天然産二硫化モリブデンの走査トンネル顕微鏡(STM)画像
Contents
1. STM 2002 2 CalrSn STM STM Atomi2. AFM STM AFM FM AFM Giessibl 1995 FM AFM Fukuma et al 2005 STM AFM
3. STM X STM STM II STM STM mV V nm
4. pA nA Chen 2008 I 4 I d 1 z d xy xy z 1978 IM IBM Zurich Research Laboratory Rohrer Binnig
5. X X 2012 STM STM STM
6. STM STM STM nm 100nm STM i ii STM
7. 0 2V Fig 3 Fig 6 MoS STM 10nm Xx 10nm 5nm 5nm Fig 3 Fig 4 STM MoS 0001 basal plane Komiyama et al 2004 Fig 2 PTr 0 25mm Fig 4 HOPG STM It 1 6nA E 0 2V 3nm X3nm z 0 09nm STM 93 Fig 5 MoS STM It 0 8nA E 0 25V 10nmX10nm z 0 30nm V V 1
8. 1964 20 1 64p Binnig G Rohrer H Gerber Ch and Weibel E 1983 7X7 reconstruction on Si 111 resolved in real space Phys Rev Lett 50 120 12 Chen C J 2008 Microscopy 2nd Ed Oxford Science Publications Eggaleston C M and Hochella Jr M F 1993 spectroscopy applied to PbS 001 surfaces Fresh sur Introduction to Scanning Tunneling Tunnelign faces oxidation and sorption of aqueous Au American Mineralogist 78 877 883 Fukuma T Kobayashi K Matsushige K and Yamada H 2005 frequency modulation atomic force microscopy Appl Phys Lett 86 193108 Giessible F J 1995 7X7 surface by atomic force microscopy Science 267 68 True molecular resolution in liquid by Atomic resolution of silicon 111 71 2011 1955 16p Komiyama M Kiyohara K Li Y Fujikawa T Ebina T Kubota T and Okamoto Y 2004 on a molybdenite basal plane observed by ultra high Crater structures vacuum scanning tunneling microscopy and its implica
9. nm HRTEM Scanning tunneling microscope STM STM I 20 STM
10. 61 89 94 2013 89 STM 2012 9 26 Imaging of natural IMoS by scanning tunneling microscopy Kazuo YOSHIKAWA Department of Earth Science Faculty of Education Gunma University Maebashi 371 8510 Gunma Japan Shin ya KISHIOKA Department of Chemistry Faculty of Education Gunma University Maebashi 371 8510 Gunma Japan Accepted on September 26th 2012 ABSTRACT Natural MoS molybdenite delivered in Gunma Prefecture was imaged using scanning tunneling microscope STM under ambient condition Before imaging the crystal structure was confirmed by X ray powder diffraction analysis and the lattice constants and the unit cell volume were determined as a 0 31619 2 nm c 1 2305 2 nm and 0 10653 2 nm respectively STM images of natural MoS clearly showed that the surface structure was 0001 basal plane as pioneering studies indicated Conditions for STM sample preparation of natural minerals were briefly discussed and the usage of STM images in the lecture of crystallographic science for under graduate level was considered X
11. X 2H JCPDS 37 1492 a 0 31619 2 nm c 1 2305 2 nm V 0 10653 2 nm X Cu Ka Guinier Hagg NaCl 16 2003 CellCalc ii STM STM easyScan2 STM Nanosurf Fig 1 Nanosurf easyScan2 STM 15cm Fig 1 70mm 350g STM
12. PbS STM ZnS 011 Zn Fe STM 94 V 2 STM STM
13. Eggaleston and Hochella Jr 1993 STM STM STM g MoS molybdenite G 2H 3S mm 1955 1957 1964 2013 mm
14. Highly Oriented Pyrolytic Graphite HOPG Highly Oriented Pyrolytic Graphite HOPG STM STM STM Pt Ir easyScan2 STM 0 25mm Pt Ir 80 20 HOPG STM mechanically polishing 2 M mol dm NaCl 0 253mm Pt Ir 80 20
15. MoS mm Fig 6 MoS STM It 0 8nA E 0 25V Snm X Snm z 0 25nm HOPG STM iii NaCl 100
16. Fig 2 STM SPM Gwyddion Necas and Klapetek 2012 92 IV Fig 3 Fig 4 HOPG STM 10nmX10nm 3nm 3nm HOPG 6 3 mV STM Fig 2 a Pt Ir 0 253mm Fig 3 HOPG STM It 1 6nhA E 0 2V 10nm X10nm z 0 llnm
17. tion to hydrotreating J Mol Catal A 215 143 147 2002 17 212 221 2003 CellCalc Windows 45 2 145 147 Necas D and Klapetek P 2012 source software for SPM data analysis Cent Eur J Phys 10 181 188 1957 7 p241 2013 61 21 33 Gwiddion An open
18. c Force Microscope AFM SPM STM Si 111 7x7 STM Binnig et al 1983 STM 20 Si 111 7X7 Binnig Rohrer 1986 Si STM STM 91 STM
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