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海洋観測ガイドライン 第三巻 採水分析(溶存態)
Contents
1.
2. 3 4 WEB D BHC DON TDN DIN
3. Decon 90 10 2 6 3 EK
4. DOC DON
5. Val 3 Chap 10 DOC DON DOP 2015 G310JP 001 013 G310JP 13 2
6. iT Vol 3 Chap 2 2015 G302JP 001 017 G302JP 14 18MQcm vs
7. 2 6 2 HROBBE REF TOR Zhang et al 1999 Decon 90 As HIT LES YO LUT
8. Vol 3 Chap 8 CFC_SF6 2015 G308JP 001 009 G308JP 3 Ni 63 A D HAT 5 2 3 BOTBIEFMAO A
9. CFC SF CFC SE ppt E 1 1072
10. 2 2 CFC SF CFC 11
11. 5 6 DOC 1 uM TDN 0 1 uM
12. CFA CFA CFA Vol3 Chap 2 KER gt X 4 zh 1H
13. Vol 3 Chap 2 2015 G302JP 001 017 TF BEY A c EVA 2 3 3 4 20C
14. Vol 3 Chap 10 DOC DON DOP 2015 G310JP 001 013 G310JP 8 pH 1 2
15. Strickland and Parsons 1972 Adas etal 1971
16. DON DOP DOM DOC CO2 DON NO DOP DOC DON DOC DOP DON DOC DOP
17. 1964 Godometric titration Winkler 1888 Carpenter 1965a Strickland and Parsons 1972 Grasshoff 1976 Culberson 1991 JGOFS 1994 Dickson 1996 Hansen 1999 Langdon 2010 Broenkow and Cline 1969 Pai et al 1993 Labasque et al 2004
18. DIC 2 3 4 5 6 2 2 1 C PC 7C He Rsa BCPC Rsr 83C o 3C RsA Rsr 1 x 1000 1 Pee Dee Belemnites PDB 23 BC PC
19. WAR RCGC RUME F ART
20. 2 replicate n WOA replicate div do ds dn ES s 5m d 272n 3 0 1umol kg
21. AWK SFs CFC 12 CFC 11 CFC SF 15 30 CP Silica Plot Agilent
22. 50 mM 1 1 1 TDN TDN
23. EK 11 3
24. 10 2 4 WIEK H202 2F 2HT b 2H20 32 1 0 5 1 05 DIW Mgo Wong et al
25. BH 603 225 NL m 1 Vol 3 Chap 8 CFC SF6 2015 G308JP 001 009 G308JP 6
26. DOC DOC
27. 6 11 BRAS 30 TERY TOR HOBRSRROZ F UHR C DIW 200 umol kg
28. CFA AA I CFA 3 D 2 3
29. 2 3 3 4 OI OD ERE 4 10 CFC SF
30. OU ICP MS e lcs E
31. 1999 2010 WOCE GO SHIP IOCCP Report No 14 2010 Repeat Hydrography n 8L
32. GO SHIP 1990 World Ocean Circulation Experiment WOCE WOCE RMNS Reference Materials for Nutrients in Seawater RMNS
33. E TOC NO
34. 200g L 5 1 2 RKF 2 7 DIW Vol 3Chap 1 BAKKE 2015 G301JP 001 030 Dickson 1996 2 G301JP 7
35. 10 2 gt 10 KLE EY F747 EREDA 10 1 traceability ISO 2015 SI NMI CRM 3006 a 4 5
36. DIN DOC TDN DOC 0 100 uM 20 uM 6 TDN 0 60 pM 10 pM 6 2000 4 ELIR DOC TDN CRMs Consensus Reference Materials
37. EXC SAL 7 5b 2 52055 SISSE 3 E R mE TY E 3 G301JP 2 m TY E E H JW Huc v4vZ7 ik 3 6 7 8 9 10 OD
38. 6 6 IL BRO O 6 7 EAR BRON I I 1mL 2mL
39. 6 E 7 1 7 2 7 3 7 1 FABLE eS EEO RUGS SE SL BRIONY I II DIW TW Vol 3Chap 1 ZSUKBB2015 G301JP 001 030 G301JP 12 Langdon 2010 72 eine Da 1 oy e ee
40. 3 2 RE D 1980 1990 DOC DOC og DOC 2 Vol 3 Chap 10 DOC DON DOP 2015 G310JP 001 013 G310JP 6
41. 13X 2 1 V L amp h Fy TB amp 3 E Vol 3 Chap 8 CFC_SF6 2015 G308JP 001 009 G308JP 2 CFCs ml CFCs 3 SF 200ml Bullister and Wisegarver 2008 Law et al 1994
42. 4 1 CO DIC DIC CO SrCl BaCl CO Drimmie et al 1991 pH CO Nz CO McNichol and Jones 1992 pH CO 2000 Salata et al 2000 McNicholet al 2010 Ay RF Institute for En
43. 5 G310JP 001 013 G310JP 5 DOP Yoshimura 2013 1 5 10 mL 550 C 5
44. TDN DIN TDP DTP DON DOP DIN 40 45 uM DON 2 uM TDN 4 5 DON DON 5 40 1 uM TDN DIN 0 3 2010 TDN uuM DON 5 10 DIN
45. 2 l c E WELG 5 4 9 Fd 0 E 11 3 4 8 01 1 11 2 1 WU 11 3 2 1
46. uj uz us on u Uc we uy 21 GUM 9 1 THERA OLERER 17 19 C t mol L S 1 Vir V Csam ts 1000 CNa s 0 EUN DO seg Vnasi ts Veg 22 Cn s o NasS2O3 mol L Vit mL Volk mL DO TI mol Vaask ts t PC mL Veg HERK I IL mL DOr
47. 2 C 3 6 HEFIR 6 1 EA BE E Vol 3 Chap 5 eon EJ 20 2015 G305JP 001 010 G305JP 5 1
48. E 5 1 3 TERRI AI ESSE E ERASE IE 4 1 II 42 1mL E 2 QL Ops ITO RVC C 5 I 200g L A F I 2mL 8 3 3 25 Vre
49. 2015 G302JP 001 017 G302JP 11 Interference filter Lamp diode Waste I Reagent Pump Computer Reagent 1 CUTE TNT Reagent 2 X gt f Reagent 3 Coils Air injection Sample inlet From sampler Figure 1 Schematic of a CFA system 1 CFA CFA Pu
50. E management practices personnel training technical operations Taylor and Oppermann 1986 Taylor and Oppermann 1986 Taylor 1987 Vijverberg and Cofino 1987 Dux 1990 Good Laboratory Practices GLPs Good Measurement Practices GMPs Standard Operating Pr
51. TOC GB CRMs LCW GEB ON ARERR LEDO TIY 1
52. AasAa 6 5 2 pH DHA Vol 3 Chap 5 2015 G305JP 001 010 G305JP 7 Ey Mal pil pH 6 6 Aas Aaa 25 g HI e 4 HI pH pK log a m 54 HI Caio Aaaa 2s Esa T sa HI HT mol kg soln pK log K 4 2699 2 758x10 35 S 7 S 4 i 444 616nm 444 nm ET 4 ig444 5 2 4 i440 4 i 44455 7C
53. DIP DOP ZOE DIP DOC TDN CRMs DOP TDP Yoshimura and Sharp 2010 WHE X DOP
54. Anderson E C W F Libby S Weinhouse A R Reid A D Kirshenbaum and A V Grosse 1947 Radiocarbon from cosmic radiation Science 105 576 577 1999 AMS 99 007 pp 22 Aramaki T T Mizushima Y Mizutani T Yamatoto O Togawa S Kabuto T Kuji A Gottdang M Klein and D J W Mous 2000 The AMS facility at the Japan Atomic Energy Research Institute JAERI Nuclear Instruments and Methods in Physics Research B172 18 23 Aramaki T Y Nojiri H Mukai S Kushibashi M Uchida and Y Shibata 2010 Preliminary results of radiocarbon monitoring in the surface waters of the North Pacific Nuclear Instruments and Methods in Physics Research B 268 1222 1225 Becker M N Andersen B Fiedler P Fietzek A K rtzinger T Steinhoff and G Friedrichs 2012 Using cavity ringdown spectroscopy for continuous monitoring of 3C CO gt 2 and f CO in the surface ocean Limnology and Oceanography Methods 10 752 766 Bowen R 1966 Paleotemperature analysis Elsevier Publ Co Amsterdam pp 265 Drimmie R
55. 2 3 LBL NSOP 2 4 ABO NSOP 7 E HEE C Hee s OS WA v NIE CA LC v S Gn vitro
56. DOP DOC DON 3 DOC DON 3 1 iiec DOC DON DIC CO NO NDIR Non dispersive Infrared detector CLS Chemiluminescence detector TOC
57. Vol 3 Chap 10 DOC DON DOP 2015 G310JP 001 013 WERK 2 H NN 1 4 2 n ei CHR ON 10 20 L eres
58. 0 027 Cxro tr 3 21 0 030 Vi 7 2 8 0 02 CN o Ckro tr Vs 0 036 9 3 ARETE X MESHED A ER Vga a t ORTES HRA IC XE IRE OO REO IK LIE OR YE zi e ATE ETKA RERE EAT BARTER SEAT SW EMRE LEE 0 015 Vi
59. CO Swagelok A L MN 4 2 4 2 HK APE 3 1 1 No VARA 1 Stripping Probe KE 4 mL
60. 1999 HIRES X5 L 1 4 2 5 11 Z77ry4bkOXE 5 4 CO gt CO 5 7 70 90 60 AWC Kitagawa et al 1993 6 Vol 3 Chap 9 AMC bC 6 2015 G309JP 001 018
61. 8 C A C AMC Asn Aass 1 x 1000 8 IIT Asn 83Cvppg Asa CC FE Asn Asa 1 2 25 48PCvppg 1000 9 Asn Asa 1 25 1000 1 8 Cyppg 1000 10 9 893Cvpps 30 5 0 13 0 02 83Cvpps 25 6 Cvsps 0 o 10 AMC 83C C259 84C DIC OBA AMC 87C 50 z y
62. TDN JL MO ON DIC Val 3 Chap 10 DOC DON DOP 2015 G310JP 001 013 G310JP 10 DOC TDN Lv DOC TDN
63. 1 Acropak PALL 0 2um 0 1M 1 H GEOTRACES GEOTRACES pn LAL dump JECT 4 7v 2 pde euet band didt Ru ue m
64. DOC DON DOP DOC DON DOP 2 DON 3 DOC DON DOP a
65. 7 2 8 FLEMIOHR 3 Va mL 1 600 mol L 0 04 mol L 2 53mL 8 2 n 7 3 ART TV OME 2 SM SET FV 7
66. E 2nd QC Johnson et al 2001 Vol 3 Chap 8 CFC_SF6 2015 Q308JP 001 009 G308JP 8 1 CFC SFs mol kg atm CFC 11 CFC 12 SF i 232 0411 220 2120 82 1639 a 322 5546 301 8695 120 152 a3 120 4956 114 8533 30 6372 a4 1 39165 1 39165 bi 0 146531 0 147718 0 0293201 b 0 093621 0 093175 0 0351974 bs 0 0160693 0 0157340 0 00740056 Warner and Weiss 1985 2 Bullister et al 2002
67. ON 1 DIC PoE Le 1 2 3 aire E TDN DON
68. CO 5 5 5 6 5 7 4 11 6mm CHA AMS comparability IAEA MC IAEA C7 Oxalic Acid pMC 49 53 Co TL AMS AMS AMS T
69. ltll 7 Iz 252027 gt 317 S408 8 1 2 1 4 4
70. 4 5 LEEPER LIHEKT OTN ORR Ta Re Ze VSI L CHB AR Tv BERS COURS LL HERR YSN Eo THE LE REI 46 BHKEACHFEN 444nm 616nm 750nm 8cm 10cm 4 7 faite 25 0 0 1C 5 7 BHO
71. 1 1 Carpenter 1965b Culberson etal 1991
72. DOM DON DOP DOM 3 DOC 3 DON DOP DON DOP
73. 2015 9 1 ISBN 978 4 908553 02 8 ISBN 978 4 908553 02 8 49085 908 553
74. 1993 2 13 32 1996 63 68 ITRE IU 2000 HUEK E00 SA 0 ER C338 0 o ETE OOTATETH FR ORE BA 305 265271 2003 340 176 182 2004 2007 i a 2010 ER n 559 563 20 2 309 319 Ridal J J and R M Moore 1999 A re examination of the measurement of dissolved organic phosphorus in sweater Mar Chem 29 19 31 Yoshimura T an
75. Breland IL J A and R H Byrne 1993 Spectrophotometric procedures for determination of sea water alkalinity using bromocresol green Deep Sea Res I 40 629 641 Dickson A G 1981 An exact definition of total alkalinity and a procedure for the estimation of alkalinity and total inorganic carbon from titration data Deep Sea Res 28A 609 623 Dickson A G Afghan J D and Anderson G C 2003 Reference materials for oceanic CO analysis a method for the certification of total alkalinity Mar Chem 80 185 197 Yao W and Byrne R H 1998 Simplified seawater alkalinity analysis application to the potentiometric titration of the total alkalinity and carbonate content in sea water Deep Sea Res I 45 1383 1392 Vol 3 Chap 5 2015 G305JP 001 010 G306JP 1 pH 4 DIC 6 pH 7 pCO2 CDIAC OF web lt SOP http cdiac ornl gov oceans Handbook 2007 html Vol 3 Chap 6 pH G306JP 001 DUMMY G307JP 1 pCO
76. 8 1 8 2 8 3 DIW 10 2 8 1 AVRBVI GA KIO3 HERRORE 8 1 1 HAEN KIO Crio Imolkg Pkros Wkios fpuoy KIO3 Ckio 13 mkiog WdwtWxi03 fbuoy dw pkro KIO wko KIO OE g 4 5 4 fbuoy KIO KIOs 11 3 3 mgro KIO3 214 001 2012 Waw Wig DIW KIO kg 4 5 5 fouoy dw KIO 11 3 3 8 1 2 RATIA Vol 3Chap 1 AKER 2015 G301JP 001 030 G301J
77. JE E 100 DON 3 E pH DIC DON 90
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79. 2 gt Qo 5 Carpenter 1965a 5 2 4 AREY OAR RADE 1 10mL Zl KALB 11 3 5 2 5 Ak ied gf 5 1 4 EI UH Vol 3 Chap 1 E
80. Vol 3 Chap 2 2015 G302JP 001 017 G302JP 13 Decon 90 Bis 2 6 AEDES 2 6 1 BROGR CFA J
81. 1937 Skeggs CFA Skeggs 2000 Atlas et al 1971 Mee 1986 Aminot and Kerouel 2007 GBEOSECS gt a _ IH Vol 3 Chap 2 2015 G302JP 001 017 G302JP 8 Gouretski and Jancke 2001 2 2 EH HEH 20
82. 8 Aminot A and D S Kirkwood 1995 Report on the results of the fifth ICES Inter comparison study for Nutrients in Seawater ICES Cooperative Research Report No 213 79 pp Aminot A and R Kerouel 1995 Reference material for nutrients in seawater stability of nitrate nitrite ammonium and phosphate in autoclaved samples Mar Chem 49 221 232 Aminot A and R Kerouel 2007 Dosage automatique des nutriments dans les eaux marines methodes en flux continu 188p In Methodes d analyse en milieu marin Ifremer ed Editions 25 Quae ISBN 978 2 7592 0023 8 Aminot A R Kerouel and S Coverly 2009 Nutrients in Seawater Using Segmented Flow Analysis Pp 143 178 Chapter 8 in Practical Guidelines for the Analysis of Seawater Oliver Wurl ed CRC 2009 408pp ISBN 13 978 1420073065 Aoyama M J Hamanaka A Kudo Y Otsubo K Sato A Yasuda and S Yokogawa 2005 Nutrients Pp 57 73 in WHP P6 A10 I3 I4 Revisit Data Book Blue Earth Global Expedition 2003 BEAGLE2003 Volume 2 Hiroshi Uchida and Masao Fukasawa eds JAMSTEC Yokosuka Aoyama M S Becker M Dai H Daimon L I Gordon H Kasai R Kerouel N Kress D Masten A Murata N Nagai H Ogawa H Ota H Saito K Saito T Shimizu H Takano A Tsuda K Yokouchi and
83. Vol 3Chap 1 ARER 2015 G301JP 001 030 G301JP 22 10 2 2 3 FH 10 2 1 2 0 150m 0 4 0 5 umol kg 0 6 0 7 umol kg 0 5 umol L 0S 035 umol L Wong and Li 2009 1 5 8 3 1 0 35 0 5 umol L 0 52 0 75 umol L 2
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85. 2 5 PUREO b LS ELS COPGERLOUSICHO CRS SRE 2 5 1 CFA CFA J LOE H Aminot and Kerouel 2007 Aminot et al 2009 CFA 1 CFA Zhang 1997 DA ZEA KO i gt Jv C
86. 25 8 3 1 25 5C Murray et al 1968 6 2 BEXIAD RS Dickson 1996 ABE 3 Horibe etal 1972 6 3 RKF2 7ORY ftit
87. CFC 11 CFC 12 4 0 005 pmol kg H 1 SF 0 030 fmolkg 6 Sasaki etal 2014 2 3 1 EKA amp CFCs 120ml mint CFC SF 220ml min CFC SF 8 99 CFC SF CFC SF 15
88. 1 2 3
89. Vol 3 Chap 2015 G305JP 001 010 G305JP 2 4 RE 4 1 REO 1 KL 4 2 WEKVYv7MOZ2 lt 50 cm 1 pmol kg 0 1 3 E v ExE
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91. Advantec PP 47 Inlet fi Outlet 250 mL A OIC Babel SORORIS WEE ix Li C OIN 3
92. 6 4 BHD K Vol 3Chap 1 BAKKE 2015 G301JP 001 030 G301JP 10 5 2
93. Gouretski and Janke 2001 Tanhua et al 2009 Olafsson and Olsen 2010 RMNS 2006 KANSO PA 55 Aoyama 2007 KANSO Aoyama 2007 RMNS Alain Aminot Don Kirkwood ICES
94. b c 10 10 10 G G G a a Q w 100 100 100 E 5 5 L L g a a a A 1000 1000 A 1000 o Oo 0 1 2 3 0 1 2 3 0 1 2 3 Seawater blank umol kg Seawater blank umol kg Seawater blank umol kg E 2 MRO0S 0S 2005 11 A 2006 1 H hmol ke a 29 1 N 123 9 W b 25 5 N 164 3 W c 24 2 N 172 8 E 10 2 3 HERB 2NO gt 21 4H b 2NO 2H20 28 1 0 5 1 0 25 28 2NO O2 H20 NO7 NO3 2
95. Vol 3 Chap 2 2015 G302JP 001 017 G302JP 9 Gordon et al 1993 2 3 HEAT 2 4 1 Rki NSOP 7 f Decon 90
96. 2 6 5 FAIZ LPDR LNSW low nutrient seawater LNSW LNSW lum 40 gl 35 ASW artificial seawater
97. ET 24 ee G302JP 10 EFT Fo LA Macdonald et al 1986 Zhang and Ortner 1998 40 uM kg
98. 99 CFC SF 30 mm 500 mm CFC SF 116 Imm CFCs Porapak T Waters SF Porapak T Porapak Q Waters Carboxene1000 Supelco Analytical
99. Bulsiewicz et al 1998 Vollmer and Weiss 5 amp 1 2 12
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101. DIC DOC DOC DIC 3 mL ON 1 Hitt 30 50 mL vit 5 10 ORY 1 ui gt E
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103. 1 4 5 10 DIC 15 20 1 DOC TDN DIC DIC DOC TDN O DOC
104. DOC DOC DOC 4 6 pM DOC 35 90 uM 5 20 TDN 4 47 uM 0 5 20 0 3 0 8 uM CLS
105. 1 200 1 3 CFC SFs
106. Cm Ie ae Vol 3 Chap 2 2015 G302JP 001 017 IH G302JP 15 7 2007 11 INSS best practice WOCBE
107. SW uS SET TYTO 3 3 EET HO
108. DIP TDP TDP 3 TDP 0 225 M 100 mL 5 g 8 125 2
109. 10 umol ke suboxic water Rue et al 1997 Id 5 3c O EF 3c a Fa E Lr
110. 9 2 4 5 7 10 2 10 2 1 nmolkg 0 50 0 50 umol kg 0 29 umol kg 0 50 3
111. replicate sampling 5 Aramaki et al 2010 Kumamoto et al 2013 McNichol et al 2010 AMS 6 2 8 WRR L BIFA AMS 5 2 lL C free CO 4 5 IAEA uC IAEA C1 Carbonate pMC 0 00 CO 850 6 1 1 AMS
112. AMC 513C G308JP 001 009 G309JP 001 018 ot 3 E E ay mi x Beth LA B Ax H OF SH 34 4 LIEGE E BEAKER Chap 10 Vol 4 Chap 1 Chap 2 Chap 3 Chap 4 Chap 5 Chapter 5 1 Chapter 5 2 Chap 6 Chap 7 Chap 8 Chap 9 Vol 5 Chap 1 Chap 2 Chap 3 Chap 4 Chap 5 Chap 6 Vol 6 Chap 1 Chap 2 Vol 7 Chap 1 Chap 2 Chap 3 Chap 4 Chap 5 Chap 6 Vol 8 Chap 1 DOC DON DOP T POC 2854 PN PP 23
113. Vol 3 Chap 5 2015 G305JP 001 010 G305JP 8 pH 3 8 4 2 730nm 0 01 pH 7 0 02 AG Dickson
114. LOL COR 7 6 x 10 mol D0 10nmol L DO 1 10 Vurk V Vir Vana k t 1 107 1 1000 1 50 CN s o Vat OVaask ts 3 Vol 3Chap 1 BAKKE 2015 G301JP 001 030 G301JP 19 mol L mol kg 9 2 FART bY O ABSGR OT EX CN s o
115. 1999 350nm 2013 1999 10 0 1umol kg SERIE
116. Zhang et al 1999 2 6 4 PRETI IRK CFA CFA
117. NSOP 12 Vol 3 Chap 2 2015 G302JP 001 017 G302JP 12 1 3 AA II Technicony
118. 3 1 R PAR hI DEE Bullister and Tanhua 2010 0 Je 3 CTD Vol 3 Chap 8 CFC_SF6 2015 G308JP 001 009 O G308JP 5 3 O 24 O 2 3
119. Q 1 450 C 3 KAZ GFF
120. X Uu E xx RR JG MEKK wl A3 X Int Vol 1 Chap 1 Chap 2 Chap 3 Chap 4
121. DIW 1L 4 4 FACET h Y CARER 0 04M 248 19 XJ 10g IL DIW 0 04M mol LD Strickland and Parsons 1972 GOES 1994 DIW 2007 2 5 Langdon 2010
122. anoxic water Cli Gite Ou Vol 3 Chap 1 XE VERE IXCKBE 2015 G301JP 001 030 G301JP 25 11 11 1 fix OBE Internatonal E
123. 6 5 6 9 PEPPER Vol 3Chap 1 BAKKE 2015 G301JP 001 030 G301JP 11 20 6 10 RE SOA 7 OO BBAY ICBC DIW DIW DIW DIW
124. T S gt CFC SF F mol kgl atm iX In F a a 100 T a3 In T 100 a4 T 100 7 S bi bz T 100 bs T 100 SF 4 CFC SF atm CEFC SF 100 1 CFC 1 100
125. DIN DON DON DOP TDN TDP DON DOP gt b Ei Vol 3 Chap 10 DOC DON DOP 2015 G310JP 001 013 G310JP 2 cn
126. 444 nm 25876 21904 18460 21891 0 1464 616 nm 36542 38921 25615 38912 0 1542 730 nm 13936 12734 13873 12736 0 0020 0 1542 0 0020 A616 414 0 1464 0 0020 1 0540 Aoi6 A414 25 1 0470 pHr 3 9678 H r 107 7 umol kg Ar 2373 8 umol kg Vol 3 Chap 5 R2015 G305JP 001 010 G305JP 10 9 9 1 fA OFFEMORE pH 730nm LT 9 2 EUEWEKOZMT CRM 9 3 RAH
127. TDN DIN oc Ws GIU TDN DOC TDN Vol 3 Chap 10 DOC DON DOP 2015 G310JP 001 013 DIN DOC TDN G310JP 9 y DIN
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129. 250umo kg 0 040 CN s o Va t Vi4 0 036 Vol 3Chap 1 ARR 2015 G301JP 001 030 G301JP 20 0 015 0 040 0 056 k 2 0 11 250umol kg 0 14umol kg 0 28umol kg VuL 0 1umol kg 100umol kg IOumol kg 0 10 1 0
130. STD PHILS DARDS BEC puteus E i 1 ie DELS ATA S50C 5 E i ZX YY ASA Fit eg c d qu 722325 8E OD US c Lone Vol 3 Chap 10 DOC DON DOP HAO B 201 PTFE
131. XU CBE 5 2 3 5M LOW LOL E 1 MBA AER 1mL Zt pd FA H pH 2 eo Fe S 25 30mm o gt BELAY 11 3 350 LOO MEREL VT RTA YI RAIO HO 6
132. 9 5 x 10 PC Vol 3 Chap 1 2015 G301JP 001 030 G301JP 28 3 5 x 10 C 1 1994 1 73 x10 CC 10C 0 03 Barnett G R and E Hurwitz 1939 The Use of Sodium Azide in the Winkler Method for the Determination of Dissolved Oxygen Sewage Works Journal 11 781 787 Broenkow W W and J D Cline 1969 Colorimetric determination of dissolved oxygen at low concentrations Limnology and Oceanography 14 450 454 Carpenter J H 1965a The Chesapeake Bay Institute technique for the Winkler dissolved oxygen method Limnology and Oceanography 10 141 143 Carpenter J H 1965b The accuracy of the Winkler method for dissolved oxygen analysis Limnology and Oceanography 10 135 140 Craig H 1961 Isotopic variations in meteoric waters Science 133 1702 1703 Culberson C H 1991 Dissolved Oxygen In WOCE Operations Manual Part 3 1 3 WHP Operations and Methods
133. H iu 4 1 Hite HO TRR GM JERK IU 700mL deionized water LAF DIW 600g 197 90 DIW 1L Vol 3Chap 1 ARR 2015 G301JP 001 030 G301JP 4 2 AM BEET RU v A 8M BARR EVEAR I 600mL DIW 320g 39 997 149 89 600g
134. CFC SF Bullister and Weiss 1988 CFC SF m uil 1 Vol 3 Chap 8 CFC_SF6 2015 Q308JP 001 009 H
135. TARTE Ln Chap 2 Chap 3 Is Chap Chap Nn Chap Chap Chap Chap Oo 00 10 Vol 9 Chap 1 Chap 2 Chap 3 Chap 4 Vol 10 Chap 1 Chap 2 Chap 3 Chap 4 Chap 5 Chap 6 XBT XCTD CTD CTD DEE Yay RE LADCP ul D RAIE 2009 G802JP 001 013 G803JP 001 011 G805JP 001 018 G808JP 001 008 G809JP 001 007 G902JP 001 008 G903JP
136. NSOP Nutrient Standard Operating Procedures NSOP CFA assembly T 2010 Hydes DETERMINATION OF DISSOLVED NUTRIENTS N P SI IN SEAWATER WITH HIGH PRECISION AND INTER COMPARABILITY
137. 4 DOP iT 4 1 DOP OPE HIE EX Voal 3 Chap 10 DOC DON DOP 2015 G310JP 001 013 WETAb0OCHS DON DIP TDP G310JP 12 DIP
138. 2 CCFA 2 1 2 2 2 3 2 4 2 4 1 2 4 2 2 4 3 2 4 4 2 5 2 5 1 CFA 2 5 2 2 6 2 6 1 BIRO LEA 2 6 2 2 6 3 2 6 4 2 6 5 2015 6 25 2 7 2 7 1 2 7 2 2 7 3 2 8 1 C 3 3 1 3 2 3 3 3 3 1 3 3 2 QC 333 3 4 H Vol 3
139. ITS 90 IPTS 68 Jones and Harris 1992 ae ITS 90 0 0002 0 99975 IPTS 68 34 0 40 C 11 2 EK OBE 1 t C S Ooifzk FAKE p t Skemi Vol 3Chap 1 EKER 2015 G301JP 001 030 G301JP 26 p t S pw b bo by tb t b C bg t S H Co Cy t 6t SzRdy S 35 LIC pwlt kgm 3 11 1 bo 8 24493 x 10 1 co 5 72466 x 1073 b 4 0899 x 10 3 c 41 0227 x 10 4 b 47 6438 x 1075 c 1 6546 x 1075 b 8 2467 x 1077 b 45 3875 x 10 dy 44 8314 x 1074 cR qc IPTS 68 2 40 S Practical Salinity Scale of 1978 PSS 78 0 42 11 3 ERBAROFR RAKE 5 1
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145. 2 1 2 DON DOP DON DOP DON DOP
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161. sodium hyposulfite 2 1 400 umol L 100mL 40 umol 0 04mol L 4ml 4ml 10mL Vol 3Chap 1 BAKKE 2015 G301JP 001 030 G301JP 5 2
162. CFC SF KAO CFC SFs 1990 CFC 11 CFC 12
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164. 20mL COH 231 5 400umol CO 20mL 0 5 Ho 1 1 5 5 7 hme 630 C 6 12 CO 9mm 10 mm DFO 13
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166. CO 1 GER 1987 2 CO Gurfinkel 1987 3 CO Vogel et al 1984 1 AMS COS 2 3 AMS 3 NES 3
167. 5 2 AEK 5 3 GB E ITK OR DABI 0 05 mol dm 0 65 mol dm 80 umol dm 5 31 ARUBA KFF 200 g 0 01 mg LAND PEZ S Chit CE 5 60 600C 25 0 0 1C 5 3 2 PMIZLEL BAR e 3 dm3 1 Vol 3 Chap 5 2015 G305JP 001 010 fuu A OIE 100 cm FRR cm 500 cm 300 cm PIRU DELAR 0 5 mol dm 5 3 4 RFM SHOTT DURAN JIS
168. C uo ee 650 C 1 oe m Em CO gt 5 9 5 10 5 3 AMDE 1 5 4 AROPE Kitagawa et al 1993 Img 2 Reduction Tube 9mm Vol 3 Chap 9 AMC BC 6 que Jn ER E E 2cm
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170. 4 DIC 6 pH 7 pCO2 CDIAC web SOP http cdiac ornl gov oceans Handbook 2007 html Vol 3 Chap 7 pCO2 G307JP 001 DUMMY 1 O LAU HE CHE 12 CCbE CFCs 1930 1980 CFC 11 CFC 12 CFCs CFC 11 CFC 12 1930
171. TXCKBE 2015 G301JP 001 030 G301JP 13 7 2 1 HDBRHELEO YEN 7 1 1 1 I 5M 7 2 2 JAD HE DIW 3 2 REEE FRAP TF eANS 7 2 3 FURBO D AERO 4 5 5 2 4 10mL 52 5 tC 7 2 4 FEM 1mL 7 2 5 AEA KW mL 10 lt DORT Oo 2 v 382538BfE L CIR Ee STS 7 2 6 VERZI SAI 1 mL I L DIW 1I W 7 2 7 HE
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174. CFC SF CFCs 0 10pmol kg pmol 10 mol SF 0 fmolkg fmol2 10 5 mol Bullister and Weiss 1988 Bulsiewicz et al 1998 fiir jv 5 CFCs SE Vollmer and Weiss 2002 Bullister and Wisegarver 2008 CFCs SFe Sasaki et al 2014 CFC SF amp
175. DOM DOC Dissolved Inorganic Carbon DIC DIC 100 DOC DON DOP Dissolved Inorganic Nitrogen DIN Dissolved Inorganic Phosphorus DIP 100 Total Dissolved Nitrogen TDN Total Dissolved Phosphorus TDP DINE EO DIP DON TDN DIN DOP TDP DIP DIN DIP TDN DON TDP DOP
176. ICP MS ER Vol 3 Chap 2 Eg ry ev 2015 G303JP 001 004 G303JP 3 X ICP MS Sohrin et al Milne et al Biller and Lagerstrom et Minami et al Refer S Lee et al 2011 bic 2008 2010 eetal 2011 Bruland 2012 al 2013 2015 ar E i er MnFeCoN Fe cu cd pp Mm Fe Co Ni Mn Fe Co Ni es D S b ES Baty A Cu Zn Cd Pb NE Cu Zn Cd
177. LNSW ASW NSOP 10 ASW PO NO Si Si uM ks 1 Aminot et al 2009 LNSW ASW
178. AY m 2 FARE Ax a Gm C pH E fa 4
179. Vol 3 Chap 2 Brown amp Bruland 2008 Lohan et al 5 Gosnell et al 2012 Jakuba et al 2008 Lohan Eg ry ev 2015 G303JP 001 004 bay
180. 95 CO 4 10 N 4 8 GAA vU N 1 T1 2 T2 1966C 3 T3 72C CO T1 T2 T3 4 9 BRU ORF 10 T3 4 10 CO DEIR TI KU T2 CO
181. UR G308JP 7 HH H vm KY RICKI IT OVER HS CFC 11 CFC 12 SIO 98 Prinn et al 2000 SFe SIO 05 http bluemoon ucsd edu pub cfchist T T NOAA PMEL Ocean Tracer E
182. Cro tr Vio tr Vr Vuik 8 2 2 Vjk Va Vo tt CNa s o Crkro tL Vra 13 14 Ckro tr pkro Gmkro wkjo DIW KIO3 NMIJ CRM 3006 a 4 5 0 0090 SIL 0 0080
183. 0O Bullister and Tanhua 2010 Bullister and Wisegarver 2008 O 3 2 RKO D DAPRIM EMERY TIL CFC SFs CFC SEF CFCs 100cc SF
184. CO A23 5A C 87C 1 A B US C A B CO 8 C C CO 83C CO A B C CO A C 1 NIES A C 83C COS 4 1 250 mL 500 umol 400 umol 100 umol CO AVC
185. SIO 98 SIO 05 5 1st QC CFC SF CFC SF 11 CFC 12 SE
186. CLS CN DIN DON TDN DIN DON DIN Vol 3 Chap 2 DOC TDN 3 DOC TDN DON
187. Vol 3 Chap 9 AMC bC 6 2015 G309JP 001 018 G309JP 8 4 6 UJ BRIA pH DIC CO 4 7 EFRR OPR 2 1 No N 0 1 0 1 250mL CO 10
188. web site http es ucsc edu kbruland GeotracesSaFe kwbGeotracesSaFe html Biller D V and K W Bruland 2012 Analysis of Mn Fe Co Ni Cu Zn Cd and Pb in seawater using the Nobias chelate PA1 resin and magnetic sector inductively coupled plasma mass spectrometry ICP MS Mar Chem 130 131 12 20 Brown M T and K W Bruland 2008 An improved flow injection analysis method for the determination of dissolved aluminium in seawater Limnol Oceanogr Methods 6 87 95 Gosnell K J W M Landing A Milne 2012 Fluorometric detection of total dissolved zinc in the southern Indian Ocean Mar Chem 132 133 68 76 Jakuba R W J W Moffett and M A Saito 2008 Use of a modified high sensitivity anodic stripping voltammetry method for determination of zinc speciation in the North Atlantic Ocean Anal Chim Acta 614 143 152 2015 G303JP 001 004 el
189. DIW IL 4 3 PMA 6M 600mL DIW 4 3 98 079 1 84g mL 280mL DIW DIW
190. FEA 1 Dickson A G Sabine C L and Christian J R Eds 2007 Guide to best practices for ocean CO measurements PICES Special Publication 3 191 pp http cdiac ornl gov oceans Handbook_2007 html 4 SOP 3a amp SOP 3b 2000 2500 umol kg 2 4 1 kg 0 2 K lt 1045 gt 1045 1 4 HCO3 2 CO3 B OH OH HPO 2 PO SiO OH 5 NH3 HS H r HSO
191. C C MC A AY BRIT AY dissolved inorganic carbon DIC BCPC Dual Inlet FRO Isotope Ratio Mass Spectrometry IRMS McKinney et al 1950 DIC PC C IRMS DIC CO CO IRMS 2012 cavity ringdown DIC BC PC
192. 4 5 6 PaPPRRE 1 4 5 7 B BEENtODIR EE T8f83 7 AHR 250mL 300mL 1 1 SL S 5 1 APARRA ORA 5 1 1 BRM 100mL 8 RSI KA
193. Vol 3 Chap 2 2015 G302JP 001 017 G302JP 16 A Youenou 2007 Recent comparability of Oceanographic Nutrients Data Results of a 2003 Intercomparison Exercise using Reference Materials Analytical Science 23 1151 1154 Aoyama M J Barwell Clarke S Becker M Blum Braga E S S C Coverly E Czobik I Dahllof M H Dai G O Donnell C Engelke G C Gong Gi Hoon Hong D J Hydes M M Jin H Kasai R Kerouel Y Kiyomono M Knockaert N Kress K A Krogslund M Kumagai S Leterme Yarong Li S Masuda T Miyao T Moutin A Murata N Nagai G Nausch M K Ngirchechol A Nybakk H Ogawa J van Ooijen H Ota J M Pan C Payne O PierreDuplessix M Pujo Pay T Raabe K Saito K Sato C Schmidt M Schuett T M Shammon J Sun T Tanhua L White E M S Woodward P Worsfold P Yeats T Yoshimura A Youenou and J Z Zhang 2008 2006 Inter laboratory Comparison Study of a Reference Material for Nutrients in Seawater Technical Reports of the Meteorological Research Institute 58 104 pp Tsukuba Japan Aoyama M C and co authors 2010 2008 Inter laboratory Comparison Study of a Reference Material for Nutrients in Seawater Technical Reports of the Meteorological Research Institute 60 134 pp Tsukuba Japan Atlas E L S W Hager L I Gordon and P K Park 1971 A practical manual for use of the Technicon Autoanalyser in seawater n
194. 5 2 replicate sampling 0 03 McNichol et al 2010 IRMS 6 2 AMC AMS High Voltage Engineering Burope HVEE AMS 6 AMS Ix KET
195. Becker et al 2012 C C 2 BCPC CC POTC DIC BCPC C C CO BCPC 1 IRMS 1940 MC 10 104 Anderson et al 1947 Libby et al 1949 C PC 5730 MC C B
196. F m Vol 3 Chap 9 AMC PC 2015 G309JP 001 018 G309JP 2 MC Tsunogai et al 1995 1970 Accelerator Mass Spectrometry AMS Muller 1977 Purser 1977 1000 1 C 1990 2 3MV AMS AMS 1990 WOCE World Ocean Circulation Experiment 1
197. NDIR NDIR DON TDN CLS NO 2 TOC TOC
198. 6 6 1 RAKE EKARI EESEXR LEO E Y ROI2 EKOA oN ERIK 1 Ti
199. 8PC S3C ppg LAL PDB dT CICA LTH 0 PDB Vienna International Atomic Energy Agency IAEA Vienna PDB Vol 3 Chap 9 AMC 8PC 2015 G309JP 001 018 G309JP 3 3C SBCyppg 2 2 AMC BC C C C Asa CI As 8 C 900 z 61C Asa Asr 1 x 1000 2 AC C 19 C National Institute of Standards and Technology
200. Gordon et al 1993 Lou Gordon A Suggested Protocol for Continuous Flow Automated Analysis of Seawater Nutrients Phosphate Nitrate Nitrite and Silicic Acid in the WOCE Hydrographic Program and the Joint Global Ocean Fluxes Study by Louis I Gordon Joe C Jennings Jr Andrew A Ross James M Krest 1993 WOCE Hydrographic Program Office Methods Manual WHPO 91 1 SOP Dickson et al 2007 Dickson A G Sabine C L and Christian J R Eds 2007 Guide to best practices for ocean CO2 measurements PICES Special Publication 3 191 pp NSOP SOP NSOP Dickson et al 2007
201. Scm 20cm SF 70 170
202. fC 2 GEOTRACES E eo LV y 2006 Measures et al 1995 Obata et al 1993 et al 2003 3 J 4E
203. nij BOUES WE SS TP TN COD Underway pCO2 ADCP TSG G310JP 001 013 G401JP 001 006 G402JP 001 004 G403JP 001 007 G404JP 001 005 G4051JP 001 006 G4052JP 001 004 G406JP 001 006 G407JP 001 003 G501JP 001 003 G502JP 001 006 G504JP 001 003 G505JP 001 011 G601JP 001 009 G602JP 001 006 G701JP 001 007 G702JP 001 004 G704JP 001 141 G705JP 001 037 BH BH BH BH BH Dat HROHR ROME HR OH i rn rn rr Hw
204. 10 2 HEQE Vol 3Chap 1 AKER 2015 G301JP 001 030 G301JP 21 1 umol kg 0 1umol kg 10 2 1 10 2 2 10 2 3 10 2 4 10 2 5 10 2 1 KZZ 2 ORB Vsw_bk mL Vi Vp Vo
205. Vol 3 Chap 2 N G303JP 4 Lagerstr m M E M P Field M S guret L Fischer S Hann R M Sherrell 2013 Automated on line flow injection ICP MS determination of trace metals Mn Fe Co Ni Cu and Zn in open ocean seawater Application to the GEOTRACES program Mar Chem 155 71 80 Lee J M E A Boyle Y Echegoyen Sanz J N Fitzsimmons R Zhang R A Kayser 2011 Analysis of trace metals Cu Cd Pb and Fe in seawater using single batch nitrilotriacetate resin extraction and isotope dilution inductively coupled plasma mass spectrometry Anal Chim Acta 686 93 101 Lohan M C D W Crawford D A Purdie P J Statham 2003 Iron and zinc enrichments in the northeastern subarctic Pacific Ligand production and zinc availability in response to phytoplankton growth Limnol Oceanogr 50 1427 1437 Lohan M C A M Aguilar Islas K W Bruland 2006 Direct determination of iron in acidified pH 1 7 seawater samples by flow injection analysis with catalytic spectrophotometric detection Application and intercomparison Limnol Oceanogr Methods 4 164 171 Measures C I J Yuan J A Resing 2005 Determination of iron in seawater by flow injection analysis using in line preconcentration and spectrophotometric detection Mar Chem 50 3 12 Milne A W Landing M Bizimis P Morton 2010 Determination of Mn Fe Co Ni Cu Zn Cd and Pb in seawater usin
206. 6 8 Jic Hit ts C 100 umol kg 2 0 3 umobkg 0 3
207. OORE 3 Ec c a cc um 4 dead volumes 5
208. Aminot and Aminot et al 2009 Dickson et al 2007 NSOP Dickson et al 2007 RE RMNS Reference Materials for Nutrients in Seawater 7 2 EKORBHERBA RMNS OFA
209. f SF CFCs CFCs CFC 11 CFC 12 SK G308JP 1 B CFCs CFCs CFC 11 CClF CFC HH WE SFe Mie DS FE BE Z Repeat Hydrography GO SHIP Repeat Hydrography Manual CFC SF Bullister and Tanhua 2010 2 CFC 11 CFC 12 SFe
210. 1 7 3 ImL 7 2 10mL Eia o at TZSCKBE 2015 G301JP 001 030 G301JP 9 Ng 5 2 6 JETT 250mL 500mL DIW DIW 7 1 2
211. av 11 3 4 8 2 2 RATIH 1 6 4 5 CN _s o Imol CNa s o 6 Ckio tL Vio ti Vsta Voi 16 Cro tr ilit PC KIO mol L 8 1 2 Vio ty tr PCH KIO mL 8 2 1 Vsa NasS gt O mL 7 2 8 b bb LCS Volk E 3E mL 7 3 10 8 3 ABP RPERORE 8 3 1 APP ORREA n moll 7 1 7 2 CN _s o molL 7 3 Vol 3 Chap 1 ARR 2015 G301JP 001 030
212. dud etu ee ea is pia d oo d ud LUE Froelich and Pilson 1978 Dias et al 2006 2 5 2
213. Aon 0 7459 ANox 1 2 25 8 Cypps 1000 5 IO 869 Cvpps 17 8 5 0 02 Aon 0 7459 ANox 1 25 1000 1 SBCvppB 1000 6 MC Aon 1950 Aass Stuiver amp Polach 1977 Vol 3 Chap 9 AMC BC 2015 G309JP 001 018 G309JP 4 Aass Aon ex 1990 7 y A X MC 1 8267 yr 2 Asr Aars E INA LC 6C 4C C SBC 25 DIC C 0 15 MC 6 C
214. CLS CLS TDN 4 5 uM 100 pL 0 4 0 5 nmol 6 7 ng TDN NO NO CLS NO NO NO NO NOx NO
215. 11 3 2 ERBROBRE te C V t mL V t 1000 w fruoy Pw te 36 w gh Vol 3Chap 1 BAKKE 2015 G301JP 001 030 G301JP 27 fbuoy 11 3 3 pw t te C kgm 11 1 11 3 3 AIREZ 5 T Pai Pwes on fy 1 Pair Psample grc
216. DOP DOP TDP 0 1 uM TDP 0 02 uM DOP DOP
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219. 1 T1 5 7 CO VADER T1 CO CO Pressure Gauge CO 5 8 KERRE CO H CO gt 2H C 2HO 13 53 7 CO 2 H 2 1 2 2 H Kitagawa etal 1993 5 9 KEZ ORE COW AR ERED SIRT EO PRC SES CORRS
220. 2 3 7 3 2 HRBRWERE Og 7 2 1 7 3 3 FADER 2 DIW 3 2 7 3 4 3 ORY Y V ABROR 2 KORRI S VREY OD ARW ImL 2mL 2mL 1mL 2 1mL 2 1mL 2mL 7 3 5 MBI mL 1mL Vol 3Chap 1
221. 2012 http www chemistry or jp international atomictable2012 pdf 1994 JIS R3503 http kikakurui com r3 R3503 2007 01 html 2013 JIS K 0102 http kikakurui com k0 K0102 2013 01 html Pai S C G C Gong and K K Liu 1993 Determination of dissolved oxygen in seawater by direct spectrophotometry of total iodine Marine Chemistry 41 343 351 Rue E L G J Smith G A Cutter and K W Bruland 1997 The response of trace element redox couples to suboxic conditions in the water column DeepSea Research I 44 113 134 Strickland J D H and T R Parsons 1972 A Practical Handbook of Seawater Analysis Fisheries Research Board of Canada Ottawa 310 pp 2007 56 327 332 FH Vol 3Chap 1 RKR 2015 G301JP 001 030 G301JP 30 UNESCO 1981 Tenth report of the joint panel on oceanographic tables and standards UNESCO tec
222. 2 Asay HBO Ald Str Asa O Asn e VC 2 Asr AAss 8 Anps Aon Stuiver and Polach 1977 dC AsA Aon 1 x 1000 11 DC Asn Aon 1 x 1000 12 dC 0 DC HIZ C AMC EE Asal Aon pMC percent modern carbon MC Stuiver and Polach 1977 Mook and van der Plicht 1999 3 Vol 3 Chap 9 AMC 8PC 2015 G309JP 001 018 G309JP 5 1 DIC 89C LAMC 3 CO
223. 500 mL AMS MC Key et al 2004 MC B NN NN Fi Img 30 0 5 ORE MC AMS AMS AMS C WOCE McNichol and Jones 1992 McNicholet al 2010 1997 AMS 1999
224. CP Silica Plot CP PoraBONDQ Agilent X SF 1 16 3A 10cm 2 3 2 EZR 38 J OC SNEOBLD AMET A UV amp bkv 7 0A J 7V EE A U lt LEEK RE AT D Vol 3 Chap 8 CFC_SF6 2015 G308JP 001 009 G308JP 4 1
225. Kitagawa et al 1993 5 7 NES 3 4 Vol 3 Chap 9 AMC 8PC 2015 G309JP 001 018 a G309JP 10 MIT CO Tube for CO volume measurement Reduction Tube z Sample Cracker ae rease less Pirani Gauge Grease le Stop Valve E Pressure Gauge d Stainless steel Joint Glass Tube Stainless steel Tube Quartz Tube M3 5 2 FMR OEE Vacuum Pump Cylinder NIES 10 um
226. Aminot and Kirkwood 199 RMNS RMNS 1 3 3 3 RNIOZ van Ooijen Bakker EA IH FH FIZY Vol 3 Chap 2 2015 G302JP 001 017 G302JP 7 7 3 BABAR OH ARDER
227. L mol 15 9994 1 g mol 3 E io amp Wi E Vol 3 Chap 1 eil XE VE 2015 G301JP 001 030 G301JP 3 Mn 20H gt Mn OH J 2 2Mn OH 0 gt 2MnO OH J 3 4Mn 0H 0 2H 0 gt 4Mn OH 3 1 4 2MnO OH 417 8H 2Mn 21 6H20 5 4Mn OH 3 417 12H gt 4Mn 21 12H 0 6 1 2 CHS
228. 99 98 G305JP 4 Ff 1 dm 3 1 1 120 g 600 C 1 De 113 9180 g 1 95 mol ACEH 1dm 2 AIC 0 1818 g 240 umol FERCA 0 5 mol dm 0 30 dm 0 15 mol HCD 1 3
229. 4 813C AMC 3 1 LELBA RE 3 1 1 EKRA KAP CO 250 mL 300 mL McNichol et al 2010 AMS C 1 mg 80 umol IRMS 8 C 1710 DIC 2000 umol L 100 mL 10 450 3 7 2 L M N 10mL 3 1 3 LEER II
230. 3 0 01 6 4 4 6 4 5 ER BA 300 cm
231. Certified Reference Material CRM 7 1 FUR 6 4 CRM pH 3 8 4 2 3 7 2 IHE DP A hmol dm 10 Ar VcrM H Veg YHcl PCRM 10 Vua Cua ArCRM CRM Vcsw CRM 2 Vew psw CRM CRM 25 0
232. ii 3 2 WEF Vol 3 Chap 2 Ridal and Moore 1999 Yoshimura et al 2014 DOP DON TDP amp DIP DOC DON DTP H amp TDP A DP
233. 2015 CARE 8 1 0 0100N 1 6 14100N 1600M Cooperative Study of Kuroshio Standard Solution 034 10251 1 4 5 1 ETRO a KAFE 200g 0 01mg X TCH ET DEREZ AVIA VAOP BACHE 10kg 10mg WE CR ZELMA DH Melis 2 4 5 2 I VRBES Y VADER 0 5 g ZLATE FHL OST FEE IC BE LC PER AIT HO 130 C c 2 4 5 3 AVKBVY GADE 0 36g Lf 4 5 4 I ORR Y DA OE 1L
234. 6 2 FELDE 6 3 WEBROOT ERE Dickson A G Sabine C L and Christian J R Eds 2007 Guide to best practices for ocean CO measurements PICES S
235. ASHE 1987 2015 G309JP 001 018 G310JP 1 DOC DON DOP 1 Dissolved Organic Matter DOM 3 Dissolved Organic Carbon DOC Dissolved Organic Nitrogen DON Dissolved Organic Phosphorus DOP DOM DOM
236. CO IRMS 6 1 AMS SC A2C 2003 AMS AMS BCPC IRMS A C 63C A C MC Vol 3 Chap 9 AMC PC 2015 G309JP 001 018 G309JP 16 2
237. quality assurance program quality control quality assessment Taylor 1987 traceable in control
238. 2 4 2 RKF E PEE BR NSOP 7 ES 3 1 3 3 4
239. DIC C 1950 Linicketal 1978 CO 1970 GEOSECS Geochemical Ocean Section Study 39 18 230L CO CO Stuiver and stlund 1980 stlund and Stuiver 1980 Stuiver and stlund 1983 1980 E Gamo and Horibe 1983
240. uncertainty 1999 Vol 3Chap 1 CABS 2015 G301JP 001 030 RE
241. 5 69 C IRMS 6 1 CO 4 12 PEREO ERHI 4 11 CO CO 1 5 ANC 83C 88C S 2 CO0z AMS MC CO
242. 8 8 1 CRM CL GIG BERE OHE CRM ArCRM 2224 65 umol kg CRM 33 357 Verm 42 7495 cm Vc 2 05 cm CRM 25 14 C 1 0221 g cm 25 32 C Vol 3 Chap 5 2015 G305JP 001 010 8 2 G305JP 9 J K p BOGE 444nm 25827 21890 18305 21863 0 1490 616nm 36417 38894 27596 38868 0 1202 730 nm 13883 12699 13816 12679 0 0014 0 1202 0 0014 Aeie A414 0 1490 0 0014 0 8050 Aoi6 A414 25 0 8026 pHr 3 8483 H r 141 8 umol kg Caci 0 050577 mol dm EKE VOS YS YE 34 424 Vow 42 7495 cm Cha 0 050577 mol dm Vua 2 15 cm 25 22 C 1 0228 g cm 25 73 C
243. 6mm N 4 m 5 3 3 2015 G309JP 001 018 G309JP 11 6500 5 10 5 5 CO ZR Oe fi CO 4 11 3 1 Sample Cracker CO 4 NIES 4 M4 5 6 CO WX OMA CO 196eC
244. 1 av ts tJ 18 Va k t t C mL 5 1 1 av 11 3 4 8 3 3 RATIA t C C t mol L ae Csam ts 1000 nsam Vaask ts z Vise 19 nsam mol 8 3 1 Vaask ts t PC mL 8 3 2 Veg HERK I IL mL 5 1 3 25 5 C 8 3 4 BEEN S t C p t S kg m C t mol L C mol kg 11 2
245. G309JP 13 6 1 56 C 6 1 1 EGE X IRMS 89C 8 C CO IAEA 2 1 83C CO 8PCvpps 1 95 NBS19 Bowen 1966 100 4 2 25 CO 25 f I CO 98 C 880 Oztech 89Cvpps
246. HF H3PO D HT k 3 2 toa s c mu N Kk pH Vsy dm Cc mol dm Cc dm HTr 10 D psw kg dm 2 Cpa Vici H r Vsw Vui 2sw 2 Ay Vow Psw
247. 2010 Vol 3Chap 1 TXCKBE 2015 G301JP 001 030 4 0 01 umol L Wong et al 2010 Wong etal 2010 E E EE 10 2 5 Da2 FEN E 69 mp PRBRREOMEH CTD Pressure dbar Concentration umol kg 3 L umol kg 9 ii X hi Concentration umol kg N w Winkler Oxygen umol kg eo 0 1 0 06 0 3 umol L 7 0 15 umol kg G301JP 24 a gt BC 1 umol L 1 2 3 Se
248. 3 pH 3 8 4 2 4r a 65 BFADIVEOHR 6 5 1 WE LE RKEORIE 444 nm 616 nm 730 nm 3 7 H amp t 7v Zeit 7 A Ax EA 5 0 3 730 nm
249. Chap 5 Chap 6 Vol 2 Chap 1 Chap 2 Chap 3 Chap 4 Chap 5 Vol 3 Chap 1 Chap 2 Chap Chap Chap Chap Chap Chap oc 10 MN BB WwW Chap S Fy St te SI A Ei B Bl ae G101JP 001 007 GOOS G102JP 001 009 G103JP 001 006 Essential Ocean Variables TEOS 10 2010 3A rH amp G105JP 001 010 rH G201JP 001 019 G202JP 001 002 G203JP 001 015 G204JP 001 G205JP 001 002 G301JP 001 030 G302 P 001 017 N P Si G303JP 001 004 DIC G304JP 001 G305JP 001 010 pH G306JP 001 pCO G307JP 001
250. ARKE 2015 G301JP 001 030 G301JP 15 7 3 6 HERKEN KU IL mL 10 lt CV FRETS AURA BEL CHEE 53 5 7 3 7 ERIE KU 1 1mL eMACHETS 1 L DIW 7 3 8 WHE Vi mL 7 3 9 2 KA OE 2mL 7 3 7 3 8 MS V2 mL 7 3 10 REZI Z ORF 12 Vi VRALL PART IVY RATA bRORKT I V 7 hee ee 2 3 Vox ml 8
251. G301JP 17 16 17 1 1 5 cada Vit Vok _ pg reg Nsam 4 CNa s 0 1000 17 Ca s o NasS2O mol L 8 2 2 Vac mL 7 1 6 Vok mL 7 3 10 DO TI mL 7 6 x 10 mol Murray etal 1968 5 1 3 2mL 8 3 2 BRMORA t C 6 8 Va t mL Vaask ts Vaask te
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255. 1 5 1 3 5 2 1 2 4 DW 113 1 EFRA OH fi 3E EGRE LC FH ETKI 200 g ClassE2 0 3mg 0 001 g
256. 33 umol kg 10 nmolkg umol kg 10 2 5 NaN Barnett and Hurwitz 1939 3N3 NOz 4H gt 5N 2HO 31 2013 IL 4 2 1L 10g 9 OK Wong 2012
257. C S Wong 1986 Storage of reactive silicate samples by freezing Limnol Oceanogr 31 1139 1142 Mee L D 1986 Continuous flow analysis in chemical oceanography Principles applications and perspectives Sci Total Environ 49 27 87 Mostert S A 1988 Notes on improvements and modifications to the automatic methods for determining dissolved micronutrients in seawater S Afr J Mar Sci 7 295 298 Olafsson J and A Olsen 2010 Nordic Seas nutrients data in CARINA Earth Syst Sci Data Discuss 3 55 78 Vol 3 Chap 2 XEM 2015 G302JP 001 017 G302JP 17 Skeggs L T Jr 2000 Persistence and Prayer From the Artificial Kidney to the AutoAnalyzer Clinical Chemistry 46 1425 1436 Strickland J D H and T R Parsons 1972 A practical handbook of sea water analysis 2nd Edition J Fish Res Bd Canada 167 311 pp Tanhua T P J Brown and R M Key 2009 CARINA nutrient data in the Atlantic Ocean Earth Syst Sci Data 1 7 24 Taylor J K and H V Oppermann 1986 Handbook for the quality assurance of metrological measurements National Bureau of Standards NBS Handbook 145 Vijverberg F A J M and W P Cofino 1987 Control procedures good laboratory practice and quality assurance ICES Techniques in Marine Science No 6 Zhang J Z 1997 Distinction and quantification of carryover and sample interaction in gas segmented continuo
258. CEFC SF CEFC SF 2 6 CFC SF Bullister J L and Tanhua T 2010 Sampling and measurement of chlorofluorocarbons and sulfur hexafluoride in seawater In The GO SHIP Repeat Hydrography Manual A Collection of Expert Reports and Guidelines E M Hood C L Sabine and B M Sloyan eds IOCCP Report Number 14 ICPO Publication Series Number 134 Available online at http www go shi
259. Chap 2 2015 G302JP 001 017 G302JP 4 3 4 1 4 4 1 4 2 4 2 1 422 4 2 3 4 3 4 3 1 2008 INSS Imternational Nutrients Scale System 5 RMNS 5 1 RMNS 6 6 1 7 8 Vol 3 Chap 2 K R 2015 G302JP 001 017 i G302JP 5 Nutrient Standard Operating Procedures NSOP Vol3 Chap 2 KEM Bir
260. Pb Cu Zn irc E Pb Pb Resi Nobias chelate jm NTA Superfl Nobias chelate Nobias chelate Nobias chelate M PAI dan em PAI PAL PAL IDA resin Magnetic Magnetic Magnetic Magnetic ICEMS dubols Sector Quadrupole Sector Sector Sector Automatic Automatic Automatic Detection Limit nM Fe 0 036 0 021 0 07 0 014 0 014 0 09 Cu 0 005 0 007 0 12 0 052 0 003 0 02 Pb 0 001 0 0002 0 0005 0 00056 0 0009 Mn 0 01 0 007 0 002 0 002 0 003 Zn 0 06 0 005 0 03 0 016 0 1 S Cerufied valne National Research Council Canada NASS 6 GEOTRACES GBOTRACES SAFe GEBOTRACES
261. x 3 E S bai NSOP 1 NSOP2 NSOP 3 NSOP4 NSOP5 NSOP6 1 NSOP 7 NSOP 8 NSOP9 CFA NSOP 10 control charts NSOP 11 NSOP 12 2015 G302JP 001 017 1 G302JP 6 11 KXBOFF CFA CFA Kerouel 2007
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268. FARK AR IT 10 g 100 mL D 20C 100 mL g ID ID 3 1 4 BIE OD 50 uL 10 mL 3 2 2 as 3 1 5 FATS TE REHE 3 2 2 LI fv u 3 2 RRF 3 2 1 FEKAR 3 4 DIC DIC
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273. P 16 tj PC 7 2 3 KIO E55 Co t moLL Cio Pw tL Ckro tr 4000 14 Crio KIO ERRO mol kg 8 1 1 pw tr KIO tt DIW kg m 11 1 p tr KIO 0 04 DIW 1 8 2 FIRT hU A Na2S203 BEDRE 8 2 1 KIO EYED OZ E KIO 5 2 4 tr PC 7 2 3 tc PC1 t C KIO Vo tr mL Vito ti Vigo tc 1 ay t te 15 Vo tc tc PCH KIO mL
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277. g mL 13 25 5 5 1 4 KAF HS HAICERER v 6 1 3 Hr 0 1C cr 0 30C AAA HL 1kHz WL xy xx c LCD CERE E M ee M1 2009 Vol 3Chap 1 EKER 2015 G301JP 001 030 5
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285. pecial Publication 3 191 pp 4 SOP 12 SOP 13 http cdiac ornl gov oceans Handbook_2007 html 6 4 FERK PHEKY IADE 6 4 1 EIL PL EKG OTALEBATS 730 nm 616 nm HT 444 nm 3 Z Vol 3 Chap 2015 G305JP 001 010 G305JP 6 6 4 2 P TNIH AXI pH 3 8 4 2 Kb PUT VERE LIZED TERZA CURT 5 6 4 3 CAEKTEREORHKELWET S 6 4 1
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