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1. 2 _ 9 34mm 3 ON SPL1 17 MODE SPL R SLESS_ OFF2. BTOPI RESET 1 E 2 22
3. 21 0 10007V GC 14B GC 14A FID 10 11 12 18 14 15 16 17 18 19 20 2
4. 80mL min V ek
5. o 3mL min 2mL min IFUNC le ENTER ENTER 27 44 GC 1700 w FID
6. 1 1 2 50mL min 7 9 10
7. SAMPLE Immmrrmnrrmrrrrrrrmmrrmmmlll WASH Y SOLVBENT 1 5mL 4mL WASH 4mL NUMBER OF 1 INJECTIONS SAMPLE S1ZE oron rcrio BER ResET RUN STOP START I 49
8. 100 1 2 60cm 27 1cem 3
9. ICOL 5 GC YSTEM GC W 5min 6 O 9 ON Off 9 ON Of PEGC GC o FiLE ooo II L kPa L R kPa R 40 0 40 0 NN te oo I C MAO 1500 DD rio IIDI C EY 1500 40 0
10. 30kPa 2mL min ENTER FUNC 8 IENTERI O ENTER ESC 35 GC 18A FTD bg OO LOT 10 11 12 18 14 15 16 17 18 19 20 21 22 FID 2 9
11. PURGE VRENT 1 9 1 5mL min 1 1 1 w FID FID 2 FID 2 100 5 10mm 3 0 583mm FID SPL SPL l
12. 100 1 2 60cm 27 1cm 3 cm E
13. 14BPFsc 75kPa 30 50mL min IGNIT cm sec Qm 100 min X60 30m 40 70cm sec 120 170 kPa 2 s mlimin ao 50mimin so i20uPa
14. 6 7 8 9 10 11 100kPa 3mL min 2 27 39 GC 18A SOSOO EY OS OL ES CO 11 12 13 14
15. 0 0 0 3 NTER 50 60kPa 9 75kPA 9 FID IGNIT ON ENTER COL INTT TEMP 60 2min 10C min 200 2min 60 COL PROG I 6 ENTER 9 ENTER VY 1 0 ENTER Oo 0O ENTER 2 ENTER 1 RATE TEMP PURGE VENT 19 10 0 200 1 5mL min GC ZERO 0 1000V 2 SPLIT VRENT 17 50mL min
16. 7 8 9 APC 10 100kPa 3mL min 30kPa 2mL min FEUNC NTER ENTERI 0 ENTER ESC 2A 31 GC 17A w FTD IN Oo oo MN 10 11 12 13 14 15 16 17 18 19 20 21 22 FID
17. 6 34mm TFID FTD 2014 99mm 2 8mm Alt K haFC ITCD TTD 2014c 69mm 2 83mm FPD 120mm ECD 75mm TTD FTD 2014 99mm 112mm
18. 2 80mL min
19. 7 8 Y 9 10 11 100kPa 3mL min 30 50kPa HU 30kPa
20. 80mL min E10 E11 19 13 C R7A 7A plus C R8A GC
21. PRSS FLOW 0 ENTER 8 0 ENTER VY 17 7 1 BO ENTER 5 IO IENTERI 18 250 INJ 0O NTERI 19 250 DET 2 Bo ENTER 30m 20 0 Co 0 ENTER 100 150 kPa 1 2 2 5 mL min 1 30 100 0 32 mm 60 100 kPa 2 4 mL min 1 15 30 21 GC 1700 25 40 kPa 5 8 mL min 1 2 10 SYSTEM 22 MONIT mon 23 69mm
22. ET kPa PF2Fine 16 LOW PF1f SPLITLESS min 1 00 Off IPF3EOn Off On _ He 99 SPLITLESS 9 Gas Saver
23. 10mg 25mm 12mm 0 0 0 0 850 1 4 5 6 E7 8 9 34mm ECD 87mm 1 2
24. mL min mL min 30mL min 25 GC 14B GC 14A FID 1 Ll 2 3 10 11 12 13 14 15 16 17 18 19 20 2
25. SAMPLING SET BPL NTER 7 1 5 1 ENTER ON OFF ON ELOW1 ON ENTER CAR1 PRSS FLOW 9 0 25mm 30m a A 2 ENTER Oo ENTER CNN ams os 1 Oo ENTER Oo ENTER A 250 CFLW INJ Oo ENTER 0 0 250 DrT oh ENTER ee BD 0 6 80m NN OE BN gurrzn MONIT IA 69mm
26. SS SE 1 GC 2010 2010 Plus GC 2025 FID KK 2 GC 2010 2010 Plus GC 2025 TDK 5 GC 2014 ED aR ES 8 GC 2014 TCD i 10 GC 2014 AT ED ERR 1 1 12 GC 2014 SS sD CS RR RR ES Sls 15 GC 14B GC 14A FID i 18 GC 14B GC 14A FID 19 GC14B GCA4A CD SE 20 GC 14B GC14A 0OD KA 21 GC14B GCI14A ED RR EE 22 GC 14B GC 14A FID KEKEKEKRK KS 26 GCLTA DRT I EI WD AR R 30 GCATADAIT YY RKRR GED ERE EE SE EE 32 GC 17A w FID SPL WBI kk 34 GOLSADOAT GIES ED 36 GCASAIDART V5 RR SW ED RS EEE EE SE 38 GEISA OG CkFE 40 GC 1700 wRID 28062000326080082 0360 42 GEA DAT FER ED SE EE 45 AOC20i nS kD EE ES 48
27. FTD SPL SPL 0 8 TTD 1 2 5 2cm 6
28. 10mL min 7 8 9 V 10 APC 11 12 100kPa 3mL min SE 30 50kPa Du
29. 4 TCD 2 2 5 6 7 9 C R7A 7A plus C R8A GC GC
30. 1 10 4 GC 2014 TCD UL 1 GC READY 2 oh 3 RT 60 0 ES TO i NA L kPa 4 L 400 5 R kPa 6 ON R 40 0 7 Line TT es oo SET
31. 50 60kPa RANGR O ENT POL GC 0 1000 NT 40 50mL min 10 GC POWER ON CARRIER HYDROGEN
32. 1 2 8 3 10 11 34mm 12 13 ON SN 14 SPL1 17 MODE BPL NTER BIS SMG 15 ON OFF ON IFELOW1 ION ENTER 16 8 0 25mm 30m 0 CO RO ji
33. 9 SPLIT 9 8 Gas Saver 3 15mL min 17 18 19 20 25cm sec 1 50 2 ENTER ENTER ET 9 IDET Off
34. PFfZero 13 GC 2 COL 1 2 3 Cee 3 min C mmn CC mn READY o FiLE 43 9 0 00 min 1 2 8 WBI 2
35. 5 6 7 APC 8 C R7A 7A plus C R8A GC GC 1 X2 4 5 C R7A 7A plus C R8A GC GC
36. 30mL min 9 10 11 12 18 APC 14 C R7A 7A plus C R8A GC
37. 11 12 3mL min 18mm 2mL mn IFUNC le ENTER ENTER 47 AOC 201i Oo na 9 OT 10 11 12 19 14 15 16 17 GC GC Q 5mL 2 4mL
38. 12 _ 6 42 250C COL IINIT TEMP IO ENT 43 50C COL INTT TEMP 5 0 ENT 44 GC FID ZERO 0 V 45 GC 1 25mm AOC 20i 25mm AOC 17 23mm AOC 14 20mm 3 10mg 2
39. 1 TCD 2 3 4 5 600kPa 40 50mL min 6 7 TCD VENT 10 8 GC POWER ON 9 HEATER ON 10 TCD ON POL 2 11 POL 1 CARRTER DET M ENT 12 0mA CURR ENT 13 200 INJ 2 Ol MO ENT 14 220 SIFT DOWN DET T TCD T 0 ENT DET T
40. 1 2 TCD 3 20 GC 14B GC 14A TCD 1 16 17 18 19 20 21 22 23 15 TART IMONTT IINJ DET T TCD T 1 5 o ENT MONIT SIFT DOWNI
41. 10 11 34mm 12 lt 13 ON FN 14 SPL1 17 MODE SPL ENTER SE SPL SLESS OFF 15 1 5 1 ENTER SAMPLING SET 16 ON 1 5 OFF ON ELOW1 oNi ENTER A CAR1 PRSS FLOW 17 9 N RDY 150 0 25mm 30m a 0 BNTERI BO ENTER COLUMN 18 9 cami 1 0 IENTER 5 0 ENTER A 19 250 INJ NTERI 20
42. 30mL min IPF1 ENTER Advanced 1 XxX1 X2 4 GC x x1 X10 4
43. 4 GC 2010 2010 Plus GC 2025 HID GC 0 A 0 CO Nr CC TD 2 np 4 FLE LNE 5 0
44. START 1 5mL 3 5mm 3 11 3 1 1 6 B
45. GC 1 X2 4 C R7A 7A plus C R8A GC GC 1 10 4 14 GC 2014 FID 10 11 12 13 14
46. Off 9 ON Off 9 ON O 12 IPF1 GC GC READY 17 0 FILE DET 8 1 C 43 9 Of On 29 29 min 000 _ Hs 55kPa Air 40kPa MakeUp 75kPa Ns 80kPa He C mn C mn 1 3 18 MONIT
47. 075 500 1 2 SPLIT 9 II INJ C 150 0 10 DN Fo UII 11 C 150 0 34mm INJ 5 a 12 69mm 13 14 ON 15 Line
48. 2 FID AFC AFC GC FUNC Function 6 9 W DAFC DAFC AMC LR DAFC AMC LR DAFC
49. 1 2 7 m Line1 4 Line1 NTER 8 GC 2014 He 20cm sec 40cm sec X
50. ENTER FUNCTION NO TFUNCTTON NO 1 NTERI 1 5mL 10L FUNCTION NO 93 D1 DD DD A ei
51. I 0 1000gV ELOW1 rv ENTER ENTER ho Oo ENTER 1 w FID FID 2 w FID 2 100 20mm AOC 20i 21mm AOC 17 18mm AOC 14 15mm 10mm 3 10mg 3 FID AOC 30i 21mm 1 2 AO 4
52. OgL 8 SBAMPLE WASH 003 5 SOLVENT WASHI D0g 5 INUMBER OF INJECTION 0D05 1 0z BAMPLE SIZ 01 0 5 IEUNCTTION IF01 6 NTER 005 FUNCTION
53. 1 X2 4 C R7A 7A plus C R8A GC GC x1 X10 4 8 11 GC 2014 FID 10 11 12 18 14 GC 1 1
54. Wp Oh SPLITLESS 9 9 15 READY 0 FiLE ITI EE UOTUULL C 60 0 coo II oN kPa SPLIT UNI tt se TN C 150 0 150 0 EE I isoo 130 9 0 75 Line PH IT kPa He IPFal 3 15mL min 1 25cm sec 1 50 W 2
55. 0O 0 0 350C 4 100 5 6 7 8 9 ECD 37mm 1 2 34mm FID 69mm TCD 9 Line1 4 Line1
56. 8 15mL min 40cm sec 50mL min 1min ENTER 17 ETI m 9 ICOL DET Off On PF Gas READY H2 40mL min MakeUp 30mL min Air 400mL min o FILE 1 0 Of PF On Off On
57. 5 a AR1 PR FL 24 amp S38 BW 7 150 50 MONIT 42 25 26 27 28 29 30 31 32 99 34 35 36 97 9 200 COL 0 0 ENTER ON 9 DET ON ENTERI lt 0 0 0 4 IRNTERI FLOW2_ 50 60kPa 9 60kPa ELOW2 ON ENTER 6 IO ENTER 50 60kPa ON NTER 6 0 NTER 75kPA 9 60kPa ELOW3S ON ENTER UR ENTER FID IGNTT
58. a i 34mm E SPL1 18 MODE SPL_ SLESS ACT COLUMN CAR1 CFLW VEL 0 0 0 ID 60 100 kPa 2 4 mL min 0 25 30m 25 50cm sec 100 150 kPa 1 2 2 5 mL min 1 30 100 1 15 30 25 40 kPa 5 8 mL min 1 2 10 IMONIT A 69mm IMONITJ 9 150 IMONIT ON 8 0 0 0 3 CO O OO ENTER DET ON ENTER ENTERI 36 7 200C 23 24 25 26 27 28 29 30
59. 2 6 7 8 9 100 20mm AOC 20i 21mm AOC 17 18mm AOC 14 15mm 10mm 3 10mg TID 1 2 FID GC 18A
60. 48 ef 1 1 10 NTERI 1 0 1 1 0L NTER
61. 9 12 READY oFILE II EE UTU C 60 0 II EE OTOL kPa _ 1309 _ 075 _ 500 SPLIT IND te se TN 1500 HO FoT I C MM 1500 kPa 8 He 1 9 3 15mL min 25cm sec 1 50 lt 2 5 s ENTER s e 5 0 s ENTER 1
62. GOC 2010 2010 Plus GC 2025 E 1 g 50mm FPD ENTER 82mm 2mg 25mm 5mm 0 FTD 69mm 1
63. 2 O 3 1 12 5 34mm INJ 6 O
64. 2 MONIT DET T 50 COL IINTT TEMP 5 0 ENT IGNIT FID V IGNIT 18 GC 14B GC 14A FTD 1 lt 7 8 GC POWER ON 9 HEATER ON 10 FID ON 11 200 INJ MM ENT 12 220 DET T 0 NT 13
65. J 8 4 85mm 1 4 mm TAN 3 105mm 75mm or 105mm 1 4 GC POWER ON HEATER ON FID
66. Cs Ce 2 18 OO R 43 9 SES IPF8FZero 1 2 3 WBI 2
67. 0 1000V 46 1 w FTD FID 2 w FTD 2 20mm AOC 20i 21mm AOC 17 18mm AOOC 14 15mm boa 3 100 4 FTD 1 2 AQOC BOi 21mm 5 Adc FID 6 GC 1700
68. H 6 O 99mm Wo Line ON es ISET 1 PF2Fine FLOW W IPF1 Off IPF3EFOn Off On
69. IENTER 2 s IENTER 1 5 6 15 ETI ILS eS ce ENTER 9 COL 16 GC BYSTEM GC m 5min 1
70. 12 221 50595 91 4 0 25mmX30m 100 150kPa 0 32mmX30m 60 100kPa 5 GC 14BPFsc IINJ IIFT DOWN 6 7 GC 14BPFsc 75kPa 30 50mL min 9
71. 9 2 0 IENTER FLOW 14 250 INJ MM IO NTERI 15 250 DET IO ENTER MONIT_ 16 0 7 COL 0 ENTER 17 GC 17A SYSTEM 18 IMONTH 3 19 69mm 3 20 IMONIT 21 9 200C COL M ENTER 22 ON 9 DETHA ON ENTE
72. 10 1 IRANGH 0 2 ENT FID POL FTD IENT 23 5 37 100 L GC 97 88 25 50cm sec 25 50cm sec 2 37 39 40 SPLIT VENT 1 50 50 41 PURGE VENT 10 15mL min
73. WBI 2 2 10mg 20mm 12mm 0 0 0 0 850 1 4 100 13
74. 10 80mL min 250 COL INIT TEMP 5 IO ENT 50C COL INIT TEMP 5 0 ENT GC FID ZERO 0zV 1 SIFT DOWN 7 PROG SIFT DOWN 4 DEL ENT 1 3 SIFT DOWN 8 EVENT ENT SIFT DOWN ESCP 3 SIFT DOWNI 8 REVENT 9 1 ENT GC E START 28 2
75. 10 lcol IEROG RATE Ho ENT 250 COL FINAL TEMP 9 5 Oo ENT COL FINAL TIME 5 ENT 27 28 1 29 30 81 8 4 FTD 250 H 1 32 33 30 60mL min 9 34 IGNIT 9 85 10 1 IRANGR 0 2 ENT 36 FTD POL FID
76. 50 60kPa 9 75kPA 9 FID COL IGNTT ON ENTERI 60C 2min 10C min 200C 2min 60 COL PROG 68 IO ENTER ENTER VM 1 RATE TEMP 1 PROG INIT TEMP ol ENTER 0 0 ENTER ENTER PURGE VENT 0 10 0 200 1 5mL min GC ZERO A I 0 1000V SPLIT VENT 1O 1 to w FID FID 2 FID
77. TTD 5 GC 17A 1 1 2 80mL min 6
78. TID 5 GC 17A 1 1 2 50mL min 6 7
79. C 150 0 AR TNI sae oo 0 8 C _ 1500 PE2Fiine 2 C 1500 8 IFLOW Off PF3 On Off On 3 9 BET C ICOL min 5 C mn C mn 10 GC YSTEM GC m 5min
80. GC 2 FID TCD or RD SN OSN OD BO 1 2 3
81. 2 DRI WBI 3 4 5 6 7 OR 8 9 ON 3 3 MS 10 OFF PMODE FMODE SPL ENTER 11 MS FUNC 3 ENTER P ENTER IESC 12 ON OTFE ON FLOW1 ON IENTERI 13
82. E ON BPL NTER 0 25mm 30m ON OFF ON ELOW1 ON NTER ENTER 3 0 ENTER V 5 O ENTER gt S 250 INJ BO ENTER 250C DET 0 ENTER 0 6 COL 0 ENTER GC 18A SYSTEM 0 32 mm
83. 2 min 3 0 1 100 2 m 9 Line1l 4 Line1 NTER 3 INJ
84. 250C 30m 21 0 0 25 mm 1 1 5 min COL ETER 22 GC 1700 SYSTEM 23 MONIT NR CAR1 PRSS FLOW 24 69mm 5 150 50 45 25 26 27 28 29 30 31 32 99 34 95 36 97 MONIT 8 200 COL 0 0 ENTERI ON F lm ha 1WFID ATTN 9 DETH ON ENTER T 0 0 4 ENTER 0 FLOW2
85. 50 60kPa IN 5s0 21 IGNIT 3 FID n 0 20 40 22 min IRANGE M ENT 23 POL 1 NT 24 GC 0 1000V 4 19 GC 14B GC 14A TCD
86. On 3 Off 8 Of PF1EGC GC PTOD VENT min 10 11 DET On 9 _ Me I Le TN 0 kk 0 NN 1 kPa L 40 0 12 L N2 MAONTT
87. COL IINTT TEMP 150 500C 3min 10 C min 150 C 10min COL INIT TEMP 5 O ENT COL INIT TIME 3 ENT COL IPROG RATE 1 ENT 2 COL FINAL TEMP lt 5 O ENT COL FINAL TTME MO NT 30mA CURR 8 NO ENT IPOL NT Ll H 200 1 R50 RR 0 0 10 20 min GC E5 SE Bl 4
88. 2 15 Cs s ET 6 5 5 EE 10 _ SE NER ICOL 3 16 GC ISYSTEM GC 2 5min 17 O ON Of W
89. He E 30cm sec 60cm sec ELOW 10 11 E12 E13 250 350kP a C R7A 7A plus C R8A GC C R7A 7A plus C R8A GC
90. GC X1 2 4 C R7A 7A plus C R8A GC GC 1 10 4 G
91. SYSTEMI ONITJ 17 A I ER RW MONIT A 18 69mm 3 19 9 30m 25 50cm sec 9 MONTT 2 2 75 4 150 50 100 150 kPa 1 2 2 5 mL min 1 30 100 Ni 20 60 100 kPa 2 4 ml min 1 15 30 200 25 40 kPa 5 8 mL min 1 2 10 COL 2 0 0 ENTER 21 ON 8 7 1WFID TTN DET H ON ENTER DET ON 0 22 0 0 4 IRNTERI
92. 100 FID 69mm TCD 50mm FPD 82mm FTD 69mm m 9 Line1 4 Line1 ENTER GC 2010 2010 Plus GC 2025 1 He 20cm sec 40cm sec
93. G 0 8 FID 1 2 4 2cm 5 10mL min 6
94. TITTLE EE UTU 6 CC EN eo II EE UTU TUI kPa 130 9 8 075 500 1 2 SPLIT 9 II INJ C 150 0 10 FroT TIL 11 C 150 0 34mm INJ 5 Line 2 LE EE 69mm 3 en ey 9
95. kl PRSS FLOW 9 MONIT 200 co A D 0 ENTER A ON 9 SN DETA ON ENTER 32 0 9 0 4 ENTER 50 60kPa 75kPA FTD IGNTT ION IENTER 60 60 C 2min 10C min 200 2min COL PROG I 6 ENTER ENTER VY 1 RATE TEMP TIM 1 0 ENTER 0O IO ENTER 2 ENTER 10 0 200 2 PURGE VENT 1 0 1 5mL min 1 1
96. 27 28 29 30 31 50 C 1 10 250C 5 50 C COL IINIT TEMP 5 OQ ENT 1 COL INIT TIME 1 ENT 10 COL IPROG RATE 1 0 ENT 250 COL IEINAL TEMP 9 5 IO ENT 5 COL FINAL TIME 5 ENT 4 FID 32 99 34 35 36 50 60kPa 30 60mL min 9 IGNIT 9 FID
97. 1 w FID FID 2 FID ei 2 100 20mm AOC 20i 21mm AOC 17 18mm AOC 14 15mm FID 1 2 AOC 2Oi 21mm AOC117 18mm 4 FTD 5 GC 18A
98. 99mm 112mm 1 2 7 9 Line1 4 Line1 NTER 8 GC 2014 He
99. DAFC AMC LR DAFC 6 34mm TFID FTD 2014 99mm 2 8mm Alt K haFC ITCD TFTD 2014c 69mm 2 8mm FPD 120mm ECD 75mm FID FTD 2014
100. 99mm 6 O 1 Line SET PF2Fine FLOW ON Off IPE8 On Off SPLIT IPF1 On W
101. ON 26 75mm 2 21 BIFT DOWN INJ AUX2 280 DET T 8 I ENT 9 COL INTT TEMP 0 ENT 2 ISTOP MONIT SIFT DOWN INJ AUX2 H IMONIT 5 0 ENT 22 23 START 24 25 26 DET T 3 50 1 10 250 5 50 COL INIT TEMP 5 0O ENT COL INTT TIME 1 ENT
102. SHIFT DOWN 4 DEL 29 GC 17A w FTD 1 FID 2 Re 3 4 3 5 6 34mm 3 7
103. mw 000 CC mmn C mn 19 GC YSTEM GC 5min 22 Off 3 ON Of W 9 ON min O 13 PF1 GC GC 20 IMONTT ENTER lt s 0 ENTER 2 SU W
104. 1 FID 2 3 4 5 6 7 1 2 8 9
105. 10 11 100kPa 3mL min AA 97 GC 18A FTD IN 2 1 FID 34mm ON 9 SPL NTER V 10 1 5 1 ENTER
106. DET 2 BO ENTER 0 COL 0 NTERI 9 250 250 6 GC 18A SYSTEM H IMONTIT A FLOW CAR1F N RDY CAR1 2 3 ACT SET 10 PRSS FLOW 20 20 69mm 3 0 IMONTT 2 0 Oo ENTER ON 9 ON NTER 0 ENTERI 9 O FID
107. 18 APC 14 C R7A 7A plus C R8A GC GC X1 2 4 C R7A 7A plus C R8A GC GC 1 X10 4 5 17 GC 14B GC 14A FTD
108. _ IE Cee I L kPa L co L Ns II Fier UII R 6 R kPa R N2 2 CE 11 IDET Off On 2 se Sa 9 2 o FiLE Hz 55kPa Air 40kPa 43 9 NN mn 0 00 NO L 8 eo a 0 WI rp CC mm IMONTT IPF3 Zero 1
109. 100 16 2 FID AFC AFC GC FUNC Function 6 9 W DAFC DAFC AMC LR
110. 50 60kPa 0 23 2 AI 30 24 25 26 27 28 29 30 75kPA FID IGNTT ON ENTERI 60 2min 10 C min 200 2min COL IPROG 6 IO ENTER ENTER VY 1 0 ENTER 0O IO ENTER 9 ENTER PURGE VENT 19 1 5mL min 1 GC ZERO AA 5 COL INIT TEMP TIME 60 2 0 PROG Ni 1 RATE TEMP TIM 10 0 200 2 ul 1 100
111. Line ON EE 1 ETI PF2iline IOW Off IPF3EOn Off 3 BET 2 On 1H gt XE E
112. 2 COL IINTT TEMP O ENT 14 TART 15 MONIT INJ 16 MONIT DET T 17 4 150 COL IINTT TEMP 1 5 Oo ENT 18 50C 3min 10C min 150 C 10min Col NiT TEMP bB 0 ENT ICOL INTT TIME ENT OU ICOL PROG RATH fl OQ ENT COL ITNAL TEMP 0 ENT 6 CO FINAL TIME 1 Oo ENT To 19 100 20
113. ON Of 2 IBF1 GC GC READY 17 o FiLE DET C 43 9 Off On min 000 Hz 55kPa Air 40kPa MakeUp 75kPa Ns 80kPa He C min C mn 1 9 18 IMONTT IPF3 Zero min 3 0 1
114. cm E J 8 4 85mm 1 4 3 35mm 75mm 105mm 8 1 4
115. 8 9 APC 10 18mm al 100kPa 3mL min 11 30kPa 2mL min FUNC 68 ENTER ENTER 3 0O ENTER ESC 33 GC 17A w FID SPL WBI 1 FID
116. GC ZERO Iy 0 1000V 1 w FID FID 2 w FTD 2 100 D 20mm AOC 20i 21mm AOC 17 18mm AOC 14 15mm 21mm 3 FTID AOC 20i 1 2 AOC 1 4
117. IGNITI ON ENTER 60C 2min 10C min 200 C 2min COL IDET y 72 200 6 DET ON 0 8 75kPA ENTER V COL IPROG 8 0 ENTER 1 0 ENTER 0 0 ENTER 2 ENTER 10 0 40 1 RATE TEMP ATTN 0 50 60kPa 9 9 60 200 26 GC 27 ZERO 0 1000 V
118. 21mm AOC 17 18mm AOC 14 15mm 10mm 3 10mg 100 FID 1 2 TTD GC 1700
119. 30cm sec 60cm sec X 30mL min 9 10 11 12
120. NL 50 60kPa 9 60kPa A FLOW2 ON IENTER 6 0 IRNTER 50 60kPa 9 60kPa ON ENTER 8 0 ENTER 75kPA FLOW3 FLOW3 ON ENTER 7 5 ENTER FID IGNIT ON ENTER i 60C 2min 10 C min 200C 2min COL IPROG 6 0 ENTER 2 ENTER IV INIT TEMP 1 0 ENTER 2 0o ol ENTER 2 ENTER ROG PURGE VENT Rr ZERO 1 5mL min 2 60 1 NE 1 RATE TEMP GC IM 10 0 200
121. i 8 ON a SS Ne 9 SPL NTER 10 ON OFE ON FLOW1 ON ENTER A 11 0 25mm 30m 0 NTER 8 0 ENTER IM a ON 2 0 12 W N RDY 150 50 1 5 IO ENTER 5B 0 ENTER 18 250 COLUMN ID NJ A BO ENTER CAR1 0 25 14 250 A DET 0 ENTER CFLW VEL SPL R 15 0 9 0 0 0 50 COLU 0 ENTER 16 GC 17A
122. 0 ENTI 1 15 37 COL IINTT TEMP 0 ENT 16 TART 17 MONIT INJ 18 3 MONIT SIFT DOWN IDET T TCD T 19 50C COL IINTT TEMP 5 Oo ENT 20 30mA CURR 3 o ENT 21 POL 1 BN 22 GC 0 1000xV HEATER POWER
123. GC POWER ON 175mm or 105mm HEATER ON FID ON 22 2 21 22 23 24 25 26 250 SIFT DOWN IINJ AUX2 ENT 280 BK 0 EN NN 1 o POL 2 NN CARRIER coll NIT TEMP M ENT BOT Re TART Ro 2 BTOP SPLIT YEANT PURGE VENT MONIT SIFT DOWN INJ AUX2 7 MONIT DET T POWER 3
124. OS 59 11 ON OFF ON ELOW1 ON ENTER 12 0 25mm 30m OE NTER 8 0 ENTER VY 13 1 0O IENTERI 14 250 INJ IO ENTER 15 250 DET 2 IO ENTER 16 0 9 30m SPL1 18 MODE SPL SAMPLING SLESS_ SET 1 5 CAR1P ACT ID 0 25 SET 0 150 40 70cm sec
125. E EE COL 0O ENTER 120 170 kPa 2 3 mL min 1 1 5 min 17 GO 184 18 IMONTT 19 69mm 20 9 IMONTT CAR1 21 7 200C CO 0 OA ENTER 22 ON IDET ON NTER DET 38 SYSTEM EL 0 mi PRSS FLOW 150 23 24 25 26 27 28 29 30 31
126. ON ENTERI 60C 2min 10C min 200C 2min COL PROG 68 IO ENTER 2 ENTER V 1 10 ENTER 0 0 ENTER ENTER PURGE VENT 1 5mL min GC 1 1WFID ATTN ET A INIT TEMP 60 1 RATE TEMP ZERO 9 1 100 FLOW1 YENTER ENTER 1 0 0 ENTER 43 10 0 200 0 1000gV w FID FID 2 w HID 20mm AOC 20i
127. OO EY OS OL RT OL FF 13 14 15 16 17 18 19 20 21 22 23 FID 600kPa HEATER ON FID ON BS 200 INJ 2 jo 0 ENT 220C DET ENT COL INIT TEMP 0 ENT ETART IMONTT IINJ
128. 2 On IPF2 Gas H2 40mL min MakeUp 30mL min Air 400mL min 0 Off IPF8LOn Off On 1 1 GC BYSTEM 5min 12 Off W ON Off W Ee GC 9 ON O PF1 GC MONTT
129. Adyanced GC HH GC 2014 FTD 1 OO 10 GC 1 2
130. GC 1 2 b O 3 ia 1 2 34mm INJ 6 1
131. IPF8FZero P min 3 0 1 WEHI 2 WBI 2 2mg 25mm 5mm 0 0 0 0 850 1 4
132. ssmlimin 30 s0mLmin so soxpa oi0 mLimin 90 s0 mLmin mL min 3 14 X mm 2 2 X m min J yi a J 1 5 X P2 1 P3 1 P 1 kPa kPa 101 3kPa T IME TIME
133. 1GNIT 10 cm sec m X100 min X60 24 4 11 mL min 3 14 X mm 2 2 x m min J 30m 25 50cm sec J 1 5 X P2 1 P3 1 P 1 kPa kPa 101 3kPa
134. 2mL min FUNC l8 ENTER ENTER Bo ENTER Esd 41 GC 1700 w FID FID 2 5 6 7
135. 15 16 17 18 19 20 21 22 23 24 25 FID ON ON OFF ON FLOW1 ON ENTER 2 0 INJ 2 5B OA ENTER
136. 27 2 ENT SPLIT VENT PURGE VENT 50 60kPa FTD FID POL 1 5 97 38 39 40 41 100 40 70cm sec 1 SPLIT VENT 1 2 PURGE VENT 6 42 43 44 45 46 47 48 49 50 51 10 2 37 HH GC 30 60mL min
137. 3 13 14 ON Flow CAR1 15 Line RE 5 ae kPa PE2Hiine 3 16 0 IELOW IEF 5 5 Of IPF3 On Off On 2 _ He
138. 3 10 11 13 14 25mm AOC 20i 25mm AOC 17 23mm AOC 14 20mm 1 2 221 50595 91 0 25mm X30m 120 170kPa 0 32mmX30m 80 120kPa GC 14BPTsc IINJI BIFT DOWN
139. C 2010 2010 Plus GC 2025 FID 1 GC 2 8 seep Cowe ere 4 SECEDED 2 READY 5 0 0 FLE TITTLE EE UTU 6 CC EN so0 IIIT mE HU UOT kPa 130 9 8
140. I NN Riere NN R kPa PF3LZero R 400 R N 1 2 EE 1 100 2 m 9 Line1 4 Line1 NTER 3 INJ
141. R 23 0 A 0 NTER 0 4 VN 24 50 60kPa 9 25 75kPA 9 26 FID IGNTT ION ENTER 27 34 29 30 28 60C 2min 10C min 200 2min COL PROGI 68 0 ENTER 2 ENTER V 1 ENTER IM ENTE
142. RI ENTER INIT TEMP TIME GC 60 2 0 ERO Ni ERATEN EEME HM 0 1000V 10 0 200 2 PURGE VENT 1 5mL min 1 2 1 w FTD FID 2 w FID 2 2 AFC 1 AFC 2 3 100 5 10mm 4 0 53mm
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