trap filter Note Drain the water trap as needed a 5 From the 10m length of tubing for the bypass line cut a piece of tubing long enough to reach from the water trap filter to the bypass filter on the back of the 1405 unit Figure 2 3 and 2 4 Install the tubing into the quick connect fittings on the water trap filter and bypass filter 6 Insert one end of the remaining section of bypass tubing into the quick connect fitting at the end of the coiled piece of tubing connected to the water trap filter Note The other end of the bypass tubing will be connected to the bypass connection on t
280. mber 2010 For PM Change in measured value at B maximum Bo within the volt age interval 230 15 20 V 740300_2011_936_21209885B_eng doc For particulate measuring devices for PM10 this test shall be performed ac cording to minimum requirement 5 4 2 Equivalency of the sampling sys tem Not applicable Not applicable The permitted surrounding tempera ture at the test site of the measuring device pursuant to the manufacturer is 8 C to 25 C When observing the values output by the device a maxi mum influence of the surrounding temperature on the zero point of 2 3 ug m in the range 8 C to 25 C could be detected At reference point no deviation gt 0 4 to the default value at 20 C could be observed Due to voltage changes no deviation gt 0 4 could be detected for PM10 referring to the standard value of 230 V TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B filled 5 3 9 Cross sensitivity The change in the measured value caused by interfering components in the sample gas shall not exceed the require ments of Table 2 of Standard VDI 4202 Part 1 September 2010 at zero and reference point Pa
281. mbers The decimal number reported by the unit must be compared to the list of status codes Table A 1 If the exact decimal code does not appear in the list multiple status codes are present and the decimal must be converted to hexadecimal number in order to determine which codes are being reported by the unit Note The status code list in this section Table A 1 shows codes for both single and dual 1405 systems as well as those equipped with the FDMS system a Operatine Guipe TEOM 1405 F A 1 Appendix A Troubleshooting Table A 1 1405 DF Status Codes A 2 Code Warning Decimal Reason for warning 0x40000000 RH High Side A 1 073 741 824 gt 98 0x20000000 Dryer A 536 870 912 gt 2 0x10000000 Cooler A 268 435 456 gt 0 5 C deviation 0x08000000 Exchange Filter A 134 217 728 gt 90 0x04000000 Flow A 67 108 864 gt 10 deviation 0x02000000 Heaters Side A 33 594 432 gt 2 deviation 0x01000000 Mass Transducer A 16 777 216 frequency lt 10 Hz 0x00400000 RH High Side B 4 194 304 gt 98 0x00200000 Dryer B 2 097 152 gt 2 0x00100000 Cooler B 1 048 576 gt 0 5 C deviation 0x00080000 Exchange Filter B 524 288 gt 90 0x00040000 Flow B 262 144 gt 10 deviation 0x00020000 Heaters Side B 131 072 gt 2 deviation 0x00010000 Mass Transducer B 65 536 frequency lt 10 Hz 0x00004000 User 0 Device 16 384 0x00002000 FDMS Devi
282. mends that you use the vacuum pump provided with the unit If you choose to install a different pump it must be oil free and able to maintain a 21 Hg vacuum at a flow of 16 67 I min a Figure 2 30 Outdoor enclosure with inlet installed THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 2 25 Section 2 SETUP AND INSTALLATION 2 26 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section3 Basic Operation This section describes the steps to begin data collection with the TEOM 1405 F monitor as well as leak check the instrument and download data The instrument will not begin collecting data until the operating mode message in the status bar reads Fully Operational Figure 3 1 Users must install clean conditioned filters in the unit prior to sampling Users can select flow rate data and other settings while waiting for the unit to become fully operational Figure 3 1 TEOM Data screen with TEOM 1405 F Fully Operational message TEOM Data System Status MC ipyimie hin WC nig 1 Hr ME ug B Hour value pagim fc Instrueteent 12 Hr Bet pgm Conditions z4Hr MC jugis Filter loading Settings Fraguamey Hoi ai Fuly eparina Morena elaliurs Ei OFZAOOF Ti Status bar THERMO FISHER SCIENTIFIC Operatinc Guine TEOM 1405 F 3 1 Section 3 Basic OPERATION Starting the Instrument 3 2 Operatinc Guipe TEOM 1405 F To program the instrument and begin collecting data
283. minute base MC This field contains the mass concentration value recorded by the TEOM filter while the FDMS system draws dried ambient ait base flow through the sample flow lines This value is a rolling 30 minute average updated every 6 minutes 30 minute reference MC This field contains the mass concentration value recorded by the TEOM filter while the FDMS system draws dried filtered and cooled ambient air reference flow through the sample flow lines This value is a rolling 30 minute average updated every 6 minutes THERMO FISHER SCIENTIFIC FDMS Cooler Temperature Setting THERMO FISHER SCIENTIFIC Section 4 SCREENS AND SETTINGS e Dryer temperature This field contains the dryer temperature of the flow channel Dryer dew point This field contains the current dew point of the air stream exiting the dryer of the flow channel e Dryer relative humidity This field contains the current relative humidity of the air stream exiting the dryer of the flow channel e Current valve position This field contains the current valve position base or reference Select the Cooler temp button to change the temperature C of the FDMS cooler The default settings for the FDMS cooler temperatures are 4 C If the dewpoint of the sample gases are greater then 2 C a status warning will occur Under this condition check and verify the performance of the sample dryers Under certain ambient conditions the capability of the
284. ms to the requirements of Standard EN 14907 The filters used in the field test are weighed manually The filters including control filters are placed on sieves for the purpose of conditioning to avoid overlap The specifications for pre and post weighing are specified beforehand and conform to the Standard Before sampling pre weighing After sampling post weighing Conditioning 48 h 2 h Conditioning 48 h 2h Filter weighing Filter weighing Re conditioning 24 h 2 h Re conditioning 24h 2h Filter weighing and immediate packaging Filter weighing The balance is always kept ready for use An internal calibration process is started prior to each weighing series The standard weight of 200 mg is weighed as reference and the boundary conditions are noted if nothing out of ordinary results from the calibration process Deviations to prior measurements conform to the Standard and do not exceed 20 ug refer to Figure 75 All six control filters are weighed afterwards and a warning is displayed for control filters with deviations gt 40 ug during evaluation These control filters are not used for post weighing Instead the first three acceptable control filters are used while the others remain in the protective jar in order to replace a defective or deviating filter if necessary Figure 76 shows an exemplary process over a period of more than 4 months All filters which deviate more than 40 ug between the first and sec
285. multaneous operation of all measuring channels 740300_2011_936_21209885B_eng doc aT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 28 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 2 Task definition 2 1 Type of test Thermo Fisher Scientific has commissioned TUV Rheinland Energie und Umwelt GmbH with the performance of a suitability test of TEOM 1405 F Ambient Particulate Monitor with PM pre separator The test was conducted as a complete suitability testing 2 2 Objective The AMS shall determine the content of PM25 suspended particulate matter in ambient air within the concentration range of 0 to 1000 ug m The suitability test was carried out based on the current standards for suitability tests while taking into account the latest developments The test was performed in consideration of the following standards e Standard VDI 4202 Part 1 Minimum requirements for suitability tests of automatic ambient air measuring systems Point related measurement methods of gaseous and particulate pollutants September 2010 or June 2002 1 e Standard VDI 4203 Part 3 Testing of automatic measuring systems Test proce dures for point related ambient air quality measuring system
286. mum requirements for suitability tests of automatic ambient air measuring systems General parameters for the related tests are given in Standard VDI 4203 Part 1 Testing of automatic measuring systems General concepts of October 2001 and furthermore specified in VDI 4203 Part 3 Testing of auto matic measuring systems Test procedures for point related ambient air quality measuring systems of gaseous and particulate pollutants of August 2004 The fulfilment of the require ments from VDI standards is mandatory in Germany Standard VDI 4202 Part 1 and VDI 4203 Part 3 were republished after an extensive revision with latest update September 2010 Unfortunately after this revision uncertainties and con tradictions remain regarding the concrete minimum requirements on the one hand and the general relevance of the test points on the other hand while testing particulate ambient air measuring devices The following test points require clarification 6 1 5 3 2 Repeated standard deviation at zero point no minimum requirement defined 6 1 5 3 3 Repeated standard deviation at reference point not relevant for particulate devices 6 1 5 3 4 Linearity Lack of fit not relevant for particulate devices 6 1 5 3 7 Sensitivity coefficient of the surrounding temperature no minimum requirement defined 6 1 5 3 8 Sensitivity coefficient of the electric voltage no minimum requirement defined 6 1 5 3 11 Standard deviation from paired measur
287. n or red colour Furthermore the five criteria from chapter 6 1 Methodology of the equivalence check are taken into account the related cells are highlighted in colour 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Table 31 23 3 gt 28 ug m3 PM10 1405F FOMS Orthogonal Regression A TUVRheinland Betw een Instrument Uncertainties WCM All Data lt 30 ug m3 gt 30 ug m3 SN 20006 Dataset Teddington Summer Cologne Winter Individual Datasets Bornheim Summer Teddington Winter nc s r2 Slope b ub 169 0 882 1 055 0 028 46 0 963 0 992 0 029 Intercept a ua 0 567 0 501 0 218 1 274 Orthogonal Regression Reference Candidate Limit Value of 50 ug m3 nc s r2 Slope b ub 0 895 1 112 0 987 0 992 0 931 1 134 0 987 0 959 Intercept a ua 0 055 0 883 0 327 0 461 2 097 0 750 1 549 0 337 WCM gt 28 ug m3 3 6 16 7 lt 30 ug m3 0 860 1 069 1 377 0 528 2 2 Precisely Right Page 151 of 422 Overview equivalence test TEOM 1405 F Ambient Particulate Monitor for PM10 Criterion 1 Criterion 2 Criterion
288. nce point drift SN 20107 t Dev KO value permissible dev Deviation from previous value Figure 33 Drift of the measured value SN 20107 measured component PM 19 740300_2011_936_21209885B_eng doc aT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 108 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 1 5 3 13 Short time drift The short term drift at zero point and reference point shall not exceed the requirements of Table 2 of Standard VDI 4202 Part 1 September 2010 within 12 h for benzene 24 h in the laboratory test and within 24 h in the field test A value ct at 70 to 80 of the upper limit of the certification range shall be used as reference point Note According to the decision of the competent German body see module 5 3 1 this test point is not relevant for particulate measuring devices 6 2 Equipment Not applicable 6 3 Performance of test Not applicable 6 4 Evaluation Not applicable 6 5 Assessment Not applicable Minimum requirement fulfilled 6 6 Detailed representation of the test results Not applicable 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland
289. nded particulate matter PM10 Type of instrument TEOM 1405 F Measured values in yg m ACT Serial No SN 20006 amp SN 20107 No Date Ref 1 Ref 2 Ref 1 Ref 2 Ratio SN 20006 SN 20107 Remark Test site PM2 5 PM2 5 PM10 PM10 PM2 5 PM10 PM10 PM10 ug m ug m ug m yg m ug m ug m 301i 992011 68 71 57 9 9 8 11 1 Bornheim 302 9 10 2011 12 9 13 1 Summer 303 9 11 2011 5 7 5 5 59 5 7 9 9 9 304 9 12 2011 5 2 6 1 48 5 9 2 10 8 305 9 13 2011 6 3 7 2 40 6 12 5 14 8 306 9 14 2011 6 7 7 2 44 9 11 6 12 8 307 9 15 2011 11 1 12 2 47 4 22 8 23 1 308 9 16 2011 13 0 13 7 55 4 Inlet gt Zero filter 309 9 17 2011 Zero filter 310 9 18 2011 3 2 3 9 50 4 Zero filter 311 9 19 2011 7 8 8 2 66 2 11 3 10 7 312 9 20 2011 6 2 6 2 50 8 13 3 12 7 313 9 21 2011 6 6 6 6 53 6 10 5 11 4 314 9 22 2011 6 4 7 8 37 3 15 7 15 4 315 9 23 2011 12 2 13 4 49 1 24 7 23 4 316 9 24 2011 22 3 20 6 317 9 25 2011 15 7 14 5 70 0 21 7 21 2 318 9 26 2011 12 0 12 0 60 8 Audits 319 9 27 2011 21 9 21 9 56 0 39 7 37 3 320 9 28 2011 15 5 15 5 60 2 27 8 SN 20107 leak repairs 321 9 29 2011 17 1 16 0 65 1 26 6 29 4 322 9 30 2011 12 4 11 8 50 6 23 1 25 7 323 10 1 2011 20 7 23 0 324 10 2 2011 37 6 40 6 325 10 3 2011 13 5 14 8 66 2 27 4 30 4 326 10 4 2011 15 0 17 8 327 10 5 2011 6 4 6 7 328 10 6 2011 9 1 10 8 740300_2011_936_21209885B_eng doc TUVRheinland Precisely Right Page 186 of 422 Annex 5
290. ne Winter c cceeeessseeeenecceeeeteeneeeeseeeeees 136 Figure 50 PMio flow rate at candidate SN 20006 Cologne Winter cece 136 Figure 51 Total flow rate at candidate SN 20006 Cologne Winter cece 137 Figure 52 Course of time of the PM concentration ug m and the filter load Candidate SN 20107 Cologne Winter ccceceessseeeenneeeeeeeeeeeseeenenenee 137 Figure 53 PM o flow rate at candidate SN 20107 Cologne Winter eeeeeeeeees 138 Figure 54 Total flow rate at candidate SN 20107 Cologne Winter cee 138 Figure 55 Results of the parallel measurements with the candidates SN 20006 SN 20107 measured component PM p all test sites eee ecccseseseseeseeeeees 144 Figure 56 Results of the parallel measurements with the candidates SN 20006 SN 20107 measured component PM o test site Teddington Winter 145 Figure 57 Results of the parallel measurements with the candidates SN 20006 SN 20107 measured component PM o test site Teddington Summer 145 Figure 58 Results of the parallel measurements with the candidates SN 20006 SN 20107 measured component PM test site Cologne Winter 146 Figure 59 Results of the parallel measurements with the candidates SN 20006 SN 20107 measured component PM p test site Bornheim Summer 146 Figure 60 Results of the parallel measurements with
291. ne aes 41 Zero filter during field TESU ssccotacccee tiie adsense ee see ielyenscbensitvnasucseladeiacterdedstivvelacnctins 42 Set of filters for the check of the calibration Constant Ko 0 0 cceeeeeeeeeeteeeees 43 Course of time of the PM19 concentrations Reference at the test site Teddington WINKEE ee c ccc c cee ccceccceeecceecceeeceeeeeeeceeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeteeenaess 50 Course of time of the PM19 concentrations Reference at the test site py F CCINGTON SUMME rssi cccccceccceceeeceeceeeeceeceeeeeeeeeceeeceeeeeeeceeeceeeeeneseeesenestneseness 50 Course of time of the PM concentrations Reference at the test site Cologne parking lot Winter cccccccccccccccceccceeeceeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeteetetes 51 Course of time of the PM19 concentrations Reference at the test site Bornheim mo torway parking lot SUMIMEN cccceccecceeeeceeeeeeeeeeeeeeeeeeeeeeess 51 Field test site Teddington ssssbicochccavetinadt de nctietdacmctasatuatnbentonth Ashatiietcenebietadidvecags 52 Field test site Cologne parking lot scctcischerenstecsesseseduciedcarsteeredaemastesienniewiaaade 52 Field test site Bornheim motorway parking lOt cceeeeeeeeeeeettteeeeeeeeeeeeenee 53 Grubbs test results for the PM reference method Teddington Winter 56 Grubbs test results for the PM1o reference method Teddington Summer 57 Grubbs test results for the PM1o reference method Co
292. ng VDI 4202 Part 1 imum requirements stated in Stand ard VDI 4202 Part 1 September 2010 The test points 5 3 2 5 3 7 5 3 8 5 3 11 and 5 3 12 are evaluated as before based on the minimum re quirements stated in Standard VDI 4202 Part 1 from 2002 i e using the reference values BO B1 and B2 The testing of the test points 5 3 3 5 3 4 5 3 13 and 5 3 18 is waived as they are not relevant for particulate meas uring devices 5 3 2 Repeated stand The repeatability standard de The detection limit was determined ard deviation at viation at zero point shall not from investigations on 0 82 g m for zero point exceed the requirements of device 1 SN 20006 and 0 82 g m Table 2 in the certification for device 2 SN 20107 range according to Table 1 of Standard VDI 4202 Part 1 September 2010 For PM Maximal Bo Repeated stand The repeatability standard de Not applicable ard deviation at Viation at reference point shall reference point Not exceed the requirements of Table 2 in the certification range according to Table 1 of Standard VDI 4202 Part 1 September 2010 740300_2011_936_21209885B_eng doc TUVR h T V Rheinland Energie und Umwelt GmbH ein and Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Page 22
293. ng the 1405 unit or pump into the enclosure install a 3 8 inch elbow fitting provided with the outdoor enclosure into the quick connect fitting inside the pump compartment where the pump tubing goes through the bulkhead into the enclosure Install the other 3 8 inch elbows into the pump connection on the back of the 1405 unit and into the connection on the pump Figures 2 20 2 21 and 2 22 Figure 2 20 Enclosure Pump compartment bulkhead connection i Pump connections Figure 2 21 left Back of the 1405 unit Figure 2 22 right Pump THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 2 19 Section 2 SETUP AND INSTALLATION Figure 2 23 Water trap filter Pump compartment bulkhead connection 2 20 Operatine Guine TEOM 1405 F 2 a Install the water trap filter and bracket into the two pre drilled holes on the side of the pump compartment Figure 2 23 Cut a 14 inch 35m piece of tubing from the 3 foot section that came with the enclosure package Place the pump in the enclosure and connect the elbow fitting on the pump Figure 2 22 to the elbow fitting on the inside of the pump compartment using the 14 inch piece of tubing 4 Locate and cut the piece of the 15m green tubing that came in the 5 6 1405 packaging into two pieces one about but not less than 5m Install the one end of the 5m pump tubing into the quick connect fitting on the outside bulkhead wall of the pump comp
294. ng the respective values with the measured values of the previous test and the measured values of the first test It should be noted that using the test of the calibration constant Ko no concentration values can be simulated Therefore an assessment in the range of B4 was not possible 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 10301484 6 5 Assessment The maximum deviation found at zero point was 1 5 ug m with reference to the previous value and 1 6 ug m with reference to the start value and are thus within the allowed range of Bo 2 ug m The values for the drift of the sensitivity referring to the respective previous values determined within the scope of the test have been at maximum 1 3 for PM The found deviations on 07 03 2010 SN 20006 and on 06 02 2010 and 07 02 2010 SN 20107 could be ascribed to not correctly installed TEOM filters and therefore cannot be evaluated for the drift test On 26 05 2010 a measured value of SN 20006 could not be eval uated because the measuring signal produced a strong noise due to a leak of the switching valve The switching valve was changed on 11 06 2010 Min
295. ns at gt 2 C Warning message Pump vacuum gt 510 mm Hg Storage capacity data internal 500 000 Data set gt 2000d when storage in a 6 minute interval Device in and outputs 1 x 25 pin USER I O interface for analogue in and output and digital output 1 x RS232 interface for the communication via RP Comm Software or AK Protocol 1 x Ethernet interface for the connection with a PC for data transfer and remote control via ePort Software 2 x USB interfaces for the direct data download and for Firmware update Status signals error messages Available overview see annex A of the instruc tion manual 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH WT Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 47 of422 4 Test program 4 1 General The suitability test has been performed with two identical devices with the serial numbers SN 20006 und SN 20107 The test was performed with firmware version 1 51 The software has been constantly developed and optimized up to version 1 55 during the test program During the testing the software was constantly developed and optimized up to the version 1 55 During the development problems with t
296. ns tat iscssascaiencenonannonnossaninecamersemiens 5 62 AppendixA Troubleshooting cssccsssssssssccsssssssssesssrstessseessseeeearseeasseceearsesessees A 1 Converting Decimal Hexadecimal Numbets isis ansesssaesrrassoasirsieddsreis A 3 Deciphering Status Codes cii icscais asivecivsatisdotvertedtveetoaveriutiocnsasraaautiveriaetiaeets A 4 Example rurau casts ttoecensengs tienes a a i sees A 4 AppendixB Serial Communication ccssscsssesessesecsecessesecseseseeseesessseeeees B 1 X Operatine Guipe TEOM 1405 F THERMO FISHER SCIENTIFIC Section Introduction The TEOM 1405 F Ambient Particulate Monitor with FDMS is a mass measurement monitor that incorporates the patented Tapered Element Oscillating Microbalance TEOM to measure particulate matter mass concentrations continuously The TEOM 1405 F Monitor is a true oravimetric instrument that draws ambient air through a sample filter for collection at a constant flow rate The monitor continuously weighs the filter calculating near real time mass concentrations The 1405 F can be used to sample PM 10 by using a standard PM 10 inlet or can be used for PM 2 5 sampling by adding a cyclone in addition to the PM 10 inlet The TEOM 1405 F utilizes FDMS technology to provide a representative determination of the mass concentrations of the PM as it exists in ambient air The FDMS unit automatically determines mass concentration measutements that account for both non volatile and
297. o point 4 of this re port In doing so the different seasons and different levels of concentrations were taken into account At each test site at least 15 valid data pairs were determined 6 4 Evaluation Requirement from EN 12341 The calculated functional relationship y f x between concentration values measured with the candidate sampler y and concentration values measured with the reference sampler x has to be limited by a two sided acceptance range This acceptance range is given by y x 10 ug m for concentration averages lt 100 ug m and y 0 9x ug m respectively 1 1x ug m for concentration averages gt 100 g m Moreover the variance coefficient R of the calculated reference equivalence function shall be at least 0 95 The test procedure focuses on the functional relationship between the concentration values which were determined through double measurements with candidate and reference sam pler Ideally both instruments sample the same fraction of suspended particulate matter which leads to the relation y x The evaluation process is as follows A linear regression analysis based on the measured values was done for every single test site and after merging the overall measured data for all four test sites together One receives for every measurement value y of the candidate sampler i and the concentra tion x measured with the reference sampler both in ug m a reference equivalence function accord
298. of For the test of PM2 5 measur The determined uncertainties WCM 148 the expanded ing systems the equivalency without application of correction fac uncertainty of the With the reference method shall tors lay for all observed data sets be instruments be demonstrated according to neath the defined expanded relative chapter 9 5 2 2 to chapter 9 5 4 uncertainty Wdqo of 25 for particu of the guidance document late Demonstration of Equivalence of Ambient Air Monitoring Methods in the field test at least at four sampling test sites representative of the future ap plication 5 4 11 Application of If the maximum expanded un The candidate systems fulfil the re 161 correction factors certainty of the systems under quirements on the data quality of am and terms test exceeds the data quality bient air quality measurements during objectives according to Annex the test already without application of A of Standard VDI 4202 Part 1 correction factors for the test of PM2 5 measuring systems the application of cor rection factors and terms is al lowed Values corrected shall meet the requirements of chap ter 9 5 2 2 ff of the guidance document Demonstration of Equivalence of Ambient Air Monitoring Methods Requirements on Multiple component measuring Not applicable 166 multiple systems shall comply with the component requirements set for each measuring sys component also in the case of tems si
299. of the instrument was told that any change to the instrument software shall be reported to the test body 6 4 Evaluation The present software is shown in the display when turning on the device At any time it can be looked at in the menu system status The suitability test was performed with the software version 1 51 2009 During the test the software was developed and optimized constantly up to the version 1 55 Appearing problems with the touch screen display were resolved during the development E g there have been problems with the availability of the button reboot during a possible system crash Due to the changes up to the version 1 55 no influence on the instrument performance is to be expected 6 5 Assessment The version of the instrument software is shown on the display The test institute is informed on changes in the instrument software Minimum requirement fulfilled yes 740300_2011_936_21209885B_eng doc a T V Rheinland Energie und Umwelt GmbH TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 84 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 6 Detailed representation of the test results TEOM 1405 F Operating mode RS232 mode Vacuum pump pressure Protection level IP address Serial numbe
300. on to begin the Flow Audit Wizard Figure 5 54 Select the Next gt button Figure 5 54 Flow Audit Wizard Welcome to the Flow Audit Wizard This wizard hross you perform flow audits on the TEGM Ambient Particulate Monitar The imstrument will be put in Setup mode for the mit To continue press Mexi Mex gt Cancel 5 44 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 3 The Select a Flow Audit Device screen will display Select a flow audit device Select Direct Flow Device to audit the flow using a direct flow measuring device reading 1 min adjusted for temperature and pressure such as the Streamline Pro Select FTS to audit the flow using the FTS system FTS users will enter the device calibration constant and the change in pressure from the FTS Select the Next gt button 4 The Select Flow to Audit screen will display Select which flow to audit Press the Next gt button Note If you selected the FTS option in the previous screen you will be prompted to enter the correct calibration constants before proceeding with the audit Figure 5 55 a Figure 5 55 Enter FTS Constants Enter FTS Constants screen THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 45 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Figure 5 56 Flow adapter meter attached to the flow splitter Figure 5 57 Bypass line cappe
301. ond weighing are excluded during the pre weighing process Filters which deviate more than 60 ug are not considered for evaluation after post weighing as conforming to standards 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH M Luftreinhaltung A TUVRheinland Genau Richtig Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 2093 01 424 Weighed filters are packed in separate polystyrene jars for transport and storage These jars remain closed until the filter is placed in the filter holder Virgin filters can be stored in the weighing room for up to 28 days before sampling Another pre weighing is carried out if this period is exceeded Sampled filters can be stored for not more than 15 days at a temperature of 23 C or less The filters are stored at 7 C in a refrigerator 740300_2011_936_21209885B_eng doc TUVRheinland TUV Energie und Umwelt GmbH Precisely Right Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Seite 210 von 422 Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B A2 Filter evaluation The filters are evaluated with the help of a corrective term
302. onent PM10 Report No 936 21209885 B 6 1 5 2 7 Maintenance interval The maintenance interval of the measuring system shall be determined during the field test and specified The maintenance interval should be three months if possible but at least two weeks 6 2 Equipment Not required for this minimum requirement 6 3 Performance of test This test was done in order to determine which maintenance procedures are required at which period to maintain correct functionality of the measuring system Moreover the results of the drift test for zero and span point according to point 6 1 5 3 12 Long term drift were included into the determination of the maintenance interval 6 4 Evaluation No unacceptable drifts were detected for the measuring systems during the entire field test period Therefore the maintenance interval is determined by scheduled maintenance procedures refer to module 4 1 2 During operation the maintenance works can be limited to checks on contamination plausi bility and status error message 6 5 Assessment The maintenance interval is defined by necessary maintenance procedures and is 1 month Minimum requirement fulfilled yes 6 6 Detailed representation of the test results Necessary maintenance works can be found in module 4 1 2 of this report and in chapter 5 of the operating manual 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH WT Luftreinhaltung A TUVRheinland
303. or of the Page 18 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 1 2 Proposal of declaration of suitability On the basis of the positive results that have been achieved the following recommendation is made for the notification as a suitability tested measuring system Measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator for PM10 Manufacturer Thermo Fisher Scientific Franklin USA Suitability For continuous monitoring of suspended particulate matter of the PM fraction in ambient air stationary operation Measuring ranges during the suitability test Component Certification range Unit PMio 0 1000 g m Software version 1 55 Restrictions The allowed range of ambient temperature at the installation test site is 8 C to 25 C Notes 1 The requirements to the variation coefficient R according standard EN 12341 were not kept for the test sites Teddington Summer and Bornheim Summer 2 The requirements according to guide Demonstration of Equivalence of Ambient Air Moni toring Methods are fulfilled for the measured components PM 3 The measuring system is to be calibrated on test site in regular intervals by application of the gravimetric PM reference method according to EN 12341 4 The test report on the suitability test is visible in the internet under www qal1 de Test report TUV Rheinland Energie
304. ored Select the OK button when all the desired variables have been selected 4 Use the V and A buttons to scroll through the list of selected variables to ensure that all desired variables are selected 5 When in the Data Storage screen select the Storage Interval button to select the interval for data storage Enter the desired data storage interval into the keypad and select the Enter button For example if the storage interval is 10 seconds every 10 seconds the instrument will log save the data in the selected variables 6 The storage order of the variables may be set by moving individual storage registers up or down in the list on the screen To adjust the order touch the desired variable and then move the position by pressing theV and A arrows to the right of the data variable list For this ordering to work properly with data downloads version 1 40 or later of ePort is required 7 When all the desired variables are selected and the Storage Interval is set select the lt Back button to return to the Settings screen THERMO FISHER SCIENTIFIC Section 3 Basic OPERATION Downloading D ata The ePort software allows users to download data from the TEOM 1405 F monitor using a personal computer PC with the Windows XP or later operating system The monitor must be attached to a local area network LAN or directly to a router using the Ethernet connection on the back of the instrument Figure 3 14 In order to use ePor
305. p SN 20107 No Date Ref 1 Ref 2 Ref 1 Ref 2 Ratio SN 20006 SN 20107 Remark Test site PM2 5 PM2 5 PM10 PM10 PM2 5 PM10 PM10 PM10 yg m ug m ug m ug m ug m ug m 151 6 30 2010 4 4 5 5 9 6 9 5 51 7 12 0 12 7 Teddington 152 7 1 2010 6 9 6 1 11 0 11 6 57 7 14 2 13 8 Summer 153 1 27 2011 8 9 8 8 12 8 13 3 67 8 Audits Cologne 154 1 28 2011 28 3 28 5 36 3 36 8 77 8 Audits Winter 155 1 29 2011 Zero filter 156 1 30 2011 62 0 62 1 82 7 83 7 74 6 Zero filter 157 1 31 2011 81 6 81 8 95 5 94 0 86 2 Zero filter 158 2 1 2011 61 9 62 0 75 3 73 6 83 2 75 5 76 0 159 2 2 2011 20 6 20 1 25 2 24 7 81 8 22 7 25 1 160 2 3 2011 14 1 13 4 20 1 20 4 67 7 18 9 19 6 161 2 4 2011 6 1 6 2 11 0 11 4 54 6 10 4 10 6 162 2 5 2011 8 6 9 1 163 2 6 2011 8 4 8 5 14 8 15 0 57 0 14 1 16 0 164 2 7 2011 9 7 10 0 17 5 18 8 54 2 18 5 19 2 165 2 8 2011 18 0 17 3 30 6 31 3 57 2 28 7 30 3 166 2 9 2011 21 2 21 9 29 6 30 6 71 5 28 1 30 6 167 2 10 2011 19 4 20 8 24 9 26 7 77 9 25 8 26 9 168 2 11 2011 10 5 11 3 13 2 14 1 80 0 12 8 14 7 169 2 12 2011 18 3 18 9 170 2 13 2011 11 5 12 5 17 0 18 5 67 5 16 6 16 6 171 2 14 2011 21 1 19 5 23 8 24 2 84 6 23 9 25 3 172 2 15 2011 16 4 16 0 19 0 19 7 83 7 20 8 19 6 173 2 16 2011 24 5 24 0 34 0 34 2 71 1 35 2 33 4 174 2 17 2011 36 0 35 5 42 2 42 1 84 8 44 1 44 1 175 2 18 2011 36 5 36 7 43 4 43 5 84 3 45 6 47 2 176 2 19 2011 56 1 55 3 177 2 20 2011 27 6 27 8 29 5 29 8 93 5 30 7 28 8 178 2 21 2011 31 3 31 8 36 6 36 2 86 6
306. pany Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page11 0f422 Figure 40 Reference equivalence function SN 20006 test site Bornheim Summer 120 Figure 41 Reference equivalence function SN 20107 test site Bornheim Summer 120 Figure 42 Reference equivalence function SN 20006 all test sites ee 121 Figure 43 Reference equivalence function SN 20107 all test sites eeee 121 Figure 44 Result of the parallel measurements with the candidates SN 20006 SN 20107 test site Teddington Winter cc cceecceeeeeeeeeeeeeeeeeeeeeeeeeeeeenaaees 124 Figure 45 Result of the parallel measurements with the candidates SN 20006 SN 20107 test site Teddington Summer cc cceceeeeeeeseeeeeeeeeeeeeeeeeeeeneaaees 125 Figure 46 Result of the parallel measurements with the candidates SN 20006 SN 20107 test site Cologne parking lot ccccceccccccceccceeeceeeeeeeeeeeeeaeeeaeenes 125 Figure 47 Result of the parallel measurements with the candidates SN 20006 SN 20107 test site BOPMNeIM cee ceccc cece cceeeeeeeseeeeeeeeeeeeueeeeeaueeeaeeeaeeeaes 126 Figure 48 Result of the parallel measurements with the candidates SN 20006 SN 20107 AlIMESUSIGS ccccefites cc ccsactdtts orenis cettenesdaboudalieacasnonatacaieheudeatstdteesdimendaades 126 Figure 49 Course of time of the PM concentration ug m and the filter load Candidate SN 20006 Colog
307. pennix B SERIAL COMMUNICATION AK Protocol Enter Register Command EREG COM 2 WAY SETTINGS RS Para 1 ASCII code for the 1 digit Station Number for example 4 052 The Station Number is always 1 digit in length RS Para 2 75048 ASCII code representation of the 2 digit Channel Number for example K0 075 048 The Channel Number is always 2 digits in length RS Para 3 13010 Optional Up to 3 ASCII codes can be added to response from the instrument In this case lt CR gt and lt LF gt ASCII codes 013 and 010 are appended to the response Enter 0 if nothing is to be appended RS Para 4 Not used COCO nome evo oem Enter Register command 4 digit Enter Register command a E a oe Kk 2 digit Channel Number as defined oo o Number of Gurren stats conditions E ee oe p variable whose value is being ie ak d y A igite long and Is not digits long Do not right fill if the Up to 3 digits appended to the end of 15 New value to be entered for variable J 15 the response transmission according to referenced by Program Register the entry for RS Para 3 varying length and is not restricted os 14 byes a a B 6 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Appenpix B SERIAL COMMUNICATION AK Protocol Set Function Command SFxx RS Para 1 ASCII code for the 1 digit Station Number for example 4 052 The Station Number is always 1 digit in length RS Para 2 75048 ASCII code representat
308. place the filter or post a fail message Figures 5 13and 14 21 When the frequency stable the system will display the Completing the TEOM Filter Replacement Wizard screen Figure 5 12 Select the Finish gt button Figure 5 12 Finish screen with successfully completed message Completing the TEOM Filter Replacement Wizard You have sucessiuly completed the TEGM Filter Replacement Wizard Te close this wizard press Finish THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 11 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Note If the system still cannot detect a stable frequency for the filter it will display a filter could be damaged message and prompt for replacement of the filter Figure 5 13 If the system fails to establish the frequency again the filter change procedure will fail completely and recommend appropriate service Figure 5 14 a Figure 5 13 Try Another Filter screen Y nother Filter The TEOM filter could be damaged The TECH filter ls still loose This could be becouse itis damaged Please replace the filter with a new Figure 5 14 Fail service message Completing the TEOM Filter Replacement Wizard The TEOM Fiter Replacement Wizard has completed unsucenstully _ Please reference the TEOM Series 1405 To Serice Manual ter troubleshooting insiructions 5 12 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PRO
309. quirements of EN 14907 The procedures of filter handling and weighing are described in detail in Appendix 2 of this report 740300_2011_936_21209885B_eng doc aT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 60 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 5 Reference measurement procedures The following devices were used during the field test in accordance with EN 12341 1 Reference equipment for PM Small filter device Low Volume Sampler LVS3 Manufacturer Ingenieurb ro Sven Leckel Leberstrafe 63 Berlin Germany Date of manufacture 2007 PM19 Sampling inlet Two reference devices each for PM and PM25 were simultaneously operated during the testing with a controlled volume flow of 2 3 m h The accuracy of the volume flow control is below lt 1 of the nominal volume flow under standard conditions The sampling air is sucked in via the rotary vane vacuum pump through the sampling inlet for the small filter device LVS3 The sampling air volume flow is measured with a measuring ori fice which is installed between filter and vacuum pump In order to collect any dust created by the abrasion of the vanes the incoming air passes a separator before flowing to the air outlet The
310. quirements on measuring systems for particulate air pollutants Page 25 of 422 5 4 1 General Test according to the minimum The test took place according to the 114 requirement stated in Table 5 minimum requirement stated in Table of Standard VDI 4202 Part 1 5 of Standard VDI 4202 Part 1 Sep Furthermore the particle mass emper ATIU concentration shall be related The measuring unit TEOM 1405 F to a defined volume The rela Ambient Particle Monitor is a gravi tion to volume with respect to metric measuring device which de pressure and temperature shall termines the mass depotest sited on a be comprehensively described filter via oscillating micro weighing The determined mass is related to a defined and actively regulated sam pling volume and thereby the particu late concentration is determined 5 4 2 Equivalency of The equivalency between the The reference equivalence functions 115 the sampling PM10 sampling system and the lay within the limits of the respective system reference method according to acceptance range Furthermore the EN 12341 shall be demon variation coefficient R of the calculat strated ed reference equivalence functions in the relevant concentration range for the data sets All data set Tedding ton Winter and Cologne Winter is 2 0 95 For the data sets Tedding ton Summer and Bornheim Sum mer the variation coefficient is lt 0 95 Both test sites are cha
311. r Instrument firmware version Figure 29 Display of the software version here 1 51 in the menu System Status 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH w Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 89 9f422 6 1 5 3 1 General The testing is done based on the minimum requirement according to Standard VDI 4202 Part 1 September 2010 6 2 Equipment Not required for this minimum requirement 6 3 Performance of test The test is made on the basis of the minimum requirements of Standard VDI 4202 Part 1 September 2010 6 4 Evaluation Standard VDI 4202 Part 1 and VDI 4203 Part 3 have been republished after a detailed revi sion in September 2010 Unfortunately after this revision uncertainties and contradictions remain regarding the concrete minimum requirements on the one hand and the general rele vance of the test points on the other hand while testing particulate ambient air measuring de vices The following test points require clarification 6 1 5 3 2 Repeated standard deviation at zero point no minimum requirement defined 6 1 5 3 3 Repeated standard deviation at reference point not relevant for particulate devices 6 1 5 3 4 Linea
312. r Placing a temperature or barometer in the desired location allows users to audit those values compared to an external measurement device Flows can be individually audited for accuracy using the flow audit wizard For changing or calibrating the values refer to the following sections Refer to the flow temperature and pressure calibration section for information on how to attach external measurement devices to the TEOM 1405 unit Figure 5 51 Instrument Audit screen TEOM 1405 F Gmr on gt Cali allon Sinsirument Supe Aaah inet Deage rata re 29 16 C Abin parE 100 rhe Maire eluent rie Tew rate SL lp Bypass yoRimebric Boe rabe 13 67 j Vaca pimp prette O28 atm Ko Const nt ae lt Back i Faiy operational Hoerial states a peresan 10 56 THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 41 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES Calibrating the Ambient Temperature Figure 5 52 Ambient Calibration screen 5 42 Operatine Guine TEOM 1405 F Perform the ambient air temperature calibration pressure calibration and leak check Section 3 before executing the flow calibration procedure To calibrate the ambient air temperature 1 In the TEOM Data screen select the Service button to display the Service screen then select the Calibration button to display the Calibration screen Figure 5 32 2 Select the Ambient Calibration button to display the Ambient Calibration screen Figure
313. r information on setting up a data folder The default folder location is C Program Files Thermo ePort Data Figure 3 35 Data csv file opened in Excel SO Se ira an Ses Gd Ga Pe eel ae ee y tmoTECMAKD tmoTEOMEHD tmoTEOMAReMCRsw imoTEOMABseeNICRaw tmoTEOMAFreqSiat imoTEOMAFrequancy imoTEOMBFreqStan tmoTEOMEF requ 255 50621 2 EERE 18 V7 1847 14406 25973 o o o o 204 3 652016 18 17 1578 407 14405 2323 0 0 0 266 40621 0 204 41650006 18 17 15918486F 14406 25979 o o o 255 50621 o 2504 S GSN 10 17 SNAP 1440526323 0 0 0 265 00901 0 250 4 6 6S5O006 18 17 15918486F 14406 253979 o o o 265 508008 0 2504 G26 10 10 ISNA 14405 0323 0 0 0 266 50961 0 20 4 8 SS72006 18 18 19591848F 14406 25579 o o o 265 983 o 204 9 652008 18 10 157a A6 14405 0323 0 0 0 26 40977 0 0 4 10 S572006 1818 _15918 4269F 1406 25979 o o o 7265 908567 o 204 11165206 18 18 1578 469 144050323 0 0 0 265 00539 0 250 4 12 650006 18 18 15991848F 1406 25579 o o o 25 510035 o 2504 135 652006 10 19 1570 4697 14405 0323 0 0 0 255 900306 0 w04 14 S572006 18 19 19918483F 14406 523 o o 765 98375 265 9875 250 440046 204 15 65206 18 19 157a 46 14405 0323 0 0 205 OBES 265 90866 1 250 440046 20 4 16 S572006 1819 15918486F 14406 255979 o o 755 98975 765 B82 250 440046 204 ASAMA 10 19 1676 AHF 14406 26929 0 0 205 005 205 00065 250 480046 250 4 18 S572006 18 19 15918 487 14406 254979 o o 7255 98575 25510019 2504446 204 19 65206 1020 15704269F
314. r Scientific for the component PM10 Report No 936 21209885 B a Teddington Summer a Cologne Winter a Bornheim Summer e Teddington Winter lt 30 pg m 3 Line gt 30 ug m 3 Line All Data Line 0 10 20 30 40 PM Reference pg m 50 60 70 80 90 100 Figure 62 Reference vs candidate SN 20006 amp SN 20107 measured component PM all test sites 100 90 a SN 20006 80 70 4 60 50 4 40 PM 1405F FDMS pg m 30 0 10 20 30 40 PM Reference ug m 50 60 70 80 90 100 Figure 63 Reference vs candidate SN 20006 measured component PM all test sites 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 19501484 100 90 a SN20107 80 PM 1405F FDMS pg m 40 50 60 70 80 90 100 PM Reference ug m Figure 64 Reference vs candidate SN 20107 measured component PM all test sites 100 90 4 4 SN 20006 Teddington Winter 80 70 dD a 607 ra u 50 va o a a 50 60 70 80 90 100 PM Reference pg m Figure 65 Reference vs candidate SN
315. r Windows XP software select the Next gt button Note The ePort software MUST be installed on a PC with the latest Windows XP or later updates If you have not updated your Windows XP system select the Cancel button and use the Windows Update function of the PC to update the operating system before attempting to install the ePort software a Figure 3 16 i i ePort 0 12 8 InstallShield Wizard Windows Update notice eaii PAESE tae Readme Information Please read the Following readme information carefully Important Note e Supported Operating Systems o Windows XP sp2 o Windows 2000 sp3 and sp4 o Windows 2003 Server BEFORE installing rp Communicator EXIT this installation and install the Critical Windows Updates shttp windowsup date microsoft com gt 5 The Customer Information screen will display Type in the information and select the Next gt button THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 3 15 Section 3 Basic OPERATION 6 The Ready to Install Program screen will display Figure 3 17 Select the Install button Figure 3 17 appre Ready to Install the Program screen Ready to Install the Program The wizard is ready to begin installation Tf you want to review or change any of your installation settings click Back Click Cancel to exit the wizard Current Settings Setup Type Destination Folder C Program Files Thermo User Information Name Compan
316. r adjustable wrench Note Hand tighten both nuts on the bracket before tightening them with the wrench to ensure thatthe bracketis positioned properly on the tripod leg and tripod foot a Repeat steps 1 through 4 for each leg of the tripod THERMO FISHER SCIENTIFIC Section 2 SETUP AND INSTALLATION Installing the Inlet The TEOM 1405 F can be assembled with a variety of inlet configurations For PM 10 sampling only a traditional or modified PM 10 inlet is used PM 2 5 and PM 1 sampling is accomplished by adding a cyclone to the inlet assembly downstream of the PM 10 inlet Two types of cyclones are available for use in PM 2 5 sampling the VSCC and the SCC Figure 2 9 The VSCC is required for U S EPA sampling For PM 1 sampling a single type of cyclone is available Figure 2 9 Modified PM 10 Inlet installed THERMO FISHER SCIENTIFIC VSCC PM 2 5 inlet Operatine Guine TEOM 1405 F 2 9 Section 2 SETUP AND INSTALLATION To install the inlet 1 Set the 1405 unit on a bench or other support directly below the location of the inlet on the roof of the sampling structure Figure 2 1 In its finished state the entrance to the sample inlet must be 1 8 to 2 1 m 70 to 82 inches above the roof Note This measurement may vary based on the inlet height required by the local regulatory agency The height of the inlet is the same if sampling PM 10 PM 2 5 or PM 1 a 2 Install the assembled flow splitter into the tripod
317. r ore te reeteree reer 28 2 1 TYME Of OS liccarecdastaceontecetexcasazansticconteegnemaanucen tees sae deane EEEE ENANA TAAAK ANIE EENES 28 3 DESCRIPTION OF THE TESTED MEASURING SYSTEM cceeeeeeeeeeeeteeeeeeeeees 29 3 1 Measuring principle cece eeeeeeeeeeeeeeee cece eeeeeeeeeeaee sees eee degeeeeeeeeeeegeesegeseeeeeeeeeeeeeeeeeeeeeeeeeea 29 3 2 Functionality of the Measuring system eee ec eeeeee eee e eee eeeeeeee cnet settee teeeneeeeeeeeeeeeeneeeaaaae 31 3 3 AMS scope and layout sais cceseccatiicansseasdsicabnceeseccennaphastueiarberarkctantddennschidexsteueaintneeteecanmeuahaee 32 A TEST PROGRAM scctscstastacereudapundansstesstiaxndtslubsdensannvenvewbactibcuarkddentiieasddeenedcmagdetadavajenunstgantines 47 4 V General i epee bate ota ete eae ia eat one i A a a tet Olas oes asatneg ned ak 47 42 laboratory NOS sate cte tia asi ta tease uacetcceans seta cuasa cated metic Sese aE A ao aria sa RaRa 47 4 3 Field toSt gasses ad cepted A A Sue adaware doe cel E AE E naaets 48 5 REFERENCE MEASUREMENT PROCEDURE S isccccccesscccoseestvonevesstreeetissetiecnneaionswedense 60 2 ON Beso tlc I open ener ee meen eee eee E er oe ee eer ee ee 61 6 1 4 1 1 Measured value USDA vrais icscsisteriectvtissasis mackemeeineanaanentasnermactnatttneactianiaisamdtectes 61 6 1 4 1 2 Easy maintenance axe sic sisicabdcctdccentansaseuboetaezaradiescdeeseanntvbadakeiwenneeteexedencapaccatiex 63 6 1 AAS Functional WSU ie dio Sate aN ce marc
318. racterized by a low variation of the particulate con centrations The equivalence test ac cording to 6 1 5 4 10 Calculation of the expanded uncertainty of the in struments is fulfilled nevertheless for all test sites Reproducibility of The PM10 sampling systems of The two sided confidence interval 122 the sampling two identical systems under Cl95 is with a maximum of 2 57 ug m systems test shall be reproducible beneath the demanded value of among themselves according 5 g m for all test sites to EN 12341 This shall be demonstrated in the field test Calibration The systems under test shall A statistically secured relation be 127 be calibrated in the field test by tween the reference measuring pro comparison measurements cedure and the instrument display with the reference method ac could be demonstrated cording to EN 12341 Here the relationship between the output signal and the gravimetrically determined reference concen tration shall the determined as a steady function 740300_2011_936_21209885B_eng doc A TUVRheinland Precisely Right TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Page 26 of 422 Report No 936 21209885 B Specification Test result Page filled 5 4 5 Cro
319. rage 100 6 101 2 101 3 100 7 Rel humidity Range 62 9 98 3 43 9 86 7 34 2 94 2 53 8 86 9 Average 87 6 63 7 67 73 9 Wind velocity m s Range 0 0 2 5 0 1 2 3 0 3 7 1 0 3 2 9 Average 0 6 0 8 2 3 1 2 Precipitation mm Range 0 0 23 1 0 0 9 4 0 0 33 0 0 0 51 7 Average 2 3 0 7 1 4 3 3 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 33 0142 Sampling period EN 12341 defines a sampling period of 24 h However at lower concentration levels a long er at higher concentration levels a shorter sampling period is permissible The sampling period was constantly set to 24 h during the field tests 10 am 10 am for Teddington and Cologne and 7 am 7 am Bornheim Data handling All paired reference values determined during the field tests were subject to statistical test ing according to Grubbs 99 to prevent influences of obviously implausible data on the measuring results Paired values which are identified as significant outliers can be discarded until the critical value of the test statistic is exceeded The January 2010 version of the Guid ance 4 stipulates tha
320. ration mass equivalent to the filter mass allows all measurements to be made at essentially the same operating point as the original calibration Refer to Section 1 for a detailed explanation of how the calibration constant K is derived To audit verify the KO number requites a mass calibration verification kit 59 002107 which includes a pre weighed filter a filter exchange tool desiccant and a humidity indicator and the pre filter with a half inch quick connect fitting supplied with the instrument Note Refill kits for the mass calibration verification kit are available from Thermo Scientific 59 002019 a THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES To confirm the system s K calibration il Figure 5 79 Welcome to KO Verification Wizard screen THERMO FISHER SCIENTIFIC Confirm that the KO number entered into the instrument and the KO number on the plate near the mass transducer are the same The KO number entered into the unit can be found in the Audit screen Figure 5 51 Ensure the instrument is at the normal operating temperature and condition Ensure that the pre weighed filter in the kit matches the humidity conditions for the test as shown on the card provided with the kit Note If the filter does not match the conditions listed on the humidity indicator follow the instructions provided with the kit to dry the filter to an acceptable level a In the TEOM Data screen
321. rc When the file is selected it will display in the window below Choose the File to Upload Select the Next gt button 4 38 Operatine Guipe TEOM 1405 F THERMO FISHER SCIENTIFIC Section 4 SCREENS AND SETTINGS 8 The Upload Software screen will display Figure 4 32 The software will restart the instrument then install the firmware The Upload Progress bar will show the status of the upload When the process is complete select the Next gt button Figure 4 32 _ Thermo 1405 Installer al Upload Software screen Upload Software Upload the new software file to the instrument Settings Filename rpco_dev rc 9 Restarting Instrument This may take a few minutes Upload Progress Cancel Note It may take several minutes to upload the new firmware depending on the speed of the uploading PC and the speed of the network During the upload the TEOM 1405 instrument touch screen will display a text message then a scrolling cursor to indicate progress A THERMO FISHER SCIENTIFIC Operating Guioe TEOM 1405 F 4 39 Section 4 SCREENS AND SETTINGS 9 The Software Upload Completed screen will display Figure 4 33 Select the Finish button Close ePort and return to normal operation Figure 4 33 Thermo 1405 Installer Joe Software Upload Completed screen Software Upload Completed 1405 Installer Transfer of software to the instrument has completed Setup will automatically
322. rd is fin shed To close this wizard prese Finish 15 Install a new TEOM filter in the mass transducer Section 5 3 10 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Storing Data Figure 3 12 Settings screen THERMO FISHER SCIENTIFIC Section 3 Basic OPERATION The unit stores only those variables selected by the user If instrument variables are not set up to be logged THEY WILL NOT BE SAVED To select data storage variables 1 Select the Settings menu button to display the Settings screen Figure 3 12 TEOM 1405 F Settings ab Aria Home si a CHENG 1 System Status Instrument Conditions Settings Service 2 When in the Settings screen select the Data Storage button to display the Data Storage screen Figure 3 13 Operatine Guine TEOM 1405 F 3 11 Section 3 Basic OPERATION Figure 3 13 Data Storage screen 3 12 Operatine Guine TEOM 1405 F TEOM 1405 F Setlings gt Data Storage instrument variables to More You can change order gtvariabim ae clicking on the field and dragging it up or doen usimg the arrow Gutboms on the right miii mn Moise 3 When in the Data Storage screen select the Edit List button to display the Edit Data Storage screen Press the names of the variables you wish to log up to the maximum allowed of 30 Use the Next Page gt and lt Previous Page buttons to scroll through the entire list of variables which can be st
323. re described in this appendix The AK Protocol allows the user to query the present value of any system variable remotely and allows the user to change those system variable values The user also can download information from the internal data logger The RPComm software program uses this protocol for two way communication directly to a personal computer or through a modem The following AK Protocol commands are presented in detail on the following pages e AREG Ask Register Command The user can query the TEOM 1405 Monitor for the current value of any system variable e EREG Enter Register Command The user can assign a new value to any system variable Great care must be taken when using this command as the value of variables should only be changed when the monitor is in the appropriate operating mode e SFxx Set Function xx Command The user can send commands using the lt RUN gt key and the lt DATA STOP gt key to the instrument Each command is designated by a two digit code xx e ASTO Ask Storage Command The user can download a specified number of records from the internal data logger from the current position of the data storage pointer The location of this storage pointer may be defined by the SSTO command The values on each line of output are delimited by commas e SSTO Set Storage Command The user can change the location of the data storage pointer in the internal data logger and is used in conjunction
324. red value transducer using the Ko check kit also is possible at any time 6 5 Assessment All system functions listed in the manual are available activatable and functioning The cur rent system status in continuously monitored and displayed by a set of different status mes sages operation warning and error messages 740300_2011_936_21209885B_eng doc A T VRheinland T V Rheinland Energie und Umwelt GmbH Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 66 of 422 The results of the external checks of the zero point with a zero filter during the field test peri od as well as periodically performed checks of the calibration constant Ko are described in chapter 6 1 5 3 12 Long term drift of this report Minimum requirement fulfilled yes Detailed representation of the test results Refer to chapter 6 1 5 3 12 Long term drift 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH F Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 6 01422 6 1
325. reference devices for PM 153 Table 33 Summary of the results of the equivalence test SN 20006 amp SN 20107 measured component PMyo raw data cccccecceseeccececeeseeaeeeeeceeeeeeseasaeaeeeseeees 153 Table 34 Summary of the results of the equivalence check SN 20006 amp SN 20107 after in tercept correction ccc ccccccccceccceecceeeeeeeeceeeeeeeeeeeeeeeeneeeeeseeeeseeseaaeenaeeaas 165 Table 35 Stability standard WEI HM eiccceccesascanctfartndsbidelss sol diinddisbdadsscnsaddeptdabsiddeesaddaehedensbens 211 Table 36 Stability of the Control filters cece cc cec cece cece cceeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeteeeeeeeeeess 213 Table 37 Conditioning and weighing timeScCales ccceceeeeeeeeeeeeeeeeeeeentaeeeeeeeeeeeees 214 740300_2011_936_21209885B_eng doc A TUVRheinland TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Precisely Right Page 10 of 422 Figures Figure 1 Figure 2 Figure 3 Figure 4 Figure 5 Figure 6 Figure 7 Figure 8 Figure 9 Figure 10 Figure 11 Figure 12 Figure 13 Figure 14 Figure 15 Figure 16 Figure 17 Figure 18 Figure 19 Figure 20 Figure 21 Figure 22 Figure 23 Figure 24 Figure 25 Figure 26 Figure 27 Figure 28 Figure 29 Figure 30 Figure 31 Figure 32 Figure 33 Figure 34 Figure 35 Figure 36 Figure 37 Figure 38 Figure 39 Report on the suitability test of the ambient air quality measuring
326. reference mass concentration negative in case mass of the filter evaporates After the mass determination the sampling flows are directed over a mass flow rate regula tor To guarantee a constant sampling volume flow at the inlet taking into account the ambi ent temperature and pressure the volume flow control shall be operated in the mode active actual 740300_2011_936_21209885B_eng doc aT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 32 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 3 3 AMS scope and layout The particulate ambient air measuring device TEOM 1405 F Ambient Particulate Monitor is based on the measuring principle of oscillating micro weighing The tested measuring unit consists of PM sampling inlet flow splitter the respective sam pling tubes a tripod to support the sample tubes the measuring device TEOM 1405 F incl FDMS tower the vacuum pump with its respective power supply cord and cables as well as adapters the roof lead through incl a flange and a manual in German English Figure 2 Overview of complete system TEOM 1405 F Ambient Particulate Monitor 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinl
327. reference point check at the two candidates SN 20006 and SN 20107 the calibration constant Ky was tested to check the stability of the sensitivity The surrounding temperatures in the climatic chamber were varied in this order 20 C 8 C 20 C 25 C 20 C After an equilibration time of approx 24 h per temperature step the recording of the measured values at zero point per temperature step 3 X 24 h each as well as the measured values at reference point per temperature step 3X each started 740300_2011_936_21209885B_eng doc aT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 94 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 4 Evaluation Zero point The measured values for the concentration of the respective 24 h single measurements were read out and evaluated The absolute deviation in ug m per temperature step is observed in relation to the default point of 20 C Reference value Bo 2 g m Reference point The deviation as a percentage of the determined measured values for the calibration con stant Ko was observed for each temperature step in relation to the default point at 20 C As note it should be mentioned that by using the check of the calibration const
328. reinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B page 12901422 6 1 5 4 5 Cross sensitivity The interference caused by moisture in the sample may not exceed 10 of the limit value in the range of the limit value 6 2 Equipment Not necessary for this minimum requirement 6 3 Performance of test The determination of the interference caused by moisture in the sample has been carried out under field conditions Instead the differences between the determined reference value nominal value and the measured value of the respective candidate system were calculated for days of more than 70 relative humidity during field test and the average difference was set as a conservative estimation of the interfering effect of humidity contained in the measured medium In addition the reference equivalence functions were determined from the field investigations for days of more than 70 relative humidity for both candidate systems 6 4 Evaluation The average difference between the determined reference value nominal value and the measured value of the respective candidate system was calculated for days of more than 70 relative humidity during field test and the relative deviation of the average concentra tion was
329. remains in a stabilizing phase Stabilizing after the return of the power supply until reaching a stabilized condition regarding the instrument temperatures The duration of the stabilizing phase depends on the ambient conditions at the sampling test site and on the thermic instrument condition when switching on In the scope of the suitability test the stabilizing times were between 30 min and 90 min After reaching of the stable condition the device starts to collect first data Collecting Data This data are not used yet for the determination of the mass concentrations The collecting of the first data is followed by first computing of data Computing Data Afterwards the device is ready to operate Fully operational The intermediate steps Collecting Data and Compu ting Data take one hour Afterwards the device delivers moving 1h average values of the mass concentrations which are updated every 6 minutes refer to point 6 1 4 1 4 Set up times and warm up times 6 5 Assessment All instrument parameters are protected against loss through buffering After the power sup ply has returned the measuring device goes back into a failure free operational condition and continues independently the measuring operation after achieving the instrument status fully operational Minimum requirement fulfilled yes 6 6 Detailed representation of the test results Not required for this minimum requirement 74030
330. rence pg m PM 1405F FDMS pg m gt Figure 74 Reference vs candidate SN 20107 measured component PM10 values 2 30 g m 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH w Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B page 161101422 6 1 5 4 11 Application of correction factors and terms If the highest resulting expanded uncertainty of the candidate method is larger than the ex panded relative uncertainty which is defined in the requirements on the data quality of ambi ent air measurements according to EU Guideline 7 the application of correction factors or terms is permitted The corrected values have to fulfill the requirements according to point 9 5 2 2 et seqq of the Guide Demonstration of Equivalence of Ambient Air Monitoring Meth ods The tests are performed as well for the component PM10 6 2 Equipment Not required for this minimum requirement 6 3 Performance of test Refer to module 9 5 2 2 9 5 6 6 4 Evaluation If evaluation of the raw data according to module 9 5 2 2 9 5 6 leads to a case where Wc gt Wago which means that the candidate systems is not regarded equivalent to the reference method it is permitted
331. resentation of the 2 digit Channel Number for example K0 075 048 The Channel Number is always 2 digits in length RS Para 3 13010 Optional Up to 3 ASCII codes can be added to response from the instrument In this case lt CR gt and lt LF gt ASCII codes 013 and 010 are appended to the response Enter 0 if nothing is to be appended COCO fe meer ev oewmion Ask Register command 2 digit Channel Number as defined Number of current status conditions of current status conditions a aaa ae ee DEREN Program Register Code of the variable hose value is being requested The Program Register Code of the a w A variable whose value is being PRC may be up to 3 digits long and is requested The PRC may be up to 3 ae not right filled in the response digits long Do not right fill if the Ts sf 7 Current value of the variable referenced length oes D ooe M ee 0 ee B 4 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Appennix B SERIAL COMMUNICATION AK Protocol Ask Register Command AREG continued Transmission to Instrument Response from Instrument ee Up to 3 digits appended to the end of the response transmission according to the entry for RS Para 3 Description of Status Codes PRC 008 1 Mass Transducer 2 Temperature 4 Flow Rate 8 Filter Exchange 16 Voltage pes w a O 37 im lt e BEM THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F B 5 Ap
332. resentation of the test results Refer to point 6 4 of this module 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Page 74 of 422 Report No 936 21209885 B 6 1 5 2 1 Certification ranges The certification range for the testing must be determined 6 2 Equipment No additional equipment required 6 3 Performance of test The certification range for the testing must be determined 6 4 Evaluation Standard VDI 4202 Part 1 contains the following minimum requirements for the certification ranges for particulate ambient air measuring devices Table 9 Certification ranges CR Measured com Lower limit Upper limit Limit value Evaluation period ponent of CR of CR in ug m in pg m in g m PM 0 100 50 24h The certification range is oriented at the limit value of the smallest assessment period of the measuring device in the range of the limit value This assessment of the measuring device in the range of the limit value is made within the scope of the determination of the advanced uncertainty of the candidates according to the Guide 5 For this purpose according to the Guide the following values are used as reference value
333. rinciple used in the tapered element oscillating 0 per ation microbalance TEOM mass transducer Figure 1 2 is similar to that of a laboratory microbalance in that the mass change detected by the sensor is the result of the measurement of a change in a parameter in this case frequency that is directly coupled via a physical law or from first principles to that mass change Figure 1 2 Schematic of mass transducer _ Exchangeable TEOM Filter Cartridge Frequency Counter THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 1 7 Section 1 INTRODUCTION 1 8 Operatine Guine TEOM 1405 F The tapered element at the heart of the mass detection system is a hollow tube clamped on one end and free to oscillate at the other An exchangeable TEOM filter cartridge is placed over the tip of the free end The sample stream is drawn through this filter and then down through the tapered element The tapered element oscillates precisely at its natural frequency much like the tine of a tuning fork An electronic control circuit senses this oscillation and through positive feedback adds sufficient energy to the system to overcome losses An automatic gain control circuit maintains the oscillation at a constant amplitude A precision electronic counter measures the oscillation frequency with a 10 second sampling period The tapered element is in essence a hollow cantilever beam with an associated spring rate and mass As in any spring
334. ring range 0 1 000 ug m Standard Upper limit of the certification range PMio 100 ug m 6 5 Assessment A measuring range of 0 1 000 ug m is set by default Other measuring ranges up to a maximum of 0 1 000 000 g m are possible The measuring range value of the measuring device is higher than the respective upper limit of the certification range Minimum requirement fulfilled yes 6 6 Detailed representation of the test results Not required for this minimum requirement 740300_2011_936_21209885B_eng doc aT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 76 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 1 5 2 3 Negative output signals Negative output signals or measured values may not be suppressed life zero 6 2 Equipment No additional equipment required 6 3 Performance of test The AMS was tested on its ability to display negative output signals in the laboratory and in the field 6 4 Evaluation The AMS was tested on its ability to display negative output signals in the laboratory and in the field 6 5 Assessment Negative measuring signals are displayed directly and are output correctly via the respective measured value outputs by the measuring system
335. rity Lack of fit not relevant for particulate devices 6 1 5 3 7 Sensitivity coefficient of the surrounding temperature no minimum requirement defined 6 1 5 3 8 Sensitivity coefficient of the electric voltage no minimum requirement defined 6 1 5 3 11 Standard deviation from paired measurements no minimum requirement defined 6 1 5 3 12 Long term drift no minimum requirement defined 6 1 5 3 13 Short time drift not relevant for particulate devices 6 1 5 3 18 Overall uncertainty not relevant for particulate devices For this reason an official request to the competent German body was made to define a co ordinated procedure for dealing with inconsistencies in the Standard 740300_2011_936_21209885B_eng doc aT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 86 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B The following procedure was suggested The test points 5 3 2 5 3 7 5 3 8 5 3 11 and 5 3 12 are evaluated as before based on the minimum requirements stated in Standard VDI 4202 Part 1 from 2002 i e using the refer ence values Bo B and Bz The testing of the test points 5 3 3 5 3 4 5 3 13 and 5 3 18 is waived as they are not rele vant for particulate measuring devices
336. rts or software furnished to Seller by third party suppliers shall be limited to the assignment by Seller to Buyer of any such third party supplier s warranty to the extent the same is assignable In no event shall Seller have any obligation to make repairs replacements or corrections required in whole or in part as the result of i normal wear and tear ii accident disaster or event of force majeure iii misuse fault or negligence of or by Buyer iv use of the Products in a manner for which they were not designed v causes external to the Products such as but not limited to power failure or electrical power surges vi improper storage of the Products or vii use of the Products in combination with equipment or software not supplied by Seller If Seller determines that Products for which Buyer has requested warranty services are not covered by the warranty hereunder Buyer shall pay or reimburse Seller for all costs of investigating and responding to such request at Seller s then prevailing time and materials rates If Seller provides repair services or replacement parts that are not covered by the warranty provided in Section 9 of the Terms and Conditions of Sale agreement Buyer shall pay Seller therefore at Seller s then prevailing time and materials rates With respect to spare parts the above referenced warranty applies however such warranty is limited to ninety 90 days from the date of shipment ANY INSTALLATION MAINTENAN
337. rurart Prraare we i aa I Cownived Snip bate Last Downoad or Selected Dote and Tine Ment dosenload wil start with dete alter 3i Jon D007 Oe 2 20 ER 3 22 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 3 Basic OPERATION Finding Instruments You may use the ePort software to search for all instruments connected to On a Network the local network This function will only locate instruments on a local network To connect to instruments on other connected networks you must know the IP address of the instruments and connect to the unit manually using the New Instrument function of the software Figure 3 23 Refer to the previous section for information on connecting to an instrument off the local network Instruments on a network must have a unique IP address or be connected through a router To locate all instruments on the network 1 Open the ePort software program and select Find Samplers in the Open screen Figure 3 22 2 The ePort Main screen will display with a Searching for Figure 3 26 Instruments message As instruments are located by the software ePort Main screen with they will be added to the list in the Instrument frame on the left side of Searching for Instruments the screen Figure 3 26 message Pie minar t Help a A 1406420016085 1406420017085 W 140600018085 g 126509 wW n5 aa 12365789 THERMO FISHER SCIENTIFIC 1234567890 DichotFO
338. s PM Reference is made to test point 6 1 the instruments in this report 50 yg m 5 4 10 Calculation of the expanded uncertainty of 6 5 Assessment The assessment of the measuring device in the range of the relevant limit values is possible Minimum requirement fulfilled yes 6 6 Detailed representation of the test results See test point 6 1 this report 5 4 10 Calculation of the expanded uncertainty of the instruments in 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH w Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Pade oases 6 1 5 2 2 Measuring range The upper limit of the measuring range shall be greater or equal to the upper limit of the certi fication range 6 2 Equipment No additional equipment required 6 3 Performance of test It was tested whether the upper limit of measuring range of the measuring system is greater or equal to the upper limit of the certification range 6 4 Evaluation At the measuring devices measuring ranges up to a maximum of 0 1 000 000 ug m can be set theoretically As appropriate default setting of the analogue output for European conditions a measuring range of 0 1 000 yug m is recommended Measu
339. s According to the decision of the com petent German body see module 5 3 1 reference is made alternatively to the following pre vious version of Standard VDI 4202 Part 1 June 2002 The temperature dependence of the zero point measured value shall not exceed the refer ence value By when changing the surrounding temperature by 15 K in the range between 5 C and 20 C or respectively by 20 K in the range between 20 C and 40 C The temperature dependence of the measured value in the range of the reference value B shall not exceed 5 of the measured value when changing the surrounding temperature by 15 K in the range between 5 C and 20 C or respectively by 20 K in the range between 20 C and 40 C 6 2 Equipment Climate chamber for the temperature range 8 to 25 C zero filter for zero point check Ko test kit for reference point check 6 3 Performance of test The permitted surrounding temperature at the test site of the measuring device pursuant to the manufacturer is 8 C to 25 C For this reason the test was limited to this surrounding temperature For the investigation of the dependence of the zero point and the measured values on the surrounding temperature the complete measuring devices were run in the climatic chamber For the zero point check the two candidates SN 20006 and SN 20107 by installation of zero filters were fed at both device inlets each with particulate free sampling air For the
340. s 100 23 during field test for the complete data set The maximum deviation found at ze 102 ro point was 1 5 g m with reference to the previous value and 1 6 g m with reference to the start value and are thus within the allowed range of BO 2 ug m The values for the drift of the sensitivity referring to the re spective previous values determined within the scope of the test have been at maximum 1 3 for PM10 Not applicable 108 740300_2011_936_21209885B_eng doc A TUVRheinland Precisely Right Page 24 of 422 5 3 14 Response time 5 3 15 Difference be tween sample and calibration port 5 3 16 Converter effi ciency 5 3 17 Increase of NO2 concentration due to residence in the measuring system 5 3 18 Overall uncer tainty TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B filled The response time rise of the measuring system shall not ex ceed 180 s The response time fall of the measuring system shall not ex ceed 180 s The difference between the re sponse time rise and re sponse time fall of the meas uring system shall not exceed 10 of response time rise or 10 s whatever value is larger The difference between the measured valu
341. s 2000 7 Directive 2008 50 EC of the European Parliament and of the Council of May 21 2008 on ambient air quality and cleaner air for Europe 8 Report UK Equivalence Programme for Monitoring of Particulate Matter Report No BV AQ AD202209 DH 2396 of June 5 2006 740300_2011_936_21209885B_eng doc TUVR h T V Rheinland Energie und Umwelt GmbH ein and Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 170 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 9 Appendix Appendix 1 Measured and calculated values Annex 1 Detection limit Annex 2 Temperature dependency of zero point Annex 3 Temperature dependency of the sensibility Annex 4 Dependency on supply voltage Annex 5 Measured values at the field test sites Annex 6 Surrounding conditions at the field test sites Appendix 2 Filter weighing procedure Appendix 3 Manuals 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B TUVRheinland Precisely Right Page 171 of 422 Annex 1 Detec
342. s been used The instrument will always show a nonzero value even if no filter is mounted in the mass transducer New filters generally exhibit filter loading percentages of 15 to 30 at a flow rate of 3 1 min and less at lower flow rates TEOM filter cartridges must be exchanged before this value reaches 100 to ensure the validity of the data generated by the instrument At some point above 100 the main flow drops below its set point If the filter loading percentage is higher than 30 when a new TEOM filter is placed on the mass transducer or if the lifetime of consecutive TEOM filter cartridges becomes noticeably shorter inspect the in line filter for the flow line Section 5 and replace it if necessary THERMO FISHER SCIENTIFIC Figure 4 3 Number entry keypad showing current value and setpoint THERMO FISHER SCIENTIFIC Section 4 SCREENS AND SETTINGS Users enter values into the settings screens using a number keypad Figure 4 3 Select the button for the value that needs to be changed such as setpoints for flow rates temperatures or pressures and a keypad will automatically display The keypad will display the current setpoint and the current value when applicable Enter the value into the keypad then select the Enter button to set the value or press the Cancel button to exit the keypad screen and return to the screen Cap temperature 0 00 C Cap temperature set point 30 00 C Operatine Guine TEOM 1405 F 4 5
343. s between the reference devices Urer from the field tests In Table 33 a summarized representation of the results of the equivalence test incl the determined expanded measuring uncertainties Wcw from the field test is shown 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 19301482 Table 32 In between instrument uncertainty Uret of the reference devices for PM Reference Test site Amount Uncertainty ups device values Teddington Winter 67 i 83 Cologne Winter 268 All test sites The uncertainty between the reference devices U e is for all test sites lt 2 ug m Table 33 Summary of the results of the equivalence test SN 20006 amp SN 20107 measured component PM raw data 23 3 gt 28 ug m3 Orthogonal Regression Betw een Instrument Uncertainties PM10 1405F FDMS a ea Slope b up Intercept a ua Reference Candidate All Data 215 0 973 0 994 0 011 0 395 0 291 lt 30 ug m3 169 0 882 1 055 0 028 0 567 0 501 gt 30 ug m3 46 0 963 0 992 0 029 0 218 1 274 Orthogonal Regression Limit Value of 50 ug m 3 ERA Slope b up Intercept a ua Wem gt
344. s of gaseous and particu late pollutants September 2010 or August 2004 2 e Standard EN 12341 Ambient air quality Determination of the PMio fraction of sus pended particulate matter Reference method and field test procedure to demon strate reference equivalence of measurement methods German version EN 12341 1998 3 e Guide Demonstration of Equivalence of Ambient Air Monitoring Methods English version of January 2010 4 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 29 el 422 3 Description of the tested measuring system 3 1 Measuring principle The ambient air measuring system TEOM 1405 F Ambient Particulate Monitor is based on the measuring principle of oscillating micro weighing For the weighing principle which is used in the TEOM mass transducer in the measuring system TEOM 1405 F Ambient Particulate Monitor the change in mass determined with the sensor results from the measurement of the change in frequency of the tapered element The tapered element at the heart of the mass detection system is a hollow tube clamped on one end and free to oscillate at the other An exchangeable TEOM fil
345. s voltage Cycle 2 TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Standards RP Cycle 3 Page 1 of 1 Ko Test SN 20006 Voltage V Measured value Ko 14869 8 14932 1 14937 7 14957 5 14938 1 Measured value Kg 14875 9 14927 6 14875 3 14943 2 14900 0 Dev SN 20107 Measured value Ko Measured value Ko Dev V ia 6 740300_2011_936_21209885B_eng doc 17213 3 17283 1 17265 2 17274 6 17256 4 17270 2 17247 2 17221 8 17283 3 17239 3 Measured value Ko Measured value Ky Dev TUV Rheinland Energie und Umwelt GmbH TUVRheinland 8 Luftreinhaltung z Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 175 of 422 Annex 5 Measured values from field test sites related to actual conditions Page 1 of 22 Manufacturer Thermo Fisher Scientific Suspended particulate matter PM10 Type of instrument TEOM 1405 F Measured values in yg m ACT Serial No
346. se period sample is collected normally and the base mass concentration is determined During the reference period the flow is diverted through a chilled filter to remove and retain the non volatile and volatile PM Under normal operation the chiller is maintained at a temperature of 4 C However under ambient conditions of high temperature and humidity operating the chiller at 10 C is recommended to prevent condensation in the chiller during instrument operation Based upon mass concentration MC measurements obtained during the base and reference periods the FDMS system updates a one hour average of the following results every six minutes e Base mass concentration Base MC PM concentration of the particle laden sample stream e Reference mass concentration Ref MC PM concentration of the particle free sample stream after passing through the chilled filter e Mass concentration MC Base mass concentration Base MC adjusted by the reference mass concentration Ref MC Base MC usually positive minus Ref MC negative when mass volatilizes from the filter For example the unit draws a base flow for six minutes and measures a mass concentration of 5 g m Base MC 5 Then the unit draws a reference flow for six minutes and measures a mass concentration of 1 ug m Ref MC 1 Therefore the mass concentration is 6 ug m THERMO FISHER SCIENTIFIC Section 1 INTRODUCTION Mass Transducer the weighing p
347. select the Mass Calculation Variables Mass Transducer or Serial Number buttons to set advanced frequency parameters and check the KO constant and serial number Select the Setial Number button to display the Serial Number screen The screen shows the instrument s serial number DO NOT adjust this value Select the Mass Calculation Variables button to display the Mass Calculation Variables screen The Mass Calculation Variables screen contains the following control buttons System wait time This field contains the length of time sec in which the temperatures and flow rates must remain within a range around their setpoints before the instrument changes from Stabilizing Mode to Col lecting Data Mode The default setting is 1800 seconds To adjust the setpoint select the button to display the keypad Note Thermo Scientific recommends that the user set the Wait Time to 1000 or higher to avoid damaging the instrument and to maintain accurate data reporting a THERMO FISHER SCIENTIFIC THERMO FISHER SCIENTIFIC Section 4 SCREENS AND SETTINGS Frequency gate time The basis of mass change is raw frequency Raw frequency is calculated by comparing cycle counts of a highly stable 10 megahertz Mhz clock to the cycle counts of the oscillating tapered element TE The gate time controls how often the comparisons are made To adjust the setpoint select the button to display the keypad DO NOT adjust this value
348. sher Scientific Suspended particulate matter PM10 Auf enluft Type of instrument TEOM 1405 F Measured values in g m STD Serial No SN 20006 amp SN 20107 No Date Ref 1 Ref 2 Ref 1 Ref 2 Ratio SN 20006 SN 20107 Remark Test site PM2 5 PM2 5 PM10 PM10 PM2 5 PM1q PM10 PM10 yg m g m ug Nm ug Nm ug Nm yg Nm 181 2 24 2011 35 8 35 9 37 6 39 0 Cologne 182 2 25 2011 30 6 30 1 31 5 30 6 Winter 183 2 26 2011 19 5 19 4 184 2 27 2011 15 6 15 1 15 8 16 1 185 2 28 2011 44 3 44 0 43 0 44 0 186 3 1 2011 75 5 75 3 72 9 76 9 187 3 2 2011 60 6 59 0 59 2 61 0 188 3 3 2011 50 6 49 1 48 3 49 5 189 3 4 2011 PM10 Grubbs outlier Inlet gt Zero filter 190 3 5 2011 Zero filter 191 3 6 2011 13 5 14 1 Zero filter 192 3 7 2011 13 7 12 5 Zero filter 193 3 8 2011 44 7 45 0 43 7 43 2 194 3 9 2011 31 2 29 6 29 4 29 8 195 3 10 2011 Power cut complete 196 3 11 2011 34 2 34 0 30 6 32 4 197 3 12 2011 32 5 35 1 198 3 13 2011 16 9 16 4 15 7 16 2 199 3 14 2011 28 6 26 6 Power cut only Thermo 200 3 15 2011 46 1 45 5 46 0 46 8 201 3 16 2011 70 2 69 1 69 1 71 2 PM2 5 Grubbs outlier 202 3 17 2011 69 4 69 1 68 7 70 5 203 3 18 2011 38 9 39 2 37 8 39 0 204 3 19 2011 18 3 19 1 205 3 20 2011 28 5 28 3 27 2 28 7 206 3 21 2011 34 7 34 6 34 3 31 5 207 3 22 2011 56 3 55 8 55 3 51 1 208 3 23 201
349. sisacasasonsvinsveseastaveivecavaacenstint 1 1 Overview Of Manual sosstescserier sensone Nena EEE Eaa NEEE EAER 1 4 Applicaton RaMp Eanna a 1 5 Theory of OperatiOi ccscincisanivctrscindsmycinctetimananomnnavanmnadusinna 1 6 Mass Transd cer OperatiOnsssnisii tioin osanna Ea a 1 7 Mass Flow Controll rSiassianeeninmnunniininnn unia n 1 10 Section2 Section 2 Setup and Installation cccsccssssseescesseeseseeeseeeeensens 2 1 Installation Considerations ercstscvdvetsseadsncaseieransasnsesiisansauntasnssneviannsvesanbists 2 2 Standard System TL APA AEE yas uisdipsauvsssinieieratscathennnearanceniagesdinlaieaequaedipiaiieatts 2 3 PUI Connections ssssrsretiavepetrepanieeniaiinacrwaerwerivenmieiatncrtenannnaaias 2 4 Adjusting the Flow Splittetiecsresnanininiainiinnnei aai 2 6 Assembline the Ta pod erra 2 8 Installing the Tralet sciccsiscatsatsnonsesssnssstbesstvintectelsnopesss sates sinsnsendusenidentbiatavnteives 2 9 Applying Power to the Insttument ssiiinsissiisssiinsiiiiisisniiisinsi 2 15 Turning Off the Instrument spisie aiani ianiai 2 17 Rest rting the Li itr esaeo esasen En a EEE ina i 2 17 Using the Outdoor Shelter ss sssssissisisisrsiresisesssussivssiresenssanesinsisiniseiesirassness 2 18 Section3 Basic Operation viissstivecersueinasi ixtantencsesranicatiiniviterie ineadicinnlendievorss 3 1 Startno the TNStr mMENt s sisssiinir rsin ierni yisi ET r etena r enisi 3 2 Petforming a Teak Check onesie iisninirin iion an 3 4 St ting Data Mn ne
350. splay Attach the leak check flow audit adapter to the top of the flow splitter 10 Slowly close the valve on the leak check adapter Select the Next gt button 11 The Stabilizing screen will display Allow 1 minute for the flows to stabilize then select the Next gt button 12 Slowly open the leak check adapter valve Select the Next gt button Failure to release the vacuum before proceeding may damage the seals in the switching valve THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 3 7 Section 3 Basic OPERATION 13 The Select Valve Position screen will once again display this time with the just completed valve position unavailable Select the second valve position Figure 3 8 and select the the Next gt button Figure 3 7 F Leak Check Wizard screen Select TEOM en with completed valve i denai Figure 3 8 pF Leak Check Wizard screen with second valve position 14 The Replace Inlet screen will display Slowly open the leak check valve to restore flow to the system Remove the flow audit leak check adapter and attach the inlet to the top of the sample inlet tube Figure 3 5 Select the Next gt button 3 8 Operatinc Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 3 Basic OPERATION After completing the leak check with the FDMS in both the base and reference positions the select valve position screen will again appear but this time with both valve positions desabled Select the Next gt b
351. sponsibility for consequential damages Use of this product in any manner not intended by the manufacturer will void the safety protection provided by the equipment and may damage the equipment and subject the user to injury Preface Equipment Rating The following information can be used to determine the power service FUSES Ref Designation Main Fuse 2 F201 F202 F203 F204 F201 F206 F401 402 VI Operatine Guine TEOM 1405 F requirements of this product Line Voltage 440VA 47 63 Hz IMPORTANT Disconnect the power cord from the power source output while servicing the instrumentto prevent electrical hazard a Environmental Ranges The instrument and its sample pump must be installed in a weather sheltered location that is heated in the winter and air conditioned in the summer Note There may be hazardous line wire accessible inside the enclosure amp Installation Category Category 11 Current Rating Location F 4A 250VAC F 5A 250VAC F 4A 250VAC F 1A 250VAC F 2A 250VAC F 2A 125VAC T 6 3 250VAC Input Module Power Distribution Board Power Distribution Board Power Distribution Board Power Distribution Board Head Controller Board FDMS Board THERMO FISHER SCIENTIFIC Electrical Safety Certifications CE Disposal of the Instrument THERMO FISHER SCIENTIFIC Preface The product has been tested and has been documented to be in compliance with the following U S
352. ss sensitivity The interference caused by No interference caused by moisture in moisture in the sample may not the sample gt 1 9 g m deviation from exceed 10 of the limit value in the range of the limit value 5 4 6 Averaging effect The measuring system shall al low for formation of 24 h aver ages The time of the sum of all filter changes within 24 h may not exceed 1 of this averaging time Constancy of The sample volumetric flow sample volumet averaged over the sampling ric flow time shall be constant within 3 of the rated value All in stantaneous values of the sample volumetric flow shall be within a range of 5 of the rated value during sampling Tightness of the The complete measuring sys measuring sys tem shall be checked for tight tem ness Leakage shall not ex ceed 1 of the sample volume sucked 740300_2011_936_21209885B_eng doc nominal value for PM10 could be ob served During the field test no negative in fluence on the measured values could be noted at changing relative humidi ties The comparability of the candi dates with the reference method ac cording to Guide Demonstration of Equivalence of Ambient Air Monitor ing Methods 4 also is given for the days with a relative humidity gt 70 The formation of valid daily averages is possible All determined daily averages deviate less than 3 all instantaneous values less than 5 from the nomi
353. stem TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 13501484 The graphical representation of the flow rates for PMio Nominal 3 l min and the total flow rate Nominal 16 67 l min show that all values determined during sampling deviate less than 5 from the respective nominal value The deviation of the 24h average for the total flow rate of 16 67 l min are as well significantly smaller than the demanded 3 of the nominal value All determined daily averages deviate less than 3 all instantaneous values less than 5 from the nominal value Minimum requirement fulfilled yes 6 6 Detailed representation of the test results In Table 27 and Table 28 the determined parameter for the flow are shown Figure 49 to Fig ure 54 show the graphical representation of the flow measurements at both candidates SN 20006 and SN 20107 Table 27 Parameter for the total flow measurement 24h average Cologne Winter SN 20006 No of 24h values Average l min Dev from nominal value Std Dev l min Max l min Min l min 16 65 0 096 1 77 1656 Table 28 Parameter for the total flow measurement 24h average Cologne Winter SN 20107 No of 24h values Average l min Dev from nominal value Std Dev l min Max l min Min l min 16 67 0 001 73 16 59 740300_2011_936_21209885B_eng
354. suring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Page 176 of 422 Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Annex 5 Measured values from field test sites related to actual conditions Page 2 of 22 Manufacturer Thermo Fisher Scientific Suspended particulate matter PM10 Type of instrument TEOM 1405 F Measured values in yg m ACT Serial No SN 20006 amp SN 20107 No Date Ref 1 Ref 2 Ref 1 Ref 2 Ratio SN 20006 SN 20107 Remark Test site PM2 5 PM2 5 PM10 PM10 PM2 5 PM10 PM10 PM10 ug m ug m yg m ug m ug m yg m 31 1 8 2010 14 6 14 9 80 3 16 5 Device not yet in Teddington 32 1 9 2010 7 1 6 9 47 4 13 2 operation Winter 33 1 10 2010 16 0 16 1 82 9 17 3 34 1 11 2010 45 7 46 2 89 1 48 7 SN 20107 Zero filter 35 1 12 2010 43 2 43 6 90 4 47 6 47 2 36 1 13 2010 48 0 48 3 90 6 51 4 52 8 37 1 14 2010 14 1 14 4 87 5 17 1 17 5 38 1 15 2010 14 6 14 4 53 6 19 2 19 9 39 1 16 2010 6 5 6 1 46 1 10 7 11 4 40 1 17 2010 11 0 10 5 52 3 17 3 17 9 41 1 18 2010 21 0 20 4 76 7 24 9 25 6 42 1 19 2010 20 4 20 2 76 4 Power supply interrupted 43 1 20 2010 26 6 27 0 83 8 28 3 29 5 44 1 21 2010 20 5 20 9 75 0 23 9 23 7 45 1 22 2010 7 8 7 6 78 5 9 2 10 1 46 1 23 2010 21 0 20 9 82 3 23 1 23 3 47 1 24 2010 16 2 15 9 78 4 18 5 18 4 48 1 25 2010 36 1 35 8 85 1 39 8 49 1 26 2010 50 7 51 1 84 2 55 7 56 7 50 1 27 2010 27 1 27 3 69 7 33 9 33 2 51 1 28 2010 8 3 8 0 58 3
355. t Particulate Monitor The instrument will be put in Setup mode tor calibration To continue press Next Next gt Cancel 3 The Select a Flow Audit Device screen will display Select a flow audit device Select Direct Flow Device to audit the flow using a direct flow measuring device reading l min adjusted for temperature and pressure such as the Streamline Pro Select FTS to audit the flow using the FTS system FTS users will enter the device calibration constant and the change in pressure from the FTS Select the Next gt button 4 The Select Flow to Calibrate screen will display Select the Calibrate Main Flow or Calibrate Bypass Flow button to calibrate the selected flow Select the Next gt button THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 5 51 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 5 The wizard will prompt you to attach a flow meter to the appropriate flow channel a To calibrate the main flow channel remove the inlet and attach the 1 1 4 inch flow adapter meter to the top of the flow splitter Figure 5 64 Disconnect the bypass line from the side of the flow splitter don t let it fall to the ground and cap the bypass fitting with the 3 8 inch Swagelok cap provided with the system Figure 5 65 Figure 5 64 Flow adapter meter attached to the flow splitter Flow meter adapter Figure 5 65 Bypass line capped Bypass cap 5 52 Operatine Guine
356. t it must have a valid IP address Figure 3 14 Back of instrument Ethernet connection THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 3 13 Section 3 Basic OPERATION Installing ePort Users must first install the ePort software on a personal computer PC connected to the same network as the TEOM 1405 that data will be downloaded from At the same time the ePort software is installed the installer will install Microsoft NET Framework software if the PC does not already have an up to date version of NET Framework To install the ePort software 1 Locate and double click on the setup ePort _XX exe file where XX is the version number on the software CD that came with the TEOM 1405 monitor The Welcome to InstallShield Wizard screen will display Figure 3 15 Figure 3 15 Fear enero eR Teen ePort Welcome to InstallShield Wizard screen Welcome to the InstallShield Wizard for ePort 0 12 8 The InstallShield R Wizard will install ePort 0 12 8 on your computer To continue click Next WARNING This program is protected by copyright law and international treaties 2 Select the Install button 3 The wizard will display the software license agreement Select Yes then select the Next gt button 3 14 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 3 Basic OPERATION 4 The Windows update screen will display Figure 3 16 If you have recently updated you
357. t Response from Instrument ere eame vesener f e Noe er f vesener RS Para 2 75048 Question marks inserted in place of unrecognizable command es a C a ane Ya Up to 3 digits appended to the end of the response transmission according to the entry for RS Para 3 B 10 Operatine Guipe TEOM 1405 F THERMO FISHER SCIENTIFIC
358. t exceed the reference value Bo within 24 h and the maintenance interval The temporal change of the measured values in the range of the reference value B shall not exceed 5 of B within 24 h and the maintenance interval 6 2 Equipment Zero filter for zero point check Ko test kit for reference point check 6 3 Performance of test The test was performed within the scope of the field test with a total time period of 22 months Within the scope of a regular check approx once a month incl at the beginning and the end of every test site the measuring device was run for a time period of at least 24 h each with zero filters at the device inlets the measured zero valued were evaluated The zero measurements were performed as planned with a monthly change of the TEOM filter and the 47 mm filter Furthermore the stability of the calibration constant was tested and evaluated for the refer ence point check at the beginning and end auf each test site 6 4 Evaluation An evaluation of the drift at zero point and the measured value within 24 h is not possible The evaluation at zero point is done on the basis of the measuring results of the regular ex ternal zero point measurements by comparing the respective values with the measured val ues of the previous test and the measured values of the first test The evaluation at reference point is done on the basis of the measuring results for the cali bration constant Ko by compari
359. t is updated every 60 minutes on the hour This value cannot be changed by the user Note Mass concentration averages of less than 24 hours can be averaged using data logging equipment to compute sliding 24 hour averages and 24 hour averages that do not necessarily start and end at midnight as well as averages on other user defined time scales A 12 Hr MC ug m This field contains the 12 hour mass concentration average This is a sliding average that is updated every 60 minutes on the hour This value cannot be changed by the user 24 Hr MC ug m This field contains the 24 hour mass concentration average This is a sliding average that is updated every 60 minutes on the hour This value cannot be changed by the user Frequency This field contains the oscillating frequency of the tapered element TE in the mass transducer This value varies from one TEOM 1405 unit to another but generally ranges between 150 and 400 Hz This value cannot be changed by the user Noise This field contains the mass transducer s performance This value should be less than 0 10 after the system has been in Operating Mode 4 for at least 30 minutes This value cannot be changed by the user Operatine Guine TEOM 1405 F 4 3 Section 4 SCREENS AND SETTINGS 4 4 Operatine Guine TEOM 1405 F Filter loading This field contains the filter loading percentage Section 5 It indicates the portion of the TEOM filter s total capacity that ha
360. t kit for reference point check 6 3 Performance of test To check the dependence of the measuring signals on the mains voltage the voltage was reduced from 230 V to 210 V and afterward increased with an intermediate step of 230 V to 245 V For the reference point check at both candidates SN 20006 and SN 20107 the calibration constant Ko was tested to check the stability of the sensitivity Since the mobile use of the AMS is not planned an additional check of the dependence of the measuring signal on the mains frequency was waived 6 4 Evaluation At reference point the change as a percentage of the determined measured value for the cal ibration constant Ko is observed for each test step in relation to the default point at 230 V As note it should be mentioned that by using the check of the calibration constant Ko no con centration values could be simulated an assessment in the range B was not possible for this reason 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Pager ordag 6 5 Assessment Due to voltage changes no deviation gt 0 4 could be detected for PMio referring to the standard value of 230 V Minimum requ
361. t not more than 2 5 of the paired values in total for each field test site may be identified and removed as outliers Within the scope of the Combined MCERTS and T V PM Equivalence Testing program we agreed with our British partners not to discard any measured value for the candidates unless the implausibility is caused due to technical reasons During the entire testing period no measured value of the candidates was discarded Table 6 shows an overview on the amount of paired values reference which were recog nized and removed as significant outliers at each test site Table 6 Results Grubbs outlier test Reference PM Graph Number i Sampler Bamber of data Maximam Numoer Number Identified Number Deleted Mumper of data pairs that can be deleted pairs remaining Teddington Summer Cologne Winter Bornheim Summer Teddington Winter 740300_2011_936_21209885B_eng doc WT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 56 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B The following data pairs were removed Table 7 Removed data pairs reference PM according to Grubbs Test site Date Reference 1 ug m Reference 2 ug m Teddington Winter 22 12 2009 32 7 34
362. t the field test sites Page 2 of 11 No Date Test site Amb temperature avg Amb temperature max Amb pressure Rel humidity Wind velocity Wind direction Precipitation C C hPa m s mm 31 1 8 2010 Teddington 1 6 1 6 1022 91 1 0 8 225 0 3 32 1 9 2010 Winter 0 9 2 2 1018 79 3 1 8 161 0 0 33 1 10 2010 1 4 2 8 1015 90 5 0 7 92 1 3 34 1 11 2010 1 5 2 4 1015 86 0 0 3 137 0 3 35 1 12 2010 1 4 2 8 1000 85 9 1 5 103 0 0 36 1 13 2010 1 5 3 0 998 94 8 0 1 151 8 6 37 1 14 2010 2 5 4 4 1008 97 0 0 1 229 0 3 38 1 15 2010 5 6 6 7 1011 90 0 1 8 151 1 8 39 1 16 2010 5 7 7 8 1003 96 3 0 4 202 9 1 40 1 17 2010 4 1 9 4 1019 93 9 0 1 219 0 0 41 1 18 2010 6 2 7 8 1021 97 8 0 1 199 0 0 42 1 19 2010 6 4 8 7 1012 83 7 1 4 111 1 0 43 1 20 2010 3 0 3 9 1012 92 1 0 2 227 3 8 44 1 21 2010 6 1 8 3 1015 85 2 1 1 154 0 3 45 1 22 2010 7 6 8 6 1014 95 0 0 5 209 7 4 46 1 23 2010 4 8 6 7 1018 87 0 0 2 262 0 0 47 1 24 2010 4 4 6 7 1022 91 1 0 1 241 1 3 48 1 25 2010 3 2 5 0 1033 80 0 0 9 161 0 5 49 1 26 2010 0 0 3 3 1037 83 2 0 5 167 0 0 50 1 27 2010 4 4 7 2 1018 85 5 0 3 247 1 0 51 1 28 2010 5 5 7 6 1000 86 4 0 5 247 8 1 52 1 29 2010 1 3 6 2 992 76 9 0 9 279 0 3 53 1 30 2010 0 9 4 5 1001 84 4 0 2 240 0 0 54 1 31 2010 0 0 4 0 1005 91 2 0 1 241 0 0 55 2 1 2010 3 1 TA 1010 83 9 0 4 222 0 3 56 2 2 2010 5 9 8 4 1002 89 6 0 3 229 1 0 57 2 3 2010 6 7 8 9 1004 91 0 0 2 180 2 0 58 2 4 2010 7 6 8 9 997 86 1 1 3 153 2 3 59 2 5 2010 7 2 12 8 1000 84 9 0 6 14
363. ta will be incorrect To adjust the value select the button to display the keypad a Operatine Guine TEOM 1405 F 4 31 Section 4 SCREENS AND SETTINGS Service Screen Figure 4 25 Service screen 4 32 Operatine Guine TEOM 1405 F The Service button displays the Service screen Figure 4 25 and provides access to maintenance and verification wizards and procedures as well as advanced troubleshooting and service tools TEOM 1405 F Serice System Status Instrument Conditions Senings sopra Worse _ RETF When in the Service screen select the Maintenance Verification Calibration Install Uninstall Accessories Advanced and Instrument Control buttons to reach the desired screens Figure 4 26 Note Refer to Section 5 for information on the Maintenance Verification Calibration Install Uninstall Accessories screens and other screens accessible through those buttons a THERMO FISHER SCIENTIFIC Section 4 SCREENS AND SETTINGS 26 4 igure F Screens accessible through the Service screen uoneiqijes 3ndjno Bojeuy uonesqued Mold uonemqued quaiquiy ainpayos uonesqujed t i j SUOISIOA mud NLA SINGS I1S L ssedAq urew moja H Eqn Aly Jayeay ese JayeayH deg WO3L suonouny quawn su aiqesiq aiqeuy i j paoueapy yooqsy dois dnjas uny 10
364. tenance e g change of TEOM filter cleaning of the cooler etc instrument checking flow rate leak test check of the calibration constant Ko instrument calibration flow rate temperature and pressure sensors and other functionalities can be obtained By using the maintenance assistant of the software the user is lead step by step through maintenance and audit work via different screens Therefore no manual is needed at the test site for the performance of this work 740300_2011_936_21209885B_eng doc ss TUV Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 42 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Besides the direct communication via operating keys display extensive possibilities exist to communicate via different analogue outputs RS232 interfaces USB interfaces as well as Ethernet interfaces The following possibilities are available 1 x 25 pin USER I O interface for analogue in and output and digital output 1 x RS232 interface for the communication via RP Comm or HyperTerminal software 1 x Ethernet interface for the connection to a PC for the data transfer and remote control via ePort software 2x USB interfaces for direct data download and firmware update For th
365. ter cartridge is placed over the tip of the free end The sample stream is drawn through this filter and then down the tapered element Sampe flow Exchangeable TEOM Fitter Cartridge er Tapered Element l l m Tor Controller Md J Figure 1 Schematic set up of the mass transducer 740300_2011_936_21209885B_eng doc TUVRh T V Rheinland Energie und Umwelt GmbH ein and Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 30 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B The tapered element oscillates precisely at its natural frequency much like the tine of a tun ing fork An electronic control circuit senses this oscillation and through positive feedback adds sufficient energy to the system to overcome losses An automatic gain control circuit maintains the oscillation at a constant amplitude A precision electronic counter measures the oscillation frequency with a 10 second sampling period The tapered element is in essence a hollow cantilever beam with an associated spring rate and mass As in any spring mass system if additional mass is added the frequency of the oscillation decreases This can be seen by observing the frequency on the display of the de vice and operating the moni
366. ter the seasonal average temperature Ave Temp and average baromettic pressure Ave Pres at the measurement site to allow the instrument to sample at the correct volumetric flow rate Section 4 The microprocessor calculates the correct mass flow set point Flow_Rate following formula srp With this information using the P x Tempg 273 15 FlowSP FlowSP x 2 ee Poy Temp ayo 273 15 where FlowSP passys Control set point to mass flow controller equivalent flow at 25 C and 1 Atmosphere FlowSP Volumetric flow rate set point l min Temp vg Average temperature entered by the user C Temp Standard temperature 25 C Pira Seasonal average barometric pressure entered by the user Atmospheres where 1 Atmosphere 1013 2 millibars or 760 mm Hg Pon Standard pressure 1 Atm Alternately Active flow control can be set up to automatically measure the ambient temperature and pressure using the hardware supplied Note When using actual conditions for active volumetric flow control substitute the actual local temperature and pressure as measured by the instrument for the average temperature and pressure variables in equation above a THERMO FISHER SCIENTIFIC THERMO FISHER SCIENTIFIC Section 1 INTRODUCTION PM 10 mass concentration data reported to the U S EPA must be referenced to standard cubic meters of air based on a standard temperature and pressure of 25 C and 1 Atmosphere
367. test Ups Algorithm for the calculation of ordinate intercept a as well as slope b and its variances by or thogonal regression are described in detail in annex B of 4 The sum of the relative residuals RSS is calculated by the following equation RSS y a bx i 1 Uncertainty uc s is calculated for e All test sites e Each test site separately e 1 data set with measured values 2 30 ug m Basis average values of the reference measurement Preconditions for acceptance of the full dataset are that e The slope b is significantly different from 1 b 1 lt 2 u b and e The intercept a is insignificantly different from 0 a lt 2 u a Where u b and u a are the standard uncertainties of the slope and intercept respectively calculated as the square root of their variances If these preconditions are not met the can didate method may be calibrated according to point 9 7 of the Guide refer to 6 1 5 4 11 Application of correction factors and terms The calibration shall only be applied to the full dataset 740300_2011_936_21209885B_eng doc aT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 150 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Point 9 5 3 The combined unc
368. the instrument Refer to the previous section for information on connecting the instrument to a network 2 In the System Status screen of the machine from which you want to download data locate and record the IP address Figure 3 21 of that unit Figure 3 21 System Status screen TANPE TEOM 1405 F ik i SS System Status System Status Operating mode Stabilizing ASz37 mode Mone Vacuum pump SSUES 10 m Enclosure temperature 1t t Instrument Protection level Lin locined IP address P address 132 188 183 129 Serial number 2458750 instrument firmerare version 102 Settings Service THERMO FISHER SCIENTIFIC 2 aiiis Haoa siie ae a 2 Operatine Guine TEOM 1405 F Section 3 Basic OPERATION 3 Start the ePort PC software using the icon on the PC desktop or the Start menu of the PC The ePort Main screen with the Open screen will Figure 3 22 display Figure 3 22 ePort Main screen with Open screen Fired Sampler Dren Saved Conkgurekon Saved Configadon Fie 4 In the ePort Open screen Figure 3 19 select create new configuration A blank ePort Main screen will display 3 20 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 3 Basic OPERATION 5 Select Instrument then New Instrument from the menu bar at the top of the ePort Main screen Figure 3 23 Figure 3 23 Selecting New Instrument from the menu bar aP ePort Edit Instrument Delete Instrument Ne
369. the system s hardware and sampling system Section 3 Basic Operation This section provides instructions on how to turn on the instrument and initiate a sampling run It also explains how to download data and how to leak check the instrument Section 4 Screens and Settings This section explains how to set up the instrument s firmware and its operating modes Section 5 Maintenance and Calibration Procedures This section describes the routine maintenance and verification procedures fot the TEOM 1405 Monitor Appendix A Troubleshooting This appendix includes the information on deciphering status codes and as well as key schematics for troubleshooting purposes Appendix B Serial Communication This appendix includes information on the instrument s program register codes and built in AK protocol THERMO FISHER SCIENTIFIC Section 1 INTRODUCTION Application Range The TEOM 1405 F Monitor is a real time device used for measuring the THERMO FISHER SCIENTIFIC particulate matter mass concentration of particulate matter TEOM instruments are the only filter based mass monitors that measure the mass of particulate matter suspended in gas streams in real time This is made possible through the use of an inertial mass transducer patented in the U S and internationally by Thermo Fisher Scientific The monitor is ideally suited for applications demanding real time air particulate matter monitoring in outdoor indoor or industria
370. ticulate Monitor for PM1o is indeed being penalised by the mathematics for being accurate It is proposed that the same pragmatic approach is taken here that was previously undertaken in earlier studies Namely as some of the individual da ta set slopes are greater than 1 and some are less there should be no need to correct the data for this slope offset In this particular case the slope for the All data comparison was 0 994 therefore no slope correction could be done The intercept for the All data comparison lays at 0 395 Therefore under point 6 1 5 4 11 Application of correction factors and terms an additional evaluation using the re spective calibration factor for the data sets is done The reworked version of the Guide of January 2010 requires that when operating in net works a candidate method needs to be tested annually at a number of sites and that the number of the instruments to be tested is dependent on the expanded measurement uncer tainty of the device The respective realisation is the responsibility of the network operator or of the responsible authority of the member state However TUV Rheinland and their UK part ners recommend that the expanded uncertainty for the full data set is refered to for this namely 8 4 which again would require an annual test at 2 measurement sites Guide 4 chapter 9 9 2 table 6 Detailed representation of the test results Table 32 shows an overview on the uncertaintie
371. tification range Note This test point is not evaluable for particulate measuring devices on the basis of the currently valid version of Standard VDI 4202 Part 1 September 2010 and VDI 4203 Part 3 Septem ber 2010 due no non defined minimum requirements According to the decision of the com petent German body see module 5 3 1 reference is made alternatively to the following pre vious version of Standard VDI 4202 Part 1 June 2002 The detection limit of the measuring device shall not exceed the reference value Bo The de tection limit shall be determined during field test 6 2 Equipment Zero filter for zero point check 6 3 Performance of test The determination of the detection limit is done for the candidates SN 20006 and SN 20107 by operating the devices with the respective zero filters which are installed at both measuring device inlets The offering of particulate free sampling air is done for a time period of 15 days for 24 h each The determination of the detection limit is done in the laboratory because under field condi tions a provision of particulate free air for such a long time period was not possible 6 4 Evaluation The detection limit X is determined from the standard deviation Sxo of the measured values at the intake of particulate free sampling air by both candidates It corresponds with the standard deviation of the average Xo of the measured values Xo multi plied with the student factor for the respe
372. tigation on the tightness of the sampling system Investigation of the dependency of the measured values on humidity Determination of the maintenance interval Determination of availability Determination of the total uncertainty of the candidates The following devices were used for the field test e Measurement cabinet of TUV Rheinland air conditioned to approx 20 C e Weather station WS 500 of the company ELV Elektronik AG for the determination of meteorological characteristics such as air temperature air pressure air humidity wind velocity wind direction and rainfall Two reference samplers LVS3 for PMio according to point 5 Gas meter dry 1 mass flow rate measuring device Type 4043 Manufacturer TSI Measuring device Metratester 5 Manufacturer company Gossen Metrawatt for the determination of power consumption Zero filter for external zero point check e Ko check kit Two TEOM 1405 F Ambient Particulate Monitor systems and two reference devices for PM1 were simultaneously operated for 24 h each during the field test The reference equipment operates discontinuously i e the filters must be changed manually after each sample 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher S
373. tion limit Page 1 of 1 Manufacturer Thermo Fisher Scientific Type 1405F Standards ZP Measured value with zero filter Serial No SN 20006 SN 20107 No Date Measured values yg m Date Measured values yg m SN 20006 SN 20107 1 6 7 2011 1 0 10 25 2010 1 3 2 6 8 2011 1 3 10 26 2010 1 6 3 6 9 2011 0 9 10 27 2010 1 8 4 6 9 2011 0 9 10 28 2010 2 1 5 6 10 2011 0 7 10 29 2010 1 4 6 6 11 2011 0 2 10 30 2010 1 6 7 6 12 2011 0 3 10 31 2010 1 0 8 6 13 2011 1 2 11 1 2010 1 3 9 6 14 2011 1 5 11 2 2010 1 4 10 6 15 2011 1 3 11 3 2010 0 8 11 6 16 2011 1 5 11 4 2010 0 8 12 6 17 2011 1 2 11 5 2010 1 2 13 6 18 2011 0 6 11 6 2010 1 4 14 6 19 2011 1 0 11 7 2010 1 2 15 6 20 2011 0 8 11 8 2010 0 6 No of values 15 No of values 15 1 Mean 0 96 Mean 1 28 DALAS Ky Standard deviation s o 0 38 Standard deviation Sxo 0 38 a n 1 4 oi o Detection limit x 0 82 Detection limit x 0 82 740300_2011_936_21209885B_eng doc TUVRheinland Precisely Right Page 172 of 422 Annex 2 Dependence of zero point on ambient temperature Manufacturer Thermo Fisher Scientific Type 1405F Serial No SN 20006 SN 20107 SN 20006 SN 20107 x cl 740300_2011_936_21209885B_eng doc Measured value ug m yg m Measu red value ug m TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre
374. to Adjusting the Flow Splitter earlier in this section 10 Install the sample tube from the flow splitter through the roof opening Figures 2 24 and 2 25 Note Cap the extra opening in the enclosure roof a Operatine Guine TEOM 1405 F 2 21 Section 2 SETUP AND INSTALLATION 11 Install the adjustable elbow fitting and male swivel fitting from the enclosure package onto the piece of 19 inch section of pipe that came with the enclosure Lightly tighten the screws Install the elbow fitting and support pipe onto the flow splitter and enclosure top Figure 2 26 Slide the support pipe up or down until the flow splitter is sitting plumb then attach the arm to the shelter and tighten all the screws on Figure 2 26 the support arm Support pipe connections Adjustable elbow fitting Flow splitter Support pipe Male swivel fitting 2 22 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 2 SETUP AND INSTALLATION 12 Cut a piece of tubing from the remaining section of bypass tubing step 8 long enough to reach from the bypass connection to the top of the 1405 unit The section should be long enough to include a loop Figure 2 27 to ensure there will be no kinks in the line when it enters the enclosure Connect the bypass tubing to the bypass fitting on the flow splitter using the 3 8 inch Swagelok fitting Figure 2 27 Insert the other end through the fitting on the roof Figure 2 25 and into the
375. to apply a correction factor or term resulting from the regression equa tion obtained from the full data set The corrected values shall satisfy the requirements for all data sets or subsets refer to module 9 5 2 2 9 5 6 Moreover a correction factor may be applied even for Wem S Wago in order to improve the accuracy of the candidate systems Three different cases may occur a Slope b not significantly different from 1 b 1 lt 2u b intercept a significantly different from 0 a gt 2u a b Slope b significantly different from 1 b 1 gt 2u b intercept a not significantly different from 0 lal lt 2u a c Slope b significantly different from 1 b 1 gt 2u b intercept a significantly different from 0 a gt 2u a With respect to a The value of the intercept a may be used as a correction term to correct all input values y according to the following equation Y icon yi a 740300_2011_936_21209885B_eng doc aT T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 162 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B The resulting values of yicor may then be used to calculate the following new terms by linear regression Y i corr C dx and u s Yicor
376. tor both with and without a filter in place In a spring mass system the frequency is obedient to the following equation pe M With F Frequency K Spring rate M Mass K and M are consistent units The relation between mass and frequency change can me ex pressed as follows dm Ky z 1 ie ty with dm Mass change Ko Spring constant incl of the mass conversion fo Initial frequency Hz f End frequency Hz After transposing the equation it can be solved for the spring constant Ko dm 1 1 fe te Ky Therefore Ko calibration constant of the device can be determined easily by measuring the frequencies with and without known mass e g with a pre weighed TEOM Filter from the Ko calibration kit 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH F Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 3191422 3 2 Functionality of the measuring system The particle sample passes the PM1o pre separator with a flow rate of 16 67 l min 1 m h Subsequently the flow is directed over a flow splitter and divided into two sub flows the PM o flow of 3 I min and the bypass flow of 13 67 I min The PM o flow is directed to the ac tual meas
377. tric Firar Carina Report te thee bellowing ened itio tes ED Sippel Horna shat me ENE Leo The Flow Control screen contains the following control buttons gt Volumetric Flow Control Active or Passive These buttons allow the user to select active using actual temperature and pressure or passive using average temperature and pressure to adjust the flow Report to the following conditions Actual or Standard These buttons allow the user to select Actual reporting the mass concentration measured per actual volume sampled through the inlet or Standard reporting the mass concentration adjusted based on a set standard temperature and pressure e Standard temperature This field contains the standard temperature C setting The default setting is 25 C To adjust the setpoint select the button to display the keypad Figure 4 3 e Average temperature This field visible only when passive is selected contains the average temperature C setting for passive flow control The default setting is 25 C To adjust the setpoint select the button to display the keypad Figure 4 3 e Standard pressure This field contains the standard pressure atm setting The default setting is 1 atm To adjust the setpoint select the button to display the keypad Figure 4 3 Operatine Guine TEOM 1405 F 4 15 Section 4 SCREENS AND SETTINGS e Average pressure This field visible only when passive is
378. ts in the field test It shall not exceed the requirements of Table 2 of Standard VDI 4202 Part 1 September 2010 Note This test point is not evaluable for particulate measuring devices on the basis of currently val id Standard versions of the Standard VDI 4202 Part 1 September 2010 and VDI 4203 Part 3 September 2010 due to a lack of defined minimum requirements According to the deci sion of the competent authorities in Germany see Module 5 3 1 alternatively the following specifications of the previous version of Standard VDI 4202 Part 1 June 2002 are referred to The reproducibility Rp of the measuring device shall be determined with repeat determina tions of two identical measuring devices and shall not fall below the value 10 The reference value B shall be used 6 2 Equipment Additional measuring devices as stated in Chapter 5 were used when determining the repro ducibility 6 3 Performance of test Reproducibility Rp is defined as the maximum deviation of two randomly chosen single val ues which were obtained under equal conditions in relation to each other This test has been carried out with two identical devices which were simultaneously operated during the field test The measured data from all four field tests was used for this test 6 4 Evaluation The reproducibility Rp is calculated as follows n R Si a10 where U 85 timos and sp Jo 2 Xi X2 e R Reproducibility Rp at B e U Uncertainty
379. ts system variables to the original values that were set by the user However this does not set the unit to its default parameters The instrument will remain in the Stop All Mode until you select the Run button in the Instrument Control screen Operatine Guine TEOM 1405 F 4 7 Section 4 SCREENS AND SETTINGS System Status The current status condition is located in the status bar at the bottom of S creen the TEOM Data screen Figure 4 4 and most other instrument screens If there are no status conditions the field at the bottom of the screen will read Normal status Figure 4 4 If there are status conditions present the field at the bottom of the screen will read Warning s and a warning triangle will appear in the instrument title bar at the top of the screen Figure 4 5 Figure 4 4 TEOM Data screen with TEOM 1405 F Normal status message TE OM Gata System States MC pym Hahn ARE igen T Hr Bet igh B Howur value pgm iE Instrureent 12 Hr MC age Conditions BHr bet dugim Filter loading Settings Fraquancy Note ap Fuly spm Harmat status orman i5 Figure 4 5 TEOM Data screen with Warning s message and warning triangle TEGH Data System Status ME pgm ahin hE dugim 1 Hr Mee pgm B Howr walwe gim jc insbamnt 12 Hr Mt ugm Sonditions meHr ME ug Filter loading Settings Fraguaney Note aj Fly apma Waring s Eg eTA LET 4 8 Operatinc
380. tter for which the Member State concerned can demonstrate displays a consistent relationship to the refer ence method In that event the results achieved by that method must be corrected to produce results equivalent to those that would have been achieved by using the reference method 2008 50 EC Annex VI B The Guidance Demonstration of Equivalence of Ambient Air Monitoring Methods 5 which was developed by an ad hoc EC task group Source http ec europa eu environment air quality legislation pdf equivalence pdf Version January 2010 describes an equivalence check method for non standard measurement methods The specifications of the Guide for the equivalence testing were included in the last revision of the VDI Standards VDI 4202 Part 1 as well as VDI 4203 Part 3 The following limits were applied during suitability testing PM1o Daily limit value 24 h 50 yg m Annual limit value 1 a 40 ug m as well as for the calculations according to the Guide 4 PM1o Limit value 50 yg m 740300_2011_936_21209885B_eng doc a s T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 14 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Standard VDI 4202 Part 1 of June 2002 describes all Mini
381. tus neinamteri Conditians ai Saig onal sixties ai EFIKA 157 Settings Service When in the Settings screen select the System Analog amp Digital Outputs Data Storage and Advanced buttons to reach the desired screens Figure 4 18 Note Refer to Section 3 for information on using the Data Storage button to select variables for data storage a THERMO FISHER SCIENTIFIC Section 4 SCREENS AND SETTINGS 18 4 igure F Screens accessible through the Settings button Jequunu jenas ups g jJuejsu09 y queysuog paouenpy JequINN ees yue suo9 0 seonpsuely ssey anjen JH XX Ou yem Wa skS sajqeue uonejnojeg sse paoueapy raqeyreae jou uaym UappIY ase YoIyM suondo reatjoe pue pekeidsip shemje suondo pu 7 yewo 3ed joquiAs jewi99q Aejdsiq uoleinbyuo9 JOMION uoN09 01d piomssed awit 49S i f JBAsa U abes0 s py ISI B qeueA NPA i re mau e6es0 S 4S B QeWeA abeiojs eea jauueyo yy apoo uolyels yy PON ZEZSH c amp cSy ainsojo yoe U0D s ndjno Bojeuy t sindjno leuia 3 Bojeuy 4 23 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 4 SCREENS AND SETTINGS System Screen The
382. u may adjust the flow rate to reflect the value on the audit device Select the Yes button to adjust the flow based on the results of the flow audit Select the No button to leave the original flow settings in place Select the Next gt button to return to the Select Flow screen and audit another flow channel __ Figure 5 59 Flow Audit Results Flow Audit Results screen Your flow has dired 323 percent sirce your asi calibration Previous flow sdjusimemi factor 1 0000 Current Tys adjustment facbor 10323 Touki you like fo adjusi ihe flow based on ihis sudit pe l 8 The Select Flow to Audit screen will display again The flow channel that was just audited will be grayed out on the screen to show it was audited during this session If you want to audit another flow channel select another channel and follow steps 3 8 and the wizard to complete additional flow channels Otherwise ensure that no flow channel buttons are selected and select the Next gt button Note If the difference is more than 10 percent the flow will fail the audit and the unit requires a leak check flow calibration Figure 5 61 a 5 48 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES 9 The Completing the Flow Audit Wizard screen will display Figure 5 60 Remove the flow meter and flow adapter s and install the inlet Ensure all lines including the bypass are reconnected Se
383. u09 JUaUNASU ajqeene jou uaym u pp y ae YoIUM SUOdO ealjoe pue paAeidsip s emje suondo pu 7 uoneoHaA 0A 139NpSULI L ssey Y99493 4ee7 upny mold upny u wnysu i s oss 2 y nesutun esu uonesqued LA Buyay ms ueajy 19 009 uea D A siail4 WOAL 20e dey ainpayos eoueualuley t f uoneoya eoueuaquley Bd1NIaS 4 33 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 4 SCREENS AND SETTINGS Instrument Control Screen Figure 4 27 Instrument Control screen 4 34 Operatine Guine TEOM 1405 F Select the Instrument Control button to display the Instrument Control screen Figure 4 27 The Instrument Control screen allows users to change the unit operating mode and restart or shut down the instrument TEOM 1405 F ml Contral SEEM TIFIC See oes olin Ful OES 1i When in the Instrument Control screen select the Run Setup Stop or Reboot buttons to change the instrument operating mode The Instrument Control screen contains the following control buttons e Run This button returns the instrument to normal operating mode Fully Operational Refer to the beginning of this section for more information on operating modes e Setup This button manually puts the instrument in
384. ulfilled to proof the equivalence 1 Of the full dataset at least 20 of the results obtained using the standard method shall be greater than the upper assessment threshold specified in 2008 50 EC for annual limit values i e 28 ug m for PM 9 and currently 17 ug m for PM25 2 The intra instrument uncertainty of the candidate must be less than 2 5 yg m for all da ta and for two sub datasets corresponding to all the data split greater than or equal to and lower than 30 yg m or 18 g m for PM1 gt and PM2 5 respectively 3 The intra instrument uncertainty of the reference method must be less than 2 0 ug m 4 The expanded uncertainty Wcm is calculated at 50 g m for PM19 and 30 g m for PM2 5 for each individual candidate instrument against the average results of the refer ence method For each of the following permutations the expanded uncertainty must be less than 25 e Full dataset e Datasets representing PM concentrations greater than or equal to 30 wg m for PM or concentrations greater than or equal to 18 g m for PM25 provided that the subset contains 40 or more valid data pairs e Datasets for each individual test site 5 Preconditions for acceptance of the full dataset are that the slope b is insignificantly different from 1 b 1 lt 2 u b and the intercept a is insignificantly different from 0 a lt 2 u a If these preconditions are not met the candidate method may be cali brated using the valu
385. ument Temperatures screen Figure 4 14 shows the current Temperatu res Screen temperatures of the unit Figure 4 14 Instrument Temperatures screen 4 18 Operatine Guine TEOM 1405 F Incirumment Conditions gt lnebruty TEOM 1405 F ent Temperatures The Instrument Temperatures screen contains the following control buttons Cap temperature This field contains the current value of the temperature C of the mass transducer s cap The default setting is 30 C To view or adjust the setpoint select the button to display the keypad Figure 4 3 DO NOT adjust this value without contacting Thermo Scientific Case temperature This field contains the current value of the temperature C of the mass transducer case The default setting is 30 C To view or adjust the setpoint select the button to display the keypad Figure 4 3 DO NOT adjust this value without contacting Thermo Scientific Air tube temperature This field contains the current value of the temperature C of the air stream The default setting is 30 C To view or adjust the setpoint select the button to display the keypad Figure 4 3 DO NOT adjust this value without contacting Thermo Scientific THERMO FISHER SCIENTIFIC Section 4 SCREENS AND SETTINGS Analog Inputs Screen The Analog Inputs screen Figure 4 15 gives the current values of the units four analog input channels The inputs accept 0 5 VDC and can be converted to a desired s
386. und Umwelt GmbH Cologne Germany Report No 936 21209885 B of November 25 2011 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 1 3 Summary of test results Minimum requirement Specification Page 19 of 422 Test result Fulfilled Page 4 Requirements on the instrument design 4 1 General requirements 4 1 1 Measured value Shall be available The measuring device comprises a 61 display measured value display 4 1 2 Easy mainte Necessary maintenance of the Maintenance works can be carried out 63 nance measuring systems should be with commonly available tools taking possible without larger effort if reasonable time and effort possible from outside 4 1 3 Functional test If the operation or the function All system functions listed in the 65 al check of the measuring sys manual are available activatable and tem require particular instru functioning The current system status ments they shall be consid in continuously monitored and dis ered as part of the measuring played by a set of different status system and be applied in the messages operation warning and er corresponding sub tests and ror messag
387. ure Low Setting screen will display Figure 5 76 Compare the reading on the volt meter to the reading on the screen If the readings are different select the Current reading button to display the number keypad and enter the current reading and press the Enter button Select the Next gt button Figure 5 76 Measure Low Setting Measure Low Setting screen EB 10 The Measure High Setting screen will display Figure 5 77 Compare the reading on the volt meter to the reading on the screen If the readings are different select the Current reading button to display the number keypad and enter the current reading and press the Enter button Select the Next gt button Figure 5 77 Measure High Setting Measure High Setting screen 5 60 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Figure 5 78 Completing the Analog Output Calibration Wizard screen THERMO FISHER SCIENTIFIC 11 12 Section 5 MAINTENANCE AND CALIBRATION PROCEDURES The Select Channel to Calibrate screen will display again The channel that was just calibrated will be grayed out on the screen to show it was calibrated during this calibration session If you want to calibrate another analog output channel select another channel then the Next gt button and follow steps 1 9 and the wizard to complete additional channels Otherwise ensure that no Analog Output Channel buttons ate selected and select the Next gt button The Comp
388. urer Thermo Fisher Scientific Suspended particulate matter PM10 Auf enluft Type of instrument TEOM 1405 F Measured values in g m STD Serial No SN 20006 amp SN 20107 No Date Ref 1 Ref 2 Ref 1 Ref 2 Ratio SN 20006 SN 20107 Remark Test site PM2 5 PM2 5 PM10 PM10 PM2 5 PM1q PM10 PM10 yg m g m ug Nm ug Nm ug Nm ug Nm 61 2 7 2010 Zero filter Teddington 62 2 8 2010 20 1 SN 20006 Zero filter gt Inlet Winter 63 2 9 2010 11 7 11 9 11 0 12 0 64 2 10 2010 11 8 12 4 10 9 13 2 65 2 11 2010 20 0 20 2 16 3 18 9 66 2 12 2010 12 5 12 4 10 1 12 6 67 2 13 2010 15 1 15 5 11 2 13 2 68 2 14 2010 16 0 16 5 12 7 16 5 69 2 15 2010 16 3 16 4 13 8 15 6 70 2 16 2010 18 7 19 2 15 9 17 6 71 2 17 2010 53 6 54 1 48 9 50 0 72 2 18 2010 15 2 15 5 12 7 16 9 73 2 19 2010 22 0 22 3 19 0 21 3 74 2 20 2010 19 6 20 0 17 6 20 2 75 2 21 2010 10 6 10 7 8 6 10 5 76 2 22 2010 17 0 17 2 13 8 15 5 a 2 23 2010 22 9 23 3 18 3 20 6 78 2 24 2010 18 6 18 7 15 5 16 8 79 2 25 2010 9 7 10 0 9 2 10 3 80 2 26 2010 11 5 11 9 10 8 11 6 81 2 27 2010 19 8 20 3 19 1 18 5 82 2 28 2010 9 7 9 9 7 2 10 0 83 3 1 2010 26 4 27 0 84 3 2 2010 21 8 21 3 18 8 20 8 85 3 3 2010 20 9 21 6 18 0 19 9 86 3 4 2010 16 3 16 6 15 0 16 4 87 4 27 2010 20 9 21 8 22 0 21 4 Teddington 88 4 28 2010 27 0 26 4 28 1 27 3 Summer
389. uring system TEOM 1405 F via the FDMS unit There it is secreted to the respec tive TEOM filter constantly heated at 30 C and the secreted mass of particles is quantified To take into account non volatile as well as volatile particulate during the measuring the FDMS technology is used The FDMS unit is placed between the flow splitter and the meas uring device TEOM 1405 F in the so called FDMS tower The FDMS unit compensated au tomatically the part of the semi volatile particulate using a switching valve and two operation modi the base mode and the reference mode Every six minutes the switching valve changes the sampling flow rate from base to reference mode In the base mode the sampling is done on a straight way via a dryer directly to the mass measuring In the reference mode the air flow is directed through a cooled filter after the dryer to remove and restrain the non volatile and volatile part of the particulate from the sample During normal operation the temperature of the cooler is maintained at constantly 4 C Based on the mass concentration measuring during the base and reference modi the FDMS system updates every six minutes the 1h average of the following results Base MC Particle concentration of the particle loaded sampling flow Ref MC Particle concentration of the particle free sampling flow after passing through the cooled filter MC Base MC adjusted for Ref MC Base mass concentration normally positive minus
390. utton Figure 3 9 E Leak Check Wizard screen with both valve positions disabled 15 The Completing the Leak Check Wizard screen will display If the leak check passes a You have successfully completed the Leak Check message will display Figure 3 9 THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 3 9 Section 3 Basic OPERATION Figure 3 10 Leak Check Wizard finish jum a screen with pass message Complete Leak Check Wizard Tihe Leak check was suctedsiul Replace the TEOM Miers in the mass transducer mow Partition kara ura Reference cara PH 2 5 Flor Shilo He i cera Limit 15 15 mpos Flo sobs GR i bt Limit 1 80 60 The instrument ill be pul in Run mode when this wizard is finished To close this wizard press Finish x Back Finish Note If a leak check fails a fail message will display Figure 3 7 Isolate the leak tighten the appropriate tubing and or other connections and attempt the leak check again a Figure 3 11 Leak Check Wizard finish screen with fail message Eik Complete Leak Check Wizard The Leak check was umsuccessiul Reterence tailed Replace the TEOM filter s in the mass transducer now Paritian lma ara Reference xara PH Z G Flr sle W w A 05 15 Poe 1 15 WR Limit abalr Epas Flo bt Hi limit 5 60 i160 The insfrument will be pul in Run mede when this wiza
391. value 2 26 g m Combined measurement uncertainty Wem 4 52 Expanded measurement uncertainty Woy 9 03 Status equivalence test pass Table 25 Comparison candidate 20107 with reference device rel humidity gt 70 all test sites measured component PM Comparison candidate with reference according to Guide Demonstration of Equivalence Of Ambient Air Monitoring Methods January 2010 Candidate 1405 F SN SN 20107 Test site All test sites rH gt 70 Limit value 50 Status of measured values Raw data Allowed uncertainty 25 Results of regression analysis Slope b 1 00 not significant Uncertainty of b 0 02 Ordinate intercept a 0 15 not significant Uncertainty of a 0 39 Results of the equivalence test Deviation at limit value 0 27 g m Uncertainty Uc_s at limit v alue 2 13 ug m Combined measurement uncertainty Wem 4 26 Expanded measurement uncertainty Wem 8 52 Status equivalence test pass 740300_2011_936_21209885B_eng doc a s T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 132 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B 6 1 5 4 6 Averaging effect The measuring system shall allow for formation of 24 h averages The time of the sum of all filter changes within 24 h may not exceed 1 of th
392. ve been recently calibrated to a primary standard and should have an accuracy of 1 at 3 l min and 16 67 l min and a pressure drop of less than 0 07 bar 1 psi If you are using a mass flow meter you must make any necessary corrections to translate this reading to volumetric 1 min at the current ambient temperature and barometric pressure No adjustment is necessary in the case of a volumetric flow meter Thermo Scientific offers the Streamline Pro Multi Cal system 57 008887 to measure volumetric flow measurements Note To audit the total flow you will need a 1 1 4 inch flow adapter Remove the inlet and attach the flow adapter and meter to the top of the inlet tube Figure 5 62 a Figure 5 62 Flow meter adapter attached to top of inlet tube for total flow audit Flow meter adapter Flow splitter 5 50 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 5 MAINTENANCE AND CALIBRATION PROCEDURES To calibrate the main or bypass flow 1 In the TEOM Data screen select the Service button to display the Service screen then select the Calibration button to display the Calibration screen Figure 5 48 2 Select the Flow Calibration button to start the Flow Calibration Wizard Figure 5 63 Select the Next gt button to begin the procedure Figure 5 63 Welcome to the Flow Calibration Wizard screen Welcome to the Flow Calibration Wizard This wizard helps you perform tlow calibration on the TEOM Ambien
393. ve the best results locate the TEOM sensor unit in an environment with relatively slow temperature fluctuations Avoid sampling locations with direct exposure to sunlight or that are in close proximity to a heating or air conditioning outlet To avoid condensation in the sample tubing Thermo Scientific strongly recommends that the user insulate the sample tube extensions with pipe insulation when operating the instrument in areas of high humidity THERMO FISHER SCIENTIFIC Section 2 SETUP AND INSTALLATION Standard System the TEOM 1405 F Monitor is supplied with the following components THERMO FISHER SCIENTIFIC Hardware TEOM 1405 F unit Temperature humidity sensor and cable 10 m 3 8 green tubing for bypass flow 10 m 3 8 green tubing to pump 5 m 16 5 ft 2 Sample tubing extensions 1 m 40 Box of 20 TEOM filter cartridges Pallflex TX40 Filter exchange tool Filter cassette Box of 25 47mm FDMS filters 1 small filter element 1 large bypass filter element Flow splitter PM 10 inlet Water trap filter assembly Flow audit adapter leak check kit Cooler cleaning kit Vacuum pump 2 Operating Manuals one hard copy one on CD Quick Start Guide Pre filter silicone tubing Operatine Guine TEOM 1405 F 2 3 Section 2 SETUP AND INSTALLATION Pum p Connections Folowthese steps to attach the pump 1 Locate and cut the piece of the 15m green tubing into two pieces one about but not less than 5m the lengths
394. veinsiatiorinutinaiesennnseianaennaiasnanvutiie 5 2 FDMS Dryer Replacement Refurbishment s issssassssssisosarsoasaeieiaaveenn 5 3 TEOM Vilter Replicementiennorinsi erenn aaa aa 5 4 Filter LAMA orioneu aaie ira an EEEN aa EE EEEE 5 4 Chaneine the TEOM FiltetSeersiiinninn 5 6 Adyan ed Filter mate v sisscndsiasssassenvenvenareestieivenaannmaverenoonneneceie 5 13 Conditioning the TEOM Filters saricariicenamesinnnaiei iias 5 15 Replacing the 47 mm Filter aerarcinnsnerom onn ononiianun unni 5 16 Cleaning the PM A40 Toletani casi ithcasicatessisuabasntatasutinnvsitae aasi EEA 5 18 Eyzchanoino In Line Paces oss icsssasscsissriatancanisnuitananstabsiviaganisteasiesatansaians 5 22 Cleanine the Air Tet oerein enen ae nii i 5 26 MMe ena the ONES sire e a EE ES 5 28 Cleanine th Switching Valve sicisst nncssveviessevessvestnvtevs iiti 5 34 Audit Calibration Procedures ccccecccsssscessessssssscsssscescescsssscsseesesaceaseesees 5 38 PTAA the Syste erarinta Eae araa ENEN 5 41 Calibrating the Ambient Temperature scsi acsss avanseieunicuatsitesatansenstssetateies 5 42 Calibrating the Ambient PresSsUfe sissiiisrueisiisisrsitaiiitainsisiri iasi 5 43 Auditing the Flow Rates csseisadisssdiastesaiessatassenetsonnssscsavariotaroraesetvianevernveintad 5 44 Calibrating the Flow RAteSisaisiissisisisnsnisiessissreiiiioerrotusnsniiesses seres spinis ii 5 50 Calibrating the Analog Outputs iscsesssssisssisensscnrssiavcevnisssnearsrnaieessieenies 5 56 Verifying the Calibranon CO
395. volumetric flOW c cc eeeeeeeeeeeeeeeteeeeeeeeeteeeeeteneeeeeeeeeees 133 6 1 5 4 8 Tightness of the measuring SyStOM c cccceeeeeeeeseeeeeeceeeeeeeeseseeeensneeeeeene 139 6 1 Methodology of the equivalence check modules 5 4 9 5 4 11 eeeeeseeeeeeeeeeeeee 141 6 1 5 4 9 Determination of uncertainty between systems under test Ups ceeeeeeeees 142 6 1 5 4 10 Calculation of the expanded uncertainty of the instruments ee 148 6 1 5 4 11 Application of correction factors and terms ccccccccececeeeceeeeeeeeeeeeeeeeeees 161 6 1 5 5 Requirements on multiple component measuring SySteMS eeeeeeeeeees 166 7 RECOMMENDATIONS FOR PRACTICAL USE 00 cc c cctecdetesdeseeedeetsecneedaneneeeesecnteneee 167 8 LITERATURE coerce recto decease shea E R a de eee 169 9 APPENDIX ace ieee td eter same ee cece ee ae eee 170 740300_2011_936_21209885B_eng doc a s T V Rheinland Energie und Umwelt GmbH A TUVRheinland Luftreinhaltung Precisely Right Page 8 of 422 Tables Table 1 Table 2 Table 3 Table 4 Table 5 Table 6 Table 7 Table 8 Table 9 Table 10 Table 11 Table 12 Table 13 Table 14 Table 15 Table 16 Table 17 Table 18 Table 19 Table 20 Table 21 Table 22 Table 23 Table 24 Table 25 Table 26 Table 27 Table 28 Table 29 Table 30 Report on the suitability test of the ambient air quality measuring system TE
396. w Group Refresh All Instruments 6 The Add New Instrument screen will display Figure 3 24 Enter the IP address the name assigned to the instrument and the group if any assigned to the instrument and select the OK button Figure 3 24 Add New Instrument screen aP Add New Instrument o a Instrument Name PL 1405 IP Address 10 210 96 144 Group Engineering THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F 3 21 Section 3 Basic OPERATION 7 The ePort Main screen will display with the selected instrument displayed in the top window Figure 3 25 Repeat the process to add additional instruments to the list 8 To save this as a configuration select File then Save from the menu bar at the top of the Main screen The Save As screen will display Type in the desired name for the configuration and select Save Note Once you have connected to an instrument or instruments and saved a configuration file select Open Saved Configuration in the ePort Open screen to open that configuration and Figure 3 25 l ePort Main Screen with automatically connect to all the instruments that were saved in instrument information that configuration A displayed 14054200100605 DichotFDMS Saia hemden 14064300100505 IP Address 10 210 98 145 States Active Corrmeands Download Detade Py Domnia Date Desanboad folder Location lt Frogram Fissi ThermclePort J Last dosenbowd E Rewete natae Dots g Urracte mi
397. w rate at candidate SN 20107 Cologne Winter 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH 7 Luftreinhaltung A TUVRheinland TS l Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page 13901482 6 1 5 4 8 Tightness of the measuring system The complete measuring system shall be checked for tightness Leakage shall not exceed 1 of the sample volume sucked 6 2 Equipment Adapter for flow rate check tightness check 6 3 Performance of test The AMS TEOM 1405 F Ambient Particulate Monitor can perform a tightness check using a device internal implemented tightness check assistant The tightness check assistant compares the different measured values between zero flow with turned off vacuum and flow through the device when the inlet is blocked ideally again a zero flow should be measured The tightness check is considered as passed when the flow values during blocked inlet de viate no more than 0 15 I min from zero flow at the PM path and no more 0 60 l min from zero flow at the bypass path The tightness check includes the base path as well as the reference path The tightness check may only be performed using the tightness check assistant in order to avoid damages of the instrument This proc
398. will display Figure 5 84 Correctly install and properly seat the pre weighed calibration verification filter onto the mass transducer using the calibration filter exchange tool Follow the instructions for changing a filter earlier in this section Select the Next gt button Note DO NOT use the calibration filter exchange tool for installing or removing ANY filter other than the pre weighed calibration filter a Figure 5 84 Install Calibration Filter Install Calibration Filter screen The instrument will measure the Irequency with he calibration filter ivetaed Open the instrument door amd mass irensducer Correctly install and properly seal ihe preeweighed calibration verification filter onto the mass transducer ising the calibration Mier exchange tool Close ihe mass transducer and festrument door x Back Mex gt Cancel 11 The Stabilizing screen will display while the instrument waits for the frequency of the TEOM calibration filter A countdown timer on the screen will show the progress of the stabilization step Figure 5 82 When the stabilization Complete message displays select the Next gt button Note If the frequency doesn t stabilize the wizard will display a screen with instructions to re seat the filter Re seat the filter and select the Next gt button The Stabilizing screen will display If the unit is unable find a stable frequency the second time the unit will fail the K
399. with the ASTO command described above The data storage pointer is always located immediately after the last record transmitted through the RS232 port via the AK Protocol If the circular buffer overwrites this location or if the ASTO or SSTO commands have not been used the data storage pointer is positioned at the oldest record in the internal data logger Operatine Guipe TEOM 1405 F B 1 Appenpix B SERIAL COMMUNICATION For AK communication the COM port settings are Figure B 1 AL COM Port Settings COM Properties x Port Settings Bits per second 9800 W Data bits 8 x Parity None x Stop bits 1 ix Elow control None Ey The following pages list the common PRC codes and show how RS Para 1 through RS Para 4 are defined in the AK Protocol and also detail the format of the transmission and response messages of the commands listed on the previous page B 2 OperaTinG Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Appenpix B SERIAL COMMUNICATION Table B 1 1405 F Main PRC Codes on a a on _ ai oa E C M o C e E EE i BE 4 I D a THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F B 3 Appenpix B SERIAL COMMUNICATION AK Protocol Ask Register Command AREG COM 2 WAY SETTINGS RS Para 1 ASCII code for the 1 digit Station Number for example 4 052 The Station Number is always 1 digit in length RS Para 2 75048 ASCII code rep
400. without contacting Thermo Scientific Frequency wait time This field contains the time interval sec after a valve position change before the instrument begins collecting frequency data The default setting is 90 seconds To adjust the setpoint select the button to display the keypad DO NOT adjust this value without contacting Thermo Scientific Equivalency Designation Equivalency Designation is reserved for future use XX Hr MC This field contains the XX Hr MC parameter This value gives the user a choice of averaging times hours shown on the Main screen following the 1 hour mass concentration average The default value for this parameter is 8 which causes the monitor to compute 8 hour averages The user can set an averaging time of any whole hour greater than 1 hour for this parameter To adjust the setpoint select the button to display the keypad Select the Mass Transducer KO Constants button to display the Mass Transducer KO Constants screen The Mass Transducer KO Constants screen contains the following information TEOM KO This field contains the calibration constant K K0 Section 1 for the TEOM Note You can find your monitor s KO number on the label located near the mass transducer Each TEOM 1405 monitor has a unique KO for the TEOM in the unit The constant listed in the Mass Transducer KO Constants screen must match the value shown on the label near the mass transducer or the mass concentration da
401. wo Sa Ke Ke vt Ww Ww ite Ke oO Figure 17 Course of time of the PM concentrations Reference at the test site Teddington summer 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Ty 7 Luftreinhaltung A TUVRheinland TS l Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Page91 0f422 N E D a O a ot o c e gt l m m e m q q z a c c x O O O O O O O O O O O O O O O N N N N N N N N N N N N N N N d _ _ N le S N e S N N D N N N Oo x N v gt y N N D N oO S a E 15 N N N o M o ap lt vt t Figure 18 Course of time of the PM concentrations Reference at the test site Cologne parking lot winter Conc PM10 Ref in g m 7 25 2011 8 1 2011 8 8 2011 8 15 2011 8 22 2011 8 29 2011 9 5 2011 9 12 2011 9 19 2011 9 26 2011 10 3 2011 Figure 19 Course of time of the PM19 concentrations Reference at the test site Bornheim mo torway parking lot summer 740300_2011_936_21209885B_
402. works were carried out according to the instructions of the operating manual 6 4 Evaluation The following maintenance works should be carried out 1 Check of device status The device status can be monitored and controlled by controlling the system itself or controlling it online 2 In general the sampling inlet shall be cleaned according to the manufacturer s instruc tions taking into account the local suspended particulate matter concentrations dur ing suitability test every 4 weeks 3 A monthly change of the TEOM Filter as well when a filter loading gt 90 is reached is necessary 4 Simultaneously with the change of the TEOM filter the cooled 47 mm filter of the FDMS unit has to be changed 5 According to the manufacturer s instructions a monthly check of the sensors for am bient air and ambient pressure shall be done 6 According to the manufacturer s instructions a monthly leak check shall be done 7 According to the manufacturer s instructions a monthly check of the flow rate shall be done 8 Every 6 months or if necessary the inline filter for PM10 and the Bypass path shall be changed in order to avoid a contamination of the flow rate regulator 9 Once a year or if necessary the cooler the switching valve and the air inlet system shall be cleaned 10 Once a year the calibration of the mass transducer has to be checked using the Ko check kit 11 Once a year or if necessary the dryer of the
403. x 70 60 50 Candidate 2 ug m 40 30 20 10 0 10 20 30 40 50 60 70 80 90 100 110 120 130 Candidate 1 ug m Figure 58 Results of the parallel measurements with the candidates SN 20006 SN 20107 measured component PM o test site Cologne Winter 1405 F SN20006 SN20107 Bornheim Summer Raw data 130 120 110 100 o Measured values 90 Regression line 80 seecesy y x 70 60 50 Candidate 2 yg m 40 30 20 10 0 10 20 30 40 50 60 70 80 90 100 110 120 130 Candidate 1 yg m Figure 59 Results of the parallel measurements with the candidates SN 20006 SN 20107 measured component PM o test site Bornheim Summer 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH F Luftreinhaltung A TUVRheinland Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B Pade 147 of4a4 1405 F SN20006 SN20107 All test sites gt 30 ug m Raw data 130 120 110 100 o Measured values 90 Regression line 80 Ee y x 70 60 50 Candidate 2 ug m 40 30 20 10
404. y 7 The wizard will post messages showing the progtess of the installation When the process is complete the Finish screen will display Figure 3 18 Select the Finish button ee i i ePort 0 12 8 InstallShield Wizard Completed screen InstallShield Wizard Completed The InstallShield Wizard has successfully installed ePort 0 12 8 Click Finish to exit the wizard 3 16 Operatine Guine TEOM 1405 F THERMO FISHER SCIENTIFIC Section 3 Basic OPERATION 8 If the PC does not have an up to date version of Microsoft NET Framework software the system will automatically begin installing that software The Microsoft NET Framework Welcome screen will display Figure 3 19 Select the Next gt button Figure 3 19 Mi gog z Microsoft NET Framework 2 0 Setu 1 x Microsoft NET Framework Welcome screen Welcome to Microsoft NET Framework 2 0 Setup This wizard will guide you through the installation process j Cancel 9 Select Install The system will begin installing the Microsoft NET Framework software The wizard will post progress messages during the installation Note If the Microsoft NET Framework software is already installed on the PC the wizard will ask you to Repair or Remove the software Select Repair to ensure the latest version is installed on the PC or select Cancel to skip the Microsoft NEW Framework installation a THERMO FISHER SCIENTIFIC Operatine Guine TEOM 1405 F
405. y Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the Page 38 of 422 company Thermo Fisher Scientific for the component PM10 Report No 936 21209885 B In the case of warning messages an additional button appears in the centre of the display View Warnings After its confirmation the pending warning messages can be looked at In addition an overview of the warning messages can be received at any time by clicking at the triangular warning symbols located at the right of the TEOM Data button SCIENTIFIC System Status Operating mode Fully operational R5232 mode AK protocol Vacuum pump pressure 0 29 atm Protection level Unlocked IP address 10 175 240 169 Serial number 1234567890 Instrument firmware version 1 51 CE da oT Figure 10 Warning messages display triangular warning symbol button View Warnings 740300_2011_936_21209885B_eng doc TUV Rheinland Energie und Umwelt GmbH Luftreinhaltung A TUVRheinland a a i Precisely Right Report on the suitability test of the ambient air quality measuring system TEOM 1405 F Ambient Particulate Monitor with PM10 pre separator of the company Thermo Fisher Scientific for the component PM10 P f 422 Report No 936 21209885 B age 33 0 alx TEOM 1405 F SCIENTIFIC Instrument Conditions CA Figure 11 Menu Instrument conditions In the menu

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