What is new in OPUS 6.5
Contents
1. New Toolbar Design The OPUS toolbars and toolbar buttons have been redesigned graphically The configuration of toolbars and the menu has been simplified The following graphs just show an example KK n HE LETTER Single Click Operation only OPUS MENTOR The OPUS MENTOR package offers a true Single Click operation with a single left click on a toolbar symbol in a toolbar the selected function is immediately executed with the currently loaded spectrum Toolbar symbols showing an additional small triangle can open a separate pop up menu with further options leren Auswerten Anzeige Drucken Makro Walidierun 23851 jager Spektrensuche Einstellungen ndern Hilfe Subskanzinl OPUS 65 Release Notes E Rev 1 doc Page 5 of 15 April 26 2007 we BR KER CeL Clean Test for ATR Accessories A new function allows checking if an ATR accessory is clean or has to be cleaned After measuring a reference spectrum a contamination level can be specified Both reference spectrum and contamination level are used for the clean test itself When the clean test fails you can immediately repeat the test after cleaning the crystal Setup f r Reinheitstest i S X Setup F r Reinheitstest Reinheitstest F r ATR Kristalle Bevor Sie eine Referenzmessung starten vergewissern Sie sich bitte dass der ATR Kristall sauber ist Referenzmessung Die Referenzmessung ist gespeichert Bitte definieren Sie2. in its own display window e The option Autoscale all spectra ensures that the display window is automatically scaled whenever a new spectrum is loaded measured or when a spectrum is modified al x General HERT Rights Preferences Display Mew File Diagnostics Company Settings In case of a new spectrum file C Add new spectrum to window Stack all spectra in the same window Replace the current spectrum by the new one Show then new spectrum in a new window Autoscale all spectra on new and changed data Show spectrum file in OPUS browser with Show all data blocks C Show only main data block OPUS 65 Release Notes E Rev 1 doc Page 2 of 15 April 26 2007 C BR KER CeL Simplified Measurement Dialog Similar to the validated mode the measurement dialog for the ALPHA only offers the possibility to start a measurement The most relevant measurement parameters can be setup using a separate function and can then be stored as an experiment All other parameters are automatically set by OPUS to their optimum values This makes sure that measured spectra are not falsified by wrong parameter settings A separate page in the Setup Experiment dialog allows you to choose additional input parameters which are then shown on the measurement dialog Thus the measurement dialog can be configured according to you specific needs x Parameter Experiment default xpm No optical bench connecte
3. integration limits can be modified and the result of the change can be observed immediately comp mg ETITTIETTTITTITITA elt Method C New Add spectrum C Change BHESNSFEFEFEEF EBEN cue 16 142 15 2 A Wee SBZ UE WES Zhe Bee 2432 Method file Meu q1 Correlation coefficient 0 919 Calibration equation 465 274 0 070273 X Print irAnalyze The program irAnalyze of the company LabCognition can be called directly from OPUS irAnalyze is a tool which assist you during spectrum interpretation A separate license is required for irAnalyze Storage of 3D Data as Data Point Table You can now store 3D files as data point table for further evaluation of the data with external programs OPUS 65 Release Notes E Rev 1 doc Page 12 of 15 April 26 2007 Compare Parameters A new function in the File menu allows comparing the measurement parameters of two spectra Different parameters and their values are displayed in a window Compare Parameters Frincipal File Lompare Parameters E El C AProgrammes OPUS EDAD atas amp bbaena 0 1 File to compare E sPragramme LPLISBDISD ata S earch 0 1 Compared Files LJ Li Sy stemsDocumentation ValidationiOvP TESTYOG PO Teste TENSOR2 7 Tensor 27 RTDLaTGs20070220 1623951100 Tensor 27 Sample Compartment _RT BLaTos_ 514 0 Li S stemsDocumentation ValidationiOvP TEST OQ PQ Tests TENSOR2 7 Tensor 2
4. 7 RTDLaTGsY200702201162351V0Q Tensor 2 Sample Compartment RT DLaTia5 Resalutian Parameters with different values ASS GFW GEW PKA PEL PRL DAQ RSM DUR TSC 1 ANZ ARS DEL DLY NSS PLF RES TDL APF LFG ZFF APT SNM Number of Sample Scans Number of Good Fw Scans Number of Good BW Scans Peak Amplitude Peak Location Backward Peak Amplitude Backward Peak Location Data Aquisition Status Running Sample Number 5 Lime sec Scanner Temperature Max Velocity Deviation Analog Signal 1 Analog Signal 2 Number of Background Scans Delay Before Measurement Stabilization Delay Sample Scans Result Spectrum Resolution To do list 4podization Function End Frequency Limit For File Start Frequency Limit Far File zero Filling Factor Aperture Setting Sample 5 lt lt gt 16 3 cc 8 2SIX 8 10256 lt lt gt gt 4663 365 lt lt gt gt 26701 10802 lt lt gt gt 4885 363 I gt gt 20693 256 zz 120 lt lt gt gt 119 4 208 lt lt gt gt 47 676 dg oe 56 7 0 0955914 lt lt gt gt 0 110289 0 229177 lt lt gt gt 0 229162 16 2638 lt lt gt gt 16 2695 Soe a2 1 lt gt gt 5 been 5S cc 16 Transmittance lt lt gt gt Absorbance 4 lt ac gt gt 1 15777255 aes Blackman Harris 3 Term lt lt gt gt Four point 3 0 lt lt gt gt 350 7000 lt lt gt gt 4000 mm 273mm Sensitivity Test lt lt gt gt Resolutio
5. What is new in OPUS 6 5 General Some of the changes in OPUS 6 5 are related to our new small IR spectrometer ALPHA and the new OPUS package OPUS MENTOR which allows unskilled personnel to measure manipulate and evaluate spectra All ALPHA relevant functions are marked with the ALPHA image These functions 9 are described in detail the OPUS 6 5 supplement a PDF file if you are i working with an ALPHA in the ALPHA user manual The supplement can be added to the Help menu using the Customize Menus function OY Functions marked with the OPUS symbol can be used by all standard OPUS users If necessary a reference to additional documentation is given Bug corrections All known bugs from OPUS 6 0 and earlier versions which have been notified to Bruker have been corrected in OPUS Version 6 5 The Problems amp Solutions document gives you important hints for the OPUS installation how to update from previous version of OPUS and lists possible problems which can still occur with this version Most of the problems described are caused by computer hardware depend on versions of the operating system or are related to improper handling of the instrument and or software Please read this document carefully in case you encounter a problem If the problem you find is not described in the Problems amp Solutions document please notify Bruker This will help us to continuously improve our products OPUS 65 Release Notes E Rev 1
6. d Carca Setup Measurement Parameters Basic Advanced Optic Display Background Prompt only Check Signal Before each measurement OPUS is to prompt the following items MW Sample name jw Sample form File name Fath Resolution Sample scan time x Parameter Experiment default xpm Sample name Sample description Sample scan time fi Scans 7 To perform a sample measurement put the sample in the measurement position of the spectrometer To perform a background measurement make sure that there is NO sample in the measurement position of the spectrometer Start Sample Measurement Start Background Measurement Save and Exit Cancel Help OPUS 65 Release Notes E Rev 1 doc Page 3 of 15 April 26 2007 C BR KER gt lt Automatic Accessory Recognition for the ALPHA only for ALPHA The intelligent measurement modules which are used for the ALPHA are recognized automatically without any user interaction The automatic accessory recognition function runs a quick accessory test and loads the proper measurement experiment The dialog which is shown after the test also allows running a background measurement Accessory Test Ww Accessory test performed Fassed X Measurement parameter loaded TRANS PM Accessory ready Start background measurement OPUS 65 Release Notes E Rev 1 doc Page 4 of 15 April 26 2007 C BR KER gt lt
7. doc Page 1 of 15 April 26 2007 New Functions in the OPUS Basic Packages OPUS IR and OPUS MENTOR g New Installation with automatic Search for connected Instruments only ALPHA The installation program searches if requested during installation the whole network for a connected ALPHA spectrometer If an ALPHA spectrometer is found OPUS registers itself with the OPUS MENTOR package OVP with automatic Setup of the Test Channels OVP is setting up all possible test channels when OPUS communicates for the first time with an instrument This function is only available for instruments which are equipped with beam path information currently only ALPHA MPA MATRIX and VERTEX series instruments For the ALPHA in addition the laser wavenumber is calibrated and a full PQ test is run New File Handling Single Spectrum Mode You can specify the behavior of OPUS when a new spectrum is loaded or measured in the User Settings dialog The following options are available e new spectrum is added to the existing spectrum window this is the default behaviour of OPUS e Spectra are automatically shown in stacked mode e new spectrum shall replace the existing one this is the new Single Spectrum mode which only allows viewing and using a single spectrum at a time This mode is the default for the OPUS MENTOR package e he new spectrum is loaded into a new display window that means that each spectrum is shown
8. ease Notes E Rev 1 doc Page 15 of 15 April 26 2007
9. easure a spectrum and to run an instrument test The Assist area shows context sensitive help while the Help button invokes the online help The manipulation page with buttons for predefined functions and a selectable manipulation function The Measure Next Sample button returns to the measurement dialog to measure the next sample The Assist area shows context sensitive help while the Help button invokes the online help OPUS 65 Release Notes E Rev 1 doc Page of 15 April 26 2007 C BR KER CeL OPUS Wizard x The evaluation page offers also fixed functions and an option 2 Quick Compare to choose additional functions J Spectrum Search aif Quantitative Analysis a gindiugw Quant Builder co The Measure Next Sample button returns to the measurement dialog to measure the next sample Measure Next Sample Choose an evaluation Function SjenjeAZ The Assist area shows context sensitive help while the Help button invokes the online help OPLIS Wizard n x M Save Changes Print FF Unload The final page allows you to save changes print results unload the spectrum and if required returns to the Mest Sampl Bilbo vu measurement dialog for the next sample ajgindiugw 5 Decide how to deal with Ehe current spectrum by activating m the corresponding check box es The Assist area sho
10. im Folgenden den maximal zul ssigen Kontaminationsleyel Typische Kontaminationsleyel 1 1 5 geringe Verschmutzung detektiert 1 5 2 mittlere Verschmutzung detektiert 2 3 starke Verschmutzung detektiert Kristall sauber 1 gemessener Kontaminationslevel 1 0 maximal zul ssiger Kontaminationslevel 2 0 OK OPUS 65 Release Notes E Rev 1 doc Page 6 of 15 April 26 2007 OPUS Wizard OPUS Wizard Load File Advanced Measurement a Instrument Test Either load an existing speckrum File or measure a spectrum OPUS Wizard Ms Baseline Correction Atmospheric Compensation AB lt gt TR Conversion 4 Normalization spectrum Subtraction gt GO Measure Next Sample Strictly speaking the IR spectrum of a mixture is the sum of single spectra In case of such a multi component spectrum you can get information about one single component by spectrum subtraction aunboy 3 Eu E i m ajeneng ajeindiuueyy EE C BR KER de dh An intelligent OPUS Wizard guides you through all steps from measurement via manipulation and evaluation function to the final print out of the spectrum and evaluation results Thus even unskilled personnel can run through the whole procedure with a few mouse clicks The Wizard automatically advances to the next page when a step has been started The start page with the option to load or m
11. ion area 3546 92 A 3189 32 boundaries with the mouse or edit wave numbers in the edit fields and press Return key 0 300 0 200 OPUS 65 Release Notes E Rev 1 doc Page 10 of 15 April 26 2007 C BR KER gt lt Result Views New result windows for different evaluation functions have been added thus presenting the results in a clearly arranged view Depending on the evaluation function the views are automatically opened and shown It Administrator EvalResults Display default1 ows 2 ndow Measure Hense Evaluate Display Print BO validation Setup Help Result of QUANT evaluation Component Prediction Sigma Unit Integr Result Comp 1 16 74 1 63 my 704 88 Status Report of the Instrument only OPUS MENTOR In case of problems with the optics bench the status report of the instrument can be stored on disk You can pass these reports to Bruker for further diagnosis EC Send Report Save Report 8 Graphic Macro Editor Additional functionality has been added to the graphic macro editor e Variables e Calculations e Integration in the OPUS Wizard e Use of graphic macros in Visual Basic Scripts OPUS 65 Release Notes E Rev 1 doc Page 11 of 15 April 26 2007 C BR KER CeL Quant Builder The Quant builder helps you setting up a QUANT 1 method You setup the method step by step by just adding a single spectrum at a time and observe the result Integration method and
12. l 26 2007 we BR KER LL 8 Information View The permanent information view shows you automatically the report of the last evaluation function without further user interaction When a spectrum is loaded either the contents of an existing report or the spectrum parameters are shown The information view can be switched on or off in the View menu j 4000 3300 3600 3400 3200 3000 2500 2600 2400 eS EJ Display Alphal ows lt Info 3350 2103 1 001 0 666 02 0119 57 068581 0 2991 0523 1 209 0 991 95 6341 75 175446 0 2755 9041 0 6 9 0 259 30 6250 21 556660 0 1459 8232 0 609 0 495 20 9031 42 371445 0 1394 1783 0 470 0 332 17 0351 28 278545 0 1241 3565 0 380 Ol 216300 23 163363 0 1047 5095 0 632 0 522 10 1296 44 506142 0 quar 5143 nif ae ee Rh 2 73839 Active Task New interactive Integration Methods New integration methods have been added to the interactive integration function The calculation of the integration can now be invoked immediately from the interactive mode 1 300 Method No integration method loaded Integration mode Area 1 of 1 3351 48 Integral 0 662 Delete Area Delete All Load Methad Store As Method 0 800 0 900 1 000 1 100 1 200 0 700 Cancel Help Hint 0 500 Add new integration area 0 500 Drag the mouse with pressed left mouse button or double click 0 400 Edit integration area Move integrat
13. n Test m OPUS 65 Release Notes E Rev 1 doc April 26 2007 Page 13 of 15 we BR KER LL OPUS IDENT Identity Test Method Setup A preview window shows the selected spectra after data pre processing This makes it easier to select the suited data pre processing method for your specific problem BE Tel We NS Wie I 19 ei a 0 050 0 000 0 050 0 100 0 150 sooo S500 2000 500 Food 6500 6000 S500 D GroupName FileName Yp428y02 11 Geto Setup identity Tot Yp428y02 12 First derivative Vector Yp428y02 15 normalization Yp428y03 11 Yp428y03 12 Interactive Region Selection OPUS LAB OPUS LAB with Metrohm Autosampler i OPUS LAB now supports the Metrohm Autosampler OPUS 65 Release Notes E Rev 1 doc Page 14 of 15 April 26 2007 Further enhancements Extended OPUS Packages The OPUS packages listed below have been extended and modified as well A detailed description of the changes can be asked for OPUS VIDEO and OPUS 3D Enhanced Autofocus Simplified change of traces Spectrum extraction Macro capability of different functions OPUS PROCESS e OPC access to spectra e Useof EFA in Process e Integration of the RPD Tools Reaction Monitoring e Integration of the evaluation of methods Time limited Demo Licenses For test purposes time limited licenses for certain OPUS packages can be issued OPUS 65 Rel
14. ws context sensitive help IF you wank to proceed with the measurement of the next sample activate the corresponding check box while the Help button invokes the online help OPUS 65 Release Notes E Rev 1 doc Page 8 of 15 April 26 2007 Yellow Status Tool tip The Yellow status tool tip automatically shows additional information about the instrument status e g when an instrument test has expired or indicates currently running tests Buttons in this tool tip give you access to the online help or further functions like the instrument diagnosis S An instrument test is required or ane af the instrument components does not meet its specifications Far details click on Diagnosis Diagnosis close Help 1400 1200 1000 sun Bun 400 Performance test iz running Please wait TN Single Peak Pick The option Single Peak Pick is used to select and find single peaks in a spectrum which are then added to the peak table The function does not just set a peak mark at the selected position but performs a real peak pick To invoke the function make a right click in the spectrum window and choose the mode from the popup menu which is also used for other display functions Zoom Scale All Spectra Shift Curve Crosshair Fr F F Add Annotation Add Region Copy All Paste 4254 Integrate Single Peak Pick Properties OPUS 65 Release Notes E Rev 1 doc Page 9 of 15 Apri
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