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1. iPad iPad iPad HI EIDO T2. 80 75 75 2 4 3 NM A CARCELL PAK BCX ME nnn 1 35mmol L NaCIO4 in methanolwater 65 35 70 30 i IEEOORO0 S51 3 1 0 mL min 2 2 0 8 16 24 32 40 mmn IO AL benzalkonium chloride homologous CAPCELL PAK SCX 2 CAPCELL PAK SCX 500 0 8 A 3 ee mm500 _
3. HA BA ARCE RAK SN b the typical chemical bonded SCX Nucleosil 5SA ES RE I i NE TY 0 8 16 min 0 8 16 min 200mmolL NH4HsPO4 pH3 0 adjusted with HsPO4 1 0 ml min 40 UV 254 nm 10 L T uracil peak 1 2 thymine peak 2 3 guanine peak 3 4 cytosine peak 4 5 adenine peak 5 CAPCELL PAK SCX 3 NMR SMMS 2 CAPCELL PAK SCX Si H gt 1 250 mm x 4 6 mm 1 D 8200mmol LNHaHsPO4 pH3 50 adjusted with HsPO4 1 0 mL min 22406
4. 38 BMS BMS 01 1 MS 8011 7 10 18 NASCAJ Nucleonavi 4 BMAS201 1 8011 8 31 9 LC MS LC MS 59 2011 9 13 9 15 INASCA 6 S 6 1
5. MSDS MSDS O HPLC 1 HPLC
6. UV 254 nm a T uracil peak 1 thymine peak 2 G guanine peak 3 4 cytosine peak 4 5 adenine Deak 5 ODS CAPCELL PAK SCX 8 CAPCELL PAK SCX QjlMl PNG HPLC CAPCELLPAK C1g MGIII lt CAPCELL PAK Cs MGIll HS3 ICAPCELL PAK Cg IF lt CAPCELL PAK Ca IF2 gt
7. 6 1 S S S S GOmm 5S G00 1 S LC cafe No 18 CAPCELL PAK SCX
8. H4 MW 240 CAPCELL PAK SCX p 96 1 ot IM Cis Ci4 Cie 1 R C12Has Oi
9. HPLC 1 2011 No 18 CONTENTS CAPCELL PAK SCX FE S NN 9 54 BI ee Sa de a a hb a pe sr bu a CAPcELL PAK SCX CAPCELL PAK SCX CAPCELL PAK SCX CAPCELL PAK 010 1 1 LC cafe CAPCELL PAK SCX CAPCELL PAK SCX
10. A 2 2 um e IF2 2 2 um e E 1 8 um 1 8 um 2 0 2 1 mm i d X 50 mm CHsCN Ha0 60 40 40 1 mm AU UV 254 nm E 1 8 um 1 0 gL 4 C 2 um 0 4 D 2 um A A e BK6 m 200 400 OO 800 1000 1200 0 100 00 300 400 500 600 700 gL min 50 2 1 mm i d x 50 mm He0 CHaCN 50 50 7OMPa 40C 40 2 UV 254 nm 1 0 L 30 MPa 20 oO mm 10 Ree 0 200 400 800 800 1000 1200 CuL min MGIll MGIlI H Ci8AQ Atlantis TSK 80TsQA Hydrospherer Xterra MS Cig 0 5 0 45 YMC Triart De ee F MC MG TSK ODS100Z Inertsil ODS 3V 0 L column YMC Pro C1 XBridge CeS6120 i 8 0 4 Ci8gAG1 200 Zorbax Extend CisACR CsUG80 Cadenza Unison US C1g Symmetry C1g ka
11. CAPCELL PAK Ca MGII HS3 2c10 0 0 Pa W 50MPg 120 100 MGIII H 80 60 MGIII 40 20 N 0 mm i d x 50 m Hze0 CHaCN 08 50MPa 40 C 8 5 nm Da 500 MG 50MPa e MGII H 82 7 um e A 2 2 um 2 2 um e E 1 8 um 1 8 um 2 0 2 1 mm id X 50 mm CHaCN He0 60 40 e 9 e e e oe UV m ee ee a e 1 0 9 e 5 3 Se 200 400 00 800 1000 1800 uL min 200 400 600 800 1000 1200 L min 155 100MPa 1 OOMPa e MGIH 87 um e
12. R C1 S Co IF2 L coumz 9 SUPERIOREX 35 CAPCELL PAK Cie IF2 S22 mm mm 9 889 1 0 8 000 CAPCELL PAK Ca MGIII H S3 mm mm 92782 0 0 77 000 92885 2 1 80 000 92784 50 78 000 82 000 927886 2 0 100 79 000 TCAPCELL PAK Cie MGIII H S3 TCAPCELL PAK Cg IF2 a EJ lt 4 hh 2 Me gs 4 So z a a HPLC HPDLC 8 SeN gt vg 01 1 6 8 1
13. r105 0081 1 1 16 FS TEL 03 6253 1412 FAX 03 6253 1416 Tr601 80937 12 TEL 075 671 0301 FAX 075 671 0302 http www shiseido co jp HPLC NO 18 5000 2011 7
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