LC-P-2313 - Gazanaliz.ru
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1. Number LCP 2313 ay gt lt Approved By John Mills AP Gary Burce Seamus Flanagan VARIAN Charlene McKenney Product Information Bulletin INTERNAL VARIAN USE ONLY Worldwide LC Distribution Introducing ProStar 325 Dual Wavelength UV Vis Detector Dell Axim X5 Summary Note Galaxie has not yet been fully tested with the ProStar 325 and therefore requires special ordering considerations that are detailed in the Ordering Information section of this PIB We anticipate Galaxie s full functionality with the ProStar 325 very soon The driver will provide full module control and digital data collection 1 The ProStar 325 UV Vis Detector is a completely new product designed and built by Varian Inc Melbourne 2 The ProStar 325 has both single and dual optional wavelength as well as extended absorbance range linear up to 70 AU capabilities 3 The ProStar 325 can monitor two wavelengths simultaneously either in the ultraviolet range with a deuterium lamp or in the visible range with a quartz halogen lamp 4 The ProStar 325 has significantly improved signal to noise for all applications compared to the ProStar 310 320 340 and 345 5 The ProStar 325 has signal to noise specifications equivalent to the best UV Vis detectors on the market today and is the clear S N leader in dual wavelength mode 6 The functions of the ProStar 325 are controlled by Star WorkStation or Galaxie CDS WS through Ethernet communi2. 30 Recorder Integrator Contact Cable 210187500 325 Relay Interface Board Provides Peak Sense 4 relays One cable 01 107441 00 100 needed per desired function 325 Analog Signal Cable Provides dual channel data Needed for fraction collection collection external integrator etc Needed when Star WorkStation or Galaxie is not being used Handheld computer with Allows stand alone control of cradle 325 detector Cradle holds handheld in an upright position and provides an additional battery charging slot Communication Accessories Ethernet 8 port 10 100BaseT Autosensing 100 240 VAC Switch power supply Ethernet Cat 5 patch cable For 10 100BaseT Ethernet 10 foot connection Ethernet Cat 5 patch cable For 10 100BaseT Ethernet 20 foot connection Notes About Ordering UV versus Vis The ProStar 325 can handle wavelength settings from 190 nm to 900 nm However the customer will get optimum performance with the greatest S N ratios using the D2 light source in the range from 190 nm up to 350 nm If the customer will be using the detector in the range from 350 nm up to 900 nm we recommend that they utilize the quartz halogen light source Which flow cell to order For dedicated microbore or analytical HPLC applications it is recommended that the semi micro P N 210182100 or analytical flow cell P N 210181800 be ordered Operating at flow rates best suited for these applications with the flow cells previously recommended enabl
3. 70 AU with preparative flow cell Response time selectable 0 05 0 5 1 and 2 sec Data rate 20 Hz single channel Analog outputs two with selectable absorbance range of 0 001 to 100 AU full scale at 1V Flow Cells Pathlengths single and dual interchangeable Single pathlength flow cells Semi Micro 4 mm 1 5 uL analytical 9 mm 15 UL Dual pathlength flow cells preparative 9 mm x 1 mm Super Preparative 4 mm x 0 15 mm Maximum flow rate a Semi Micro flow cell 20 mL min Q Analytical flow cell 100 mL min QO Preparative flow cell 500 mL min O Super Preparative flow cell 10 L min Pressure 1000 psi maximum Control External Ethernet IR with handheld Contact closure outputs four time programmable external event relays one peak sense relay three synchronization signals ready out start out and fault out Contact closure inputs lamp off autozero three synchronization signals ready in start in and fault in Software Star Workstation Galaxie Workstation Galaxie Chromatography Data System handheld computer Dual channel ratio calculation peak detection through Star or Galaxie software Environment e Operation 10 C to 35 C relative humidity from 5 to 95 e Non operational storage 20 C to 65 C Dimensions and Weight e Size 8 3 in 21 1 cm h x 11 7 in 29 6 cm w x 18 7 in 47 7 cm d e Weight 34 2 lb 15 5 kg Introductory CD Contents ple S Yni
4. Documents _ _ O o Operators manual o Service manual oo S Introductory PIB o o Data Sheet oo Competitive comparison do ooo Technical Details Paper describing the technical details of the product Suitable for American Lab Service Strategy Software S Star Driver o Handheld computer software C Software video director Place to keep all of the videos about software operation Diagnostics Pictures o O
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6. cations 7 In place of an onboard keypad detection parameters for the ProStar 325 can be programmed through a handheld PC using infrared technology 8 Data from the ProStar 325 can be collected via one of the 3 ways below e through an Ethernet communication cable directly to the PC e through an analog cable to the Star 800 MIB e through an analog cable to the internal pump CIM 9 The ProStar 325 can be upgraded from a single wavelength detector to dual wavelength 10 The 325 can be upgraded from the ultraviolet range to include the visible range with the addition of a field upgradeable visible lamp option 11 Dual wavelength detection coupled with peak ratio calculations in Star WS Galaxie CDS WS provide peak purity sensing capabilities ProStar 325 Introductory CD and its contents A summary of what is included on the CD is at the end of this PIB Product Overview See Technical Paper Performance Specifications See ProStar 325 Specifications at the end of this PIB or in the ProStar 325 Dual Wavelength UV Vis Detector data sheet Competition See The Competition at the end of this document Product Positioning Best dual wavelength detector on the market Lowest dual wavelength noise Wavelength ratioing with sophisticated peak detection Operates across the entire wavelength range 190 to 900 nm Easy upgrade from single to dual wavelength Buy dual wavelength now and save 2000 Outstanding analytical detector Low noise fo
7. es the 325 to meet its given noise specifications Using the preparative or Super preparative flow cells will cause the detector to not meet Its noise specifications Communications cable ordering lt is recommended to order an Ethernet hub listed above when ordering the 325 This is due to the fact that the customer may want their workstation computer to be connected to the company s network while at the same time being connected to the 325 detector This will save the customer from having to install an additional Ethernet card in their computer An Ethernet crossover cable is included with the 325 that allows direct connection to the workstation PC however an Ethernet patch cable listed above will need to be ordered to connect the 325 to the Ethernet hub The Ethernet patch cable can also be purchased from a local computer supply store Helpful Hints To get the best sensitivity you will need to add the visible lamp if you are going to be working above 350 nm Ifthe 325 will be used as a preparative detector it works exactly the same way that the 320 operates so an analog cable should be ordered and connect one output to the fraction collector and one to the CIM on the pump This will display a chromatogram in the Dynamax window The handheld computer will only work between 1 and 2 feet away from the 325 and will always disconnect if it is not pointed at the unit Ifthe ProStar 325 is connected directly to the PC it will alway
8. g or is not going to be operated using either Star Workstation nor Galaxie CDS WS the optional handheld computer will need to be ordered Galaxie Orders Until the Galaxie driver for the ProStar 325 is fully tested when quoting the ProStar 325 with Galaxie it should be quoted as follows 325 Connected to ProStar 210 218 QTY needed 7891084900 Handheld computer with cradle 558 210186500 325 Sync Interface Board 100 110744100 Shielded Recorder Integrator Contact Cable 325 Connected to ProStar 220 230 240 QTY needed 7891084900 Handheld computer with cradle 558 210186500 325 Sync Interface Board 100 110744100 Shielded Recorder Integrator Contact Cable 110744200 325 Analog Signal Cable 393614291 O Control Board for ProStar 230 310 190 O 1 390793701 Star 800 MIB w 2 ADC channels 1 450 390793802 Analog Cable tinned ends 3 meter 1 single wavelength or 2 dual wavelength Barrier strip from a local electronics store A The cases above allow the 325 to be operated as a stand alone detector with data acquisition through analog outputs The ProStar 325 operates in Star WorkStation much like the ProStar 310 ProStar 325 UV Vis Detector ProStar 325 UV Single Wavelength Includes Diagnostic software handheld pc driver 5 500 Detector software manuals LC Verify NOTE Flow cell not included one must be ordered below ProStar 325 UV Vis Single Includes Diagnostic software handheld pc driver Wavelengt
9. gh performance electronics and optics for lowest noise Best sensitivity easy to measure trace amounts Full dual beam design to minimize drift Best sensitivity little baseline wander Thermostat controlled Internal flow cell Low band spreading for sharpest peaks and best sensitivity Customer Need Productivit po Feature Benefit Fully controlled from Star or Galaxie Can take advantage of all automation features No changes needed for single or dual wavelength Can run single or dual channel wavelength methods within the same sequence 9x1 flow cell can be used for analytical and prep Can run both analytical and prep runs in automation Customer Need Reliability Po Feature Benefit Downloadable firmware Easy to update firmware if needed Modern reliable design including surface mounted single Highest reliability of parts and manufacturing techniques board system Customer Need Flexibilit Po Feature Benefit Analytical and prep flow cells for the same detector One detector for both types of applications Low back pressure flow cells High flow rate range for prep applications Use of handheld computer for status and method Can use all of the Personal Digital Assistant software on download handheld computer Complete set of synchronization signals and analog Can work with anyone s HPLC system outputs CO ed Customer Need Ease of Use Ease of Learning Change flow cells and lamps through the front panel No need to mo
10. h Detector software manuals LC Verify NOTE Flow cell not included one must be ordered below ProStar 325 UV Dual Wavelength Includes Diagnostic software handheld pc driver 6 500 This is an Detector software manuals LC Verify NOTE Flow cell not introductory price included one must be ordered below that will last at least until January 1 2004 ProStar 325 UV Vis Dual Includes Diagnostic software handheld pc driver 7 100 Wavelength Detector software manuals LC Verify NOTE Flow cell not Introductory Price included one must be ordered below ProStar 325 UV Vis Detector Parts Options and Accessories 210182100 Flow Cell Semi micro 4x0 mm 1 5 uL 20 mL min max flow rate 1 000 Flow Cell Analytical 9x0 mm 15 uL 100 mL min max flow rate 1 000 210181900 Flow Cell Preparative 9x1 mm 500 mL min max flow rate 1 500 10182000 Flow Cell Super Preparative 4x0 15 mm 10 L min max flow rate 1 500 110723100 Dual Wavelength Option Field Upgrade _ Field Installed 3 000 10720100 D2 Lamp Prealigned For wavelengths from 190 nm 450 nm 625 110743900 Visible Lamp Option Field Upgrade Must be installed by a Varian Service 1 200 Representative 325 Sync Interface Board Needed when Star WorkStation One cable P N 100 or Galaxie is not being used 110744100 needed per Provides Auto Zero Lamp Off desired function Start In Start Out Ready In Ready Out Fault In Fault Out 110744100 Shielded tinned end 3 wire
11. r high sensitivity Low band spreading flow cells Outstanding preparative detector Dual path flow cells for extended range operation High flow rate operation up to 10 L min Choice of flow cells for preparative operation 2 programmable analog outputs for operation with fraction collectors or other devices Single detector for both analytical and preparative applications Only need to switch flow cells Easiest detector to operate Change flow cells or replace lamps from the front of the detector without tools Full control from Star or Galaxie software Full set of synchronization signals to work with any manufacturers system Manual control and status through a handheld computer Personal Digital Assistant Use general purpose PDA to monitor status of detectors in the lab Use general purpose PDA with all other applications Use one PDA with all ProStar detectors in the lab No need to attach PDA to detector uses IR communication Handheld Computer 1 The handheld computer provides method building instrument control and the ability to monitor the chromatogram in real time 2 The handheld computer does not provide data handling capabilities like that of Star WS or Galaxie CDS WS 3 With the 325 detector being operated in the stand alone mode stored methods in the handheld computer can be run 1 at a time or a Sequence can run 1 method multiple times Needs Features and Benefits Customer Need Performance Oo AAA WWW Benefit Hi
12. s start when the rest of the modules start If the ProStar 325 is connected to a hub or network network traffic might slow down the start command from being transferred from the PC to the 325 The result will be a variability in retention times for different chromatograms although all of the peaks should be offset by the same amount The areas heights and peak shapes will not be effected If this is routinely happening the sync board may need to be added and a contact closure cable from the pump or AutoSampler connected to the start input of the ProStar 325 Nothing further needs to be done in this configuration Hgg SA0CE SA0CE cere DEL Oh Aug eng MO 002206 MUTI WUE ied Oh Sb WU 5 WU PSE IT SOLS EHH SOA SB OWES SB OWES hya PERLE AIO ajui SIA AZO 002 064 aL MAA Ae SOLS ZUNE bro LEE awansean UJUI A eng S0994 do MY HiNT BUIUUEIS SJA Aza 006 06 WU pot WUE j wag Pi gOS E i 4 SOLS cite SIU SS14 yaang WSUS ABA saa afue Fy eng SJA Ned 008 06 ve oja WG PUB pse MA MEST WUpEZ Jae f Obs i E HTT JA ve OF WU PUB PoC IE SOL Lt pipz 3 y HiNT WA G SE 83 Ap 9 0 KO p POL ees on or a 2S Lm Pond 05E 06l 009 06H WUSe y WUE i za TTL Tp Eng 00t 06H MUO MUL i a8 Z auy poz Eny pajp AEE apop uo paseg WU f asuodsay oo XO f Hoh UU j Ws Ja z aul i hh SJA 29 009 06 WU p oa g asuodaay 90g 2 Tpl Magumu BLES aunan paueya aupa duel ajep
13. ve instruments to change lamps or flow cells Full control through Ethernet Simple interconnection with no distance limit already built into most computers Drivers for Star or Galaxie If you Know Varian software there is no learning curve Customer Need Miscellaneous Po Feature Built by the same people who build Cary Best optical designers on the market spectrophotometers ee 1 Extended absorbance range saves analysis time by cutting down on the need to dilute concentrated samples 2 Peak ratio capabilities in the Star WS Galaxie CDS WS software gives a way to more accurately determine peak purity 3 Front accessible flow cell cartridges allow quick and easy cell changes 4 Semi micro to super preparative flow cells for analytical to preparative detection in one detector saves the customer money 5 Front accessible lamp compartments enable fast lamp replacements to be performed by the user 6 Many software packages available for the handheld computer expand its capabilities to double as a personal digital assistant Ordering Information When placing an order for the ProStar 325 please be aware that the unit does not come with a flow cell The appropriate flow cell must be ordered separately Flow cells come in a variety of configurations covering semi micro to preparative flow rates so make certain to order the correct one for the customer s application Also if the 325 is going to be operated in a stand alone settin
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