キラル分取テクノロジー
Contents
1. 2013 11 1m kg 2015 9 GMP HPLC SFC HPLC SFC SFC Alcyon su 10 3 8 0 25 mg injection 6 V12. 2015 5 Y7M 600 8106 284 YMC 4F TEL 075 342 4503 FAX 075 342 4530 108 0014 5 29 20 601 TEL 03 5439 9790 FAX 03 5439 9791 URL http www ymc CO JjD 15052K
3. LC Forte R LC Forte R 1 g SMB SMB 30 mm 4
4. 0 1 m 50 L min GMP 2015 9 uy X IN 20 30 mm i 3 FF F X mm 1 5 g day 20 X 250 1 LC Forte R 50 mL min 4 140 000 2 10 g day 30 X 250 1 LC Forte R 50 mL min 4 800 000 120 600 g month 50 X 250 1 LC Forte R300 300 mL min 9 700 000 0 5 2 5 kg month 100 X 250 1 LC Forte R750 750 mL min 0 2 1 ton year 600 mm 2 20 L min 0 6 3 ton year 1000 mm 2 50 L min 1 2 Amylose C KAN99S05 2520WX KAN99S05 2530WX KAN99S11 2550
5. 2 0 1 10 1 5 1 0 0 5 Column YMC Omega 10 um 250 X 20 mml D Eluent methanol Flowrate 20mL min Temperature ambient Detection UV at 210 nm Sample EPA 4 mg mL Injection 2 mL 5 10 15 min 1 05 mL g L ads hr 7 L ads mL mg g g ton J ti 100 1000 mm 1000 mm A kpeeue 50 mm 0 100 600 mm API GMP 2 0 recycle SFC SMB
6. LC Forte R LC Forte R 50 mL min 20 20 100 g 0 2 1 kg LC Forte R 50 mL min 2 10 g 40 200 g 0 5 2 kg LC Forte R300 300 mL min 120 600 g 1 7 kg mm LC Forte R750 750 mL min 25 125 g 0 5 2 5 kg 6 30 kg 20 L min 18 90kg 02 1ton 50L min 1000 3 13 kg 50 250 kg 1 1 8 2 1 20 3 1 240 A _ nn 1 J LU 3 9 0 Flurbiprofen gt mAU 750 Column CHIRAL ART Cellulose C 5 um 250X4 6 mml D Eluent hexane 2 propanol TFA 95 5 0 1 Flurbiprofen Flow rate 1 mL min 500 Detection UV 254 nm Injection 5 AL 1 mg mL Rs 2 07 250 T
7. I T LT 12 mg 560 mg Flow rate 45 mL min Flow rate 45 mL min i 0 0 87 4 89 mg racemate hr L g product 2 5 3 9 SMB 0 4 0 1 5 5 8 9 50 0 mL min 30 MPa 20 30 mm 250 mm 4 PLC WxDxH 780x385x760 mm YMC EPA HPLC EPA EPA SMB SMB 1 5
8. S KAN99S11 25A1 S um X mm 5 20X250 5 30X 250 10 50X250 10 100X250 A 1 16 B 1 8 SFC X Gn Cellulose C KCN99S05 2520WX KCN99S05 2530WX KCN99S11 2550 S KCN99S11 25A1 S Alcyon SFC CSP Amylose C Alcyon SFC CSP Cellulose C Amylose SA KSA99S05 2520WX KSA99S05 2530WX KSA99S11 2550 S KSA99S11 25A1 S 24 Cellulose SB KSB99S05 2520WX KSB99S05 2530WX KSB99S1 1 2550 S KSB99S11 25A1 S Alcyon SFC CSP Amylose SA Alcyon SFC CSP Cellulose SB 840 000 1 500 000 2 200 000 3 950 000 500 000 1 450 000 10X250 KAN99S05 2510WTS KCN99S05 2510WTS KSA99S05 2510WTS KSB99S05 2510WTS 20X250 KAN99S05 2520WTS KCN99S05 2520WTS KSA99S05 2520WTS KSB99S05 2520WTS um Amylose C 10 KAN99S11 1 200 000 20 KAN99S21 1 000 000 Cellulose C 10 KCN99S11 1 200 000 20 KCN99S21 1 000 000 Amylose SA 10 KSA99S11 1 400 000 20 KSA99S21 1 200 000 Cellulose SB 10 KSB99S11 1 400 000 20 KSB99S21 1 200 000
9. 30212D5 4 V130212B5 CHIRAL ART CHIRAL ART Cellulose C Cellulose C 2 1 2 3 4 5 6 7 min 0 0 01 0 10 1 00 10 00 mg injection lt 5 mg injection UP O X 20 V130212D7 7 Stilb Id rans Stilbene Oxide CHIRAL ART LE UE EE ESEC Cellulose C 0 1 2 3 4 5 6 7 min SFC 3 trans Stilbene oxide Column Alcyon SFC CSP Amylose C 5 um 250 X 4 6 mml D Eluent CO2 methanol 60 40 Flow rate 3 0 mL min Temperature 40C Detection UV at 220 nm Back pressure 17 2 MPa 2500 psi mAU Column CHIRAL ART Amylose C 5 um 250 X 4 6 mml D Eluent n hexane 2 propanol 90 10 Flow rate 1 0 mL min Temperature 25C Detection UVat220 nm 300 200 100 LC Forte R combination g 1 0 kg ton 0
10. 7 MM 1980 HPLC SFC Alcyon SFC
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