X線を用いた無機物の同定
Contents
1. 0 000 L 00 0 0 00 00 0 0 0 6 00 0 00 00 O 000 0 00 00000000 0 0 0 0000000 0 0 0 0 0 0 0 000 00000000 00000000 00000 00 0 0000 0 0 0 00 0 0 0 1 00000 0000 000 00000 0 0 0 000 0 0 0 000 000 00000 00 0 00 00 00 0000 006 000 00 060 0 0060 0 0 0 0 0 0 00000 03 1 0000 00000 00000 0 00000 00000000000 000 0000 00 0 0000 000000000000 000000000000 000000000 00000 000 0000 00000000600 000000000 0000 00060 0 0 0 00 00 0 O O L 000 00 0 0 0 0 0 0006 0 0000 000 0 0 00 0 00 0 0 0 00 00 0 0 00 0 0 0 00 0 0 0 0 00 900 00 0 00000 0000000 000 01996 210 000000000000 00000 0000 987 Introduction X Jenkins Heyden amp 1974 4 and Practice of X 52. 009000 0000 0000000000000 00 00 0000 00 00000 0 00000 12 53 K LAIKA EE 13 0000000000 A 05100 0 0 0000 00 0091 00 0 0 0 00 09000 0 0 0 0 0 0 00 0 00000 0 00000 An 0 1 1 1 0 1 0000 0 0040 000 00 0 0 0 0 00 000 00 6 00 0 00 6 000 000 0 0 00000 0 00 00 0 0 00 00 6 0 000 0 0 0 L 0 00 00 00 0 00 00 000 OO 00000 0000 00 00 0000 4 O O Ogo 00000 000 00 0 0 0 000000 0 O O 00000 L wavelength dispersive X ray spectroscopy 5 ener
3. 0 00 000 0 OOOO 00 00 0 0 0 000 0000 00 0 0 0 0 0000 000 00 0 0 0 00 0 0000 00000 000 000 000 00 00 000000 00 00 00 0 0 00 00 0 00 0000 000 0000 0 00 000 00 0 00 00 0 000000 000 000 0 0 0 0 00 0 0 000 0000000 0 00 00 00 0 0 0 L 0000 00 00 0 0 EE 0 00 0 0 00 000 0 0 0000 00 00 00 0 0 0 000 0 0 06 00 000 0 0 0 00 000 0000 00 00 0 0 0 0 0 0 0 0 00 00 000 0 000 000 000 0000 0 0 00000 0 00 0 00 00 0 0 0 0 6 00000 0 00 0 0 0000 0000 0 00 0 0 038 00 0 00 000 0 0 0 0 0 00 0000 00 0 000 000 0000 000 000 0000 0 00 0 0 000 000 0 8 000 00 0 0 0000 0 0000000 0000 0 0 0300M 0 00 00 0 0000 0 0000 00 0 0 0 00 0 0 0 L 00 00 0 0
4. 00 0000 0 0 0 0 00 000 000 0009000 0 2 O O D 0 EE 1000 00 0 00 0 00 OUD L 0 002 0 00 000 OL 0000 10 np 000 EE 00000 104400 1 0 0000 00000001 0 15 000 0 000 000 00000 00 0 0 0 0 0 0 E e E 000 0 0 000 0 0 0 00 000 00 00 00000000000 00000000 2400 0 000 0000 0 0 0 0 0 0 000 000000000000 30 00 0000 2 0 00 0000000000 00 00 000000 0 0
5. Analysis Eugen P Bertin Plenum Press 1984 50 000 000000 0000 01979
6. 00 0 0 0000 0 000000000000 BO 0 00 0000000 000 0 00 00 00 000 9 0000 0000 00 0 000 000 00000 0 0 00000 0 00 000 000000000 00 0 0 0 0 0 00 0 00000 00000 0 0 0 00 000 00000 00 00 0 0 00000 00 0 0 0 0000 0 0 00 0 0 0 0 00 O 000 0000 0 0 0 00 0 000 0 0 0000 00 0 International Centr for Diffraction OO 000 O 0 OLL Committee Powder Diffraction S
7. 0000010 000 00 0 00 00 00000 0 0 0 0 0000 00000 00000 00 00 00 0 0 0 0000 0000 0 00000 00 0000 000 000 0 00 00 0 00 0000 0 00000 00 0 00 0 0 00 0000 000 0 00 O O 0 0 0 00 O 00 0 00000 60 0 0 0 00 00 OAO 00 0 00 0 0 0 0 01 0 11 000 0 018950 O OOOO W C R ntgen 0 O00 0 0000 Laudi 00 19120 0000060 1901 0 1 0000 0000 0 00000 DO 0000 A L 000 0 00 000 0000 1 00000 00000 00 00 00000 0
8. 000 0 00 0 0 00 0000000000000 00 00 00 00 0 00000 1 0 0 0 00 0 L 0 00000000000 1 2 L 000 00000 00000 0 000 060 0 00 000 000000 0 06000 0 00 0 0000 0 0 00 0 00 00 0 0000 0 00 0 0 0 00 0000 00 0 0 00 0000 0000 0 00 0000 00 0 0 00000 00 0 0 0 0 0 0 0 0000 0 000 000 00 0 0 00000 0 00 000 0 0006 0000 0000000 00000000 20 24500 000 0 410000 090 0000 00 0 000000 00 00 00000 0 0 00 00 00 00000 U 00 0 00 00060 00 00 0 00 0000 0 000 0 0 00 0 00 00 00 000 0 0 0 0 00 0 0 0 0 E 00 0 0 000 00000 0 000 00 0 00 0 0 00 0 0 0 0 000 00 0 000 O O 0000 0 0006 00 00 0 0 00 0 0 0 00 0 000 0000000000 0 0 0 0 0 0 6 00 0 0 0 0 0000 000 0 0 5 1538 000 0 0 0 00 0 000 0 0000 0 0
9. 0 0000 000 0 0 10 0 0000 00 0 000 00000 0 0 0 0 00 0 00 0000 00 0000 0 000000000 0 000 0000000000 0 0O00 L 000000 00 10 0 0000 0 0000 00 0000 00 00 0 0 00 0 0 00 E U EEA C 000 000 00 0 0 00 00060 00 0 000 00 0 0 00 00006 0000 OO O O 000 000 00 00 00 0000 00 0 0 http vww chemt u experiment bunseki 04050243 htni 0 0000 00 00600 000 00 00 0 0000 0 0000000 00 0 000000 000000 0 0 0 000000 000000000000 00 0000 0 0000 0000 0 000 0 000000 00000 00 00 00000000 00 000000000600 00809 0000000000 000 00 00 000000 0000 0000 00000 000 000 000 000 0 0 0 0 0 00 000 00000 0000 00000 0 00 000 00 00 O O OU OO 00 00 0000 0 L 1000 0000 000 0000 00 0 OOO O 0000 L 00 0000 0000 0 00 00 000 000000 0 000 00000 0 5 00 00 0 0 0 000 00 00000 0 0 00 000 00 0 00 00000 0000 0000 00 00 00 O OOOOO 0000 0 000 00000 00 0000 O READYOO O 000 0 0 00 0 0 00 00000 00000 0 0 000 0 0 0000 0 000 00 000 000000
10. 75 2 88 2 63 1 72 25 572 Oxide t Neodymium Zirconium 4 2 3 07 1 88 1 61 17 458 Neptunium 3 47 2 68 4 18 18 871 i 7 Neptunium NpO 3 14 1 92 1 64 269 Neptunium 2 88 2 49 1 51 6 433 ide Neptunium 4 14 3 45 2 12 13 i eds Molybdenum 3 45x 493 3 56 22 415 i Thorium Molybdenum 2 91 1 90 3 57 22 420 Vanadium Np VO 3 70x 5 48 2 61 23 422 Nickel 209 2 41 1 48 22 1189 12 Alphabetical Index Manual 00000 0 0 0 0 0 00 0000 00 0 0 0 0 00 0 00000 00 0 090 0 0 50 00000 0 00000 0000 000 000 0 00000 00 000 0000 00006 0O 0 O O OO OU DOOL O00000 00 OOOD 0 00 L 00 0000 00 00 00 00000 0 6 0000 0000 00000000 0s ULMO 0 0 0 000 0 00 000 000 000 0 0 0000 0 081 0 0
11. 0 00 0 00 000 0000 0 0000 0 0 00 000 00 00 000004010 0008 0 e 0 0 0 0 0 00 000 00 000010 0000 00 6 0 000 0 0 0 0 060 0 0 00000 000 0 0 6 000 00 00 00 000 0 00 0 0 0 00 0 0 0000 0 0 0 005 00000 0 0 0000 00 0 00 0 0 00 0 00 0 000 OOOO 00 0 000 00 00 0 0 01 0 0 0 0 00 00 00 0 0 00 0 000 OOL 000 0 000 0 00 0 0 0 000 000000090 00900000 0100000 0000 0000010000 00 0000 0 0 00 0 0 0 000
12. 00 000 000 00000 0000 000 000000 00 000 000 0 0 00000 0 00 0 0 6 0 0 0 0 0 0 00 0 0 0 000 00 0 0 00 0 0 13 0 0 X0 000 00 0 0 0 0 00 0 000 0 0 0 0 00 00 000 0 0 000 0 0 000 0 0000 0 0 9 000 0 0 0000 00 0 00 0 0 0 0000 00 0 0 00 0000 00000 0 0 00 0 0 000 0 000 0 0 0 0 001 00 0 000 0000001000010 00 00080 0 00 0 0 00 0000 0 0 00000 00 0 00 0000 00 0000 00 0 0 0 0 0 00 0 00 0 00000 000 00 00 0 00 0 0000 00 0 000 0 0 00 60 0000 0 000 200 000 0 0 00 00 05000 0 0 50 0050 00000 0 00 00 00000 005 0 00 000 000 00 0000 0 0000 0 0 0 0 0 0 0 00 0 000 0 00 00 0 0 000 000 000 0
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14. 00 60 0 0 0 0 0 6 0 0000 00 0 00 000 000 0 000 000010 0000000900 0000 0 000 000 OOOO 000 OOOO 0 0000 0 0 00 000 00000 0 0 000 000 000 900000000000 09000 00 000 0 0 000 00 000 00 0000 0 000 006 00 0 00 0 00 0000 00 000 000 00 00 0 00 0 00000 00000 00 00 0 0 00 0 00 0 000 0 000 0 0 0 00000 0 000 0 000 00 0 COO 000 00000 0 0000 0 0 0 0 0 00 000 0 000 0 0 0000 000 00 00 0 0 0 0 0 0 00 00 0 0 000 00000 00 00 0 00 000 0 000 000 00 000 000000000 0 00 0000 0 0 000 0 0 000 0 000 0 00 0000 0 0 0 00 0 0 0 000 0 000 00 0 0 00 6 00000 0 000 0 000 0 0 00 0000000000 000000000 0000 00 0 00 00 000 0 0 0 00 00 0 000 0 00000 0 0 0 0 0 9000000000 000 00 000 0 0 0 0 L 00 0 0 0 00 000 000 0 0000 0 00 0 00 000 00 00 00000 0 0 000 00 0 0 00 0 000 00
15. 000 00 0 000 00 00 00 0 00 00 000 000 e E E N p E e E ed 00 0 0000 0 000 0 0 000 00 00 0 0 0000 0 00 0 00 0000 0 0 0 0 0000 MELFI 000100000 0000000000000000 0000000000000000 0 00000000000000000 0000000000000000 000000000000000 0000000000000000 00000000010 010 Torr 0000000000000000 0000000000000000 0000000000000000 00 000 0 00 00 0 0 00 000 0 00 00000 0 00 0 0 0 00 0000 000 0 00 00 0 00 000 0000 00000 001 0 0 00 00 0 00 00 0000 000 0000 0 00 0000 00 00 000 0000000 09 0000 0 0080000000000 OOO OOO 08 0 000 00 L 0 00 0 0 000 0 0 0000 00000000 0 0 00 00 0 0000 0 0 0 0 0 00 00 0 00 0 00 00 0 0 00 00000 00 00 00 0 000 0 0 000 00 0 00 00 000 0 8 000 00 0000000 0000 0 00 00 0 0000 00 0 0000000000 0 0000 0 000 0000009000 0000 OOO 000 0 00000 00 0 0 0 L 000 0 OOO 000 0 0 0 0 00 0000 0000 0 0 0 0 000 00000 0 00 000 00
16. 0 60 00 0 000 40 00001 0 0000 00000 0 0 0 0 00 eD 11 10 7 000 21 100 00000 000 0 0000 COOCOO 00000000 000000 000000 90000 000 000 009000 00 000 0 00 0 00 00000 0 00 0 0 00 0000 00 00 00 00 0000 00 0 0 0000 0 0 000 000 00 10 00000 00 0 00 000 0 0 0 00 00 DO O 00000 00 00 0 0 00 0 00000 00 0 00 6 000 000 0 6 mi 0000 00 0 0 000 00 0 0 0 00 6 00 0 0 0 000 00 00000 0 0 0 OOOO OOO 00 0 OL EXER 0 0000 00 0 0000 0 5 0 7 09 OOOO 0000 00000000000 0000 0 0 0 0 000 1 00000000 02 0000 000 00 0000000 000 0000 0 00 0000 00 000 000 0 000 L 000
17. 0 E 0000 0 0 00 0 0 0 00 00 00 00 00000 0 0 0000 00000 0 00 0 000 0 00 000 000 00 0000 00 00 0 0 0 0 00 0 0 00 0 2900 0 00 090000000 OOOO 00000 0 00 00000 OL 00 0 0 00 00 0 0 00 00 0000 0 1 0 0 0 0 0 0 0 00 0 00 0 0 0000 00 0000 0 00000 0 000 00000 00 0 0 0 00 0 0 0 0 0000 000 000 000 0 00009000009 0000000 0 0000 0000 00 0 000 0 0 0 0 00 0 0 00 0 000 0 0 00 00 000 0000000 0 0 40 0 00 00 00 00 0 0 00 0 0 000 00 00 0 00 0000 0 00000 0 000 0 00 0 00 000 0 0000 0000 0000000 00 0000 0 0 0 0 0 0 00 00 00 000 00 000 0 00 0 00 00000000000 0000 0 000 0 0 0 00 0 0700 00 00 000 00 0 0 00 0 0 0 00 00 a 3 04 3 00 01 File 303 2631 262 3 71 214 5 24 2 74 1 98 5 30 263 242 22 20 1738 1 314 11 256 3 03 2 63 2 19 217 216 214 1864 15 26 52
18. 000 8 0 00 0 0 00 0 000 0 000 0 0 00 0 00 0 L 00 00 0 000 000 0 0 0 0 0 000 0 0 0 00 00 00 000 0 0 0000 O 0 0 0 00 0 00 0 00 00 0000 0 00 UL O 000000 0 000 00 100000 0 00 0 060 0 00 0 0 00 00 0000 000 000 0 00 0 00000 00000 0000 A000 00 006 Index OOO 0 000 0 0 0 0 0 0 00 00 0 00 00 00 0 0 0 00 0 00 00 0 00000 0 0000 0 0 0 0 0 0 60 0 0 000 0 0 00 000 00000 0 0 0000 000 0 000 000 00 0 000 0 0000 0 00 Index 000 000 0 0 6 Oxide 8 Neodymium 3 13 2 753 e Neodymium Tungsten 3 35 3 28 3 16 23 1268 2 2 are Neodymium Tungsten 3 12 2 73 3 25 24 784 Neodymium Tungsten 3 20 3 14 1 94 22 1180 Oxide Neodymium Tungsten Nd WO 3 21 3 14 1 94 23 1267 4 5 __ Neodymium Uranium 3 17 2 76 3 25 19 830 lt Oxide Neodymium Uranium 00 3 17 2 76 3 25 20 1342 Oxide Neodymium Vanadium NdYO 3 66x 2 73 1 88 15 769 Neodymium Vanadium NdYO 2 75 2 73 1 58 25 i _ Neodymium Vanadium Tungsten NdVWO 2 94 3 02 4 42 26 1279 Neodymium Ytterbium Gallium
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20. 6 2917 3 y 2 4 790 994800 620 Ref Copper M Rouse K Acta Crystallogr 29 514 1973 948500 622 2908100 444 1 988 1 990 55 15 88 0086 20 872500 640 1 4904 Sign 2V Ref Winchell A Winchell H Microscopic Character of Artificial Inorg Solid Sub 15 1964 Color White Peak height intensities Sample from Mallinckrodt Lot analysis showed sample as 99 9 pure Sample recrystallized from 50 50 ethanol water solvent system and heated at 600 for 72 hours 0 07 Si used as internal standards cF8 To replace 4 587 and validated by calculated patterns 26 920 and 26 921 74 55 Volume CD 249 06 Strong lines 3 15 2 23 4 1 82 4 1 41 1 1 57 1 1 28 1 1 05 1 0 99 1 3 63 1 1 90 1 11 100010000 21 00000 0000 00 00000 000 000 0001 000 00 0 0 0 00 0 00 0 0 00 0 L 00000 000000 00000 O O O L OOOO OOO O 0000000000000 O 0 UU GO O e E 000 00 0 S 0
21. gy dispersive X ray spectro 5 1 O OOO O O 0000 0 0 00 00000000000 00000000 000 0 0 000 0 00 000 000000 0 0 0 0 00 250 00 0 000 0 000 000 0 00 0000 00 0 0 00 0 00 00 00 0 0 0 0 000 000 0 000 00 06 0 0 00 0 0 00 0 00 0 00000 e 00000000 00 00 0 00 0 0 0 0 0 0 0 0 00000 000 00000 000 0 0000 000 0 0 0 00 0 0 01 00 00 000 0 0 0 00 0 0 0 0 0 00000 0 000 00 00 0000 0 00005000 0 00 000 0 000 00 00 0 0 0 00 00 0 0 0 000 000 0 0 000 0 0 6 0 0 0 OED 000 000 DU 0 000 EDS 0 06 0 00 00 7250 4380 0 06 0 000 00 0 00000 0000 00 1 00 0 0 0 00 00 000 000 0 00 0 00 000 0 0 000 00 000 00 00 00 00 00 0 0 0 0 00 00 000 0 06 00 0 000 000 000 00 05 0 0000 0 00 0 000 000 0
22. tandards 0000 0 000 00000 00 000 0 00 0 00 000 0 0 0000 O 0 0 0 0 0 000 0 00 0 0 0 000 000 00 00 00 00 0 000 00 00 0 00 000 0 00 00000 00 0 0 0 0 00 0000000 00 0 0 0000000 0 0 00 00 000 0 0 0 0 006 OOOO 0 0 0008 OO 0000 OOOO OO 000 00 000 00 0 Book 9 00000000 000 000 00 00 00007 00 000000 00000 O O 00000 O 000 9 00 00900000000 00 000 0000 0 0 0000 0 000000000 00 00 000 0 000 0 00000 00 0 0 00 0 000 0 00 000000000 00 0 000 0000 0000000000 00 00 0 0 Index 00 000 0000 00000 0 0 Alphabetical Index Manua 00000 00 41 1476 Copyright JCPDS ICDD 1999 PDF 2 Sets 1 49 plus 70 86 Quality x KCI dA int hki 3 63300 111 Potassium Chloride 3 14600 200 2 22510 220 syn 1 89720 311 1 1 54056 Filter Mono d sp Diff TIGN Cutoff 15 0 Int Ref Welton J McCarthy G North Dakota StateUniv Fargo USA ICDD a 2 5 Grant in Aid 1989 4 28390 422 Sys Cubic S G Fm3m 225 8
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