2009 Vol.58 No.6 資料 日本アイソトープ協会 核薬学ワーキンググループ
Contents
1. 2 2 FC C 1 a2. 4 pH pH Whatman Type CF 127 346 RADIOISOTOPES 5 Vol 58 No 6 Whatman Partisil 10 SAX 4 6 mmx 250 mm 10 mmol L 1C 11 8 mL Merck 7 5 mm x HC 9 6 mL 4 PC 1 OOOOOO 2 NC
3. PET 1 1 1 161
4. nC CO2 0 2 0 5 NO eg TC PC CO PC CO ITC CO Shimalite Ni Molecular Sieve PC CO FC NC AgOTf PC PTC nC FC CI PC 3 2
5. 3 1 0 molL LiAIH4 THF THF 0 1 mol L 0 1molL LiAlH4 THF ABX F 151 370 RADIOISOTOPES e C e 1 N N FC FC Vol 58 No 6
6. 2009 4 145 364 RADIOISOTOPES Vol 58 No 6 2 SK603 3 2009 11
7. b PET 3 c
8. b PET 3
9. Desmethyl flumazenil DMF 0 4 mL NaH DMF 0 5 20C PC FC Desmethyl fiumazenil DMF C FC PTC 0 22 um Jun 2009 2009 377 Waste
10. 4 pH pH Whatman Type CF 5 TIonPak AS14 4x250 mm IonPak AG14 4x50 mml 3 5 mmol L NazCOs 1 0 mmol L NaHCO 1 2 mL 18F 3 0 6 TSG 1 15 SHINCARBON A60 80 3 2x3100 mm 900 180 C FTD 180 C Nz 70 kPa 4 1 FE 1 OOO
11. RADIOISOTOPES Do Vol 58 No 6 2 2 nC nC
12. b L 3 a 1 1 10 122 3
13. 5 pH pH Whatman Type CF 6 Finepak SIL C 18S 4 6mmx 150 mm 0 1 molL 250 250 1 2 mL min CH 1 5 7 FID TSG 1 15 SHINCARBON A60 80 3 2x3 100 mm 90C 180 C FTD 180 C 70 kPa 4 1 6 7 4 FC FC 1
14. Jun 2009 2009 333 4 1 0 mol L LiAIH4 THF THF 0 1 mol L 0 1 mol L LiAIH4 THF ABX e NC e 1 1mol L 0 1 molL fh ooo 1 2 e 2 C18 3 QMA
15. 6 1 2 2 FC C 6 2 129 348 7 1 a RADIOISOTOPES Vol 58 No 6 1 b
16. PET 3 b Jun 2009 PET 3
17. BE a 2 ooo ooo a 1 2 et oo0 ooc AA 5 5 ee 5 az ef 5 ooo ooo gt 99 9999 1 2
18. b PET 3 3 a 1 1 10
19. IT 1 1 1 1 ITILT 141 360 RADIOISOTOPES 1 4 3 2009 RADIOISOTOPES 58 221 245 2009 2009 RADIOISOTOPES 58 247 289 2009 7 F
20. 2 V 6 159 378 6 1 6 2 1 360 1080 MBq 6 18 MBq kg 1 5 nmol kg 2 2 1
21. 0 35 E 0 22 gm x 3 2 3 4 4 4 1 7 2 4 3 EO HLO 4 FE LO HO O D n FE E 5 FE
22. SS 2 2 1 340 2 2
23. C LHC AgOTf C nC nC PC PC TC 4 4 1 4 2 4 3 C 338 2 RADIOISOTOPES Vol 58 No 6 Lr HHC
24. 1 a b PET 3 160 Jun 2009 _ 2009 379
25. 2 2 1 50 cm 2 2 50 cm 8 4 5 pH pH pH 6 7 7 1 7 2
26. 0 2 0 5 99 9999 5 1 nC J CO2 OO O OOOO 1 C 1 2 113 332 RADIOISOTOPES d C d 1 C
27. 3 1 1 1 3 3 135 354 RADIOISOTOPES Vol 58 No 6 2 2 1 1 1 CI
28. 1 1 1 3 3 116 Jun 2009 2009 335 2 2 1 1 1 L C l 50cm
29. 7 8 1 L HC 2009 4 2 SK 603 3
30. 1 1 1 3 3 126 Jun 2009 2009 345 2 2 1 1 1 CI 50 cm 1 2 Cl 13 1
31. Cc EF HH 2009 341 1 MS 3 5 C 1 1 CC 2 1 mL 1 CI ooo MBq oo GBq ooo MBq o0 GBq
32. 7 O 1 HHC 2009 4 2 HHC 1C nC
33. 1 360 960 MBq 6 16 MBq kg 30 2 15 30 2 2 1
34. Vol 58 No 6 Shimalite Ni Molecular Sieve Carbosphere CICO Cl Molecular Sieve 4A 60 80 Iodine Cl Porapak N Ascarite AgOTf 1 CI CICO Cl Cl ee ooo 2 3 d 2 NC 1 0 mol L LiAlH THF THE 0 1 mol Cl 1 0 molL LiAIH4 THF BB 50
35. 2009 11 117 336 RADIOISOTOPES 4 Vol 58 No 6 4 pH pH Whatman Type CF 5 20 5 95 ki 0 83 6 CAPCELL PAK C18UG120 4 6 mmX 250 mm 10 mmolL 2 mL min
36. UM Vol 58 No 6 7 1 a 1 b PET 3 HEPA 2 a
37. 3 MILLIPORE Millex GS 4 MILLIPORE Dualex 5 Fm HC 1 153 372 RADIOISOTOPES Vol 58 No 6 2 2 1 1 1 1 19mL1mL 1 2 1 3 2
38. 154 Jun 2009 2009 373 2 2 1 1 1 CI 50cm 1 2 CH 1 3 CH H 1 4 CH 2 2 1
39. 9 6 mL 7 CP WAX 0 32 mmx 25 mm 30 mL min 50 C 220 10 C min 6 5 8 Spelco SUPELCOSIL ABZ Plus 5 gm 4 6 mmx 150 mm 0 1 50 1 1 mL M Z 90 1 MH 4 HTC 1 C 2 EC
40. 1 FC 2009 4 2 SK 603 3 2009 11
41. TC LTC Spelco SUPELCOSIL ABZ Plus 5 gm 4 6 mm x 150 mm 0 12 50 1 1 mL M Z 104 1 M 136 Jun 2009 2009 355 3 SK 603 4
42. 2009 11 5 pH pH Whatman Type CF 6 GL Sciences Inertsil ODS 2 6 mmx 250 mm 0 001 mol L 2 0 05 mol L 11 7 mL Whatman Partisil SCX 10U 4 6 mm 250 mm 0 25 mol L 4 1
43. 3 3 2 2 1 1 1 SFINaF 50cm 1 2 FINaE 1 3 SF NaF 2 2 1
44. R 8 4 HEPA 2 a PET 3 b
45. nC uCO2 OOOOOO OOOO c PC 132 Jun 2009 4 2009 4 ooo 1 2 d nC l d 1 1 0 molL TLiAIH4 THF 9 THE olL LiAl1H4 THF R 0 1 mol L LiAIH THE
46. 147 2 2 1 366 RADIOISOTOPES 2 2 E
47. 1 2D 240 900MBq 4 15MBq kg 5 1 3D 20 2 2 1 RADIOISOTOPES 9 Vol 58 No 6
48. 1 2 L TC H 1 3 L UC H 2 2 1 50cm 2 2 50cm 3 4 H 5 pH pH pH 6 7 7 1 ER EE OR PE I 7 2
49. 3 4 4 3 1 NC 10 NC mL 10 mL 5 FC 10 mL 4 5 3 2 Sep Pak Plus C18 nC 4 6 3 3 LTC PTC 3 4 0 22 um 4 7
50. V 1 V Waste Lr HHC 1 Jun 2009 2009 337 1 nC COz 0 2 0 5 NG g TC TC CO LiAIH4 THE 20C 1 0 1 mol L LiAIH4 THEF nC CO2 NC COz 0 1 mol L LiAlH4 THF nC CO
51. 1 RN ooo gt 99 9999 1 2 3 C18 Waters Sep Pak Plus C18 4 QMA Sep Pak Light Accell QMA Waters 5 CM Sep Pak Plus Accell CM Waters 6 MILLIPORE Milex GS 7 MILLIPORE Dualex 8
52. 148 Jun 2009 3 a 1 1 10 b PET 2009 367 3
53. 6 1 1 2 b nC WCO2 1 0 2 0 5 2 oooc ooo ooo 3 4 0 2 0 5 99 9999 1
54. 2005 123 342 RADIOISOTOPES Vol 58 No 6 2 OOOOOO C 3 1 a LPC CCOz gt 2 0 2 0 5 4 2 02 0 5 99 9999 NH i 1 nC WCO2
55. 130 PET 3 b PET
56. i 7 2 7 3 7 9 1 LC 2009 4 2 nC
57. 50cm 2 2 50cm 8 9 4 NG 5 pH pH pH 6 7 7 1 7 2 7 3 7 4
58. 50cm 2 2 50cm 83 4 3 H 5 pH pH pH 6 7 7 1 7 2 7 3 0 1 SF NaF
59. t 1 2 ooo 2 ooo 8 ooo 1 134 Jun 2009 2009 353 2 2 1 1 8 12 GBq zmol 4 19 21 5 0 8 0 511 keV 7 1 511 keV 1022 keV 7 2 95 7 3 350 nmol mL 1
60. 7 ooo es Ba ooo a 1 ooo 9 oooc ooo ooo ooo gt 99 9999 1 2 Waters Sep Pak Plus Accell Plus QMA 3 MILLIPORE Millex GS Vented 4 MILLIPORE Millex GS 5 2 2 1 1 1 1
61. 50cm 1 2 LC 1 8 CH 1 4 CH 2 2 1 50 cm 2 2 50cm 3 4 5 pH pH pH 6 I 7 7 1 OT
62. OOOOOO OOOO b NC ooo 1 2 c NC c 1 1 mol L CH MgBr THP ooo CH MgBr THF THE ooo 1 mol L H ooo ooo ooo pH ooo 124 Jun 2009
63. kd flumazenil W 3 3 a 1 1 10 c b
64. 0 2 0 5 300 mm 40 JC 5 10 mL pH 0 5 mL 1 JC COz 3 3 1 0 2 0 5 NG eg TC C CO 3 2 TC CO 0 nC CO2 3 3 nC CO2 20 mL min 0 3 0 5 mol L CH MgBr THF 3 4 1molL C 3 5 0 22 um
65. 115 334 RADIOISOTOPES Vol 58 No 6 C sosf 1 2 2 1 4mL 1mL 19 21 5 0 7 5 511 keV 4 NN EMREIN nylmyln NN NN Re 511 keV 1022 keV 95 7 3 2 000 ppm 1 3
66. 128 4 4 1 4 2 OnGuard Ag OnGuard H 20 mL 4 3 Waste 4 4 0 5 mL 5 10mL 4 5 4 6 4 7 0 5 mL 2 mL 0 3 0 5 mol L CH MgBr THF 0 4mL
67. LSE FE RS T 2009 365 SF 0 22 um 5 5 6 6 6 1 6 2 1 150 300 MBq 2 5 5 MBq kg
68. OO OOO 1C 2 FC C 1 0 2 0 5 FC CO oco GBq 0 1 molL LiAIH THF Cl CH 0 4 mL CIH 5 AgOTf 0 8g 1 nC CO2 156 Jun 2009 3 3 3 1 3 2 3 4 0 2 0 5 NG C NC CO2 PC CO 0 1 mol L LiAIH4 THF THF PC
69. 0 1 mol L NaOH Sep Pak Plus C18 NC Sep Pak Plus C18 QMA CM 0 22 um 3 3 4 4 1 Sep Pak Plus C18 70 80 8 4 2 120 Waste Preparation 4 3 4 4 1 3mg 0 1mol L NaOH 0 5 mL 0 2mL
70. 1 2009 RADIOISOTOPES 58 221 245 2009 2009 RADIOISOTOPES 58 247 289 2009 ha 6 CC 2009 RADIOISOTOPES 58 291 442 2009 4 FDG PET 2 17 10 42 2005 16 PET
71. CCOz 0 2 0 5 oooc ooo ooo 0 2 0 5 99 9999 L J 1 150 Jun 2009 _ 2009 369 FC CCO OOOOOO OOO c
72. QI Desmethyl fumazenll 0 5 mg mL 0 2 molL HPLC 1 2 Desmethyl flumazenil 0 5 mg 0 2 mol L 5 uuL DMF 1 mL 1 0 25 mL nC 3 3 1 HFC flumazenil DMF NaH DMF mol L TC HPLC Desmethyl C
73. lmL 5 10 mL 2009 RADIOISOTOPES 58 221 245 2009 2009 RADIOISOTOPES 58 247 289 2009 am pk 2009 RADIOISOTOPES 58 291 442 2009 FDG PET 2 17 10 42 2005 16 PET FDG PET
74. HPLC 0 22 um 3 2 TC Desmethyl flumazenil 0 2 158 0 22 um 4 4 1 TC 2 V Waste 0 1 mL 5 gL 10 mL HPLC
75. PET 3 2 a b CHsMgBr 3 a 1 1 10
76. c 1 1 1 2009 RADIOISOTOPES 58 221 245 2009
77. OO 2 SF sO0 POIH O E 2 5 mL 7 0 35 1 SF 146 Jun 2009 3 3 1 O HzO O G n FE LE PF
78. 0 1 mL 5 gL 10 mL HPLC Desmethyl flumazenil 0 25 mL 0 2 moLL 5 L PTC FC Des methyl flumazenil PC HHC TC 0 22 um 5 4 2 PC
79. CH L 0 1 molL 1 molL QMA C18 QMA CM 1 C 2 3mg 0 1 mol L 0 5 mL 1 0 2 mL 3 3 1 HC 3 2 I
80. 137 356 0 2 0 5 RADIOISOTOPES PTCICO Vol 58 No 6 CICO 0 1 molL LiAlH THE C Cl Ascarite THC cola 1 1g 1 3 3 1 0 2 0 5 NG gw C NC CO2 3 2 nC CO2 0 1 mol L LiAlH4 THF 3 3 THF FC 3 4 PC FC 3 5 PC C 4
81. nC NC nC Des methyl flumazenil N N DMF HC AgOTf IC Desmethyl flumazenil 4 4 1 V 1 2 V Waste FC 1 OO
82. r TC 2 8 PARTTISIL 10 SCX 4 6 mmx250 mm Whatman 50 mmol L 10 1 2 mL min r TC 3 4 7 FID TSG 1 15 SHINCARBON A60 80 3 2x3100mm 90 180 C FTD 180 70kPa 4 1 PC 1 OOO 2 2 1 4N D ga nC nC COz2 Shimalite Ni Molecular Sieve C
83. Finepak SIL C 18S 4 6 mm x 150 mm 0 1 mol L 250 250 1 2mL min UV 254 nm Desmethyl flumazenil 1 2 PC 1 5 155 374 RADIOISOTOPES Vol 58 No 6 3 SK603 4 2009 11
84. 3 Jun 2009 c 2009 349 n 3 1 1
85. C Ne NC nC 3 3 1 0 RR 680 730 C OY nC 2 Rk AgOTf PC NN CIRREE NG ge TC CO NC C 118 AgOTf CA 980
86. Jun 2009 3 1 CE a 1 2 WO H O ooo ooo ooo 2009 Hz O gt 97 lt 0 8mS m 361 0 1 t CH
87. nC 1 2 d C NC FC PC 4 THF 1 0 molL LiAlH4 THF 0 1 mol L EE LiAIH TH FC FC d C HCl i MC LiAlH4 THF TA ANIA ho 3 2
88. 1 b PET 3 140 Jun 2009 2009 359 W 13 HEPA 2 a
89. FDG PET 2005 1 1 C 2 1 mL 1 TC ooo MBq oo GBq ooo MBq oo GBq 1 mL 5 gt 10 mL 2 OOOOOO nC 131 350 RADIOISOTOPES Vol 58 No 6 3 1 a 1 2 OH NCH CH OH 2 ooco ooo ooo 3 99 0 4 5
90. L TC nC RADIOISOTOPES 8 Vol 58 No 6 1 a 1 b PET 3 HEPA 2 a
91. NC looo 1 125 344 RADIOISOTOPES Vol 58 No 6 2 2 1 5 10 mL 2 2 3 150 EU 6 511 keV 1 7 7 1 511 keV 1022 keV 1 7 2 95 1 3
92. 2009 375 4 3 4 4 4 5 4 6 4 8 nC 157 1 2 nC CO2 0 2 0 5 NG ge TC PC CO LiAIH THF 20C 1 0 1 mol L LiAIH4 THF nC CO2 IPC CO 0 1 mol L LiAIH4 THF nC CO2 PC C AgOTf nC nC NC Des methyl flumazenil
93. ooo HPLC 4 HPLC 5 SR 11 2 i 5 1 2 3 MILLIPORE Millex GS 4 MILLIPORE Dualex
94. OOO b OOOO SF see 1 143 362 RADIOISOTOPES Vol 58 No 6 c Us 21 ooo H ooo 5 NT ooo
95. 4 8 THC CO0 nC CO 4 9 TC CO 0 2 0 5 NG ge C FC CO 4 10 nC CO2 LHC CO rNC COz 4 11 PC 4 12 nC C 0 22 um 5 6 5 6 Jun 2009 _ 2009 347 Sr o
96. C L HC 4 12 L TC NC 0 22 gm 5 6 6 1 121 6 7 Jun 2009 2009 339 6 2 1 180 1 800 MBq 3 30 MBq kg 1 1
97. E mL 1 8 105 115 2 2 150 EU 5 0 9 0 1 511 keV 511 keV 1022 keV 7 2 95 2 000 ppm 144 Jun 2009 2009 363 1 3 1 1 1
98. 2 1 2 2 3 4 3 5 5 0 8 0 6 511 keV 1 7 7 1 511 keV 1022 keV 1 95 E 7 4 164 ppm 1 1 7 5 2000 ppm 1 3 1 1 1 3 3
99. oooc CM 0 ooc MM 7 Ss A gt 99 9999 1 2 3 4 5 6 7 C18 Waters Sep Pak Plus C18 CM Sep Pak Plus Accell CM Waters MILLIPORE Millex GS MILLIPORE Dualex nC
100. 2009 RADIOISOTOPES 58 247 289 2009 8 C 1 WiC 2 149 2009 RADIOISOTOPES 58 291 442 2009 4 FDG PET 2 17 10 42 2005 16 PET FDG PET 2005 KI DA 368 RADIOISOTOPES Vol 58 No 6 1 mL 1 CH ooo MBq oo GB
101. C 4 8 PC 4 PTC 4 1 NC 0 22 um 5 4 2 100 gL Sep Pak Plus C18 6 4 3 Sep Pak Plus C18 6 1 Sep Pak Plus C18 CM 6 2 139 358 6 7
102. DMF FC AgOTf EEC Des methyl flumazenil 376 RADIOISOTOPES Vol 58 No 6 2 nC 2 1 NC HC Desmethyl flumazenil DMF 1 mg mL NaH DME 0 2 g mL HPLC 1 PTC 2 Desmethyl flumazenil 1 mg DMF 1 mL 1 0 4 mL 2 2 HTC
103. 4 1 V 1 V 4 2 1 LPC 1 OOOOOO 2 138 1C nC COz Waste 4 3 1 4 4 TC CO 0 2 0 5 NG gw TC NC CO2 4 5 LiAIH4 THF 20C 1 0 1 mol L LiAIH4 THE 4 6 FC CO PC CO 0 1 mol L LiAIH4 THE
104. Sep Pak Plus C18 4 5 QMA 1molLLNaOH 5 mL OH 4 6 CM 4 7 Sep Pak Plus C18 Sep Pak Plus C18 4 8 CM QMA 4 9 4mL 4 10 PC C 4 11 PTC
105. 5 152 gt 99 9999 So BB E Jun 2009 2009 371 e 2 NC C 0 2 mol L ooc ooo ooo HPLC ooo HPLC
106. O1 Vol 58 No 6 2009 RADIOISOTOPES 58 291 442 2009 FDG PET 2 17 10 42 2005 16 PET FDG PET 2005 1 1 SF F NaF 2 1 mL 1 ooMBq ooGBq ooMBq 00GBq 6 8mL 7 2 OOOOOO 142 OO
107. 44 ww 6 eee ooo ooo ooo 5 6 a ooo 6 J LL NE ooo gt 99 9999 1 2 3 MILLIPORE Milex GS 4 MILLIPORE Dualex 5 OnGuard Ag OnGuard H 6 d
108. ooo Fine a nl i gt 99 9999 1 2 e LTC e 1 133 RADIOISOTOPES Vol 58 No 6 e 2 1 2 t 18 a Cy Og
109. Ascarite 20 30 mesh 1 4 1 0 molL LiAIH4 THF THF 0 1 mol L 0 1 mol L LiAIH4 THF 2 3 lt ABX d 2 1 HiAIH THF ooo
110. lt 80 mesh 20 30 mesh gt 99 9999 gt 99 9999 oooc TiAlH4 THE Cl ooo C L C Cd HC H HI LiAlIH4 THF a V _ ooo ooo gt 99 9999 1 2 3 114
111. nC CO 4 7 C 4 8 TC FC C Jun 2009 2009 357 PC HTC H 5 10 mL C18 1 CM 1 1 1C
112. 009 RADIOISOTOPES 58 291 442 2009 FDG PET 2 17 10 42 2005 16 PET FDG PET 2005 OO OO OOOOOO 1 a 112 nC OOOO Jun 2009 2009 L CHzNOS HOC1 o
113. 2009 343 1 2 3 1mol L CHaMgBr THF THF 0 3 0 5 mol L c 2 ooo ooo ooo 1 ooo ooo es
114. RADIOISOTOPES 330 1 1 3 4 3 2009 RADIOISOTOPES 58 221 245 2009 2009 RADIOISOTOPES 58 247 289 2009 4 C 1 Lr Q C 2 1 mL 1 L IC ooo MBq oo GBq ooo MBq oo GBq 1 mL 8 5 mL mn Vol 58 No 6 2
115. ooc ooo ooo 185 191C gt 99 0 1 2 1 b nC uCO2 1 0 2 0 5 ooo ooo ooo
116. q ooo MBq oo GBq 1 mL 8 10 mL 0 01 mL 0 1 mL 2 OOOOOO nC 3 1 a 1 Desmethyl fumazenil C14Hi2FN303 b Cl ooo ooo ooo to 286 289 99 0 1 2 1 Desmethyl flumazenil
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