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UniBloc Moisture Analyzer

1. 0 0 0 0 0 cee eee ee 69 MI Setting the Password lllllslllllllsn RR BRI 70 Bl Setting the Moisture Analyzer ID nunnana anann aee 72 Calibrating Moisture Analyzer 0 0 0 0 eee eee 79 B Span Calibration xa duce sabes hebr ir rich Ped ance Eck RES WR aside rur 73 BI Calibrating the Temperature Option a oonan naaa aaea 73 Bl Output of calibration record aussa aana eee T1 4 Connection to Peripherals When Connecting MOC63u to Peripheral Devices 78 Using Windows Direct Function 204 av0 ss qos CREE RR Ec eeu 19 Mi Enable the Windows Direct Function 0 00 000 c eee eee 79 BI Connecting the Windows System and the Moisture Analyzer 81 Bl Displaying the Measurement Result in the Windows System 83 B ifthe Windows Direct Function does not Work Well Lue 84 a gus zie sil AYNSVAW Q o Z Z m O O zZ O JONVN3LLNIVIA 3din9 9NILOOHS318n08 L Control Moisture Analyzer from PC 0 0000 ee eee 85 Bl Setup and Use of the Communication Tool 0 0 0 00 ee 85 ME How to Use the Command Codes LLulseleeeles RR 88 E Command Code List nce cease verde pads S mots be re dea E TS S E ESSE 89 OMEeTEUDCASTRERROROTQUICO QT E EEEE EE E 90 Printer Output Option o a aoaaa aa aaa ee ees 91 Connecting a Dedicated Printer 0 0 0 00 aaea eee eee 91 Setting the
2. When replacing fuses be sure to use the fuse written in the Accessories 1 Hook the fuse holder with a slotted screwdriver and pull it toward you 9 Fuse holder Slotted screwdriver 2 Remove the fuses from the fuse Fuse holder bl ag Fuse holder iss Insert new fuses in the fuse holder Press the fuse holder all the way seated in JE Gad 104 Clearing Measurement Data from Memory G m Com AJ O m J m You can clear the measurement data from memory Once cleared it cannot be recovered 1 Start the menu CUM m MENU PROGR T zs fm The menu opens 2 Select the Clear Memory option MEM CLR from the menu B MEMCLR gt even CLR ok z PROGRAM tatata H r Start to clear memory UL JU T ML MI 1 O lt 73 O ENTER gt END gt MEMCLR IL IE LIP S Z 7 RUE m Arry Q The measurement data is cleared from memory S of the moisture analyzer E O JONVN3LNIVIA i Return to the standby state sett gt Press esc to return to the standby state measurement display where measurement can be performed ACIND 9NILOOHS3 18008 105 106 MAINTENANCE Initializing Moisture Analyzer Settings The moisture analyzer can be initialized to the factory defaults All programs are initialized Therefore no specific program numbers can be initialized 1 2 Start the menu MENU PPa GR The men
3. gt ACIND 9NILOOHS3 18008 m V Continued on next page 55 56 3 Detailed Measurement V Setting Measuring Conditions Measuring Samples by Raising Temperature Rapidly RAPID Rapid drying mode Rapid drying mode raises the temperature rapidly until the amount of change in moisture content per 30 seconds drops below the set value then dries a sample at the set temperature As the ending condition you can select either the amount of change in moisture content per 30 seconds or the time When the amount of change in moisture content per 30 seconds drops below the set value or the time reaches the set value the measurement terminates automatically Set AM and temperature in rapid drying and AM or time as the ending condition This mode is suitable for measuring liquid or other samples that take time to be dried off Start the menu MENU PROGRAM The menu opens Select RAPID mode for measuring conditions j PRG N5 gt RAP gt ENTER Specify AM for rapid drying T AM input gt ENTER Specify the moisture change rate per 30 seconds within the range from 0 1 to 9 9 in 0 01 percent increments opecify the temperature Temperature input ENTER Specify the temperature within the range from 50 C to 200 C in 1 degree increments PROGRAM PROGRAM PROGRAM I W PROGRAM L 1 17 NNA opecify the ending condition
4. M The adjusters shrink and the front of the unit drops 2 Rotate the right and left adjusters until the air bubble in the level gauge appears at the lateral center At this step you can neglect the longitudinal position of the air bubble Rotate the front right adjuster clockwise When the air bubble is on the left IN3IN3SHDSVMW JHOod3g When the air bubble is on the right AYNSVAWN Rotate the right and left adjusters at the same time until the air bubble in the level gauge appears at the longitudinal center Adjust them until the air bubble appears at the center of the red circle When you rotate two level screws clockwise at the same time GaaliviaGd The air bubble moves forward When you rotate two level screws counterclockwise at the same time The air bubble moves backward 9 Q O Z Z m O d O zz O JONVN3LLNIVIA 3din9 9NILOOHS3 18008 37 7 Before Measurement Preparing for Measurement Turn on the power of the moisture analyzer before starting measurement 35 Turning the Power On page 38 When you use the moisture analyzer for the first time we recommend the span calibration after installation 35 The Span Calibration after Installing the Moisture Analyzer page 40 Turning the Power On The following explains how to turn the power on 1 Connect the power cable Insert the female end of the power cable into the power in
5. si GS Pe S IVdaHadltid OL NOILOANNOO JONVN3LLNIVIA ACIND 9NILOOHS3 18008 V Continued on next page 81 4 Connection to Peripherals V Using Windows Direct Function Connection via the USB cable Use the following procedure to connect the moisture analyzer to the Windows system the PC using the USB cable Turn the power off 35 Turning Power Off page 50 Unplug the power cable from receptacle USB connector at the rear of the moisture analyzer Install the USB driver software on the PC by following the on screen instructions Connect the USB cable to the PC Plug the USB cable into the Mi Displaying the Measurement Result in the Windows System Use the following procedure to display the measurement results in the Excel running on the Windows system The results can also be displayed using the Notepad or other programs Turn on the power switch of the moisture analyzer T m 340439 35 Turning the Power On page 38 2 Start the Excel on the Windows system Press ST The moisture analyzer data is displayed on the Excel AYNSVAWN Ed Microsoft Excel Book J m gt gt UO SHIMADZU CORP TYPE MOCB3u SN D209400007 ID 0000 CODE 0098 DATE 10 12 13 TIME 12 47 PNO 1 UNIT MAN MODE TIME TEMP 180C STOP 00 10 S IVdaHadltid OL NOILOANNOO 5112 JONVN3LLNIVIA TIME MAN S 00 00 00 UU 00 00 05 Ls ACIND 9
6. 35 Removing the Glass Case page 99 2 Unplug the connector of the used Heater heater cable Cable supports Pull out the cables through the onnector cable supports 102 i Remove the heater from the clips uou Hold the prongs indicated with circles in the figure at right located on both sides of the heater and detach them form the clips n Install a new heater 9 Q Install the heater using the clips Plug in the cable with connector cable supports Install the heater using the clips Hold the cable with cable supports Plug in the connector 6 Install the glass case on the moisture analyzer Do not touch the glass part of the heater when installing the heater on the clip Doing so may shorten the service life of the heater L Installing the Glass Case page 101 Face the connectors in the correct direction Plug the connectors into sockets in the correct direction as Instructions shown above 103 aanviaa JUS Val 340438 OL NOILOANNOO ACIND 9NILOOHS3 18008 JONVN3LNIVIA MAINTENANCE Replacing Fuses ENESUO Aco CONMNS Q Before replacing fuses turn the power switch of the moisture analyzer OFF and remove the power plug from the socket Instructions Otherwise you could sustain an electric shock Do NOT use any fuse other than those specified Prohibitions Doing so could cause a fire or short circuit
7. I Check the measurement result Short beep sounds indicate that the measurement is completed The display panel shows the measurement result and the measurement completed indicator 3K You can output the measurement result to a printer or PC if necessary The factory default setting for the output results is FINAL 35 Setting a Measurement Data Printout Timing page 92 The heater fan stops automatically ESC Reset the measurement result PROGRAM p The water content indicator and measurement completed indicator relating to the measurement result disappear and the mass after drying process appears Proceed to After Measurement page 49 BE To Obtain the Best Results The following explains how to measure moisture content correctly Precaution for carrying out measurements in succession Placing a sample on the warmed sample pan may cause moisture from the sample to evaporate before starting measurement causing an error in measurement result Be sure to use a sample pan kept at room temperature when measuring another samples When measuring samples in succession keep a constant interval between the measurements wherever possible If the temperature inside the moisture analyzer is not stable errors may affect the measurement results Quantity and placement of powdered particulate and viscous sample materials A sample must be placed on the sample pan flatly Samples cannot be heated prop
8. Product label Shows the model name and the Level gauge Sas cd unit number Q O Z Z m O d O 2 O Used to adjust the level of the moisture analyzer I gt page 36 Keyboard Used to adjust the level of the z Used for menu manipulation tare moisture analyzer z cancellation setting measuring conditions 35 page 36 m or functions or span calibration z ISF page 27 z Q ACIND 9NILOOHS3 18008 V Continued on next page 25 1 BEFORE MEASUREMENT V Names and Functions of Parts Rear Kensington security slot A mounting hole for anti theft key This slot complies with the Kensington standard If a fuse breaks replace it with a fuse in this fuse holder Fuse holder 0 DATA I O connector Used to connect a printer EP 80 EP 90 etc F page 91 Power inlet Connect the power cable to supply power to the moisture analyzer RS 232C connector 9 pin socket USB connector Used to connect the main unit to a PC via serial interface Used to connect the main unit to a PC 26 Mi Keyboard The following explains the keys placed on the top of the moisture analyzer MOC63u Max 60g d 0 001g E 0 IN3IN3SHDSVMW JHOod3g e MENU Se AYNSVAWN Description Turns the power on or off GaalviaG Calls the menu during the standby state measurement display Ret
9. Select a timing ENTER You can select one of the following timings Option Description B Printing Stored Measurement Data The moisture analyzer saves the measurement results automatically You can manually output any of the moisture analyzer data saved in the memory to a printer For further information on clearing the stored measurement data see Clearing Measurement Data from Memory IR page 105 Connect a printer to the moisture d If the number of measured data sets analyzer exceeds 100 35 Connecting a Dedicated Printer page 91 The oldest data is overwritten by new data 2 Turn the printer power switch on For further information on turning the printer power on refer to the printer instruction manual Start the menu PROGRAM MENU PRa GR The menu opens Output the memory data from the printer y i AD imn Z gt ENTER PROGRAM A MEMORY gt ENTER The measurement result is output from the connected printer A short peep sounds at the end of memory data output V Continued on next page zio siti AYNSVAWN J m gt gt UO S IVdaHadltid OL NOILOANNOO JONVN3LLNIVIA ACIND 9NILOOHS3 18008 93 4 Connection to Peripherals V Printer Output Option How can abort the measurement data output Press ESC Return to the standby state EEE Press ES to return to the standby state BE Outputting th
10. in minutes Press murs to save the measurement conditions PROGRAM VS 7 f 77v PROGRAM W Z N 77 N PROGRAM PROGRAM 1 NAZI a AO aA AAN 2711 EE Ve at WZ SA a pe Z IV E EN z Nc d 7 V Continued on next page 61 AYNSVAWN jHoJ3g IN3IN3SHSVAIN qaiivrad Q o Z Z m O d O 2 JONVN3LLNIVIA ACIND 9NILOOHS3 18008 62 3 Detailed Measurement V Setting Measuring Conditions Return to the standby state Press 96 to return to the standby state measurement display where measurement can be performed PROGRAM gt Changing Moisture Analyzer Settings w m TI AJ O m 7 m You can change the MOC63u moisture analyzer settings by setting a sample code or by setting a moisture analyzer ID B Setting the Measurement Standard E You can select the values to be referenced for measurements gt The following shows the denotation of symbols used for formulas calculating the measurement standard m W Mass of undried material when measurement starts D Mass of dried material when measurement ends M The weight obtained by deducting the weight of dried material from the weight of undried material before measurement W D Moisture content Wet Base M W Indicates percentage of evaporated moisture mass vs the mass before drying process IN3IN3SHDSVAIN qa
11. refer to our Web site http ww w shimadzu com products balance index html When I restart the PC the Windows Direct Function does not work Some PCs may not recognize the serial key device settings during startup For further information on solutions refer to our Web site http www shimadzu com products balance index html want to use the Windows Direct Function on the Windows Vista or Windows 7 system The serial key device setup window required for Windows Direct Function setting is not displayed when the PC is running on the Windows Vista or 7 OS You can download an alternate serial key device tool from our Web site http www shimadzu com products balance index html Install the downloaded tool on your PC For further information on the setup procedure refer to our Web site http www shimadzu com products balance index html Garbled data is entered in the PC The Windows Direct Function is not set on the moisture analyzer or on the PC See Enable the Windows Direct Function IR P 79 and set up this function When I enter data in the Excel the cursor does not move into the next cell Disable the 2 byte characters conversion function of the Windows system 9 n Excel select Options from the Tools menu and click the Edit tab in the Options dialog box Then make sure the Move selection after Enter box is checked it is OK if moved to another cell Check the entry data in another a
12. 2010 Shimadzu Corporation All rights reserved Microsoft Windows and Excel are the registered trademarks of Microsoft Corporation All other company names and product names in this document are the trademarks and registered trademarks of their respective owners The symbol that represents the trademark or is not used in this document Company names organization names product names etc in this document are the trademarks or registered trademarks of their respective owners The Company does not guarantee that Windows Direct Function can run normally on all personal computers The Company is not responsible for any problems caused by this function Introduction Thank you for choosing the MOC63u Shimadzu Moisture Analyzer Shimadzu Corporation with more than 80 years experience in manufacturing high precision balances is confident in the high quality of the MOC63u moisture analyzer The MOC63u provides prompt and accurate measurement of moisture contents With the full adoption of UniBloc cell which we started to use for electronic balances in 1989 the MOC63u also features improved reliability The cross key dedicated to menu manipulation has improved the operability of the MOC63u making it easier to use The MOC63u is also equipped with the Windows Direct Function that can transmit measurement results to a PC without requiring any software to be installed as well as other various functions that users can use conveniently accordin
13. 56 Routine inspection lt 5 eb RREE A 0505 107 RS 232C connector i ens 26 8l S von P ia eam iia 9 45 47 Sample Coad cesarea E ee 30 67 95 sample Pan sis 24 31 35 47 98 SLOW Slow drying mode 29 58 Slow drying mode 29 58 Span Calibration 0 40 SPCCINCAUIONS 24522040 orsa zen 113 Stability mark oon orar gx aes 28 45 66 Standard drying automatic ending mode iu exceed d doaat anus 25 55 Standard drying timed SNGING Mode ous ados acc tee gees 28 55 PIAR PEREEMT 27 45 66 STEP Stepped drying mode 29 60 Stepped drying mode 29 60 STOP TTC 27 48 wd D 86 Stop measurement 48 T Temparature Calibration 73 Temparature sensor 2 2 res 6 23 TIME Standard drying timed ending mode ouis ere eR 285 99 Troubleshooting Guide 110 119 120 WON PEPPER 30 64 95 USB connector 00 26 82 W Warming E 40 Wandbreak i i 24 35 98 Windows Direct Function 79 110 Z Zero POINT 4245 ana RTRRQRATRSESqAS 27 45 121 7 SHIMADZU CORPORATION TOKYO OFFICE 3 Kanda Nishikicho 1 chome Chiyoda ku Tokyo 101 8448 Japan Phone 81 3 3219 5641 Fax 81 3 3219 5710 Cable Add SHIMADZU TOKYO Overseas Telex No 0232 3291 SHMDT J KYOTO OFFICE 1 Nishinokyo Kuwabaracho Nakagyo ku 604 8511 Japan Phone 81 75 823 1200 Fax 81 75 81
14. Printer Output Method 0 0 ces 92 Setting a Measurement Data Printout Timing llle 92 Printing Stored Measurement Data 0 2 0c ccc ees 93 Outputting the Moisture Analyzer Settings from a Printer 94 QUIDUL Dale s saucia eee EEEE P A YURREVdO LS NNI EF Ive sd Pedorace 95 5 Maintenance Maintenance of Moisture Analyzer 00 000 eee 98 E Removing the Glass Cases oa dbo aees ave Pega hws bane BO Rr deber dopegr d 99 B Installing the Glass Case 6 een eens 101 Replacing Heater s uu 4G04oe4dne neu ca ees SOROR weeded 9 yn eae 102 ISCDIacIHo FUSES uestis d du S demde us E SI REPRE RSdq EP eds 104 Clearing Measurement Data from Memory LL 105 Initializing Moisture Analyzer Settings ll 106 JEE ES E p P eee dewe Sado he ea dae ee dey mer 107 ME Routine Inspection 0 0 0 BB RR eee eee ee 107 EN Periodic Inspection sr aces aaau aaaea E EPGESQ pa ee de RES SM 108 Troubleshooting Guide llle 110 B if You Have a Problem een RR RRRRRRRRRR RR I 110 ME When These Messages Appear lsles n RR ee eee 111 When Regule en x 579 dom oy an E rd CPP SEP oS dep oo oe oO eS 113 B Specifications main unit sus eosasmd RR ELER ERE GE Ge 4 Rer4redu xs 113 Ia ACCBESSOHES S Leine re 9 ee ee UR ACE EUER Ara iod dd CE ar tX d PIRE ER RR ded 114 Menu Map ss oe pens ee chro oo ec aa arse
15. at the position displaced for the specific amount and evaluate the difference in their measurements Instrumental error Select three to five observation points and evaluate a difference between the actual weight and the value measured by the moisture analyzer at these points Temperature Calibrate the temperature using the optional temperature calibration kit Criteria Weight When the actual value measured by the moisture analyzer is under 50 g the accuracy should be 5 mg when it is over 50 g the accuracy should be 10 mg Temperature During temperature calibration Temperature on the pan should be within 5 C if the set temperature is 100 C Temperature on the pan should be within 5 C if the set temperature is 180 C 108 MAINTENANCE BEFORE CONNECTION TO TROUBLESHOOTING GUIDE O O v MEMO 110 Troubleshooting Guide BE f You Have a Problem If the MOC63u moisture analyzer does not operate normally check the following points Nothing appears on the display The display does not change even when a sample object is placed on the pan The display is unstable E No stability mark appears The measurement result is incorrect Desired measurement unit is not shown The Windows Direct Function does not start If you forget your password The heater does not light up The power cord is unplugged The switchboard is turned off The s
16. closed When hidden Press Sra and start measurement manually If the stability mark is shown while EASY appears the Easy method is If the stability mark is hidden while EASY appears the Normal method is set Setting Sample Codes Set sample codes to identify the sample object from output measurement results The sample code consists of four digits The first and second digits allow 0 to 9 hyphen A to Z or underscore to be entered and the third and fourth digits only allow 0 to 9 Sample code 0000 is set as default Start the menu MENU PRa GR The menu opens Select the sample code setting CoDE from the menu I o3E gt enen 0000 A 4 digit number appears and the first digit flashes Enter a sample code Code input gt Repeat for four digits gt ENTER LET 35 How to Enter Dada page 43 To shift the digit to shift the digit Press to return to the standby state PROGRAM PROGRAM N E f inm om eA ns PROGRAM PROGRAM PROGRAM PROGRAM V Continued on next page 67 AYNSVAWN 340439 IN3IN3SHDSVAIN qaiivrad Q O Z Z m O d o zi O JONVN3LLNIVIA ACIND 9NILOOHS3 18008 3 Detailed Measurement V Changing Moisture Analyzer Settings B6 Setting the Date and Time Set the date and time to be output as a measurement result Select from the follo
17. condition Samples that tend to change in composition in rapid temperature shift may burn dry making it difficult to measure their moisture contents properly Slow drying mode can set the heater temperature to rise gradually This mode is suitable for measuring samples such as protein and high molecular compound that change largely when heated in a high temperature or rapid temperature rise Start the menu PROGRAM MENU PPS GRM The menu opens Select SLoW mode for measuring conditions PRG Nol gt SL oh lt gt ENTER Specify the temperature Temperature input gt ENTER Specify the temperature within the range from 50 C to 200 C in 1 degree increments Specify the ending condition LMI TINE gt ever gt 9 5 AM or time input gt ENTER As the ending condition you can select either the amount of change in moisture content per 30 seconds or the time If AM is selected specify the value within TUN the range from 0 01 96 to 0 1 9o in 0 01 percent increments If TIME is selected you can set a time between one minute and four hours or a time in minutes up to 12 hours The time to be set here is the time period after the first slow heat drying PROGRAM 4 Lob UA e WON 0 s um ON Z2 NLA Press murs to save the measurement conditions Return to the standby state PROGRAM gt Press ESC to return to the standby state measurement display w
18. in again If the same message appears again call a service representative Unplug the power cord and then plug it in again If the same ERR 005 Memory error The heater cover was left open for more than one minute during measurement message appears again call a service representative Stop the measurement by pressing ESC ERR 101 ERR 102 The heater temperature sensor has failed Unplug the power cord and then plug it in again If the same message appears again calla service representative Press ESC and close the heater cover correctly You started measurement more than three minutes after the zero point had been adjusted Stop the measurement by pressing ESC ERR 121 ERR 122 ERR 123 Heater failure The heater cover or the heater has failed Unplug the power cord and then plug it in again If the same message appears again call a service representative Recheck the AM value or the set The AM value is not reached four hours after measurement temperature The frequency judgment is abnormal Unplug the power cord and then plug it in again If the same message appears again call a service representative Unplug the power cord and then plug it in again If the same message appears again call a service representative V Continued on next page 111 0 uonoeuuoo oJnseo N jueujeJnse
19. l l i l l l l l I M I IIS WN Tl std JL V MT Fl LI 4 Select the minimum value to be displayed during measurement J Unit selection gt ENTER l Press amp to display the step 1 screen Press Esc again to return to the standby state X zie siti Display selected in step 3 Selectable units Z 0 1 or 0 01 in AYNSVAWN IN3IN3SHDSVAIN qaiivrad Q O Z Z m O d o zi O JONVN3LLNIVIA ACIND 9NILOOHS3 18008 V Continued on next page 65 66 3 Detailed Measurement V Changing Moisture Analyzer Settings Mi Setting the Method to Start Measurement Select the method to start measurement from the following two types e Easy Place a sample and close the heater cover and the measurement will start automatically You can quickly start the measurement without pressing M e Normal Press to start the measurement manually You can start the measurement even with the heater cover open This is useful when you measure the weight of a volatile sample before it 1s dried Start the menu PROGRAM MENU PRoGRMI The menu opens From the menu select the method to start measurement START gt ENTER The method to start measurement currently selected The methods are switched each time ENTER is pressed Option Method Description Measurement starts automatically when the heater cover is p When shown Easy
20. menu opens 2 Select the output setting BROGRAWIT CoM SET from the menu JO B IFaMSET gt enter Select an output port PROGRAM QB lot nrourz1 gt 1 9 Output port Output port PROGRAM selection OOOO connection RS 232C or DATA I O i Set the output to the Windows PROGRAM Y gt LB ININ gt enter COMSET Setting the Windows Direct Function on the Windows system The Windows Direct Function must also be set on the Windows system to allow data transmission between the Windows system and the moisture analyzer For further information refer to the following Web site http www shimadzu com products balance index html Mi Connecting the Windows System and the Moisture Analyzer The following two ways are available for connecting to the Windows system e Connection via the RS 232C cable IRF page 81 E e Connection via the USB cable IRF page 82 gt w m TI AJ 9 Connection via the RS 232C cable E Use the following procedure to connect the moisture analyzer to the Windows system the PC via the RS 232C interface cable Turn the power off 35 Turning Power Off page 50 m E rs m Unplug the power cable from receptacle Plug the RS 232C cable into the RS 232C connector at the rear of the moisture analyzer J m gt gt UO Tighten and secure the setscrews Connect the RS 232C interface cable to the PC Tighten and secure the setscrews
21. to our Web site http www shimadzu com products balance index html The moisture analyzer may not operate normally in certain environments with Windows XP In that case optional tools may be required If you have a problem f communication software is already installed on the PC the Windows Direct Function is not used even when the PC is running on the Windows OS When using the dedicate printer and the Windows direct function simultaneously Attach the dedicate printer to the DATA I O connector of the analyzer Then attach the PC to the USB connector of the analyzer For the connection of dedicate printer see Printer Output Option E35 page 91 Enable the Windows Direct Function The Windows Direct Function must be set at both the moisture analyzer and on the Windows system e Setting the Windows Direct Function on the moisture analyzer IRF page 80 e Setting the Windows Direct Function on the Windows system IRF page 80 V Continued on next page 79 zie sit AYNSVAWN J m gt gt UO S IVHaHadltid OL NOILOANNOO JONVN3LLNIVIA 3din9 9NILOOHS318n08 L 80 4 Connection to Peripherals V Using Windows Direct Function Setting the Windows Direct Function on the moisture analyzer Select the following settings and all communication options will be set appropriately for the Windows Direct Function 1 Start the menu PROGRAM MENU PP 55RM The
22. you want to learn about in this instruction manual Cover Page Index You can search for the item on the cover page of the instruction manual What You Can Do page 4 You can search for the item based on what you want to do You can quickly search the menu item for the function or procedure you Menu Map page 115 want to use Table of Contents page 20 You can search for the item in the instruction manual s table of contents You can search for the item using a previously known name or keyword Notation for menu manipulations In the instruction manual some menu manipulations are indicated using simplified symbols Example Press VEW in the standby state to Information shown select the menu item on the display Li venu PROGRAM 5o Press J to move to the Menu manipulation Select the numeric next item in the menu flow value or setting ee 1 PH ia 1 x MIPRG Nok gt iener Non gt i 96 D a value gt ENTER Non User s operation or Press ENTER to accept the supplement setting or selected item Indication on the display panel The instruction manual describes the indication on the display panel corresponding to each operating procedure The operations of the display panel flashing lighting up and confirmation are indicated as follows e Flashing e Lighting up e Confirmation WIS X NN nr U
23. zt O JONVN3LLNIVIA ACIND 9NILOOHS3 18008 fT L CONNECTION TO PERIPHERALS When Connecting MOC63u to Peripheral Devices When the MOC63u moisture analyzer is connected to a PC and a printer the following functions are available Display the moisture analyzer data in an application of the PC 35 Using Windows Direct Function page 79 Control the moisture analyzer using command codes issued by the PC 35 Control Moisture Analyzer from PC page 85 Output the measurement result and the settings of the moisture analyzer to a printer is Printer Output Option page 91 Using Windows Direct Function Values shown on the moisture analyzer display can also be shown in any Windows application such as Microsoft Excel or the mass entry window of an analyzer A value transferred from the moisture analyzer is automatically entered in the cursor position of an application like the keyboard entry If keyboard entry is enabled data can be obtained directly from the moisture analyzer 35 Displaying the Measurement Result in the Windows System page 83 Differences depending on the OS used When the Windows XP operating system OS is running you can use the Windows Direct Function without using special connection and transfer applications However the dedicate tools are required to use the Windows Direct Function on the Windows Vista or Windows 7 OS For further information refer
24. 2 3438 Cable Add SHIMADZU KYOTO Overseas Telex No 05422 166 SHMDS J SHIMADZU INTERNATIONAL TRADING SHANGHAI CO LTD Shanghai Office Block E No 570 West Huaihai Road Shanghai 200052 P R of China Phone 86 21 2201 3888 Fax 86 21 2201 3666 SHIMADZU SCIENTIFIC INSTRUMENTS INC 7102 Riverwood Drive Columbia Maryland 21046 USA Phone 1 410 381 1227 Fax 1 410 381 1222 SHIMADZU EUROPA GmbH Albert Halm Strasse 6 10 D 47269 Duisburg F R Germany Phone 49 203 7687 0 Fax 49 203 7666 25 SHIMADZU ASIA PACIFIC PTE LTD 16 Science Park Drive 401 01 The Pasteur Singapore Science Park Singapore 118227 Republic of Singapore Phone 65 778 6280 Fax 65 779 2935 SHIMADZU DO BRASIL COMERCIO LTDA Avenida Marques de Sao Vicente 1771 Barra Funda CEP 01139 003 Sao Paulo SP Brazil Phone 55 11 861 1688 Fax 55 11 861 2209
25. 2006 95 EC are 10 Note 1 This declaration becomes invalid if technical or operational modifications are introduced without manufacturer s consent Note 2 This declaration is valid if this product is used alone or in combination with the accessories of this product which are mentioned in attached Appendix 1 or other instruments which fulfill with the requirement of mentioned directive Note3 Importer Distributor and Authorised Representative in EU is as follows SHIMADZU EUROPA GmbH Address Albert Hahn Strasse 6 10 47269 Duisburg F F R Germany Place and date of issue Name Title EJ sHimapzu Action for Environment WEEE To all user of Shimadzu equipment in the European Union Equipment marked with this symbol indicates that it was sold on or after 13th August 2005 which means it should not be disposed of with general household waste Note that our equipment is for industrial professional use only Contact Shimadzu service representative when the equipment has reached the end of its life They will advise you regarding the equipment take back With your co operation we are aiming to reduce contamination from waste electronic and electrical equipment and preserve natural resource through re use and recycling Do not hesitate to ask Shimadzu service representative if you require EE further information WEEE Mark MEMO Table of Contents OCO aarne ENA EEE 3 ae Ae OaD e E E E EE Sos 6S oo L EEE E
26. 3 2 Measure Measuring Moisture Content 0 0 0 0 eee eee ee 44 Bl To Obtain the Best Results 0 0 0 0 00 eee eee ee 47 Aborting Measurement 0 000 ccc eee ee 48 After Measurement lees 49 Turning Power Off 6 4 scarce thse sie T ES ooo SRSFrbRPPPSERES 50 3 Detailed Measurement Setting Measuring Conditions llle 52 BI Selecting the Measurement Condition Program No llssslllllnsese 52 Mi Setting Temperature and the Amount of Change in Moisture Content AM as Measurement Conditions AUTO Standard drying automatic ending mode 53 E Setting Temperature and Time as Measuring Conditions TIME Standard drying timed ending mode 0 0 eee eee 55 lI Measuring Samples by Raising Temperature Rapidly RAPID Rapid drying mode kids ea Rr xxx ere EORR RR ER 56 Mi Measuring Samples by Raising Temperature Gradually SLOW Slow drying mode sucum CERRAR E OR eoen es bee dod ween d 58 Bl Measuring Samples by Setting Temperature Step by Step STEP Stepped drying MOG dus dux ghe Chew e OE ER CE EUR RUE ARR Coe Ras 59 Changing Moisture Analyzer Settings llis 63 BI Setting the Measurement Standard 20 0 00 cece eee 63 Bi Setting the Method to Start Measurement 0 0 e eee eee 66 B Setting Sample Codes 1 teen eens 67 M Setting the Date and Time 0 eee eee 68 BI Restricting the Menu Display
27. 30 Level SCIEWS 4 ci o006444onsoue odes 25 36 Eo e e e knee aes nescence ekaenceevack 69 M Maintena c 244ctecacueeanaskawnens 98 Measurement date and time 30 68 95 Measurement environment 9 32 Measurement of moisture content 44 Measurement result print 9 Measurement standard 63 95 Measurement time sss es 30 Measuring conditions 25 52 Measuring temperature 30 MEM S cd oh aes eek Oe ede eee 27 42 hus MCCC 42 115 Menu map s 232022 9254 FPES EERLISTE 115 Method to start measurement 66 Moisture analyzer control by the Windows system 000005 85 N NG awed TP 70 71 O Observation window 25 Output xaiiple iccinseees055e2404 95 P Package Contents zer mms 24 POM gece etna eee ORE ee a Sample Pan Pan supporter aei ced oeeuea ox 24 31 35 Parity Dif PT 86 lg to E EEEE EET EEEE 70 a 22 2a aS en We xe 70 110 Periodic inspection iis sa sk eR be 108 POWE 2s star do cete e ux 27 38 50 Power IMI C lt s sa os dsdwd ds me terkems 26 38 Prepare for measurement 38 PRINT a xetedauaeteeeeueeds 30 92 93 94 auc sesa ce ratre NE neei ODIT 91 Print your Settings us esce nor x RE s 93 Product label us oua eq dr eade 25 PEO ORAM NOR Ea ace rocked 50m E een 28 52 Ro RAPID Rapid drying mode 29 56 Rapid drying mode 29
28. Bue UDE gt even gt YD AM or time input gt ENTER As the ending condition you can select either the amount of change in moisture content per 30 seconds or the time If AM is selected specify the value within the range from 0 01 96 to 0 1 in 0 01 percent increments If TIME is selected you can set the time to 12 hours or any time period between one minute and four hours in one minute increments Press enter to save the measurement conditions Return to the standby state Press ESC to return to the standby state measurement display where measurement can be performed AYNSVAWN 30439 IN3IN3SHDSVAIN qaiivrad Q O Z Z m O d o zi O JONVN3LLNIVIA ACIND 9NILOOHS3 18008 V Continued on next page 58 3 Detailed Measurement V Setting Measuring Conditions Measuring Samples by Raising Temperature Gradually SLOW Slow drying mode Slow drying mode raises the temperature more gradually than measurements in normal conditions taking about five minutes from the time the measurement begins until the temperature reaches the preset level As the ending condition you can select either the amount of change in moisture content per 30 seconds or the time When the amount of change in moisture content per 30 seconds drops below the set value or the time reaches the set value the measurement terminates automatically Set the temperature for rapid drying and AM or time as the ending
29. C flashes enter the calibration temperature Flashing indicates that the temperature is stable After 15 minutes has elapsed the temperature indication flashes When END is displayed the temperature calibration terminates and the moisture analyzer returns to the standby state after a short period of time Temperature input ENTER Enter the temperature indicated on the thermometer If it is left while the indicator is flashing Finish entering the figure within 15 minutes after the indicator starts flashing If it is not finished AboRT will be displayed and the calibration will finish Press HWER to terminate the heating process in high temperature range 76 Output of calibration record Start the Menu MENU PPa 51 The menu opens Select the temperature calibration record from the menu UE Jum even on 9090 2 CRLREL gt ENTER Outputs the currently selected PROGRAM calibration record The calibration record output is switched each time ENTER 1S pressed Option Description ei Calibration record sen shoves The record is output li When hidden Calibration or The record is not output For the data output of temperature calibration record see Output Data E33 page 95 Return to the standby state PROGRAMS Press amp to return to the standby state AYNSVAWN 340439 IN3IN3SHDSVAIN qaiivrad Q O Z Z m O d o
30. Moisture Analyzer Instruction Manual MOC63u ini Bos Read the instruction manual thoroughly before you use the product Keep this instruction manual for future reference 7 SHIMADZU CORPORATION KYOTO JAPAN ANALYTICAL amp MEASURING INSTRUMENTS DIVISION alizing Moisture Analyzer gS ing Package Contents uring Moisture Content Measurement easurement ing Power Off ting Measuring Conditions hanging Moisture Analyzer ing Moisture Analyzer Connecting MOC63u P 106 P 107 321 78013 Jan 2011 NOLLVIWSIOJNI M3H LO ANY STVasHdldad IENE CRAE L OL NOILO3NNOO Egi JXNSVIN LNAWSAYNSVAW Ete E EL AONVNALNIVIN AGINDS 9NILOOHS3 180081 z Ul Requests If you lend or transfer this product to others attach this instruction manual to the product If you lose or damage this instruction manual contact your Shimadzu sales representative immediately zd Ul Remarks The information in this instruction manual is subject to change without notice for the purpose of improvement All information in this instruction manual has been carefully verified to ensure its accuracy Any errors or missing information should any be found may not be corrected immediately Shimadzu Corporation the Company owns the copyright to this instruction manual Neither part nor the entirety of this document may be transferred or reproduced without the prior written permission of the Company
31. NILOOHS3 18008 V Continued on next page r 4 Connection to Peripherals V Using Windows Direct Function BE Ifthe Windows Direct Function does not Work Well If the Windows Direct Function does not work well check the following points If the problem continues contact an authorized Shimadzu representative I have set the Windows Direct Function but it does not work Check the communication cable type the Shimadzu s genuine parts or a commercial cable and check its connection status f you are using a USB to serial port converter the COM number may have been set to a number greater than 4 Change the COM number to a usable number COMI to COMA using the serial key device For further information on the COM number check and modification refer to our Web site http www shimadzu com products balance index html The USB to serial port converter driver may have failed to set up correctly Uninstall the driver first and then reinstall it on the PC The notebook may have been set to disable the RS 232C port for power saving Be sure to enable the RS 232C port before this setup Communications with other applications and PCs via a LAN may interfere with the serial key device settings Try using WindowsDirect communication without using the LAN The moisture analyzer may not operate normally in certain environments with Windows XP In that case optional tools may be required For further information
32. Option Description HS HW Sets the hardware handshaking n PROGRAM LI HS SW Sets the software handshaking HS TIM Sets the timer handshaking HS oFF Skips the handshake setting PROGRAM T What is the handshaking 9 This is the transmission shutdown and restart control method to be used when measurement result data 1s transferred from the moisture analyzer to the PC When an output port is not in use If you set the handshaking for an output port that is not in use the output timing may be delayed at ports currently being used To maintain the preset timing set the handshaking setting to HS oFF at the output port that is not in use Set a delimiter PROGRAM Select a delimiter gt ENTER Description Feeds a line ASII code 0DH PROGRAM T Returns a line ASII code OAH ICR LF Feeds a line and returns n What is the delimiter PROGRAM LJ oy This 1s a character used to delimit the data that 1s transferred from the moisture analyzer to the PC V Continued on next page 87 zie sit AYNSVAWN UO m gt gt UO S IVdaHadltid OL NOILOANNOO JONVN3LLNIVIA ACIND 9NILOOHS3 18008 88 4 Connection to Peripherals V Control Moisture Analyzer from PC How to Use the Command Codes You can use command codes to control the MOC63u moisture analyzer from the PC The following explains how to use the commands Command acceptance When the PC
33. R ENTER ENTER Items displayed during menu restriction Program No Selection Oo 9 Em er Hoga iH J800 A550 ENaNE ok Parity bits a GEEL 5 nr I ENTER ENTER ENTER ENTER ENTER ENTER ENTER emm OO Stability mark shown hidden Start automatic measurement owes It is turned on in the initial settings E AL RE n Stability mark shown hidden Calibration record output It is turned off in the initial settings ENTER ENTER ENTER ENTER ENTER I3 p 52 3 p 53 3 p 55 3 P 56 l3 p 58 3 P 59 L P 63 IL P 63 L P 66 U3 PA40 L P73 l3 P 80 RF P 85 L P 86 IL P 86 ENTER BABE Sample code entry s ams 2 parny Date and time setup ver even UNLaLH Menu restriction Password setup 0000 9999 ENTER Input ENTER 0000 ZZ99 Initialization os ENTER Memory output ENTER Output of settings s Handshaking HS LA HETIM LA He of F LR Delimiter MI U MI ur Setup of output interval ENTER ENTER ENTER ENTER ENTER ENTER ENTER ENTER ENTER ENTER ENTER ENTER ENTER ENTER ENTER ENTER ENTER ENTER 3 P 87 L3 P 87 3 P 67 3 P 68 I P 69 gt P 70 I P72 L P 106 3 P 105 I P 92 3 P 93 mes P 94 117 jueuieJnsee N 940jeg eJnsee N 0 uonoeuuoo eoueuejure A jueujeJnseeyw paled uoneul
34. SUJU g LLLILILI g ZA Sample page The following is a sample page to show the layout of this document The content does not provide actual operations Linked to the cover page index right pages only Changing Moisture Balance Settings 340438 Explanation of terms Mi Setting sample codes Set sample codes to identify the sample object fr Describe terms used for gt output measurement results MOC63u 9 A sample code is used to identify the sample from the output sample result 3Hnsval The code consists of four digits The first and second digits allow 0 to 9 hyphen A to Z or underscore to be entered and the third and fourth digits only allow 0 to 9 Sample code 0000 is set as default Start the menu z TO MENU PROGR am DE mr zm The menu opens m o f Select the sample code setting Menu operation E o P Y E 5 5 S A 4 digit number appears and the first digit flashes OL NOILO3NNOO 3 Enter a sample code Code input gt Repeat for four digits 3 enten CET 3ONVN3ANIVIA The following information will help you to use the device correctly 3dIn9 9NILOOHS3 180031 Depiction of the display Continued on next page The following appears on the top of the next page V Changing Moisture Balance Settil The title of the previous page is shown B Se
35. T Safety Notes Be sure to follow the safety guidelines 6 PICCAUMONS D C 9 How to Search for Desired Items 2 00000 cee aes 14 After Sales Service 0 0 0 0 ees 16 Supply of Parts uus dead Reda OE ARR DODA RATER CAS AGERE RE 16 Action for Environment WEEE 0 00000 0c eee 18 Table Dr Cone 44442564 0 eee 2444 GSS 5 eee oe oo EA 20 Before Measurement Checking Package ContentS 2 0 00 cee eee ee ees 24 Names and Functions of Parts x2 8 3 2 of Res m nm 29 Oe al WGI EEE EE E E E E EEE 25 E KVD oeiee oh es eh E ee es oes A 27 EI Display Pallelczs ai sa ore a an aa e e XE GERA cade oA esa ba dade arn dedos 28 El Ee a P c ET 32 BI Determining Installation Location lllllllllllllnnRRzRMmRSMese 32 E installing Pane cee sun vog tear tirk iaa E Exp re eer eed ean RE HERR A dH ee 35 BI Adjusting the Level of the Moisture Analyzer llle 36 Preparing for Measurement llle 38 Bl Turning the Power On usssesseeel RR RII II 38 B The Span Calibration after Installing the Moisture Analyzer 40 MENUS 2204 4Gdesreeun ey ough eeotwede genes E EET E EEEE 42 E How to Use the Mesias v ach ieee ares 446 0 ROO HS 8 A91 09 3003 3 FEE 3 Ee E d Ud 42 B Howto Use the MenuMap sse n I n nRRnzrP MIROR RR II 42 B How to Enter Data acd Xu oe ER be woe hie Bao Rie SSR ON E obser ec 4
36. The drying process continues until the time set as the ending condition is reached Display RAPID Rapid drying mode 35 Measuring Samples by Raising Temperature Rapidly RAPID Rapid drying mode page 56 SLOW Slow drying mode 35 Measuring Samples by Raising Temperature Gradually SLOW Slow drying mode page 58 s STEP Stepped drying mode 35 Measuring Samples by Setting Temperature Step by Step STEP Stepped drying mode page 59 Description The measurement is started The temperature is rising Continues drying at the maximum temperature after the temperature has reached the maximum and it also reaches A M amount of change in moisture content per 30 seconds set as the rapid drying mode condition The temperature is dropping to the preset level The measuring temperature has reached the preset level The drying process continues until AM moisture change rate per 30 seconds or the time set as the ending condition is reached The measurement is started The temperature is rising The measuring temperature has reached the preset level The drying process continues until AM moisture change rate per 30 seconds set as the ending condition is reached The measurement is started The temperature is rising The set first step temperature is reached The temperature is rising to the second step level The set second step temperature or AM moisture change rate
37. V Inspection What is an instrumental error This is a difference between the actual value and the value indicated by the moisture analyzer A weight equivalent to the observation point is measured by the moisture analyzer and a difference between the measured value and the weight is evaluated BB Periodic Inspection Periodic inspection is a regular inspection to be carried out periodically for example once a year The periodic inspection should cover the general measurement items such as performance and functions of the moisture analyzer The calibration certificate showing the JCSS logo for uncertainty can be issued for the moisture analyzer only We recommend that you consult our authorized service agency for actual inspection For further information refer to our Web site http www shimadzu com products balance index html The following outlines the periodic inspection Outline of periodic inspection Example Method Check the appearance and functions of the following parts for abnormalities Display panel Keyboard Sample pan Level gauge Check the following performance Reproducibility Repeat to measure a weight which is approximately half of the weighing capacity of the moisture analyzer for five to 10 times and evaluate these values Balance error due to Place a weight which is approximately one displacement fourth to one third of the weighing capacity of the moisture analyzer at the center of the pan and
38. Where dust electromagnetic waves or magnetic fields are present Place the moisture analyzer on a rigid stable and flat table or on the floor Instructions Placing the moisture analyzer on an unstable surface may cause personal injury or a malfunction Secure a sufficient space for your measurement work in consideration of the total weight of measuring objects and the moisture analyzer loaded on the installation location Use the moisture analyzer with the specified power source and in the specified voltage environment Instructions Using the moisture analyzer with an inappropriate power source or voltage level may result in fire or malfunction Also note that the optimal performance may not be achieved when power source or voltage is unstable or power capacity is insufficient 34 Installing Parts Take the following steps to install the moisture analyzer parts Install the heater insulation plate Install the heater insulation plate onto the case Align the hole in the heater insulate plate with that in the pan supporter and place the heater insulation plate on the case Install the Windbreak Align on the case with on the windbreak and place them on the heater insulation plate Install the pan supporter Place the pan supporter on the axis of the moisture analyzer main unit Align on the pan supporter with on the windbreak and insert them onto the bottom Place a sample pa
39. access the desired menu item quickly For further information on menu display and operations see Menu ESS page 42 How to use the menu map Notation of Explanation of operation menu map Select a menu item by pressing Or EN Press to move to the next menu item Press to return to the previous menu item You can return to the standby state by pressing this button on the first layer of the menu Applies the setting You can return to the standby state by pressing ES during menu display Refer to the specified page of the Instruction Manual Indicates the restriction of menu item selection Indicates the factory default to be set during menu reset V Continued on next page 115 jueujeJnseeyy eJojeg eJnsee A eoueuejure N jueujeJnsee N pejreyeq 0 uonoeuuoo uoneuloju Jeuo pue epinc BunoousejqnoJ 116 V When Required Menu map Press MENU in the standby state Defaults Hi o ENTER TIME ENTER OO OO AOAO 80 o in T es ul 2 ENTER M TEP ENTER w MW Moisture content Wet Base d HIN Dry content Wet Base r e nog Moisture content Dry Base a W Dry content Dry Base GRAM Display in grams Span Calibration ENTER ENTER 9 a FAL HE M Temperature calibration a Se Se ME Serial aee Ade slg USB connection Use the same settings for OUT 1 6 TROUBLESHOOTING GUIDE AND OTHER INFORMATION ENTER ENTE
40. ault 1 Start the menu ay anne MENU PRG 5RH The menu opens 2 Select the password setting PROGRAM PASS from the menu PASE gt even P 9999 70 Enter the password PROGRAM i E Password input gt j Repeat Zr I for four digits gt ENTER ok PROGRAM E zie sit Press to shift the digit 35 How to Enter Data page 43 If NG is displayed The entered password is not correct Repeat the procedure from step 1 AYNSVAWN Enter a new password PROGRAM Password input gt Repeat for four digits gt ENTER 5E 7 PROGRAM Press L to shift the digit P 35 How to Enter Data page 43 IN3IN3SHDSVAIN qaiivrad 4 Return to the standby state PROGRAM When PASS is displayed press to return to the standby state measurement display PROGRAM Q O Z Z m O d o zi O JONVN3LLNIVIA ACIND 9NILOOHS3 18008 V Continued on next page 71 3 Detailed Measurement V Changing Moisture Analyzer Settings Mi Setting the Moisture Analyzer ID To use several MOC63u moisture analyzer units set the moisture analyzer IDs so that you can identify which unit is responsible for measured data when you check the data The ID consists of four digits and each digit allows 0 to 9 hyphen A to Z or underscore to be entered ID 0000 is set as default 1 Start
41. be transferred at a higher baud rate ACIND 9NILOOHS3 18008 V Continued on next page 85 4 Connection to Peripherals V Control Moisture Analyzer from PC What are the WIN settings Certain Windows settings are required to use the Windows Direct Function For details see Enable the Windows Direct Function ic page 79 i Set the parity m F Select parity bit setting gt ENTER Currently selected stop bit PROGRAM Select any of the following parity bit settings Option Description Skips parity setting P NoNE eight bits long PROGRAM T Sets an odd parity PEVEN PCCE AI EVEN PANNY seven bits long What is the parity bit 9 When the measurement result data is transferred from the moisture analyzer to a printer parity bits are added to this data so that a transmission data error can be detected 4 Set the stop bit Select a stop bit gt ENTER Currently PROGRAM O selected handshaking PROGRAM T DIKT ENY Stop bit D What is the stop bit When the measurement result data is transferred from the moisture analyzer to a serially connected printer the stop bit is finally sent to identify the end of data transmission 86 b Set the handshaking PROGRAM LJ gt Select a handshaking gt ENTER Currently selected delimiter PROGRAM LJ When you use the EP 80 or EP 90 printer be sure to select the HS HW handshaking
42. ce the hole of glass case upward and slide the case down from the heater cover Place the screws where the glass case was removed through the wider opening of the glass case hole by following the step 3 described in Removing the glass case IR Page 100 slide in the glass case to the bottom and securely install it Securely tighten the two screws placed in step 3 indicated by the arrows in the figure at right Use a hexagonal wrench SB2 5 M3 101 aanviaa JUS Vah 340438 OL NOILOANNOO ACIND 9NILOOHS3 18008 JONVN3LNIVIA MAINTENANCE Replacing Heater When the heater has deteriorated or when the heating unit needs to be replaced due to the blow of lamp replace the heater with a new one Use the following heater replacement procedure BE A warns CONNNNNNGN Pull out the power cable from a receptacle Otherwise you may receive an electric shock A warnne NN Start the service only after the heater and the heater cover have cooled down Doing so may result in a burn injury Instructions Instructions Service life of heater The halogen heater of the moisture analyzer deteriorates or its lamp may blow after approximately 5 000 hours although it depends on the application conditions of the moisture analyzer If you have replaced the heater The heater output may change We recommend that you calibrate the temperature IF page 73 Remove the glass case
43. e end Place a sample pan Place a sample pan on the pan supporter Use a sample pan that is kept at room temperature 44 gt Be sure that the stability mark is displayed and adjust the zero point Before adjusting the zero point be sure that the pan supporter and an empty sample pan are placed 35 Installing Parts page 35 Do not expose the moisture analyzer to wind or vibration before adjustment is completed What is the zero point adjustment 9 An operation that cancels the mass of tare such as sample pan to measure the mass of sample correctly The heater cover during the zero point adjustment Always be sure that the heater cover is closed when adjusting the zero point After adjusting the zero point Start measurement within three minutes after the zero point adjustment If you do not start measurement within three minutes a measurement error ERR 111 occurs If an error occurs press ESC to return to the standby state measurement display Start measurement promptly after adjusting the zero point Place a sample object on the sample pan Be sure to place the sample as flat as possible on the pan so that heat 1s applied evenly to the sample during measurement Use a sample pan kept at room temperature 35 To Obtain the Best Results page 47 A sample that is less than 0 02 grams cannot be measured A sample that is less than 0 02 grams may be detected as a ba
44. e Hot During and Immediately after Measurement RE Acton 0ONNNNNNN Do not touch the shaded areas during and immediately after measurement Prohibitions The shaded areas in the following figure become extremely hot Only touch the round marks when operating Additional Notes PR Acaro When the device will not be used for a long period of time turn the power off and disconnect the power cable Instructions ILS Turning Power Off page 50 o After a power failure turn the power switch on If a power failure occurs the power is automatically turned off Turn the power switch off once Instructions then turn it on again 35 Turning Power Off page 50 35 Turning the Power On page 38 Warning labels on device N WARNING Caution Hot Do not touch the black grill or the observation window on the upper part of the heater cover Doing so may result in a burn injury Warning labels Caution Hot Start your operation only after heated parts have completely cooled down Doing so may result in a burn injury Preventing measurement of flammable materials Do not measure flammable materials N WARNING Caution High voltage Pull out the power cable from a receptacle when changing the heater Otherwise you may receive an electric shock When the glass case is removed How to Search for Desired Items There are various methods you can use to search for the function or operation
45. e Moisture Analyzer Settings from a Printer You can output the current settings of the MOC63u moisture analyzer to a printer For further information on initializing the current settings see Initializing Moisture Analyzer Settings 35 page 106 Connect a printer to the moisture analyzer 35 Connecting a Dedicated Printer page 91 Turn the printer power switch on For further information on turning the printer power on refer to the printer instruction manual Start the menu MENU PRoGRMI The menu opens Output the moisture analyzer settings from the printer epum Geo P Amma gt lt ENTER lw PROGRAM ON RoLT gt ENTER je The current settings are output from the connected printer 4 Return to the standby state PROGRAM Press to return to the standby state 94 Output Data The following explains the calibration and measurement result output from the printer When a printer and a PC are used as an output device and the Windows Direct Function is set the time measurement result is printed with a period instead of a colon Measurement result output example e Name of manufacture Shimadzu Corporation e Model MOC63u ABL gl Serial number D00000000000 Ei Device ID 0000 1 e Sample code 0006 2 Date Oct 19 2010 3 pols Time 17 14 e Program No 6 e Measurement sta
46. edicated printer operations refer to the printer instruction manual When you do not use a printer turn off the power and disconnect the cable Turn the power off J m gt gt UO 35 Turning Power Off page 50 Unplug the power cable from receptacle Plug the DATA I O cable into the DATA l O connector at the rear of the moisture analyzer S IVdaHadltid OL NOILOANNOO Connect the DATA I O cable to the dedicated printer dum 6G Pea A When turning the power switch on First turn on the power switch of the moisture analyzer Otherwise the JONVN3LLNIVIA printer may malfunction ACIND 9NILOOHS3 18008 V Continued on next page 91 4 Connection to Peripherals V Printer Output Option B Setting the Printer Output Method Use the following procedure to set up the measurement result output to the printer 1 Start the menu PROGRAM MENU PP GRM The menu opens 2 Select CoM SET from the menu e Ty LCoMSET gt ENTER GUT 1 Select an output port oT 9 ENTER NIN i Set each option Setting item Description The parameters shown at right will be set Mi Setting a Measurement Data Printout Timing You can set a time when the current measurement data is output from the printer 1 Start the menu PROGRAM MENU PPa GR The menu opens 2 Set a data output timing from the printer B UNTIL gt enter gt
47. er a 50 gram calibration weight is recommended Turning the power on 35 Turning the Power On page 38 Wait for at least one hour to warm up the moisture analyzer To calibrate the sensitivity for precision measurement the moisture analyzer must be in a stable state wherever possible To stabilize the moisture analyzer we recommend you leave it to the standby state for at least one hour This is called Warming up Start the menu MENU PPS 6AM The menu appears Start the span calibration DO D ERLI gt ees CBRL gt DARET ENTER 50000 If TEMP is displayed instead of BAL press Or to display BAL Open the heater cover PROGRAM PROGRAM wimlalilg g s r g WU ji ETAS LQ L 11106 1006 1g pmi LILILILI g Orepyp ihe 4 a Place a 50 gram calibration weight on the sample pan VURRIA When you use a weight other than 2 m LILI LI LI S m 50 grams 54 4 SI u x Z M yonne 2 Welgntother tian ihg When the mass indication flashes B 50 gram one reset the corresponding place the weight Then mass by pressing press ENTER and place the weight When the weight is placed the measurement of 50 grams starts AYNSVAWN To Calibrate with the heater cover closed Ensure that the glass protect plate does not come in contact with the calibration weight when the heater cover is closed If it does open the heater cov
48. er and perform calibration within an environment without any disturbance vibration wind GaalviaG Lower the calibration weight when S VUL m 0 000 starts to flash UU e The measurement of 0 grams starts MGR TI TI s When the mass indication flashes remove the weight Q O Z Z m O d O 2 O Wait until END is displayed The span calibration ends when END is displayed JONVN3LLNIVIA The display returns to BAL after a short period of time Press ESC to enter the standby state You can also calibrate the temperature For further information see Calibrating the Temperature Option IRF page 73 ACIND 9NILOOHS3 18008 41 7 Before Measurement Use the menu to configure measuring conditions for the MOC63u moisture analyzer or to set the display and output of its measured values B How to Use the Menu The following describes how to use the menu e Press MENU to call up the menu e Press or to select the item and press ENTER to accept the selection If a lower level of the menu tree is shown move to the lower level e Press gt to move to the lower level e Press to return to the upper level e To return to the standby state from the menu press ESC EE How to Use the Menu Map The menu map allows the user to conveniently and quickly access menu items 35 Menu Map page 115 42 B How to Enter Data Some menu items such as temperature t
49. erature calibration may not be accurate Should you be forced to open the cover close the cover in less than a minute to continue the calibration process When one minute has elapsed ERR 100 appears on the display panel and the calibration is interrupted Press ESC to return to the TEMP mode PROGRAM PROGRAM I zie sit l i AYNSVAWN IN3IN3SHDSVAIN qaiivrad Flashing indicates that heating has begun Q O Z Z m O d o zi O JONVN3LLNIVIA ACIND 9NILOOHS3 18008 V Continued on next page 19 3 Detailed Measurement V Calibrating Moisture Analyzer I When temperature indication 100 C flashes enter the calibration temperature Temperature input gt ENTER Flashing indicates that the temperature is stable After 15 minutes has elapsed the temperature indication flashes Enter the temperature calibration temperature indicated on the thermometer of the temperature calibration kit Press ENER to start the heating process in high temperature range Enter the temperature indicated on the thermometer If it is left while the indicator is flashing Finish entering the figure within 15 minutes after the indicator starts flashing If it is not finished AboRT will be displayed and the calibration will finish Press WER to start the heating process in high temperature range o When temperature indication 180
50. erly if they are not placed flatly Placing samples in mounds or in layers of varying thickness may cause the highest points to be burned leading to inaccurate measurement results Placing a larger amount of sample flatly can lead to more accurate measurement However if the amount is too large the surface of the sample may burn before inside is dried out See the following figures to place the appropriate amount of sample flatly Proper placement Incorrect placement L C O Measuring liquid samples Depending on the sample you can reduce the measurement time and improve the measurement accuracy by using fiberglass option zie sit AYNSVAW a mue 8 OL NOILOANNOO JONVN3LLNIVIA ACIND 9NILOOHS3 18008 47 Aborting Measurement You can abort the measurement in process Press during measurement 5j ABORT A long beep sound is heard and ABoRT appears on the display PROGRAM 2 Return to the standby state PROGRAM gt ESC gt Standby state The moisture analyzer enters the standby state without saving the measurement result When the STOP key is pressed again the measurement completed indicator is displayed the measurement results are stored in the moisture analyzer and the device enters the standby state Do not touch the moisture analyzer immediately The heat dispersing component of the heater cover and the sample pan release heat during and
51. etting the Date and Time page 68 S IVdaHadltid OL NOILOANNOO JONVN3LLNIVIA ACIND 9NILOOHS3 18008 97 98 MAINTENANCE Maintenance of Moisture Analyzer ENESC Aco ONMNM Q Unplug power cord from receptacle before servicing as If the power cord is being plugged into receptacle you may be shocked during servicing Start the service only after the heater and the heater cover have cooled down Prohibitions ey are hot you may burn yourse Sample pan Main unit d m Wipe and clean the main body i E jj Ren x ae i dm e o with a soft cloth moistened with a ro M ee re e small amount of mild detergent wash it in the water af Dry the pan well and place it on e the pan supporter Windbreak The windbreak can be detached from the heater insulate plate to be washed Dry it thoroughly before installing it to the heater insulate plate 6 Oo eoo O e O o Q e e T e Heater insulation plate The heater insulate plate can be detached from the main unit to be washed Dry it thoroughly before installing it to the main unit e e Q Glass case Carefully remove the glass case IRF page 99 and wipe and clean it with a soft cloth moistened with a small amount of mild detergent Q Display panel and keys Do not use organic solvents and chemicals Also do not use a chemical dust cloth They may damage the paint surface and the display
52. eyy eJojeg jueujeJnsee A pejrejeq eoueuejure N UOIJEWJOJU Jeuyo pue epinc BunoousejqnoJ 6 TROUBLESHOOTING GUIDE AND OTHER INFORMATION V Troubleshooting Guide Unplug the power cord and then plug it in again If the same ERR 202 The source voltage is abnormal Page 38 message appears again call a service representative A large error in the zero point or the sensitivity of the pan ERR CO01 ae Press to return to the ERR C02 A tare remains on the pan ERR C04 The sample pan is not mounted standby state Page 40 ay correctly Place the correct weight at the Span Calibration error 9 Incorrect weight is placed on center of the sample pan the pan E ERR oL The oL oL status was entered Check the sample pan pues ERR oL into during measurement The error code appears and the CoM ERR Anunrecognizable command moisture analyzer enters the error Page 89 Command error code was received state s Issue the correct command code L Too may samples have been ii placed oL Mount the sample pan correctly Page 35 The sample pan is not mounted Overloading correctly ABoRT e Span calibration or Press ESC to return to the standby Page 48 Operation aborted measurement was aborted EO 112 When Required B Specifications main unit Evaporation weight loss method Heat drying and weight loss method Sample weight 0 02 60 g Minimum display External wei
53. g to their aims To make full use of the performance and functions of the MOC63u moisture analyzer please read this instruction manual carefully and follow the usage instructions Please keep this instruction manual with the product so that you can refer to the manual at anytime necessary You can download the instruction manual PDF format from our web site http www shimadzu com products balance index html For information on the following points please contact your Shimadzu Balance representative e Product warranty e After service What You Can Do You can search the usage instructions for information about functions you want to try or learn about by aim Various want to measure moisture content measu ri ng Measuring Moisture Content page 44 want to set measuring conditions in detail methods Setting Measuring Conditions mm page 52 want to measure data easily Standard Drying Automatic Ending Mode mm page 53 want to measure data by setting the time Standard Drying Timed Ending Mode gt page 55 want to measure samples that change largely with Slow Drying Mode map page 58 want to measure the amount of change in moisture content at different temperatures Stepped Drying Mode ms page 59 For accurate want to measure data accurately with the moisture analyzer measurements Calibrating Moisture Analyzer m page 73 want to span calibration of the moisture analyzer Span ca
54. ght range for 10 60g span calibration Measurable quantities Moisture content Wet Base and Dry Base weight solid content Sample weight 2 g 0 15 Sample weight 5 g 0 05 Sample weight 10 g 0 02 Standard drying automatic ending mode Standard drying timed One to 240 minutes of measurement or 12 hours Measurement modes ending mode of maximum continuous measurement Rapid drying mode Automatic or timed ending mode is selectable Slow drying mode Automatic or timed ending mode is selectable Repeatability Standard deviation Stepped drying mode Automatic or timed ending mode is selectable Heater temperature range 50 C to 200 C in 1 C increments Backlit LCD display 120 x 30 mm RS 232C interface External output Data I O interface USB interface Allows for data output using Windows Direct function Storage of measurement Allows for storage of 10 sets of measurement conditions conditions Allows for storage of 100 pieces of data Tp ratore pen 5 C to 40 C maximum of 85 RH operating range Halogen straight tube Heat source Power supply AC 100 120 V AC 220 240 V Approx 202 OW 336 D 157 H m 1 The repeatability standard deviation is shown for the standard measurement when disodium tartrate dihydrate is sampled Measurement of other types of samples under various environments and measuring conditions is not guaranteed eoueuejure N 7 The temperature on the pan is
55. h a sample may burst Prohibitions Do not use the moisture analyzer only to dry a sample e The moisture analyzer is for measuring the moisture level of a sample and should not be used Prohibitions for any other purposes Measure samples within the safety range e Use the moisture analyzer only for measurements that vaporize moisture by heating Instructions v e Set the drying temperature within the safe temperature range of each sample Environment for Measurements ENEESUO Acun S Do not place flammable objects near the moisture analyzer Prohibitions If lightning is expected to strike turn the power off and disconnect power cable Instructions 3 Turning Power Off page 50 Mi Handling the Moisture Analyzer During and Immediately after Measurement EEA caution Install the parts correctly Install the sample pan and pan supporter correctly Instructions pep P PP y 35 Installing Parts page 35 Do not touch the sample pan and surrounding parts with bare hands during or immediately after measurement The sample pan and surrounding parts become extremely hot immediately after measurement Be sufficiently careful so as not to suffer a burn injury e Be sure to use the Sample pan handler when removing the sample pan Prohibitions e Never touch any metal parts of the heater or surrounding parts when removing the sample pan Otherwise burn injuries may result Parts that Becom
56. here measurement can be performed PROGRAM gt s Measuring Samples by Setting Temperature Step by Step STEP Stepped drying mode In the Stepped Drying mode you can set the drying temperature and time in one to three steps for measurement purposes As the ending condition you can select either the amount of change in moisture content per 30 seconds or the time After measuring a sample by changing drying temperature in two or three steps when the amount of change in moisture content per 30 seconds drops below the set value or the time reaches the set value the measurement terminates automatically Set the temperature and time of the first step the temperature and time of the second step AM if measurement ends at the second step the temperature of the third step and AM or time as the ending condition If the crystal of hydrate is dried off heat changes its composition As a result moisture content may be measured differently depending on the drying temperature Stepped drying mode setting the drying temperature in maximum three steps is suitable for measuring moisture content at different temperatures V Continued on next page AYNSVAWN 340439 IN3IN3SHDSVAIN qaiivrad Q O Z Z m O d o zi O JONVN3LLNIVIA ACIND 9NILOOHS3 18008 59 3 Detailed Measurement V Setting Measuring Conditions 1 Start the menu The menu opens Select STEP mode for measuring co
57. hieved when power source or voltage is unstable or power capacity is insufficient Q Ground the product To prevent electric shock and to maintain stability in operation of the product be sure to ground the product Instructions The product will be grounded when its power plug is inserted into a 3 wired power socket equipped with a ground terminal PE Ac ONNNNN S Do not place anything on S Do not attempt to measure samples top of the heater cover that may undergo dangerous chemical Prohibitions Prohibitions reactions when heated Doing so may result in fire Doing so may result in an explosion or release of toxic gas Do not place flammable materials near the moisture Prohibitions analyzer Some parts of the moisture analyzer become extremely hot during operation and could cause a fire if flammable materials are placed nearby Do not touch the heat dispersing Do not place any non heat component of the heater cover or sample resistant objects near the Prohibitions pan with your bare hands during and Prohibitions moisture analyzer immediately after measurement Some parts of the moisture analyzer Doing so may result in burn injury become extremely hot during operation and could lead to damage or deformation of non heat resistant objects This moisture analyzer is extremely hot during and immediately after measurement When touching the moisture analyzer only use the specified control knobs and acces
58. iivrad x 100 Dry content Wet Base D W Indicates percentage of the residual mass after drying process vs the mass before drying x 100 Q O Z Z m O d o zi O Moisture content Dry Base M D Indicates percentage of the evaporated moisture mass vs the mass after drying process 999 99 is the maximum value x 100 JONVN3LLNIVIA Dry content Dry Base W D Indicates percentage of the mass before drying process vs the residual mass after drying 999 99 is the maximum value x 100 Mass GRAM Indicates the mass after drying process ACIND 9NILOOHS3 18008 V Continued on next page 63 3 Detailed Measurement V Changing Moisture Analyzer Settings Either of the following is selectable for the minimum value to be displayed For mass 0 001 grams or 0 01 grams For others 0 1 or 0 01 1 Start the menu 2 MENU PPS RIT The menu opens Select the measurement standard setting UNIT from the menu UNIT gt ENTER The display currently selected Select the type of value to be referenced Measurement standard selection gt ENTER Display Description Moisture content Wet Base Dry content Wet Base Moisture content Dry Base Dry content Dry Base Wi j j 4l 4l M 1 tl T 4l M 1 tl INI LA PROGRAM PROGRAM PROGRAM PROGRAM PROGRAM PROGRAM i AUTO UNIT
59. ime AM Moisture change rate for 30 seconds and password require input of values Key operation Key Input data ENTER Accepts the entered value Temperature Time AM The value 0 to 9 increases If this key is held down the value changes from 9 to 0 and the tenth digit is incremented The value decreases If this key is held down the value changes from to 0 and the tenth digit is decremented Returns to the previous setting Goes to the next setting Operation Password ID In the password field The display value changes from 0 to 9 sequentially In the ID input field Values 0 to 9 a negative sign characters A to Z and a space are displayed sequentially In the password field The display value changes from 9 to 0 sequentially In the ID input field A space characters Z to A a negative sign and values 9 to 0 are displayed sequentially Shifts the active digit that is flashing to the left by one Four digits for a password or ID Shifts the active digit that is flashing to the right by one Sample code First and second digits Values 0 to 9 a negative sign characters A to Z and a space are displayed sequentially Third and fourth digits The value 3 to 9 increases First and second digits A space characters Z to A a negative sign and values 9 to 0 are displayed sequentially Third and fourth digits The value dec
60. ime output TEMP Temperature Single time output Key operations zie sit Command Function Command Function Command Function me m Q 9j System control AYNSVAWN Command Function o Sets an ID consisting of 4 ID xxxx alphanumeric characters STATE Outputs all function settings Span calibration J m gt rx m UO Command Function IECAL Calibrates the span externally Sets the standard calibration ECAL W XxXX xxx weight where xxxx xxx is 9 5 grams or more GLPO0 GLP output OFF GLPO0 GLP output ON Others S IVdaHadltid OL NOILOANNOO Command Function space Clears the buffer Selects the Echo Back mode JONVN3LLNIVIA alphanumeric characters ACIND 9NILOOHS3 18008 V Continued on next page 89 4 Connection to Peripherals V Control Moisture Analyzer from PC Bi Cable Tie IBM PC AT DOS V for AX series PC D sub9 pin straight cable ties PCside MOC63u side Printer Output Option 7 w m TI AJ O E P m Connect a printer to the MOC63u moisture analyzer to output the measurement and calibration results to the printer Mi Connecting a Dedicated Printer E Any of the following printers can be connected to the DATA I O port of the MOC63u moisture gt analyzer e EP 80 m e EP 90 The DATA key and other buttons are not enabled For further information on the d
61. immediately after the measurement Do not touch the moisture analyzer with your bare hands The heater fan is still running and stops after a short period of time Proceed to After Measurement page 49 48 After Measurement After the measurement of a sample is completed dispose of the sample and cool off the heater to prepare for the next measurement Open the heater cover BE A caution M The heater cover is hot during and immediately after measurement Hold the handle when opening or Prohibitions closing the heater cover Dispose of a sample used for measurement Hold an edge of the sample pan with the handler as shown and remove the sample pan and dispose of the sample The sample pan and the sample are hot Wait until they are cooled off After the disposal return the sample pan onto the pan supporter If you used an aluminum pan disposal dispose of it together with the used sample For further information on measuring another sample in succession see Precaution for carrying out measurements in succession EG page 47 BE A caution M During and immediately after measurement the inside of the heater cover and the sample pan Prohibitions is very hot Use the Sample pan handler to take out the sample pan zie sit AYNSVAW OL NOILOANNOO a mue 8 JONVN3LLNIVIA ACIND 9NILOOHS3 18008 Turning Power Off The following explains how to tur
62. ing functions are available when the menu is restricted 35 Measuring Moisture Content page 44 IN3IN3SHSVAIN qaiivrad 35 Restricting the Menu Display This page 35 Printing Stored Measurement Data page 93 For further information on the menu to be displayed see Menu Map IR page 115 1 Start the menu PROGRAM MENU PRoGRMI Q O Z Z m O d O Z The menu opens 2 Select the restriction of menu E display LoCK from the menu ILoCk gt ever PASS JONVN3LLNIVIA PROGRAM gt SS SSS AUTO I ACIND 9NILOOHS3 18008 V Continued on next page 69 3 Detailed Measurement V Changing Moisture Analyzer Settings 3 Enter the password PROGRAM Password input gt Repeat for four digits gt ENTER ok Press gt to shift the digit 35 How to Enter Data page 43 The restriction of menu display is switched on or off When LoCK is displayed press to return to the standby state measurement display If NG is displayed The entered password is not correct Repeat the procedure from step 1 Return to the standby state i gt Press ESC or to return to the standby state PROGRAM Mi Setting the Password Restrict the menu display by setting the password The password consists of four digits and each digit allows 0 to 9 to be entered Password 9999 is set as def
63. installed IN3IN3SHDSVMW JHOod3g AYNSVAWN GaalviaG Q O Z Z m O d O 2 O JONVN3LLNIVIA ACIND 9NILOOHS3 18008 31 7 Before Measurement Installation The following explains the process flow from installing the moisture analyzer to starting measurements B6 Determining Installation Location Measurement performance of the moisture analyzer depends largely on environments where the moisture analyzer is installed To ensure safe and accurate measurements follow the following precautions ENESSC A cauno cONNMMNM Do not use the moisture analyzer in the following locations e Where corrosive gas or inflammable Prohibitions gas 1s present e Where a flammable material is present 32 EA caution S Do not use the moisture analyzer in the following locations aged The measurement result may be incorrect Prohibitions INAWSenNsvan JHOod3g e Where there is an air flow near an air conditioner air vent door window etc AYNSVAWN e Where temperature changes extremely Gaalviad e Where vibration occurs Q O Z Z m O d O 2 O e Exposed to direct sunlight AONVNALNIVA ACIND 9NILOOHS3 18008 V Continued on next page 33 1 BEFORE MEASUREMENT V Installation ENERO A canon cCONNNNNNN Do not use the moisture analyzer in the following locations Prohibitions e
64. lance error Place a sample with at least 0 02 grams on the sample pan Check whether the stability mark is displayed zie sit AYNSVAW Qa 1Ivlad OL NOILOANNOO AONVNALNIVA PROGRAM gt ACIND 9NILOOHS3 18608 V Continued on next page 45 PATI V Measuring Moisture Content b Close the heater cover The measurement starts automatically If the measurement does not start automatically Manual start is set for measurement Press Sra to start the measurement Switching between automatic and manual start modes As the default setting measurement start automatically after a sample is placed and the heater cover is closed PROGRAM You can switch the mode to manual start D Setting the Method to Start Measurement page 66 To check the AM When is pressed in any measurement mode the display switches and the AM value is shown Press this key again to return to the previous display 9 What is AM AMisthe rate of moisture change after 30 seconds 35 Setting Temperature and the Amount of Change in Moisture Content AM as Measurement Conditions AUTO Standard drying automatic ending mode page 53 Do not touch the inside of the heater cover immediately The heat dispersing component of the heater cover and the sample pan release heat during and immediately after the measurement Do not touch the moisture analyzer with your bare hands
65. let located at the rear of the main unit Plug in the male end of the power cable to the outlet To prevent electric shock and to maintain stability in operation of the product be sure to ground the product Instructions Use the specified power cord 10A rating Instructions 38 When the power switch is turned on the version number 1 is displayed and the internal system is checked automatically Then oFF appears on the display panel 1 The version number is subject to change without notice IN3IN3SHDSVMW JHOod3g AYNSVAWN 2 Press msn The entire display lights up GaalviaG gt CHECK gt 2000 The device enters the standby state If you start measurement by using the program No displayed on the upper left of the display proceed to step 4 of Measuring Moisture Q O Z Z m O d O zz O Content ISF page 44 a PROGRAM P10 00 00 400 wt 4 smn NIC NI NE o c MUTO UNIT COMSET CODE DATE CAL PRINT AONVNALNIVA PROGRAM gt ACIND 9NILOOHS3 18008 V Continued on next page 39 40 1 BEFORE MEASUREMENT V Preparing for Measurements The Span Calibration after Installing the Moisture Analyzer After installing the moisture analyzer we recommend you warm it up and perform span calibration to stabilize the moisture analyzer The span calibration is possible between 10 and 60 grams howev
66. libration mm page 73 want to calibrate the temperature of the moisture analyzer Calibrating the Temperature 1 umb page 73 1 The temperature calibration kit option is required Outputting measurement results and settings Others want to transfer the measured data to PC Excel etc Using Windows Direct Function ma page 79 want to set the ID for each moisture analyzer unit to control several units Setting the Moisture Analyzer ID ms page 72 want to set sample codes for the moisture analyzer to control samples Setting Sample Codes mm page 67 want to set the date and time for the moisture analyzer to control the measurement date and time Setting the Date and Time mmy page 68 want to print out measurement results Printing Stored Measurement Data mm page 93 want to print out the settings Outputting the Moisture Analyzer Settings from a Printer mm page 94 want to switch types of values to be referenced for measurement Setting the Measurement Standard mm page 63 want to restrict menu items to be displayed Restricting the Menu Display mmi page 69 want to set the password Setting the Password mm page 70 want to clear measurement data from memory Clearing Measurement Data from Memory mm page 105 want restore the default settings of the moisture analyzer Initializing Moisture Analyzer Settings mm page 106 Safety Notes To u
67. lue terminates the measurement automatically Set the drying temperature and the ending condition of moisture change rate per 30 seconds When GRAM is selected for measurement standard E33 Page 63 specify AM for Moisture Content Wet Base Start the menu MENU PRoGRMI The menu opens Select AUTO mode for measuring Pena conditions m I PR5 No1 C 9 A AUTO gt enter PROGRAM V Continued on next page ACIND 9NILOOHS3 18008 AYNSVAWN 340439 IN3IA3SHDSVAIN qaiivrad Q O Z Z m O d o zi O AONVNALNIVA 54 3 Detailed Measurement V Setting Measuring Conditions opecify the temperature Temperature input gt ENTER Specify the temperature within the range from 50 C to 200 C in 1 degree increments Specify AM AM input gt ENTER Specify the moisture change rate per 30 seconds within the range from 0 01 96 to 0 1 9o in 0 01 percent increments Press to return to step 3 Press murs to save the measurement conditions Return to the standby state Press esc to return to the standby state measurement display where measurement can be performed When measuring a sample that has low moisture content If you use the standard automatic drying operation mode to measure a sample that has a low moisture content 0 196 or less it may reach the ending condition at once and your measurement may fail To measure a sa
68. mple that has a low moisture content we recommend that you use the standard drying time mode as explained on the next page PROGRAM PROGRAM gt oetting Temperature and Time as Measuring Conditions TIME Standard drying timed ending mode Standard dry time ending mode dries a sample at the set temperature and when the time set as z the ending condition is reached terminates the measurement automatically Set the temperature P w RB ES and drying time d Im uU im This mode is suitable for measurements to be completed within a limited time z Start the menu MENU PPS GR T The menu opens gt es 7 m Select TIME mode for measuring conditions J PR65 No1 Qu UIME gt enter Specify the temperature Temperature input gt ENTER Specify the temperature within the range from 50 C to 200 C in l degree increments Specify the time Time entry 9 ENTER You can set the drying time to 12 hours or any time period between one minute and four hours in one minute increments Press _ to return to step 3 Press murs to save the measurement conditions Return to the standby state Press ese to return to the standby state measurement display where measurement can be performed PROGRAM m IN3IN3SHDSVAIN qaiivrad Q O Z Z m O d o zi O PROGRAM T AS PT IF IL ee TS N JONVN3LLNIVIA PROGRAM
69. n Place a sample pan on the pan supporter so that brim of the supporter can secure the sample pan Sample pan fe Pan supporter A o Windbreak e DD O Heater s m insulation plate gt gt e SQ Z5 iw V Continued on next page INAWSenNsvaAWN JHOod3g AYNSVAWN GaalviaG Q O Z Z m O d O 2 O JONVN3LLNIVIA ACIND 9NILOOHS3 18008 35 36 7 BEFORE MEASUREMENT V Installation Adjusting the Level of the Moisture Analyzer This moisture analyzer unit maintains the level with three points on the bottom One fixing point at the rear middle position and two level screws on the front right and left positions You can check the level gauge to determine the level How to operate the level screws The height of the level screws can be changed by rotating it Rotate it clockwise as seen from the top to increase the height of the adjuster and so is moisture analyzer unit Rotate it counterclockwise as seen from the top to reduce the height of the adjuster and so is moisture analyzer unit 7 A Level gauge After installing or moving the moisture analyzer unit take the following steps to adjust the level of the unit Rotate the right and left level screws e E a counterclockwise as seen from the top Ooe eooo Rotate them carefully until they stop d pen e eee
70. n Span calibration 50 002 g Balance weight reading after calibration Span calibration 50 000 g Span calibration completed Signature title Variable value 35 Setting the Moisture Analyzer ID page 72 2 Variable value IRF Setting the Date and Time page 68 3 Variable value 33 The Span Calibration after Installing the Moisture Analyzer page 40 96 Temperature calibration output example Name of manufacture Shimadzu Corporation E S d i To Model MOC63u EC i n agre Serial number D00000000000 Tr Device ID 0000 1 o l Date Oct 19 2010 2 NEN XN Time 17 21 15 2 Set temperature 100 C m RENNES Temperature before calibration 100 C 2 EN VN Temperature after A calibration 100 C e _____ _ _ __ _ Set temperature 180 C Temperature before calibration 181 C Temperature after calibration 180 C Temperature calibration completed Signature title J m gt gt UO Variable value 35 Setting the Moisture Analyzer ID page 72 2 Variable value IRF S
71. n carrying out actual inspections Mi Routine Inspection The operator or manager needs to routinely check the moisture analyzer You can determine the minimum number of points to check The following gives examples Routine inspection Example 1 NN Before starting measurement and before Inspection time Before starting the measurement important measurement Method Check for an instrumental error Check for an instrumental error at a single at a single point point Determine a single observation As the inspection point before measurement point which is a little higher determine a single observation point which than the upper limit of actual is a little higher than the upper limit of the Routine inspection Example 2 measurement range entire possible range in actual measurement As the inspection point before conducting an important measurement determine an observation point that is slightly larger than the mass of the sample object to be actually measured Criteria The value actually measured The value actually measured by the by the moisture analyzer and moisture analyzer and it shall be within 5 it shall be within 5 of an of an additional decimal place added to the additional decimal place added required level of accuracy to the required level of accuracy V Continued on next page 107 aanviaa JUS Val 340438 OL NOILOANNOO ACIND 9NILOOHS3 18008 JONVN3LNIVIA MAINTENANCE
72. n off the power of the moisture analyzer 1 Press and hold _ o until oFF PROGRAM C appears on the display M 2 i at least 0 2 second If you hold down gt for about 0 2 second the power switch is turned off READY appears on the panel and the analyzer is ready for use To cut the power completely remove the power cable Ready status is The moisture analyzer is in the energy saving mode and ready for use When the moisture analyzer is in the ready sate electricity is supplied and the analyzer is kept heated even though it is in the energy saving mode 50 MEASURE BEFORE DETAILED CONNECTION TO TROUBLESHOOTING GUIDE MAINTENANCE LO MEMO 52 3 Detailed Measurement Setting Measuring Conditions There are four types of drying modes standard drying rapid drying slow drying and stepped drying for measurement conditions There are two types of ending modes automatic ending and timed ending Configure the temperature time or AM amount of change in moisture content per 30 seconds for all modes Saving the measuring conditions enables you to call relevant conditions when needed and measure moisture content based on these conditions A maximum of 10 measuring conditions can be saved The procedures to set measuring conditions are as follows Setting Temperature and the Amount of Change in Moisture Content AM as Measurement Conditions AUTO Standard drying aut
73. n the temperature calibration kit refer to the instruction manual attached to the kit The calibration record can be output automatically if a printer is connected in advance i Printer Output Option page 91 Q O Z Z m O d o zi O 1 Insert the thermometer probe firmly into the temperature calibration kit JONVN3LLNIVIA ACIND 9NILOOHS3 18008 V Continued on next page 73 3 Detailed Measurement V Calibrating Moisture Analyzer 2 Open the heater cover of the moisture analyzer take out the sample pan and place holder of the temperature calibration kit assembled in step 1 Align the hole in the holder hole with that in the Windbreak Close the heater cover and check that the sensor probe fits the indentation in the heater cover A Start the menu MENU PPa GR The menu opens 2 Select the temperature calibration from the menu YD cri oem un 9739 03 TEMP gt enter BC To calibrate the temperature correctly Calibrate when the temperature of the moisture analyzer is the same as the temperature of the room Start heating at 100 C A heating process begins What if you open the heater cover during the heating process It is dangerous to touch the heater cover and the inside of the cover during calibration as they become extremely hot Basically do not open the heater cover during temperature calibration Otherwise the temp
74. ndard Moisture Content Wet Base 4 e Measurement mode Standard drying timed ending mode TIME e Drying temperature 120 C e Ending condition 2 minutes e Mass before measurement 1 638g e Measurement time e Measurement time 5 and measured value based on the standard u e Mass after aiiud measurement 1 635 g Variable value 35 Setting the Moisture Analyzer ID page 72 2 Variable value 33 Setting Sample Codes page 67 3 Variable value 33 Setting the Date and Time page 68 4 Variable value 35 Setting the Measurement Standard page 63 5 Variable measurement interval lIG3 Setting the Printer Output Method page 92 V Continued on next page 95 zie siti AYNSVAWN J m gt gt UO S IVdaHadltid OL NOI LO3NNOO JONVN3LLNIVIA ACIND 9NILOOHS3 18008 4 Connection to Peripherals V Printer Output Option Span calibration output example Name of manufacture Shimadzu Corporation Model MOC63u SESS eo Serial number D00000000000 Device ID 0000 1 Date Oct 19 2010 2 Time 17 20 06 2 NENNEN Weight used 50 000 g 53 Balance weight reading before 9 calibratio
75. nditions LPRG No1 gt 9 C B STEP gt even Specify the temperature of the first step Temperature input gt ENTER Specify the temperature within the range from 50 C to 200 C in 1 degree increments Specify the time of the first step Temperature input gt ENTER Set the value within the range from one minute to 240 minutes in 1 minute increments opecify the temperature of the second step Temperature input gt ENTER Specify the temperature within the range from 50 C to 200 C in 1 degree increments opecify AM or the time of the second step M ran umi en 9 7860 AM or time input gt ENTER If the measurement ends at the second step Select AM specify the value within the range from 0 01 to 0 1 9o in 0 01 percent increments and proceed to step 8 If the measurement proceeds to the third step Select TIME and specify the value within the range from 0 minute to 240 minutes in 1 minute increments If set to zero 0 no measurement starts in subsequent steps opecify the ending condition p CIM TIME gt enter gt 7 WA 3 AM or time input gt ENTER As the ending condition you can select either the amount of change in moisture content per 30 seconds or the time If AM is selected specify the value within the range from 0 01 to 0 1 9o in 0 01 percent increments If TIME is selected you can set a time between 0 and 240 minutes
76. oju Jeuo pue epinc BunoousejqnoJ 118 OO MT 27 45 Alphabets A CCESSOT ES 545 cao hehe eee desta ds 114 AUTO Standard drying automatic ending Mode ace actes oor hae es 28 59 Boe Baud 308 22d ura Rari ars 85 92 C q c 30 40 75 77 Calibration record 24445 iier bes TT Calibration Weight 4 Cleat MCMOly us 24 40 kee RR RP ROS S 105 CODE 24 542224480450 ERATE 30 67 95 CONLSBL 252532 Es gt COMSET Command eode uai erm erm 88 89 Communication symbol 28 COMSET o ese5e nceui URSUS 30 80 85 D DATA I O connector x zr na 26 91 DATE Lud aRERUAUR oe a i 30 68 95 IBI IT o aoe 4 os Bee bee tee ee 87 Display 20 conte eawset Sa dee 28 98 110 E ENTER 2 o2 omi e b X EENAA 27 42 43 Enter duld zenuesosed aoa pd bw qa dd 43 TIS Dang ergo a G4 E OE ee ed ee 111 Elf Ol c2 de erem ERO RES ae 110 111 OG Words PAS RA EATERSIREASERES 27 42 NCC aed aa ad oe oie outs eae ee oo 83 84 F Fuse holder piece mier RES Uer 26 MM Handshaking sa us oues E eee oo oes 87 Healtek ood iac vod reis 25 31 102 110 Heater COVEN sedo vut e erm 25 31 44 98 Heater Insulation Plate 24 35 98 lj rm 12 95 RC CIDIDIMEREEEETT TS TT TT ease 106 T stallatlOth 12 ato 3x hoa aereo dear s 32 Koo Kensington Security Slot 26 Keyboard uu cura ae cea uS ES raw 27 98 L LeVel PdUBO os esce Onsen en eee eos 25
77. omatic ending mode page 53 e Setting Temperature and Time as Measuring Conditions TIME Standard drying timed ending mode page 55 e Measuring Samples by Raising Temperature Rapidly RAPID Rapid drying mode page 56 Measuring Samples by Raising Temperature Gradually SLOW Slow drying mode page 58 Measuring Samples by Setting Temperature Step by Step STEP Stepped drying mode page 59 To protect the heater You cannot use the heater for more than one hour with the temperature set above 180 C B Selecting the Measurement Condition Program No Select the program No to store measurement conditions 1 Start the menu PROGRAM C MENU PPa GR The menu opens 2 Select the program No to save IRAE measuring conditions PRG No gt ENTER Non n indicates the PROGRAM program No currently selected M S 7 o R l D Nog No9 gt enter 6 1 023 XXX indicates setting of th No wy indicates setting of the program No S 2 m The program No is changed m INL 1 X l AUTO ug J Press Es to return to the standby state _ z PROGRAM gt Setting Temperature and the Amount of Change in Moisture Content AM as Measurement Conditions AUTO Standard drying automatic ending mode Standard drying automatic ending mode dries a sample at the set temperature and when the amount of change in moisture content drops below the set va
78. onnecting other peripherals may cause abnormal operation To prevent problems be sure to connect peripherals using the procedure specified in this instruction manual If an abnormal situation occurs for example a burning odor is smelt remove Instructions the power cable immediately After a power failure turn the power switch on Instructions l If a power failure occurs the power is automatically turned off See Turning the Power On IY Page 38 to restore operation If you continue operating the device in an abnormal situation fire or electric shock may result Precautions The moisture analyzer includes a heater that heats samples to dry them off during measurement The heater becomes hotter than the preset heating temperature Incorrect handling may cause fire explosion burn injury or other injury To ensure your safety during measurements carefully read this section along with Safety Notes IRS page 6 and follow the guidelines outlining correct operation procedures Samples The samples measured with the MOC63u moisture analyzer are heated during the measurement Measuring hazardous samples may lead to burn injuries or fire ENEESCO Acun CON Do not measure the following hazardous samples e Samples in which the characteristics are unknown Measuring hazardous samples may lead to burn injuries or fire e Any sample whose surface hardens or solidifies by heating causing high inner pressure Suc
79. ource voltage is incorrect The power fuse may be blown or dismounted The sample pan or its supporter may have become dismounted The moisture analyzer is unstable on the table The pan or the sample may have come in contact with the windbreak or heater cover Span calibration has not been performed 9 Zero is not shown before measurement The desired measurement unit has not yet been set Check the power supply and source voltage and connect the power cord correctly Mount the fuse correctly Keep the moisture analyzer way from vibration wind and other disturbance 9 Place the moisture analyzer on a stable desk Clear the display by pressing 3 o and start measurement Set the desired measurement unit to be displayed For further information see If the Windows Direct Function does not work well The heater cover may be open The heater may be turned off The power cable of the heater may be unplugged Close the heater cover 6 TROUBLESHOOTING GUIDE AND OTHER INFORMATION Phenomenon Possible cause Actions taken EM Page 32 Page 84 B When These Messages Appear When any of the following messages appears on the panel take actions given ERR 001 ERR 002 Hardware error The temperature sensor has failed The hardware information is incorrect Unplug the power cord and then plug it
80. outputs a command the COM ERR message may be displayed and the command may be rejected by the moisture analyzer according to its conditions A command ending with a digit a character or a symbol other than Equal sign A delimiter C R ASCII code 0DH is added after each command code and this code is sent to the moisture analyzer Example 1 Input command code Command code to be sent Result The moisture analyzer ID is read A command ending with an Equal sign Enter an argument after each command code and this code is sent to the moisture analyzer with a delimiter in the end Example 2 Input command code Command code to be sent Result ID 1234 ID 1234 C R e analyzer ID is set to Echo back command A string consisting of n characters which begins with an echo back command and ends with a delimiter is retransmitted from the moisture analyzer N lt 30 if the queued commands do not remain in the receive buffer of the moisture analyzer Example 3 Input command code command eode Result to be sent When the moisture analyzer receives this command it outputs A BCDEFG12345 C R This character string or any character string can be printed out on a printer if connected A BCDEFG12345 ABCDEFG12345 C R B Command Code List When controlling the MOC63u moisture analyzer from the PC the following commands are available Data output gt Command Function U Single t
81. panel Mi Removing the Glass Case To clean the glass case carefully remove it from the moisture analyzer EN Acro S Do not directly touch the heater or the sensor Prohibitions 1 Open the heater cover 2 Loosen two setscrews shown by E arrows Use the SB2 5 M3 hex wrench in the accessory kit Doing so may shorten the service life of the heater or result in malfunction V Continued on next page 99 qativiaad JUS Vah 340438 OL NOILOANNOO ACIND 9NILOOHS3 18608 JONVN3LNIVIA 100 MAINTENANCE V Maintenance of Moisture Analyzer Detach the glass case Slide the glass case to remove it through the wider opening of the glass case hole Do not touch broken glass with your bare hands Prohibitions If the glass case is broken be sure to handle the broken glass carefully so that you do not get injured Place the glass case on a flat surface and clean it Glass case carefully Main glass When replacing the glass Remove two setscrews as shown and remove the front glass by sliding it upward Then remove the main glass by sliding it toward you Glass case setscrews Front glass 2 pieces Installing the Glass Case After you have cleaned the glass case and replaced the heater install them on the moisture analyzer 35 Replacing Heater page 102 Open the heater cover Install the glass case on the moisture analyzer Fa
82. per 30 seconds is reached The temperature is rising to the third step level The set third step temperature is reached The drying process continues until the time or AM moisture change rate per 30 seconds set as the ending condition is reached V Continued on next page IN3IN3SHDSVMW JHOod3g AYNSVAWN GaalviaG Q O Z Z m O d O 2 O JONVN3LLNIVIA ACIND 9NILOOHS3 18008 29 7 BEFORE MEASUREMENT V Names and Functions of Parts No DISP M Description e C Li Ji h Indicates the time elapsed after the start of measurement Ol se oa Indicates Indicates the temperature inside the heater cover during measurement temperature inside the heater cover during measurement Indicates the measurement result display currently selected For further information on changing the display see Setting the Measurement Standard 35 page 63 of yw pmeomem WeBas PMID Moisture content Dry Base wo pmeewem DBa O o Mass Standby state coud ce a value by the balance is 1234 Main display Mem Mem The moisture analyzer is in the energy saving mode and ready for use 35 Ready status is page 50 The selected menu item is for setting the format to display the current measurement U Setting the Measurement Standard page 63 The selected menu item is for setting the method to output data to a printer or PC gt Setup and Use of the Communica
83. pplication such as the Notepad The PC operation sometimes becomes unstable When the processing speed of the PC is insufficient it may malfunction Set the interval of data transmission from the moisture analyzer longer When the moisture analyzer is sending data to the PC do not touch its keyboard and mouse 84 Control Moisture Analyzer from PC zie sit The moisture analyzer can be controlled from the PC The programming using command codes US page 89 is required for it B Setup and Use of the Communication Tool To control the moisture analyzer from the PC you need to setup and use the special communication tool For further information on the communication tool refer to the following Web site AYNSVAWN http www shimadzu com products balance index html 1 Start the menu MENU PROGAM The menu opens J m gt gt UO select CoM SET from the menu seme d b J J CoM5ET gt ENTER o UT 1 Select an output port PROGRAM N b J 507 11 othe gt enter WIN S IVdaHadltid OL NOILOANNOO Set a baud rate MI i Go Pa Option Description B1200 1200baud B2400 2400baud B4800 4800baud B9600 9600baud B19 2k 19200baud B38 4k 38400baud JONVN3LLNIVIA What is the baud rate Baud rate is a communication speed to transfer the measurement result from the moisture analyzer to a serially connected printer More information can
84. reases Shifts the active digit that is flashing to the left by one Four digits for a sample code Shifts the active digit that is flashing to the right by one Upon date entry Upon time entry The value increases The value decreases Shifts the active digit that is flashing to the left by one Specify each of the year month and date in two digits Shifts the active digit that is flashing to the right by one INAWSenNsvaAWN JHOod3g AYNSVAWN GaalviaG Q O Z Z m O d O 2 O AONVNALNIVA ACIND 9NILOOHS3 18008 43 Measuring Moisture Content You can call preset measuring conditions for measurement with the moisture analyzer When you use the moisture analyzer for the first time set measuring conditions For further information on how to turn the power on see Turning the Power On IR Page 38 For details on setting the measuring conditions see Setting Measuring Conditions IRF Page 52 The following explains how to start measurement after the standby state 1 Confirm the standby state PROGRAM gt Confirm that the device is in the standby state measurement display as shown in the figure at right Press ESC to set it to the standby state when the menu items and measurement results are displayed on the display panel 2 Open the heater cover Hold the handle of the heater cover shown in figure at right and carefully open the lid to th
85. ronment where the moisture analyzer is installed and adjust the level of the moisture e p analyzer Flashing during menu display indicates that the setting corresponding to the menu item is valid gt Measuring Moisture Content page 44 When shown The measurement is completed Press Esc to return to the standby state measurement display When hidden Currently in the standby state or measurement process or settings are being changed Displays the setup mode and measurement state of measuring conditions The current measurement state is available from flash of the bar encircled by the dotted line The setup mode and measurement state of measuring conditions AUTO Standard drying automatic ending mode 35 Setting Temperature and the Amount of Change in Moisture Content AM as The measurement is started The temperature is rising 28 Measurement Conditions AUTO Standard drying automatic ending mode page 53 quo Ga ae l AUTO TIME Standard drying timed ending mode 35 Setting Temperature and Time as Measuring Conditions TIME Standard drying timed ending mode page 55 l S _ jj n The measuring temperature has reached the preset level The drying process continues until AM moisture change rate per 30 seconds set as the ending condition is reached The measurement is started The temperature is rising The measuring temperature has reached the preset level
86. se the moisture analyzer safely and properly carefully read and observe the following safety guidelines The levels of danger and damage that will arise if the moisture analyzer is used incorrectly are classified and indicated as shown below Indicates a potentially hazardous PAN CAUTION situation which if not avoided Indicates a potentially hazardous PAN WARNING situation which if not avoided may result in minor to moderate injury or equipment damage could result in serious injury or possibly death Precautions are classified and explained by using one of the symbols below depending on the nature of the precaution Indicates an action that must be Indicates an action that must performed NOT be performed S Never disassemble remodel or repair this Do not use the moisture product and accessories analyzer outdoors or in a Prohibitions Prohibitions location where it can be Doing so may result in an electric shock or lead to splashed with water abnormal operation If you believe the moisture analyzer may be malfunctioning contact an authorized Shimadzu representative Doing so may result in an electric shock or lead to abnormal operation Use the moisture analyzer with the specified power source and in the specified voltage environment een Using the moisture analyzer with an inappropriate power source or voltage level may result in fire or malfunction Also note that the optimal performance may not be ac
87. shown 5 Measurement date time measurement conditions weight before and after drying sample codes measurement results etc V Continued on next page 113 jueujeJunseeyy eJojeg eJnsee u 0 uonoeuuoo jueujeJnsee A pejreyeq uoneuloju Jeuo pue epinc BunoousejqnoJ 6 TROUBLESHOOTING GUIDE AND OTHER INFORMATION V When Required BM Accessories The part numbers and specifications given are subject to change without notice Standard Accessories and Consumables List Item Part number Description Front glass Size 34 5x149 mm Plate for Temprature calibration kit 32171521201 fo The attached power cable which is specified in the user s manual may be substituted for a cable that meets the regulation of each country Optional accessories list Part number Description Display protect cover five sheets 321 71512 10 EE UOI i Aluminum t 0 1 disposable pans Aluminum pan disposal 321 71571 10 One package G0 sheets For measuring liquid sample Fiberglass sheets 321 71731 One package 100 sheets Temperature calibration kit 321 71520 01 EE UOI Sample pan SUS 321 71572 10 Stainless steel t 0 3 5 sheets Sample pan 321 71572 11 Aluminum t 0 3 5 sheets RS 232C cable 321 61967 D sub9P lenghth 1 5m for DOS V USB cable set 321 71730 41 FERAE long attached CD ROM for USB 114 Menu Map The Menu Map illustrates the menu system in an easy to understand form You can
88. sories Prohibitions Prohibitions N CAUTION Do not use the moisture analyzer in the following locations Doing so may result in a malfunction e Where there is an air flow near an air conditioner air vent door window etc Where temperatures change markedly Where vibrations occur In an area exposed to direct sunlight Where corrosive or inflammable gases are present Where dust electromagnetic waves or magnetic fields are present Do not use the moisture analyzer as a proof of transaction Instructions The law does not allow the moisture analyzer to be used for proof of transaction such as medical preparation Handle the moisture analyzer carefully The moisture analyzer is a precision device Subjecting it to impact may result in a malfunction When moving the moisture analyzer main unit securely hold it with both your hands If long term storage 1s required use the original package box to pack the product Place the moisture analyzer on a rigid stable and flat Instructions table or on the floor Placing the moisture analyzer on an unstable surface may cause personal injury or a malfunction Secure a sufficient space for your measurement work in consideration of the total weight of measuring objects and the moisture analyzer loaded on the installation location m Only connect peripherals that have been specified by us to the connector of the Prohibitions moisture analyzer C
89. t otk oe Ose oe oe eee eee ee 115 jns P 118 MEMO Before Measurement Checking Package Contents Be sure to check that the package contains all of the following parts and that all parts are undamaged A number shown in indicates a quantity If you find that any of the parts are missing damaged or deformed contact an authorized Shimadzu sales representative EN Moisture Analyzer unit 1 Sample pan 3 _ Pan supporter 1 Windbreak 1 Heater insulation plate 1 2 Display protect cover 1 vi lt Instruction manual 1 NEN Menu map sheet 1 Hexagonal wrench SB2 5 1 N Names and Functions of Parts IN3IN3SDSVIN dJHOd3g The following explains the individual parts and components of the MOC63u moisture analyzer B Main Unit Front Observation window AYNSVAWN You can observe the condition of the sample object even when the heater is turned on and the heater cover is closed Heater cover A heater is included in the heater cover Close the heater cover before Set the pan supporter and measurement sample pan on this then place an object GaaiviaGd DIETO EVASIT Displays measurement results information for function settings functions currently running errors and other information IRS page 28 Temperature sensor Detects temperature
90. the menu PROGRAM MENU PPa 51 The menu opens 2 Select the ID setting ID from the menu DI gt enrer PROGRAM A He nn I pa n LK LIL pom HUUU A Enter the ID PROGRAM ID input gt Repeat for four digits gt enTeR 5E 7 PROGRAM Repeat the above procedure for four digits Press j to shift the digit 4 Return to the standby state PROGRAM Press ESC or to return to the standby state PROGRAM 72 Calibrating Moisture Analyzer w m TI AJ O m D m Span calibration can be performed to ensure accurate measurements by the moisture analyzer Periodical calibration is recommended to ensure more accurate measurement results The following two types of calibrations are provided for the moisture analyzer e Span calibration e Calibrating the temperature Option E D T m Mi Span Calibration For accurate measurement of the moisture analyzer span calibration by using a weight The calibration result can be recorded if a printer is connected in advance 35 Printer Output Option page 91 For further information on the span calibration procedure in The Span Calibration after Installing the Moisture Analyzer IRF page 40 IN3IN3SHDSVAIN qaiivrad W Calibrating the Temperature Option To calibrate the temperature of the MOC63u moisture analyzer the optional Temperature Calibration Kit is required For further information o
91. tion Tool page 85 35 Enable the Windows Direct Function page 79 The selected menu item is for setting sample codes to be output as a measurement result gt Setting Sample Codes page 67 The selected menu item is for setting the date and time to be output as a measurement result 35 Setting the Date and Time page 68 The selected menu item is for calibrating the moisture analyzer gt Calibrating Moisture Analyzer page 73 The selected menu item is for setting the output of measurement results and the timing of the output 35 Printer Output Option page 91 30 Description Indicates the moisture analyzer status When shown The heater cover is open When flashing You must close the heater cover currently open When hidden The heater cover is closed Middle When shown The heater cover is closed When hidden The heater cover is open When flashing The heater is running and the measurement is in process When hidden The heater is not running When shown A sample is placed on the sample pan vam J When flashing A sample is not placed on s the sample pan Place a sample on the sample pan When hidden A sample is not placed on the sample pan When shown A sample is placed on the sample pan When flashing Cancel the tare of the sample pan When hidden A sample pan is not placed When turned on The pan supporter is installed Blinking The pan supporter is not
92. tting the date an After Sales Service If this product does not operate normally follow the guidelines in Troubleshooting Guide IR P 110 to analyze and manage the problem If the problem still persists or a symptom occurs presumably caused by another failure contact our service representative details on back cover Supply of Parts Repair parts for this product shall be kept for a period of seven years after this product is discontinued Please note that after the above mentioned period a requested spare part may not be able to be supplied As exceptions non genuine repair parts shall be supplied during the period determined by the relevant manufacturer Ct Died el At dann uanu uat nnumu nm nma n n w u rumu er ee uumuumans Declaration of Conformity Manufacturer s Name SHIMADZU CORPORATION LEE Analytical amp Measuring Instruments Division Address _ 4 Nishinokyo Kuwabara cho Nakagyo ku Kyoto 604 8511 Japan declares in sole responsibility that the following product Product Name Electronic Moisture Balance Model Name _MOC63u MOC63 P N Depend on configuration See Appendix 1 referred to in this declaration conforms with following directives and standards EMC Directive 2004 108 EC EN 61326 1 2006 Low Voltage Directive 2006 95 EC EN 61010 1 2001 EN 61010 2 010 2003 The last two didit of the year in which CE marking was affixed for Low v Voltage Directive
93. u opens Select the RESET option from the menu RESET gt enter PSF ok 7 Start the initialization ENTER gt LENT gt RESET The setting memory inside the moisture analyzer will be initialized The calibration weight setting values for span calibration cannot be initialized by the menu rest process Return to the standby state Press esc to return to the standby state measurement display where measurement can be performed PROGRAM LU SOURIS N a a lt gt BURNS E cm pep p MM SS PROGRAM PROGRAM Because the moisture analyzer may have an error due to its application and operating conditions the customer needs to routinely and periodically check if the moisture analyzer maintains the required performance and functions normally The customer should determine the actual inspection including the inspection method and criteria as the control criteria depend on the purpose of application and management of the moisture analyzer If the requirement level of inspection 1s low some problems may not be found However if this level is too high the application efficiency may drop You should determine the well balanced inspection level by considering the risk of overlooking detection of a problem and the required measurement performance The following provides a guideline for carrying out routine and periodic inspections Use this guideline as a reference whe
94. urns to the upper level of the menu tree y Shifts the digit to the left when the date and time password sample code or ID is entered Selects the menu item The setting value increases when the code date and time temperature or password is entered Selects the menu item Decreases the setting value when the code date and time temperature or password is entered Q O Z Z m O m o zi AONVNALNIVA Returns to the menu during setting Press this key again to return to the standby state measurement display Returns to the standby state measurement display when the measurement ends Releases the error when an error occurs Stops the measurement Use this function when Manual mode is selected for the method to start measurement ACIND 9NILOOHS3 18008 V Continued on next page 27 7 BEFORE MEASUREMENT V Names and Functions of Parts B6 Display Panel 0 Q 9 o DICTEN Description Indicates the program No 0 to 9 currently selected For further information on how to select the program No see steps 1 to 3 of PROG RAM UJ Li Selecting the Measurement Condition Program No ES page 52 When shown Communicates with other equipment printer PC etc via N RS 232C DATA T O or USB When hidden No equipment is communicating using RS 232C DATA I O or USB When shown The measured value is stable When hidden or flashing The measured value is not stable Re examine the envi
95. wing the format to output the date Use two digits to enter the year e YYMMDD Year Month Day e MMDDY Y Month Day Year e DDMMY Y Day Month Year 1 Start the menu PROGRAM MENU PPa GR The menu opens 2 Select the date setting DATE ROO from the menu LIATE gt even Cry Select the date format sagen a b 1 b ENTER Date PROGRAM Select one of the following Display Date format Year Month Day PROGRAM Month Day Year 29MM Y Day Month Year 4 Enter the year month and day PROGRAM l ENTER J Year month and day input gt igo Move to the next entry item gt Time Enter the date in the format selected in step 3 Press ENTER to save the settings and move to the next item Press to move to the next item 68 4 Enter the hour and minute ENTER Hour and minute input gt y J y zie siti Press ENTER to save the settings and move to the next item Press to move to the next item PROGRAM E When the time does not need to be changed press esc to return to the standby state measurement display b Return to the standby state PROGRAM l gt Press ESC or to return to the standby state AYNSVAWN Restricting the Menu Displa Restrict the menu display so that the moisture analyzer settings cannot be changed without authorization To cancel the restriction take the same procedure The follow

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