液体クロマトグラフィー
Contents
1. Table 1 Elution behaviours of aromatic compounds on Porons Polymer Flow rate Benzyl alcohol Benzene Naphthalene Anthracene ml min N H Eercnr E i e E Lm fn N H r N H trt N H 0 5 2 86 545 0 46 4 06 784 0 32 7 95 618 0 41 23 4 487 0 51 1 0 1 55 460 0 54 2 23 614 0 41 4 46 462 0 54 13 2 420 0 59 1 5 1 06 371 0 67 1 52 468 0 53 3 02 392 0 64 8 96 338 0 74 2 0 0 80 381 0 66 1 18 432 0 58 2 32 375 0 67 6 78 282 0 89 N Number of thecretical plates H Height egnivalent to a theoretical plate 4 Mitte EER ELLE LEE HEEL HELLE ATATA ELE HELLE LEE LEE ETE OTTO DTC L TO EOE OED RA COED ED UOC EO COO CIEE OTT DOT ETT LET ETE TERT 17 344 26 38 9 1974 9 WF A 3H 0 2 4 6 8 10min Fig 1 Separation of Aromatic Compounds by using Hitachi Gel 3011 HETP mm c 35 0 25 0 24 L 1 1 1 1 1 10 20 30 40 50 60 70 80 90100 Samplex 1078M Fig 2 Relationship between Sample Size and HETP in Benzene Polymer Hitachi Gel 3011 Sample Benzyl alcohol Detector 254 nm Range 0 16 Chart Speed 5 mm min A EMA HHIUIHHIOHOIHIIOIHIRHIHIHIHIOIHIIIOHIIHIHHIIHIHIHHIIHIIHHIIIIIIHIIIIHIHHIOIHIHHIIUHUHHIHIHHHIHHIUIHHUUUHHHHUUUUIHIHUD Benzene Nap2. Du Pont Varian 2 X ES Hitachi Gel 3011 Hitachi Gel 3010 10 15 gm Hitachi Gel 3010 634 3 0 x250 mm K
3. 1974 6 12 NULLE LLL EET UELLE ELE LLL ELE ELLE EE LEE LEE LLL HEEL ELE ELLE EE LL ATAA 18 26 38 9 amp 1974 9 Hog OLX 345 THHEHTLLLLTHTLHTELIEETTELLIELELULTELLTLLLTLIHUEELLELRELHELTEHLULIEELRLLTELELEHHLLTEIHIVLITHLUHLERLHELENRLILLETLTLHLUEIRCULHLLTHTLEUERLHEUREHLLETHLLILIRLULLLE E xk ig PPE RNET OERE EE MEE MUN SEM 0 2 4 6 min 0 2 4 min Sample DEP Length 25cm Diam 3mm Sample DD nithrophenol Length 25 cm Diam 3mm GDBP Temprature O nithrophenol Temperature GDOP Eluent CHsOH Detector 254 nm Eluent CHOH Detector 254 nm Flow Rate 2 ml min Chart speed 5 mm min Flow Rate 2 ml min Chart Speed 5 mm min Pressure 51 kg cm Column Hitachi Gel 3011 Pressure 28 kg cm Column Hitachi Gel 3011 Fig 4 Separation of nitropheno by using Fig 3 Separation of Phthatic Acid Ester Hitachi Gel 3011 by using Hitach Gel 3011 AOEHLLLELLELELLLLLLLLLLTLULLILEELLHTTTLHLELHLHTTVLHETERLTLECHLLLLLEVEELLTELTHETLLTLIELLTECLELELLLELLELULLLEETULLELUHLTTNLELTLELTEATLELEHLELLEYTLELHTLLULELLLLTEHTLTENTLVTULTTLULIULTLELEHLLEELTTTLYLLETATLLLLET CETT DCEO TT ORT RETTO LLL TRINITY 19
4. 25x10 3 3 DEP DBP DOP 5 4 O P 3 Hitachi Gel 3011
5. 1 634 C 1 3 Hitachi Gel 3011 3 0 x250 mm Hitachi Gel 3011 2 1 500 mm Hitachi Gel 3010 Hitachi Gel 3010 Hitachi Gel 3011 Va tr
6. 26 38 9 1974 9 343 RIETI TIT RIT TI naa aan nannan E T X UDC 543 544 42 High Performance Liquid Chromatography on the Small Column Packed with Porous Polymer m Xj R Nobuharu TAKAI and Takeo YAMABE le
7. htalene Anthracene Length 25cm Diam 3mm Temperature Eluent CH OH Column Hitachi Gel 3011 Flow Rate 2 0ml min Pressure 51 kg cm 0 5 m hr 2 0 m hr 1 N tre zx 1 1 8 HETP HERT 2 2 89x200mm
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