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Analytical Circle No.38（2005.9）

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4. No uuuuduue o ue 000000000 635 05791 NMIJ CRM 4201 a o DDTI 0 0 Y 199 13 600 638 05801 NMIJ CRM 4202 a p p DDE 0 0 190 13 600 635 05811 NMIJ CRM 4203 a y HCHO 0 i 9 196 13 600 632 05821 NMIJ CRM 4204 a p p DDT p p DDE y HCH i j li 9 1g 15 420 x4201am204aq niynngaggggaagga dgnue gaggduanugnangangnagngamnganggaggaaannuaunugngaggnggnagnnagungdnaunn nue G S Wako Analytical Circle No 38 O i J J J00 1 Droe IDUDDUUIUDUATPDOUUIUDUDDDUUIUDUDUDDUUIUIUDUDUDOFDAI DODOPATE OOO DD ODO DD OOO DD 0D 0D 0D 000000000 ODO DO OOO D ODO FDAQO DO DO DD 000 00D 000000000 pagagadgc ooo li li ga 00000000080 00000000000006 ATPJ000006 ATP Mg DO0B00ATPDODODDD0 gggagagnagaaagnaggnue d Luciferin Oxyluciferin Ll Ll ll ll i ll ll l1 l l ATP NS DO J IJ LJ LJ Li i IJ Il ll J LJ LJ Li Li Li ji O2 CO PPi CA uuutdmiubtulettATRIE AMP Luciferase oooo3o00 00000000006 j ATP J DO 00000000 D00000000000000000 w pooooooo0o00000004000000000000000 A a ea ogooo10000000000 SES A ATP PA li i li li Ii li Ii ji i i Ii li li Il li i II 1 i sali 1 8 oD0000000000ATPg000 Me werk epooo00 000000000000 Se sx 20000 RLUDO 0 0 e 1 Pallehak 124 ZALUM E 23 ATPODOD0 0 RLUJ cful 0 0 pgapbogo00000000000010 0000ATPOOO OC 000000 0 RUH cfud ago 0000010 cfu pooo000
5. j j ODO DDD i Li i LJ J Ll H ll i Hl l 0000000000000 No 0000000009 632 05941 000000000 EPMADI are J4x10x1500000 169 100 639 05951 i Se ane eist 210 169 100 636 05961 H HUDUDUDUPEPMADUS serine 1 191500000 169 100 o god Hl Il 0000 48 000000 0000 Polystyrene 2400 IIS DADO DO LI LJ DO DO DO DO Ll i Ll LJ i LJ LIJ ji Li Li ji ji II DO DO ODO MD OD DO DD ODO ODO DO DDD ODO DT B D UU EI CI C oooo000000000000 25 0000000000 sEcDpePCIHD DU UU DU EB IB J III TI 000000 ucuMmgnagagagagnagadune No uuguguue ge 000000000 634 05521 NMIJ CRM 5001 a po000000000 00000 PS2400 0 290 8 220 631 05531 NMIJ CRM 5002 a 0000000000000 III 55500 0 499 9 480 638 05781 NMIJ CRM 5003 a 0000000046000 0 2 o 57 140 LL DD 00 0 H NI Sl p DDT 0 0 i L L L L L L POET in 2 2 4 Trimethylpentane pU ugmammpbpupsbpuumnu uugupaubpgmmummugiilubuiybHW DH m Hi ll HI B DO DO OD TI j j j j J J J Ll LI Lb pop Ii i H po00 TI J II TI IJ DSCH J J LI TI III T II TI III II 0000000 040000000 6 00 000000000 1 1 1800 00 2 210 00 441 O Ll Ji LJ a dd 000 p e 2BB100 00000000 000000002 24N0000 0 Hl Hi HH ooo oo II li 00000000000 LU DD Li Li EI mg kol p P DDTODO 9 74 0 65 a LI
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7. Os miunjj VIl Joxide PEM Microencapsulated PEM MC OsO 9 D0d0000 000000 KsF CND LJ II Li DE J II J UO BI UO IJ II LI j J 7 Ji 00Rp0000000060 d40002000 000000000000 0000 0000000000 PEM 00000 Phenoxyethoxymethyl polystyrene 000000000 i y ugPEMggudauguggudagggduggagaugugagguugauucg e 4 ge ugggaagmuuuguaauggtaguuttdtttttruksrFe CND O O o OPh L LI IJ IJ Li gg da 1 LI III ooo I I i I I J li III J III 00000 lj li Ii i li li IH li li n PEM polystyrene 4 000 PEM MC OsOg 5mol q1 9 OH DHQD PHAL 5mol HO Ee Gr PH H20 acetong 11176 KsFe CN s K2COs 30 C 5h Run 1 2 3 Yield of Produdti 8560 6660 8460 e amp 9q19 789 789 7869 Recovery of Catalyst 6 quant quant quant OR N OR OMe DHODPPHAL 0 0 O No ne Uu D TI Ijj i l mon 158 02411 Osmiuntj Vlljoxide PEM Microencapsulated 20 000 0000000 DO P T Anastas J C Warner Green Chemistry Theory and Practice Oxford Univ Press 1998 49 D00000 00000 070000000000 lH p149 199916 O O S Kobayashi M Endo S Nagayama J Org Chem 63 6094 19980 DO S Kobayashi T Ishida R Akiyama Org Lett 3 2649 2001 eillbnuluubBsuguubpguguupbpuvmmnmimuougnmnsagguspaagpgmbgBWdmusgHWibdgHdu Lulu 0000 ER EHI N HI H N DI DD EKR KH D HINO HI HENIN DI D DIDA H D H H D DID B H HAH I N DI NI DD H NE H N H li H l
8. li ji li ll l Wako Analytical Circle No 38 2 OO J LI IJ J J IJ LI II LI II Hi CHEMICAL DESIGN Ver 3 0 oo U 938100 38 FI DES C 2 2 5 REN PR TED EDROD Te Y E CHEMICAL DESIGNO 0 0 gt 000000000000000000000000 E une E a CHEMICAL DESIGNH DD D n Bag DU li EE J EM ME Er B HEN N c UU D J J Ll e 00000006 j i Li i i i i i a ii Hi i i i i i i i HL l LL gt 0000000000000000000000000 m 0000000 0000000 0000006 1 i Li j i i jIj 00000000 HI N HI HE N N D DIHI HI l li PocketP C PDA 0000000 HED HEN HEHE H HI HI HEB 11111111 HI HI N DIR HEJ DIR ED ET ET ET ET ET ET ET ET DD DH gi mi TELA DE ELE 0000 0000 0 HAUT cw N E HIN N EHI a NNN N N S GER E ET ET ET ET ET i HB E EL G M D Wako Analytical Circle No 38 9 specification 000000000000000 Dj Dj DD D Di j Dj jj d H li li j li li li li l li li Ii li 1 Ii 1 I1 l 1 ll l Il 1 1 E I I
9. 10025 4 Hydroxy 2 chlorobiphenyl 100ug m 9 1mi Isooctane 3 800 585 70791 HPCB 1003N4 4 Hydroxy 3 chlorobiphenyl 5mg Neat 6 000 HPCB 100356 4 Hydroxy 3 chlorobiphenyl 100ug m 9 1mi Isooctane 3 800 588 70801 HPCB 1004N0 4 Hydroxy 4 chlorobiphenyl 10mg 9 Neat 12 000 1004 4 Hydroxy 4 chlorobiphenyl 100ug m 1m Isooctanee 5 000 585 70811 HPCB 2001N4 2 Hydroxy 2 5 dichlorobiphenyl 9 10mg 9 Neate9 15 000 HPCB 2001S4 2 Hydroxy 2 5 dichlorobiphenyl 100ug m 9 1m 0 Isooctane9 5 000 582 70821 HPCB 2002N4 3 Hydroxy 2 5 dichlorobiphenyl 10mg Neate9 15 000 HPCB 200256 3 Hydroxy 2 5 dichlorobiphenyl 100ug m 9 1mi Isooctane 5 000 589 70831 HPCB 2003N94 4 Hydroxy 2 5 dichlorobiphenyl 10m9 Neat 15 000 HPCB 2003S4 4 Hydroxy 2 5 dichlorobiphenyl 1004 9 m 4Y 1mi Isooctanee 5 000 586 0841 HPCB 2004N4 4 Hydroxy 3 5 dichlorobiphenyl 9 10mg Neate9 15 000 HPCB 2004S4 4 Hydroxy 3 5 dichlorobiphenyl 100ug m 9 1m 0 Isooctane9 5 000 583 70851 HPCB 2005N 2 Hydroxy 2 3 dichlorobiphenyl l0mg Neate9 15 000 HPCB 200556 2 Hydroxy 2 3 dichlorobiphenyl 100ug m 9 1m 0 Isooctane 5 000 580 70861 HPCB 2006N6 2 Hydroxy 3 4 dichlorobiphenyl 10mg Neat 15 000 HPCB 2006S 2 Hydroxy 3 4 dichlorobiphenyl 100ug m 9 1m 0 Isooctane9 5 000 587 70871 HPCB 3001N4 2 Hydroxy 2 4 6 trichlorobiphenyl l0mg 9 Neat 15 000 HPCB 3001S4 2 Hydroxy 2 4 6 trichlorob
10. o00000000000000000000000000000 LC nn ied eiue Methanol 0000000000000000000000000000000 Methyl Alcohol 00000000000N0000000000Nd Lot Norman 9 Ay Jj 9 3 F7 p 7 4 00000000000NeoJ 0 0 D No 6 Coe sa 000 No Ii Il ll I No I Il 123 45678 nnn 9 rs NM FEET 030 50000000006 cx EEA CIN 0000000000000000 CET 000No 00000000No00ABC123400000 UR 4 cemmrxasen a ca reique Methanol JUUL U 11 n na 9 0049009 CH OH 32 04 67 56 1 UN1230 BIGE ent p 20 Q 0 791g ml 998 GCH 889165 S 99 T GC Y for Chromato 00000000 for Preparative Chromato 0000000000 for LC MS MS for Trihalomethane Anal 9000000000 for Boron Anal 000000 for Dioxins Ana 0000000000 e for Enviroment Anal J for Spectrochemical Anal J Methanol 300 00000 300 for REJPCB Anal 0 0 O DOPCBO i A El n 67 56 10 UN1230 D WE ABE Methanol 5000 5000 for REJPCB Ana 1D D HI PCBI DD 9 Ami Dhenia maj l 67 56 11 UN1230 SIE BENE Metanol Dehydrated HOOD O 0 0 A O D 50ppnri O 6 Organic Synth 0 0O 000 b Ch eninge CH OH 32 04 67 56 11 UN1230 D WE ASE OWako 3L rd SE Le u mn r pi p a n H
11. 100 AquaTestil AT 1000 10 3 500 305 15531 PXR 03 AT 1000 500 00 00 17 9 8 000 306 15321 PXR 02 000000 ATI 1000 ne 10 6 8 000 Wako Analytical Circle No 38 O No H Li i i li i i ue ne 0000000006 308 13201 ATB 50 9 AquaTest Il ATB 50 D50mpx50000x208 25 000 304 14401 ATB 100 Aqualest ll ATB 100 100m x 5 x 2 0 30 000 ugaggaegsnungupngm nuaduuguue No H Li i i i j i ue ne 0000000006 307 13411 ATB 50C9 AquaTest Il ATB 500 000000 10 2 000 306 14581 ATB 100C9 AquaTest ll ATB 1000 ge 3 000 304 13421 PXR 01 000000 00000 0000 5 000 D0000 3 Ii i Ii 1 i 000000000000 No H Li i i i j i ue ne 0000000006 309 09441 8 02 Du n a n nu 0000000 00 e 5 600 300 09471 BL4BLB peo 0000000000 Do e 1 700 KN B nnn nnn nn IZ CR Jas 000000 00 0000 DH li DU DN NIN D N H i BAN B N No37roooid 000000 00 00 O 00 puuugezu ammpigulutlutlutlt 00 H il TI Il 101 HHH 00 0000 201010 000020109 00100010000 000009 0 00 4740 0008 D I l Li HT HO LL HET LI l i HIL H E I HR Ri N NL Hi Hi li L N HL N N HN N N ll Hi lI 0000006
12. Di DEN DL N D N a DID D N O oo0000000000 JE N TE L T I 9 forte BPX5 po0o00 0000000 360 370 Q 1u mil i i 9 5000060 uMspnpnune forte BPX35 3a5wnpnuue 000080000000 360 370 l MSH li 0 forte BPX50 5ownpnuue 000080000000 360 370 ce l MSH li forte 0000000 TET EN E TET EE Ey a Bear eo Figure TINWUBERDEREENETI 0 nue BPX5 BPX35 BPX50 0547519 forte BPX50 0 5 m film 30mx0 25mm ID Split Splitless 240 C0 8081 mix with internal standards 10mg L 5ng per component on column L 1 3mL min 9 40 C 1min 30 C min 1 90 C 3 min 10 C min B 00 C 5 min FID 9 310 C9 HEHE DD DD NNN N E o o DEHN TTE D Organochlorine Pesticide 8081 Mix A 2 4 5 6 9 xylene9 B 8 C B BHC D y BHC E 6 F Heptachlor Aldrin H Heptachlorepoxy tetrachloro meta 9 a Chlordane 9 Endsulfan AG pp DDE9 Dieldrin y Chlordane Endosulfan Endrin Aldehyde pp DDT Endosulfan Sulphate Methoxychlor9 Endrin Ketone 9 Decachlorobiphenyl See BPX 5 0 17e D D L H C LI 30m 60m mene mane P N 000000000 P N 0000000009 0 25 0 25 054101 72 100 054102 126 700 032 0 25 054145 81 400 054146 140 700 029 0 25 054701 72 100 054702 126 700 0 32 0 25 054724 81 400 054725 14
13. Hydroxy 2 3 4 5 tetrachlorobiphenyl 10mg Neat 15 000 4004 5 3 Hydroxy 2 3 4 5 tetrachlorobiphenyl 100ug m 9 1m Isooctane 5 000 583 70971 HPCB 4005N6 3 Hydroxy 2 3 5 6 tetrachlorobiphenyl 9 l0mg 9 Neat 15 000 HPCB 4005S4 3 Hydroxy 2 3 5 6 tetrachlorobiphenyl 100ug m 9 1m 0 Isooctane 5 000 580 70981 HPCB 4006N4 4 Hydroxy 2 2 4 6 tetrachlorobiphenyl 5 Neat 12 000 HPCB 40065 4 Hydroxy 2 2 4 6 tetrachlorobiphenyl 100ug m 9 1mi Isooctane 7 500 587 7170991 HPCB 4007N94 4 Hydroxy 2 3 4 5 tetrachlorobiphenyl 10mg Neat 15 000 4007 4 Hydroxy 2 3 4 5 tetrachlorobiphenyl 100ug m 9 1m 80 Isooctanee 5 000 584 71001 HPCB 4008N60 4 Hydroxy 2 3 4 6 tetrachlorobiphenyl 9 5mg9 Neat 15 000 HPCB 4008S4 4 4 Hydroxy 2 3 4 6 tetrachlorobiphenyl 100ug m 9 1mi Isooctanee 5 000 581 71011 HPCB 4009N4 4 Hydroxy 2 3 5 5 tetrachlorobiphenyl 10mg Neat 15 000 4009 4 Hydroxy 2 3 5 5 tetrachlorobiphenyl 100ug m 9 1mi Isooctane 5 000 588 71021 HPCB 4010N6 4 Hydroxy 2 3 5 6 tetrachlorobiphenyl 9 l0mg 9 Neat 15 000 HPCB 4010S4 4 Hydroxy 2 3 5 6 tetrachlorobiphenyl 1004 9 m 4 1mi Isooctanee 5 000 585 71031 HPCB 5001N4 2 Hydroxy 2 3 4 5 5 pentachlorobiphenyl 9 l0mg 9 Neat 15 000 HPCB 5001S4 2 Hydroxy 2 3 4 5 5 pentachlorobiphenyl 100ug m 9 1mi Isooctane 5 000 582 71041 HPCB 5002N94 2 Hydroxy 2 3 5 5
14. O 0520772 0788 0 9e 0 U O DO O 029 8582278 0 el i O 02212223072 0 9e 1 0 0 O O 0117271 0288 0 6 e0000 O 0822856381 0 16 0300700 0120 052 099 Jg 0120 052 806 WODODDDDDDDDDD DMDDDDDDDDDDDDD D E mail analytigwako chem co jp n e URL http www wako chem co jp 05 913 01H D 0 10nm j De MDGRAPE 2 4 9sec step IRF Xeon MDGRAPE 2 v 919419 jponAqpuy N O de Y eo
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16. i li e LC MSHI Hi i Ii Ii li i 9 9 m z50 20000 0000000000 epooo000000 Hl III IIIE ag li li j ji li j ji 000000000006 00400 LC MSH i i li li i li li li j Wakopak MS 5C18 GT einmugggnpnnmgaunpnmnpnuaugaugggpnuuge eQ000000000000000000000000 No e 0e 0000000000 214 01301 110 1 600 210 01303 gitrapure Water LC Mg 319 2 800 016 19854 100m 0 1 900 012 19851 Acetonitrile LC MS 9 1 5 600 018 19853 3 13 000 132 14524 100m 4 1 050 138 14521 Methanol LC MS 9 1 1 600 134 14523 3 3 450 018 20061 LC MS 9 50m 5 500 067 04531 Formic Acid LC MS 9 50m7 9 000 No 00000 Tinnnn 1 TITIT e TI j j Ti TI TI D De 001 00030 Wakopak MS 5C18GT 2 0mmex100mm nguune 9 000 56 000 59 000 Wako Analytical Circle No 38 G TK q u u n n uni e ll ll j J j j j j j Il j J LI i i DADO BO ll OD LJ Il J LJ LJ Li Li Li Li ne ji Li UBDDBDBDDLL 1i 00006 000 MESO Trise 00000 00000080000 H6 3 3 0 095 c LZ H l ii li Hi i l li i j j i li l D l ll D H6 30300 60 C9 D gt 4D D D 95 00000P 000 200m D 06 kanonne 00 PAD 000006 000000000
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19. 0 700 0 25 0 25 054751 72 100 054752 126 700 0 32 0 25 054761 81 400 054762 140 700 o Wako Analytical Circle No 38 G W Ginn nnunsone C Wako Q HDPRLCUDUDUUDUDUUDUUDUUDUUDUUDOUDUOUDODUDUDUDUDUDUDUDUDUUD UU Li Li j BOBO jI jJ ji ji ji Li ji ji i J i LJ Li Li Li LJ J J LJ J LI J J i i J LJ J Li 0000006 A uBpuggugpaopugugbpuauguggpuggugsagpBuguppbtuluuuHPLC DUDUUButtutubu pooo000000000000006 IUDUDDDUUDUDUOUUUDUoRUDUDUDDUUIUUUUUUUUUUTI ooo000000000060 0000 6 0000 i 00000 ooie 0000000 0000000000000000000000000000000000 00000000000000000000000000000000000 0mo00000 0000000000 000000000000000000000000 0000000000000000000000000000 000000 00000 0000000000000000000000000000000000 ee 0000000000 Je gt 000000000000000000000000000000000 0000000000000000000000000000000000 0000 000000000000000000000000000000 0004 00000000000000000000000000000000000 0000000000000 00000000000000000000 Ee 00000000000000000 000000000000000000 00000000000000000000000000000000000 0000000000000000 9 BE nun DOUDDUDUDUDOUUDUDUUDUUDUDUDUDUUUUUDUDUUDDUDDDUOUUOUOUDUDDUOUUDDUDUDUDUOUODUI
20. 000000000000 SERRA AT PIRSINEN P TEBER PL UCCFLIORRE A ni ena roc 18404 eg d y AE 0110 A ammo E Ba a IEE Wi LEE Ki HT LEX INNER La LTE LALIE EEN LEET ATP EAE 00 e 0000006 0000000 WE 000000000000 egoggg000000 egogo00000000 egog00000000 li Il li lI li lI sp00000000000000 O Wako Analytical Circle No 38 0000400000 000000000000 H li j j li li l1 SCDH Hi 8002400 00RLUD O m 24 D BD D 4D DU UL UO DO D RLU UI gele az lati OB DO DO DD OD DO DD ODO RLU E dure ATC MIE FP aeruginosa ATL DT EU NH e A D min ATOE piir ALI H MAA AA Ll i i j i i ii l HHH 0000000 ue 0 ge po00000006 373 01901 136736 0000000 10 1 800 000 373 01881 71429 00000000 500 00 ue n 35 000 370 01891 7150 10 0 46 000 ugmngnue l HHH 0000000 ue 0 ge aggggumuue 372 01851 71399 nguuugggguggsg 9 1000 9 4 400 SU T2 71466 00000000000000 000000 0 1000 6 6 700 Dero NN 7147 uggaguggggmnpuuuguggunpnagnpnnnnogune 1000 6 6 700 ugaagnue l HHH 0000000 ue 0 ge 000000000 378 00851 131579 0000000 9 10 120 000 370 00931 15402 unnpngnamuanunrne 10 168 000
21. 6 pentachlorobiphenyl 10mg Neat 15 000 HPCB 50025 2 Hydroxy 2 3 5 5 6 pentachlorobiphenyl 100ug mi9 1m 0 Isooctane 5 000 589 71051 HPCB 5003N94 4 Hydroxy 2 2 3 4 5 pentachlorobiphenyl 9 5mg Neat 12 000 5003 4 Hydroxy 2 2 3 4 5 pentachlorobiphenyl 100ug m 9 1mi 9 Isooctane 7 500 586 71061 HPCB 5004N94 4 Hydroxy 2 2 3 5 6 pentachlorobiphenyl 9 5mg Neat 12 000 HPCB 5004S4 4 Hydroxy 2 2 3 5 6 pentachlorobiphenyl 100ug m 9 1mi Isooctane 7 500 583 71071 HPCB 5005N4 4 Hydroxy 2 3 3 4 5 pentachlorobiphenyl 5mg9 Neat 15 000 HPCB 500556 4 Hydroxy 2 3 3 4 5 pentachlorobiphenyl 1004 9 m 4 1mi Isooctane 5 000 580 71081 HPCB 5006N80 4 Hydroxy 2 2 3 4 5 pentachlorobiphenyl 9 5mg Neat 15 000 5006 4 Hydroxy 2 2 3 4 5 pentachlorobiphenyl 100ug m 9 1mi Isooctanee 5 000 587 71091 HPCB 5007N 4 Hydroxy 2 3 4 5 6 pentachlorobiphenyl 9 l0mg 9 Neat 15 000 50075 4 Hydroxy 2 3 4 5 6 pentachlorobiphenyl 100ug m 9 1mi Isooctane 5 000 HPCB 5010S4 2 Hydroxy 2 3 4 5 6 pentachlorobiphenyl 100ug m 9 1m 89 Isooctane 12 500 580 71101 HPCB 6001N 4 Hydroxy 2 3 3 4 5 5 hexachlorobiphenyl 9 l0mg 9 Neat 15 000 60015 4 Hydroxy 2 3 3 4 5 5 hexachlorobiphenyl 100ug m 9 1mi Isooctane 5 000 587 71111 HPCB 6002N6 4 Hydroxy 2 3 3 5 5 6 hexachlorobiphenyl l0mg Neat 15 000 HPCB 6002S 4 Hydroxy 2 3 3 5 5 6
22. Ana T Peru Circle TAN 2005 9 0000000 The United States Pharmacopeial Convention Inc 0 0 0 0 00 d O 4 03 No 38 EMISIT TT 96 TUUM 97 OC E IE ICC A e A A E A S 98 CR 7 4 TE 49 ppp 0000000000000 0000000 NM CE TIRO TT 0 ERE HEN A EET 92 COE PE DEDI NN N 4 4 4 94 Eft f B LIE DE DD DIDIN EE TO R T DP entero ORE 94 Bin D AH li Lj pns Hl DER nnt Je Hp Hn a li n an Bn OL BI S caet ree 2 po o00000 0000000000000 Aquarestl DD O 44 00 e 46 ugmuugggugg CHEMICAL DESIGN Ver 3 0 98 Bb j E E EL 010 0 D o ED L E E 0 l HI B HIN ER N B SMe 0 0000 WEBBER ccm uc K A TT TT 95 mma u Ba EE E 260181 T 9 00000000 P 276 LC MSHI O O P 60 0000000000 P 776 pe cmm EE p i 2 40091 L li i i i li g uUBDbpBpuupgapnppuuutuioppiuutututututuututudtuduutul uUuggugpuguugsmiuuliuiiutuwHor Li Li i Ii i i Li li Di i li Uuugggmuguppuguggispusupubpuguubmuiuuuputctern a4 L LJ Ll LJ i J Li J Li TI Li Li ji Li i LIJ J LJ J LJ LJ J LJ Li Ll ji Li Li Li jJ Li ji pooo000000000000006 00000 Hl L li Ii 1 li 1 Ii 1 HH 1 I I po0000 NN Tt pon n N ugeuuunn unnme Halogenated Acetic Aci
23. G TK U O O OUUU ng miim HIJ pee eeeee 0 0 ad T 0000000000000 VA J qm E n u N n n N a na n BA e 30r li li li ji li Ii Ii li Il i li Il Ii 9 80 9 pooo0000000000 D nneannnuuuuuuue YAT ETT TIE Q 9 210229 927429 I 9 uuuugaoo5e 10 50 7 0 p O0 O0 0 0 0780000000 10 190229 ne 10 20 21 0 0 0 0 0 0 p8s8p 40000000004 g EL Ni a B os ue 11 150 170 9 ugivzgunaggggguauue 11 160179 I 9 e p28q0000000000 12 705109 J ALI HI UDI U U UU U U e p 035000000000 12 13015 Do0000000000000 Wako Analytical Circle No 38 Q Ll IJI HI HL L1 0000 AquaTestt 88 TJp ZA 2YTAhklIz AICBS SB X Xef AA A 7 515658 U 2 U 7c DOO0O 0C00O0C0COO0O0C0000001000000000000000000000000 uugguumnmnaubpaugsgbugbiuusmuiumiuliluuATB 50 50m0 Il ATB 104 10009 00000006 Dado ng o god 0 0000000000000 ATI 101 10m 0 0 ATI 100 100m ooo 000000000 DOABODO DO DO OD DO DO DO DD OD DO DDD ODO ODO J Li Li i Li ji oo00000000000000000000000000000000000000 DOABOBDO DO DO OD DD O DO DD OD DO DDD ODO ODO Li Li Li i H li H
24. N i lia B N Il Hi Ni N Di Ni H N N Di HIN D N ed 000010000000 00 0000000000000 ugue ID ND DN DII N ND HIN N N li 40000000 epa aa 0000000000000 00 0 0 00 0 0000 li li Hl Ii HE 00000 j j j J ll 0000 lij i li li B B E B J L li li Fl iuuiutture DEEE Lal 1 E li 111111 000000 ugggnuuguggagiugaggnduduue l N N N H L N 000000000000 0 00000 DD DN RE EHE ELS EE LEE EE LED E BID N i a dp loto D DI ND DN aa E D B ND DIJ E E ER Rn n eoe DI DHI DI N DI HD N N HI N li iwnugaggangguggmgiuaggougagga ggagagg pom o00000000 00 0 0 0 G M Wako Analytical Circle No 38 0000000000000000 11640 Wako pegao 0000000000 12000 D0000 10000000000000000 BOBO DO 0 00000000 2000099000000000 m uggudgggaugdgugugauuduue 2 l j i j ji l i i l II i i TI lI i i i i I i HIN DI ND NIN ND Ni HO DL DI DI DI DIDN N DIJID TN N D uggagagmgmuudiuudtatztuerttytubtuttutlut 4 p paagaggagagagaguue uggagagmgpgudugugutgztmtmututertbtuttLtutlut gdggnagagune Hugagamgmiubpuegttziustu erttyttubtlutt 6 000948000000000 ugguggggagagggdgugagduuuese E N L V uuggggaggdgugugggdgdggugau
25. OH PCB IL li D Y 21 DO00000000000000000000000000000000000000000000000000000 AccuStandard punuuuennunuuuue D ne D n D n ue nuun mnne HBP 001N 2 Hydroxybiphenyl 100 Neat 3 800 0015 2 Hydroxybiphenyl 100ug m 9 1mi9 MeOH9 3 800 HBP 002N 3 Hydroxybiphenyl 100mg Neat 3 800 HBP 0025 3 Hydroxybiphenyl 100ug mi9 1m i9 MeOH9 3 800 HBP 003N 4 Hydroxybiphenyl 100mg Neat 3 800 HBP 003S 4 Hydroxybiphenyl 100L g mi 1mi9 MeOH9 3 800 HBP 004N 9 2 2 Dihydroxybiphenyl 100mg4 Neat 3 800 HBP 004S 2 2 Dihydroxybiphenyl 100ug mi9 1m MeOH9 3 800 HBP 006N9 4 4 Dihydroxybiphenyl 100mg Neat 3 800 HBP 006S 4 4 Dihydroxybiphenyl 1000g mi9 1mi9 MeOH 9 3 800 HBP 009N9 2 5 Dihydroxybiphenyl 100mg Neat 3 800 HBP 009S 2 5 Dihydroxybiphenyl 100ug m 9 1 MeOH9 3 800 581 70771 HPCB 1001N4 2 Hydroxy 5 chlorobiphenyl 9 5mg Neat 6 000 HPCB 1001S 2 Hydroxy 5 chlorobiphenyl 100ug m 1m lsooctane 3 800 EN Wako Analytical Circle No 38 AccuStandard pnuunuuennunuune D LD E 588 70781 HPCB 1002N9 4 Hydroxy 2 chlorobiphenyl 9 5mg9 Neat 6 000
26. d Mixture Standard 086 07261 EL M I Butyl Methyl Ether Solution 100006 O 12 000 l j HI N TI HTH HITD HHH 3 Chlorinated Acetic Acids Mixture Standard 035 19321 Solution 1mg m t Butyl Methyl Ether Solution 10000 Lmx5 AO 7 000 po une ll Il ll HI HHHNn 0000000 3 Chlorinated Acetic Acid Methyl Esters Mixture Standard Solution 1mg ml t Butyl Methyl Ether Solution 00 000 DD D DD DD 000000000 00000000004 New 030 19631 uuguue 2 m x5A 8 000 e ggggue O O No ge ge 0 000000000 Phenanthrene d o Standard Solution NEW b 1mg m Hexane Solution j 000006 Eun did dune Ne nu9 ugue D u9nuununmmuune osea a on Sandard Soton 6 some Ap 034 19411 nn 000000000004 50m 4 000 H Li li li ii li i i i i i nnne Ne 0 0 D D D n nn nnn m n engen DEET Doonga 2mxsa 5400 nune i No 023 15301 t Butyl Methyl Ether Standard Solution 1mg m Methanol Solution Wako Analytical Circle No 38 NEW 10000 pugpgnggggpgngg 000 O O U No 012 20341 ne Acrylamide Standard Solution 1mg m Methanol Solution H i li i I1 1 1 IH Ii i No 220 01561 0e Vinyl Acetate Monomer Standard Solution 1mg m Acetone S
27. hexachlorobiphenyl 100ug m 1m Isooctane 5 000 ciini 0000 uunuuennunuuue A3 A 0 ne LD n rn n n 00111101 302 000 Wako Analytical Circle No 38 8 AccuStandardjj 0000000000 pnunuuennunuuune D D naa e iii MSCB 30496 3 Methylsulfonyl 2 2 4 5 tetrachlorobiphenyl 50u g ml 1m lsooctane 37 500 MSCB 30524 3 Methylsulfonyl 2 2 5 5 tetrachlorobiphenyl 50u g m 1m Ilsooctane 37 500 MSCB 30704 3 Methylsulfonyl 2 3 4 5 tetrachlorobiphenyl 50u g m 1m lsooctane 37 500 MSCB 30874 3 Methylsulfonyl 2 2 3 4 5 pentachlorobiphenyl 50u g ml 1m lsooctane 37 500 MSCB 30914 3 Methylsulfonyl 2 2 4 5 6 pentachlorobiphenyl 5 0u g ml 1m lsooctane 37 500 MSCB 31016 3 Methylsulfonyl 2 2 4 5 5 pentachlorobiphenyl 50u g ml 1m lsooctane 37 500 MSCB 31104 3 Methylsulfonyl 2 3 4 5 6 pentachlorobiphenyl 50u g ml 1m lsooctane 37 500 MSCB 31326 3 Meihylsulfonyl 2 2 3 4 5 6 hexachlorobiphenyl 50u g ml 1m lsooctane 37 500 MSCB 31416 3 Methylsulfonyl 2 2 3 4 5 5 hexachlorobiphenyl 50u g ml 1m lsooctane 37 500 MSCB 31496 3 Methylsulfonyl 2 2 4 5 5 6 hexachlorobiphenyl 50u g ml 1m lsooctane 37 500 MSCB 31746 3 Methylsulfonyl 2 2 3 4 5 5 6 heptachlorobiphenyl 50u g ml 1m lsooctane 37 500 MSCB 40496 4 Methylsulfonyl 2 2 4 5 tetrachlorobiphenyl 50u g ml 1m lsooctane 37 500 MSCB 40524 4 Methylsulfonyl 2 2 5 5 tetrachlorobiphe
28. i Ii li 00000000000000000006 0 AquaTest 1000000 0000 0000 50989 0000000000 DU gg 500 0000000000 1 EO LU LL UU 0 00 XGal aaa 1 00 0 MUG 0000000000 0 1014 IPTG H li Hi i 2001H j i i i lI li i Hi li li li li H li Hi li Ii li Hi i li Hi li i li i i Hi li H ii i li Hi li Hi li Hi li Hi li Hi i Hi li j li li i ne uggue 10 m 100 mi 000000000024000 egnggmagggagnagnmnunue ak egnmugmumsuggggggnunue HI ll Il l1 Il Il H J 100ml 0000000000 BU ji i II ji i li li ji mM0000001000000 0 H AquaTestil j 000000000000000 pDo0000000 0 100m5 0000000010 000000002400036 1 910000 80000000000 000000 H lJ Hi pg og I1 og gg o gd Il Ii Ii Ii i Ii Ii 000000 enunundggagaunune unge u ugggugdgdagwgigggmggugudmmgduu ieri rn a m E 00000M000000000000000000 e n n j ATB100Cu n ATI 10061 H H H HH HEH 0000000000006 D00000000000000000000000000 enununguagaunuuue 5 l go gd II II II Bl i 0000000000000 000000000 H i i No ugunnnuue D 08 D Jnunnnmune 304 1660 30 000 ungngegeunuguungwmnngununuandnunanunue H j I1 No 0000000 ne ne 0000000006 307 14251 ATI 10 Aquatest Il ATII 10 10m x100 0x20 28 000 309 14691 ATII 100 Aquatest Il ATII 100 100m x100 0 e 43 000 Hl ll III nop Ii i i Ii 1 000000004 H j No 0000000 ne ne 0000000006 309 14571 ATI 10 AquaTest ll AT 100 j 1 j i I 10 1 500 302 14701 ATI
29. i li H ooo 100000000000000000 ELE IJ E EH EL 200 00 0 027 638 05541 uum 0O00 0000 0 O00 0000000000000 00 00 BE HIP DODODOD i TI Ll i Ll LJ jJ jJ Li J Li J LJ LJ Ll Li LJ J Li Li jJ ji ji po0000006 IIJ ll BIIBII DILL Li 0000000000000 100000000000 Li i li O No 0000000 Y je ge 000000009 637 05511 NMIJ CRM 1016 a p 0000000 cr 40 XI 0 e nm3aopmnenunnn9 154 400 637 05751 NMIJ CRM 5202 a 113x1300000000 36 660 634 05761 NMIJ CRM 8001 a TJ Ij Tj jj li li II Ij poo ooo meo I I j Ij j 50g 16 910 631 05771 NMIJ CRM 8002 a II P IL j 500 16 910 Wako Analytical Circle No 38 2 0000 4 1 gu nu ddunmue Li wm DAD BOB HI Ll DO ll i J L Li J i Ll i DI j 1 j Li i ji 00000000 EP MALI i li li li li i Il 1 H IH I I Il H HIL DO DO J TI Li i J J i i LI J J Li LJ J LJ J Li LJ C ll j U U E B OO DD J Li J ILI LIJ Li Li i Li Li Li ji Li TI UI J H U EL
30. iphenyl 100ug m 9 1m 80 Isooctanee 5 000 584 70881 HPCB 3002N0 2 Hydroxy 2 5 5 trichlorobiphenyl 10mg Neate9 15 000 HPCB 300256 2 Hydroxy 2 5 5 trichlorobiphenyl 100ug m 9 1m 0 Isooctane 5 000 581 70891 HPCB 3003N4 3 Hydroxy 2 4 6 trichlorobiphenyl 10mg 9 Neat 15 000 HPCB 3003S4 3 Hydroxy 2 4 6 trichlorobiphenyl 100ug m 1m Isooctanee 5 000 584 70901 HPCB 3004N 4 Hydroxy 2 2 5 trichlorobiphenyl 9 5mg Neat 12 000 3004 4 Hydroxy 2 2 5 trichlorobiphenyl 100ug m 9 1mi 9 Isooctane 7 500 581 70911 HPCB 3005N 4 Hydroxy 2 3 5 trichlorobiphenyl 5mg 9 Neat 15 000 HPCB 30055S4 4 Hydroxy 2 3 5 trichlorobiphenyl 100ug m 9 1mi 9 Isooctane 5 000 588 70921 HPCB 3006N4 4 Hydroxy 2 4 6 trichlorobiphenyl 10mg Neat 15 000 HPCB 3006S4 4 Hydroxy 2 4 6 trichlorobiphenyl 100ug m 1m Isooctane 5 000 585 70931 HPCB 4001N 2 Hydroxy 2 3 4 5 tetrachlorobiphenyl 9 l0mg 9 Neat 15 000 HPCB 4001S4 2 Hydroxy 2 3 4 5 tetrachlorobiphenyl 1004 9 m 4 1m 80 Isooctaneb gt 5 000 582 70941 HPCB 4002N80 2 Hydroxy 2 3 5 6 tetrachlorobiphenyl 10 Neate9 15 000 40025 2 Hydroxy 2 3 5 6 tetrachlorobiphenyl 100ug m 9 1m 0 Isooctane 5 000 589 70951 HPCB 4003N 2 Hydroxy 2 4 5 6 tetrachlorobiphenyl l0mg Neat 15 000 HPCB 4003580 2 Hydroxy 2 4 5 6 tetrachlorobiphenyl 100ug m 9 1m Isooctane 5 000 586 70961 HPCB 4004N94 3
31. iphenyl ether 4 OH BDE 49 50ug mi 1 AcCN9 62 500 HBDE 4003S CN 3 Hydroxy 2 2 4 4 tetrabromodiphenyl ether 3 OH BDE 47 504 g mi 1m AcCN 18 800 HBDE 40045S CN94 5 Hydroxy 2 2 4 4 tetrabromodiphenyl ether 5 OH BDE 47 50ug mi 9 1m AcCN9 18 800 HBDE 5001S CN 4 Hydroxy 2 2 3 4 5 pentabromodipheny ether 4 OH BDE 90 50u g m 1m AcCN 81 300 CLD 0 a 1 OHBDE 51906 6 Hydroxy 2 2 4 4 tetrabromodiphenylether 13C12 99 6 0H BDE 47 5 0u g m 2 Hydroxy 2 4 4 5 6 pentabromodiphenyl ether 13C12 99 AccuStandard l 00 0 0 0 06 unuuneuuuunumue L Ue ueu pen i j n n MOBDE 200154 3 Methoxy 2 4 dibromodiphenyl ether 3 MeO BDE 7 50u g m 1m MeOH9 18 800 MOBDE 300154 4 Methoxy 2 2 4 tribromodiphenyl ether 4 MeO BDE 17 504 g m 1m MeOH9 35 000 MOBDE 30025S 4 3 Methoxy 2 4 4 tribromodiphenyl ether 3 MeO BDE 28 50ug mi 1m MeOH 9 18 800 MOBDE 400154 4 Methoxy 2 2 3 4 tetrabromodiphenyl ether 4 MeO BDE 42 50u g mi9 1mi MeOH9 70 000 MOBDE 40025S 4 4 Methoxy 2 2 4 5 tetrabromodiphenyl ether 4 MeO BDE 49 50ug mi 1m MeOH9 62 500 MOBDE 4003S 3 Methoxy 2 2 4 4 tetrabromodiphenyl ether 3 MeO BDE 47 50ug mi 1m MeOH9 18 800 MOBDE 400454 5 Methoxy 2 2 4 4 tetrabromodiphenyl ether 5 MeO BDE 47 50u g mi 9 1mi MeOH9 18 800 MOBDE 50018S 4 Methoxy 2 2 3 4 5 pentabromodiphenyl ether 4 MeO BDE 90 50u g m 1 mi MeOH 81 300 0000000000000
32. n OHBDE 5206 1 2 6 Hydroxy 2 2 4 4 tetrabromodiphenylether 6 0H BDE 47 5049 m 12m Nonane 99 700 550 67271 OHBDE 5206 1 2 6 Hydroxy 2 2 4 4 tetrabromodiphenylether 6 0H BDE 47 50u g m 4x1 2mi Nonane 395 000 OHBDE 5212 1 24 4 4 Hydroxy 2 2 4 5 tetrabromodiphenyl ether 4 OH BDE 49 50u g mi 1 2mi9 Nonane 131 400 557 67281 OHBDE 5212 1 2 6 4 Hydroxy 2 2 4 5 tetrabromodiphenyl ether 4 OH BDE 49 50u g mii4x1 2mi Nonane 521 900 OHBDE 5214 1 249 6 Hydroxy 2 2 4 5 tetrabromodiphenylether 6 OH BDE 49 50u g mi 1 2mi9 Nonane 163 900 552 67471 OHBDE 5214 1 2 49 6 Hydroxy 2 2 4 5 tetrabromodiphenylether 6 OH BDE 49 50u g mi 44x1 2ml Nonane 652 000 OHBDE 5 2 28 1 2 6 Hydroxy 2 2 4 4 5 pentabrmodiphenylether 6 OH BDE 99 50u g m 1 2mi9 Nonane 131 400 554 67291 OHBDE 5228 1 2 6 Hydroxy 2 2 4 4 5 pentabrmodiphenylether 6 OH BDE 99 50ug mi 4x1 2m Nonane 521 900 AccuStandard puunueuuuuuuue 0 ne H n n uu n r nnn m n HBDE 20015S CN4 3 Hydroxy 2 4 dibromodiphenyl ether 3 OH BDE 7 50u g m 1m AcCN 18 800 HBDE 30015S CN 4 Hydroxy 2 2 4 tribromodiphenyl ether 4 OH BDE 17 50ug mi iml AcCNe 35 000 HBDE 30025S CN4 3 Hydroxy 2 4 4 tribromodiphenyl ether 3 OH BDE 28 50ug mi 1m AcCN 18 800 HBDE 40015S CN94 4 Hydroxy 2 2 3 4 tetrabromodiphenyl ether 4 OH BDE 42 50ug mi 9 1m AcCN9 70 000 HBDE 4002S CN 4 Hydroxy 2 2 4 5 tetrabromod
33. nyl 50u g m 1m lsooctane 37 500 MSCB 40644 4 Meihylsulfonyl 2 3 4 6 tetrachlorobiphenyl 50u g ml 1m lsooctane 37 500 MSCB 40706 4 Methylsulfonyl 2 3 4 5 tetrachlorobiphenyl 5 0u g m 1m lsooctane 37 500 MSCB 40876 4 Methylsulfonyl 2 2 3 4 5 pentachlorobiphenyl 5 0u g m 1m lsooctane 37 500 MSCB 409168 4 Methylsulfonyl 2 2 A 5 6 pentachlorobiphenyl 5 0u g ml 1m lsooctane 37 500 MSCB 41014 4 Methylsulfonyl 2 2 4 5 5 pentachlorobiphenyl 50u g m 1m lsooctane 37 500 MSCB 4110 4 Meihylsulfonyl 2 3 3 4 6 pentachlorobiphenyl 5 0u g m 1m lsooctane 37 500 MSCB 41324 4 Methylsulfonyl 2 2 3 3 4 6 hexachlorobiphenyl 50u g ml 1m lsooctane 37 500 MSCB 414194 4 Meihylsulfonyl 2 2 3 4 5 5 hexachlorobiphenyl 50u g ml 1m lsooctane 37 500 MSCB 41496 4 Methylsulfonyl 2 2 3 4 5 6 hexachlorobiphenyl 50u g ml 1m lsooctane 37 500 MSCB 4174 4 Methylsulfonyl 2 2 3 4 5 5 6 heptachlorobiphenyl 50u g m 1m Isooctane 37 500 O icmspoon LE MSPO BOO O BO DO OO BBD OOO DO DO OO DDD OOO DDD OOO DD 00000000000 DADO N R H R B H B R ODO DD ODO ODO DD ODO B RR B DD ODO ADO DDD DD ODO BD LED B T E CI 000000006 D0Oo0OoLtc MS OO O0DoD0oLce MS ODO Doo o 00000 BBD DDD DO 000000000 Li Li Li Li li ooooooLemsggad000000 4 e 0 00 po000000000M4ppp00006 sf li ll Hl HI 0000000006 sf lj i j li i l Ii II gg HHH 00000006 lj li ji 1 Ii Ii li
34. olution NnNgodo i i 1 I1 1 1I O No 043 29431 LI lI LI Li i O No 197 13791 ne N N Dimethylaniline Standard Solution 1mg m Methanol Solution 0000 ne otyrene Monomer Standard Solution 1mg m Methanol Solution Hl LI Ii i i li Ii i li li i li Il i l1 1 AH 1 O O No 165 21881 ne Pyrene d o Standard Solution 0 2mg m l Dichloromethane Solution H III Hi 1 Ii l Ii H li H Ii H li o Ii 200000000 De The United States Pharmacopeial Convention Inc 0 0e ggnunue 0 e ggnunue ue ggnuue 0 ue ggnuue 0 0e i i l 0 Ll li li i Ii i e 2m x5A 9 300 0 00000006 2mix5A 4 700 ueuuuuuuue 2m x5A 4 900 0 000000006 2m x5A 4 500 ueuuuuagdue 2m x 5A 8 000 KN S lj ji li li Il U SP II i i e USP i i IJ Li IJ II II TI USP L Li ji i i II II II i Li i Li Li Li li li II II LI TI U SP Li Li Li Li i Li Li Li i DUU po00000000006 10000 Uu DULL HEB HINE uuguguue LB HL E BEBE HIN BNN EH BEER 000006 No 20000000 ue poo 0000000 531 13371 123550360 0000000 10000EU 52 300 572 36941 160900264 000004 125mg0 41 900 524 94401 155900664 250mg0 52 300 536 72921 155950564 pon 0000 1000000004 30Tablets 60 200 533 72931 1609501 ugupngapnmginnnuunone 33Tablets 52 300
35. uue 8 Q uudggmyggyupgmgugguggHuHmg ummmnunnunuuuuuuuuununne MID DUIUDUDIUIUDDUID DUDU UI OO000000000000000000000000 DOOC0O 0C0O00C0000C00M0O000000000000000000000000000000000000000 0 ggggmagganugaagnaggaaaauagaagagngaagaggdgnme 0 06 MEN 0000000006 00000000006 H Hi li i ll lI I iil 1 1 7 00000006 T pw oo000000000000000006 OsDa M stla Blank Get MG Det 2 min 3days MC OsO4ggnnangunupngpangggugngddllH 0504 dee SA 000060 50mg T OO MC OsO4 OsO4 J O 50mg TI O ugmumnauuguuguMc osod gogoo 000060 UD uu n i li HE WI o000000006 VIl Joxide Microencapsulated MC OsO 9 Hl Hi li li i Hi li li ji i li i li li li li l li li 1 li 0 E 9 ne DO0000000000000N00000000 N0 0000 NMOLH Hl 0008000000000 000 OH MC OeCH 5mol9e NMO Acetone H 0 CHsCN 1 1 1169 rt 12h OH Recovery and reuse of MC OSCH Run l 2 3 4 5 Yield of Produd 94 9 849 849 830 810 830 Recovery of Catalyd j quant quant quant quant quant 000 No 0 e ud n n nnnnnmnn 153 02081 Osmiunfj VIljoxide Microencapsulated 15 000 AN Wako Analytical Circle No 38 200000000 MODpPEMDDDDDDDDDDD DU

Analytical Circle No.38（2005.9）

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