油分析に影響する各種要因について
Contents
1. C17 140 120 gt 2 X fo 100 c gt 2 2 C13 C14 C15 C16 1 GC v 8 C10 C11 7 3 3 1402. GC MS Key words analysis of oil oil class incident of oil flow GC MS infrared absorption spectrometry 1 1 S IS 9 S 316
3. 2 60C 6 H 997 3 5 H 997 S 316 H 997 H 997 6
4. Effects of various factors on analysis of oil Hiroichi Fujiwara Toshiyuki Yoshioka Katashi Kenmotsu Motoharu Nakagiri Toyohiro Urayama 32 67 74 2008 Effects of various factors on analysis of oil F Hiroichi Fujiwara Toshiyuki Yoshioka Katashi Kenmotsu Motoharu Nakagiri Toyohiro Urayama GC MS JIS GC MS
5. S 316 H 997 19 3 2 2 1 OCE OCB 1lmg mL S 316 H 997 1 B 1mg mL 2 2 2 2 1 GC MS Automass Sun 5 Phenyl Methypolysiloxanc J amp W DB 5MS 0 25zm 30mX0 25mm
6. 100mg 20 10mg 50 A a Haat C17 C10 S 316 C 6
7. H 997 S 316 JIS KO0102 60 65 1998 JIS KO102 305 306 1998 561 576 1997 53 56 2004 40 103 106 2006 GC MS 33 82 88 2006
8. 100mg 20 10mg 50 A C 3 3 100mg mg mg 90 C 1 7 18 8 C1 7 15 8 C 1 7 3 68 Chronato 9 1 Soale Abundancel OM Doil088 ll il A i100y hil0ly B i109 C oe 0929 C14 loillg LI M
9. A 2 10mL 100 so A 2n 2 8 C10 C11 C12 C13 C14 C15 C16 C17 C18 C19 C20 C21 C22 3 500mL 100mL 120 RE 5mL Hex a RE 2mL Hex RE Hex RE DCM RE Hex 2 S 0 60 40 250 7 g 0 10mL 200ml 0 10mL oy CN CO
10. OCMA 305 2005
11. oil oil it il C17 C27 C29 Id LTLLLHLT ed 5 i M0 0 2 7l 250 g ml 1ml 1ml GC MS 2 1ml 3 C10
12. we ee WEC H 997 5 g ml S 316 7 5 4 gt nS 2 L C 0 CCI4 CCI4 36 A C OCB B C H OCB B 60
13. 40 S 316 OCB B 40 S 316 73 4 GC MS JIS 1 74 GC MS A B C GC 90
14. HW WW ok oC rr CX 200mL 4 72 250zg 200mL 5mL 5s lt lt lt lt lt lt lt lt 4 4 C12 0 CCI4 CCI4 A C OCB B 3 4 S 316 5 S 316 ed EE 2 S 316 3 A gt gt 60C 30 60 30
15. 50C 2 7 310 C 5 250 1 gl 1 0mlmin 1 5 70eV EI 300 uA 230C 67 2 2 2 OCMA 305 H 997 OIL 105 S 316 2 2 3 1 GC MS 10ml 1ml GC MS 1000ml 50g 100ml 50ml 2 1ml GC MS 2 1
16. 1 20mlX 2 300rpm 2 10 20 80 30 20C30 3 H 997 100ml 1 1 H 997 50ml 5 10 20 0CMA 305 4 S 316 100ml 1 1 S 316 1 10mg 20ml 300rpm 5 10 20 S 316 0 TL 105 3 3 1
17. GC MS 1 C10 C9 C14 C9 C23 A B C GC 5W40 3 2 A C 10mg 100mg 1 90
18. ill5 il il MM Mu Do 0 II MI MM 0 HI MI 1 1 GC MS 69 Chronato TIC YSoale iD MM HMIE VG10 HE MVG10 Mu 4 1 M 2 VG10 MM N05 VG22 MM 006 VG32 1 1 VG32 MM 006 5W 40 MM gt 1 2 GC MS 70 wll 85 Te iA gt loillty il il oil loilt oil ll oilO06 ll A IM A i100 ll oi B oil B ll LLLL fil HL hil a NM foilll id oil C C
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