Analytical Circle No.76 （2015.03）
Contents
1. Chromadex 2 CAS ASB 00001051 250 250mg 19 000 ASB 00001051 500 Acetaminophen 103 90 2 C H NO P 500mg 31 400 ASB 00001117 005 5mg 42 800 Re 80 ASB 00001117 010 Ref Acetylcorynoline 18797 80 3 C HaNO P 10m2. 0 45 m 1
3. 100 5 4 6mm 1mL min 20 2 100 6
4. SunShell C8 30HT SunShell C8 30 26m 0 5 m 16nm C18 2 C18 SunShell SunShell HFC18 16 C18 WP C18 C18 SunShell HFC18 16 SunShall HFC18 15 Sunshell 18 W
5. 4 Yt 0 30 10 1 2 30 30 3 1 NMR qNMR eVolWNMR 115mm 180mm NMR eVol XR eVol XR NMR O O 5uL O 115mm
6. ie 2014 1863
7. SGE SGE Focus Liner GC 1 a LF 0 3 i 4122 NZ2 1 a 2 9
8. Wako No 038 09002 J TD 90 0 Ti 1 70 3 35mm 6 10mesh 25g 5200 035 09012 JL ID 90 096 Ti 0 85 2 36mm 8 20mesh 25g 4 300 036 09461 90 096 Ti 710 1180 m 14 24mesh 100g 9 200 536 14661 HL Perkin EImer Oak Brook Instrument Div 40g 83 000 No 036 09961 300 lt 850 m 20 50mesh 100g 15 000 038 11371 180 425 m 40 80mesh 100g 12 000 031 13701 150 250um 60 100mesh 100g 11 000 032 10811 0 4 x 5mm
9. ODS C18 pH 10096 ODS pH pH2 lt 7
10. 3 i a 4 http www siyaku com 2015 3 No 76 ANALYTICAL CIRCLE Wakopak
11. SunShell C8 30 2 6 hm 30 nm 100 150 x 2 1 mm Mobile phase A 0 1 TFA in water Gradient YA B 20 65 Flow rate 0 5 mL min 25 C 60 C 80 CC Temperature 25 C 60 Cand 80 C Oo BA C 2 Lysozyme 3 BSA BSA Ovalbumin 4 Myoglobin 5 Ovalbumin 25 C 80 C OAL I 80 C pH2 N_ Retention time min SunShell C8 80 C pH2
12. 2 72 0 3 0 1day 1 2day 2 3day 1 96 1 66 1 69 4 0 3day 6 K NA 1 SunShell RP Guard Filter J SunShell RP Guard Filter 2um C18 C18 5 8 CBGAAC CBGAKN HEX 14mm PEEK http www wako chem co jp siyaku product analysis ChromaNikSunShell index htm O Y Q amp A rhttp www wako chem co jp siyaku pickup chromato index htm 15 ANALYTICAL CIRCLE 2015 3 No 76 C ChromaDeX
13. 15 25 35 L 5 3 8 LL AS ee C Mobile phase A 0 1 TFA in water a Gradient etn i 35 min BSA Ovalbumin mowrte05mUmn NMe tr 9 19 Sample 1 Cytochrome C 2 Lysozyme 3 BSA 4 Myoglobin 5 Ovalbumin SunShell URL http www wako chem cojp siyaku product analysis ChromaNikSunShell index htm op 2 yhttp www siyaku com 2015 3 No 76 ANALYTICAL CIRCLE
14. 225 02231 F 5mg 60 000 264 02141 F 5mg 34 000 1 Nakagawa H ez g J Anal Bioanal Technigues Special lssue 6 002 2014 E No 233 6375 C18 5 3 0mm x 250mm D 1 62 000 12 http www siyaku com 2015 3 No 76 ANALYTICAL CIRCLE a lt IF 018 24341 l 1mL x 5A 28 000 B B G G 25 g mL RR TIF B a 010 24301 1mLx 5A 20 000 25 g mL T F B 0 017 24311
15. 0816 1 ff A A 100 100 ss 0 x 40 20 20 0 0 0 20 40 60 80 100 0 20 40 60 80 100 9 6 OB B G G B B G G 7 9 0 B 94 100 97 91 97 97 86 104 B 95 98 95 89 98 98 88 115 Gn 78 105 101 99 88 99 87 99 85 103 98 99 86 99 88 102 16ng g 9 M AFLAKING M
16. AG ee FAX E mail FAX Mail 10 3 000 27 4 31 No 75 43 10 103 0023 4 1 5 a a 5 Mg Eh i RR AA lt NMR
17. Analytical Circle Wako Bio Windowd Wako Organic Square http www wako chem cojp siyaku journal index htm KN B Q amp A rhttp www wako chem co jp siyaku pickup chromato index htm 19 ANALYTICAL CIRCLE 2015 3 No 76 D gt OW k g dKO Ref Na Metabolite IM 2 1 Standard IM 2 1 019 25851 100mg 28 000
18. Accuracy 0 296 Precision 5L RSD 0 59 6 50wL RSD 0 496 100 uu L RSD 0 496 500 uuL RSD 0 3 6 1mL RSD 0 39 6 wL L L wD 5 0 2 5 50 2 50 100 4 100 100 uL syringe 500 20 500 PE 1000 40 1000 LU Q amp A rhttp www wako chem co jp siyaku pickup chromato index htm ANALYTICAL CIRCLE 2015 3 No 76
19. ATP 2 8mm 3 2mm 2 1a LS 2 8 400 LS LS 3 2 400 mE GA EA 0 ye 1 127 13cm Pen200A
20. SFC 1 2 CO DAICEL DCpakY SFC A DAICEL DCpak SFC A PBT SFC O O DAICEL DCpak SFC A gt lt 4 SFC 3 PBT _ 2 Hydroxyflavanone s 3 Hydroxyflavanone _ OH _ O ea pe 3 Column size _ 0 46cm Xx 25cmL ON Column size _ 0 4
21. 5 0 2 ux m 60
22. RR Standard 069 Em 100mg 18 000 9 98 09 qNMR a SN ocHs O 4 Dimethylsulfamoylphenyl O O Dimethyl Phosphorothioate Ci Hi NO PS 3 O 325 34 C A S 52 85 7 01 http www wako chem cojp siyaku info env article positivelist_1 htm Ref 2 10 F 20 80 80 I I TT H I Ll 1 2
23. Pen00A Pen AQUA No 383 06821 60337 Re LS 2 8 400 Re 24 000 380 06831 60338 LS 3 2 400 24 000 No 384 04911 6
24. MycoJudge No 309 95411 Ref MycoJudge 96 72 000 389 02401 IRef MycoCatch 20 30 000 G KN Q amp A rhttp www wako chem co jp siyaku pickup chromato index htm 11 ANALYTICAL CIRCLE 2015 3 No 76 _ Vako 5 T 2 HT 2 25 g mL HT 2 5 g mL 25 g mL 25 g mL T 2 5 g mL Peak No 5 LC
25. rhttp www siyaku com 2015 3 No 76 ANALYTICAL CIRCLE MycoJudge MycoCatch IMycoJudge MycoCatch MycoJudge ELISA MycoCatch R Axe NR 0 B B G G 1 25ppb 2 5ppb 20ppb HPLC ELISA
26. 98 096 qaNMR HPLC 5mg 80 000 204 17731 Ref T 2 98 096 qNMR cGC 5mg 45 000 266 01981 Ref 98 0 HPLC 5mg 50 000 K M FE Wako 3 2014 8 2010 2 FEMA GRAS 99 09 CAS No 38837 70 6 CO H IN O0 303 31 Glutamy Valy Glycine 1 Ueda Y et g Agrt Biol Chem 54 1 163 9 1990 2 Ichikawa M et g J Agric Food Chem 54 4849 54 2006 3 Shaw ML et g Phytochemistry 66 515 22 2005 4
27. 0816 7 MycoCatch 40 10 M B B G G M gt lt gt ek MycoCatch Cr Ei MycoCatch HPLC ELISA
28. 2 1 600 196 15645 500mL 2 100 316 90101 100mL 4 000 312 90103 100mL x 6 15 600 318 90105 500mL 9 000 012 11872 25g 1 800 016 11875 500g 6 800 HPLC 2014 12 2014 9 1 2015 4 30 10 10 Sunniest C18 2 m 3 m 5m WVK ChromaNik Technologies Inc 1 30 000 SunShell RP Guard Filtery SunShell C18 2 6um 5um http www siyaku com 2015 3 No 76 ANALYTICAL CIRCLE GLP
29. M M 87 M 0 5ng g 9 50g 90 200mL 5 PBS 5 Tween20 18 AFLAKING 25mL 10 i rh PBS3 3 i 1mLx3 HPLC pOCHRAKING M A B 309 A 2 48 No 308 34201 AC01 25 Ref AFLAKING 25 25 45 000 304 34203 AC01 50 Ref AFLAKING 50 50 80 000 300 83091 AC02 25 Ref OCHRAKING 25 45 000 G KN
30. OECD WV OECD 72 72hrEC OECD V OECD OECD 201 Pseudokirchneriella subcapitata 72 100 1 6 0 80 0 40 0 20mg L OECD IV OECD 100mg L 21 24C 2 0 75 x 10 cells mL 600mL 100mL x6 300mL 100mL x 3 500mL
31. PD NO No 30 CW6931 65 000 cW6331 65000 CW6431 65 000 50 382 04211 CW6941 66000 CW6341 66 000 CW6441 66 000 6 75 cWe951 71 000 cW6351 71000 CW6451 71 000 100 CWe6961 79 000 CW6361 79 000 385 04201 CW6461 79 000 150 cWe971 84000 cW6371 84000 CW6471 84000 ES 50 383 04121 CG6941 66 000 CG6341 66 000 CG6441 66 000 2 100 CG6961 79 000 CG6361 79 000 386 04111 CG6461 79 000 150 CG6971 84000 CG6371 84 000 CG6471 84 000 50 387 04021 C46941 66000 C46341 66 000 C46441 66 000 AN ioo C46961 79000 C46361 79 000 380 04011 C46461 79 000 150 C46971 84000 C46371 84000 C46471 84 000 2 50 C36941 66 000 C36341 66000 0C36441 66 000 Ns 100 C36961 79 000 C36361 79000 C36461 79 000 150 Co36971 84000 Co36371 84000 C36471 84000 Ee 50 C26941 66 000 C26341 66 000 C26441 66 000 26 100 C26961 79 000 C26361 79000 C26461 79 000 150 C26971 84000 C26371 84000 C26471 84000 50 C55941 68 000 0 5 C55961 81 000 4 7 m 150
32. E mail analyti wako chem cojp O
33. pH
34. 1L CaCL 2H 0 1 800 00 18 0000 1 MgSO 7H O 1 500 00 15 0000 OECD KH_PO 160 00 1 6000 OECD 201 OECD Medium OECD Stock Solution T x1000 19903921 90mL EacGL 6H O 6400 00640 1L OECD EDTA Na 2H 0 100 00 0 1000 y OECD Medium AO x1 000 x 1 OECD T x1000 1mL CL 4H O 41500 04150 OECD x 1 000 1mL 150 03331 50mL iR OECD WM x 1 000 1mL a 5 2 12 1L CuCl 2H O 001 0 00001 Na MoO 2H O 7 00 0 0070 OECD Medium 157 03341 50mL Stock Solution IV x 1 000 ON NaHCO 50 000 00 50 0000 No 158 03315 Ref OECD 1 x 100 500mL 7 000 153 03321 R OECD 1 x1 000 50mL 7 000 150 03331 Ref OECD x 1 000 50mL 7 000 157 03341 Ref OECD V x 1 000 50mL 6 500 No 162 03652
35. 1mL Xx 5A 20 000 25 g mL HI IF G 014 24321 1mL Xx 5A 20 000 25 g mL HT F G _ 011 24331 a 1mL x 5A 20 000 25 g mL F M 013 25751 1mL Xx 5A 40 000 0 5 g mL Ncoc 014 22621 Rf 3 98 0 HPLC 5mg 70 000 018 23481 Ref 15 95 09 qNMR HPLC 5mg 80 000 015 23491 Ref B 98 096 qaNMR HPLC 5mg 70 000 014 24201 Ref B 98 096 qaNMR HPLC 5mg 70 000 018 23501 Re G 98 096 qNMR HPLC
36. No 192 07832 425 850um 20 35mesh 25g 12 600 536 14661 1 Perkin EImer Oak Brook Instrument Div 40g 83 000 195 07562 99 59 Ti 0 1mm 25g 22 000 194 07912 850 2360um 8 20mesh 25g 9 500 No 013 11721 2g 3 400 No 537 18091 Perkin EImer Oak Brook Instrument Div 10g 330 000 176 00351 1 6 m 1g 3 150 512 82431 ICP MS 1000 g mL in Water Accu Standard Inc 100mL 13 500 204 07162 VD 25g 2 900 2015 2 Siyaku com http www siyaku com GJ rhttp www siyaku com 2015 3 No 76 ANALYTICAL CIRCLE EE
37. 30nm 500 10nm 10nm ChromaNik Technologies Inc 30nm SunShell 2 pm gm gm nm SD EM SunShell C18 WP 2 6 1 6 0 5 16 90 8 5 2 5 1 5 10 SunShell HFC18 16 2 6 1 6 0 5 16 9
38. C18 No 237 01511 Guard Cartridge Column Wakosil II 5C18 AR 4 6mm x 10mm 3 26 000 234 01521 Guard Cartridge Column Wakosil II 5C18 RS 4 6mm x 10mm 3 26 000 231 01391 Wakopak Cartridge Holder 10mm 1 10 000 1 PEEK SunShell RP Guard Filter C18 2 1 mm 4 6 mm No 380 04131 CBGAKN SunShell RP Guard Filter Starter kit a holder a cartridge a tubing 1 20 000 CBGAAC SunShell RP Guard Filter for exchange 5pcs 1 20 000 CBGAAH SunShell RP Guard Filter holder 1 12 000 2 No 360 00991 ODGHPC34 GHP MF
39. LS2 8 400 LS3 2 400 kikkomaw LS2 8 400 LS3 2 400 Pen Pen AQUA LS PD 20 PD 30 PD 10 N Pen AQUA ATP AMP ATP AMP 2 1 ATP 2 AMP
40. eVol 1 100L 9 115mm 180mm 1mL QO 115mm 180mm eVo AC O O O O 8cmCD O O eVo No 515 93771 2910200 eVol XR 1 119 000 551 02001 2910100 eVol XR NMR 1 119 000 512 93781 2910205 eVol XR 1 87 000 eVoP EN 0 a mm mm mm 519 82201 2910020 eVol 5 ux L 50 25 0 5 0 12 5L 1 9500 2910380 4 400 516 82211 2910022 eVol 50 uu L 50 25 0 5 0 2 50 L 1 9500 2910382 4 400 514 93741 2910029 eVol 100 ux L 50 25 0 5 0 2 100 L 1 10 100 2910383 4 400 513 82221
41. 5mg 90 000 015 23511 Rf G 98 096 qNMR HPLC 5mg 110 000 047 31041 RW 98 096 HPLC 5mg 90 000 044 31051 Rf 98 096 qaNMR cGC 5mg 30 000 061 05771 Rgg B 95 096 qaNMR HPLC 5mg 90 000 066 06181 IF B 95 096 qNMR HPLC 5mg 7 065 05431 Ref X 95 096 HPLC 5mg 130 000 087 09871 F _HT 2 97 096 qNMR cGC 5mg 100 000 142 08971 R 98 096 qNMR cGC 5mg 80 000 149 08741 RF 98 0 HPLOC 5mg 90 000 153 02961 IF A 98 096 HPLO 5mg 75 000 168 21631 IF 98 596 HPLC 10mg 30 000 190 16081 Ref
42. 250g 16 000 034 11253 a 100g 7 900 0 6x5 mm 250g 16000 No 538 02075 HTI II 8 20 Thomas Scientific 500g 37 000 194 09771 HI 80 0 Ti 1 70 3 35mm 6 10mesh 50g 5 200 No 133 00323 JIS 50g 6 100 83 096 Ti 1 18 3 35 6 14mesh BB 6 Ti mm mesh JIS K8228 250g 15000 134 07891 JIS 50g 6 100 83 0 Ti 710 m 2 36 8 24mesh 65 6 Ti um mm mesh JIS K8228 250g 15000 133 07981 _ JIS 50g 6 200 83 0 Ti 300 850 20 48mesh 2 6 Ti um mesh JIS K8228 400g 21500 512 31565 GFS Chemicals ACS 500g 29 500
43. 4 0mm 6 3mm 78 5mm 5 12 500 559 75311 092002 4 0mm 6 3mm 78 5mm 5 13 800 556 75321 092003 4 0mm 6 3mm 78 5mm 5 18 100 550 75341 092007 4 0mm 6 3mm 78 5mm 5 10 900 585 70551 092017 4 0mm 6 3mm 78 5mm 5 17 600 554 75361 092018 0 0 KKE CR2 0 0 4 0mm 6 3mm 78 5mm 5 21 700 551 75371 092019 F ree 4 0mm 6 3mm 78 5mm 5 19 000 GC 2010 SPL 2010 GC 2014 SPL 2014 GC 17A SPL 17 092058 2010 3 4mm 5 0mm 95mm 5 25 100 558 75381 092059 2010 3 4mm 5 0mm 95mm 5 19 500 555 75391 092062 17 2014 3 4mm 5 0mm 95mm 5 19 500 555 75411 092068 17 2014 3 4mm 5 0mm 95mm 5 25 000 554 71101 092071 3 4mm 5 0mm 95mm 5 24 200 552 75421 1092077 2010 3 4mm 5 0mm 95mm 5 17 600 559 75431 1092085 17 2014 3
44. 0 45 m 100 28 000 369 01321 4450T PVDF 0 2 m 13mm 100 23 000 365 00181 4452T PVDF 0 45 m 13mm 100 23 000 Q amp A http wako chem cojjp siyaku info chromato article FAQ htm Q amp A HP Q45 Wakopak ODS OY spTRAIAN GLP GMP FDA NMR
45. 2 siyaku com http www siyaku com 540 8605
46. 10mg 30 000 ASB 00013644 025 Rf Methylsynephrine HCI 7437 54 9 CH jaNO HCI P 5 45 100 ASB 00013890 005 5mg 27 900 Re ASB 00013890 010 Ref Mitragynine 4098 40 2 C H N 04 P 10mg 44 700 ASB 00013955 005 5mg 61 900 F on 7 ASB 00013955 010 Mitraphylline 509 80 8 C jH N 04 P 10mg 93 500 ASB 00014539 200 Nortriptyline HCI 894 71 3 C HiN HCI 200mg 28 400 ASB 00015480 005 5mg 19 000 ASB 00015480 010 Oxymatrine 16837 52 8 Ci H N O P 10mg 25 200 ASB 00015480 025 25mg 31 400 ASB 00016049 010 10mg 12 600 ASB 00016049 025 F Palmatine Chloride 10605 02 4 C iH NO CI P 25mg 15 800 ASB 00016049 100 100mg 47 300 ASB 00016869 010 10mg 9 500 ASB 00016869 025 Piperine 94 62 2 C H NO P 25mg 19 000 ASB 00016869 100 100mg 31 400 ASB 00018040 010 10mg 9 500 ASB 00018040 100 100mg 28 000 ASB 00018425 005 5mg 21 600 ASB 00018425 010 Rutaecarpine 84 26 4 Ci H N O P 10mg 40 000 ASB 00018425 025 25mg 84 700 ASB 00019280 005 5mg 31 400 ASB 00019280 010 Sinomenine Hydrochloride 6080 33 C H NO HCI P 10mg 47 300 ASB 00019280 025 25mg 94 800 ASB 00019368 005 5mg 61 900 ASB 00019368 010 Ri Stylopine 84 39 9 C H NO P 10mg 93 500 ASB 00019368 025 25mg 205 500 ASB 00020155 005 5mg 47 300 ASB 00020155 010 F Tetrahydroberberine Canadine 522 97 4 C H NO P 10mg 79 000 ASB 00020155 020 20mg 125 200 ASB 00020340 005 5mg 47
47. ss ANALY TICAL http www wako chem co jp SunShell P2 Q amp A 56 NG SER ENE RE RENE EE TREE CERES RE SE a P4 eVole XR On NR P5 SGE GC GE ES CE CESS P DAICEL DCpak SFC A RE CE eS SE Che Pg OECD Ti P14 A i P16 IRCLE LS2 8 400 LS3 2 400 ee P9 AFLAKING OCHRAKING uec P10 MycoJudge MycoCatch P11 ee P12 ee P13 ee P20 RNN P20 1 0 VN 062Me8keeah as ais P14 64 ren P18 P19 Wako ANALYTICAL CIRCLE 2015 3 No 76 SunShell SunShell C18 WP SunShell HFC18 16 SunShell HFC18 30 SunShell C8 30 SunShell C8 30HT SunShell C4 30
48. 2 A 2222 PTV PTV LVI A 17 EN 3 WW sse FocusLiner j Si OH DDT DDT 12 DDD SGE i 2 SGE 0 0 420 C et TE I 2 No 5890 6850 6890 7890 HP4890 571 69741 092001
49. C55971 86 000 O Y Q amp A rhttp www wako chem co jp siyaku pickup chromato index htm 3 ANALYTICAL CIRCLE 2015 3 No 76 Q amp A 56 Wako HPLC
50. CH 98 09 6 qNMR lt NN MM 6 Chloro 3 pyridy methyl M cyanoacetamidine N a D gt C H CIN ee 208 65 Ref Difenoconazole Metabolite D Standard D 045 33661 100mg 30 000 98 09 qNMR CI lt 0 1 2 Chloro 4 4 chlorophenoxy phenyll 2 17 1 2 4 triazole 1 yl ethanol Cl rr Ci HiaClN 0 a rT 350 2 CAS 117018 19 6 Ref lsoxaflutole Standard 090 07101 100mg 20 000 98 0 qNMR Tk lt 5 Cyclopropy 4 2 methylsulfony 4 trifluoromethylbenzoyl isoxazole N CH FNO4S 8 359 32 C AS 141112 29 0 OW k aKo
51. 1 2 TEL 06 6203 1788 103 0023 4 1 TEL 03 3270 8243 TEL 092 622 1005 TEL 052 772 0788 TEL 029 858 2278 TEL 011 27 1 0285 TEL 082 285 6381 TEL 0466 29 0351 TEL 022 222 3072 0120 052 099 0120 052 806 esWako Chemicals USA Inc http www wakousa com Head Office Richmond VA Tel 1 804 714 1920 Boston Sales Office MA Tel 1 617 354 6772 esWako Chemicals GmbH Europe Office http www wako chemicals de Tel 49 2131 311 0 DM E mail analyti wako chem co jp URL http www wako chem co jp 15312 4 o1DN NO m Qu
52. 90 E m s 2096 1596 0 3day 0 lday 2 3day 1 2day 96627 O72 72hrEC 7 1 1mg L 187 16 1096 359 1 196 7 OECD T V OECD 1000 1 4 50X10 cells mL 0 eS 28x10 cells mL a 5 3x 10 cells mL 1 se E F 1 1 24 48 hours 1
53. 16 91421 75 9 C HJaNO P 10me 125 200 ASB 00004167 005 Dihydroflavopereirine Chloride 98890 48 3 CH N CI P 5mg 84 700 ASB 00005006 100 F Eburnamonine Vinburnine 4880 88 0 C H N O P 100mg 54 600 ASB 00005395 005 _ ee 5mg 31 400 ASB 00005395 010 Ref Evodiamine 518 17 2 C H N O P 10mg 47 300 ASB 00006066 005 es 5mg 68 600 ASB 00006066 010 Flavopereirine Perchlorate 6 784 38 9 CHigN CIO P 10me 116 200 ASB 00006120 200 Flutamide 13311 84 7 C H F N 0 P 200mg 25 200 ASB 00007065 005 a 5mg 42 800 ASB 00007065 010 Semine NN Va 10mg 71 700 ASB 00007241 025 25mg 30 000 ASB 00007241 100 Ref Glaucine HBr 50722 32 2 C HaNO4 HBr P 100mg 58 800 ASB 00008315 005 5mg 31 400 ASB 00008315 010 Rg Homoharringtonine 26833 87 4 C H NO P 10mg 50 500 ASB 00008315 025 25mg 110 600 ASB 00008331 010 10mg 25 200 ASB 00008331 025 Hordenine Sulfate 622 64 0 C H N 0 H SO04 P 25mg 31 600 ASB 00008331 050 50mg 47 300 ASB 00008350 010 10mg 15 800 ASB 00008350 025 F Hydrastine B AHP Verified 118 08 1 G LNO P 25mg 31 400 ASB 00008350 100 100mg 85 700 ASB 00008875 010 _ a 10mg 15 800 ASB 00008875 050 Yoscyamine JPI Via 50mg 31 400 ASB 00009181 100 a a 100mg 13 900 ASB 00009181 250 Ref Indole 3 Carbinol 700 06 C H NO P 250mg 27 900 ASB 00009100 250 250mg 17 900 ASB 00009100 001 Indomethacin 53 86 1 CoH gCINO
54. 47 300 ASB 00025509 010 10mg 15 800 ASB 00025509 025 Yohimbine HCI 65 19 0 CuH N O HCI P 25mg 31 400 ASB 00025509 100 100mg 45 100 ChromaDex P NMR MS HPLC GC ChromaDex UTN Q amp A rhttp www wako chem co jp siyaku pickup chromato index htm ES 21 a le FL H ANALYTICAL CIRCLE 2015 3 No 76 7 A s 18 64 C H N O 4
55. 4mm 5 0mm 95mm 5 17 600 42mm GC O Y Q amp A rhttp www wako chem co jp siyaku pickup chromato index htm ANALYTICAL CIRCLE 2015 3 No 76 SFC DAICEL DCpak SFC A SFC 2 CO cj SFC
56. MS 2020 LC MS LLC Wakopak Ultra C18 5 3 0mm x 250mm A 0 19 0 5mM B 0 19 Peak No 4 _ B Peak No 2 Peak No 3 0 ee 15 25 90 Peak No 1 0 3mL min ESI MS 5 i 1 371 149 08741 Ref 5mg 90 000 2 355 047 31041 Ref 5mg 90 000 3 HT 2 483 087 09871 F _HT 2 5mg 100 000 4 T 2 484 204 17731 Ref T 2 5mg 45 000 5 317 266 01981 Ref 5mg 50 000 No 1 068 06401 IF 1mL x 5A 40 000
57. P 1g 28 400 ASB 00009165 005 5mg 61 900 ASB 00009165 010 Re Irinotecan HCI 100286 90 6 C H N O HCI P 10mg 110 600 ASB 00009165 025 25mg 237 200 ASB 00009230 010 lsocorydine HCI 13552 72 2 C H NO HCI 10mg 41 900 ASB 00009417 005 _ 5mg 61 900 ASB 00009417 010 IF Isomitraphylline 4963 01 3 C H N 04 10me 93 500 ASB 00010150 001 1mg 28 600 ASB 00010150 005 Jatrorrhizine 3621 38 3 C H NO P 5mg 56 000 ASB 00010150 010 10mg 101 900 yhttbp www siyaku com 2015 3 No 76 ANALYTICAL CIRCLE CAS ASB 00010200 010 _ 10mg 61 900 ASB 00010200 050 Servine T0009 CHssNO som 283 400 ASB 00012073 005 5mg 47 300 ASB 00012073 010 R Lappaconitine 32854 75 4 C H N O P 10mg 61 900 ASB 00012073 050 50mg 251 700 ASB 00012310 010 oO 10mg 31 600 AB n0012310 100 Obelanidine HOI 6112 86 3 CgHNOrHCI P HOOme 9266 ASB 00013644 010
58. Toelstede S et g J Agric Food Chem 57 3138 48 2009 No 077 06391 Ref Glutamy Valy Glycine Standard 100mg 10 000 K M Q amp A rhttp www wako chem co jp siyaku pickup chromato index htm 13 ANALYTICAL CIRCLE 2015 3 No 76 14 I OECD MV WET Whole Effluent Toxicity WET OECD 201 9 8 OECD M RE Vi cf OECD Mad 5 0 2 um Stock Solution I x 100 OECD 201 NH CI 1 500 00 15 0000 158 03315 500mL MgCl 6H O 1 200 00 12 0000 OECD
59. 0 C18 2 5 1 2 1 5 9 SunShell HFC18 30 2 6 1 6 0 5 30 40 E18 2 1 5 9 SunShell C8 30 2 6 1 6 0 5 30 40 C8 1 2 2 5 1 5 9 SunShell C4 30 2 6 1 6 0 5 30 40 C4 0 9 3 1 5 8 Sunniest endcapping 60Mpa 8 570psi 30nm 4 6mm 50MPa P A 3 6 m 0 2 m 20nm 3 4 m 0 2 m 40nm 20nm 2 7 m z SunShell 30nm 2 6 m 5
60. 0486 PD 30 1 303 83841 60331 Rf Pen 100 300 83851 60333 R Pen40 40 381 04921 60336 Re Pen AQUA 100 Q amp A rhttp www wako chem co jp siyaku pickup chromato index htm 9 ANALYTICAL CIRCLE 2015 3 No 76 AFLAKING OCHRAKING HORIBAAcvancedTechno 29 AFLAKING OY 209 409
61. 2910024 eVol 500 ux L 50 26 0 63 0 32 500L 1 10 500 2910384 4 400 511 93751 2910035 eVol 1mL 50 26 0 63 0 32 1mL 1 11000 2910385 4 600 1mL eVol eVoI Classic eVo mm mm mm No 50 25 0 5 0 12 518 82151 036910 5 4 900 51 2 22 0 028 0 17 LC 036912 5 4 900 NE 50 23 0 63 0 11 036914 5 4 900 MG 70 25 0 5 02 036916 5 9 000 70 26 0 47 0 11 036918 5 10 100 115 25 0 5 0 2 036920 2 3 900 50 25 0 5 0 2 038110 5 4 900 eVelA100 gL 115 23 0 63 0 24 038161 5 8 100 180 23 0 63 0 24 038138 2 3 600 _ 50 23 0 63 0 32 039110 5 4 900 MOIG00MM 2 115 23 0 63 0 32 039160 5 11200 eVol 1mL 180 23 0 63 0 32 039138 2 4 500 G TK 6 http www siyaku com 2015 3 No 76 ANALYTICAL CIRCLE GC qp TRAIAN SGE Analytical Science SGE GC
62. 300 ASB 00020340 010 _ 10mg 79 000 ASB 00020340 025 Ref Topotecan HCI 119413 54 6 C H N O0 HCI P a 167 700 ASB 00020340 100 100mg 568 100 ASB 00020353 010 10mg 22 300 ASB 00020353 025 Trigonelline 535 83 1 C H NO P 25mg 36 300 ASB 00020353 050 50mg 61 900 ASB 00020601 050 a 50mg 25 200 ASB 00020601 100 Tyramine HCI 60 19 5 C H NO HOI P 100mg 31 400 ASB 00021220 005 _ 5mg 61 900 ASB 00021220 010 Carne GC 092 CHzeNeC4 Oe 93 500 ASB 00021230 001 _ 1mg 61 900 ASB 00021230 005 Sncarine D OD CaaN2O4 5mg 170 800 ASB 00021225 005 _ 5mg 61 900 ASB 00021225 010 Jncarine E DT Vila on 93 500 ASB 00021235 005 ss Undec 2 ene 8 10 Diynoic a 5mg 73 400 ASB 00021235 010 AcidIsobutylamide USE CeHgNO ON 119 800 ASB 00021250 250 250mg 31 400 ASB 00021250 001 99322 8 CaHANzO2 1g 61 900 ASB 00022326 005 5mg 47 300 ASB 00022326 010 Vasicinone Shh CHieNeO2 0 61 900 ASB 00022518 005 5mg 28 400 Re h ASB 00022518 010 Ref Vinblastine Sulfate 143 67 9 CueH oN4013S P 10mg 50 500 ASB 00022524 100 a 100mg 31 400 ASB 00022524 001 Incamine PII nl 1g 156 800 ASB 00022521 010 F Vincristine Sulfate 2068 78 2 C H N O H SO 10mg 84 700 ASB 00022531 025 25mg 19 000 ASB 00022531 100 Pocetine 0009 ET 100mg 61 900 ASB 00024101 010 J 10mg 31 400 ASB 00024101 025 anthosine 99939 CoHrzN4O6 ome
63. 6cm Xx 25cmL Er Mobile phase CO CH OH CH COOH H O o Mobile phase CO CH OH CH COOH H O li 97 3 v Y 97 3 v Y CH OH CH COOH H O CH OH CH COOH H O a 1000 1 1 v v v 1000 1 1 v v v OH Flow rate 4 0mL min Flow rate 4 0mL min Temperature 40 C Temperature 40C Back pressure 150bar Back pressure 150bar Detection UV 210nm Detection UV 210nm Injection 5u Lleach 200mg L in CH OH 7 Hydroxyflavone Injection 5 L each 330mg L in CH OH O DAICEL DCpak SFC A No mm cm um 383 03901 AA424 4 6 15 5 85 000 E Nh 380 03911 AA425 4 6 25 5 95 000 DAICEL DCpak SFC A AA435 10 25 5 250 000 AA445 20 25 5 520 000 DAICEL DCpak hk mn DAICEL DCpak SFC A O Y 8 http www siyaku com 2015 3 No 76 ANALYTICAL CIRCLE ATP AMP Fi
64. WP 1 Frtentiarl tirmermin 0 100 x 2 1 mm Sunshell C8 30HT 3 4 um 0 2 um SunShell C8 30 2 6 um 0 5 um 80 C 5 min gradient 0 5 0 87 sec 4 Ak W 5s 0 93 sec 2 5 3 Retention time min 150 x 2 1 mm W 8 0 sec 80 C 60 min gradient 3 4 W 6 0 sec Sunshell C8 30HT 3 4 um 0 2 hm SunShell C8 30 2 6 um 0 5 um 25 30 Retention time min Column SunShell HFC18 16 2 6 u m 16nm 150 Xx 4 6mm SunShell C18 WP 2 6 m 16nm 150 x 4 6 mm Mobile phase A 0 196 TFA in Acetonitrile water 10 90 B 0 196 TFA in Acetonitrile Gradient program Fime B 50 Flow rate 1 0mL min Temperature 25 C Detection UV 210nm Sample Tryptic digest of cytochrome C C18 HFC18 C18 C8 C4 C18 5 _ gt _
65. g 71 700 Tm ASB 00001340 005 _ a 5mg 17 100 ASB 00001340 010 Ref Aconitine 302 27 2 C H4NO P 10mg 27 600 ASB 00001491 010 ee 10mg 12 600 ASB 00001491 050 cne ON CHNos 50mg 51 800 ASB 00001657 050 50mg 15 000 ASB 00001657 100 Ammeline Min CaHgNsD 100mg 24 100 ASB 00001691 025 Arecoline Hydrobromide 300 08 3 C H NO HBr 25mg 25 200 ASB 00011012 005 _ 5mg 61 900 ASB 00011012 010 Ref Aristolochic Acid B 475 80 9 Cj H NO 10mg 93 500 ASB 00011074 010 10mg 12 600 ASB 00011074 025 Atropine Sulfate 55 48 CH NO0 SH O0 4 19 000 ASB 00002050 010 Bathophenanthroline 1662 01 7 C 4H N 10mg 26 600 ASB 00002201 010 10mg 12 600 ASB 00002201 025 Berberine Chloride AHP Verified 633 65 8 C H NO CI P 25mg 15 800 ASB 00002201 100 100mg 25 200 ASB 00002259 005 __ _ a 5mg 28 600 ASB_00002259 010 IF Bicuculline 485 49 4 6 JNO P 10mg 45 800 ASB 00003085 010 10mg 19 000 ASB 00003085 025 Ref Camptothecin 7689 03 4 C H N O4 P 25mg 31 600 ASB 00003396 005 5mg 28 400 ASB 00003396 010 Chelerythrine Chloride 3895 92 9 C Hj NO CI P 10mg 47 300 ASB 00003396 025 25mg 110 600 ASB 00003645 001 Cimetidine 51481 61 9 C H N S P 1g 9 500 ASB 00003814 005 5mg 42 800 Re 79_ ASB 00003814 010 Ref Corynoline 18797 79 0 C2 HNO P 10mg 71 700 ASB 00004225 005 _ 5mg 79 000 ASB 00004225 010 IF Deoxyvertaline B
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