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0011 Users Guide 681..
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1. 25 6 10 4 e e wn Race e gre n UR o o 25 6 11 Calibration ParameterS 222552545 REI 25 6 11 1 KR E C REOR S Ad RU EC e eR P a 26 6 11 2 CO SL SH and y Ou xo 26 7 Digital Communication Interface Optional 27 7 1 Serial 27 7 1 1 BGs eod 27 7 1 2 Sever alate HR Wl Re 27 Tod v es dah Don stan 28 TLAX Sample a os ee ec A 28 FADS Duplex 6 Bees wae He Sethe esae ar al 28 1 1 2 4 Tiboli A 28 7 1 3 Serial Operation Bee 28 12 Interface Commands 29 8 Maintenance 4 39 8 1 Replacement 34 9 Calibration Procedure 35 9 1 Temperature 35 10 Troubleshooting 4 97 10 1 Troubleshootng s eas ra eras Rex 37 102 CE Comments 22 3 Rx ERG Sea EG ee ead 38 10 2 1 EMG Direcuye tok amp hah do ede bee LOSE e amp bs 38 10 2 2 10 2 2 Low Voltage Directive
2. 38 11 Appendix SAE Test Method 39 12 Appendix DIDP Material Safety Data Sheet 41 1 Before You Start Symbols Used 1 1 Before You Start Symbols Used Table 1 lists the International Electrical Symbols Some or all of these symbols may be used on the instrument or in this manual Table 1 International Electrical Symbols Symbol Description No AC Alternating Current AG AC DC Battery CE Complies with European Union Directives MA DC Double Insulated Electric Shock Fuse PE Ground Hot Surface Burn Hazard Read the User s Manual Important Information Off On O Oi gt o 0011 Fogging Test Chamber User s Guide Symbol Description Canadian Standards Association Us OVERVOLTAGE Installation CATEGORY II Pollution Degree 2 per IEC1010 1 re fers to the level of Impulse Withstand Voltage protection provided Equipment of OVERVOLTAGE CATEGORY II is energy consuming equipment to be supplied from the fixed installation Examples include household office and laboratory appliances The European Waste Electrical and Electronic Equipment WEEE Directive 2002 96 EC mark Australian EMC Mark 1 2 Safety Information Use this instrument only as specified in this manual Otherwise the protection provided by the instrument may be impaired The following definitions apply to the terms Warning and
3. A Material Safety Data Sheet MSDS for the fogging compound Jayflex DIDP Plasticizer has been included with each vial of the chemical As with all chemicals please read the MSDS carefully to become familiar with the han dling storage and safety considerations associated with this product 41
4. Hart Scientific 9 OO11 Fogging Test Chamber User s Guide Rev 681501 681501 Limited Warranty amp Limitation of Liability Each product from Fluke Corporation Hart Scientific Division Hart is warranted to be free from de fects in material and workmanship under normal use and service The warranty period is one year for the Fogging Test Chamber The warranty period begins on the date of the shipment Parts product repairs and services are warranted for 90 days The warranty extends only to the original buyer or end user cus tomer of a Hart authorized reseller and does not apply to fuses disposable batteries or to any other prod uct which in Hart s opinion has been misused altered neglected or damaged by accident or abnormal conditions of operation or handling Hart warrants that software will operate substantially in accordance with its functional specifications for 90 days and that it has been properly recorded on non defective me dia Hart does not warrant that software will be error free or operate without interruption Hart does not warrant calibrations on the Fogging Test Chamber Hart authorized resellers shall extend this warranty on new and unused products to end user customers only but have no authority to extend a greater or different warranty on behalf of Hart Warranty support is available if product is purchased through a Hart authorized sales outlet or Buyer has paid the applicable internation
5. The Factory Reset Sequence should be performed only by authorized personnel if no other action is successful in correcting a malfunction You must have a copy of the most recent Report of Test to restore the test pa rameters DO NOT operate this instrument in an excessively wet oily dusty or dirty environment Authorized Service Centers Please contact one of the following authorized Service Centers to coordinate service on your Hart product Fluke Corporation Hart Scientific Division 799 E Utah Valley Drive American Fork UT 84003 9775 USA Phone 1 801 763 1600 Telefax 1 801 763 1010 E mail support hartscientific com Fluke Nederland B V Customer Support Services Science Park Eindhoven 5108 5692 EC Son NETHERLANDS Phone 31 402 675300 Telefax 31 402 675321 E mail ServiceDesk fluke nl 1 Before You Start Authorized Service Centers Fluke Int l Corporation Service Center Instrimpex Room 2301 Sciteck Tower 22 Jianguomenwai Dajie Chao Yang District Beijing 100004 PRC CHINA Phone 86 10 6 512 3436 Telefax 86 10 6 512 3437 E mail xingye han fluke com cn Fluke South East Asia Pte Ltd Fluke ASEAN Regional Office Service Center 60 Alexandra Terrace 03 16 The Comtech Lobby D 118502 SINGAPORE Phone 65 6799 5588 Telefax 465 6799 5588 E mail antng singa fluke com When contacting these Service Centers for support please have the following information available
6. Model Number Serial Number Voltage Complete description of the problem 2 Introduction Introduction The automotive industry has developed standard test methods for determining fogging characterstics which is the tendency of interior trim materials to pro duce a light scattering film or mass deposit on a glass surface Fogging is caused by the vaporization of volatile components from materials within the passenger compartment and the condensation of these volatiles on the cooler glass surface of the windscreen The various test methods written by the auto manufacturers SAE and ASTM require the use of a test chamber that simulates the conditions under which fogging takes place see Appendix A SAE Test Method The Hart Model 0011 is an approved instrument for simulating the environment where Fog occurs The basic requirements for a test chamber or apparatus include a heated cham ber or bath that controls the temperature of glass beakers at a set point between about 60 C and 120 C according to the test method procedure A glass test plate is placed on a silicone seal which rests over the opening of the beaker The glass plate must be cooled by the apparatus to a temperature set point be tween 20 and 40 The test method specifies the temperature set points to use see Appendix A SAE Test Method The user places a sample of the material being tested cut to 58mm at the bot tom of each glass beaker used for the test
7. data Numeric data denoted by may be entered in decimal or exponential notation Characters are shown in lower case although upper case may be used Spaces may be added within command strings and will simply be ignored Backspace BS ASCII 8 may be used to erase the previous character A termi nating CR is implied with all commands 29 0011 Fogging Test Chamber User s Guide Table 2 Interface Command Summary Command Command Returned Acceptable Command Description Format Example Returned Example Values Display Temperature Read current set point s etpoint S set 9999 99 C or set 150 00 C Set current set point to n s etpoint n 450 Instrument Range Read temperature t emperature t t 9999 99 C or F t 55 69 C Secondary Menu Read proportional band setting pr op band pr pb 999 9 pr 15 9 Set proportional band to n pr op band n pr 8 83 Depends on Configuration Read heater power po wer po p 9999 po 1 duty cycle Configuration Menu Probe Menu Read RO calibration parameter 0 r r0 999 999 r0 100 578 Set RO calibration parameter ton r 0 n r 100 324 98 0 to 104 9 Read ALPHA calibration al pha al al 9 9999999 al 0 0038573 parameter Set ALPHA calibration parameter al pha n al 0 0038433 00370 to ton 00399 Read DELTA calibration delta de de 9 99999 de 1 46126 parameter Set DELTA calibrat
8. 8 2 SET Accept the new proportional band setting Cut out The cut out temperature appears in the secondary menu but is not used A hard ware cut out has been installed Changing or setting this parameter does not af fect the instrument Controller Configuration The controller has a number of configuration and operating options and calibra tion parameters which are programmable via the front panel These are ac cessed from the secondary menu after the cut out set point function by pressing SET There are four sets of configuration parameters probe parameters operating parameters serial interface parameters and controller calibration pa rameters The menus are selected using the UP and DOWN keys and then pressing SET Probe Parameters The probe parameter menu is indicated by Probe parameters menu Press SET to enter the menu The probe parameters menu contains the pa rameters RO ALPHA and DELTA which characterize the resistance tempera ture relationship of the platinum control sensor These parameters may be adjusted to improve the accuracy of the fogger The probe parameters are accessed by pressing SET after the name of the pa rameter is displayed The value of the parameter may be changed using the UP and DOWN buttons After the desired value is reached press SET to set the parameter to the new value Pressing EXIT causes the parameter to be skipped ignor
9. Caution WARNING identifies conditions and actions that may pose hazards to the user CAUTION identifies conditions and actions that may damage the in strument being used 1 2 1 WARNINGS To avoid personal injury follow these guidelines GENERAL DO NOT use the instrument for any application other than calibration work The instrument was designed for temperature calibration Any other use of the unit may cause unknown hazards to the user DO NOT use the unit in environments other than those listed in the User s Guide The unit is not equipped with wheels It is considered to be permanently set once it has been installed If the unit must be moved for some reason two should people pick the unit up carefully lifting at the same time Follow all safety guidelines listed in the user s manual Calibration Equipment should only be used by trained personnel If this equipment is used in a manner not specified by the manufacturer the protection provided by the equipment may be impaired Before initial use or after transport or after storage in humid or semi hu mid environments or anytime the instrument has not been energized for more than 10 days the instrument needs to be energized for a dry out 1 Before You Start Safety Information period of 2 hours before it can be assumed to meet all of the safety re quirements of the IEC 1010 1 If the product is wet or has been in a wet environment tak
10. controller cannot respond very well to changing conditions or noise in the system If the proportional band is too narrow the temperature may swing back 6 Controller Operation Proportional Band and forth because the controller overreacts to temperature variations For best control stability the proportional band must be set for the optimum width an Proportional Band too Narrow Proportional Band too Wide Optimum Proportional Band o Figure 4 Strip chart recordings showing various proportional band settings The proportional band width is set at the factory to about 8 0 C The propor tional band width may be altered by the user if he desires to optimize the con trol characteristics for a particular application The proportional band width is easily adjusted from the front panel The width may be set to discrete values in degrees C or F depending on the selected units The proportional band adjustment is be accessed within the secondary menu Press SET and EXIT to enter the secondary menu and show the heater power Then press SET to access the proportional band ser exr Access heater power in secondary menu x To accept the new setting and access the cut out set point press SET Press ing EXIT exits the secondary menu ignoring any changes just made to the proportional band value 21 0011 Fogging Test Chamber User s Guide 22 6 6 6 7 6 8 6 8 1 6
11. cooled by heat conduction in the cooling plate by thermoelectric devices using the Peltier effect This eliminates an external chilled cooling bath and the problems of circulated fluid flow and its tempera ture gradients Figure shows the side view of the Fogging Test Chamber Figure 2 shows the controller temperature displays and top view of the Fogging Test Chamber CONDENSING PLATE HANDLE THERMOELECTRIC PLEXIGLASS COVER COOLING DEVICE CLAMPING KNOB LED DISPLAY COOLING STAGE PLATE HEATSINK ELECTRONIC TEMPERATURE CONTROLLER COOLING FAN 2 Introduction PLEXIGLASS COVER m CLAMPING KNOB LED DISPLAY CONDENSING PLATE ATYPICAL CONTROLLER LJ FUNCTION BUTTONS EMPERATURE CONTROLLER 9 ET E CONDENSING PLATE GLASS BEAKER a REMOVED 72 SILICONE SEAL CONDENSING PLATE GLASPLAE UMS GUIDE PIN COOLING STAGE TEST WEL HEATING BLOCK COOINC FAN AND FILTER INSULATION XS N C Figure 2 Top View 3 Specifications and Environmental Conditions Specifications 3 1 3 2 Specifications and Environmental Conditions Specifications Test Wells Four Glass Beakers 400ml Pyrex 5 3 x 2 82 134 62mm x 71 63mm Temperatu
12. failure of a component or part Contact an Authorized Service Center see Section 1 3 Authorized Service Centers for further assistance 37 0011 Fogging Test Chamber User s Guide 38 10 2 10 2 1 10 2 2 Problem Causes and Solutions The controller does not Note Before performing the memory check you need to record the controller maintain controller pa calibration parameters found in the CAL menu of the instrument and any rameters or parame user adjusted parameters that you have changed such as the programmable ters are reset each set points and proportional band time the power to the Memory Check unit is removed Doing a memory check is the easiest way to verify the ability of the battery to maintain controller parameters 1 Power off the instrument 2 Disconnect the instrument from AC power for 10 seconds 3 Reconnect the AC power and power on the instrument 4 If the displays show InIT and or the cycle count shows a low number such as 0002 the battery is spent and should be replaced Contact an Authorized Service Center for assistance 5 After replacing the battery you must reprogram the calibration and user adjustable parameters into the controller CE Comments EMC Directive Hart Scientific s equipment has been tested to meet the European Electromag netic Compatibility Directive EMC Directive 89 336 EEC Selection of Light Industrial or Heavy Industrial compliance has b
13. value need not be changed then press EXIT to resume dis playing the well temperature Press UP or DOWN to adjust the set point value C 110 80 New set point value When the desired set point value is reached press SET to accept the new value and access the temperature scale units selection If EXIT is pressed in stead then any changes made to the set point will be ignored Accept new set point value Secondary Menu Functions which are used less often are accessed within the secondary menu The secondary menu is accessed by pressing SET and EXIT simulta neously and then releasing The first function in the secondary menu is the heater power display Heating Power The temperature controller controls the temperature of the well by heating or cooling the well with the thermoelectric modules The amount of heating or cooling power depends on the temperature set point of the well This heating 19 0011 Fogging Test Chamber User s Guide 20 or cooling power value may be estimated by watching the red green control indicator light or read directly from the digital display By knowing the amount of heating the user can tell if the calibrator is heating up to the set point cool ing down or controlling at a constant temperature Monitoring the percent heater power lets the user know how stable the well temperature is With good control stability the percent heating power should not fluctuate
14. 1 Unpacking 22222 2 2 2 4 2 ImtalSetup ee 4 3 POWG ep v E DOR WIE TUR S E d deed E 5 General 5 1 Setting the Temperature 2 2 Testing Set Up a 6 Controller 6 1 WellTemperature 6 2 Temperature 6 2 1 Programmable 5 6 2 2 Setpoint dox em dense don de A 6 3 Secondary 6 4 Heating Power 22 oce o m RR 6 5 Proportional 6 6 549 SUE EP Shan s 6 7 Controller Configuration 6 8 Probe Parameters 2 6 8 1 ea nd oe Ble ae 6 8 2 ALPHA S doe v vd 6 8 3 DELTA o1 re GEO Bete ne 6 9 Operating Parameters 17 17 dede etas d 19 6 9 1 Temperature Scale Units 4 03 45 Sd wae 23 6 9 2 Cut out Reset Mode 2 23 6 10 Serial Interface Parameters 23 6 10 1 BAUD Rate e Ud dex eS OR a 24 6 10 2 Sample we hea epe Ris 24 6 10 3 Duplex eode URS ae
15. 999 99 Read SH calibration paramter sh sh sh 999 99 sh 05 Set SH calibration parameter ton sh n sh 04 999 99 to 999 99 These commands are only used for factory testing Read software cutout mode sco sco Sco ON or OFF Sco ON Set software cutout mode sco ON OF F ON or OFF Set software cutout mode on sco ON sco on Set software cutout mode off sco OF F sco off Miscellaneous not on menus Read firmware version number ver sion ver ver 9999 9 99 ver 0011 2 24 Read structure of all commands h elp h list of commands Legend Note Optional Command data Alternate characters or data 0 Returns either information n Numeric data supplied by user may be entered in decimal or exponential notation 9 Numeric data returned to user x Character data returned to user When DUPLEX is set to FULL and a command is sent to READ the command is returned followed by a carriage return and linefeed Then the value is returned as indicated in the RETURNED column 31 8 Maintenance The instrument has been designed with the utmost care Ease of operation and simplicity of maintenance have been a central theme in the product develop ment Therefore with proper care the instrument should require very little maintenance Avoid operating the instrument in an oily wet dirty or dusty environment Batteries are used to maintain operating parameters in the unit All operat
16. After the fog test chamber has stabilized at the temperatures you have set you are ready to load your test samples and run a test Remove the plexiglass cover Refer to Figure 2 Remove the condensing plates and place a sample in the bottom of each beaker Use the stainless steel sample retaining rings to hold your sample flat if needed Carefully position a glass plate centered over the beaker mouth and silicone gasket Replace the condensing plate using care not to move the glass plate from its position Tighten the clamp knob MAKE SURE THE CONDENSING PLATES SIT ABSOLUTELY FLAT ON THE COOLING STAGE PLATE Replace the plexiglass cover The fog test chamber may take as long as 20 minutes to re equilibrate after loading with samples and closing the cover The duration of your test is deter mined by the test method you are following Remove your samples from the fog test chamber at the end of the test period and follow the instructions given in the test method you are using to obtain proper results 15 6 Controller Operation Well Temperature 6 1 6 2 6 2 1 Controller Operation This chapter discusses in detail how to operate the temperature controller using the front control panel Using the front panel key switches and LED display the user may monitor the well temperature set the temperature set point in degrees C or F monitor the heater output power adjust the controller proportional band set the cut out set point and progra
17. EXIT Select Setpoint st I SET Y Y EXIT Set Cutout Temp lt EXIT Adjust Setpoint SET TE Y lt EXIT Configuration Menu SET i EXIT EXIT EXIT EXIT i Operating e gt Serial down Parameters Down Interface DOWN 4 Menu lt Menu lt SET SET SET 5 Y Y Y Y res Gom SET EXIT SET EXT SET EXIT SET EXIT E SET EXIT E SET EXIT Y Cutout Sample 2 wm Ca SET EXIT SET SET EXIT EXIT gt Adj Cutout Adj Sa a Reset Mode SET EXIT SET EXIT SET EXIT m SET EXIT Y Duplex 5 SET Exit gt SET EXT EXIT 8 Adj Dupl a WI qe SET EXIT SET EXIT Y SET Ext H gt sr Adjust SET EXIT Figure 3 Controller Operation Flowchart 18 2 SET E Adjust SH SET EXIT sco SET SET EXIT pe 6 Controller Operation Secondary Menu 6 2 2 6 3 6 4 pd 90 0 New set point memory 4 90 0 Press SET to accept the new selection and access the set point value SET Accept selected set point memory Set point Value The set point value may be adjusted after selecting the set point memory and pressing SET The set point value is displayed with the units C or F at the left t 90 00 Set point 4 value If the set point
18. L INDIRECT INCIDENTAL OR CONSE QUENTIAL DAMAGES OR LOSSES INCLUDING LOSS OF DATA WHETHER ARISING FROM BREACH OF WARRANTY OR BASED ON CONTRACT TORT RELIANCE OR ANY OTHER THEORY Since some countries or states do not allow limitation of the term of an implied warranty or exclusion or limitation of incidental or consequential damages the limitations and exclusions of this warranty may not apply to every buyer If any provision of this Warranty is held invalid or unenforceable by a court of com petent jurisdiction such holding will not affect the validity or enforceability of any other provision Fluke Corporation Hart Scientific Division 799 E Utah Valley Drive American Fork UT 84003 9775 USA Phone 1 801 763 1600 Telefax 1 801 763 1010 E mail support hartscientific com www hartscientific com Subject to change without notice Copyright 2006 Printed in USA Table of Contents 1 Before You 1 1 1 symbols Used s pre ate u aace 1 2 Safety Information 1 2 1 WARNINGS c eer ace u dx 1 2 2 CAUTIONS 4 x 1 3 Authorized Service 2 Introduction 7 3 Specifications and Environmental Conditions 3 1 Specifications 3 2 Environmental 4 Installation 4
19. able has been attached and the interface set up properly the control ler immediately begins transmitting temperature readings at the programmed rate The serial communications uses 8 data bits one stop bit and no parity 7 Digital Communication Interface Optional Interface Commands 7 2 The set point and other commands may be sent via the serial interface to set the temperature set point and view or program the various parameters The inter face commands are discussed in Section 7 2 All commands are ASCII charac ter strings terminated with a carriage return character CR ASCII 13 Interface Commands The various commands for accessing the fogger functions via the digital inter faces are listed in this section see Table 2 The commands are terminated with a carriage return character The interface makes no distinction between upper and lower case letters hence either may be used Commands may be abbrevi ated to the minimum number of letters which determines a unique command A command may be used to either set a parameter or display a parameter depend ing on whether or not a value is sent with the command following charac ter For example s CR will return the current set point and s2150 00 CR will set the set point to 150 00 degrees In the following list of commands characters or data within brackets and are optional for the command A slash denotes alternate characters or
20. al price Hart reserves the right to invoice Buyer for importation costs of repairs replacement parts when product purchased in one country is submitted for repair in another country Hart s warranty obligation is limited at Hart s option to refund of the purchase price free of charge re pair or replacement of a defective product which is returned to a Hart authorized service center within the warranty period To obtain warranty service contact your nearest Hart authorized service center or send the product with a description of the difficulty postage and insurance prepaid FOB Destination to the nearest Hart au thorized service center Hart assumes no risk for damage in transit Following warranty repair the prod uct will be returned to Buyer transportation prepaid FOB Destination If Hart determines that the failure was caused by misuse alteration accident or abnormal condition or operation or handling Hart will provide an estimate or repair costs and obtain authorization before commencing the work Following repair the product will be returned to the Buyer transportation prepaid and the Buyer will be billed for the repair and return transportation charges FOB Shipping Point THIS WARRANTY IS BUYER S SOLE AND EXCLUSIVE REMEDY AND IS IN LIEU OF ALL OTHER WARRANTIES EXPRESS OR IMPLIED INCLUDING BUT NOT LIMITED TO ANY IM PLIED WARRANTY OF MERCHANTABILITY OR FITNESS FOR A PARTICULAR PURPOSE HART SHALL NOT BE LIABLE FOR ANY SPECIA
21. and sets the SST ring on top of the material Next the beaker is inserted into the well covered with a silicone seal and glass plate Finally the condensing plate is placed over the glass plate and screwed into place During the test volatiles condense on the glass plates which are later removed and measured with a gloss meter if running the photo metric test or an analytical balance when performing the gravimetric test to de termine an actual fogging test number Each test method has specific procedures that must be followed in order to maintain test consistency and ac curacy see Appendix A SAE Test Method Normally three samples of the same material are tested simultaneously Some of the test methods in use require the simultaneous test of a standard material DIDP Thus four test wells may be required one for the standard and three for material samples see Appendix A SAE Test Method The Hart Scientific Model 0011 Fogging Test Chamber is designed specifically for the requirements of the various suggested test methods Four heated test wells are machined into a solid aluminum block which is heat controlled by an adjustable precision temperature controller Each Fogger ships with Pyrex beakers to run the tests which are inexpensive and easily replaced The test wells are heated and controlled by two digital micro processor based tempera ture controllers They operate independent of each other to heat the beaker well and cool the c
22. e necessary measures to remove moisture prior to apply ing power such as storage in a low humidity temperature chamber operat ing at 50 degree centigrade for 4 hours or more Overhead clearance is required Do not place the instrument under a cabi net or other structure Always leave enough clearance to allow for safe and easy insertion and removal of samples e The instrument is intended for indoor use only BURN HAZARD e Extremely cold temperatures may be present in this equipment Freezer burns and frostbite may result if personnel fail to observe safety precau tions e High temperatures may be present in this equipment Fires and severe burns may result if personnel fail to observe safety precautions ELECTRICAL HAZARD e These guidelines must be followed to ensure that the safety mechanisms in this instrument will operate properly This instrument must be plugged into a 115 VAC 60Hz 230 VAC 50Hz optional AC only electric outlet The power cord of the instrument is equipped with a three pronged grounding plug for your protection against electrical shock hazards It must be plugged directly into a properly grounded three prong receptacle The receptacle must be installed in accordance with local codes and ordi nances Consult a qualified electrician DO NOT use an extension cord or adapter plug DO use a ground fault interrupt device This unit contains a fluid ground fault device is advised in case fluid is prese
23. ee Section 1 3 4 Poor temperature uniformity between condensing plates Remove and clean the air filters on both sides of the chamber Make sure there are no ob structions on the bench top that are preventing sufficient air flow through the filters 5 Ambient temperature and relative humidity fluctuations The test method being used provides guidelines for environmental controls see Section 11 Appendix A SAE Test Method Temperature readout is not the actual tempera ture of the well With the unit stable slowly rotate the unit If no change occurs the unit may need to be calibrated Contact an Authorized Service Center If the display changes more than twice the normal display deviation another unit in the area could be emitting RF energy Move the unit to a different location and ro tate the unit again If the temperature is correct in this new area or deviates differently than the first area RF energy is present in the room Instrument will not power up The unit is equipped with two external fuses and one internal transformer fuse Before servicing the internal fuse contact an Authorized Service Cen ter If a fuse blows it may be due to a power surge or failure of a component DO NOT replace fuses with one of a higher current rating Always replace the fuse with one of the same rating voltage and type see XXXSection 3 1 Specifications for fuse details If a fuse blows a second time it is likely caused by
24. een based on the intended use of the instrument Units designed for use in a calibration laboratory have been tested to Light Industrial Standards Units designed to be used in the field have been tested to both Light Industrial and Heavy Industrial Stan dards The Declaration of Conformity for your instrument lists the specific standards to which the unit was tested A slight degradation of accuracy may be noticed between 300 350 Mhz A piece of equipment in proximity to the unit under test must emit greater than 1000 times the permissible CE standard EN55022 at these specific frequen cies to have any effect on the unit See the Section 10 1 2 10 2 2 Low Voltage Directive Safety In order to comply with the European Low Voltage Directive 73 23 EEC Hart Scientific equipment has been designed to meet the IEC 1010 1 EN 61010 1 and IEC 1010 2 010 EN 61010 2 010 standards 11 Appendix SAE Test Method 11 Appendix A SAE Test Method There are many recommended test methods such as SAE J1756 ASTM D5393 97 or ISO 6452 Due to copyright restrictions we are not able to pro vide copies of these standards Standards can be purchased from these agencies or any other appropriate standards authorities These standards can also be ac cessed through their web sites www sae org www astm org www iso ch iso en 39 12 Appendix B DIDP Material Safety Data Sheet 12 Appendix B DIDP Material Safety Data Sheet
25. es in memory The set points can be quickly recalled to conveniently set the fogger to a previously programmed temperature set point To set the temperature first select the set point memory This function is ac cessed from the temperature display function by pressing SET The number of the set point memory currently being used is shown at the left on the display followed by the current set point value 17 0011 Fogging Test Chamber User s Guide Display SECONDARY FUNCTIONS Temperature SE SET ELI Display Power I gu Reset Cutout J SET I f SET Y ec Gta Adi EXIT Set Proportional Band
26. g linearly to 50 at 40 C pressure 75kPa 106kPa mains voltage within 10 of nominal vibrations in the calibration environment should be minimized altitude does not effect the performance or safety of the unit indoor use only 4 Installation Unpacking 4 1 4 2 Installation Unpacking Carefully unpack the fogging test chamber and confirm that all parts listed be low are included with your chamber e Test Chamber e Power Cord e Plexiglass Cover e 4 tension plate assemblies in place in the chamber 4 condensing plates with clamping knobs in place e 6 glass beakers ground on top and bottom e 4 silicone seals e 4 sample retaining rings e 12 3mm glass cover plates e DIDP sample vials e MSDS for Jayflex DIDP Plasticizer e Material Sample Cutter e Instruction Manual e Report of Calibration e tension plate removing tool Packing material has been placed in each test well to cushion the tension plates during shipment To remove this padding you must remove the condensing plates One plate at a time turn the clamping knob counter clockwise until it comes off the threaded stud Using the condensing plate handle carefully lift the plate from the chamber exposing the test well Remove the padding from the test well Initial Set up Place the fog test chamber in your lab so that it is not directly under heating or air conditioning vents or any other location subject to wide variance in room
27. he menu Sample Period The sample period is the next parameter in the menu and prompted with SAm PLE The sample period is the time period in seconds between temperature measurements transmitted from the serial interface If the sample rate is set to 5 then the instrument transmits the current measurement over the serial inter face approximately every five seconds The automatic sampling is disabled with a sample period of 0 Press SET to choose to set the sample period Adjust the period with UP or DOWN and then use SET to set the sample rate to the displayed value Duplex Mode The next parameter is the duplex mode indicated with dUPL The duplex mode may be set to half duplex HALF or full duplex FULL With full duplex any commands received by the thermometer via the serial interface are immediately echoed or transmitted back to the device of origin With half du plex the commands are executed but not echoed The default setting is full du plex The mode may be changed using UP or DOWN and pressing SET Linefeed The final parameter in the serial interface menu is the linefeed mode This pa rameter enables or disables OFF transmission of a linefeed charac ter LE ASCII 10 after transmission of any carriage return The default setting is with linefeed on The mode may be changed using or DOWN and pressing SET Serial Operation Once the c
28. ing any changes that may have been made RO This probe parameter refers to the resistance of the control probe at 0 C The value of this parameter is set at the factory for best instrument accuracy ALPHA This probe parameter refers to the average sensitivity of the probe between 0 and 100 C The value of this parameter is set at the factory for best instrument accuracy 6 Controller Operation Operating Parameters 6 8 3 6 9 6 9 1 6 9 2 6 10 DELTA This probe parameter characterizes the curvature of the resistance temperature relationship of the sensor on the cooling side The value of this parameter is set at the factory for best instrument accuracy Operating Parameters The operating parameters menu is indicated by Par Operating parameters menu Press SET to enter the menu The operating parameters menu contains the units scale set and cut out reset mode setting Temperature Scale Units The temperature scale units of the controller may be set by the user to degrees Celsius C or Fahrenheit F The units are used in displaying the well tem perature set point and proportional band The temperature scale units selection is the first function in the operating pa rameters menu Press SET to accept the new selection and resume displaying the well temperature Cut out Reset Mode The cut out reset mode is not used A hardware cut out has been installed Serial Interface Pa
29. ing parameters both on the cold and hot side including calibration pa rameters should be checked on a regular basis to insure accuracy and proper operation of the instrument See the troubleshooting section for the procedure on checking the status of the battery Cooling Fan Filters should be removed and cleaned periodically Block age from dust or other material affects the temperature uniformity of the cooling stage plate and thus the uniformity between condensing plates Keep the cooling stage plate clean and free of dust or other material Care should be used to protect the surface of the cooling stage plate and the bottom surface of the condensing plates A good flat surface contact should be maintained between these parts during fog tests so that heat conduction between the surfaces is not hampered If the outside of the instrument becomes soiled it may be wiped clean with a damp cloth and mild detergent Do not use harsh chemicals on the surface which may damage the paint If a hazardous material is split on or inside the equipment the user is re sponsible for taking the appropriate decontamination steps as outlined by the national safety council with respect to the material If the mains supply cord becomes damaged replace it with a cord of the appropriate gauge wire for the current of the instrument If there are any questions contact an Authorized Service Center for more information Before using any cleaning or decontami
30. ion parameter de lta n de 1 45 0 0 to 2 9 ton Operating Parameters Menu Set temperature units u nits c f CorF Set temperature units to Celsius u nits c u C Set temperature units to u nits f u f Fahrenheit Serial Interface Menu Read serial sample setting sa mple sa sa 9 sa 1 Set serial sampling setting to n sa mple n 0 0 to 4000 seconds Set serial duplex mode du plex f ull h alf FULL or HALF Set serial duplex mode to full du plex f ull du f Set serial duplex mode to half du plex h alf du h Set serial linefeed mode Iffeed on of f ON or OFF Set serial linefeed mode to on Iffeed on Set serial linefeed mode to off Iffeed of f 30 7 Digital Communication Interface Optional Interface Commands Interface Command Summary continued Command Description Command Format Command Example Returned Returned Example Acceptable Values Calibration Menu WARNING changing the following calibration values may change the accuracy of the instrument Read calibration parameter 0 0 9 0 0 Set calibration parameter to 0 c0 0 999 9 to 999 9 Read CG calibration parameter cg cg cg 999 99 cg 406 25 Set CG calibration parameterto n cg n cg 406 25 999 9 to 999 9 Read SL calibration paramter s s sl 999 99 sl 04 Set SL calibration parameter ton sl n sl 04 999 99 to
31. m the probe calibration parameters operating parameters serial configuration and controller calibration parame ters Operations of the functions are summarized in Figure 3 on page 18 In the following discussion a solid box around the word SET UP EXIT or DOWN indicates the panel button while the dotted box indicates the display reading Explanation of the button or display reading are to the right of each button or display value The explanation that follows applies to both the heating and cooling controllers Well Temperature The digital LED display on the rear panel allows direct viewing of the average of the four well temperatures This temperature value is what is normally shown on the display The units C or F of the temperature value are displayed at the right For example 100 800 C Well temperature in degrees Celsius The temperature display function may be accessed from any other function by pressing the EXIT button Temperature Set point The temperature set point can be set to any value within the range and with res olution as given in the specifications Be careful not to exceed the safe upper temperature limit of any device inserted into the well A safety cut out is set to monitor the heated block to help prevent this occurance Setting the temperature involves two steps 1 select the set point memory and 2 adjust the set point value Programmable Set points The controller stores 8 set point temperatur
32. mber of the instrument calibration constants namely CG SL SH and SCO These values are set at the factory and must not be altered The correct values are important to the accuracy and proper and safe operation of the fogger Access to these parameters is available to the user only so that in the event that the controller s memory fails the user may restore these values to the factory settings The user should have a list of these con stants and their settings with the certification sheet provided 25 0011 Fogging Test Chamber User s Guide 26 6 11 1 6 11 2 DO NOT change the values of the calibration constants from the factory set values The correct setting of these parameters is important to the safety and proper operation of the fogger The calibration parameters menu is indicated by CAL iJ Calibration parameters menu Press SET five times to enter the menu CTO Parameter CTO sets the calibration of the over temperature cut out This is not adjustable by software but is adjusted with an internal potentiometer The Model 0011 does not use this function CO CG SL SH and SCO These parameters calibrate the accuracy of the temperature set point These are programmed at the factory when the instrument is calibrated Do not alter the value of these parameters 7 Digital Communication Interface Optional Serial Communications 7 1 7 1 1 7 1 2 Digital Communication In
33. more than 1 within one minute The heater power display is accessed in the secondary menu Press SET and EXIT simultaneously and release The heater power is displayed as a percent age of full power Heater power in percent Negative numbers indicate the well is being cooled 100 means the well is being cooled at maximum power 0 means the well requires neither heating nor cooling 100 means the well is being heated at maximum power To exit out of the secondary menu press EXIT To continue on to the propor tional band setting function press SET Proportional Band In a proportional controller such as this the heater output power is proportional to the well temperature over a limited range of temperatures around the set point This range of temperature is called the proportional band At the bot tom of the proportional band the heater output is 10096 At the top of the pro portional band the heater output is 0 Thus as the temperature rises the heater power is reduced which consequently tends to lower the temperature back down In this way the temperature is maintained at a fairly constant temperature The temperature stability of the well and response time depend on the width of the proportional band See Figure 4 If the band is too wide the well tempera ture will deviate excessively from the set point due to varying external condi tions This is because the power output changes very little with temperature and the
34. nation method except those rec ommended by Hart users should check with an Authorized Service Cen ter to be sure that the proposed method will not damage the equipment If the instrument is used in a manner not in accordance with the equip ment design the operation of the fogger may be impaired or safety haz ards may arise No other regular service is required General cleaning of all accessible parts of the chamber is good idea The various test accessories such as the glass plates gasket beakers and seals are consumable items and need replacements Maintenance and use of these accessories is covered in the various test methods see Appendix A SAE Test Method 33 0011 Fogging Test Chamber User s Guide 8 1 Replacement Parts The following parts need to be replaced over time Refer to the model number when reordering Model Description Unit 2000 Sample Retaining Ring 1 2002 Glass Beakers Set of 6 2006 Beaker Seals Set of 4 2004 Glass Cover Plates Set of 24 34 9 Calibration Procedure Temperature Calibration 9 1 Calibration Procedure Temperature Calibration Complete calibration of your fog test chamber was performed at the factory This includes a test of temperature stability over time a test of the accuracy of the digital temperature settings as compared against NIST traceable thermome ters and sensors and a test for uniformity between each of the heated wells and each of the conden
35. nt in the electrical sys tem and could cause an electrical shock e Always replace the power cord with an approved cord of the correct rat ing and type If you have questions contact an Authorized Service Center see Section 1 3 e High voltage is used in the operation of this equipment Severe injury or death may result if personnel fail to observe the safety precautions Before working inside the equipment turn off the power and disconnect the power cord e The instrument is equipped with operator accessible system fuses If a fuse blows it may be due to a power surge or failure of a component Re place the fuse once If the fuse blows a second time it is likely caused by failure of a component If this occurs contact an Authorized Service Cen ter see Section 1 3 Always replace the fuse with one of the same rating voltage and type Never replace the fuse with one of a higher current rat ing 0011 Fogging Test Chamber User s Guide 1 2 2 1 3 CAUTIONS Always operate this instrument at room temperature between 20 and 24 65 F to 75 F Allow sufficient air circulation by leaving at least 6 inches 15 cm of clearance around the instrument DO NOT use fluids to clean out the test wells If a main supply power fluctuation occurs immediately turn off the fogger Power bumps from brown outs and black outs can damage the in strument Wait until the power has stabilized before re energizing the fogger
36. ooling plates to the set point entered by the user Silicone rubber gaskets are also provided which seal the test beakers to the glass plates The beakers rest on a spring loaded tension plate at the bottom of each test well to insure contact with the electrically cooled metal plate No ex ternal cooling or liquid hookups are required to cool the plates The cooled 0011 Fogging Test Chamber User s Guide CLASS PLATE SILICONE SEAL THERMAL BARRIER HEATING BLOCK GLASS BEAKER TEST WELL TENSION PLATE ASSY INSULATION Figure 1 Side View condensing plates are easily removed for access to the beakers in the test wells The temperatures of the heated test wells and the condensing plates are conve niently set via the LED displays on the panel at the back of the instrument The Fogging Test Chamber is carefully calibrated at the factory to insure accuracy of the set point temperatures uniformity between the four test wells and be tween the four condensing plates and temperature stability during the test pro cedure The chamber is compact and self contained occupying only 14 x 19 of bench space The heated beakers are controlled in a dry heated block assembly No bath oils or fluids are required which means the glass beakers are never subjected to oil residue The heated block has been designed for optimum uniformity and the absence of fluid heating medium reduces the impact of flow patterns The condensing plates are
37. rameters The serial RS 232 interface parameters menu is indicated by Serial RS 232 interface parameters menu The serial interface parameters menu contains parameters which determine the operation of the serial interface These controls only apply to instruments fitted with the serial interface The parameters in the menu are BAUD rate sample period duplex mode and linefeed The Model 0011 serial interface option is configured to require two seperate serial ports one for the heating and one for 23 0011 Fogging Test Chamber User s Guide 24 6 10 1 6 10 2 the cooling controller They operate completely independent of each other and require command to be send individually BAUD Rate The BAUD rate is the first parameter in the menu The BAUD rate setting de termines the serial communications transmission rate The BAUD rate parameter is indicated by Serial BAUD rate parameter Press SET to choose to set the BAUD rate The current BAUD rate value is then displayed 1210 Current BAUD rate The BAUD rate of the serial communications may be programmed to 300 600 1200 or 2400 BAUD Use UP or DOWN to change the BAUD rate value P400 b New BAUD rate Press SET to set the BAUD rate to the new value or EXIT to abort the op eration and skip to the next parameter in the menu Sample Period The sample period is the next parameter in the serial interface parame
38. re Ranges Heated Test Wells 50 to 120 122 F to 248 F Condensing Plates 20 C to 40 C 68 F to 104 F Stability 0 2 C Set point Repeatability 0 2 C Set point Accuracy 0 5 C Uniformity Between Heated Test 0 5 Wells Uniformity Between Condensing 0 5 Plates Thermal Safety Cut out 125 C 300 F Heat Time to Max 60 min Stabilization Time 30 60 min Computer Interface RS 232 Optional Power 115 VAC 10 50 60 Hz 450 W 230 VAC 10 50 60 Hz 450 W optional System Fuse 115 VAC 5 A 250 V F 230 VAC 3 15 250 V Transformer Fuse internal 115 230 VAC 1 25 A 250 V SB Weight 70 Ibs Size 19 Wide x 14 Deep x 10 High 483mm x 356mm x 254mm Shipping Weight 90 Ibs Safety OVERVOLTAGE Installation CATEGORY II Pollution Degree 2 per IEC 61010 1 Environmental Conditions Although the instrument has been designed for optimum durability and trou ble free operation it must be handled with care The instrument should not be operated in an excessively dusty or dirty environment Maintenance and clean ing recommendations can be found in the Maintenance Section of this manual The instrument operates safely under the following conditions 11 0011 Fogging Test Chamber User s Guide 12 ambient temperature range 20 24 C 65 75 F ambient relative humidity maximum 80 for temperature 31 C de creasin
39. sing by following the instructions that follow Power Plug the fogger power cord into a mains outlet of the proper voltage frequency and current capability See Section 3 1 Specifications for power details Turn the fogger on using the rear panel POWER switch The fogger will turn on and begin to heat to the previously programmed temperature set point The front panel LED display indicates the fogger temperature 5 General Operation Setting the Temperature 5 1 5 2 General Operation Setting the Temperature Section 6 2 explains in detail how to set the temperature set point on the fogger using the front panel keys The procedure is summarized here 1 Press SET twice to access the set point value 2 Press UP to change the set point value 3 Press zi to program in the new set point 4 Press en to return to the temperature display When the set point temperature is changed the controller switchs the well heater on or off to raise or lower the temperature The cycle indicator a two color LED also indicates on red when heating or off green when cooling The displayed well temperature gradually changes until it reaches the set point temperature Once the set points have been reached the instrument operator should wait at least 30 minutes to allow the instrument to equilibrate The fog test chamber may be left on continuously so that it is ready for immediate use Testing Set up
40. sing plates Actual measurement data are provided on your Report of Calibration that is included with the fog test chamber Any tempera ture calibration should be performed at the factory See Section 1 3 Authorized Service Centers 35 10 Troubleshooting Troubleshooting 10 Troubleshooting 10 1 Troubleshooting Problem Causes and Solutions Inconsistent Fog Numbers Inconsistent data between the four test wells or between one test and another can be attributed to many things If the test chamber and not the sample is suspect check the following 1 Improper beaker to plate sealing If an inadequate seal occurs then leak ing fog may occur during a test and lowering the amount of measurable fog deposits on the plate Check the positioning of the beaker in the well the seal and the glass plate positions If the silicone seal is worn or old replace the seal The beaker must be in good thermal contact with the bottom of the well and the glass plate must be firmly pressed up against the condensing plate 2 Contamination Check to see if new glass plates were used Check if the beakers seals and ring weights have been cleaned and dried according to the test method used Check that the handling of the samples and plates were consistent with the test method handling requirements 3 Temperature performance of the chamber If the instrument is suspected of being out of calibration contact an Authorized Service Center s
41. temperature Make sure that the black fan covers on the left and right sides of the chamber are not blocked allow at least 6 inches clearance Use the following instructions during the initial operation of the fog test cham ber and again when changing the set point temperatures to allow equilibration of the chamber and condensing plates to the new set points Prepare the test samples and test equipment according to the test method being followed see Appendix A SAE Test Method Place a silicone gasket over the lip of each beaker Remove the condensing plates from the chamber place each 13 0011 Fogging Test Chamber User s Guide 4 3 of the beakers in the test wells the glass plates will be installed later Replace the condensing plates by carefully guiding each one on to the guide posts of the cooling stage plate The cooling stage plate must be kept clean Avoid any damage such as nicks to insure proper contact with the cooling plates Also use the plates on the same well as they came shipped from the factory Switching plates could introduce a slight error from the original calibration Replace the clamping knobs and tighten down the cooling plates Place the plexiglass cover on the chamber Plug the chamber power cord into a grounded mains outlet and turn the power switch on the back panel to Set the Heating Well and Cooling Well set points to the temperature recommended in the test method you are u
42. ter menu The sample period is the time period in seconds between temperature measure ments transmitted from the serial interface If the sample rate is set to 5 then the instrument transmits the measurement over the serial interface approxi mately every five seconds The automatic sampling is disabled with a sample period of 0 The sample period is indicated by SAMPLE Serial sample period parameter Press SET to choose to set the sample period The current sample period value is displayed Current sample period seconds Adjust the value with UP or DOWN and then use SET to set the sample rate to the displayed value SA 60 New sample period etd 6 Controller Operation Calibration Parameters 6 10 3 6 10 4 6 11 Duplex Mode The next parameter is the duplex mode The duplex mode may be set to full du plex or half duplex With full duplex any commands received by the fogger via the serial interface are immediately echoed or transmitted back to the device of origin With half duplex the commands are executed but not echoed The du plex mode parameter is indicated by Linefeed The final parameter in the serial interface menu is the linefeed mode This pa rameter enables on or disables off transmission of a linefeed character LF ASCII 10 after transmission of any carriage return The linefeed parameter is indicated by pd Calibration Parameters The user has access to a nu
43. terface Optional If supplied with the option the fogger is capable of communicating with and being controlled by other equipment through the digital interface Each control ler is a separate device and is fitted with a separate RS 232 port This means two ports are needed to operate both simultaneously With a digital interface the instrument may be connected to a computer or other equipment This allows the user to set the set point temperature monitor the temperature and access any of the other controller functions all using remote communications equipment Serial Communications The fogger may be installed with an RS 232 serial interface that allows serial digital communications over fairly long distances With the serial interface the user may access any of the functions parameters and settings discussed in Sec tion6 with the exception of the BAUD rate setting RS 232 Cable Wiring for Wiring IBM PC and Compatibles The serial communications ca ble attaches to the fogger Instrument Computer DTE through the DB 9 connector at the back of the instrument Fig INC 1DCD ure 5 shows the pin out of this 2 RxD 2 RxD connector and suggested cable 3TxD en wiring To eliminate noise the 1 deli serial cable should be shielded 6NC 6 DSR with low resistance between the 7 RTS 2 7 RTS connector DB 9 and the 8 5 5 8078 shield MEUS dcs Setup Instrument Computer DTE Before operation
44. the serial in Connector Connector terface must first be set up by PET PEE programming the BAUD rate som and other configuration parame 3TxD 3RxD ters These parameters are pro 4NC 4 grammed within the serial we aud interface menu 7RTS 7GND To enter the serial parameter 2 gt programming mode first press EXIT while pressing SET Figure 5 Serial Cable Wiring 27 0011 Fogging Test Chamber User s Guide 28 7 1 2 1 7 1 2 2 7 1 2 3 7 1 2 4 and release to enter the secondary menu Press SET repeatedly until the dis play reads ProbE This is the menu selection Press UP repeatedly until the serial interface menu is indicated with SErIAL Finally press SET to enter the serial parameter menu In the serial interface parameters menu are the BAUD rate the sample rate the duplex mode and the linefeed parameter BAUD Rate The BAUD rate is the first parameter in the menu The display will prompt with the BAUD rate parameter by showing BAUGd Press SET to choose to set the BAUD rate The current BAUD rate is displayed The BAUD rate of the fogger serial communications may be programmed to 300 600 1200 or 2400 BAUD The BAUD rate is pre programmed to 1200 BAUD Use or DOWN to change the BAUD rate value Press SET to set the BAUD rate to the new value or EXIT to abort the operation and skip to the next parameter in t
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