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1. 16 SF FDG 1 28 29
2. 6 1 2 2 FC C 6 2
3. o 169 2009 387
4. 340 2 2 L TC nC RADIOISOTOPES 8 Vol 58 No 6 1 a
5. 16 SF FDG 1 28 29 2 2 2 LSE FDG 7 1 a
6. 2 2 nC nC 1 a
7. 1 o 4 2 3 2 3 1 E 1 1
8. 2009 4 2 nC TC LTC Spelco SUPELCOSIL ABZ Plus 5 gm 4 6 mm x 150 mm 0 12 50
9. 1 MS 3 5 C 1 1 CC 2 1 mL 1 CI ooo MBq oo GBq ooo MBq o0 GBq lmL 5 10 mL 2009 RADIOISOTOPES 58 221 245 2009 2009
10. oS 3 NS i 2 2 FN 320 ls EY 1 RADIOISOTOPES Vol 58 No 6 a ep oe nt 1
11. 168 Jun 2009 5 RS 5 1 2 PET
12. 224
13. MBq 8 181 400 RADIOISOTOPES Vol 58 No 6 2 3N OO O 3N No OOOOOO O 1 10 mmolL 500 mL ooo 500 mL CM
14. 2 1 3 6L 4 3 5 5 0 5zm 5m 100 22 M3 5 100 A lt 10 000 lt 70 100 000 M6 5 lt 100 000 3 700
15. 84 Jun 2009 2009 303 1 1 1 1 CIDG 1 3 I IL SO EEO
16. PET 3 148 Jun 2009 3 a 1 1 10
17. 3 1 2 3 1 PET PET PET PET 3 2 PET 1 3 PET 5 4 PET 4 1 2 1
18. b Jun 2009 PET 3 Cc EF HH 2009 341
19. 40 90 2 2009 311 2 1
20. SK603 90 Jun 2009 2009 309 4 2009 11 5
21. 388 6 RADIOISOTOPES Vol 58 No 6 3
22. 4 2 386 RADIOISOTOPES Vol 58 No 6 5 PET OO OO QO OO O
23. 366 RADIOISOTOPES 2 2 E UM Vol 58 No 6 7 1 a
24. Hz O gt 97 lt 0 8mS m 361 0 1 t CH OOO b OOOO SF
25. 6 1 2 1 1 1 2 1 3 1 4 2 1 2 2 2 3
26. 5 205 424 RADIOISOTOPES Vol 58 No 6 2 N OO O 3N No Nova Pak C18 3 9 mm x150 mm 5 mmolL PIC B 8 CHaCN 40 60 0 5 mL NH 2 5 1 25 mL 10 1 mL Mm Db Re y 9 5 10 5 150 EU 5 0 8 0 511 keV 511 keV 1022 keV 95 ppm 2 ppm 1
27. PET 3 2 Jun 2009 c 2009 321
28. b 3 a 1 1 10 b 3
29. M1 50 ooc M1 M50 ooo TS TL1K ooo Dualex SP ooo 18 Gx38 mm ooc 20 Gx70 mm ooo 20mLV20 9p9 UV ea WASTE RNN Po 200 mL ooo 500 mL ooo 1 2 O
30. 1 b PET 3 HEPA 2 a b L
31. 219 438 RADIOISOTOPES Vol 58 No 6 14 1 ooo 6 2 83 L min f B 9 0 5 zm gt 5 zm f 2 2 2 2 2 OL CD OLE A 4 220 Jun 2009
32. 2009 4 2 SK 603 3 2009 11
33. 2 1 2 2 PET 2 4 166
34. SK603 3 2009 11 4 pH pH Whatman Type CF 5 TIonPak AS14 4x250 mm IonPak AG14 4x50 mml 3 5
35. 20 mL 20 mL 4 4 10 mmolL 4 5 3N Op gw N SN 4 6 3N NN BN LIN 0 22 um 4 7 RE 20 mL
36. 13 PET 3 PET 3 c
37. MBq 9 HTC FCIH C 0 1 mol L NaOH C18 FC C18 PC QMA CM PC MBq 10 192 Jun 2009 _
38. SK603 4 2009 11 5 pH pH Whatman Type CF 6 Finepak SIL C 18S 4 6mmx 150 mm 0 1 molL 250 25
39. 2009 4 2 F JFDG 79 298 3 4 5 6 7 8 9 RADIOISOTOPES Vol 58 No 6 FDG 8F FDG LSF FDG FDG CarboPak PA 1 4x250 mm CarboPak PA 1 Guard 4x50 mm 220 mmolL 0 2 mL FDG 25
40. 1 SF 146 Jun 2009 3 3 1 O HzO O G n FE LE PF 0 35 E 0 22 gm x 3 2 3 4 4 4 1
41. 2009 RADIOISOTOPES 58 221 245 2009 2009 RADIOISOTOPES 58 247 289 2009 7 F O1 Vol 58 No 6 2009 RADIOISOTOPES 58 291 442 2009 FDG PET 2 17 10 42 2005 16 PET
42. 5 217 436 RADIOISOTOPES Vol 58 No 6 8 C OO C Finepak SIL C18S 5 um 4 6 mm 150 mm CHaCN 0 1 mol L CHCOzNHL CHCOzH 250 250 1 2mL UV 254 nm 1 2 HC 1 5 2 miy ITT gt i H ul 2 yy lt uh gt lmyln DID Dyny 511 keV 511 keV 1 022 keV EE ne 370 MBq
43. Check before synthesis 7 8F F FDG FE SF FDG 177 396 MBq RADIOISOTOPES 8 Vol 58 No 6 178 Jun 2009
44. 1 1 1 6 6 2 2 2 1 50 cm 2 2 50 cm 3 4 H 5 pH pH pH 6 7 7 1 RN DE RT OD WEE 7 2
45. 1 2 2 2 D FEF GN 5O CO C O G5F C 2 3 4 5 6 7 8 3 lt 292 RADIOISOTOPES Vol 58 No 6 4 7 WE 5 8 CGC 6 13 7 1 2 2 D 8 WE E FDG 9 2 N 3 GO
46. _ MBq 194 Jun 2009 2009 413 8 195 414 RADIOISOTOPES Vol 58 No 6 6 C C No OOOOOO HC OOO 1 nC ooo 0 2 0 5 gt 99 9999 0 1 molL LiA1H 4 THF 0 5 mL
47. 1 1 1 SFINaF 50cm 1 2 FINaE 1 3 SF NaF 2 2 1 50cm 2 2 50cm 83 4 3 H 5 pH pH pH
48. c NC c 1 1 mol L CH MgBr THP ooo CH MgBr THF THE ooo 1 mol L H ooo ooo ooo pH ooo 124 Jun 2009 2009 343 1 2 3 1mol L CHaMgBr THF THF 0 3 0 5 mol L
49. d 1 3 1 a 2009
50. 119 122 98 0 2 4 1 5 6 1 2 20 1 ABX M 103 GE 86 Jun 2009 2009 305 b GSF 8O LO H O ooo ooo ooo 3
51. Jun 2009 So 2 3 2 2 4 2 3 PET 3 1
52. ea i 3 a 1 1 10 10 b
53. 3 3 5 3 1 10 mmol L EN 0 22 gm 3 2 O g N BN 4 4 1 3 3 N 3 4 4 2 100
54. 1 153 372 RADIOISOTOPES Vol 58 No 6 2 2 1 1 1 1 19mL1mL 1 2 1 3 2 2 1 2 2 3 4 3 5 5 0 8 0 6 511 keV 1 7 7 1 511 keV 1022 keV 1 95 E 7 4 164 ppm 1 1 7 5 2000 ppm
55. 0 25 0 5 99 75 99 5 5 1 O OO OOOO b 8O ooc 1 c O O
56. 3 1 PN 10 PN BN 1 FN N 1 1 1 1 NN ul ylmy ND ID gt
57. 1 1 1 2009 RADIOISOTOPES 58 221 245 2009 2009 RADIOISOTOPES 58 247 289 2009 8 C 1 WiC 2 149
58. 2009 349 n 3 1 1 1 2009 RADIOISOTOPES 58 221 245 2009
59. 7 2 4 3 EO HLO 4 FE LO HO O D n FE E 5 FE LSE FE RS T 2009 365 SF
60. PET 2009 329 3 PET 3 3
61. SK 603 2009 11 pH pH Whatman Type CF 95 5 FDG 0 4
62. PET PET 3 2 PET PET PET 3 3 PET 163 2009 381
63. Jun 2009 2009 359 W 13 HEPA 2 a b PET
64. 312 RADIOISOTOPES Vol 58 No 6 pH 1 PET 3 3
65. 1 b PET 3 HEPA 2 a b
66. 10 c b PET
67. 3 2 210 Jun 2009 _ 2009 429 211 430 RADIOISOTOPES Vol 58 No 6 5 C uC No 1 PartisilL 10 SAX 4 6 mmx250 mm 10mmolL HNaPO4 1 0 mL C 11 8 mL 2
68. 117 336 RADIOISOTOPES 4 Vol 58 No 6 4 pH pH Whatman Type CF 5 20 5 95 ki 0 83 6 CAPCELL PAK C18UG120 4 6 mmX 250 mm 10 mmolL 2 mL min r TC 2 8 PARTTISIL 10 SCX 4 6 mmx250 mm Whatman 50 mmol L 10 1 2 mL min r TC 3 4 7 FID TSG 1 15 SHINCARBON
69. 2 2 FC C 1 a 1 b PET 3 140
70. C18 Waters Sep Pak Plus C18 CM Sep Pak Plus Accell CM Waters MILLIPORE Millex GS MILLIPORE Dualex nC t 1 2 ooo 2 ooo 8 ooo 1 134 Jun 2009 2009 353 2
71. PC 4 12 nC C 0 22 um 5 6 5 6 Jun 2009 _ 2009 347 Sr o 1 360 960 MBq 6 16 MBq kg 30 2 15 30 2 2 1
72. 1 3 PET 5 PET 2 1 a WHO GMP PET b 1 PET
73. 7 9 1 N 2 3 2009 2009 F 4
74. 1 1 1 3 3 2 FDG 1 FDG 89 308 RADIOISOTOPES Vol 58 No 6 2 2 1 SF FDG 50cm 2
75. 3 5 Sep Pak Plus tC18 Sep Pak Alumina N 0 22 um 4 4 1 92 100 mL NaOH 536 mg NazHPO 3 204 g 4 2 FE EO HzO O p n SF PE 4 3 Sep Pak Plus tC18 Sep Pak Alumina N 4 4 EF FDG 6 4mL 1 molL 2 mL 10 mL 30 mg 4 5 FE FDG
76. 1 2 FIFDG 1 3 SF FDG FDG 1 4 WTFIFDG 2 2 1 50 cm 2 2 50 cm 3 4 H 5 pH pH pH 6 7
77. K CO 1 5H 0 1 mol L 1mol L FY ooo ooo ooo QMA 5 I a hi 67 A Ns 1C ooo 76 Jun 2009 2009 295 6 37 PS 2 ooo S 8 B ooo FDG
78. 1 360 1080 MBq 6 18 MBq kg 1 5 nmol kg 2 2 1 RADIOISOTOPES Do Vol 58 No 6
79. 2009 371 e 2 NC C 0 2 mol L ooc ooo ooo HPLC ooo HPLC BE a 2 ooo ooo a 1 2 et oo0
80. 9 CIDG CarboPak PA 1 4x250 mm CarboPak PA 1 Guard 4x50 mm 220 mmoLL 0 2 mL CIDG 27 4 1 OOOOOO OOOOOO OOOOO 2 SF FDG 91 310 RADIOISOTOPES Vol 58 No 6 CH F O 28 30 mg NO OOIHzO FP FP 12 13 mL 20 mL pH 2 mL
81. 2 2 1 50 cm 2 2 cm 50 3 4 HMV 5 pH pH pH 6 7 7 1 7 2
82. 6 4 170 7 7 1 7 2
83. HEPA 2 a b 3 a 1 1 10 b
84. 1 PET 3 2 2 a 2 384 b RADIOISOTOPES Vol 58 No 6 c
85. C FC PTC 0 22 um Jun 2009 2009 377 Waste 0 1 mL 5 gL 10 mL HPLC
86. ooo 1 7 5 0 85 2 1 21Gx38 mm ooo 6 ooo 1 ooo 1 ooo 1 ooo 1 1 2 7 3 2 9O 3 QMA 10 mL 10 mL 7 5 mL 10 mL
87. 2009 4 2 HHC 1C nC Finepak SIL C 18S 4 6 mm x 150 mm 0 1 mol L 250 250 1 2mL min UV 254 nm Desmethyl flumazenil 1 2 PC 1 5 155 374 RADIOISOTOPES Vol 58 No 6 3
88. 3 3 a 1 1 10 b PET
89. a Jun 2009 SS b c
90. 2009 293 1 mL 1 Se 2 2 D PfF FIFDG ooo NR Ge GBq ooo MBq o0 GBq 1 mL 17 21 mL 2 OOOOOO FDG OOO OO 3 1 a CisHieFs0128 ooo ooo ooo 119 122 C 98 0 2
91. 10 mL 20 mL C18 5 30mg 4mL 1 molL 2 mL 10 mL 6 6 1 80 mg 1 2 4mL 1 8 1 mol 2 mL 1 4 10 mL 1 6 C18 12 13 mL
92. 3 b PET 3 Jun 2009 c
93. 0 oooooo RI oooo oooo SO 1 O 2009 4 2 40
94. 1 23 mL 2mL 2 3 37 MBq zmol 4 105 115 5 6 7 150 EU 8 9 pH 5 0 8 0 10 511 keV 11 511 keV 1022 keV 1 12 95 13 18 1 2 000 ppm 1 13 2 1 200 ppm 1 13 3 164 ppm 1 18 4 10 ppm 18 5 CIDG 40 ppm 1 1 3
95. 99 5 vol MAN 500 mL NR 3 1 96 Jun 2009 2009 315 CN OOOOOO OOOO b GN
96. 2009 397 2 2 F D F FDG No OOOOO FDG OO OOOOO 1 ooo ooo 30 mg 180 oooc ooo 2 3mL 1mol L ooo 2 mL oo0o 10 mL ooo 99 4 mL ooo 10 mL ooof 30 mL ooc ooo 1 C18 ooo ooo 2 ooo ooo 1 ooo ooo 1 ooo Ooo 1 ooo ooo 1 ooo OoOo 1 ooo ooo 9 ooo ooo 1 1
97. 3 1 3 2 7 171 1 20 ON 2 0 12 3 4 5
98. V 1 2 V Waste FC 1 OO 2009 375 4 3 4 4 4 5 4 6 4 8 nC 157 1 2 nC CO2 0 2 0 5 NG ge TC
99. M1 50 ooo M2 50 ooo M2 M100 ooo F2 M100 ooo FF2 250 ooo X1 50 ooo X1 120 ooo TS TL1K ooo Vented Millex GS ooo 18 Gx38 mm ooo 100 mL ooo 500 mL ooo 1 105 324 RADIOISOTOPES Vol 58 No 6 2 2 1 1 11 15 3 2 1
100. b CHsMgBr 3 a 1 1 10 130 PET
101. 3 3 1 0 2 0 5 NG gw C NC CO2 3 2 nC CO2 0 1 mol L LiAlH4 THF 3 3 THF FC 3 4 PC FC 3 5 PC C 4 4 1 V 1 V 4 2 1 LPC 1 OOOOOO 2
102. 3 O 4 5 2 6 4 3 RI O 1 2
103. 5 pH pH Whatman Type CF 6 GL Sciences Inertsil ODS 2 6 mmx 250 mm 0 001 mol L 2 0 05 mol L 11 7 mL Whatman Partisil SCX 10U 4 6 mm 250 mm 0 25 mol L 4 1 9 6 mL 7 CP WAX 0 32 mmx 25 mm 30 mL min 50 C 220 10 C min
104. CM TC M R MBq 8 10 198 Jun 2009 2009 417 7 F O F No OO 1
105. 4 5 1 GSF OOOOOO OOOO c SF FDG ooo 229 Kryptofix 2 2 2 99 8 H20 10 ppm 99 995
106. 6 3 6 4 PET PET Jun 2009 a 6 5 PET 5 6 6 PET 4 9 6 7 PET
107. c 111 E RADIOISOTOPES 330 1 1 3 4 3 2009 RADIOISOTOPES 58 221 245 2009
108. 1 1 2 2 D TE EF FDG 2 1 mL 1 6 5 2 2 pD 0 45 mL 12 13 mL 1 mol L 0 09 mL 2 mL 0 45 mL 10 mL 1 100 mL NaOH 536 mg NazHPO4 3 204 g 2 OOOOO FDG O OO OOOOO 3 1 a CFO 8 2 ooo ooo ooo 3
109. 1 3 O O O OOO 1 4 1 2 1 3 STEP1 4 STEP 1 STEP 2 STEP 3 STEP 4 5 INJECTION CHECK STEP
110. 4 2 100 gL Sep Pak Plus C18 6 4 3 Sep Pak Plus C18 6 1 Sep Pak Plus C18 CM 6 2 139 358 6 7 1 2D 240 900MBq 4 15MBq kg 5 1 3D
111. PET PET 3 4 PET PET 4 1 4 2 PET 4 3 4 4
112. LiAlIH4 THF a V _ ooo ooo gt 99 9999 1 2 3 114 Jun 2009 2009 333 4 1 0 mol L LiAIH4 THF THF 0 1 mol L 0 1 mol L LiAIH4 THF ABX e
113. 127 346 RADIOISOTOPES 5 Vol 58 No 6 Whatman Partisil 10 SAX 4 6 mmx 250 mm 10 mmol L 1C 11 8 mL Merck 7 5 mm x HC 9 6 mL 4 PC 1 OOOOOO 2 NC 0 2 0 5 300 mm 40 JC 5 10 mL pH 0 5 mL 1 JC COz
114. 2 1 2 OnGuard H OnGuard Ag 20 mL 3 OnGuard H OnGuard Ag Waste 193 412 RADIOISOTOPES Vol 58 No 6 4 0 5 mL 5 10 mL 5 nC CO
115. YY HO gt 98 150 7S cm 4 YY 5 O ooo ooo ooo CE
116. b PET 2009 367 3 c
117. Jun 2009 2009 389 2 4 a b c 2 d e 2 5 2 6 2 7 2 8 2 9 2 10 20 2 11 30 2 12
118. ooo 1 2 d nC l d 1 1 0 molL TLiAIH4 THF 9 THE olL LiAl1H4 THF R 0 1 mol L LiAIH THE Ascarite 20 30 mesh 1 4 1
119. CarboPak PA 1 4x250 mm CarboPak PA 1 Guard 4x50 mm 220 mmolL 0 2 mL CIDG 27 2009 I 8 25 9 1 Kryptofix 2 2 2 0 38 80 Jun 2009 _ 4 1 2009 299 FDG 2 SF FDG Nol NO H 0
120. 2 3 C18 Waters Sep Pak Plus C18 4 QMA Sep Pak Light Accell QMA Waters 5 CM Sep Pak Plus Accell CM Waters 6 MILLIPORE Milex GS 7 MILLIPORE Dualex 8 115 334 RADIOISOTOPES Vol 58 No 6 C sosf 1 2 2 1 4mL 1mL
121. 5 2 5 6 1 120 480 MBq 2 8 MBq kg 40 90 2 2 1 83 2009 301
122. II 511 keV 511 keV 1022 keV 95 2 000 ppm 1 3 2 3 3 3 216 Jun 2009 2009
123. PET 4 5 PET 4 6 PET PET 382 RADIOISOTOPES 4 7 4 8 6 PET 4 9 4 10
124. ooo gt 99 9999 1 2 3 MILLIPORE Milex GS 4 MILLIPORE Dualex 5 OnGuard Ag OnGuard H 6 d NC looo 1 125 344 RADIOISOTOPES Vol 58 No 6 2 2 1 5 10 mL
125. O 12 1 a 1 a b PET 3 HH 110 Jun 2009
126. 99 9999 L J 1 150 Jun 2009 _ 2009 369 FC CCO OOOOOO OOO c nC 1 2 d C NC
127. 2009 4 2 SK 603 3 2009 11 4 pH pH Whatman Type CF
128. 8 4 5 pH pH pH 6 7 7 1 7 2 1 FC
129. NG ge TC CO NC C 118 AgOTf CA 980 nC CO2 0 2 0 5 NO eg TC PC CO PC CO
130. 2 3 ooo ooo 38 0 25 0 5 0 8 gt 99 9999 10L ooo gt 99 9999 10L ooo gt 99 9999 10L ooo 1 150 OOOOOO RI OOO O OO 2 3 104 Jun 2009 d O e 2009 F
131. WASTE 50mL ns TB 18Gx38 mm Dualex SP V21 V22 5 20GX70 mm a WM je ie MM Nd WASTE NY A 50mL 18Gx38mm 2 Dualex SP V28 N Se NO ti 50 i 20G x 70 mm 18Gx38 mm i 500 mL sO M1 M50 TS TL1K
132. 129 348 7 1 a RADIOISOTOPES Vol 58 No 6 1 b PET 3 2 a
133. 3 c IT 1 1 1 1 ITILT 141 360 RADIOISOTOPES 1 4 3
134. CI 50cm 1 2 CH 1 3 CH H 1 4 CH 2 2 1 50cm 2 2 50cm 8
135. SK 603 E 11 99 318 RADIOISOTOPES Vol 58 No 6 4 pH pH Whatman Type CF 5 Shim Pak 3 9 mmx 150 mm 5mmolL 3N 4 5 mL Nova Pak C18 3 9 mmx 150 mm 5 mmolL PIC B 8
136. 1 1 mL M Z 104 1 M 136 Jun 2009 2009 355 3 SK 603 4 2009 11
137. 222 Jun 2009 2009 441 16 ooo 1 2 1 2 3 4 223 442 RADIOISOTOPES Vol 58 No 6 17
138. 20 2 2 1 RADIOISOTOPES 9 Vol 58 No 6
139. FDG PET 2005 1 1 SF F NaF 2 1 mL 1 ooMBq ooGBq ooMBq 00GBq 6 8mL 7 2 OOOOOO 142 OO Jun 2009 3 1 CE a 1 2 WO H O ooo ooo ooo 2009
140. OO 2 3 4 5 6 7 8 a b 5 25 30 CASO 9 SCDA Soybean Casein Di a a 90mm
141. 1 1 1 2009 RADIOISOTOPES 58 221 245 2009 2009 RADIOISOTOPES 58 247 289 2009 3 3 O 2009 RADIOISOTOPES 58 291 442 2009 4 FDG PET
142. 1 1 1 1 3 3 98 Jun 2009 _ 2009 317 2 2 1 1 1 N 50 cm 1 2 N 1 3 HN
143. 95 5 FDG 0 4 0 1 vol22 FDG 0 6 6 Bondapak carbohydrate 3 9 mmx30 cm 85 15 1 mL FDG 6 5 7 TSG 1 15 SHINCARBON A60 80 3 2x3 100 mm 00 180 FID 180 Nz 70 kPa 4 1 3 4 6 7 8
144. Sep Pak Plus C18 nC 4 6 3 3 LTC PTC 3 4 0 22 um 4 7 C 4 8 PC 4 PTC 4 1 NC 0 22 um 5
145. 131 350 RADIOISOTOPES Vol 58 No 6 3 1 a 1 2 OH NCH CH OH 2 ooco ooo ooo 3 99 0 4 5 6 1 1 2 b nC WCO2
146. 2009 RADIOISOTOPES 58 247 289 2009 4 C 1 Lr Q C 2 1 mL 1 L IC ooo MBq oo GBq ooo MBq oo GBq 1 mL 8 5 mL mn Vol 58 No 6 2009 RADIOISOTOPES 58 291 442 2009 FDG PET 2 17 10 42 2005 16 PET FDG PET 2005
147. 1 c ooo ooo 2 ooo ooo a 4 i ooo yy ooo a _ A aa 0 ooc ooo
148. 1 5 1 O 2 O 3 4 5 Jun 2009 1 6 0 25 0 5 N d n O O O O PO OO sO 5O O 400 MBq
149. QMA CM 1 C 2 3mg 0 1 mol L 0 5 mL 1 0 2 mL 3 3 1 HC 3 2 I 0 1 mol L NaOH Sep Pak Plus C18 NC Sep Pak Plus C18 QMA CM 0 22 um 3 3 4 4 1 Sep
150. 2009 2 Nee 7 a 0 pm nm 1 2 4 221 440 15 RADIOISOTOPES Vol 58 No 6 ul Mn M 2 4 A
151. 3 135 354 RADIOISOTOPES Vol 58 No 6 2 2 1 1 1 CI 50cm 1 2 LC 1 8 CH 1 4 CH
152. FC Waste Preparation 5 mL 5 mL C18 QMA CM 191 410 RADIOISOTOPES Vol 58 No 6 7 NC CO2 0 2 0 5 N p og C NC CO OOOOO OOOO LA 8 nC CO2 nC PC CO TC TC
153. FC PC 4 THF 1 0 molL LiAlH4 THF 0 1 mol L EE LiAIH TH FC FC d C HCl i MC LiAlH4 THF TA ANIA ho 3 2 3 1 0 molL LiAIH4 THF THF 0 1 mol L 0 1molL LiAlH4 THF ABX
154. PET 5 2 1 2
155. gt 199 418 RADIOISOTOPES Vol 58 No 6 QMA 5 E SO HzO O D n FE 6 N FE QMA PF 0 35
156. ooc AA 5 5 ee 5 az ef 5 ooo ooo gt 99 9999 1 2 3 MILLIPORE Millex GS 4 MILLIPORE Dualex 5 Fm HC
157. 0 22 um 5 5 6 6 6 1 6 2 1 150 300 MBq 2 5 5 MBq kg 147 2 2 1
158. 2009 407 4 C L TC No OOOOOO OOOOOO PC 1 C 1 1 THC 0 2 0 5 Molecular Sieve 4A 60 80 50 80 mesh 20 30 mesh gt 99 9999 Shimalite Ni Molecular Sieve Carbosphere Iodine Porapak N Ascarite AgOTf ooo ed i A FFF lu ui 1 2 1 2 Shimalite Ni Shimalite Ni Molecular Sieve
159. SE SE QMA IC HH PS 2 3 1 QSF 2 35 mL 1 mol L 15 mL 0 3 mol L 3 2 mL 28 mg 7mL 2 2 2 200 mg 0 2 mL 2 2 2 0 7 mL 4 100 mL
160. HC Desmethyl flumazenil DMF 1 mg mL NaH DME 0 2 g mL HPLC 1 PTC 2 Desmethyl flumazenil 1 mg DMF 1 mL 1 0 4 mL 2 2 HTC QI Desmethyl fumazenll 0 5 mg mL 0 2 molL HPLC 1
161. 2 5 C18 CM 6 100gL C18 100 zL C18 1 10mL 10mL 5 10mL 5 10
162. 2009 RADIOISOTOPES 58 247 289 2009 ha 6 CC 2009 RADIOISOTOPES 58 291 442 2009 4 FDG PET 2 17 10 42 2005 16 PET FDG PET 2005 1 1 C 2 1 mL 1 TC ooo MBq oo GBq ooo MBq oo GBq 1 mL 5 gt 10 mL 2 OOOOOO nC
163. PET PET 1 2 PET PET PET 1 3 PET 5 2 1 2 2
164. b PET 3 HEPA 0 2 a b 2 13
165. 2 V 201 420 RADIOISOTOPES Vol 58 No 6 1 2 V Waste 1 2 10 mL 20 mL HPLC 0 1 mL 5 uL 10 mL
166. 1 mol L 0 3 0 5 molL CHaMgBr THF 0 1 mol L 5 mL 2 0 mL 0 3 0 5 molL CH MgBr THF 0 4 mL 6 nC COz 0 2 0 5 Np g C LTC uCO2 OOO OO OOOO uA 7 nC CO2 C FC CO PC CO CHaMgBr THF TC
167. Megapak SIL C18 10 10 mm Xx 250 mm CH CN 6 mmolL H PO 160 840 6 0 mL min UV 254 nm V 0 1 mol L LiAIH4 THF 1 0 1 molL HiAlH4THF 0 5 mL 6 Desmethyl flumazenil DMF 0 4 mL NaH DMF 0 5 L 2 V 0 5 mL 0 4 mL Desmethyl flumazenil DMF 1 mg mL 0 4mL NaH DME 0 2 g mL 0 5 nL 0 5 mL nC CO2 0 2 0 5 Np g C FC
168. OO O OOOO 1 C 1 2 113 332 RADIOISOTOPES d C d 1 C Vol 58 No 6 Shimalite Ni Molecular Sieve Carbosphere CICO Cl Molecular Sieve 4A 60 80 Iodine Cl Porapak N Ascarite AgOTf 1 CI
169. Ascarite AgOTf Shimalite Ni Molecular Sieve Carbosphere PorapakN 1 3 189 408 RADIOISOTOPES 2 C 2 1 TC mC Waste Vol 58 No 6 0 2 0 5 gt
170. E 13 13 4 3 13 5 CIDG 1 F FDG
171. 3 a 1 1 10 122 3 PET 3
172. LOAD 180 Jun 2009 2009 C18 X1 50 X1 120 Millex GS Dualex 12 18 mL 7 FE DG E 399 WE FDG
173. 0 1 mol L LiAlH4 THF 1 0 4 mL 0 1 molL HiAlH4 THF 0 5 mL 190 Jun 2009 2009 409 3 L FC 0 1 molL olL QMA CM 22 Gx38 mm E 20 Gx70 mm ooo ooo 1
174. 0 1 vol FDG 0 6 Bondapak carbohydrate 3 9 mmx30 cm 85 15 1 mL FDG 6 5 TSG 1 152 SHINCARBON A60 80 3 2x3 100 mm 90 180 C FID 180 C Nz 70 kPa 4 1 3 4 6 7 10 CIDG 11
175. 9 1 O 30 2 3 328 10 11 1 gt 120 480 MBq min 2 8 MBq kg min 0 gt 480 4 800 MBq 8 80 MBq kg 1
176. mL 4 mL 1mL MBq yy myn 19 21 EU 150 EU pH 5 0 8 0 511 keV 511 keV 1022 keV 1 3 1 1 1 3
177. 3 3 1 0 2 0 5 NG eg TC C CO 3 2 TC CO 0 nC CO2 3 3 nC CO2 20 mL min 0 3 0 5 mol L CH MgBr THF 3 4 1molL C 3 5 0 22 um 128 4 4 1 4 2 OnGuard Ag OnGuard H 20 mL 4 3
178. Desmethyl flumazenil 0 25 mL 0 2 moLL 5 L PTC FC Des methyl flumazenil PC HHC TC 0 22 um 5 4 2 PC 2 V 6 159 378 6 1 6 2
179. b PET 3 160 Jun 2009 _ 2009 379 R 8 4 HEPA 2 a
180. F2 M100 FF2 250 X1 50 6 X1 120 TS TL1K Vented Millex 18Gx38mm 100 mL 500 mL 1 2 2 O V24 AC 6 20 mL 18Gx38 mm 2 20Gx70mm i 185 404 RADIOISOTOPES Vol 58 No 6 V26 WASTE V25
181. 0 1 mol L LiAIH4 THF 1 1g 1g 0 4 mL 0 1 molL LiAlH THF 0 5 mL 196 Jun 2009 _ 2009 415 4 1C gt 99 100 gL 10 mL 10 mL 5 10mL C18 1 CM eS 1 1 18 Gx88 mm 4 1 1 3 8 1 1
182. 172 Jun 2009 2009 391 t A 9 ie a 1 EI RE 1 CASO SCDA Soybean Casein Di gest Agar 2 2
183. PET 3 c 2 CIDG I 3 IL O HzO 4 O HO 5 CHCN Ml NazHPO4 WM
184. 2 1 b nC uCO2 1 0 2 0 5 ooo ooo ooo 0 2 0 5 99 9999 5 1 nC J CO2
185. 5 QMA Sep Pak Light Accell QMA Waters 6 IC H Alltech Maxi Clean Cartriges IC H 7 PS 2 Sep Pak PS 2 Waters 8 Waters Sep Pak Plus Alumina N 9 MILLIPORE Milex GS 10 MILLIPORE Dualex 1 O e PE EFDG 3 14 lesoc li 2 Chloro 2 deoxy D glucose ooo oe 1 77 296 2
186. 6 7 7 1 7 2 7 3 0 1 SF NaF 2009 4 145 364 RADIOISOTOPES Vol 58 No 6 2
187. F 151 370 RADIOISOTOPES e C e 1 N N FC FC Vol 58 No 6 ooo HPLC 4 HPLC 5 SR
188. 357 PC HTC H 5 10 mL C18 1 CM 1 1 1C 3 4 4 3 1 NC 10 NC mL 10 mL 5 FC 10 mL 4 5 3 2
189. SK 603 3 2009 11 4 pH pH Whatman Type CF 107 326 4 RADIOISOTOPES Vol 58 No 6 5 PEG 20M Carbowax 20M 0 53 mm x
190. 2 2 2 SF FDG FDG OO 7 1 a RADIOISOTOPES Vol 58 No 6 1 b PET HEPA 2 a
191. 4 12 4 OO OO OO OO O PET 1 1 2009 21 6 RADIOISOTOPES 58 221 245 2009 EDG PET 2 17 10 42 2005 PET PET 1 2 PET 165 2009 2 383
192. EN CM PPN CM N BN 7 CM OO OO OOOO uA 1 GBq 2 GBq 3 GBq 4 _ GBq 402 RADIOISOTOPES Vol 58 No 6 5 GBq 6 i GBq 8
193. 19 21 5 0 7 5 511 keV 4 NN EMREIN nylmyln NN NN Re 511 keV 1022 keV 95 7 3 2 000 ppm 1 3 1 1 1 3 3
194. 2 0 2 0 5 4 2 02 0 5 99 9999 NH i 1 nC WCO2 OOOOOO OOOO b NC ooo 1 2
195. 2 100 mL NaOH 536 mg NazHPO4 3 204 g ooo 10 00 mL 320 4 mg 2 O 2 3mL 179 398 RADIOISOTOPES Vol 58 No 6 3 FE O n FE OO OO O OO uA 4 10 mL C18 20 mL
196. 184 Jun 2009 _ 2009 403 3 O O No OOOOO OOOO 1 ea wa 0 M1 50 M1 M50 TS TL1K Dualex SP 18G x 38 mm 20Gx70mm i 20 mL V 20 30 mL V 30 WASTE 50 mL V 50 200 mL i M2 50 M2 M100
197. OO OO OOOOOO 1 a 112 nC OOOO Jun 2009 2009 L CHzNOS HOC1 oooc ooo ooo 185 191C gt 99 0 1
198. 2 2 1 50 cm 2 2 50cm 3 4 5 pH pH pH 6 I 7 7 1 OT i 7 2 7 3 7 9 1 LC
199. a GN O HzO ooo OOO OOO 3 J A a 2 8 3 99 5 CsH OH ooo ooo ooo 3
200. PET 3 b kd flumazenil W 3 3 a 1 1
201. g 370 MBq 1 3 1 1 1 3 3 2 95 218 Jun 2009 2009 437
202. 5 10 mL 19 21 150 EU Dilip ly 5 0 8 5 511 keV y 511 keV 1022 keV 1 1 1 2 95 3 1
203. PET 4 11 4 12 1 PET 2 164 Vol 58 No 6
204. 1 2 2 PET PET 2009 21 6 RADIOISOTOPES 58 221 245 2009 FDG PET 2 17 10 42 2005 PET PET PET PET
205. 1 0 2 0 5 2 oooc ooo ooo 3 4 0 2 0 5 99 9999 1 nC uCO2 OOOOOO OOOO c PC 132 Jun 2009 4 2009 4
206. 214 Jun 2009 2009 433 215 434 RADIOISOTOPES Vol 58 No 6 7 F SF LE NaF No 1 1C PaK TIon Exclusion 7 8 mmx300 mm 1 mmol L octanesulfonic acid 1 mL 7 5mL 2 150 EU
207. 6 7 0 1 8 OFF 8 1 237 390 RADIOISOTOPES 1
208. 6 6 1 121 6 7 Jun 2009 2009 339 6 2 1 180 1 800 MBq 3 30 MBq kg 1 1 SS 2 2 1
209. PET 3 b 94 Jun 2009 _ 2009 313
210. 1 1 1 161 1 2009 RADIOISOTOPES 58 221 245 2009 2009 RADIOISOTOPES 58 247 289 2009 2009 RADIOISOTOPES 58 291 442 2009 FDG PET 2 17
211. 2 1 1 8 12 GBq zmol 4 19 21 5 0 8 0 511 keV 7 1 511 keV 1022 keV 7 2 95 7 3 350 nmol mL 1 3 1 1 1 3
212. QMA FE SF 7 MBq 8 200 Jun 2009 2009 419 8 C OO O JWC No OO HC 3 1 Ei gt 3 J 1 1C
213. 4 4 1 TC 2 V Waste 0 1 mL 5 gL 10 mL HPLC Desmethyl flumazenil DMF 0 4 mL NaH DMF 0 5 20C PC FC Desmethyl fiumazenil DMF
214. O Rt 2 2 1 RADIOISOTOPES Vol 58 No 6 2 2 O
215. RADIOISOTOPES 58 247 289 2009 am pk 2009 RADIOISOTOPES 58 291 442 2009 FDG PET 2 17 10 42 2005 16 PET FDG PET 2005 123 342 RADIOISOTOPES Vol 58 No 6 2 OOOOOO C 3 1 a LPC CCOz gt
216. 1 3 1 1 1 3 3 154 Jun 2009 2009 373 2 2 1 1 1
217. 18 Gx88 mm 1 2 50 mL 29 gL 3 O O O g Ho Td 1 5 1 6 1 1 1 2 1 10 mmol L gt RT UU ooo 29 zL 2 10 mmol L 3 CM
218. 2 17 10 42 2005 16 PET FDG PET 2005 1 GO Hz O 2 1 mL 1 0 oo MBq co GBq oo MBq oo GBq 1 mL 8 12 mL 2 OOOOOOO OO 3 103 OOOO 322 RADIOISOTOPES Vol 58 No 6 1 a sO 1 ooo
219. oO 167 385 b 3 2 a b 4 1
220. 4 HEPA 2 a b pH 3 a 1 1 10
221. PC CO LiAIH THF 20C 1 0 1 mol L LiAIH4 THF nC CO2 IPC CO 0 1 mol L LiAIH4 THF nC CO2 PC C AgOTf nC nC NC Des methyl flumazenil DMF FC AgOTf EEC Des methyl flumazenil 376 RADIOISOTOPES Vol 58 No 6 2 nC 2 1 NC
222. 2 O 3 O 2 O 2 5 mL 176 Jun 2009 2009 395 3 FE O p n F E OOOOO OOOO LA 2 4 QMA F 200 QMA 10 mL 60 mL ICH
223. 1 3 0 4 5 5 0 5 5m 350 000 m 5m 2000 m 0 5 5m 350 000 m 5m 2 000 m 0 5 5m 3 500 m 5m 1 Vol 58 No 6 2
224. 138 1C nC COz Waste 4 3 1 4 4 TC CO 0 2 0 5 NG gw TC NC CO2 4 5 LiAIH4 THF 20C 1 0 1 mol L LiAIH4 THE 4 6 FC CO PC CO 0 1 mol L LiAIH4 THE nC CO 4 7 C 4 8 TC FC C Jun 2009 2009
225. 4 8 CM QMA 4 9 4mL 4 10 PC C 4 11 PTC C L HC 4 12 L TC NC 0 22 gm 5
226. 7 1 511 keV 1022 keV 1 95 2 ppm 7 2 7 3 1 3 1 3N 10 3N BN 1 3N 3N 1
227. 1 2009 RADIOISO TOPES 58 291 442 2009 2009 RADIOISOTOPES 58 MV FDG 221 245 2009 PET 2 2 17 10 2009 RADIOISOTOPES 58 247 289 2009 85 42 2005 16 PET FDG PET 2005 304 RADIOISOTOPES Vol 58 No 6
228. 95 2 000 ppm 144 Jun 2009 2009 363 1 3 1 1 1 3 3 2 2
229. LOAD Sep Pak Plus tC18 Sep Pak Alumina N Jun 2009 SF FDG LOAD 4 6 FE FE SF FDG 4 7 E FDG SF FDG 0 22 um 12 13 mL 4 8 5 5 6 1 120 480 MBq 2 8 MBq kg
230. 40 mL PS 2 10 mL 40 mL 40 mL 5 2 2 2 0 7 mL 1 3 mL 1 5 mL 6 F200 FDG O Check before preparation
231. O 1 O O 1 1 3 3 1 1 1 106 Jun 2009 2009 325 2 2
232. c 2 ooo ooo ooo 1 ooo ooo es 44 ww 6 eee ooo ooo ooo 5 6 a ooo 6 J LL NE
233. 40 60 3N 1 25 mL 6 4 3N 1 O OOO 2 SN 10 mmolL NN FNI 5 40 mL 1 50 mL 29 gL 2 NN
234. I EE Me 1 2 20 1 ABX b GSF 6 1 Y OlHzO 2 ooo ooo ooo 75 294 RADIOISOTOPES Vol 58 No 6 3 H O gt 98 150 gS cm
235. 3 4 13 PET 6 1 6 2
236. 2009 427 1 3 3 2 1 209 428 RADIOISOTOPES Vol 58 No 6 4 C OO O C No 1 Partisil 10 SCX 4 6 mm x250 mm 50 mmolL 10 1 2mL C 3 4 2
237. 16 7 g 1 molL 3 3 1 EO HzO O n FEF WE 3 2 F QMA 3 3 QMA PF Kryptofix 2 2 2 81 3 4 3 5 3 6 SF KF 0 3 molL 300 FDG CH PS 2 0 22 um
238. 2 N Jl Eu N N EE FFF EF TE CF FE FE EF FT 4 C18 70 80C 8 QMA 1 mol L NaOH 5mL 10 mL CM 10 mL 5 4 mL 3 mg 0 1 molL NaOH 0 5 mL t 0 1 mol L NaOH 0 2 mL C18 0 1 mol L NaOH C18 6
239. 2009 4 oO 109 FE 9 3 O 4 5 7 8 6
240. 3 3 BE 1 78 3 FDG Jun 2009 2009 297 2 2 1 1 1 SF FDG 50 cm
241. 8 9 10 5 30 CFU 25cm 100 lt 1 M3 5 A DODD 174 Jun 2009 2009 11 No 1
242. TCI 4 0 2 0 5 1 gt 99 9999 0 1 mol L LiAlH4 THF 4 i 20 30 mesh 1 V 22 Gx38 mm 22 Gx70 mm UCH Desmethyl flumazenil DMF NaH DMF i 22 Gx38 mm 22 Gx70 mm BS 1 ww il ooo ooo gt 99 9999 1
243. 20 mL 4 3 x 5 6 6 1 101 Jun 2009 2009 319 6 2 5 6 1 240 4 800 MBq 4 80 MBq ksg 2 2 1
244. 9 4 NG 5 pH pH pH 6 7 7 1 7 2 7 3 7 4 7 O 1 HHC
245. A CT CE SA TT CE om hw he hm V32 M2 50 18Gx38 mm F2 M100 TS TL1K M2 M100 500mL 186 Jun 2009 2009 V31 PO re hm 405 ee leww el Vented Millex 1 1
246. Prepara tion 4 4 MI gt 82 RADIOISOTOPES Vol 58 No 6 4 7 9 mL 4 8 QMA QMA IC H PS 2 4 10 2 2 2 20mg 0 88mL 0 68 mL
247. 7 1 7 2 7 3 7 4 8 7 5 3 7 6 CIDG W 7 7 Kryptofix 2 2 2 1 F FDG
248. 4 4 1 4 2 4 3 C 338 2 RADIOISOTOPES Vol 58 No 6 Lr HHC CH L 0 1 molL 1 molL QMA C18
249. 6 5 8 Spelco SUPELCOSIL ABZ Plus 5 gm 4 6 mmx 150 mm 0 1 50 1 1 mL M Z 90 1 MH 4 HTC 1 C 2 EC 137 356 0 2 0 5 RADIOISOTOPES PTCICO Vol 58 No 6 CICO 0 1 molL LiAlH THE C Cl Ascarite THC cola 1 1g 1
250. O 3 7 3 OOOOO OOO uA 1 0 sO WoO GBq mL 406 RADIOISOTOPES Vol 58 No 6 2 GBq mL 3 GBq mL 4 GBq mL 5 GBq mL 6 GBq mL 7 GBq mL 8 188 Jun 2009 _
251. 10 4 L CGC 11 5 CC 12 6 CGC 1 2 2 D 7 GT GF LE FDG 8 GC 14 2 CN 15 3 5O 4 C 16 5 CC 6 C 17 1 OO OO OO OO OO OO 2 1 2 2 p F G 1 2 2 D FE E FDG 2 74 Jun 2009
252. 2 2 3 150 EU 6 511 keV 1 7 7 1 511 keV 1022 keV 1 7 2 95 1 3 1 1 1 3 3
253. CICO Cl Cl ee ooo 2 3 d 2 NC 1 0 mol L LiAlH THF THE 0 1 mol Cl 1 0 molL LiAIH4 THF BB 50 lt 80 mesh 20 30 mesh gt 99 9999 gt 99 9999 oooc TiAlH4 THE Cl ooo C L C Cd HC H HI
254. O OOO c SF FDG ooo pH ooo 99 NasHPO V 1 JIS NaOH V 2 HCI ooo 1 mol L V 3 1 100 mL NaOH 536 mg NazHPO43 204 g 2 87 306 RADIOISOTOPES Vol 58 No 6 d t a 99 Ni ON N
255. 11 2 i 5 1 2 3 MILLIPORE Millex GS 4 MILLIPORE Dualex 5 152 gt 99 9999 So BB E Jun 2009
256. 20mg 1 3 mL 0 7 mL 0 3 mol L 4 mL 5mL 4 11 Check before synthesis 4 12 F 4 9 Jun 2009 LE F FDG 4 13 F FDG SF FDG 0 22m 4 14 5 5 1
257. Waste 4 4 0 5 mL 5 10mL 4 5 4 6 4 7 0 5 mL 2 mL 0 3 0 5 mol L CH MgBr THF 0 4mL 4 8 THC CO0 nC CO 4 9 TC CO 0 2 0 5 NG ge C FC CO 4 10 nC CO2 LHC CO rNC COz 4 11
258. 0 4 mL 20 80 mesh 1g ooo 1g 1 ooo 1 1 VV 1 Fine 8 1 22 Gx38 mm 3 22 Gx70 mm 2 1 2 1 V 2 1 V Waste 1 3 V
259. 175 393 394 RADIOISOTOPES Vol 58 No 6 12 1 2 2 p EF EF FDG G OO O 2 2 D F F FDG No OOO FDG OOOO OOOO 1 500 mL 3 Millex GS Dualex WO 2 2 2 a 1C H ooo 1 a PS 2 ooo 1 ooo 1 1
260. 2 2 50cm 3 4 H 5 pH pH pH 6 7 7 1 ER EE OR PE I 7 2 7 8 1 L HC
261. 2 2 3 150 EU E 6 511 keV 1 7 7 1 511 keV 1022 keV 1 7 2 99 1 1 3 1 1 PET O 2 SO O
262. 10 mL 60 mL 182 Jun 2009 _ 2009 401 CM 4 CM CM 5 BN O G eg N BN 6 BN
263. M2 M100 4 STEP 1 STEP 2 STEP 3 STEP 4 V32 5 1 O 2 O 3 4 5 6 O O N d n O O O sO sO O
264. ylmy ly H 206 Jun 2009 2009 425 1 3 3 2 1 207 426 RADIOISOTOPES 3 CO O No
265. 126 Jun 2009 2009 345 2 2 1 1 1 CI 50 cm 1 2 Cl 13 1 2 2 1 50 cm 2 2 50 cm
266. 2 NaOH 3 1 molL HCI 4 CHiCN 2009 5 AAD7O7SO7OPpS 58 221 245 6 C18 2009 7 SF EFDG FDG 8 PET V 1 FDG 2 17 10 42 2005 2 N 1 1 N N NH 2 1 mL 1 FPN oo MBq oo GBq oo MBq oo GBq 1 mL 9 11 mL 95 314 RADIOISOTOPES Vol 58 No 6 2 OO OOOO O OO 3 1
267. SF FDG FDG F FDG 2 E TR B PP 50cm 50cm pH Type CF pH A E Whatman E
268. WCO2 202 Jun 2009 2009 421 OOOOO OOOO uA 7 nC CO2 nC PC CO nC FC Desmethyl flumazenil DMF HPLC HC MBq 8 203 422 RADIOISOTOPES Vol 58
269. 1 1 511 keV 511 keV 1022 keV 95 2 nmol mL 350 nmol mL 1 3 1 1 1 3 3 2
270. 10 mL 4 mL FIFDG 10 mL 5 mL 1 1 C18 1 GF 2 100 mL NaOH 536 mg NazHPO 3 204 g 3 3 1 O HzO O p n SF PF 3 2 F 4 4 3 3 1 3 4 6 O 2 O 8 D 3 4
271. 116 Jun 2009 2009 335 2 2 1 1 1 L C l 50cm 1 2 L TC H 1 3 L UC H 2 2 1 50cm
272. 2 LE FDG 2009 I 4 FDG F FDG SF FDG E FDG CarboPak PA 1 4x250 mm Car boPak PA 1 Guard 4 x 50 mm 220 mmoLL 0 2 mL FDG 25 3 BB
273. PET PO 2 O O O 1 O sO 1 1 1 1 208 Jun 2009
274. 2009 411 5 C CC No OOOOO nC 1 FC 1 10 2 0 5 1 gt 99 9999 3 0 5 mol L CHsMgBr THF 1 0 4 mL molL d 2 0 mL 0 5 mL 4 d 4 Millex GS 1 Dualex 1 22Gx 38mm 1 5 22Gx70mm 1 2 18Gx88mm OnGuard Ag 1 1 OnGuard H H Fo 2 2 to 1
275. see 1 143 362 RADIOISOTOPES Vol 58 No 6 c Us 21 ooo H ooo 5 NT ooo 7 ooo es Ba ooo a 1 ooo 9 oooc ooo
276. 0 4 mL CIH 5 AgOTf 0 8g 1 nC CO2 156 Jun 2009 3 3 3 1 3 2 3 4 0 2 0 5 NG C NC CO2 PC CO 0 1 mol L LiAIH4 THF THF PC nC NC nC Des methyl flumazenil N N DMF HC AgOTf IC Desmethyl flumazenil 4 4 1
277. 2009 RADIOISOTOPES 58 291 442 2009 4 FDG PET 2 17 10 42 2005 16 PET FDG PET 2005 KI DA 368 RADIOISOTOPES Vol 58 No 6 1 mL 1 CH ooo MBq oo GBq ooo MBq oo GBq 1 mL 8 10 mL 0 01 mL 0 1 mL 2 OOOOOO nC 3 1 a 1 Desmethyl fumazenil C14Hi2FN303 b Cl ooo o
278. A 100 or 1 0 5 lt 1 M3 5 B 10000 10 0 5 5 M5 5 WO 100 000 a 100 0 2 50 M6 5 a b 4 173 392 RADIOISOTOP 10 TC 2 1 3 ES Vol 58 No 6 4 5 6 7
279. 2 Desmethyl flumazenil 0 5 mg 0 2 mol L 5 uuL DMF 1 mL 1 0 25 mL nC 3 3 1 HFC flumazenil DMF NaH DMF mol L TC HPLC Desmethyl C HPLC 0 22 um 3 2 TC Desmethyl flumazenil 0 2 158 0 22 um
280. ITC CO Shimalite Ni Molecular Sieve PC CO FC NC AgOTf PC PTC nC FC CI PC 3 2 V 1 V Waste Lr HHC 1 Jun 200
281. NC e 1 1mol L 0 1 molL fh ooo 1 2 e 2 C18 3 QMA 1 RN ooo gt 99 9999 1
282. ooo ooo ooo gt 99 9999 1 2 Waters Sep Pak Plus Accell CM 3 MILLIPORE Millex GS 4 MILLIPORE Dualex 5 97 316 RADIOISOTOPES Vol 58 No 6 2 2 1 10 mL 1 mL 9 5 10 5 150 EU 2 2 511 keV 1
283. 2 1 RADIOISOTOPES Vol 58 No 6 19 mL 2 mL 37 MBq zmol 105 115 150 EU 3 5 0 8 0 511 keV 511 keV 1022 keV 7 8 2 000 ppm 1 7 4 164 ppm 1 Ei 7 5 95 10 ppm 7 6 CIDG 40 ppm 7 7 Kryptofix 2 2 2 1 40 ppm 1 1 2 1
284. 8 5 MILLIPORE Millex GS 6 MILLIPORE Dualex e F JFDG 1 2 Deoxy 2 fHuoro p glucose oo 2 2 Chloro 2 deoxy D glucose oc 3 oo 4 oo 5 oo FT 2 Deoxy 2 fluoro D glucose SIGMA F 5006 2 2 Chloro 2 deoxy D glucose ABX 88 Jun 2009 2009 307 2 2 1
285. 99 9999 0 1 mol L LiAlH4 THF 0 5 mL 0 4 mL 20 30 mesh 1g 1g 0 8g 1 1 1 VV ooo 1 ooo 1 22Gx 38mm oooc 3 22G x70mm ooo 2 1 2 1 V 2 2 1 1 V Waste 2 3 AgOTf V
286. FDG oooc ooo ooo 9 ooo 9 ooo 2 wT i a 18 1D gt eg O ooo 11 ooo ooo gt 99 9999 1 2 3 Kryptofix 2 2 2 Merck 4 F Kryptofix 2 2 2 0 3 molL QMA
287. 3 7 4 4 1 FE OO HzO O p n SF WE 4 2 QMA QAMA QMA 10mL 60 mL 4 3 IC H 40 mL PS 2 10 mL 40 mL 4 5 0O Waste Check before preparation
288. A60 80 3 2x3100mm 90 180 C FTD 180 70kPa 4 1 PC 1 OOO 2 2 1 4N D ga nC nC COz2 Shimalite Ni Molecular Sieve C C Ne NC nC 3 3 1 0 RR 680 730 C OY nC 2 Rk AgOTf PC NN CIRREE
289. No 6 e 2 1 2 t 18 a Cy Og oooc CM 0 ooc MM 7 Ss A gt 99 9999 1 2 3 4 5 6 7
290. mL 7 FC CCO 0 2 0 5 N p gw C FC CO 197 416 RADIOISOTOPES Vol 58 No 6 OOOOOO OOOO uA 8 nC CO2 PC NC CO2 PC C MBq 9 FC TFC FC C18 C C18
291. mmol L NazCOs 1 0 mmol L NaHCO 1 2 mL 18F 3 0 6 TSG 1 15 SHINCARBON A60 80 3 2x3100 mm 900 180 C FTD 180 C Nz 70 kPa 4 1 FE 1 OOO OO 2 SF sO0 POIH O E 2 5 mL 7 0 35
292. 0 1 2 mL min CH 1 5 7 FID TSG 1 15 SHINCARBON A60 80 3 2x3 100 mm 90C 180 C FTD 180 C 70 kPa 4 1 6 7 4 FC FC 1 OO OOO 1C 2 FC C 1 0 2 0 5 FC CO oco GBq 0 1 molL LiAIH THF Cl CH
293. 0 molL LiAIH4 THF THF 0 1 mol L 0 1 mol L LiAIH4 THF 2 3 lt ABX d 2 1 HiAIH THF ooo ooo Fine a nl i gt 99 9999 1 2 e LTC e 1 133 RADIOISOTOPES Vol 58
294. 1 RI OOO Vol 58 No 6 OO O Molecular Sieve 13X 30 60 mesh 3 mmid x3m He 1 2kg cm 55 TCD O 0 1 2 11 15 150EU 5 0 7 5 511 keV 511 keV 1022 keV 99 yy 0 A NR 1 3 1 1
295. 10 42 2005 16 PET FDG PET 2005 307 10 3 30 PET 3 19 PET BR 5o baA 5 3 PET OO OO OO OO O 162 RADIOISOTOPES De Vol 58 No 6 2009 RADIOISOTOPES 58 221 245 2009 FDG PET 2 17 10 42 2005 PET PET
296. 3 3 212 Jun 2009 _ 2009 431 213 432 RADIOISOTOPES Vol 58 No 6 6 C O Q C Inertsil ODS 2 6 mm X250 mm 1 mmol L naphthalene 2 sulfonic acid 0 05 molL HsPO4 1 0 mL C 11 7 mL 2 3 MBq 19 21
297. 30 m 40 C 250 200 50 guL 99 sO O 1 OO 2 2 1 0 25 0 5 CO O 2 2 O O 2 3 O O 1 1 1 O O 1 2 O O
298. 4 CIDG 40 ppm 1 3 2 1 FDG 3 3 3 4 204 Jun 2009 _ 2009 423
299. 9 2009 337 1 nC COz 0 2 0 5 NG g TC TC CO LiAIH4 THE 20C 1 0 1 mol L LiAIH4 THEF nC CO2 NC COz 0 1 mol L LiAlH4 THF nC CO C LHC AgOTf C nC nC PC PC TC
300. N V 4 le EE a a ooo 2 MM ooo ooo a a 9 ooo V 5 V 0 i kk 8FIFDG ooo V 7 NN ooo ooo a ooo ooo V 8 ooo gt 99 9995 1 2 Waters Sep Pak plus Alumina N 3 C18 Waters Sep Pak plus tC18 4 WEF FDG SFIFDG
301. No 6 13 1 2 2 p 1F F FDG OO O 2 2 D F ISF FDG No 8 i 105 115 3 150 EU 5 0 8 0 511 keV 511 keV 1022 keV 95 23mL 2mL M pli pin 2 000 ppm 1 200 ppm 10 ppm
302. Pak Plus C18 70 80 8 4 2 120 Waste Preparation 4 3 4 4 1 3mg 0 1mol L NaOH 0 5 mL 0 2mL Sep Pak Plus C18 4 5 QMA 1molLLNaOH 5 mL OH 4 6 CM 4 7 Sep Pak Plus C18 Sep Pak Plus C18
303. RADIOISOTOPES 58 291 442 2009 2009 113 8941 2 28 45 Key Words EDG BO water 9N ammonia 1C L methionine NC sodium acetate 1C choline 18F sodium fluoride TC flumazenil drug product standard code manufacturing control standard code manufacturing hygiene control standard code quality control standard code manufacturing direction manufacturing record quality record 2009 gt Reference Materials for Standards of Compounds Labeled with Positron Emitting Radionuclides Ap proved as Established Techniques for Medical Use 2009 revision Nuclear Pharmacy Workgroup Subcommittee on Medical Application of Positron Emitting Radionu clide
304. oo ooo to 286 289 99 0 1 2 1 Desmethyl flumazenil CCOz 0 2 0 5 oooc ooo ooo 0 2 0 5
305. ooo ooo gt 99 9999 1 2 Waters Sep Pak Plus Accell Plus QMA 3 MILLIPORE Millex GS Vented 4 MILLIPORE Millex GS 5 2 2 1 1 1 1 E mL 1 8 105 115 2 2 150 EU 5 0 9 0 1 511 keV 511 keV 1022 keV 7 2
306. s Medical Science and Pharmaceutical Com Association 2 28 45 Honkomagome Bunkyo ku Tokyo 113 8941 Japan 2008 11 mittee Japan Radioisotope 6 73 2009

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