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底 質 調 査 方 法

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131. 0000
132. LAS 3 Cell 1 4
133. 1110 114 103 1 20 1 5kW 15L m
134. 50u g mL 10mL 4
135. 11 6 12 0 0005 L mL 2 0mL 6 KD 79
136. 4 00000 5 9 1 4 8 5 a 0000 ICP 193 696nm 1
137. 45 3 000000000000 4 5 3 1 000000 1 0000000 2mol L 1L 5mL op 10 C 0
138. 50 C 1min 10 C min 280 5 250 C 60sec 1u L 40cm 10096 0
139. a a di 1 3 ds DP P ds ds 1 2 d5 Gs DPCB ds trans 1 2 ds
140. 0 2mm 25m 0 25p 596 150 C 1min 10 C min 300 Q 10min 260 C 1 2u L He 15psi 260 C
141. e 000 00 11 f 200mL 500mL 9 000000 100 20mL 0000 7
142. 0 Lu 9 6 11 0 5 10mL 100mL 14 M 1000 g mL 0 20 Gi 10mL 100mL 1 1000 g mL c 2 0 2 1 11 1
143. 5mL 2 3 Fr 1 4vol 100mL F 2 15vol 150mL Fr 3 5mL Fr 1 5 10g 1 109 10mm 300mm KD mL 1000 1 000ng 1mL
144. all b 9 lu g kg D 10 11 32 4 13 5 0000 a GC MS GC GC MS GC o 00000000000000 66 559 8 0
145. o 0000 4 00000 5 1 1 4 a 5 1 1 4 b 5 1 1 4 5 a 1 1 0 100 120 30 40 600 1 000 300 40 2 200 2 700 30 6 324 8n
146. 4 00000 a 0000000 50 10 g 0 0 01g 500mL 250mL 9 5g L 100g L 1mL 2 200mL 20g L 20mL 10mL EDTA 20mL 8 2 3m L min 49 5 150mL 2 1006 10
147. 0000 6 ICP MI P b o 0000 4 00000 5 1 1 4 a 5 1 1 4 b 5 8 ICP 2080 2060 207 187 1 20 1 5kW 15L min LOL min LOL min 3 b 000 Lu gPb mL
148. 9 0000 000000 e 0000 e 00000000000 e 50 500 L b 00 o 0000 4 00000 5 9 1 4 a 5 1 1 4 b 5 a 0000 100 120 30 40 8000 1 300 300
149. 16 16 17 ds 1 0 g mL 0 005 g mL A 0 0005u g mL B A 3 MS 3 a 000000000 b 0000000 o 000000 d e 00000 f 10cm 3
150. 1 600 2 200 1 3 6 357 9nm b 23 20mL 0 1u gCr mL 0 10 Amt E 100 50u L 1 1 000 g mL 24 357 9nm 25 5 12 1 1 4 b 19 o 5 12 1 1 4 b 29 o pao 2
151. o 0000000000 GCU 0 2 0 7mm 150 30m 0 1 1 0u m 99 999 0159 20 40cm sec 35 230 0 500 35 230 0 500 150 280 C 2000 270 500 100 40 50 100 C min 2500 280 000000 450 70V 4 00000 a
152. 10x 300mm 5g lmL 50mL 8 1vol 100mL 9 1mL 30 10mL 1 1 10 11 12 GC MS 5 6 7 68 8 C 81 6 C 5 8 1 9 DEHA 10 DEHA 0 25mL 11 10x 300mm 5g
153. 5 a 25mmol L b a C 4 1 96 1g mgN g 200 1 N mgN 9 a 25mmol L mL b 25mmol L mL 25mmol L V mL W 9 0 700 25mmol L 1mL mg 00 2 25mmol L 10mmol L 4 4 1 90 19 0 N b xf
154. 40 500 100 C min 250 280 2000 25020 2 3 GC GC 4 6 4 1 4 5 00 8 GC GC 5 10059 0 25 mm 30m 0 25 m 60 C 1min 10 C mi n 140 C2 1 C min 2105 1 C min 260 C 1min 250 C
155. 5 a GC MST I I GC MS GC MS 00000000 0 2mm 25m 0 52u 5 60 C 1min 20 Q min 280 C 10min 15 260 C 1 5 2u L He 15psi 00000 El 70 250 C SIM e 00000 6 11 1 611 1 00000 17a 227 300 17p
156. 4 00000 a 4 5 1 1 4 a d 9 b 4 5 1 1 200mL 50mL 10 4 5 3 1 4 200mL 200mL d 30mL 4 5 1 1 4 b d 4 5 1 2 4 b 9 0 032mg 10 25bmmol L 50mL 5 8 630nm b 0 0
157. o 00000 1 279 5nm 5 1 1 4 a 5 1 1 4 b j 1 d mgM n kg 6 5 1 1 6 a l 5 1 2 6 8 562 1 0000000 2 00 a 5 K 0557 A3 b 000 0000000 50
158. 4 00000 5 11 1 4 a 5 a ICP 206 833nm 2 1 5kW 16L min 0 5L min 1 0L min b 000 0 1 gSb mL O 5 5mL 50mL 1mol L oor e 5mL 50mL 1mol L oer 00000 3 100mL 8mL 1mol L 8mL 50 50 Q 50mL 8 ICP 10g L
159. 5 a 0000 100 120 30 40 8000 1 300 300 40 1 900 2 400 1 30 6 217 6nm b 2 10 20mL 0 1u g mL 0 10 Amt 100 50 L 1 1 000 g mL 1 000 g mL G 32 217 6 1 0 0
160. 12 PR 60 100 130 15 FL LC Florisil 5 10g lcm 30cm 7g 2cm 1 13 5vol96 14 GC MS 5g 5 a GC MS GC MS GC MS o GC 559 0 2 0 75mm 15 30m 0 10 3 0 16 50 C 1min 20
161. 100mL b 4 al 5mL 5mL 5mL 2 30mL 10 4 a 1 3 2 3 3 19 2 5mL 5 8 880nm 710nm b 5u g mL 1 8 mL 50mL 5 e o 5 40 9 50mL 40mL 200g L
162. II 6 7 4 3 a b 00000 KD o 0000 d 00000000000000 o 0000000000 GCU 0 2 0 7mm 150 30m 0 1 1 0u m 99 999vol 20 40cm sec 35 230 0 5 C 350 230 Q 5 C 1500 280 C 2000 270 500 100 40 50 10
163. 100mL 10 500mL 100mL 10 8 309 5mL e 50mL 1mL 6 eoe b 0000 e 10mL 250mL 559 50 10mL a 10mL 10 e 3mL 20vol96 10mL 6 5mL 1mL eoe 4 2 6 a 10mL DT 10mL 1mL 2 10mL b 20vol96 10mL 2mL C Envi Carb 3mL 0 25g 10 d
164. 10mL 10u g mL 100 0 1 g mL v 00000 03 0 01g 100mL 100p g mL 100p g mL 1mL 10mL 10u g mL 1mL 10mL Lu g mL 3 1 2 JRSAX QMA MCI GEL 1 3 JR SCXD TOYOPAK SP 11 4 Sep Pak Florisil FL 1 5 99 6 100 g mL
165. PCB Congener IUPAC No 4 Chloro 3C 2 bi phenyl 3 4 4 Dichloro 3C 2 bi phenyl 15 2 4 5 Trichloro 33C 2 bi phenyl 31 2 2 5 5 Tetrachloro 3C 2 bi phenyl 52 2 3 4 4 5 Pentachloro 3C 2 bi phenyl 118 2 2 4 4 5 5 Hexachloro 3C 2 bi phenyl 153 2 2 3 4 4
166. 140 1454 5 C 4 d 30 5mL min 220mL e pH pH 5 00 6 0 409 5 f 250mL 3 4 5 a 620 nm b 2u g F mL 2 25mL F 40 50u g 2 o 00000 30mL F7 41 50u g 50mL Gi 5mL 10mL 1 20mL 1 8 30mL
167. 34 1 000000 a b 00000000 1 1 109 10mm 2 ji 10mm 20 C b 2mm 3 1 U 3100000000 0 10 n B DDD 1 1 0098 000 11 1 1 1 1 lJ U U J 2 mm
168. mgN g 200 1 N 0 a xf KO 00 XN N o b 25bmmol L 50mL 50 mmol L mL a 50mmol L mL 5O0mmol L V mL 9 0 7000 50mmol L 111 mg 6 2 b 25mmol L 7 50mmol L 30mL JIS K 8576 35g 4 5 2 5mL 1 000mL 5 K 8005 2kPa 48
169. 4 5 6 2 50 3mL min 7 1 5 a 4 10mmol L 25mL 1 1 2 8 10mmol L 1mL 9 c 4 a b 10 d 4 1 1g mg 5 9 1 S b a xf x0 1603 Sur 5 mg 5 9 a 10mmol L mL b 10mmol L mL 10mmol L 4 a 9 0 16030 10mmol L 1mL mg
170. 6 100 50 L 1 3 000 g mL 1 000 om 121 22 193 Znm 23 5 9 1 4 a Q 5 1 1 4 5 2 eo 2 000000000 6 1 1 1u gAs mL O 5 5mL 100mL 24 N 1 000 g mL 3 000 g mL 123 Cl AG 5mL 100mL 1 1 000 g mL 1 000 g mL 23 Cl AG 0 2 00000 3
171. 6 15mL 6 25 2 30 11 12 620nm OmL 50mL Glo 10 pH 13 10mL 148 0 5mL pH6 8 10m pH6 8 pH 50 8 31 20 30 12 1 d 4 1 96 19 mgCN kg
172. 171 6 00000000 a b 1 2 1 U a 000000000 1 DUDU D0000 109 00000 1000 2
173. d I 4 5 1 1 2 8 e 000000000 500 1 4 5 1 1 2 9 f 2009 1 209 100mL 00000000000000 200g L 55mL JIS K 8798 25g 115 K 8034 6mL 200mL 10 5 h logLI I 7 1296 8 10g L i I t 1mgN mL JIS K 8116 JISK 8228 16 3
174. 6 9 2 DEHA 30 G 100g 2L LU 30 1L 1L 130 C 130 5 a GC MS 33 GC MS GC MS 000000000 GC 559 0 25mm 30m 0 25 m 50 C 2min 10 C min 260 C 10min 250 C 60sec 1u L 40cm 00000 MS El 70V 2200 280 200 C SIM 14 00000 DEHA 129 147 mI DEHA 137 mi
175. 6 10 99 999 0159 200 40cm sec 35 230 0 500 35 230 0 500 150 280 C 200 270 C 50 1005 40 50 C 100 C min 2500 280 70V 4 00000 a 0000 10g 100mL 30mL 10 3 000rpm 10 100mL 20mL 596 200mL 50mL 50mL 50mL 5mL b 00000000000 1mol L KOH 0 5mL 3 0 2mL 4
176. 1 000000 GC MS 20 3 6 8 D0 11 2 00 a 00 b 2 o d alli 8 4 e 0000 2000 6 1 3 DPP s 1 2 c s DPCB I trans 1 2 trans DPCB 2 4 1 DPB f 3 6 2 4 6 1 4 1 PPET A
177. d e 00000000 FPD 8 W DB 5 DB 5ms Restek Rtx 50 HP HP 5ms Supleco SPB 50 SGE BPX 5 1 uu lU D 10g 0 1 g mL 100 9 2 1mol L 50vol 70mL 30 10 1mol L 50vol 30mL 10 100mL 60vol 50mL 5 9 60vol 30mL 150mL 20 1 1094 100mL pH 12 40 1mL 10mL 1mL min 20mL 15mL g 30mL
178. d O00000 mgM n kg 6 00000000 5 1 1 6 8 b 5 1 4 6 a 5 6 3 00000000 43 m z 2 ai 5 K 0557 3 o 0000000 3 gm 1mg mL 1mL 1 000mL 1 1 2 d 0000000 Ou g mL 1mg mL 1mL 1 000mL 1 1 2mL e 0000000 1u gMn mL 5 6 1 2 d 10u gM n mL 10mL 100mL 1 1 2mL f 000 Iu ln gPb 4 9
179. 6 63 0000000000000 1 2 1 1 1 2 1 1 1 1 1 2 1 3 1 2 1 2 p 1 GC MS 1 2 3 n 1 1 1 1 1 2 1 1 2 2 1 2 3 1 3 1 2 t 1 1 2 1 3 1 4 1 2 1 3 1 2 3 1 2 4 1 3 5 6 1 1 1 GC MS 2 3 4 2 GC MS 3 GC MS 4 SIM 2 8 5 5 88
180. 9 3 000rpm 15 0 d 0051 0 21 1g 5mL 5mL 5mL e 000000 100mL 200mL f 1010000000 200mL 500mL 000000 10 20mL i i 10 L p 0 50 19 3mL lg I 3mL 0 2 0 39 m 0 2
181. 10mL ii 0 5mL 4 5mL emL 10 10mL ii GP C 2000 Shodex 4 0mL min 16 18 16 9 PAE 2000 Shodex 5Ovol 96 4 0mL min 140 17 15 1 15 9 iv TLC HPLC b PFBB 0 5mL 3 80 30 6mL 2mL 6 e 5mL 7 6 lmL 10mL 8 5mL 9 50vol98 5mL 10mL 20u L 30 1 11 9 i 5mL 10 015 5mL 10mL 0 2mL 60mL 5mL
182. a 1 0 1 213 856 202 551 206 191nm 1 20 1 5kW l6L min 0 5L min 1 0L min b 10u gZn mL _ 2 OUT 20mL 100mL 20mL 100mL c 1 10u gCd 10u gPb 10u gCu 10u gzn 10u gFe 10u gMn 10u gNi 10u gMo 10u gCr mL 00000 3 2 100mL 0 10 0 5mol L ICP 3 4 5 5 1 1 4 a O 5 1 1 4 5 2 o 2 3 100mL 50u g mL 10mL 2 451 131nm 10u gZn mL O 1
183. u gAs 1 gCr mL D 5 1 1 2 j 0 1mgCd mL 5 2 1 2 d 0 1mgP b mL 5 3 3 2 0 1mgCu mL 5 4 3 2 0 1mgZn mL 5 5 1 2 C 0 1mgF e mL 5 6 1 2 9 0 1mgM n mL 5 7 1 2 9 0 1mgNi mL 5 8 1 2 f 0 1mgM o mL 5 9 1 2 i 0 1mgAs mL 5 12 1 1 2 i 0 1mgCr mL 10mL 1 000mL 12 1 20mL BDDDLDLIoongCdp 50ngPb 5OngCu 50ngZn 50ngFe 5OongMn 5OngNi 5OngM d 5OngAs 5OngCr mL 1u 9 1u gPb 1u gCu 1p gZn 1u gFelj 1u gMn
184. 45
185. 3mL 1 1 40mL 1 1 2mL 200g L 15mL 1 5mL 10 3 5mL 5g 25 6 5mL 10mm 510nm 200mL 5 9 1 4 a Q d mgAs k g s 0 002 0 01mg 10 10 2mL D00000 3 0000 40mL D
186. 10 KD 1moL L KOH 0 5mL 0 2mL mol L KOH 5mL 8mL 0 5u g mL 1 0mL 0 7mL GC MS Q 11 uU uuu 6 10 3 2 1 2 2 2u LO GC MS 20 GC MS 336 6 10 6 10 3
187. 5 a 0000 638 b 000 1u gCN 1 0 50 9mL 50mL 10mL 5 c 6 DU 4 25mL CN 0 50 9u g 50mL 2 5g L 1 148 pH 7 2 10mL 9 8 T 106 1 0 5 1 5 4 10mL 25 2 30 9 6 638nm 6 10 1 50mL pH 7 2 10mL GI e d 4 1 19 mgCN ko 8 pH 708 9 20 30
188. 3 GC GC 4 6 4 1 4 100 100ng 6 4 1 4 5 a GC MS GC MS 00000000 GC 5 100 0 20mm 25m 0 33 m 130 C 1min 20 C min 220 5 C min 300 C 280 C 600 90sec 00000 MS 10 000 1058 El 25 70eV 500 1000 280 300 25psi SIM 00000000000 64 10 00000000 168 9888 318 9792 230 9856 442 9729 64 11
189. 3 3 1 09 0 0039 550 2 1 20 30mL 142 2 20 5mL 5g 0 3g 900 C 20 3 200mL 5 4 5 142 6 100mL Go 1 2 3 50mL 200mL h 4 3 70 80 C 5 D 6 100mL 80mL 7 f 0 3 3 8 10 200mL 0 0019 10mL 9 10mL 5mL 5mL 10 Amt 169 5 32
190. 6 9 2 DEHA lu LO GC DEHA dio DEHA DEHA mL 1 g kg ng x aD We x 1000 wW 9 lu GC DEHA DEHA ds DEHA da DEHA DE HA de dio DEHA ds 70 1 30 13 GC 270 1 D 34 SIM 15 00 1 323 6 9 2 DEHA
191. 6 7 dis 5mL i 0 3mL 0 1mg mL 10 L 8 30mL s 6 7 1 GC MS din ds 10 de 20g 500mL 350mL 5 10mL 90 6 7 1 306 6 7 4
192. 16 10 0 10 0 5mL d 5 20 17 e 00000 18 i mL 1 g kg ng x iL Wig x1000 9 17 17a m z 300 17a m z 227 17p m z227 18 012 m z240 12 uu
193. 1 20 1 5kW 15L min 1 0L min 1 1L min b 000 2 5u gB mL 0 1 10mL 100mL 1u g mL 219 5mL 10mL 100mL 1u g mL 5mL 100mL 1u g mL 5mL 0 10 0 5mol L ICP 20 21 5 13 1 4 b 1 5 13 1 4 b 2 eo 19 1p g mL 1p g mL 9 20 m z 16 m z 2 m z 21 d 000000 mgB kg 195
194. p 17 94 176 00000000 2 4 16 16 d4
195. 4 00000 a 6 3 11 4 1a i 4 2 a b 20mL 1 18 3 50vol d 18 4mL 3 5 a 0000 GC MS GC MS VOCOL 0 32mm 60m 3 0 m 50 C 2min 10 min 200 C 2mL min 150 C 90sec 200 C E1 210 C 107 109 p dio 116 b 100 g mL 0 050 5 0u g mL 5 0012 9 00000 4 0 20 140 0 5 3 150 2 8 20mL 5mL e 1mL 10u g mL 20u L lu L GC MS Lat d 8 2 d 4 1 59 19 mg kg
196. 10 m z 16 m z 2 m z 11 m z d mgCu kg 6 5 1 1 6 a l 5 1 3 6 8 5 3 1 324 8nm 2 a 15 K 0557 b 000 0 1mgCu mL 5 3 1 2 9 d un gCu mL 5 3 3 2 6 3 000000 a 000000000000 0000 e 0000
197. 4 a 3 000 5 000rpm 20 3 000 b 00000 9 d 0 1987 pp127 1997 pp205 206 1996 pp28 39 1986 pp74 77 4 1 n
198. 4 00000 5 1 1 4 a 5 1 1 4 b 5 1 1 4 c 5 00 a ICP 327 3960 324 754 224 700nm 1 20 1 5kW 16L min 0 5L min 1 0L min b 000 10u gCu mL 0 1 20mL 2 100mL oo 20mL 2 10 gCd 10u gPb 10u gCu 10u gzn 10u 10u gMn 10u gNi 10u gMo 10u gCr mL o 00000 3 8 100mL 0 1 0 5mol L Q ICP 4 5 6 8 5 1 1 4 8 2 0 ef 5 1 1 4 5 2 0 5 1 1 4 o 3 4 100mL 50u g mL 10mL 2 451 131nm 10u gCu mL 0 10 20mL 100mL 50u g mL 10mL 2 451 131nm 5
199. 4 00000 5 1 1 4 a 5 1 1 4 b 5 8 ICP 570 54 103 1 20 1 5kW 15L min 1 0L min 1 0L min 3 b 000 10u gF e mL 890 5 50mL 100mL 1 g mL 5bmL 2 50mL 100mL 1u g mL 5mL 8 1 gCd 1u gPb gCu gzn lp gFe 1u gMn 1u gNi 1u gMo 1u gAs 1p gCr 1u gB mL 5OngCd 5OngPb 5OngCu 5OngZn 5OngFe j 50ngMn 50ngNi 50ngMo 50ngAs 5OngCr mL 1p g mL 1u g mL 5mL 00000 100mL 1u g mL 5mL 0 1 0 5mol L ICP m z 10 5 1 1 4 a e 5 1 1 4 5 2 o 9 m z 16 m z 2 m z
200. 5 a 0000 100 12001 30 40 6000 30 40 2 200 2 700 30 6 248 3nm b 3 20mL 1u gF e mL 0 31 Amt 3 10 50 12 248 3nm 13 5 1 1 4 a O 5 1 1 4 b 2 oe 2 000000000 1 000 1u gFe mL 0 5 10mL 100mL 14 0 20 10mL 100mL Cl AG 9 2 00000 3 100 50 L 12 248 3nm 13 8 5 1 1 4 8 2 5 1 1 4 5 2 oe 11 12 13 o 3 14 d mgF e kg 0000 mgF e kg
201. H H H H H H H H H H H Li d d d EE Ll H rs 5 5 L E m 5 LL 5 5 5 5 4 E LaL 4 3 E card 5 5 E 5 88 8 r1 o o EJ DI jem LH Ei Lr Hu Beau ma al ag CR COD mro Tag Diir 2000p Tag Eri 2o00 2Y pajang ja at o0 o o0 D o0 D o0 o 1 oo mm ri 3 E O ooa Ej E amHaadh
202. 2mol L 2 a 0 15 K 0557 3 b 000000 qQ2mol L 4 5 2 1 2 b 345 0 100mL IS K 8180 20mL d 0000000 0715 K 8116 100g 700mL JIS K 8085 50mL 1L e 00000000 10 f 1 39 195mL IS K 8541 5mL 00000000 700mL 80g L 70mL 115 K 8107 389 JISK 8983 N 12 5g 80g L pH 1L 4 0000000000000 000 1g L 0 4 5 3 1 2 c i 000 N 1 00000000000000 00 1g L 0 4 5 3 1 2 d p 00000000 0 1mgN mL JIS K 8548 105 110 C 100 0 7229 11 op 10 2u gmL 0 1mgN mL 20mL 1L 0 5 2mm 409 300mL 125
203. 4 00000 5 9 1 4 8 5 8 ICP 196 026nm 1 20 1 5kW 16L min 0 5L min 1 0L min b 0 1 gSe mL WO BT 5mL 50mL 1mol L c e 5mL 50mL 1mol L cen e 155
204. 217 6nm 5 11 1 4 a O 68 7 d 000000 mgSb kg 6 00000000 5 9 1 6 b a 00000 10 5gr 0 0190 200 50mL 20mL D uut 1 2 10 00050 B 20ml 0 0 111 8
205. GC 2 a 5 0557 3 b 000000000000000 3 1 56 11 1 000mL 5 8180 d 5 K 8509 e 0000 5 K 8138 f 5 K 8680 300mL 1mL 20 5u L 00000000 200g L 0 JIS K 8150 200g 11 2006 1 JIS K 8514 2009 11 i L 00000 000000000000JIS K 8470 Ez 190 J IS K 8371 0 89 115 K 8987 12 89 100mL j 0000000000 1004 gHg mL rn D DU 1008 gHo mL 13 2mg 12 5mg 100mL ki Ou ggm t Ou oioimt 100 gH g mL 100p gHg mL 1mL 100mL Il 00000 00000
206. t n 1 0 05 2 132 2 015 1 943 MDL MDL MDL 1 20 5 2050 s MDL 2 1 0 05 x s t n 1 0 05 n 1 596 t e nu 10 1 1 1 10 2 2 10 1 2 30 Ci C Cca H 100 5 30 e 00000000 10 1 1 1 10 2059 e 000000 10 60 10 d o 00000000000
207. 610 000000 6101 000000 4 4 n 4 n 4 4 4 n 2 4 1 0000000 GC MS 2 a D0000 100mL 1 11 lu L b 300mL 1mL lu L 300mL 1mL lu L d 00000000 700 C 8 e 00000000 700201 8 f gugag 5 5 9 60 100 130361 16 1 5 641 959 5mL 30 15 i 0000 60 80 j 000000 k 0 0 0 5 1107 1 99 999vol 94 I 200 1 4 1 1 1000 0 0 0 1mgmL l 4 t 0 100g 100mL 4 n 00000000000 0 moi ID 4 n 0 100g 100mL 8 4 moi ID 4 0 100g 326
208. 5 1 1 4 a 5 1 1 4 b 5 a 1 1 0 100 120 C 30 40 600 1 000 C 300 40 2 200 2 700 C 3 6 279 5nm b 0000000000 3 12 20mL 0 1u gMn mL 0 11 2mL 3 100 50 L 33 279 5nm 14 8 5 1 1 4 8 2 5 1 1 4 b O eoe c 000000000 o1 000 1u gMn mL 0 1 2mL 100mL 3 22 Gi 2mL 100mL Cl AG 0 2 00000 12 10 50 L 33 279 5nm 14 5 1 1 4 8 2 5 1 1 4 56 2 eoe 12 13 14 eoe 3 15 d 00000 mgMn kg 0000 123 5 6
209. 4 00000 a 6 11 4 ay d b 1 9 4mL 0 6mL 9 4 94mL 0 60 6mL 10mL lu L 2 1 30 2 90 9 4mL 0 6 10 100mL GC MS 5 a 6 5 GC MS GC MS o 000000000 GC 6 1 1 5 b 150 C e 00000 6 1 1 5 b b 1mg mL 0 021 10mL 10mL 7 9 4mL 0 6mL 10mL lu L cog GC MS 3 3 9 3 90 110 25 60 0 5 30 120 1 000 GC MS
210. LASO 111 1 111111 HEEN DIER 622 110 0000000900000000000 tal 0 0 62 00 6 2 1 00
211. r 1 000 mL 1u D mL O 1u g mL B 0 01p g ml C 17p 2 4 16 16 04 1 000 g mL 0 1 u O mL 1 PFBB KOH PFBB 2 10 2mL 1 9 a 346 b o 000000000 d e 000000 f 9 00000000 4 00000 8 1093 6 11 uuu 50mL
212. 43 000 1 0000000 4 1 300mL 4 3 2 b 50g 4 2 ai 5 K 0557 b K 8953 5g 500mL 115 K 8576 6g 300mL J S K 8960 70g 1L 100g L 0 JIS K 8356 129 100mL d 30 JIS K 8920 1 27g J S K 8913 5g 50mL 1L e O ImolL 1 1 11 0 0101 000 0 115 K 8637 269 JISK 8625 0 29 11 2 5 K 8005 130 C 2 0 72g 0 0039 200mL 20mL 300mL JISK 8913 2g 145 5mL 5 100mL 10g L 1mL mL 0 1mol L f b 20 k 1 100 200 x x0 003567 a 9 90 0 1mol L 1 0 003567 0 1mol L 1mL g f 10mmol L 0 1mol L 20mL 22
213. 2 a 5 K 0557 3 b 4 9 1 2 9 4 9 1 2 c d 49 1 2 4 e 2009 1 4 9 2 2 e f 1 7mmoad L 0 0000000 1 8mmol L JIS K 8622 0 1439 JIS K 8625 0 191g 1L 0 3mmot L U U 2 7mmol L gt K 8622 0 0259 JIS K 8625 0 286g 1L 00000000000 1 3mmoa L 0 0000000000 1 3mmo L 0 000 30mmo 0 0000000 0 100g L 0 p d Got In 0 314 J IS K 8866 0 5090 J IS K 8863 1 8690 JIS K 8032 100g 128mL JIS K 8295 5g 4AmL 11 I 0 HB 2 5mmol L 2 2
214. 8 209 3 000rpm 20 11 10mL 10 3 000rpm 10 10mL 10 3 000rpm 10 25 50mL 9 8mL 0 2mL 4 9 49mL 0 10 1mL 12 13 14 11 12 9096 9 8mL 0 2mL 50 50m GC MS 13 14 105 3 uu GAGASAN 4 0000000 150 C 2 220 3 0 220 C
215. II 6 7 4 di 240 b 0 10 5 g mL 0 3mL 0 1mg mL 10u L LU GC MS 18 o 00000 luL GC MS 18 d O00000 B mL 1 g kg ng x l x1000 9 35 GC 270 16 DB 10 HP 1 DB 5 HP 5 17 did 176 dio 1880 o du 244 HCB GCdT 290 18 1 310 6 7 4
216. 6 o 00000 3 200mL 200g L 10mL 111 pH9 9 5 Q 50g L 10mL 150mL 10mL 2 3 8 200mL 50mL 8 10mL 2 3 50mL 6 50mL 2 9 4mL 2mL 1mol L 5mL 25mL 10 7 0 1g 50mL 100mL 2 3 1 1 pH pH 8 9 30 10mL 5 a 0000 100 120 30 40 500 800 C 30 40 1 6000 2 200 30 6 228 8nm b 3 3 20mL 0 1u gCd mL OUT 2mL 10 50 N 1000 g mL 12 228 8nm 13 3 5 1 1 4 8 2 D 6 5 1 1 4 5 2 5 1 1 4 o 2
217. SampleName 10 09 10 0 9 1 00 5 0 mL 1 0 PCB Calculation Table PCB 1 0 mg L PCB 5 0 uL 5 0 uL MI K CBo Hi H2 CB CB CBo Hi 2 Cl2 1 0 084 1 67 20 0 3 0 0 25 0 97 Cls 2 0 231 5 78 25 0 0 0 0 00 3 0 122 2 68 22 0 0 0 0 00 4 0 085 7 57 89 0 9 0 0 77 5 0 122 5 23 43 0 2 0 0 24 3 91 Cl4 6 0 239 7 88 33 0 16 0 3 82 7 0 107 4 83 45 0 18 0 1 93 8 0 063 3 30 52 0 17 0 1 08 9 0 098 10 68 109 0 33 0 3 23 10 0 049 2 37 48 0 11 0 0 54 41 11 Cls 11 0 068 5 70 84 0 36 0 2 44 12 0 077 3 16 41 0 16 0 1 23 13 0 063 4 20 67 0 20 0 1 25 14 0 023 1 24 54 0 11 0 0 25 15 0 046 6 44 140 0 64 0 2 94 31 49 Cle 16 0 048 616 1290 50 0 2 39 17 0 029 1 68 57 0 10 0 0 29 18 0 040 4 45 111 0 37 0 1 48 16 14 Cl 19 0 051 3 45 67 0 12 0 0 62 20 0 072 3
218. PTRI A TMS 2230 357 372 2 4 TMS 1372 219 234 TMS 1883 323 338 did TMS 368 386 dio 2140 212 PTRI Programmed Temperature Retention ndek PTRI n 5 d o o g0 mL 1 0 ng x x x1000 U g kg ng UL wg w 9 5 331 6 10 6 00000000
219. 6 8 3 4 5 6 7 DBP DEHP 1 000 PCB HPLC DBP DEHP 8 PCB DBP DEHP 1 3 5000 700 q 8 3 a 30cm lom 2g lcm b 5 200 2 9 d 000000000 20034 2 6 f 9 1 1 1 i 40 000 GPO 80 20mm 300mm 10 j 0000000000 HPLC GPC k o 0000000000 GCO 0 2 0 7mm 150 30m 0 10 1 0u m 99 999 0158 20 40cm sec 350 230 Q 0 54 350 230 q 0 54 1500 280 C 200
220. 0 0394 0 115 K 8490 11mg 100mL Es 0 1g L 0 1mol L NaOH 1mol L gt 2 e m EDTA ANa 200g L 40g 200mL n JIS K 8949 0 159 10mL 1 100 L 0 1mol L NaOH 50mL 50mL o 8mmx 200mm 60 100mesh 130 C 20 3 0 59 500 20 3 0 5g p WALPOLE s BUFFER CH3COONa 200mL 600mL 1mol L HCI 200mL pH3 q 2009 1 209 100mL 211 3 000000 8 C d 5 14 2 1 3 9 000000 DUDU 000000 110100 11000 5 14 2
221. 3 a 1 1 0 b 000000 4 00000 8 10g 2mol L 100mL b C 10 4 5 1 1 4 e d 100mL 4 5 1 1 4 e h 5 a 25mmol L b 4 8 4 96 10 g 200 100 NHA N xf KE x0 700 lt W NH4 moN g a 25mmol L mL b 25mmol L mL 9 mL 25mmol L 0 700 25mmol L 1 11 mg 37 6 00000000 4 5 2
222. p 4 6mm 25cm ODS 5O 10u m 225nm 300nm 4 8 6 3 3 1 4 3 ay 4 2 all h b 50mL 100mL C 100mL 50mL d 50 50 5mL 2mL 10 e 80 200 6mL f 1mL 9 ay f 5 a HPLC HPLC NP10EO Shodex Asahipak GF 310HQ 7 6mmx 300mm A 40 C x 225nm m 300nm 6 3 2 63 2 000000 Time solvent B flow rate min 96 mL min 0 30 0 6 20 30 0 6 60 50 0 6 70 90 0 8 80 90 0 8 90 30 0 6 b 10u g mL 00 0 31 1mL 10mL 0 11 1u g mL 5 10u LO HPLC
223. 5112 1 0000000 206 833nm 2 a 5 K 0557 A3 b 000 t oimol L 5 11 1 2 d d 000000000000000 0 10g L 0 5 11 1 2 e e 00000000 0 1 5 5 11 1 2 h 3 000000 a gt 161 b 00000000
224. 12 10mL 17 d do 0 3g L 5mL 1 2 12 1 2 660nm 15mL oo 17 12 d mgB kg 6 00000000 5 13 1 6 8 b 8 a 100mL 7 3mL 249 3mL D D D 0 49 L 3mL 10mL 12 0000 0000 0 3g L 5mL 1 2 0000000000
225. 5 a 0000 ICP 520 53 103 1 20 1 5kW 15L min 1 0L min 1 0L min b 000 1u 9 1 5 0 1 1 10mL 100mL 1u g mL 5mL 2 10mL 100mL 1u g mL 5mL 2 19 1u gCd 1u gPb 1u gCu 1u gzn Lu gFe 1u gMn 1p gNi 1u gMo 1p gAs 1 gCr mL 5OngCd 50ngPb 5O0ngCu 5OngZn 5OngFe j 5 50ngNi 50ngMo 50ngAs 5OngCr mL 1p g mL 1u g mL 5mL o 00000 Q 20 100mL 1u g mL 5mL 0 1 0 5mol L ICP 21 22 5 12 1 1 4 b 19 5 12 1 1 4 5 22 amp o 20 21 22 d mgCr kg 5 12 1 1 6 b 1 b 2 5 1 3 6 a
226. 3 000000 a 00000 b 00000 00000 d o 000000 e f 0000 4 00000 8 2
227. e 5mL 2 5mL 2 6 10 2mL 50mL 100mL 100mL 8 9 10 b 2 00000 3 3 8 0 1 19 0 001g Q 5mL 2mL 11 12 100mL 2mL 50mL 5 100mL 2 2 100mL 11 12 5 00 a 1 0 ICP 267 716 206 149 205 552nm 451 131nm 1 20 1 5kW 16L min 0 5L min 1 0L min b 10u gCr mL 0 2 40mL 13 100mL 14 2 40mL 100mL OG 13 10u gCd 10u gPb j 10u gCu 10u gzn 10u 9 10u gMn 10u gNi 10u gMo 10u gCr mL 14 170 d 100mL 0 1 0 5mol L ICP
228. 10u g mL 10 14mL 100mL 5 o 00000 100mL 5g L 3 106 7 993 3 10mL 25mL 1 21 3 5 10mL 2 2 50mL 30 50mL 5mL 2 69 50mL 650nm 4 1i 4 2 h d H g 4 1 mg kg 100 1 mg kg ug x Wg 9 mL 5 245 6 00000000 a 00000 3000 DUDU 3 000rpm 500 D 0 0 000000
229. 7 MIP b o 4 00000 5 1 1 4 a 5 1 1 4 b 5 a ICP 60 103 1 20 1 5kW 15L min 1 0L min 1 0L min 3 b 1u gNi mL 30 1 10mL 100mL 1u g mL 5mL 10mL 100mL 1u g mL 5mL OG 8 lu gCd 1u gPb 1u gCu 1p gzn Lu gFe 1
230. 6 0000 4 00000 5 1 1 4 a 5 1 1 4 b 5 1 1 4 5 a 1 1 0 1000 1205961 300 40 600 1 000 Q 300 40 2 200 2 70020 3 232 0nm 0000000000 12 20mL 0 1u gNi mL OUT Amt 3 100 50 L 13 232 0nm 14 5 1 1 4 8 2 5 1 1 4 b O 5 1 1 4 9 6 1 000 1u 9 1 0 5 10mL 100mL a5 0 20 10mL 100mL 0 28 0 2 00000 32 10 50 L 33 232 0nm 14 5 1 1 4 8 2 0 5 1 1 4 6 2 5 1 1 4 9 12 gt 131
231. 200 3 202 1 4 Chloro 3C 2 bi phenyl I I 234 0 236 0 4 4 Dichloro 13C 2 biphenyl 268 0 270 0 2 4 5 Trichloro 13Ca2 bipheny 302 0 304 0 2 2 5 5 Tetrachloro 13C i2 bi phenyl I 335 9 337 9 2 3 4 4 5 Pentachloro 13C biphenyl 371 9 373 9 2 2 4 4 5 5 H exachloro 3C12 bi phenyl 405 6 407 8 2 2 3 4 4 5 5 H eptachloro 33C 2 bi phenyl 439 8 441 8 2 2 3 3 4 4 5 5 Octachloro 13Ci2 bi phenyl 473 8 475 8 2 2 3 34 4 5 5 6 Nonachloro 13C 2 bi phenyl 509 7 511 7 2 2 3 3 4 4 5 5 6 6 Decachloro 13C bi phenyl dix 264 2 b 000 RF 5 1 2u L RF RF RF 15 RF 15 RF _ As xCis Ais xCs As Ais Cis ng Cs ng o 00000 GC MS SIM RF 1g 2u LO GC 8 8 RF 15 GC MS
232. 49 49 1 1 0000000 H2SiF 2 00 a 5 K 0557 A3 b 15 K 8223 5 K 9005 d JIS K 8885 1000 150 m 2 2 29 50mL 1 2 3 N N 0 1929 1 10 4 2000 4 1 JISK 8371 419 400mL JIS K 8355 24mL JISK 8034 400mL III 0 163g 145 10mL JIS K 8085 pH 4 7 1L 1 00 0 0 0 0 0 1 9 mL JIS K 8005 500 C 100 0 221g 1L 115 0030 F 100 9 00000000000 24 op Im 0 1mgF mL 10mL 500mL h 1 2 50 1 2u g F mL 10mL 3 a b 4 00000 8 20 5g 0 019 40mL 1mL 3 40mL b 1g
233. 6 6 8 2 20 did 176 dol 1880 p du 244 HCB 8 290 21 1 304 I 6 6 0 tal Uggguu 2 3 6 00000000 U 209 0000000 1M KOH 0000000 l00mL 4 000rpm 1 1 1 5 400 1 010000 Dagpnaunp 0000000 Daupnaupnaundad 20m 20 van
234. 1 2096 2 2 30 15 3 0000000 3 1 UDUD 1 000000 ai 00000 b 2mm 000000 2 a 2mm
235. b 30 50 B 5 a 0000 540nm b 5 12 1 4 5 0 o 00000 3 Cr VI 0 0150 0 25mg 50mL 141 0 5 0 6mL 20 Q 10g L 0 5mL 8 10 10mm 540nm 100mL 142 0 5 0 6mL 95 50mL 10g L 0 5mL 10 d VI mgCr VI kg 183 5 32 00000000 1 3 100 0000000 500 000000000000000 0 4 2 0 50 Dm 1100100000 0 0 900000000000 UUDUUDUUDUUDUUDUUDUUDUU 184 5 13 5 13 000 5131 1 0000000
236. 10 m z 16 m z m z 11 m z d mgNi kg 6 5 1 1 6 a l 5 1 3 6 8 5 7 4 1 232 0 2 a 5 K 0557 3 b 000 0 1mgNi mL d 1u 5 7 3 2 e 3 000000 a 000000000000 5 7 2 0000 e 0000 5 000000 e 0000 e 000000000
237. 2 a 5 K 0557 A3 b o 0000000 1u g mL 1mg mL 1mL 1 000mL 121 2mL d 0000000 Ou oimt 1mg mL 1mL 1 000mL 141 2mL e Ou gCr mL 5 12 1 1 2 i 0 1mgCr mL WI 10mL 1 000mL 1 1 10mL f lu gCd 1u gPb 1u 1 gZn gFer ont Lu gNil 1u gMol 1 u 9 5 1u gCr mL 5 1 3 2 f 9 S0ngCd 50ngPb 50ngCu 50ngZn 50ngFe 50ngMn 50ngNi 50ngMol 5O0ngAs 50ngCr mL 5 1 3 2 g 3 000000 a 000000 000000 18 0000000000
238. 1 17 nno 4 6 60 274 KEN us 8 62 s 30 66 8 466 9 10 9 f 23 237 2 09 Cis 8 65 H2 316 65 705 Bo 420 0 99 5 ia 3 18 15 5 42 Cis 16 635 y 18 C 17 425 19 445 400 475 282 ch 023 226 Cis 157 3 30 0 08 295 J 0 28 071 C 20805 9911 2 8 9 5868 16 PCB 64 1 6 4 2 6 4 1 CBo PCB PCB 17 K PCB K 18 4 1 19 OV 1 16 16 CBo 960 22 16 16 CBo 96 24 00 266 64 PCB 64 52 000000000000000 Sample Information
239. 5 a 0000 540nm b 000 2u gN mL 10 10mL 100mL c e mgN o 00000 3 0 2 2 100mL 10mL 10mL min 30mL 30mL 10mL 4 1mL N 1 1mL 20 540nm 100mL OI o d 4 1 10 mgN g 43 I 453 001 000 6 00000000 45 2 1160 000001 0000 ND 0 20 2u g 1100000000 0 10m U gt 100 1 0 0 10mL min 00000 300 0000 30m 200 540 nm 44 im 4 6
240. 451 131nm 20u gB mL 0O 1 40mL 100mL 50u g mL 10mL 451 131nm 15 16 mgB kg 188 5 13 6 00000000 8 D ul o a 0000000000 0000 1 00 000000 0 00190 550 C 200 200 300 L00 50
241. 1 1 3 2 3 2 a 2 b 3 4 d 89 4 e s tutt l din l dae f 1mo mL 0 19 100mL 100mL 1mg mL 0 3 80 1 1mg mL 10mL 100mL 100mL 0 1mg mL 389 0 19 100mL 100mL 1mg mL i BID 0 1mg mL 1mg mL 10mL 100mL 100mL 0 1mg mL p 80000 6 1cm 30cm 5 7 50 2cm 10mL 7mm 60 80 U 2cm 2 3 4 2500 450 C 8 5 dio dio p dia 13C 6 HCB Ce 6 SI 5g LC Si 59 0 1 7 576 200 1 130 C 95g 5mL 30 15
242. 0000 4 00000 5 1 1 4 a 5 1 1 4 b 5 a ICP 55 103 1 20 1 5kW 15L min 1 0L min 1 0L min 3 b 1u 9 14 0 1 1 10mL 100mL 1u g mL 5bmL 2 10mL 100mL 1 g mL 5mL 8 1u gCd 1u gPb 1u gCu 1 gzn lp gFe 1u gMn 1u gNi 1u 1u gAs 1p gCr 1u gB mL 5OngCd 5OngPb 50 9 5OngZn 50ngFe 50ngMn 50ngNi 50ngMo 50ngAs 50ngCr mL 1u g mL 1u g mL 5mL 00000 5 100mL 1u g mL 5mL 0 1 0 5mol L ICP m z ao 11 5 1 1 4 a O 5 1 1 4 b 2O oo 9 10
243. 8 540nm b 000 0 01mgCr mL 1 50 25mL 100mL 25mL 1 2 2 1 50mL 20mL 100mL 2 e Cr 0 0150 0 25mg 100mL 2 3mL 27 1 2 6 9mL 50mL 20mL 100mL 30g L 2 3 200g L 10mL 20g L 1 28 50mL 20 C 10g L 3mL 10 29 10mm 540nm 5 12 1 1 4 2 4 on 6 27 VI 28 VI 20g L 29 10 d 000000 mgCr kg 180 00000000 5 12 5 12 1 1 6 a 8
244. 5 1 1 6 a a 1 8 lH Cd PhO Cug Fer MnO NiO Mol As Sb Cro 11 ug 000000 100ML J 0 10 0 5mol L DO Rh Re Lu g mL 5mL 2 100mL uu Cdp 111 114 208 206 207 Cul 63 65 64 66 Fe 57 54 Mn 55 Ni 60 Mal 95 97 98 As 75 Sb 121 123 Cr 52 53 Rh 103 187 11 1 1 1 1 mg kg 514 1 0000000 2 a 5 K 0557 b 000 c 0000000 50u oimt Wi 1mg mL 50mL 1 000mL 1 1 2mL d 00000000 10u gCd mL 5 1 2 2 d e gCd 10u gPb 10u gCul 10 10 gFe 10 oh nl 10 gNi
245. 4 00000 5 1 1 4 8 5 1 1 4 b 5 a 1 0 ICP 950 970 98 103 1 20 1 5kW 15L min 1 0L min 1 0L min 3 b 000 Lu gMo mL 0 1 10mL 100mL 1 g mL 5mL 2 10mL 100mL 1 g mL 5mL 2
246. 2 000000 a 00000 SOPO Standard Operation Procedure 0 0 60 9 09 9 b 000
247. 4 00000 6 3 1 1 4 1 8 i 4 28 5 a 0000000 LC LC MS LC LC MS HPLC ODS 250x 3 0mm 5u m 0 5mL min 0 1M NaClO4 65 35 40 C 10u L 225nm T 300nm LC MS I UU UBL HPLC C8 250x 3 0mm 5u m 0 5mL min A 10mM B 8 35 65 40 C 10u L MS ESI negative 2 300 Q LOL min 40psi 100V 4 000V 2970 3110 3250 339 353 b 000 LASO Cd 10 L LC LC MS Cul 61211 Cas 10 14 6 3 LC MS Cid Cu 1 6 3 2 LAS 0 1mg mL WT 0 20 5mL 1L 249 6 3 1
248. 46 lll 1 2 a 0 5 K 0557 3 b 2 1 250mL JIS K 8951 500mL 5 8905 60 JIS K 8533 Iil 0 24g 300mL 2 1 120mL JISK 8588 5g 500mL d 000000000 729 4 JIS K 9502 L 7 29 100mL 10 e 1111 1111111111 RUME DE ST BE EE EE 111101 441111111411 1 5 1 f 50 9 JIS K 9007 105 250 2 0 2197g 1 000mL 10 1 5u 9 1 1 50u gP mL 20mL 200mL 1 1 0000 0 394 1 1 15 K 8721 0 19 100mL i 0000000000 200 1 JIS K 8576 2009 11 j 0000000000 40941 JIS K 8576 409 11 k 3 35 JIS K 8951 2mL 70mL 3 4 00000 a 00 0000000 31 Dg 0 01g 10mL 5mL 8 10mL 5mL e 6096 5mL 2 30mL 5 8
249. 50u g mL 10mL 220 351nm 451 131nm 14 15 d mgP b kg 6 00000000 5 1 1 6 a l 5 1 4 6 a 92 5 3 53 1 1 0000000 5 3 324 8nm 2 a 115 K 0557 A3 b 000
250. 8 9 m z 16 m z 2 m z 10 m z mgP b kg 6 5 1 1 6 a l 5 1 3 6 8 5 2 4 1 0000000 2 8
251. L gt 8mL 2 50mL i 2mL 5mL 2 6 3 1 1 1 1 4 5 6 19 5 a 0000000000000000 3mm 400 1 500mm 1800 250 m 5 255 130 180 C 180 C N20 300 80mL min ECD 0 53mm 15m 1 5 m HR Thermon HG 1 140 160 C N20 4 5mL min ECD b 50mL 0 1u gH g mL 0 1u gHg mL 4 8 i Hg o 00000 4i 7 8 9 1mL L 1mL 2 208 5 14 2 6
252. 6 d mgCu kg 6 00000000 5 1 1 6 a l 5 1 4 6 a 5 3 3 1 0000000 m z 2 00 a 5 K 0557 3 b 000 0 Ou g mL O 1mg mL 1mL 1 000mL 1 1 2mL d 0000000 Ou oimt 1mg mL 1mL 1 000mL 1 1 2mL e J Ou gCu mL 0 1mgCu mL 10mL 1 000mL 1 1 20mL f 1 Cdp 15 gPbr 1u gCul 1 gZn 1 gFe gMnD gNil gMor 1 u gAs 1u gCr mL 5 1 3 2 f 9 50 50ngPb 50ngCu 5OngZn 5OngF 50ngMn 50ngNi 50ngM or 50 9 5 5O0ngCr mL 5 1 3 2 9 3 000000 a 00000 e 000000 7 0000000000
253. 622 a a HCH B HC HCH p p DDD trans cis trans cis HCB I PBB a B a P 1 0000000 GC MS 2 a 00 2 b 00000 co 00000 d 00000000 e 00000000 2500 450 C 20 6 f 511 1000 000 0 0 0 5 2 g 000000 60 100 130 16 2 h 5 00000000 C 200 130 C 15 95g 300mL 5mL 30 15 i 60 80 p 0000000 99 999 015 k 5 K 1107 1 99 990 94 lI 000000000 1 20 C 1 1 Up DDT p p DDE DDD HCB 0 100g 100mL m 30 g mL 100mL 1mg mL 1mL 235 6 2
254. 25bmm 60m 1 00 m 40 C 7min b C min 180 C2 15 C min 250 C 180 C 25psi 000000 MSU E1 70V 255 C SIM m z 18 300 1 amu 0 5ng 15 16 GC MS 17 Tenax TA 3 200 Tenax TA 18 AQUATIC DB 10 DB 13010 DB 624 DB WAX VOCOL 1 o 10u g mL 0 20 10mL 10mL 9 8mL 0 2mL luL lu L d G GC MS 19 3 ng 19 90 110 d 00000 20 40mL min 20 40mL min 30 10 219 e 6 1 20 40
255. 00000 5 283 3nm Gi 5 1 1 4 8 2 ef 5 1 1 4 b O 5 1 1 4 5 d mgP 6 00000000 5 1 1 6 a l c 5 1 2 6 a 52 3 1 0000000 m z 2 a 0 15 K 0557 b 000 c 0000000 Ou 1mg mL 1mL 1 000mL 1 1 2mL d lug mL 1mg mL 1mL 1 000mL 1 1 2mL e 3 g mL 5 2 1 2 e f DDUUDIp Cdp gPbr 1u gCul 1 gFerj gMnD gNi gMor 1 u gAs 1u gCr mL 5 1 3 2 f 50ngPb 50ngCu 5OngZn 5OngF 5O0ngMn 50ngNi 50ngM or 50 9 5 5OngCr mL 5 1 3 2 9 3 000000 a 000000 000000 6 e 0000000000
256. 5 a 0000 GC GC 1 2 4mm L 1 5 Am W G 149 177u m OV 1 OV 17 1 5 1596 N20 300 80mL min 180 250 C ECD b 3 8 5H L 6 4 1 6 4 2 4 5u L 8 000000 PCB CBo 96 16 6 4 1 _boe Hi 92 CB 96 K H b H2 CB2 CB2 K x H gt 8 PCB mg PCB kg B D F e x Ze 8 mg kg A PCB mg L B PCB u L C u L D CB2 PCB CBo 4 c mL G g 18 PCB CB CB CB2 Am TotalCB 96 265 64 PCB 64 1 ov inn OV 170 CBeCeo
257. NIES NIES CRM No 2 NIES CRM No 12 NIST NIST SRM 1646a Estuarine sediment NIST SRM 2704 River sediment NIST SRM 1939 River sediment NIST SRM 1941 Marine sediment NRCC NRCC MESS 1 Marine sediment NRCC BCSS 1 Marine sediment NRCC PACS 1 Marine sediment NRCC CS LHS LHS 2 Marine sediment PCBs NRCC HS 3 HS 4 HS 5 HS 6 Marine sediment BCR BCR CRM 277 Estuarine sediment BCR CRM 320 River sediment BCR CRM 462 Coastal sediment IAEA 356 Marine sediment
258. 2709 50 10054 400 509 100 C min 2500 2800 70V 9 20020 2 10 Shodex Asahipak GF 310HQ 1 4 00000 a 0000000 3 209 100mL 11 12 30mL 5 10 3 000rpm 10 2 1 4 15mL 10 5bmL 2304 15 1mL 13 16 17 GPC 1 4 15mL 5 100mL 300mL 25mL 5 2 40 0 18 10mL 1mL 50mL 19 0 5vol 100mL 20 1mL 40 0 18 10mL 1mL 21 1617 GC MS b GPC 10 23 8mm Shodex Asahipak GF 310HQ 0 50 0 6 1 1 30 C 00000000 11 DBP DEHP 314 6 8 12
259. pH6 8 0 JIS K 9007 17 09 JISK 9020 17 89 500mL h TUE 109 11 4 8 1 2 h i 5 9548 3 5 0 25g 75 100mL 3 1 5 0 02g 20mL p 00000000000 1u GEN mL 4 8 1 2 3 a 2 8 b 4 4 8 1 4 a 5 8 620nm b 000 1u gCN mL 0 51 9mL 50mL 10mL 5 0 2 4 25mL 0 5 9 9 50mL Q 5g L 1 148 pH6 8 10mL 10 T 10g L 0 25mL 5 57
260. 2 a 5 0557 A3 b 000 0000000 Ou gm 1mg mL 1mL 1 000mL 1 1 2mL d l D 0 1mgAs mL 134 100m g L e 00000 Ou gAs mL 0 1mgAs mL 10mL 1 000mL 1 1 20mL f 1 adi 1 gPb 1g gCul 3 gZnl 1 gFe i gMn gNil gMo 1 u 5 1u gCr mL ID 5 1 3 2 f 9 S0ngCd 50ngPb 50ngCu 50ngZn 50ngFe 50ngMn 50ngNi 50ngMol 50 5OngCr mL 5 1 3 2 g 3 a 000000 000000 14 0000000000 0 1ng mL
261. 5 B 10mL 5 179 5 12
262. 1 1 1 2 1 2 2 0000 21 6km 22 200 300m 50m 50m 3 1 0 2 3 10cm 10cm 3 4 pH 5 000000000
263. 6 10 3 1mol L KOH KD 4 5 6 7 8 9 5 a 0000 GC MS GC MS o GC 5 10 0 32mm 25m 0 520 m 60 min 15 C min 280 C 5min 250 C 90sec He 7 5psi 250 C 000000 5 EI 70 250 C SIM MS PFTBA PFK m z 18 300 1 amu b 3 1 0 g mL 10u g mL og 1 0mL 335 6 10 10
264. 3 1 109 0 19 1mol L 50mL 30 3 000rpm 10 1mol L 20mL 10 3 000rpm 10 100mg 1 3 9 10 100mL 40mL 100mL 5
265. 3mL 100mL 191 c 2 o 00000 2 100mL 1 1 1 1 2 11 1 1 20m 90 100 10 25mL 10g L 3 4 196 0 o 200mL 5 9 1 4 a O 6 2 1 10 000 50 300g L 5 300g L 5mL 100g L 1mL 2g V 10 3 4 02 2 100mL 1 1 1 1 2mL 8 1 1 20mL 90 100 10 25mL 1 6mol L 10g L 10 lOmL min 6 196 0 5 9 1 4 8 2 o 5 d D00000 mgSe kg 6 00000000 5 9 1 6 a 5 9 1 6 b 154 5102 1
266. 6 1 2 0 61 2 0000000 D 12 l 3 1111 11 111 1 22 57 Ig 104 78 n I B Bi D 134 91 91 106 di0 98 116 1 11 1 1 11 1 1 1 Lu 76 41 78 39 64 66 45 69 71 62 64 d 65 67 1 50 52 1000 53 55 66 132 70 55 42 11 0000000 63 65 98 831 1 0 0 0 000 0 ds 66 68 101 83 129 127 u mal 96 94 1 1 1 2 0 0000000 131 133 95 1 1 2 2 0 00000000 83 85 166 168 123 110 112 39 77 13 54 53 39 1 3 0 0 0 0 de 58 42 60 11111 1 1 1 1 49 128 130 83 85 1 1 1 1 0 0 0 0 122 43 124 39 200000 122 43 124 39 86 57 n 0 0 0 66 64 100 111111 55 85 23 5 0000 58 87 55 73 99 55 73 85 53 67 68 105 120 49 57 1 1 0
267. x b d 000000 4 1 1g mgF kg 6 4 9 1 6 8 200mL 10mL 49 3 00000000000 1 0000000 49 4251 6
268. 5 a 0000 b 25u gF 1 0 0 20 60mL 100mL oer F c 00000 1 2mL min Gi 500 200u L e d 4 1 19 mgF kg 67 6 00000000 4 9 1 6 a 1 2mL min 68 410 00000000 1 4 10 80 C
269. 1 0000000 250mL EDTA 4 2 a 5 K 0557 A3 b 000000000000 5g L 0JIS K 8799 0 5g 5 K 8102 95 50mL 100mL o9 pnuggaggagnmaudnutl aoog L rJIS K 8588 10g 100mL d 5 K 8107 10g 20 g L 100mL e 5 9005 f 1 1 0 3009 1 JIS K 8356 129 0 115 K 8085 35mL 100mL 1 K 9020 17 89 300mL 200g L pH7 2 500mL 109 11 JIS K 8318 p 0 629 50mL i 4 5 9548 3 1 5 0 3g JIS K 8500 20mL 4 1 59 40 g L 20mL 1410 pH 7 100mL 10 C 20 j 0 1mol L I 0 115 K 8550 17g 1 000mL 5 K 8005 600 1 NaCl 10094 1 169g 200mL 20mL 50ml IS K 8646 2g 100mL J5mL 2g L IS K 8830 0 29 100mL 3 4 0 1mol L 0 1mol L f b 20 1 f a x x x 100 200 x x0 005844 9 b 96
270. 1 4 3 D mg kg H g kg mg g D 3 3 1 1 0 1 1 001 L D u 11 1 96 0 1 0 D 96 0 31 uuu mg g 0 01 5 mg g 0 1 mg g 0 01 mg g 0 01 mg g 0 01 uu t mg g 0 01 1 1 mg g 0 1 mg kg 1 10 9 0 02 mg g 0 1 uuu mg kg 0 1 mg kg 0 5 mg kg 0 5 mg kg 5 mg kg 5 mg kg 5 uua mg kg 0 5 mg kg 0 5 mg kg 0 2 uuu mg kg 0 2 1 1 mg kg 0 2 uua mg kg 5 11111 mg kg 0 5 uu t mg kg 0 5 Bt mg kg 0 01 mg kg 0 01 I 1 0000 1 1 00000000000 nd DUDU 00 g kg 1 g kg 1 L24 0 B g kg 1 11 00000000 g kg 1 12 g kg 1 11 1
271. 2 3 213 5 14 2 1010 0 0000000 0 lU uu 31 10 290 0 0190 0 D 50 20mL 1mol L KOH EtOH 100 D 2mol L HCI 10mL 100mL min 5 200g L EDTA 4Na 2mL 200g L 2mL 51 019 0000 000000 10m 300 1 200rpm 3 0 O00000 8mL 0 00000 20 5mL NaoH 300 1 200rpm30 00000 1 200rpm 30 0 u uaa D D
272. e 1 0 0 9 5 13 1 2f 0 36 1 K 8965 0 159 500mL 9 1 0 494 1 JIS K 8897 0 469 100mL 10 100mL 1 2 0 0 5 K 8465 i 0 1 5 13 1 2 i p Ou gB mL 0 1mgB mL 10mL 1 000mL k 0 1u WI 1u gB mL 20mL 200mL 3 a 00000 b 000 d e 00000 h 00000000000 4 00000 5 13 1 a 5 a 660 nm b 0 1u gB mL 11 10mL 50mL o 00000 15mL 3497 3mL 149 3mL 0 4 g L 3 mL 192 5 13
273. 1 800 2 500 30 6 283 3nm b 0000000000 DI 20mL 1u gP b mL 0 31 2mL 3 Gi 100 50 L 1 1000 g mL 2 283 3 3 5 1 1 4 a O ef 5 1 1 4 b 0 5 1 1 4 c eo 2 o1 000 1u gPb mL 1 10mL 100mL 4 Uu 1000 g mL 22 10mL 100mL 1 1000 g mL 22 0 2 00000 0 100 50 L uM 1000 g mL 283 3nm 3 8 5 1 1 4 8 2 5 1 1 4 b O 5 1 1 4 9 eo 2 1 2 3 aja 3 4 d 000000 o 00000 mgP b kg e 0000 mgP 6 00000000 86 5 2 5 1 1 6 8 5 2 2 1 0000000 5 1 1 6 d
274. 5 1 1 4 8 2 5 1 1 4 b 2 3 d mgF e kg 6 5 1 1 6 a b 5 1 2 6 a 552 0000000000 1 0000000
275. 10g L 9 10 e 193 7nm 6 5 9 1 4 a Q o 8 5 10 80 1 000 9 10 o9 22 0000 20mL 1 1 4 1 200g L 2mL 8 15 10 6 0 109 10 10mL min 11 193 5 9 1 4 8 2 o 11 d mgAs kg 142 6 00000000 8 1 D ul a 1 0 Ast Se 10 590 0 0190 00000 00000 200 10 50mL Dan D 15mL 15mL 00000 EROR 110200 ADU 000000 s 10mL 0000 203m 20 3D 100mL 0000 1000000000000000000000000 000000 10m 00000000000000000000 143 b Asi Sel Sb 25mL 5 9
276. 4 00000 5 1 1 4 a 5 1 1 4 b 5 8 ICP 640 66 103 1 20 1 5kW 15L min 1 0L min 1 0L min b 000 Lu gZn mL 0 10 50mL 100mL 1 g mL 5mL 2 10mL 100mL 1u g mL 5mL OG 7 1u gCd 1u gPb 1u gCu 1 gzn lp gFe 1u gMn 1u gNi 1u gMo 1u gAs 1p gCr 1u gB mL 5OngCd 5OngPb 5O0ngCu 5OngZn 5OngFe j 50ngMn 50ngNi 50ngMo 50ngAs 50ngCr mL 1p g mL 1u g mL 5mL o 00000 3 8 100mL 1u g mL 5mL 0 1 0 5mol L ICP 3 m z 10 8 5 1 1 4 a O 5 1 1 4 b O o 8 9 m z 16 m z 2 m z 105 5 4
277. oi malli puru 3 L3 F3 o0 um GE E IESSE Ekel E LE CO ojo oloo ooa aaa pa3 ca e c1 e c3 r3 laa laa mla CHE oo ooo lama CC cceumuamiuuumuaum mes 3 r3 eai umi uu E mla laa 5 mla COOC CEO e ee cem CH T mz CO EN Cl laa laa glooo olol olol ol aol aol aol aol aol aoa 1 1 1 Jala F3 EEIELEIEILEIEILBIES Jan nawan Jaan ESL iria lama OJOJIOIOJO Li OJO OJO O OI CH O O O OJO o o o o o o o 190 190 190 190 190 o o o o o o o o o o a st CH r3 N E3 r3 i o e N x CH mla mla CH CO E iJ SE CH COOC CO CO EC O pjoo olol olol aol aola mla pea ns d E L1 IC CH 3 CH a r3 a ES LE 1 CN L3 1
278. 3 8 10mL 10mL e 50mL 5 100mL 2 3 5 a 1 1 0 217 6nm b 000 0 1 gSb mL O 5 5mL 25mL 5mL 0 1mol L 3mL 25mL c 1 0 20 5mL 25mL 5mL 0 1mol L 3mL 25mL 1 8 22 c 00000 0000000000000000 0 5mL 0 1mol L 3mL 4 25mL 10g L 5 6 8 217 6nm e 5 11 1 4 8 2 ona 4 VI 1 000 200 500 1 000 1 000 5 6 o9 22 25mL 5mL 0 1mol L 3mL 10 6mol L 109 10 lOmL min 7 8 160
279. 10u gMo 10u gCr mL 5 1 1 2 j 0 1mgCd mL 5 2 1 2 d 0 1mgP b mL 5 3 1 2 0 1mgCu mL 5 4 1 2 0 1mgZn mL 5 5 1 2 0 1mgF e mL 5 6 1 2 9 0 1mgM n mL 5 7 1 2 9 0 1mgNi mL 5 8 1 2 f 0 1mgM o mL 5 12 1 1 2 i 0 1mgCr mL 5O0mL 500mL 141 10mL 3 a 000000 82 5 1
280. 2 a JD 5 K 0557 b 0000000 50 1mg mL 50mL 1 000mL 1 1 2mL d 10u gFe mL 5 5 1 2 c 0 1mgF e mL 10mL 100mL 1 1 2mL e D 30 gCd 10u gPb 10u gCu 10u gZn 10u gFe 10u gMn 10p gNi 10 u gMo 10u gCr mL 5 1 4 2 e 3 000000 a 000000 b 00 0000
281. 1 96 MW 100 W 1 Hg 2 u 9 2 1 10 mg kg 2 46 12 590 O 120 30 29 22 1 1 1 3 000000 1 2 4 8 g mL 3 100 500mL 4 1 2 b C 30 2 2 5 a 1 5 b 4 8 a 3 100 W Hg mg Kkg T Hg mg kg x 100 W 352
282. 2 Bl a 0115 K 0557 A3 b 00000000000000 0 3 61 1 5 14 2 1 2 b o 5 14 2 1 0209 d 0000 5 142 1 02e e 00000 5 142 1 2 f f 2006 1 5 14 2 1 2 9 9 10000 000000 5342 2i 00 100p gHg mL 5 14 2 1 2 j i Ou 5 14 2 1 2 k j L 00000 0000 00 0 39 1 5 14 2 1 2 k 1 1 0 0 14 1 1 000000 0 1 g Hg mL 5 14 2 1 2 m
283. N O bis trimethylsilyl trifluoroacetamide 200u L 1 0 20 0 3mL dio 1u g mL 1mL 1mL 3 d 2 3 2 4 TMS MS bis trimethylsily trifluoroacetamide TMS 5 a GC MS GC MS GC 576 0 25mm 30m 0 25u m 60 C 1min 10 C min 280 C 5min 280 C 60sec 1u L 40cm sec 280 C e 00000 45 1 70V 250 C SIM PFTBA PFK MS m z 38 300 1 amu b 1 000000000 1 mL lu LOD GC 5 329 6 10
284. 0000 gt 133
285. 1 2 1 5kW 15L min 1 0L min 1 0L min b 000 1u gAs mL O 1 j 10mL 100mL 1u g mL 5bmL c 10mL 100mL g mL 5mL 00 100mL 1u g mL 5mL 3 0 5mol L ICP m z a9 19 5 1 1 4 b O e eo 18 m z 16 m z 2 m z 19 m z d mgAs kg 6 5 1 1 6 b 5 1 3 6 a 5 94 43 0000000 148 5 9 193
286. a b 200mL 9 000000 d 0000 e 0000 810000 10mm 300mm h i 10u L i 2000 250 q 20 Amt 1 5000 2 000cm 1800 250 C 1500 180u m OV 1 OV 7 1 50 558 2000 250 50 99 9vol9q 30 80mL min 4 5 GC GC 4 00000 a 000000000000000 0000 31 206 0 19 200mL 6 1mol L 50mL 80 09 1 50mL 8 GF A 10 1 11 20mL 30mL 9 300mL 50mL 10 10 300mL 50mL 300mL b 0000 a 50mL 11 12 200mL 300 3mL 13 0000000000000000 10mm 300mm 263 64 8 20 200mL 2 5mL min
287. 5 1 0 05 x t n 1 0 05 MDL 5 0 2 1 000000000 tu n 1 0 050
288. 2 DD a 115 K 0557 A3 b 25mmol L J 9 K 8951 1 4mL 100mL 1L 15 K 8005 600 0 53009 0 001g 20mL 25mmol L b
289. 010 3 000000 a 0000000 50mL b 0000 228 6 2 1
290. A mo ONOMA o o NOAN o Gao N m E t n oi D EE ogro gand g naga CC O HH Bob HBHU B Em m HH DDR 365857 B o naga ga jm l oH OO goof nao ESI EIER RS o a cc ELE m o0 oo Diet EIS moga CC o0 um Ana oon HH nr D DD o 1 1 pue E SE ma gada as og mB 0ua CH o0 gogo enyen jam janj jan E E Fer BHuumuuudguudggnugHgtMuum a ma EB 5 janjan jan jon jan jun janjan 2 Loop TAH COOC jun janjan jun janjan janjan 332357 3 3 1 Dr D I OG Deg Daon Dan Ga Di DIE GI Deep GO Oe EE gag 2020 omm E B Uu ioo 3 2 0 _ T ear Eccc ada IETE EI a N 1 L3 L3 e eq e Te
291. 1mL min 200mL 15 309 3mL 1 0mL 7 8
292. W N 2 a 5 0557 A3 b 000 o 000 000 e 1 3 f 115 200g L JIS K 8913 209 100mL 8 5 K 8136 1 409 100mL 2 3 10 i 1 mn 3006 JIS K 8374 N 129 1 2 100mL p 000 1 0000 1 4101 m 5 9512 N N 0 25g 0 1g 100mL Il 5 585322 m 1u gAs mL 5 9 1 2 3 a b 4 5 9 1 4 a 5 8 510nm b 1 1u 9 5 11 2 10mL 1 1 6mL 25 40mL OT 25 29 99 5mL 100mL 2 o 00000 3 151
293. 6 3 2 2 1 0000000 2 60 20 1mL HPLC FLD 2 a 5 K 0557 3 b 1 115 K 8891 o 5 8161 d e 100000 000000 0 1 2 3
294. 9 m z d mgM o kg 00000000 5 1 1 6 a l 5 1 3 6 a 5 8 2 1 0000000 1 313 3nm 2 8 5 K 0557 A3 b 000 9 0000000 i D 1000 om U M d 1 O 000g om
295. 4 00000 5 1 1 4 a 5 1 1 4 b 5 1 1 4 5 a 1 1 0 ICP 231 604 341 477 221 647nm 1 20 1 5kW 16L min 0 5L min 1 0L min b 000 10u gNi mL 0 10 20mL 2 100mL oo 20mL 100mL C 2 2 10u gCd 10u gPb 10u gCu 10u gzn 10u gFerj 10u ont 10u gNi 10u gMo 10u gCr mL o 00000 3 8 100mL 0 1 0 5mol L G ICP 4 5 6 8 5 1 1 4 8 2 D ef 5 1 1 4 5 2 5 1 1 4 oo 3 4 100mL 50u g mL 10mL 451 131nm 10u gNi mL 0 1 20mL 100mL 50u g mL 10mL 2 451 131nm 5 127
296. 1mg mL 1 10u g mL 5 C f 8 00000000 500 700 60 100 130 qd 16 1009 5 7mL 4 5 i 99 999 ij 0000000 312
297. 4 7 TOC 1111 5mL 2 500rpm ami 2 500rpm 10 2 3 100 1055 2 825 C 5 a 0000 30 b 0 31 6 0mg 0 001mg wb 10 100mg 0 001mg 10 3 2058 3 d z 4 1 1g mg g W2 0 mg g 8 b x10 94 59 W1 W2 4 7 TOC 6 00000000 a 1000 105 C 250 00000 b 000000 19 ll 124111 5mL 000000 51 48 000000 481 4
298. 0 10u g mL 010 dio D dau 10u g mL 0000 0 10u g mL 0 p p DDT 136012 HCB 3Ce 10u g mL p 6 2 2 1 PBB 6 2 2 1 10u g mL 10 62 221 2 Bromobi phenyl 3 Bromobi phenyl 4 Bromobi phenyl 2 2 Dibromobi phenyl 2 4 Dibromobi phen
299. 4 00000 5 9 1 4 8 5 8 0000 b 000 3mL 100mL 0 1u gSe mL 0 5 153
300. 4 00000 5 11 1 4 a 5 1 1 4 b 163 5 11
301. a ICP 259 9400 239 5620 238 204 238 204nm 1 20 1 5kW 16L min 0 5L min 1 0L min b 000 10u gFe mL 0 10 20mL 2 100mL 20mL 100mL 2 10u 9 90 10u gPb 10u gCu 10u gzn 10u 10u gMn 10u gNi 10u gMo 10u gCr mL c 00000 D 100mL 0 1 0 5mol L Q ICP 4 2 6 5 1 1 4 8 2 5 1 1 4 5 2 3 4 50mL 50u g mL 10mL 451 131nm 10u gFe mL 0 1 20mL 100mL 50u g mL 10mL 2 451 131nm 5 6 111 d 000000 mgF e kg 6
302. 100mL 4 1 00 0 0 DU 0 9 1 4 0 1009 100mL 4 1 1 100000 0 0 mg mL 4 t 0 100g 100mL 4 moie ID 4 0 1009 100mL o 00000000000 D 0 1009 100mL m 0000000000000000 lo g mL 100mL lmL 000000 da dio 10u g mL 20 C 1 00000000000 0 9 1111 0 100g 100mL o 24 3 9 2 4 0 1009 100mL 0000000000000 0 39 8111 0 100g 100mL umgagg amuuu tu 10u 100mL dio 1u g mL 1 1 0 0 100 0 0 0 0 de die 4 n dio 10u g mL 100mL 3 000rpm 15 000 00 IL 200mL 500mL 10 20mL 30cm 10mm 596 15g 2cm 100mL 111 01 10 10u L 1 0 o 0000000000 GCO 1 0 2 0 7mm 150 30m
303. 163 178 n 192 135 n 206 135 163 135 135 220 n 234 135 177 163 269 284 dio 164 dio 188 dio 212 4 4 4 4 t dio 4 4 n dio dio d o x5 x 20 o u g kg ng x m wig x1000 w 9 10 W DB 5ms Restek Rtx 5 HP HP 5ms Supelco SPB 5 SGE BPK _ 5 11 12 13 337 6 10 6 00000000 1 10 g wet 30mL x 2 00000 20m a 5 Naci 200mL 0000000 0 20 50mL z ET
304. 2 000 PCB 1 a 6 4 1 2 a b 6 4 1 2 0 6 4 12 9 d 00000000 6 4 1 2 d e 6 4 1 2 0 f 4 1 2 00000000000000 0 0 6 4 1 2 9 h 6 4 1 2 h i 6 4 3 2 0 000000 6 4 5 6 4 6 6 4 7 0 010g 100mL
305. 000 00 000 00 10u gm 1 1 100mL 100mL 1 3 000000 a b 00000 d e 0000 f 000000 3 000rpm 9 0 0 i 50mL NP3EO 11 NP7EO NP6EO 15cm 5cm
306. 30 20mmol L CODsed 2 a 1 0 0 0 000 20 16 JIS K 8247 3 29 1 050 1 100mL 1 2 16 G4 30 b 0 JIS 8528 6 79 11 306 1 JIS K 8659 10 10mL 100mL 1 d 0000000 0 0O 100g L 0 JIS K 8913 10g 100mL e 5 8637 269 JISK 8625 0 29 11 2 15 K 8005 130 C 2 0 72g 0 001g 200mL 20mL 300mL JISK 8913 2g 145 5mL 5 100mL 10g L 1mL mL 0 1mol L f f a Rd AUN 100 200 2xx0 003567 8 9 X 0 1mol L mL 0 003567 0 1mol L 1mL g 3 a 3 1 1 300 0 01g 20mmol L 100mL 300g L 5mL b 30 4 C 50mmol L Wal 100mL 3 7 10mL d 500mL 26 6 f 9 h
307. electrospray positive 300 C 10mL min 50psi 3 500V 63 4 5 NP2bEO NP3EO NPAEO NP5EO NP6EO NP7EO NP8EO NP9EO NP10EO 260 m z M 4Na 287 2 331 2 375 3 419 3 463 3 507 3 551 4 595 4 639 4 683 4 L L NP2EO NP3EO Na K Na LC M LC MS L Asahipak GF 310HQ B 0 1 A 40 C 10 L 0 6 3 3 000000 Time solvent B flow rate min mL min 1 0 30 0 6 10 30 0 6 30 50 0 8 35 90 0 8 40 90 0 8 001 6 3 2 261
308. 2 a 5 K 0557 A3 b 5 8625 o 5 8562 d 000 e 000 f g 5 K 9005 1 50u g mL 1mg mL 50mL 1 000mL 1 1 2mL t 0o1imgB mL JIS K 8863 1 000mL p 000000 20u gB mL 0 1mgB mL 50mL
309. 1 2 aq 0000000 GC MS 2 a 00000 b 00000 d 00000000 e 00000000 2500 450 Q 20 6 40g L 0 49 100mL 9 1 11 1 11 0115 1107 10 00 99 999 vol 4 i 975
310. 6 mgH g kg d 000000 4 1 IKg mgHg 7 8 9
311. 4 00000 5 1 1 4 8 5 1 1 4 b 5 1 1 4 5 00 a 0000 283 3 1 7L min b 000 0 1mgP bim 0 5 20mL 15L min 100mL 20mL 100mL
312. 18 4 00000 4 9 1 4 a f
313. 4 00000 5 1 1 4 a 5 1 1 4 b 5 a 0000 1 7L min b DU 15L min 0 1mgF e mL 0 1 5mL 100mL 5mL 100mL 109 248 3nm
314. e 0000000 3 e 0000000 1000000000 MDL Method Detection Limit
315. 1 220 6 1 61 1 0000000 u 1 uu L 84 86 117 119 37Cl4 125 127 1 2 62 64 1 2 0
316. 3 000000 a 000000 7 0000000000 0 1ng mL 250amu 10 lamu amp 0000 7 MIP a 0000 gt 112
317. 121
318. 5 1 1 4 8 5 1 1 4 b 5 a 100 120 300 40 600 1 000 C 30 40 2 200 2 700 3 6 213 9nm b 3 33 20mL 0 10 gzn mL OUT Amt E 100 50 L 32 213 9nm 13 8 5 1 1 4 a O 5 1 1 4 b 2 eoe o1 000 0 1u gZn mL 0 1 10mL 100mL 14 Cl AG Gi 10mL 100mL Cl AG 0 2 00000 11 100 50 L 12 213 9nm 13 8 5 1 1 4 8 5 1 1 4 b 2 eoe 11 12 13 eoe 14 d 00000 mgzn kg 0000 107 5 4 6 00000000 5 1 1 6 a 5 1 1 6 d 108 mgzn kg 5 5 5 5 1 000000000 1 0000000 5 5
319. 113 10 m z d 000000 mgF e kg 6 00000000 5 1 1 6 a b 5 1 3 6 a 554 1 0000000 248 3nm 2 a 1 5 K 0557 D b Ou ot
320. 25m 105 2 3 0000000000 200 40 e 0000000 0 50 5mm 500 300mm e 2 1 4 177 250 m 250 500 m 2500 500 m 250 500 m e 20 40mL min 30H 60 o 0000000000 20 409 1 180 280 4
321. o 00000 amp 2mL 4 8 j mg Hg kg d O00000 4 1 mg Hg kg 1
322. 0 1ng mL e 250amu 10 lamu e 0000 96 5 3
323. gt 168 a b b 1 Gi 5 12
324. 10u L 00000000 0 3mL 10 8 11 GC MS 1 2 0114
325. 5 14 1 2 1 0000000 2 00 a 00000000000000 50g L 0 1 5 K 8253 50g 1L 8 b 5 14 3 1 2 8 JIS K 8252 1 3 Op g L a 300mL b 5 14 1 1 3 4 300mL a 31 10g 0 1g 50mL b 1 3 20
326. b o 0000 4 00000 5 1 1 4 a 5 1 1 4 b 5 1 1 4 5 a ICP 220 351 216 999 405 782nm 1 20 1 5kW 16L min 0 5L min 1 0L min b 000 10u gPb mL 0 50 20 11 100mL c 20mL c 11 10u gCd 10u gPb 10u gCul 10u gzn 10u gFe 10u gMn 10u gNi 10u gMo 10u gCr mL c 00000 12 100mL 0 1 0 5mol L ICP 13 14 15 5 1 1 4 a 5 1 1 4 b 5 1 1 4 c eo 12 13 100mL 50u g mL 10mL e 220 351nm 451 131nm 10u gPb mL O 1 20mL 100mL 91
327. 231 6 2 1 l 621 1 201 166 173 100 72 125 109 185 79 145 220 121 150 91 77 103 173 145 109 255 137 179 152 304 199 264 91 204 246 288 123 125 277 109 260 79 118 162 189 204 290 105 177 77 313 130 317 287 236 173 157 169 185 141 323 dio 188 dio 212 dio 211 196 183 d 000000 41 96 19 mL 1 g kg ng x it X1000 9
328. 243 4 00000 4 1 00000 6 3 1 a 209 100mL b 30mL 300mL C 10mL d 300mL e 60mL f
329. 4 200 5141 000 6 00000000 U 3100000000 109 0 19 1 D 1 50 30g L J 10 10mL DD ma ma ma CC Lua 000 10mL 20094 0 00010 10 10mL 000000 250 201 5 14 1
330. 4 00000 5 1 1 4 8 5 1 1 4 b 5 a 1 1 1 0 600 000 30 40 1000 120 C 300 40 2 700 2 800 C 30 6 313 3nm b 2 1 20mL 0 1 gM o mL 0 31 Amt 3 100 50 L 1000 g mL 1000 om 3 313 3nm 5 1 1 4 a J 5 1 1 4 5 2 000000000 o1 000 1u gM o mL O 5 10mL 100mL 5 1 1000 g mL 1000 g mL 2 0 20 10mL 100mL N 1000 g mL 1000 g mL 2 CL AG 6 2 00000 6 100 50 L 1 1000 g mL 1000 g mL 2 e 3 313 3nm 4 5 1 1 4 a J 5 1 1 4 5 2 6 1 2 3 gt 136
331. 3 000000 a 000000000000 0000 e 0000 000000 e 0000 5 000000000000 e 000000000 50 500 L b 0000 4 00000 5 12 1 1 4 b 1 5 12 1 1 4 b 2
332. 3 000rpm 10 100mL 3 30mL 20mL 559 200mL 500mL 50mL 300mL 6 50mL 2 KD 4 50vol 1mL 10mL 1 KD 50vol 1mL 50vol 10mL 6 5vol96 6mL 10mL KD 7 2 3 000rpm 10 3 MS 17p 2 4 16 16 64 178 16 16 17 03 m z 300 227 17p 2 4 16 16 64 H D 17p _ 16 16 17 ds H D m z 227 4 5 6 3 15mL 10ml 7 KD 3 1mol L NaOH 800 5mL 50 9 0 5mL KD 3 30 10 lmol L KOH 5mL 8mL 70 C 341 6 11
333. 2 8 2 b 000000 o9 d e 00000000 f 11000 i 00000000000 100 gmL CH3 CH2 1O CH2CH20 H 0 0100g
334. 284 6 4 PCB
335. 0 1ng mL e 250amu 10 lamu 88 5 2
336. 8 S 5 9 0 LC 51 59 9 596 200 1 1300 5mL 30 15 uuu 000000 KD 11000 000000000 2 0 75mm 250 30m 5094
337. 269 270 m z 431 m z 432 11 d DD 5 20 e 00 mL 1 g kg ng x D X wig x1000 W 9 350 6 11 6 00000000 00000000 5 9 00000 30 2 lm 1101010000 1 5mL 1mL 20mLx2 50mL ul 70 C Ur 351 li
338. 279 5nm 1 7L min 10u gM n mL 1 15L min 50mL 100mL 100mL 117
339. 0000 b o 00000 0000 4 00000 5 1 1 4 8 5 1 1 4 b 5 1 2 4 a 5 a 0000
340. 2 8 DDJISK 0557 3 JIS K 8891 o 0000000000000 Got 9 e 9 1094 1 JIS K 8576 100mL 74993 JI S K 8951 f 1 0 000 15 8322 19 DUDU 0 19 100mL 30mL 11 500mL 6 8mL 50g 11 j 000000000000 1L 500mL 6 8mL 50g 11 000109 NaO0O SO CH2
341. 5 a 0000 5 1 1 4 1 7L min b DU 15L min 100mL 0 1mgCu mL O 1 4mL 4mL 100mL 93 00000 1 324 8nm Q 5 1 1 4 a O 5 1 1 4 b 2 5
342. 327 6 10
343. 2 9 2 20 60mL min 000000000 0 32 0 53nm 30 C 200 h 0000000000 GCU 0 2 0 7mm 25 120m 0 10 3u m 99 999 500 350
344. UU DD DD DU UD
345. 10u g mL 0 0 11 1mL 0 10 1u g mL 10mL 10 2u LO 45 6 2 1 1 10 2u L GC MS
346. C 1 213 9nm 101 Q 5 1 1 4 a 2 5 1 1 4 5 2 3 1 d mgzn kg 6 5 1 1 6 a b 5 1 2 6 a
347. mgNi kg 6 00000000 5 1 1 6 a l 5 1 2 6 8 572 1 0000000 2 a 1 5 K 0557 D b 3 3 0000000 50 gmL 1mg mL 50mL 1 000mL 1 1 2 30 gNi mL 5 7 1 2 9 0 1mgN i mL 50mL 500mL 141 10mL e lI H 10 gCd 10u gPb 10u gCu 10 10u gFe 10u gMn 10u gNi 10u gMo 10u gCr mL 5 1 4 2 e
348. o 00000 100mL 8mL 1mol L 8mL 50 50 o 50mL 8 ICP 2 109 10 6mol L 6 196 026nm 200mL 5 9 1 4 8 2 e OI o 6 7 d O00000 mgSe kg 6 00000000 5 9 1 6 a 5 9 2 6 a 5 103 1 0000000 1 196 0nm 2 a JD 5 K 0557 b 000 1 958 1 5 10 3 2 0 1mgSe mL 10mL 1 000mL 141 20mL d 1u 10u gSe mL 10mL 100mL 1 1 2mL e 0000000 0 1 000 g mL 1 f 000000000 1 000 oimt 0 3 a 0000 gt 156
349. 2 a 1 5 K 0557 A3 b 000 248 3nm Olmo em 134 100mg L 3 a 0000 Uu o 06 9 Q9 11 0 00 b o 00000 e 00000 0000
350. 3 00000000 590 D 0019 00 00 1 200 1050 110941 D 4000 0 0 001 g0 00 a b x10 20 0 001g 42 0000 1 000000 a 6002425 b 600 25 1 D D 0 001g 2 8 3 3 2 59 0 001g b 600 2520 2 0 0019 D 100 e e 3 00000000 0000 59 D
351. 00000 15 228 8nm 5 1 1 4 8 2 5 1 1 4 b 5 1 1 4 c 15 d 000000 mgCd kg 6 00000000 5 1 1 6 8 a 0000000000 CO PbO Cur Fer Nih 5 1 3 1 Cd Pb Cu Ni I Fe Mn Zn i unt 0 100mL 1mol L 10mL 228 8nm Fe 248 3nm 283 3nm Moll 279 5nm 2 11000 Cu 324 8nm Ni 232 0nm 2 213 9nm ICP
352. d 000000 mgZn kg 6 00000000 5 1 1 6 8 5 5 1 4 6 8 543 1 000000 m z 2 a 5 0557 b 000 c Ou oimt 1mg mL 1mL 1 000mL 13 1 2 1 Ou om 1mg mL 1mL 1 000mL 13 1 2 e 00000 1u 92 5 4 3 2 0 1mgZn mL 10mL 1 000mL 1 1 2mL f og 1 gPb 3 ou 1p 1 gFel 1 gNil 1 u 9 5 1u gCr mL 5 1 3 2 f u 50 50ngPb 50ngCu 50ngZn 50ngFe 50ngMn 50ngNi 50ngM o0 50 9 50ngCr mL 5 1 3 2 g g 3 000000 a Q 6 0 1ng mL
353. 313 6 8
354. 6 2 1 2 D 621 52 9 15 1 dio _ IS 2 dio _ 15 3 di IS 4 d _ IS 1 Is 1 Is 1 IS 2 IS 2 IS 2 IS 3 Is 1 Is 1 4 IS 4 125 167 IS 4 198 212 Is 1 8 233 6 2 1 6 00000000 20g wet 25mL x 31 3 000rpm 10min 3 D D 1120 61541 1 11 D 10mL 0000 5m
355. mL 1 g kg ng x uL SWO x1000 16 GC GC 270 17 DB 1 TC 17 HP 504 SPB 50 1 18 PET DB WAX 1 19 PET DB 1 HP 11 DB 5 303 HP 5
356. e 000000000000 000000 100000000 0 0 0000000 0 3 00000000000 a b d D 3
357. 10mL 5vol96 5mL 10mL 6 1 5mL C18 50 5mL 6mL 10mL 57i iii GPC 5 iii iv 3 4 5 10mL 3 000rpm 10
358. 60 4 9
359. 4 pH5 40mL 30 2 000rpm 10 10vol96 40mL 20mL 40 10mL 200mL C18 5mL 5mL 10mL i 5 5mL 50vol 50vol 1mL
360. 10 m z d 000000 6 00000000 5 1 1 6 a b 544 1 0000000 mgzn kg 5 1 3 6 a 213 9nm 2 00 a 5 K 0557 A3 b 000 o 0 0 0 1u gzn mL 5 4 3 2 6 1u gzn mL 10mL 1 1 2mL 3 000000 a 00000
361. 4 00000 5 1 1 4 8 5 1 1 4 b 5 1 1 4 5 a 100 120 C 30 40 500 800 30 40
362. 80 Q 80 C 5 30 30 0 0001g b 4 1 50 19 mg g 1000 mg g 8 b x
363. 2 a 1 5 0 59 25mL 50mL 1 b 000000 10u gCr mL 5 12 1 1 2 j 3 000000 a 0000 b 00000 500mL 3 1 4 182
364. 48 000000 6 00000000 481 0 0000 481 4 25mL D DD CND 0 50 ou Set 0000000000000 seti 10 2542 00000 3000000000 620nm mgCN kg 59
365. gt 128
366. 6 00000000 5 1 1 6 8 gt 139 5 1 4 6 8 mgM o kg 5 9 5 91 00000000 1 0000000 5 9 193 2 8 6 e f 9 h i DU U 0 1mgAs mL j k 3 000000 8 lD JISK 0557 A3 DDU uu 000 D D Gn D D UU 200g L 0 JIS K 8913
367. 94
368. 6 GC MS 7 1mg mL 0 1mg mL 30 50mL 100mL 100mg 10mg 100mL 1mg mL 0 1mg mL 8 65mL
369. 2 29 3 200mL 0 01g Qo 15mL 111 15mL 4 8 15mL 10mL 5 5mL 3mL 6 7 mL 50mL 5 100mL 2 3 4 5 6 10mL 7 5 a 1 1 193 b 0 1 gAs mL O 5 5mL 20mL 1 1 4 20mL C 1 22 5mL 20mL 1 1 4mL 20m c 1 22 o 00000 0 1 1 4mL 20mL 200g L 2mL 8 15 141
370. 283 3nm 2 DD a 115 K 0557 3 b 000 0 1mgPb mL 5 2 1 2 8 3 a nnl 1 0 0 0 Uu o 6 Q9 11 0 0 0 b o 00000 e 00000
371. 70V 6 1 1 9 10 2 6 gt 1 4 Tenax GC Tenax TA VOCARB3000 217 4 a b 0 d e 5 a 6 1
372. d 3 000000 a 000000 b d 0000 gt 126
373. 1 3 10 250mL 5 14 1 1 5 b 10 c 00000 5 14 1 1 5 1 1 90 11 20 96 200g L 20mL 4 b d O00000 4 1 0 5 14 1 1 5 8 mg Hg kg 10 2 204 5 14 3 6 00000000 UDUD 3
374. 10 250amu e 00000 lamu 6 ICP MIP b 00 0000 104
375. 87
376. m 6 1 51 7 DD 3 30g L 1 1 253 7nm UU 2 253 7nm 1 2 3
377. 6 11
378. ei 4 1mL 5 N 1 1 11 20 540nm 10mL d 4 96 191 g 6 00000000 4 5 2 1 6 500 4 1m iml 20 0 540 nm 41 45 330 aq
379. 9 000000 PCB d 00000000 PCB 400 C e 00000000 0 g 0000000000000000 1mol L h i 5 8550 j 630 212 m 10mm 130 18
380. 0 2mg mL VI 0 020g 100mL 180 1mg mL 0 100g 100mL 180 1 10u gmL 100mL 0 2mg mL 5mL 1mg mL 1mL m 104 g mL r rn B O U 0p om WI dij dio 10u g mL
381. d 6 4 5 6 4 6 8 window 596 phenyl methyl siloxane PCB IUPAC 0 0 10 50 190 70 540 770 104 1260 1550 169 1880 1890 2020 2050 2060 2080 209 GC 5 phenyl methyl siloxane 4 4 2 2 6 6 IUPAC 454 PCB 3 3 4 4 IUPAC 77 8 8 5 2094 PCB PCB M 70 PCB 5 20 2 PCB IUPAC 11 3 3 3 3 3 3 PCB PCB IUPAC 11 q q AL ru 3 3 0000000000 5 2090 e PCB PCB PCB RF PCB 6 4 6 Wellington Laboratories BP MS BP MS RF f 285 6 4 PCB
382. 0000 30mL min 25 619 3m 20 00000 mt 0000000 10mL 2nL 252 632 6 3 2 2 63523 41 0000000 18 GC MS
383. 44 CODsed 100mL 300mL 20mmol L 10mL 6 100g L 5mL O 1mol L lmL al g 4 1 90 19 CODsed mgO 500 1 CODsed b a xf x0 800 X100 XW CODsed mgO g a 0 1mol L mL b 0 1mol L mL 0 1mol L 9 0 800 0 1mol L 1mL mg 1 CODsed 3 2 2 40 605 109 3 4 5 20mmol L 50mmol L 6 20mmol L 10mL 10mL 20mmol L 20mL 3 b 100g L 25mL 3 7 10mL 0 25mol L 2mL 27
384. 0000000 223 6 1 e 00000000 1500 250 C
385. 542 0000000000 1 00000000 2 a 5 0557 b o 0000000 50 om 0 1mg mL 50mL 1 000mL 1 1 2mL d 0 000 10u g nt H 5 4 1 2 c 0 1mgZn mL 10mL 100mL 141 2mL e 30 gCd 10u gPbr 10u gCu 10u gZn 10u gFerj 10u gMn 10p gNi 10 u gMo 10u gCr mL 5 1 4 2 e
386. RF ng As xCis Ais XRF As Ais Cis ng z ng g kg OW W 9 5 MS 6 7 8 286 6 4 PCB 6 4 1 6 9 0000 0 25mm 0 30m 0 25 mti 70 C 2min 30 C min 170 C 5 C min 300 C 10min 250 901 EID 70V 280 287 6 4 PCB 644 1 8
387. 10g Huu 2mol L 100mL 38 4 5 1 1 6 452 2 1 0000000 2mol L 2 a 15 0557 b 10000000 4 5 2 1 2 9 d 00000 4 5 1 1 2 8 e 00000000 0 0 200g L 0 4 5 1 2 2 f f 0000000000000 0 4 5 1 2 2 9 000000000000 0000 10g L 0 4 5 1 2 2 h h l n 0 01mgN mL 4 5 1 2 2 j 3 a 000000 b 0000 00000 4 00000 3 2mol L 4 5 2 1 2 b 4 5 2 1 4 a d
388. 1 7 15 L min b 000 0 1mgN i mL O 1 5mL 100mL 5mL 100mL 125 o 00000 1 232 0nm Q 5 1 1 4 a O 6 5 1 3 4 5 2 5 1 1 4 0 d 000000
389. 9 10 11 12 13 14 15 264 64 PCB
390. o 000000000
391. 4 5 1 1 4 b 5 a 1 1 0 ICP 1210 123 103 1 20 1 5kW 15L min 1 0L min 1 0L min b 000 1u gSb mL 0 1 10mL 100mL 1 g mL 1mL 10mL 100mL 1u g mL 5bmL c 00000 100mL 1u g mL 5mL 1mol L Q ICP m z ae 17 5 1 1 4 5 2 e eo 16 m z 16 m z 2 m z 166 17 m z d mgSb kg 60 00000000 5 1 1 6 b 5 9 1 6 d
392. 6 d mgNi kg 6 00000000 5 1 1 6 a l c 5 1 4 6 a 5 7 3 00000000 1 0000000 m z 2 a 0 15 K 0557 b 000 0 Ou g mL O 1mg mL 1mL 1 000mL 1 1 2mL d Ou oimt 1mg mL 1mL 1 000mL 1 1 2mL e 0000000 1u 5 7 1 2 c 0 1mg mL 5mL 500mL 1 1 10mL f ecd gPb 1u gCul 1p gZn 1u 1u 1 1u gMor 1 u gAs 1u gCr mL 5 1 3 2 f 9 50 50ngPb 50ngCu 50ngZn 50ngF e 50ngMn 50ngNi 50ngM ol 5O0ngAs 5O0ngCr mL 5 1 3 2 9 3 000000 a 000000 e 000000 7 0000000000 0 1ng mL e 250amu 10 lamu e 0000
393. 70V 280 C SIM m z 18 300 amu 0000000000 6 4 8 O000000000 188 0 190 0 152 0 222 0 224 0 152 0 256 0 258 0 186 0 289 9 291 9 293 9 325 9 323 9 327 9 359 8 361 8 357 8 393 8 395 8 397 8 429 8 427 8 431 8 461 7 463 7 465 7 497 7 499 7 495 7 283 6 4 PCB 64 9 9
394. 2 000 a 6 1 1 2 a b 00000000 10mL 3g 6 1 1 2 b d 00000 0 1mgmL 6 1 1 2 e 1 6 1 1 2 e f 0p gmL 6 1 1 2 f 6 1 1 2 9 6 1 1 2 h 3 a 00000 DULL 6 1 3 3 8 e 6 1 1 3 8 b 000000000 o 6 1 1 3 b 00000 0000000 o 1 1 3 90 d 6 3 1 2 6 450 C e 00000
395. 196 026nm 2 a 5 K 0557 3 b 000 9 1mol L 5 9 2 2 d 091 5 10 1 2 c e 000000 0 1 gSe mL r 5 10 1 2 f 3 a 0000 000000 b 00000000
396. 33 60 q 14 GPC 8mm G PC 1 500 L 15 8mm 1 Amt GPC THF 16 17 18 19 20
397. 5 8 0000 100 120 30 40 177 500 800 C 30 40
398. 110100 LU uuu 00000000 Pak Cartridges FI lu L lu L lu L orisil 1010 111 11 11111 Ka 10 1 000 g mL Sep 1 Lu g mL 2 1 10 1
399. 75 103 147 5 9
400. 4 00000 5 13 2 4 b 5 8 0000 ICP 11 194 303 5 13
401. 188 0393 222 0003 255 9613 289 9224 323 8834 359 8415 393 8025 427 7636 461 7246 497 6826 289 190 0364 223 9974 257 9587 291 9195 325 8805 361 8386 395 7996 429 7606 463 7216 499 6797 6 4 PCB 64 12 0000000000000 200 0795 202 0766 4 Chloro 3C 2 bi phenyl 234 0406 236 0376 4 4 Dichloro 3C 2 bi phenyl 268 0016 269 9986 2 4 5 Trichloro 3C 2 bi ph
402. 58 00000 5 8 1 00000000 1 0000000 m z 2 00 a 5 K 055
403. e 0000 e 0000 0000 uultu e 0000 5 b 500 L 98 5 3
404. 2 000 PCB 1 a 6 4 1 2 a b 6 4 1 2 0 6 4 12 9 d 00000000 6 4 1 2 d e 6 4 1 2 0 f 4 1 2 00000000 6 4 2 i 6 4 1 2 0 e2410 8 0 0 45 D 0000 m 00000000 6 4 3 2 m 1 6 4 1 2 9 6 4 3 2 k PCB 3 000000 9 8 b 64 10 b 000000 d 0000 e 0000 6 4 1 2 e f 00000 000000
405. 6 00000000 5 1 1 6 a 5 1 1 6 d 24 mgM n kg 57 0000 571 000000000 1 0000000 232 0 2 00 a 5 0557 A3 b 000 D 0000000 1mgNi mL 134 100mg L 3 000000 a 000000000000 0000
406. 306
407. 500 1 0009 4 ul 46 41 1 4 ul 4 31 5 VOC e 00000000 0000 DUDU 0000 3
408. 241 6 2 6 00000000 100 20 gwet 00000 50mL x 30 D00000 15 C 3 000rpm 10min 0000000 DUDU 5 NaCI D 0000 50mL n 1 20 0 000 0 5m Fr 1111 1 Fr2 1111 114 01561 Fr 3 111 1 15 6 0 111 100mL 150 000 5 10g 111 5 0 0 0 1 1 30 0 1 90 D 0 D D RPH LH 1mL 00 00 DUU 0 25 3 30m 0 25 m 0 25nm 15m 0 25 m gt 10 C mn gt 280 C 5m C 1ni n 10 C mn 300 C n 4 ELO EX T ES ESL EST ET L3 E3 E3 E3 F3 E3 fe ama 93 ir ii 242 6 3 6 3 1 000000000 6 3 1 1 1 0000000 6 5 1
409. 30 k PCB IEH EU U Gc PCB KC 300 KC 400 KC 500 KC 600 2 1 1 1 1 0 01 1mg L 3 0000 1 PCB 2 KC 300 KC 600 11 3 262 64 PCB 3 000000 e
410. 0000 00000 A 100ml 1 11 111 1591 1 1000010000 8 109 L 0 74993 5 10m 0000000 10m 0 0 0000000 00000 B 50 30 ai 0000000 000000 50mL 11 e5onm 247 6 31 6 3 1 2 1 GCB 65 35 1mL HPLC 2 a b C d e 12 3g f 9 A3 115 K 0557 5 58891
411. d 000000 4 5 14 1 1 5 6 mg H g kg 202 5141 6 00000000 1 80 0000 80 000 3100000000 10g 0 19 0 300 00000 50 1 0 20mLD D UD 010 10 20mL0 D D D 3041 20mL 000150 00000 150000000 0009 10mL 0000000000000 2009 L0 0 0 1 1 10mL 000000 250 mgH g0 kg 203 5 14 1 3 1 0000000 110000 00000 5 14 1
412. e 000000000 5 500p L b 0000 4 00000 8 a 00000 mn 59 2 200mL 0 01g
413. 00 1 209 5 14 2 ei 000000 000000000000 E E U 109 109 0 19 0 5 200000000 i 10 0 30mL 30min 2 20 10min OmL HCI 1 1 10mL 40mL 00000 100mg U 100 11 1 0 8 0 8 0 DUDU 40mL 00000 00000 500 0000 40mL 0000000000 20 1 D 20m 20 1010 50 Umm 100 00000 11110010 000000000 00 sm 0000 0000200 0 8 0 300 BD 00000 0 50 Lomp J HE NM R Thermon HG 0 53 DU 15m0 O0 N20 4 5mL min 150 00 ECD mgH g0 kg 210 5 14 2 5 14 22 1
414. 15 9959 dae 9959 1 00 000 6 0 0 0 100mL 6 0 01g 100p g mL 1mL 10mL 10u g mL g mL 1u g mL 0 1 g mL 7 10 0000000000 dz dis 0 01g 100mL 100p 100p g mL g mL lmL 2
415. 20mL 30g L 20mL d 15 e 2 9 50g L 10mL 95 C f 5 14 1 1 4 d 9 30g L 5 00 a 0000 5 14 1 1 5 a b 1 5 14 1 1 5 b 00000 5 14 3 5 2
416. 0 1 3 0 m 99 999yo 94 20 40cm sec 35 230 0 5 C 300 6 6 8 200 270 50 100 40 50 C 100 C min 250 280
417. 115 6 00000000 5 1 1 6 8 b 5 1 1 6 d 116 56 0000 5 6 1 1 000 Du Du 5 6 279 5nm 2 Bl 115 K 0557 a b C d 11000 A3 0 1mg Mn mL 134 3 000000000000 a b 00000 e 00000 0000 D 10 gMn mL r 141 10mL n
418. m z 2 a b C 1 15 K 0557 A3 uu Ou om 0 1mg mL 1mL 79 5 1 1 000mL 1 1 2mL d 0000 lu g mL 1 000mL 1 1 2mL e f lu gcd 1u gPb 1 Ou 5 1 1 2 1mg mL 1mL gCu 1p gZn 1p gF
419. 0 2mg mL 3 000000 a 00000 o nul 50mL 1050 3 15 b o 00000 00000 0000000 216 6 1 d 0 01g e 000000000 er 50 25mL f 100000 eg 10 100 L g 0000000000 00000
420. 10m 1 20 6159 D D 5mL x 2 0000000000000000 TITIT d10 TIT 10 g mL 20 L METTE 2 234 6 2
421. D 1 3 a 00000 b o 1 d 00000 e 0000000000000 f 00000000000 h 0 5729 250mL 000000 4 00000 a b gt 185 a 0000000000 Q 3 3 5 13
422. gt 197 5141 E AUC CERE AVV Bii EE CH ELE CH E EZ 3 aN U 514 1 Et HOER DCK EE EH EET B DEER 5 14 2 0000000000 5 14 34 8088888088 8800 1114 1111411 141411111 1111111111111844111141 H 3 0 350 250mL 0 D 000000 1000 3000 0000 0 EHE HEP ED ED ERES DER GEN R HERE ER DD 0 5 31 r 20 5L mint 1111100000 5 2 1110 0 0000000000 00 115 8 0 000000000 0000 8080008000000 00000 000000 E tJ TI Er E
423. uuu lu L d 70 13059 u g kg ng K mL 1 uL 9 296 W g x1000 6 5 6 00000000 100mL U 100 0000 u 60 50mL 00000 6 30mL 00000 500 O00000 DUDU 150mL 200000 0000000 si 10mL 297 6 5 UUDUUDUUDUUDUUDUUDUUD U D 000000 30mL 5
424. 175 5 12
425. e 0000 f 0 00000 00000000 00 0 000000 i 0000 ij
426. I 44 4 1 56 10 CODsed CODsed b a xf x2 00 xr a 0 25mol L mL b 0 25mol L mL 0 25mol L W 2 000 0 25mol L Ui O 1mL mg 2 CODsed Qu 400001 EP 4 00000000 1 3100000000 60191 8 B 0 KMnO 4096000000009090 0 0 0000 0 0 0 0 0 0 3000 1010 20mmod L0 100mL 0 000 30091 5mL 100mL 300 100 0 0 20mmol L lomL DUDU 30 0000003000 0000 0000000000 60 8 804 0 omman 10mL 10mL 009 5mL 000000000 0 0 500m0 500mL 28 45 DD 451 DDD 4511 00000 1 0000000
427. mgSb kg 6 00000000 5 11 1 6 a 5 9 1 6 d 5 1 4 00000000 1 00000 5 1 1 6 b 5 1 1 6 b mgSb kg m z 2 00 a 1 5 K 0557 b 000 9 1 d 000 A3 3 000000 a
428. n 6 p q r 3 a b j k 6 10
429. 10 b 2 00000 3 3 8 0 1 19 0 001g Gi 5mL 2 3mL 10mL 11 12 1mL 10 50mL 5 100mL 2 3 100mL 68 11 12 5 a 0000 ICP 208 959 249 773 249 678nm 1 2 1 5kW 16L min 0 5L min 1 0L min b 000 20u gB mL O 1 40mL 100mL 13 40mL 100mL OG 13 o 00000 100mL 0 1 0 5mol L ICP 14 15 16 5 13 1 4 8 2 b 16 b 26 2 14 100mL 50u g mL 10mL 187 d 5 13
430. 3 a 000000 18 0 1ng mL e 000000 250amu lamu 10 5 0000 18 ICP b MIP 0000
431. 258 10u LO HPLC JOOD ul d 000000 JODO 1 ng mg kg
432. 8 5 DB 10 DB 171 SPB 11 SPB 51 SPB 7 NB 10 NB 17 BP 17 CP SIL 51 CBP 10 CBP 170 CBJ 31 CBJ 17 Ultra 1 11 0 1 232 6 2 1
433. o 69 5 0000000000 0000 U D D 410 20 309 1 D D 0191 00000 50600 80 C 30 80 5 C 3000000 0 000190 0 0000 70 5 Il 51 00000 5 11 000000000 1 0000000 228 8 2 a JI S K 0557 A3 b 000 o nu d 60 0
434. 49 200g L pH pH 5 0 5 5 11 500mL JIS K 8355 57mL JIS K 8150 5890 JIS K 8288 0 3g 200g L pH pH 5 0 5 5 11 3 a b 0 1mV pH 0000000000000000 d 3mol L
435. TOC 1511 yn D 1 2 DD a o i j 3 000000 8 9 h i j 4 e nn 000000 8 0 K 0557 1 31 1S K 8180 7 0998 N 10 3699 p E B EB ED 52 13758 N 20 2899 D D C 41 6 0 N 8 179 1 1 1 1111 EH 000000 O Uu uuu uu 0o00 uu 0000 000 0 0 001mg
436. e 000000 aas A 50941 DDTCN 6 59 100mL 009 15 K 8284 109 100mL 10g 80mL 1 1 pH 100mL 10mL 000000 10g L 2mL
437. 2 a JD 5 0557 A3 b 000 c u gAs mL 5 9 3 2 e d 0000000 00 1 000u g mL e 00000 3 000 g mL 3 a 000000000000 0000 e 0000 e e 0000 e 50 5
438. 50 gt 120 1800 28600 19 u g kg ng x mL mL x
439. 1 7L min b DU 10u gCd mL 0 5 20mL 15L min 100mL 20mL 100mL 78 5 1
440. 100mL p 000000000 10 om p d1o 0 0100g 100mL 10mL 100mL III Sep Pak Plus Accell CM Cartridges 360mg 1 1 I 1 0 Sep Pak Plus Accell QMA Cartridges 360mg 1 1 m C18 MMH Sep Pak Plus 18 Cartridges 360mg 11 CFAO whatman 11 3 D00000 a b 0000 9 000 d e 00000 f 00000 5 00000000000000 253
441. 2 00 a 1L b 0 514110 2009 1 1 JIS K 8150 3 000000 a 0000000 b 5 34 1 1 3 2009 300mL 4 00000 a 3 3 3 3 90 1 109 0 19 200g L 20mL b 95 C 5 00 5 14 1 1 4 e 8 0000 5 14 1 1 5 a b 000000 0 1u gH g mL 1 20mL
442. 48 0 0 x0 UUD O 1mol L mb 0 005844 0 1mol L 1mL g 0 mbi JIS K 8443 1 DD 0 6390 20g L 2 5mL 250mL 100mL p 0 2g L JIS K 8495 ul ul g 5 4 2 4 20mg JIS K 80347 100mL 0 5mL 0 1mol L mgCN 1 1 a xf x5 204 X100 000 cuni mgCN mL al 0 1mol L mL 0 1mol L HI 5 204 0 1mol L 1mL mg I 0D0000000000 Ou GEN mb 3mgCN mL 10mL 1000mL 20g L 100mL 10mL 100mL 1 du 1 1 1mgCN mL J 3 a 48 10 00 b e YO D p J Big D SES A S x 2 AD 500m Cr gu DI F I 1 1 I DUDU 200mL 100 U 48 53
443. 6 00000000 U 0 20g 0 5mL UI 200mL 109 0000 20m 00000 20m 00000 0000 5mL 00000 20 0 5 5 100m aa GC MS gt 311 68 000000000 6 8 1 2 1 2 13 41 0000000
444. EU QS a 252 250 DPP 92 91 196 197 c s DPCB J trans DPCB 104 208 91 115 130 208 DPP dx 97 cis DPCB ds 109 trans DPCB ds DPB ds 213 TPH ds 212 TPCH 109 109 dio 188 dia 240 1 2 di4 196 DPB 9 317 207 208 TI 91 129 207 208 TPCH 91 104 312 8 012 264 0 10 5u g mL 10u L lu LU GC MS 18 lu 1 GC MS 21 d
445. 6 00000000 1 1 100mL 20g 5omr 500 100 0 3 000rpm 1000 50mL 500 100 0 3 000rpm 1000 1 5 50m DUDUDUDU 100mL DUDU 100mL 0 H 0000 mL 324 6 9 2 DEHA 110 0 01 00 30 C 00000000000000 325 6 10
446. 5 14 2 1 3 a 5 14 2 1 3 9 5 14 2 1 3 6 5 14 2 1 3 8 5 14 2 3 3 cm 4 00000 8 3 1 0 019 1mol L 20mL EDTA 4 100mL min 5 2mL 6 50mL 10 10mL 200g L 2mL 10mL
447. lmol L KOH 0 5 1 02mL 100 000 1mol L 0 00000 5 1 0 0 0 0 intl 70 C 00 00 0 Ou g0 0 7mL 00000 3m UD D 1mL H H H L1 a I em 0 5mL 00000 338 6 11 1100100000 6 1 17a 17 6111 5 1 0000000 94 70 C di
448. o 06 9 Q9 Uu b H 0000 Uu Du 4 5 1 1 4 8 5 8 5 1 1 4 b 1 7L min b 0 1mgZn mL 0 01 15L min 2mL 100mL 100mL
449. 0 1mgCu mL 134 100mgCu L 3 a 000000000000 0000 0000 b o 00000 00000 0000 4 00000 5 1 1 4 8 5 1 1 4 b
450. 6 00000000 5 9 1 6 a 5 1 1 6 b 158 mgSe kg 5 1 1 6 d 5 11 5 1 1 00000000000 1 D 5 11 217 6nm 2 8 3430 0 1 6 1 1 15 K 8635 d D 5 K 0557 A3 DDU 10 e 0 f 00000 0 760
451. 0 0 1 000 DD 50 50 1 50 50 11 12 LAS 1mg mL DUDU 65 35 1 100mL h 12 LAS 10u g mL C127 LAS 1000mL LAS C 0 Cu B 0 D JU 1mg mL 10mL 100mg 65 35 1mg mL 2 100mL LAS Ciq 14 E LASO Cio j 10 100mg 65 35 C14 65 35 100mL 3 000000 a b i j 1mg mL 10mL
452. 0 1mgSb mL 10mL 100mL f 3 000 oimt II 3 000000 a 000000000000 o 0000 0000 000000 e 0000 00000000000 e 000000000 50 500p L 00 0000
453. b 3 000rpm 20 1 VOC 3 00000000 0 0 0 2mm 3 000 romp 20 16 32 0000 1 a 00000 b 2mm 000000
454. No CAS Registry PTRI Number 6 IH 319 84 6 1700 1809 2189 182 9 B 319 85 7 1748 180 9 218 9 182 9 y 58 89 9 1767 1809 2189 182 9 8 319 86 8 1822 1809 2189 182 9 DDT 50 29 3 2361 2350 2370 165 3 p p DDE 72 55 9 2185 2460 317 9 31629 DDD 72 54 8 2275 2350 2370 165 3 72 43 5 2487 2271 228 1 115 32 2 2473 1390 2500 113 0 309 00 2 1983 262 9 2649 66 0 60 57 1 2200 79 0 262 9 276 8 72 20 8 2245 262 9 81 0 264 9 959 96 8 2142 1950 240 9 338 9 33213 65 9 2270 1950 2409 338 9 76 44 8 1910 2718 1000 273 8 1024 57 3 2064 3528 354 8 81 0 trans 5103 74 2 2113 3748 3728 236 8 5103 71 9 2140 3748 3728 236 8 27304 13 8 _ 115 0 3868 236 8 trans 39765 80 5 2146 408 8 406 8 410 8 5103 73 1 2302 408 8 406 8 410 8 118 74 1 1705 2838 285 8 248 8 29082 74 4 379 7 377 7 3817 PTRI Programmed Temperature Retention Index 9 PTRI 5 240 6 2 2 3 0000000
455. 7 1 gCd 1u gPb gCu 1u gzn lp gFe 1u gMn 1u gNi 1u gMo 1u gAs 1p gCr 1u gB mL 5OngCd 5OngPb 50 9 5OngZn 50ngFe 50ngMn 50ngNi 50ngMo 50ngAs 50ngCr mL 1p g mL 1p g mL 5mL 00000 100mL 1u g mL 5mL 0 1 0 5mol L Q ICP m z 9 8 5 1 1 4 a O J e 5 1 1 4 5 2 oo 8 m z 16 m z 2 m z 134
456. 12 0 2 2 00000000000 D D 91 9 0 ppm NIES NIST NRCC BCR IAEA No 2 No 12 1646a 2704 MESS 2 BCSS 1 PACS 1 320 356 Pond Marine Estuarine Buffalo Marine Marine Harbour River Marine Sediment Sediment Sediment River Sediment Sediment Sediment Sediment Sediment Sediment 96 10 6 7 22 2 297 6 11 8 2 3 90 As 12 6 23 23 4 20 7 11 1 211 76 7 26 9 Ba 254 210 414 531 548 Cd 0 82 3 0 0 148 3 45 0 24 0 25 2 38 0 533 4 47 Ca 59 0 81 1 06 0 519 2 60 2 2 8 87 Ce 34 72 95 41 5 Cr 75 201 40 9 135 106 123 113 138 69 8 Co 27 16 6 5 14 0 13 8 11 4 17 5 19 15 0 Cu 210 104 10 01 98 6 39 3 18 5 452 44 1 365 Ga 5 15 20 Fe 96 4 31 2 008 4 11 6 53 4 5 2 41 Hg 1 3 1 16 0 04 1 47 0 092 4 57 1 03 7 62 MeHg 5 46 K 99 0 68 1 56 0 864 2 00 2 5 La 17 17 29 46 19 3 Li 18 47 5 73 9 Mg 1 46 0 388 1 20 2 0 Mn 770 837 234 5 555 365 229 470 800 312 Mo 1 8 2 85 1 9 12 9 0 6 4 87 Na 96 0 57 3 25 0 741 0 547 2 0 1 39 Ni 40 57 6 23 44 1 49 3 55 3 44 1 75 2 36 9 P 00 0 14 0 027 0 0998 0 11 Pb 105 101 11 7 161 21 9 22 7 404 42 3 47 Rb 42 69 38 100 71 0 S 90 0 352 0 397 Sb 2 0 0 3 3 79 1 09 0 59 171 0 6 8 33 Sc 28 5 12 15 25 6 90 S
457. 44 00000 5 1 1 4 a 5 1 1 4 b 5 a ICP 203 844 281 6150 202 030nm 1 20 1 5kW l6L min 0 5L min 1 0L min b 10u gMo mL 0 1 20mL 10 100mL CIS 20mL 100mL 2 10 10u gCd 10u gPb 10u 9 10u gzn 10u gFerj 10u gMn j 10u gNi 10u gMo 10u gCr mL o 00000 100mL 0 1 0 5mol L ICP 11 12 13 8 5 1 1 4 8 2 5 1 1 4 b O o 11 3 100mL 50u g mL 10mL 2 451 131nm 10u gMo mL 0 1 20mL 100mL 50u g mL 10mL 2 451 131nm 12 138 13 d 5 8
458. 0000 00000 e 00000 6 0000 4 00000 5 1 1 4 8 5 1 1 4 b 5 1 1 4 5 8 0000 228 8nm
459. 80 100mL 1 1 40g L b 0000 b 1 1 1 1 3 3 200mL Q 8 lg 0 0019 10mL 10mL 2 9 10mL 10mL 2mL 5m
460. 12 13 14 30 C 0 1 gF mL 1 lp 9 mL 30 15 Ou 9 mL 110 0 1mgF mL 120mV 25 C 0 1 gF mL 0 1mgF mL 00000 100mL 64 200mL pH5 2 10mL
461. 200mL 9 h 30mL 30 100mL 42 000000 a 20g 100mL 40mL b 3 000rpm 5 10 200mL 40mL d 30mL
462. D 2009 10mL 1 1 DDTC 50g L 10mL H 00 150 00000 50 1 UUDUUDUU Amt 0000 76 5 1 d 000000000 Cag PbO COD Fej Mn Mor As Ser 55 Cr o 00000 00000 0000000 0 10 2 0 0 0 0 0 20 1 ip D H D Cd Pb Cr 0 D Cu Zn Fe M Mo As Se Sb 1000m g L 0 D 0 000 n N Cd 228 8nm Pb 283 3nm Cu 324 8nm 2 213 9nm Fell 248 3am Mn 279 5nm mgCd kg e 0000 Cd Pb Cr 0 00 1000mg L D CuZn FeMn Ni l D MoAs Se Sb l 1000mg L 0 00000 228 8n Pb 283 3nm Cu 324 8nm 2 213 9nm Fell 248 3nm Mn 279 5nm mgCd kg 3000000 0 0 1 1 0 1000mg L 100 50 1 100 SouL O0 00000 100 00000 1000mg L Ni 232 0nm 313 3nm All 193 7nm seg 196 0nm Sb 217 6nm Cr 357 9nm 100 50 0000000 wogngn na dn 100 50 L 100 500 00100 0000 0 000 1000mg L Ni 232 0nm Mal 313 3nm As 193 7nm Gell 196 0nm Sb 217 6nm
463. 1 00000 00000 4 8 uu 2 29 200mL 0 01g 20mL 159
464. 181 300mL uu 250mL 000000 0000000000 050 B jot 1 1 HD b 11 n oojoo 100mL i 200 10mL 3 2 6 9mL 213 11 JD O 2 1 uut DUDU D 1 3mL 1111000000 0 0 29 1 20 30 1000 DDD 20mL D 100mL EE M SE ERR f O FL lt o 540nm 5122 000000000000 1
465. 344 6 11 6 000000000 D 10m em 1mol L 8 8 0 5mL 0000 00 50 15min 000000 0 5mL 1mol L KOHO 00000 4 5mL 3mL 70 C Ur 2 0 DUDU ol U Sm GC MS SIM 345 6 11 6 11 2 0000000000000000 GC NCI MS 1 0000000 pH5 10vol96 2 a b 2 1 0 0 0 o 00000 d e 000000 f 0000000 i j 00000000 k imo L 0 0000 1 190 18 6 19 2 50mL 1 1 m 00000000000 Sep Pak Florisil n Sep Pak Plus C18 o 2000
466. 254 6 3 2 0 0 mg kg 0 D D wu wW 9 2 3 255 6 00000000 00000 0000 30mL O 70mL 0 0000000 GF F i 00000000000000000 0000000000 00000000000 0000 10mL 8 4m L1 u 1 1 5 D 150 C 20 3g 4mL 1 1 D D HOHUA 20mL 5mL im 20 H U 000000 14100 GC MS 256 6 3 2
467. I 43 000 DD 200 000000 10g L 0JIiS K 8659 10m IJ I D jot 300000080 0 0 08 00 3 000000 l 43 1 00000000 3000 5 00 11 200ml U AU BD D D 000 DID ED D FI D 180000 tL 300mL 500mL 200mL L3 L3 E3 EJ p oana U 43 13 00000000 4 00038 a ju m D DD 00000 e D DD 3000 500m 0000 4100000000000 d 8 0 0 3000 5 00 200 30 0 0 00 DD D D D d 000000000 00094 2 0 0 0 0 00 DD DD DD DD e 00000000 Ga
468. CN OD cN Du o N e i QN m m m m m m aH zd H pedum 1 1 H L2 L3 L3 LLL LL CT HaBHHBE RH Ze m O OD et a mamada lt P EZ mamada E EE oam A nm E GO A CO CODE Es N ob o8 5 COOC a jan 1 saja ispa EE Eras D Hanar ai m E ele ee Eet EE rE aa TESI HN E m HHHH DI AA AA o GO d uoo L1L1 I o 000 me rud 2 2 O AN 00 1111 111 111101 DREIECK D I 11 1 0
469. 0 5 mol L 10mL 10mL 0 5H 9 10mL 4mL 2 TPT dis 10u g mL 100u L 10mL 47 lu Las TBT lu g TBT dz TPT GC FPD 16 FPD 17 18 FPD 10u g kg
470. 0 51452 000000000000 198 514 3 000000000000 5 14 3
471. 0000 4 0000 41 0000 1 000000 a 105 b 1 0 0 0 0 001g 1 4 2 1 b 10mm 2 DD a 10mm 0 001g b 105 110 40 C
472. 280 Q 2 20 C min 280 Q 200 2700 500 10034 271 64 PCB
473. 4 00000 5 1 1 4 a 5 1 1 4 b 5 110 5 5
474. 6 31
475. 99 99994 99 99994 99 99954 0 1mg g 100 105 250 250 9 4 a 19 100 1050 49 0 01mg 10mL
476. 3mol L 100g L e 000000000000 25 63 4 00000 4 9 1 4 a f 5 a b 000 3 0 1 gF mL 100mL 200mL pH5 2 10mL 7 2 8 9 10 11 12 13 8 14 1u gF mL 100mL 10u gF mL 100mL 0 1mgF mL 100
477. DDDD 00000 1 D I 1 00000 e 00000 00000000 4 111111 8 a 00000 140
478. GC MS EC GC MS 5 GC MS 2 00 9 a 5 6 b PCB 000000000 1mg mL 5 q d 2 0 0000000 40 100 g mL 0 1 g mL 5q e 0000004 0000000 4000000 4000000 4 00000000 d4 D DDDUDDDD gue UDDD gea 0 0 3
479. Wa Ipole s Buffer pH 3 00 1mol L HCI 2mL 50mL min 0 5mL 0 1g L 1 200rpm 1mol L NaOH 5mL 3 212 5 14 2 5 a 5 14 2 1 5 a b 000000 50mL 0 1u gH g mL 0 1u gHg mL 4 8 j
480. 2 a 5 13 1 2 4 b 131 0 o 5 13 129 d 3 97 J IS K 8951
481. GC MS 5 7mL 3 500 700 8 4 3 a 00000000000 D 30cm 5g lcm 319 6 9 2 DEHA b 000000 SPC d 5
482. 52
483. Ul e 250amu 10 lamu amp 0000 14 ICP MIP b 0000 4 00000 5 1 1 4 b 5 00 a 0000 ICP
484. 3 000000 a 000000 b 00 0000 4 00000 5 1 1 4 a 5 1 1 4 b 5 102
485. 5 7 13 14 15 d 000000 6 00000000 5 1 1 6 8 gt 132 5 1 1 6 d mgNi kg
486. 6 1 000 0 1u gCr mL 0 50 10mL 100mL Q6 Iu 1 000 g mL 0 20 10mL 100mL N 1000 g mL 0 20 9 2 00000 23 10 50 L M 1 000 g mL Q4 357 9nm 25 8 5 12 1 1 4 b 19 o 5 12 1 1 4 0 22 o 23 D 24 25 eoe 26 d mgCr kg e 0000 mgCr kg 6 00000000 5 12 1 1 6 b 1 5 12 1 1 6 b 2 5 1 1 6 d 178 5 12 1 4 000000 000100 1 0000000 2 00 a 000000000 J ISK 8231 3g b 00000000000 209 11 JIS K 8247 100mL c 20096 1 JIS K 8731 209 100mL
487. e 000000000 50 500 L b 130 5 7
488. 5 a 0000 630nm b 000 4 5 1 2 5 b 00000 4 5 1 2 5 9 e d 000000 4 1 lg 6 00000000 4 5 2 1 6 g 39 4 5 1 2 6
489. 2 a 1 1 0 1 5 K 8848 b 1 01 00 415 K 8987 3 000000 a b 000000000 805 d DU D D 802 5 e 00000 80 C 5 C 30 0 0001g 0000 805 00000 0 00019 4 a 0000 32 200 309 0 019 5 6 500mL 80 2mL
490. DI 200mL e GF F 4 f 9 70mL 50vol96 5mL 100mL h 2 3 4 D 70mL 5 a 0000 650nm b 000 244
491. d 00000000 0 0 2094 1 JIS K 8019 29 100mL e 00000000000 0 10g L JIS K 8488 1 5 0 59 25mL 1 f 10u gCr mL 5 12 1 1 2 j 3 000000 a 00000 b 0000000 00000 d 00000 e 00000 4 00000 50mL 5 12 1 1 4 a a 3 3 0 59 0 001g 550 Gi 59 50mL
492. 20 4mml 1 50 2 0m D D 177 17 Loo N20 300 80ml min 180 250 9 1 Ooo 270 64 PCB 642 000000000 000000 000 1 0000000 PCB ECD 000 PCB 1 8 6 4 1 2 a b 0 6 4 1 2 9 6 41009 d 6 4 1 2 4 e 6 4 1 2 e f 6 4 1 28 000000000000000 6 4 1 2 9
493. 4 a 3 1 1009 0 19 1 1 50mL b 30g L 20mL 1 30g L 10mL c 10 3 d 40 C 10g L 10mL 20g L e 200mL f 5 3 e 5 5 a 253 7nm b 000000 0 1u gH g mL 1 20mL 1 1 10mL 250mL c e 1 1 10mL 250mL c Hg c 00000 2 Hg 0 11 2u g 1 1 10 11 250mL 1 10mL 4 5 3 253 7nm 6 gt 199 5 14 1 7 6 4 a d 4 1 mg H g kg 4 5
494. 03 20mL 5mL 20mL 10mL 50mL 100mL 100mL D 1 2 3 4 b 00000 0 1
495. 167 5 12 1 0 0 5121 51211 41 0000000 2 a 5 K 0557 3 0 D J 342 5 K 8951 0000000 d 715 8625 e 5 8562 f 5 otemt 1mg mL 50mL 1 000mL 1 1 2mL i 0 1mgCr mL 134 100mg L 000000 30 gcr mL l 0 1mgCr mL 10mL 100mL 12 1 2mL k 90 10u gPb 10u gCur 10u gZn 10u gFe O 10u gMn 10p 10u gMo 10u gCr mL 5 1 4 2 e o
496. 6 4 3 2 i 6 4 3 2 6 4 1 2 D 0000 EE 6 4 1 2 k 1 PCB 3 000000 e a b 6 4 1 3 b 000000 d 0000 e 6 4 1 3 6 f 00000 000000000000000 6 4 103 9 e413h i 1 0 0000000 0 2 0 7mm 10 j 60m 0 1 99 999vol 59 3 2 e 1 0u m 40cm sec 10 20 q
497. 225 6 1 20g wet 3 000rpm 10min 10mL 200000 3 000rpm 10min 250 50mL UU 00000 9 4m JD 0000 0 6mL 000 1 100 0 0 226 6 1 0 00000 0 00000000000000000 0
498. 6 2 234 0 311 9 389 8 469 7 547 6 627 5 623 5 152 1 232 0 309 9 313 9 391 8 230 0 467 7 471 7 549 6 387 8 625 5 629 5 621 5 625 5 0622 4 No DDT 12612 247 0 249 0 177 1 HCB 13Cc 289 8 291 8 283 8 dio 188 1 dio 212 1 p d4 244 2 d 5 2059 000000 _ mL 1 g kg ng x i zwet 1000 9
499. 1 200rpm 8mL e 1 200rpm 1mol L NaOH 5mL 3 f 5mL 10mL 9 h 0 1g L 1 200rpm 3 bmg L 2mL 2mL 3 1mol L 1 200rpm
500. 509 11 500mL 28 19 D 3 2 3 250 450 1 8 4 8 5 6 010 dil 14 H3Ce CB 13C6 7 2 3
501. 0 1ng mL 250amu 10 e lamu amp 18 MIP b 0000 4 00000 5 12 1 1 4 b 1 5 12 1 1 4 b 2
502. 1094 100mL 1mol L 1L 0 1mgSb mL WI NaBH410g 134 g 1 h 100mL 3 8 Q b 00000000 11000 0 Ou gSb mL 000mL 100mg L 1510 0000000 0 1u gSb mL 0 1mgSb mL 10mL 1510 00000 00000000 Lu gSb mL 10mL 0000 DELETE HI 000g
503. 5 a ICP 257 610 259 373 260 569nm 1 2 1 5kW 16L min 0 5L min 1 0L min b 10u gM n mL 0 UT 20 2 100mL 00 20mL 100mL 2 10 9 90 10u gPb 10u gCu 10u gzn 10u gFe 10u gMn 10u gNi 10u gMo 10u gCr mL c 00000 3 G 100mL 0 10 0 5mol L ICP 4 5 6 3 5 1 1 4 a O 5 1 1 4 b oo 3 4 100mL 50u g mL 10mL 451 131nm 10u gM n mL 0 1 20mL 100mL 50u g mL 10mL 451 131nm 5 6 gt 119
504. 64 PCB 64 6 43 6 44 641 0000000 000000 00 41 0000000 PCB ECD 000 PCB a 1L 100mL 8
505. 5m 00000 00000 0000000 Es U D im 10 O0 10mL GC MS SIM GC FPD 296 6 6 8 2 ee 200000000 300
506. e JD 0 1 gAs mL 5 9 1 2 k 3 a 0000 000000 b 00000000
507. 000000 b o 0000 4 5 1 1 4 a 5 1 1 4 b 5 1 1 4 5 a ICP 228 802 226 5020 214 438nm 1 20 1 5kW 16L min 0 5L min 1 0L min b 10u gCd mL 21 0 11 20mL 100mL c 20mL c 21 10u gCd 10u gPb j 10u 9 10u gzn 10u gFe 10u gMn j 10u gNi 10u 10u gCr mL o 00000 22 100mL 0 1 0 5mol L ICP 228 802nm 23 24 25 5 1 1 4 8 2 0 5 1 1 4 b 0 5 1 1 4 c 22 23 100mL 83
508. HPLC LAS 2 LAS HPLC DDU UU HSS 00000000 15cm 00000 O GCB 101 0101 000000 0 uuu 4 6mm 25cm ODS 10u m 248 6 31
509. m 000000 00000000 2mol L 2 10mL 20mL 20mL 3 20mL 20mL n 10mm 0 2mol L NaOH 1mol L HCI 10mL 0 9g 4 o p q r s t 9959 00000000000 dxz0 00 e0 9959 dz 9996
510. 10000 660nm 193 5 13 5133 1 0000000 2 a D 115 K 0557 A3 b 1 00000000 p oaimt 1 000mL d 0000000 1 000mL 1mg mL 1mL 1 1 2mL 1u g mL 1mg mL 1mL 1 1 2mL e 000000 2 Su gB mL 5 13 1 2 g 0 1mgB mL 10mL 25mL
511. 100mL uugugmumnauudaunmtu 309 1 209 0 1mol L 1L 134 100mg L 1 1 20 0 1 gAs mL lk 0 1mgAs mL 10mL 1u gAs mL 10mL 1 000mL NaBH410g 100mL 1 1 2mL o 0000
512. 196 0nm 5 1 1 4 b O o 8 9 10 11 12 d 000000 o 00000 mgSe kg e 0000
513. 4 eno 3 5 d 00000 mgM o kg 0000 mgM o kg 6 00000000 5 1 1 6 a 5 1 1 6 d 583 1 2 a 5 K 0557 D b o 0000000 50 om 1mg mL 50mL 1 000mL 1 1 2mL d 0 10u gMo mL 5 8 1 2 f 0 1mgM o mL 10mL 100mL 1 1 2mL e 10 gCd 10u gPb 10u gCu 10u gZn 10u gFe 10u gMn 10p gNi 10 u gMo 10u gCr mL 5 1 4 2 e 3 000000 a 000000 9 0000 137
514. i i 1000 om N j 0000000 0 1 134 100mg L Kl Ou 0 1mgCd mL 10mL 1 000mL 1 1 20mL 00000000 0 1 gcd mL 100mL 1 1 2mL 3 a Lu gCd mL 10mL nm e 0000 5 000000 e 0000 e 00000000000 71 5 1
515. 4 00000 5 1 1 4 8 5 1 1 4 b 114
516. 40mL 4 40mL 5 207 200g L J20mL 5 14 2
517. 10006 1 Amt 25mL 10g L As 193 696nm Se 196 026nm Sb 206 833nm 000 mgkg 99 3 aq 0000000 ArCI 146
518. 13 2 4 61 1 0 41590 JIS K 9704 2 2 1 3 0 291g 1L amp f 15mmol L 0 5mol L 6 30mL 1L 25bmmol L 0 5mol L 50mL 1L 0000000000 0 1mgF mL 4 9 1 2 f i 0000000000 0 1mgF mL 25mL 100mL 16 30mL 500mL 1L 66 3 000000 a 0000 b 0000 00000 11 2mL d 17 o 000000 ani e 0000 17
519. 1u gAs mL 0 1 2mL 49
520. 301 6 6 8 0 6 6 1 000000000
521. 000 Ou g mL 5 1 3 2 9 gSb mL 5 11 3 2 0 e 15 e e 000000 lamu 6 35 250amu 0 1ng mL 10 ICP b 0000 MIP gt 165 5 11
522. 224 6 1 8 10mL 8 8 d uu 4 1 96 19 E mL 1 g kg ng x mW 9 a
523. 5 13 6 00000000 5 13 1 6 b 1 b 2 ngagagi 300 1 Rh lu g mL D D D 0 0 0 5mol LD 196 5 14 1 5 14 00 5 141 000 5 14 11 1 0000000 2 00 a 0 0JIS K 0557 A3 b DDDJISK 8541 0 1 g L 9 uas 1 JIS K 8951 1 1 g L d 00000000000 20911 JIS K 8247 015g 500mL e 3006 1 IS K 8731 50g 500mL f 20094 JIS 82
524. 1 900 300 100 592 1 0000000 20mL 25mL 200g L 2mL gt 20mL J 25mL DUDU DU 0 1094 DD 5 193 7 Se196 0nm Sb 217 6nm 193 696nm 2 a 1 1 5 K 0557 A3 b DU 00000 100mL d O000000000000 0 0 0 10g L 0 5 9 1 2 h 4mol L JIS K 8506 11 9g 144
525. 20 e 0 eo e o 4511101010000000 GC MS ng 260 C uu GC MS 218 o 00000000 GO 6 3 18
526. g kg 1 1 1 2 0 0000000 g kg 1 1 10 1 00 0 g kg 1 g kg 1 13 g kg 1 g kg 1 g kg 1 12 g kg 1 12 g kg 1 g kg 1 g kg 1 g kg 1 1 2 0 0 1 3 0 0 0 g kg 1 0000 u g kg 1 g kg 1 g kg 1 g kg 1 1 1 g kg 1 00000000 8 g kg 1 g kg 1 g kg 1 g kg 1 g kg 1 g kg 1 0000000000 CNPO g kg 1 Hu u g kg 1 11 0 0 g kg 1 g kg 1 1 1 0 0 g kg 1 g kg 1 g kg 1 g kg 1 g kg 1 g kg 1 g kg 5 g kg 5 g kg 5 g kg 1 Lu utu u g kg 1 1 1 00000000000 3 1 D Lu mulu 1 1 0 0 000000000 0 MBASH mg kg 1 mg kg 1 mg kg 0 05 PCBs GC ECD mg kg 0 01 PCB u g kg 05 0 005
527. m z 16 m z m z 11 m z d mgM n kg 6 5 1 1 6 8 b 5 1 3 6 a 564 1 0000000 279 5 2 a 15 K 0557 b 000 0000000 Ou gMn mL 5 6 3 2 e 3 000000 a 000000000000 o 0000 e 0000 e 000000 e 0000 000000000 e 0000000010 50 500 L b 0000 4 00000 gt 122
528. 100mL 305 67 4 6 7 4
529. MSO DODO msh 1 1 11 1 1 g kg 0 5 0 005 u g kg 05 0 005 u g kg 05 0 005 u g kg 05 0 005 u g kg 05 0 005 u g kg 05 0 005 u g kg 05 0 005 u g kg 05 0 005 u g kg 05 0 005 a 000 H g kg 1 8e u ul g kg 1 g kg 1 000 u g kg 1 p p LU u g kg 1 pp 000 u g kg 1 pp 000 u g kg 1 g kg 1 00000 0 H g kg 1 g kg 1 g kg 1 00000 u g kg 1 g kg g kg g kg 1 g kg 1 trans 0 0000 g kg 1 dst 0000 g kg 1 g kg 1 trans 0 0000 g kg 1 dst 0000 u g kg 1 g kg 1 g kg 1 g kg 1 DUDU H g kg 1 g kg 1 g kg 1 g kg 1 g kg 1 g kg 5 Bla P g kg 1 1 1 4 1 DUDU UU 111 1111 Daupnaupnaunp g kg 0 3 u g kg 0 3 81
530. 100p g mL D 0000 20 m dull 1 PCB 2 280 6 4 PCB 6 4 5 00000 PCBO Wellington Laboratories BP WD PCB PCB Congener IUPAC No 2 Chlorobi phenyl 1 4 Chlorobi phenyl 3 2 6 Dichlorobi phenyl 10 4 4 Dichlorobi ph
531. 115 K 0557 0o00 50 om II 6 1 000mL 10p gPb mL 5 2 1 2 0 1mg mL 50mL 1 1 2 1 3 20 e 3 8 D ut 0 1mgP b mL 10mL 100mL 10 gCd 10 gPb 10u gCu 10u gZn 10 gFe 10u gMn 10 gNi 10u gMo 10u gCr mL 5 1 4 2 e D ut D ut 90
532. 176 5 12 1 3 1 0000000 357 9nm 2 8 5 557 3 b o Du d 60 0 e 0000000 i D 300 gmL f 0 1 5 12 1 1 2 i u gCr mL 5 12 1 2 2 1 gCr mL 1u gCr mL 10mL 100mL 1 1 2mL
533. 2 00 a b 2mm 3 00000000 3100000000 DUDU 2mm 17 33 0000 a 1050 110 b 1050 110 C 1 1 109 10mm 2 00
534. 50mL 950mL p 00000 1 q 6381010 0 r 00000 9 1 17 Sep Pak Plus C18 Cartridges Sep 16 16 17 ds 2 4 16 16 4 t 000000 d u Uu ay 1 0 L mL 178 Pak Cartridges Florisil A 0 1u g mL 2 4 16 16 339 17
535. 010 e f 00000 g 0000 LI U 10u g mL 3 500 700 8 4 5000 5 w v 5 w v 60 100 130 16 100g 000000 300 2
536. 1 9 206 833nm 5 11 1 4 a OI o 8 9 d 162 mgSb kg 60 00000000 5 11 1 6 a 5 9 2 6 a 5113 000000000 1 0000000 N 217 6nm 2 a 1 15 K 0557 A3 b 0000000 00000000 1u 5 11 1 2 f 1 000mL e 3 000 gmL
537. 3 r3 maa mla mla 11 11 1513 CO 1 ma o0 mla mla Cl cag r3 c3 o2 e augu zlajz c S lng 1 orlo fgagaoo loojoo aoao aoaaa gt 1 ooga Cl oloo a ogo Ajo
538. 7 3 a 0000 b 0000 d 6 451 0000000000 GEN 8 0 250 0 3mm 30m 5 0 10 1 5u m 99 999 0159 20 40cm sec 35 300 0 5 C 150 300 200 300 e 70V 0000000000 GCU 293 4 a b 6 5
539. f DDD tn J IS K 8150 58g 1g 500mL 2009 1 pH 11 0000000000 0 1mgF mL 4 9 1 2 f JIS K 8355 115 K 8284 100mL pH5 2 og gF mL 200mL i 0000000000 p 9 mt 200mL j 0000000000 0 gF 200mL 6 500mL JIS K 8355 JIS K 8150 10u gF mt 20mL 0 1mgF mL 20mL 1u gF mL 20mL 58g 1 2
540. g kg 1 0000000 u g kg 1 0000000 u g kg 1 g kg 1 4 1 g kg 1 g kg 10 g kg 10 9 9 10 1 01 g kg 25 g kg 10 g kg 10 9 9 25 g kg 10 g kg 10 000000 2 0 0000000 u g kg 10 000000 MU DUDUDUD 9 9 5 4 g kg 5 4 g kg 5 4 g kg 5 4 g kg 5 4 g kg 5 g kg 50 g kg 5 24 g kg 5 g kg 9 DUDU 4411110000 H g kg 1 110 00 4 1100 g kg 1 4 1100 g kg 1 4 g kg 1 4 H g kg 1 4 g kg 1 g kg 10 g kg 1 24 g kg 1 g kg 1 1 g kg 0 01 178 9 9 0 01 11 1 1 u g kg 0 01 2 0000 1 000000000 0000000
541. j 12mL lg k 5mL 5mL 000 00 00000000 100mL 200mL 200mL 500m L 20mL m 000000 10 n 0000 o 000000000 10 L 257
542. 0 019 200mL b 10mL 5g 1 29 29 I 451 200 d 300m i 0 0 0 500mL b 0 000 NG 000000 000000 d 00 0000 D 300mm d 6000 DD 0 500 U 451 1 00000000 e 00000000 453 100000000000000000 50 00000000 soom 50 8 60094 0 0 000000000000 00000000 50 7m m
543. 03 0 opge 200 0 2000 L 050 B DOT 150 1000 L 189 5 13 b 0000 b 1 00000 0000 1g 0 00190 0000 0000 200mL 10mL Amt 10m 1080 000000 149 10mL 10mL 10m 20000 uuu 30011 5mL 1 1 5m PPO 0 PE RT EE uuu 10 PRI DUDU b 2 00000 0000 0 11 19 0 001g 0000 5mL Amt 3 10mL 51 B 100ML 00090 gt 190 5 13 UD 0000 000000 100ml 0 10 0 5mol L0 0 D n 50u g L 10mL gt 100mL 208 9590 249 7730 249 678nm UUDUUDUUDU mg kg 191 5 13 5132 1 0000000
544. 1 DEHP b DEHATI 1 Hi 2 1mg mL 1mg mL 0000000 DEHA diri 0 1mg mL DEHA 0 1 g mL d 00000 0 1mg mL dio T DEHA 1mg mL 5 C 1mg mL
545. 10 5ng 178 16 16 17 347 15mL 6 11
546. 357 9nm 77 51 2 1 0000000 228 8nm 2 a 5 K 0557 A3 b 000 00000 d 00000000 10u g mL r 5 1 1 2 500mL 1 3 10 3 a 000000000000 0 1mgCd mL 50mL 0000
547. 0000000 4 8 4 b 2 5 5g Fro 599 2 0 3099 Fr 3 3058 Fr 3 3 5mL p p DDE p p DDT 2u g 5mL 20mL GC MS p p DDE pp DDT pp DDE 4vol 100mL p p DDT 15vol96 150mL 4 Fr 1 5 15vol9q 150mL 5 a 000000 2 GC MS GC MS GC 590 6 0 25mm 30m 0 25 m 238 6 2
548. 2 5mL 9 15vol96 1mL 10mL 13 15vol96 D 15vol Yo 8mL KD 10 50 L 14 8 50mL 2 0g 50mL 9 15 30cm 50 2 LT du 10 11 10 12 80 90 13 15vol Yo 10mL 14 KD 10 50 L MS 00000000 60mL 5mL 342 6 11
549. 24 GC 10 GC 25 SIM 26 27 317 6 8 6 00000000 000 100mL 20g 30 51 D 1000 3 000rpm 1000 000 000 30 500 100 3 000rpm 1000 318 69 2 1 0000000 6 9 E en DEHA Du DEHA 1 2 00 a 1 0 0 PCB DEHA DEHP
550. 3 620nm d 4 1 96 lg mgF kg 6 6 00000000 aul ul a 000 20 59 0 01900 40mL lmL 40mL 0000 19 0000 340 1100100 00 0000 30 5mL min b DUDU 30mL 50mL 00 0000000000000 01 20m 62 492 1 2 a 115 K 0557 3 4 9 1 2 0 4 9 1 2 o d 0000000 4 9 1 2 9 4251 6 e 0 209
551. 48 000000 6 00000000 D 3100000000 50 10g 0 01 90 0 0 5 0 U 250mL D 59 11 0000 0000000 DUDU DUDU 0000 000000 200mL 0 g L 20mL CT EE aoa GIG CET NO 10mL 0000020 3 min 00000 350 0 U 19 0 10 1 5001 150mL 0000000000000 5911 0 0 100g L lmL 56 100mL Og L 20mL NO 10mL D Uu DU UU D 3mL min 0 0 0 90m 100mL 25mL CN 0 50 ou 9 0000000 50 mi 10mL mgCN kg 482 1 0000000 00 0000000000 250mL 2 00 a 5 K 0557 5g L 0 4 8 1 2 0 00000000000 Q
552. 6 30 7 50 C 100mL 500mL 150mL 5g L 100mL uU uU e 90mL 1 op 10 2 EDTA 100g L 1mL 35mg 3 EDTA EDTA 4 3mL min 5 15mm 6 100g L 1mL 4 9 7 pH 54
553. 10 100mL 15 6094 105 2 3 f 0000800000 000000000000000 50u m 00000000000 i j 250 60 0 5 30 120 200 5 000 L 000000000 105p L m
554. Tanah gt amad agoa mang COD oc pc Mes es lees EIS Mes es lees ES ee Do Dr o0 CH o0 o o0 o mad Tm EE fan OO o a 3 3 0352 3 0 3 513 2 223 oo ma oo Ta DOG Di na em a DI GC aH agaat Ui 9 Cpmmmbo3 L3 pc i a 1 a a E m m wa RR n n EX a ah i E el CID r8 a aga atam ata ma ma CID pnr a O OO OO O O OO O O O O dol 09 04 3 qi DIE Di 2 2 r ra A m O r3 r3 r3 Leed E e e sr CH en in in i e m ein edo mst edomsr edoamsr edowm damsrin B S pma dei ri Ir m m ist S S Dun ui DO 2 2 GO Dr rrr 106 do AAAA mud A an an ana om mum mum mme I H IHH pd L m tn m Es 63 o EZ 71 197 206 215 226 235 243 253 262
555. 0 11 1 0 m 99 999vol 20 40cm sec 35 230 0 50 35 230 0 50 150 280 C 200 270 50 100 400 50 100 C min 250 280 70V 1 DB 5ms Restek Rtx 5 5ms Supelco SPB 5 SGE BPK 5 4 00000 a 0000 20 309 5mL did 2u 9 100mL 50mL 10 e 10 3 000rpm 10 3 5 500mL 1L 50mL 10 2 0 5mL b 1 1 0 0 0 100mL 100mL 2 2mL 2mL 0000000 3 2 ds dio Lu g mL 1mL 1mL 328 6 10
556. 00000 NCI 1pg 150 C 250 C SIM 00000 6 1 2 30 6 11 2 170 17 b ooo BO CO 10mL 500p L 0 1p g mL 500p L 3 10vol96 2mL 2u LU GC MS o 00000 3 Gi 5 8 15 GC MS 10 6 12 2 TMSO 90 17a 17 m z 253 m z 277 m z 257 349 6 11
557. 40g L pH 40g L 1435 pH 3 3 5mL 20 40 15 4 e 880nm 710nm 3 pH p 1 g L 4 1 V lug 0 35 9 00 2 III 0 03g d O00000 4 1 90 19 mgP g 46 46 000 6 00000000 a 1 0 3100000000 e 1 0 19 0 019 00 DUDU 0000 100ml DH 10mL 5mL ERA gt 100mL 10mL 5mL Jut 0 0050 0 04mg 0000000 5011 000000000 2009 L 0000000000 409 L0 00010350000000 40mL eor 5 DUDU D 30mL 3 5 uuu 50mL uu gt 880 0 710nm 1 D D 4 b 0000000000000000 0 000 3100000000 0000000 39 0 039 0 DUDU D 30mL 0 1000000 000000 00050 B 48 1 0 H 100mL 46 6 a 00 0000 47 1 0000000
558. D 10 10 2mL 0000000 200g L0 15mL 5 UD 000 25 00000 100 111 1 Sot 510nm mgAs kg gt 152 5 10 5101 000000000000 1 0000000 196 0 2 DD 8 1 5 K 0557 A3 d D as 00000 1000 10g L 0 0 1mol L 1L d ULmgeimt
559. e D 0p gSe mL 1 000mg L 1mgSe mL 10mL 1 3 20 f 000000 0 1 95 8 11 10u gSe mL 10mL 3 1 20 3 000000 a 00000000 NaBH410g 1 000mL 1 000mL 0000 e 00000 ne 5 000000 e 0000 1 o 00000 e 00000 00000000
560. mL 100 1 50 Wio W g mg kg 0 0 0 ng x 0 10 20 30 40 50 60 70 80 90 min 6 3 3 259 6 3 2 0 0 000090000 0 Oo 45
561. x0 280 ues V W mgN g 10mmol L mL 10mmol L mL 10mmol L 5 V mL 9 280 10mmol L 111 mg 4 2 b 25mmol L 100mL 250mL 5 2 b 25mmol L 00 3 2 6 25bmmol L 500mL 25bmmol L 6 50mL 5 7 4 0 50mmol L 7 25mmol L 50mL 150mL 5 7 25mmol L 50mmol L mL 4 1 96 19 4 5 1
562. 1 3 5 TPCH 2 010 di9 B a P 1 2 011 1 3 ds DPP d3 1 2 ds G s DPCB d3 trans 1 2 ds rans DPCB d3 2 4 il ds DP B ds 2 4 L dio DPB 010 2 4 6 1 ds TPH dell 2 4 6 1 dis TPH d 5 1e 3e 5a ds 16 36 56 ds 1000 0 100g 100mL B a P 100mL 1 000 g mL i U 1 100p g mL r 1 000 g mL 10mL 100mL 100mL 100p g mL 1mL 100p g 7 p 1 000 gmmL r tn 000000 0 1 000 0 100g 100mL B a P di2 100mL 1 000 g mL 1 000u g mL 0000000 300 gimL r 2008 U 3 000 g mL 1 000u g mL 10mL 100mL 100mL 100p g mL 100u g mL D 8 30cm 559 3 5g 2cm 10mL m 7mm 60 80 2cm 299 0 3 8 6 6 3 504111
563. 10 2 00 a 5 K 0557 A3 b 000000 qQ2mol L 4 5 2 1 2 b c 4 15 K 9066 4 gl JIS K 8180 60mL 80mL 200mL d 000 N 1 0 0000000000000000 394 1 115 K 8197 N 1 N 1 0 2g 200mL e 00000000 0 JIS K 8019 105 1100 100 4 93g 1L f 000000000 0 24 gN mL 1mgN mL 10mL 1L 10mL 500mL 3 a b 1 00000 4 5 2 1 4 8 b 100mL 4 5 2 1 4 a b 5 00 a 540nm b 1 2 gN mL 1 10mL 10mL 10mL 4 5 3 1 5 mgN o 0 20 2u g 10 1 10mL 40 4 5 3
564. 1mol L NaOH 5mL 0000 130 0000 1 200rpm 3 D D u aat 1mol L HCI 20 Wal pole s Buffer2mL 0 191 0000 0 0 0 5 1 R Thermon H GO 0 53 DU 15m0 N20 4 5mL min 150 ECD 1919 kg 214 6 1
565. 200 30 g wet 5 50mL x 3 596 NaCI D 0000000 50m pn sm 000 0 0 5mL 0000000000000000 100m 100mL 0 0 U 000 D 2mL N O bis trimethylsilyl trifluoroacetamide 200p L 461 9 4 1 0 99 tu 90 D 332 6102 000000000000 1 000000 6 10 2 0 d e f 9 h i j k l m 0000000 3 a b GC MS 100mL 1mL 100mL 1mL 100mL 1mL
566. 20vol 10mL 50vol 5mL 1mL e 10 g mL 20 L 1mL f 4 1 a 4 1 b 3 4 5 6 5 a 230 6 2 1 GC MS GC MS GC 5 7 0 25mm 30m 0 25 m 70 C 2min gt 10 C min 200 C5 8 C min gt 12 Qmin 280 C 7min 250 60sec 10 psi 0 25psi min 16 psi 8min MS E1 70V 270 C SIM gt 220 C 3min 10psi gt 80psi min 30 psi 0 5min gt 80psi min PFTBA PFK m z 2 18 300
567. 220 28050 200 SIM 05 00000 mit 149 mu 177 n 209 209 223 237 n 251 2 167 167 206 153 mu 4 01 130 dd 136 did 164 dig 188 did 212 dii 240 di 264 b ee GPC 2 lu LO GC MS 5 1 ULI GC MS 5 o 00000 10 2u LO GC MS d 14 LU GC lu LU GC mL 1 kg ng x x x1000 ng uL wg 9 209 1 4 29 lu LU GC 316 6 8 700 130
568. 50mL 100mL 5 1 39 50mL 2 100mL 5 200mL 24 3 a b 4 00000 4 5 2 1 4 8 b 100mL 4 5 2 1 4 8 b 42 4 5 3
569. 6 00000000 5 1 1 6 a 100 mgCu kg 5 1 1 6 d 5 4 UI 5 4 1 1 uuu 5 4 213 9 2 8 b D 0 5 K 0557 A3 D 0 92 134 3 a DUDU 000000000000 100mg L Uu
570. 000000 209 100mL 5 6 50mL 5 10 3 000rpm 10 2 5 500mL 7 1 000mL e 100mL 6 30 10mL 5mL b 0000000 320 6 9 2 DEHA
571. 00000000 5 1 1 6 8 b 5 1 4 6 a 5 5 3 00000000 1 0000000 ArO ArN 2 a UJIS K 0557 A3 b 1 9 Ou g mL 1mg mL 1mL 1 000mL 1 1 2mL d Ou g mL 1mg mL 1mL 1 000mL 141 2mL e 10p gFe mL 5 5 2 2 0 f 9690 1u gPbr 1 gCu 1 gFer 1u gMn 1p gNil Lu oho 1 u gAs 1u gCr mL 5 1 3 2 f g 5 50ngPb 50ngCu 5OngZn 5OngF ell 5OongMn 5OngNi 50ngM d 5O0ngAs 5O0ngCr mL 5 1 3 2 9
572. 0019 DD 000000 000 600 25 C9 20 D 0000000 0 001 g0 00 a b mc a ai 4 3
573. 10u L 30 cm 15 mm 10 9 2 cm 100mL 30cm 10mm 5g 2cm 40mL 0000000 30cm 10mm 2 594 109 30 Yo 2cm 30vol94 30mL m 5 0 2 0 7mm 10 30m 0 10 1 0 m 99 999 500 350 9 00000 70V 4 00000 a 0000 2 200 100mL 10ng 100ng 1 50mL 10 10 3 000rpm 10 3 559 500mL 1L 50mL 5 2 237 6 2 KD
574. 19 0 001g 5mL 6 2mL 3 6 100mL 2mL 50mL 100mL 100mL 5
575. 1u g mL 5mL 00000 9 100mL 1u g mL 5mL 0 1 0 5mol L ICP m z ao 11 5 1 1 4 a O 5 1 1 4 5 2 ORO 9 gt 129
576. 21 22 23 5 a 45 1 I GC MS 8 888 GC MS 5 0 25mm 50 C 2min 30m 0 25 m 10 q min 2700 210 250 10min 6056 1u L He 4 EI 70V 315 6 8
577. 225nm 300nm 100 500h L
578. 300 227 227 324 17p ds 303 17B d4 304 012 240 b nngee A 1 0 g mL OT 50 L 1 0u g mL 50u L 5 0 11 0 5mL 2 LU GC MS 1559 1559 GC MS 15 GC 17a 17B 343 6 11
579. 5 1 1 2 d
580. 5 5 Heptachloro 13C 12 bi phenyl 180 2 2 3 3 4 4 5 5 Octachloro 3C bi phenyl 194 2 2 3 3 4 4 5 5 6 Nonachloro 3C2 bi phenyl 206 2 2 3 3 4 4 5 5 6 6 Decachloro 13C 2 bi phenyl 209 3 9 a 00000 3 2 000000 d e 6 43 3 6 000000000000000 0 0 6 4 1 3 9 6 4 1 3 h i 6 4 2 2 i p 000000000 70V 3 4 GC GC 4 00000 6 4 1 4 100 100ng 6 4 1 4 5 00 e a GC MS GC MS 000000000 GC 5 10059 0 25mm 30m 0 25 m 282 60 C 2min 20 C min 160 5 C min 300 C 5min 250 C 6 4 PCB 90sec EI
581. 6 800 90 7 8 10mL 9 5 a 6 5 348 6 11 GC MS GC MS o 000000000
582. 70V 4 00000 a 0 0 32 209 200mL 11 Q 3 100mL 1mol L 100mL 3 000rpm 10 1L e 100mL 6 100mL 50g L 50mL KD 12 lmL b 5 5mL 20mL 100mL 14 15 KD
583. 90sec 2u L 1mL min 36cm sec ECD b PCB 1 2u L 6 4 3 6 4 4 4 10 2u L PCB c 000000 PCB CBo 96 6 4 3 6 4 4 Gi 6 4 3 6 4 4 6 4 3 6 4 4 3 CBo 96 e CBo 96 272 20 Time mim 3 U 6 4 3 834 9 64 PCB 0 6 4 3 5 cB 1 D 1 CBo96 IUPAC No Structure 1 034 10 434 s 712 3 5 2 3 5 Ess 235034 3l 88 5 21 20 3315 2 34 23 4 23 3 23 0 392 2255 2235 224 5 1 2 4 5 2 4 4 6 2 2 4 412 3 5 6 334 2 2 3 5 2 3 3 6 122 34 3 4 4 71 0 791 235572346 x 12 3 4 6 2 34 5 2 2 3 4 2 4 1508 KEES 98 0083 2 2 4 5 672 2 3 4 6 70 3 549 ES 95 121 88 2284 _ 22 3 5 6 2 3 4 5 6 2 2 3 4 6 2 3 4 43 3 5 5 2346 TT 3 34 2 3 3 4 2 2 3 5 5 12 22 3 3 6 2 2 3 4 5 22 445 123 446 712 2 3 4 5 2 2 3 4 5 23 4 5 6 2 3 3 5 572 3 4 5 6 2 3 4 4 6 2 2 3 4 5 22 34 452 44 56 12 3 3 4 6 NGAN
584. bep de UD 13D 30 Bp
585. 0 d5 62 91 126 d 98 133 10000 55 70 83 112 49 77 PA atu 91 126 Cep OD DD DD 97 132 43 86 TBC DU D D 88 57 58 1 2 0 0 0 D de 64 000 105 119 134 13 105 119 134 4 1111010100 105 119 134 1210000000 75 111 146 14812 115 150 152 13 75 111 146 148 13 4 115 150 152 123000000000 109 145 180 182212 230 000 00D UU d4 148 183 185 124000000000 109 145 180 1821241100000000 93 148 183 185 1 3 5 00000000 109 145 180 182 1 3 5 000000000 d 148 183 185 44 76 78 190 224 225 260 0000 1 30 0 0 194 229 264 1 1 117 119 165 167 227 6 2 1 62 6 2 1 EN 2 DDVP BPMC IBP MEP CNP
586. 0 10 10mL 100mL 1 g mL 5mL 2 10mL 100mL 1 g mL 5mL c 7 1 gCd 1u gPb gCu 1u gzn Lu gFe 1u gMn 1p 9Ni 1u gMo 1u gAs 1u gCr mL 5OngCd 50ngPb 5O0ngCu 5OngZn 5OngFe j 5O0ngMn 50ngNi 50ngMo 5 50ngCr mL 1u g mL 1 g mL 5mL 00000 100mL 1u g mL 5mL 0 1 0 5mol L ICP m z 10 5 1 1 4 a O 5 1 1 4 b 2 o 89 d 5 2
587. 1 09 0 001g 550 2 2 o0 30mL 5g 900 3 200mL 4 50mL 5 1 1 15mL 100mL 6 7 2 3 O 4 5 6 D 7 50mL 200mL
588. 1 3 4 d 000000 mgCu kg 6 00000000 5 1 1 6 a l 5 1 2 6 8 532 0000000000 1 0000000 324 754nm 2 a 0557 b 50 g m
589. 10 1N KOH 5mL 70 5 000000000000 8mL 6 0 5p g mL 1 0mL 7 10mL KD 3g 0 7mL 3mL 8 4vol96 1mL 4vol96 10mL 4vol96 8mL 9 0 5mL 00000000 334
590. 1000 g mL II 0 1mgPb mL 134 100mgPb L 0 1mgP bim 10mL Uu 1 000mL 0000 Uu 0000 5 500 L
591. 1CH3 mt D 10094 1 009 1 000mL 0 0019 NaOsSO CH 2 10 g NaOsSO CH2uCHs mL u CH 3i mL 10mL 3 0 00000 a b i DDU lt 1 000mL 15cm 00000 1 100mL 10mL 25mL 30
592. 20 1 x x 100 200 x 0 002650 g x 25mmol L mL 0 002650 25mmol L 1 11 9 110 0115 8962 d O00 K 8983 e 0 115 K 8863 509 11 f K 8896 0 029 JIS K 8840 0 10g 95 100mL 00000000 oogL n JIS K 8576 JIS K 8102 250g 500mL 3 451 1 4 00000 8 3 3 1
593. 20 1 5kW l6L min 0 5L min 1 0L min b 000 0 1 gAs mL O 5 5mL 50mL 1mol L e 5mL 50mL 1mol L cen 00000 3 100mL 8mL 1mol L 8mL 50 50 Q 50mL ICP 2 10g L 12 1 6mol L 13 193 696nm 200mL 5 9 1 4 a O e 145 32 13 d 000000 mgAs kg 6 00000000 5 9 1 6 a a 000000 cPr Asi Se Sb Se As Sb 1 000000 sm 1 1 20mL 90 0 1000 DUDU 25ml
594. 20mL 100mL 50u g mL 10mL 2 451 131nm 4 5 103 5 4
595. 2cm 50mL 50 95 50mL 130 15 95g 5g 30 15 12 10x 300mm 5g 5 5 2cm 50mL 20 98 50mL 5g 5 95g 321
596. 400 1 500mm 1 180 250p m 2 5 2596 JIS K 1107 99 99v 96 300 80mL min 140 240 C 130 140 180 C 200 C 40ng 4 a b 0 d e f 9 S N 1 1vol96 2 1 100
597. 5 11 1 4a j 5 1 1 4 b 2 e og 000000000 1 000 1u gSb mL 1 10mL 100mL 14 Il 1 000u g mL 1 000u g mL 9 0 20 10mL 100mL N 1 000 g mL 3 000 9 Cl AG 6 2 00000 3 10 100 50 L 1 1 000 g mL 3 000 g mL Wi 32 217 6nm 13 5 11 1 4 8 2 5 1 1 4 5 2 e og D 10 11 12 164 13 14 d 000000
598. 50vol 5mL 5 50vol Yo 5mL 40 C 5mL 1mL 3 1mL 30 0 5mol L 10mL 10mL 10mL 5bvol96 2 5mL 10mL 2 10mL 3 5vol 10mL 13 0 2mL Lu g mL 20 L 294 6 5 00000000
599. 8 9 0 1mol L 0 1mol L 10 24 I 43 000 6 00000000 ERR 0000 O00mLU 000000 EI ELE CC E 2ESLE ad 1 000 20 5 9 0 0190 00 3000 500 1 1 200 30mL 1 1 0 0 200mL0 U U 100g L 20mL 0 2 50 3mL min 300 10mmol L 25 mL 10 10 2mL l0mmol L 00000000000 Daupngaupnaunp 0 0980900 0 1 080 25 4 4 44 0 0 000 000000000 0 0 0 sedi 1 CODsed
600. C min 300 C 30min 250 C 40cm 60sec 00000 MS El 70V 230 C SIM m z 18 300 1 amu 105 182 4 137 91 did 188 did 192 ds 128 309
601. Lol 0 001g 200mL 20mL 300mL 1g L JIS K 8842 0 1g 95 100mL 130 5 50mmol L 5O0mmol L f f a TM s SES 100 200 2xx0 004855 a 9 b 90 50mmol L mL 0 004855 50mmol L 1mL g 32 I 451 000 6 00000000 000 3100000000 0 230 30mg0 0 0190 0 0 0000000000 200 DH 10mL 000000 59 1 1 29 3000 000000 200mL 200mL DUDU uu 00000000 300m 500 50mL 5070 D 500g L 0000 100mL 20mL 33 45 12 000000000 1 0000000 4 5 1 A3 2 a JD 115 K 0557 b 45 1 1 2 0 1 0 1110 00 4
602. Lu gNi 1u gMo 1p gAs 1u gCr mL 50mL 1 000mL 1 1 20mL 3 a 000000 e 000000 16 0000000000 0 1ng mL 000000 5 250amu 10 lamu e 0000 16 ICP MIP b 0000 4 00000 5 1 1 4 a b 5 a ICP 80
603. did 212 b 000 DEHA lu LU GC DEHA 5 Q DEHA 010 lu L GC DEHA dio 5 DEHA DEHA ds 00000 10 2u LO GC MS d 000000 lu L GC DEHA 322
604. trans DPCB ds 2 4 1 ds DPB ds 2 4 1 dio DPB dio 2 4 6 1 ds TPH ds 2 4 6 1 dis TPH 615 1 36 58 gt 0 1e 3e 5e ds 12 30 13 PR 60 100 130901 15 1 FLO LC gt Florisil 5 10g 30cm 7g 2cm 1 14 5vol94 15 GC MS 5 a GCIMS 06 GC MS GC MS 000000000 GC 50 0 20 0 75mmf 150 30m 0 10 3 0 17 18 19 250 C 4 302 50 C 1min 20 C min 300 C 30min b 0 6 6 a 2 3 60sec e 00000 MS El 70V 230 C 2 180 300
605. 0 2 10 1 10 1010 00000 0 DUDU uU uuu 100mL e 00000000000000 0000000000 GCU 0 2 0 7mm 15 30m 0 1 1 0u m 333
606. 0 B D d4 66 68 1 1 0 0 96 61 12 96 61 1 11 97 99 1 1 2 000 97 99 1 1 2 00000000 100 102 uut 130 132 111111 166 164 13 75 110 uut 78 77 de 84 83 83 85 12 Uu utt 96 61 12 63 76 p D D D D D U D Hu 146 148 1 92 91 de 100 99 106 91 TU 96 70 p 174 95 221 6 00000000 6 1 20g Wet 3 000rpm 10min 0000 10mL 200000 3 000rpm 10min 250 50mL DU 9 8mL D uuum oam p 222 6 1 612 1 0000000
607. 0 50 L 1 1000 g mL 12 228 8nm 13 5 1 1 4 8 2 5 1 1 4 b 5 1 1 4 c 2 11 12 13 aja 3 14 d 000000 o 00000 mgCd kg mgCd kg 74 6 00000000 8 d uui a D Cag PhO Zn Fer Mn Mo 0000 20 5g 0 0190 0000 200mL 10mL 20mL 0 1D 200 gt 20mL 1000 5 E 0000 000000 lO 0000000000000000 b D PhO Cup Zn Fe Mnp Nip Mor Se 0000 75 Ni 0000 00000 200mL
608. 0 0 194 1 1 15 K 8470 5mg O 1mol L NaOH 5mL m 000000000000000 0 14 100 0 0 0 1u g Hg mL 1u gHg mL 1u 206 5 14 2 gH g mL 0 5mL L 1 200rpm 0 1g L 5mL 3 000000 8 C d e f 9 3 000rpm D 1 0 50 5 50mL 15 500mL 20 30mL 111 0 00 0 10mL 10 10u L UGC 3mm
609. 0 1u g nt 1 gFe 1u gMnH 1u gNi 1p oa 1 u gAs 1u 9 1 5 1 3 2 f 9 50ngPb 50ngCu 50ngZn 5OngF ell 50ngMn 50ngNi 50ngM or 50ngAs 50ngCr mL 5 1 3 2 g 3 000000 a 000000 000000 7 0000000000 0 1ng mL e 5 250amu 10 lamu 0000 7 ICP MIP b 120
610. 0 25mm 15m 0 10 m 50 C 1min 10 C min 300 C 250 C 60sec 1u L 40cm MS E 1 70V 220 C SIM m z 38 300 1 amu b 1 3 op 0 050 1mL 10mL 0 050 1u g mL 0 5 1g 2u LOD GC MS 00000 6 2 2 2 6 2 2 3 6 2 2 4 1 2 4 10 2u LO GC MS 2 6 8 5 5 8 5 CP SIL 5 Ultra 2 DB SPB 1j NB 3 BP 10 CBP 3 CBJ 1 Ultra 1 11 8 239 6 2 e22 2 9
611. 0 7mm 100 30m 0 10 LOu m 99 999949 500 35009 00000 70V 4 00000 4 1 0000 2099 25mL 10 10 3 000rpm 10 3 a 9 5 400mL 1L 229 6 2 1
612. 0 C min 250 280 000000 MS0 70V 4 00000 a 000 3 2090 1L 8 9 200mL 10 3 10g 20mL 10 11 e 20mL 10 KD 5mL 1mL b 3 20mL 3 5vol 100mL 13 14 KD 307
613. 00 5m 172 0000 unneoc 20 5 32 2 l 200mL 173 D 022 80mL O 60mL D IU uu Baagat 100mL b 1 00000 0000 190 0 0190 00000 200m 0 200 1 0 50ML 00 10mL PA 000000 0010200 000000 100mL 10mL 0 PPU DU 5mL 2 0009000008 9 0 0 0 20 5mL 5mL b 2 1 0 1 19 0 001mg 0000 5mL 00050 B 2mL U 174 51212 aq
614. 00 d 00000 00 4 5 1 1 2 8 IS K 8121 149 1L 600 700 e 25mmol L 4 5 1 1 2 b f 0 4 5 1 1 2 f
615. 000 1 mL 0 5mL 4 lu LU GC 5 0 6 10 1 6 10 gt 4 2 Q luL GC MS 20 GC MS 2 D 6 10 1 CAS Registry N umber PTRI 4 98 54 4 1306 135 107 4 14938 35 3 1461 107 164 4 2446 69 7 1522 107 178 4 1987 50 4 1668 107 192 4 140 66 9 1614 135 107 4 1806 26 4 1770 107 206 104 40 5 1669 1801 135 107 ds 1200 136 dio 1794 168 4 PTRI Programmed Temperature Retention ndek 330 6 10 61052 0 0 808080800800880008000800080000000 00
616. 0000000 100mL o 0000 e 0000 e 000000 e 0000 e 000000000 50 500 L b 0000 4 00000 gt 106
617. 00000000 0 0 0 6 4 1 2 9 00000000 6 4 1 2 h i 0 00 0090000 00000 j 0000000000 UU D D i 6 4 2 2 i HRGC HRMS 5 3000 ectron lonization 25 70eV Selected lon Monitoring SIM O 2 SIM 288 6 4 PCB
618. 00p L b 0000 4 00000 5 9 1 4 8 5 1 1 4 b 5 a 0000 100 120 300 40 600 1 200 300 40 2 000 2 400 30 6 b 000000 193 7nm ul 20 20mL
619. 01 209 100mL 1u g L 50mg L JIS K 8490 5mg JIS K 8322 100mL 0 5p g L 5 K 8136 109 1420 60mL 100mL lu g L 115 K 1107 1 0 5 11 JIS K 8139 0 339g 500mL 1 1 5 i 10 9 6 1 0 5mgH g mL 10mL 500mL 1 1 5mL 1 p Ou gHg mL 10u gH g mL 10mL 1 000mL 121 10mL 1 3 a 5 14 1 b C 2 d
620. 04 0 08mg 50mL 25mL 5 2 o 00000 3 0 004 0 08mg 50mL 25mL 10mL e 10g L 5mL 20 255 30 an 6 630nm le d O00000 4 1 90 19 g 11 200 25 06 30 30 35 451 6 00000000 000 31 0 0 0 NH 0 03290 0 0190 0 D 200 1 DH 10mL 000000 59 29 N 0 004 0 08mg 50 1 0 000 25 Na 00000000 10mL 000000 200mL UU 000000 000 00 DUDU 300mL 000 D 200 000000000 50 200 25 C 30 630nm 0000000000 50041 DUDU l00mL 20mL ug 36 452 00000000 4 5 2 1 00000 1 0000000 2mol L 2 0 H a 5 K 0557 b 1 1 0 0 0 Gmol L n J o 0000000
621. 100000000 1090 0 19 0 300 UI 90mL 2009 L0 20m 95 c0 00000200 UU UUDUUDUUDUUDUUD Hg 0 10 24 90 0 000 0001010 10mL 000000 250m mgH kg 205 5 14 2 5142 000000010000 51421 1 0000000
622. 100mg L 0 1mgM n mL 50mL 500mL Uu 000000 Uu D D 4 00000 5 1 1 4 8 5 a b 5 1 1 4 b
623. 15 44 0 4 0 0 29 21 0 046 3 47 75 0 10 0 0 46 22 0 049 1 27 26 0 2 0 0 10 5 68 Cla 23 0 091 1 54 17 0 2 0 0 18 24 0 073 0 29 4 0 0 0 0 00 25 0 079 0 71 9 0 0 0 0 00 0 70 Clo 26 0 105 0 21 2 0 0 0 0 00 0 00 Total 99 11 25 81 100 00 6 4 2 D 109 5 0 L CB 1mg L 5 0 L 2ng PCB TotalCB PCB mg kg PCB x x TotalCB x x 10x 5 0 25 81 5 0 1 5 0 9911 10 0 13 mg kg 267 64 PCB 15 1 5 5 Loisi 6 4 1 as BQ 518 64 52 1 268 64 PCB 6 00000000 a 000 1 1 010009000 6 51 1 50 100 50 GF A 300mL O 50 1 D 00000 0000 50mL eS 000 50mL nonumm 0000 o 3 0000000 n 109 0080 8000000000 3oq 3 269 64 PCB 0000 200 l0mL ming 0 D 1 1 mz 30 0 3mL 1mL D D GC MS 1mL GC U Bt b B Bt
624. 20 100 50u L M 1 000 g mL 1 000 g mL 20 e 22 193 7nm Q3 5 9 1 4 a 5 1 1 4 5 2 eo 20 21 22 23 eoe 24 d 00000 mgAs kg 0000 mgAs kg 6 00000000 5 9 1 6 a 5 1 1 6 b 5 1 1 6 d 59 5 1 0000000 150
625. 25mm 30m D Abu m 60 C 2min 5 20 C min 300 2 1mL 60sed 290 C MS 280 C 51 70V 250 C SIM 5pg 15 277 275 351 349 d 295 293 dis 366 364 456 318 316 m z 18 300 1 amu 14 60 C 2min 20 C min 130 C 10 C min 2105 5 C min 260 C 295 b 10 C min 300 C 2min 15 e Du Du GC 6 5 16 Du FPDI 300 C DDU 50pg 100mL 10u g mL lu g mL 0 01 Su g 10u g mL 1mL 0 1 g mL 0 05mL 1mL
626. 3 15 16 17 5 12 1 1 4 a G D 0 5 12 1 1 4 b 19 5 12 1 1 4 5 22 o 15 100mL 50u g mL 10mL 2 451 131nm 10u gCr mL O 2 40mL 100mL 50u g mL 10mL 451 131nm 16 17 1 1 0 LI U mgCr kg 5 12
627. 40 1 900 2 400 Q 30 6 196 0nm b 8 20mL 1u gSe mL 0 31 2mL 100 50 L 1 1 000 g mL 3 000 g mL 9 10 196 0nm 11 8 5 9 1 4 8 5 1 1 4 5 2 oe 2 o1 000 3 1u gSe mL 1 10mL 100mL 32 Il 1 000u g mL 1 000u g mL 11 Cl AG 10mL 100mL N 1 000 g mL 1 000 g mL 49 157 0 2 00000 8 10 50u L 1 000u g mL 1 0001 g mL 9 10
628. 51 131nm 10u gCd mL 0 1 20mL 100mL 50u g mL 10mL 00 451 1 31 24 25 d mgCd kg 6 00000000 5 1 1 6 8 a ICP I Cd PhO Cul Zn Fe Mno Ni Mo Cro TT D 100 1 5mol L 1 50u g mL 10mL nm 1 2 3 4 Cd 226 502 228 802 214 438 Pb 220 351 216 999 405 782 Cu 327 396 324 754 224 700 Zn 213 856 202 551 206 191 Fe 259 940 239 562 238 204 232 036 Mn 257 610 259 373 260 569 Ni 231 604 341 477 221 647 Mo 203 844 281 615 202 030 Cr 267 716 206 149 205 552 In 451 131 84 5 2 5 2 1 000000000 1 0000000 283 3 2 DD a b C d e 0000 Ou gPb mL r 141 20mL 3 00000 8 115 K 0557 A3 DDU U
629. 7 ICP MIP b c 1 4 00000 5 1 1 4 a 5 1 1 4 b 5 ai ICP 630 65 103 1 20 1 5kW 15L min LOL min LOL min b 000 1u gCu mL 8 0 1 10mL 100mL 1 g mL 5mL 2 10mL 100mL 1u g mL 5mL 8 1 gCd 1u gPb gCu gzn Lu gFe 1u gMn lu gNi 1u gMo 1 gAs 1u gCr mL 5OngCd 5O0ngPb 5O0ngCu 5OngZn 5OngFe j 5 50ngNi 50ngMo 50ngAs 50ngCr mL 1u g mL 1 g mL 5mL o 00000 9 100mL 1u g mL 5mL 0 1 0 5mol L ICP m z ao 11 8 5 1 1 4 a O 5 1 1 4 b O o 9 97 5 3
630. 7 A3 b 000 o 0000000 Ou g mL 1mo mL 1mL 1 000mL 12 1 2mL d 1p om 1mg mL 1mL 1 000mL 1 1 2mL e 1mg mL 0o1mgMo mL 1mgM o mL 10mL 100mL 12 1 2mL 00000000 1u 49 0 1mgMo mL 5mL 500mL 1 1 10 1 1 gPb 1u gZn 1 gFerj 1u ont 1 gNi 1u gMor lu gAs 1u gCr mL 5 1 3 2 f i I O0ngCd 50ngPb 50ngCu 5OngZn 5OngF el 5OngMn 5OngNi 5OngM d 5O0ngAs 5OngCr mL 5 1 3 2 9 3 000000 a 000000 000000 6 0000000000 0 1ng mL 250amu 10 00000 lamu 0000 6 ICP MIP a
631. 78 0 23 0 234 0 04 PCB 206 3 67 0 87 PCB 209 8 34 0 49 0 33 gt 0 10 PAH DUU Naphthalene 1010 140 9 0x 0 7 Biphenyl 175 18 Fluorene 973 8 6 13 3 3 1 Phenanthrene 130 489 23 65 20 Anthracene 184 14 13 4 0 5 Methylphenanthrene 101 27 Fluoranthene 190 981 78 60 9 Pyrene 170 811 24 399 Chrysene 51C 380 24 14 1 2 0 Triphenylene 197 Benz a anthracene 46 427 25 14 6 2 0 Benzo a fluoranthene 118 11 Benzo b fluoranthene 740 110 7 7 1 2 Benzo k fluoranthene 361 18 2 8 2 0 Benzo e P yrene 553 59 Benzo a P yrene 628 52 7 4x 3 6 Perylene 452 58 Indeno 1 2 3 cd pyrene 525 t 67 5 42 1 3 Benz a h i perlene 501 72 5 0x 2 0 Dibengzla jlanthracene 74 3 Dibenz a c Janthracene 43 1 Dibenz a h anthracene 1 34 0 5 Benzo b chrysene Picene 14 SOP
632. 82g 1 000mL 0 10 p 0 01mgN mL 1mgN mL 10mL 1 000mL 8 70 125 10mL 200mL 10mL 300mL 100mL 1 2g 1 1 6 5 50mmol L 10g L 1mL 10mL N a xf m x0 001773 g L 8 50mmol L mL fl 50mmol L 0 001773 50mmol L 1mL 9 70 125 mL 9 O00000 a 4 5 1 1 3 b 00000 34
633. 9 10mL 0 0 KDI I 1 joen D 0 d 00000 100 50 L 20 3mm i o 0000000000 GCO 0 2 0 7mm 150 30m 0 1 1 0u m 99 999 0159 20 40cm sec 35 230 0 500 35 230 0 500 150 280 C 2000 270 500 100 40 50 100 C min 2500 280 70V 4 00000 a 10920 50mL 3 30mL 10 340 b 6 11
634. 91 215 6 1 6 00000 1mgmL j 7 8 d 10u 100mL 1mg mL 1mL 100mL e 1mg mL 4 f 30 gmL 1mg mL 1mL 50 90mL 100mL 100mL g 00000 99 999 vol9q 15 K 1107 1D 0 0 99 999 vd i Dang 5 1 3L
635. 92 6 5
636. A EE a 82 0 320 2 2 3 5 5 6 2 22 3 3A 7 48 1 332 1151 1 011 274 64 PCB 6 4 3 1 1 paga 551 pa pa gaga gaga cB 2 8021 IUPAC No i Structure 2 2 3 3 6 61 2 2 3 4 9 6 3 504 107 Los 329 124 0 4301 12 3 3 45 2 34 557 109 123 2 3 3 4 5 2 3 4 4 5 el ERO Tas T 1131 165 142 0 037 22 3346 233 5 5 5 2 2 3 4 5 6 182 1 821 23 31 45 2 2 3 3 4 5 6 12 2 3 3 4 5 6 6 B 280 170 190 1 23 2 2 33 4 4 5 2 3 3 4 45 6 198 0 046 EE 334556 5 1206 DO 3344556 i 275 9 eu Time min 2 6 4 4 nnpn unnuunuunnuunnuunnuunnaunnaumnnaun 834 9 1 6 4 PCB 6 4 4 njan an aj anla nja nga pn ang nn aa dinan 1111111111 cB 1 i 80 IUPAC No i Structure NA NE O dM Ee 31 15035 66 7600 415 1234 AD 34 5 1102 95 93 2560 122 ZA 45 6 Ek 35 6 2 2 3 5 6 0 081 91 0 340 6697 E is nl t 1 408 81 0 096 3 4 4 5 117 87 125 1 312 234 56 22 345 2 345 6 oa 55 2294223355 o 0 829 1124 0 165 272 345 135 144 147 0 664 22 3 3 6 6 2 2 3 4 5 6 2 2 3 4 5 6 277 6 4 PCB 6 4 4 QUDUDDUDDIUDDDDUUDUDDUDUIUD cB 2 III C
637. Bo96 IUPAC No Structure 2 34 5 6 2 2 3 4 4 6 A 4 5 3 3 5 6 2 2 3 4 5 6 3 4 5 5 3 34 5 _ 22 3 3 45 6 12 3 4 4 5 6 2 2 3 4 5 5 6 122 3 3 4 4 2234456 234 455 12 2 3 4 5 56 12 2 3 3 4 5 6 2 3 3 4 4 5 2 2 3 3 4 4 6 2 3 3 4 4 5 2 2 3 3 5 5 6 6 ECKER EE 2 2 33 45 5 12 2 3 3 4 4 6 6 2 3 4 4 5 5 32 33 4 5 56 EEN EEN 2 2 3 3 4 5 56 22 33 445 12 3 3 4 4 5 6 2 2 3 3 4 5 5 6 2 2 33 45 66 12 2 3 3 4 4 5 6 2 2 3 4 4 5 5 6 12 3 34 4 5 5 2 2 3 3 4 4 5 6 12 2 3 3 4 5 5 6 6 2 2 3 3 4 4 5 6 6 156 0 334 171 0 284 71 0 324 1157 0 110 202 0 213 x i2 2 3 3 4 4 5 5 NE 89 0 149200 122 33 4455 5 6 100 00 27 6 n 6 4 1 6 8 D 6 4 PCB 0000 9 00090000 0 800 ECD 0 25 0 0 30m0 0000 0 254 mi 0000 0 60 C 2min 5 20 C min gt 160 C gt 5 C min 300 C 5min 280 C adu 279 6 4 PCB 643 0 00 1 0000000 8
638. GC MS SIM 2 00 a b L 00000 c n 00000 d 000000 e 00000 f 000000 00000 DD i 1 ij 0 000000 m 1mol L NaOH Li E LI B 29 n D 20 48 mesh 50mL o 0 B D 569
639. L 5mL lmL 149 10mL lmL 20 100mL OI 8 O 9 86 5 13
640. L r 1mg mL 50mL 1 000mL 1 1 2mL d DD 10u gCu mL 5 3 3 2 1 1 2 e 0 10u 9 90 10u gPbr 10u gCu 10u gZn 10 gFe 10u gMn 10p gNi 10 u gMo 10u gCr mL 5 1 4 2 e 0 1mgCu mL 10mL 100mL 3 000000 a 000000 e 0000 5 000000 b 6 0000
641. LAS Ci LAS LAS Carol 14 0 1mg mL HPLC 2 LAS 10u g mL Cid Call Ci Ci4 LAS 10 Cu LAS g mL 6 3 1 6 3721 LASO Cid 1111 1 B B D B D lU D Cu Cu Cis Cu CizLAS 10u g mL 273 4 B LAS 0 1mg mL 306 6 1017 3 896 7 480 4 156 5 LAS mmol L 0 0322 0 1069 0 0942 0 0505 0 0164 LAS u g mL 10 3 35 7 32 8 18 3 6 2 o 00000 5mL 15mL 4 GCB 6 GCB 2 70 30 7mL 6 250 M 90 100 7mL 7 100 M 90 30 7mL LAS 65 35 1mL LAS d LAS 4 1 96 19 LAS mg kg mL 100 1 mg kg ng x UL XW W g 4 10mL 10 100 L 5 GCB 5 250 631 000000000 pne 0m 7 Cu LU 0 5 10 15 20 time min 0 6 3 1 12000 abandance time min 6 3 2 5 251 6 31 6 00000000
642. V 1000 300 C N Ul o o 8 Un E3 EEN a a a 291 6 5 TPTU 6 5 1 GC MS GC FPD 2 a b D uuu Uu D uu 00000000
643. a 10mm b 105 110 2 2 40 2mm 2 3 00000000 3100000000 1 UD 1050 110 0 21 0 3 LL 1100100000 400 N ju 3o 18
644. e gMn 1p gNi gMo 1
645. e 0 72 0 43 1 09 0 214 0 76 Si 96 21 24 2 40 00 29 08 Sr 110 126 68 130 125 96 277 170 5 8 9 2 18 Ti 9 0 64 0 34 0 456 0 457 0 5 0 22 2 0 3 13 6 3 20 V 250 134 44 8 95 252 93 4 127 105 55 5 Zn 343 738 438 172 119 824 142 977 ugaagagpgaugug 13 0 2 3 000000000000000 NIST NIST NRCC NRCC River Sediment Marine Sediment Marine Sediment Marine Sediment SRM 1939 SRM 1941a HS 1 5 3 ug kg ug kg g kg pg kg Hexachlorobenzene 70 25 a HCH HCH trans Chlordane Heptachlor epoxide 510 cis Chlordane 220 2 33 0 56 trans Nonachlor 270 1 26 0 13 cis Nonachlor Oxychlordane 2 59 Dieldrin 1 26 2 4 DDE 0 73 0 11 4 4 DDE 540 6 59 0 56 2 4 DDD 20 4 4 DDD 60 5 06 20 58 2 4 DDT 44 1 25 PCB 18 1 15 PCB 26 4200 290 PCB 28 2210 100 9 8 PCB 31 6860 6 2 PCB 44 1070 120 4 80 40 62 PCB 49 95 2 4 PCB 52 4480 6 89 0 56 PCB 66 930 68 1 4 PCB 95 75 1 1 PCB 99 4 17 0 51 8 101 820 110 6 1 62 0 21 8 105 3 65 3 0 27 8 110 9 47 gt 0 85 PCB 118 510 100 1 3 8 1328 100 187 0 32 PCB 138 570 13 38 0 97 1 98 0 28 PCB 149 92 1 3 PCB 151 2 62 0 48 0 08 8 153 17 6 1 9 2 27 0 28 PCB 156 0 93 0 14 PCB 170 110 3 00 0 46 0 27 0 05 PCB 180 160 5 83 4 0 58 1 17 0 15 PCB 187 180 7 0 PCB 194 1
646. e 00000000 Ou gMolmL 5 8 1 2 9 3 000000 a 000000000000 0000 e 0000 e 000000 e 0000 0000000000 e 000000000 50 500p L b 00 9 0000 135
647. emt 5 5 2 2 0 10u 9 e mL 10mL 1 1 2mL 3 000000 a 000000000000 100mL o 0000 0000 5 000000 e 0000 e 000000000 50 500 L 0000
648. enyl 301 9626 303 9597 2 2 5 5 Tetrachloro 3C i2 bi phenyl 335 9237 337 9207 2 3 4 4 5 Pentachloro 3C 2 bi phenyl 371 8817 373 8788 2 2 4 4 5 5 H exachloro 3C 2 bi phenyl 405 8428 407 8398 2 2 3 4 4 5 5 H eptachloro 33C 2 bi phenyl 439 8038 441 8008 2 2 3 3 4 4 5 5 Octachloro 13C 2 bi phenyl 473 7648 475 7619 2 2 3 34 4 5 5 6 Nonachloro 13C 2 bi phenyl 509 7229 511 7199 2 2 3 3 4 4 5 5 6 6 Decachloro 3C bi phenyl d 2 264 169 e 00000 PFK 10 000 10 4 b 000 6 4 3 5 o 00000 6 4 3 5 0 d 6 4 3 5 d 0000000000 6 4 3 5 d O e 6 4 3 5 e f 6 4 3 5 f 4 PFK 290 6 4 PCB 6 00000000 DO0O0000000006 416a00 0000000000000000 DUDU 0 25 1 0 0 30m0 0000 0 25 130 C 1min 20 C in 220 C 5 C min sa 280 C UU CODE uw e o 1094 5 N Ul 70
649. enyl 15 2 2 6 Trichlorobi phenyl 19 3 4 4 Trichlorobi phenyl 37 2 2 6 6 Tetrachlorobi phenyl 54 3 3 4 4 Tetrachlorobi phenyl 77 2 2 4 6 6 Pentachlorobi phenyl 104 3 3 4 4 5 Pentachlorobiphenyl 126 2 2 4 4 6 6 Hexachlorobi phenyl 155 3 3 4 4 5 5 H exachlorobi phenyl 169 2 2 3 4 5 6 6 Heptachlorobi phenyl 188 2 2 3 4 4 5 5 Heptachlorobi phenyl 189 2 2 3 3 4 4 5 5 Octachlorobi phenyl 202 2 3 3 4 4 5 5 6 Octachlorobi phenyl 205 2 2 3 3 4 4 5 5 6 Nonachlorobi phenyl 206 2 2 3 3 4 5 5 6 6 Nonachlorobi phenyl 208 2 2 3 3 4 4 5 5 6 6 Decachlorobi phenyl 209 6 4 6 00000 PCBO Wellington Laboratories BP MS PCB PCB Congener IUPAC No Monochlorobi phenyl 1 3 Dichlorobi phenyl 4 8 10 15 Trichlorobi phenyl 18 19 22 28 33 37 Tetrachlorobi phenyl 44 49 52 54 70 74 77 81 Pentachlorobiphenyl 87 95 99 101 104 105 110 114 118 119 123 126 H exachlorobi phenyl 128 138 149 151 153 155 156 157 158 167 168 169 H eptachlorobi phenyl 170 171 177 178 180 183 187 188 189 191 Octachlorobi phenyl 194 199 201 202 205 Nonachlorobi phenyl 206 208 Decachlorobi phenyl 209 281 6 4 PCB 6 4 7
650. gn 00000000900000000000 8 100m 9 0000000000009099900000000000 30 00 00 8090000000008000090000 o o 000 2059000000000 23
651. i cN m set e ON em CXEXEXP STEET mn 3 3 1 o CMAHAAHAHONNN ELE EL ET ISE 1 sf sf oun om QN 3 31 os C1 6 m i omo N st sf sf sf sf sf sf ms u ANOM i 93 1 101 109 117 125 133 140 153 159 168 162 165
652. in 1 0L min 1 0L min 3 b 000 1u gCd mL 07 0 1 10mL 100mL 1u g mL mt CIS 10mL 100mL 1u g mL 5mL 17 3 9690 1u gPb 1u gCu 1u gzn Lu gFe 1u gMn 1p 1u gMo 1p gAs 1 gCr mL 5OngCd 50ngPb 5O0ngCu 5OngZn 5OngFe j 5 50ngNi 50ngMo 50ngAs 50ngCr mL 1u g mL 1u g mL 5mL o 00000 18 100mL 1u g mL 5bmL 0 1 0 5mol L ICP m z a9 20 5 1 1 4 a Q 5 1 1 4 56 2 o 18 1g L 19 m z 16 m z 2 m z 20 m z d O00000 mgCd kg 8 6 00000000
653. m b 0000000000 12 20mL lu gCu mL OUT Amt 3 Q 10 50 L 13 324 8nm 14 8 5 1 1 4 8 2 5 1 1 4 6 2 5 1 1 4 eo 2 o9 000000000 1u 9 0 5 10mL 100mL a5 c 29 10mL 100mL 0 28 0 2 0 10 50 L 2 324 8nm 3 8 5 1 1 4 8 2 5 1 1 4 6 2 5 1 1 4 eo 2 12 99 5 3 13 14 15 d 000000 00000 mgCu kg 0000
654. mL 200mL pH5 2 10mL 1u gF mL 0 1mgF mL I 1 aam 2 15 15 7 pH5 2 pH 5 2 8 0 1u gF mL O 9 10 11
655. ng D en 0 140 00000000000000000000000000000000000000000 500 600000000000000000 m i 30 1 0 000230 2 90 32 2 3 JI S00g L I 0 5 33 1011000000 0 uui 451 51 305 D D 00 0 140m 00000 0000 0000 30
656. oog L r 4 8 1 2 c d EDTA 4 8 3 2 9 e D 4 8 3 2 6 000000000 009 4 8 1 2 f
657. u g mL 1mg mL 50mL 1 000mL 12 1 2mL d 0000000 10u gMn mL 5 6 1 2 4 e H 10 gCd 10u gPb 10 gCu 10 3 gFe 10u gMn 10 gNi 10u gMo 10u gCr mL 5 1 4 2 e 3 000000 a 000000 b 00 0000 4 00000 5 1 1 4 a 5 1 1 4 b 118
658. u gMn 1u gNi 1u 1u gAs 1p gCr 1u gB mL 5OngCd 5OngPb 5O0ngCu 5OngZn 5OngFe j 50ngMn 50ngNi 50ngMo 50ngAs 50ngCr mL 1p g mL
659. yl 2 5 Dibromobi phenyl 2 6 Dibromobi phenyl 4 4 Dibromobi phenyl 2 2 5 Tribromobiphenyl 2 3 5 Tribromobi phenyl 2 4 5 Tribromobiphenyl 2 4 6 Tribromobi phenyl 2 2 4 5 Tetrabromobi phenyl 2 2 5 5 Tetrabromobi phenyl 2 2 5 6 Tetrabromobi phenyl 3 3 4 4 Tetrabromobi phenyl 3 3 5 5 Tetrabromobi phenyl 2 2 4 5 6 Pentabromobi phenyl 2 2 4 4 5 5 Hexabromobi phenyl 2 2 4 4 6 6 H exabromobi phenyl 3 3 4 4 5 5 Hexabromobi phenyl Decabromobi phenyl 1 3 000000 a b 0000 50mL 0000000 d 3 000rpm 236 6 2

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