IRsolution 用 バリデーションソフトウェア 取扱説明書
Contents
1. 1 2 3 42. A4 A4 26 5 Fi 6 1 FTIR 15 E
3. Microsoft MS DOS Windows Microsoft Corporation 2002 2007 Shimadzu Corporation All rights reserved FTIR 1 2 3
4. IRsolution c Program Files Shimadzu IRsolution IRsolution 1 IRsolution 2 3 ValidASTM ptm lt OK gt ValidASTM ptm 4 Rsoution En sl
5. 0 5 lt PASS gt 15 3000 1000cm 3000cm Scm a 1cm 4 0 5 3 3 30 2 3000 1000cm 5 0 Verification of the wave number scale
6. 3 1 2 19 3 1 2 ON Windows 3 1 3 IRsolution IRsolution 1 1 2 IRsolutio
7. ASTM Lv0 ASTM E1421 94 Level Zero Ver 1 10 ASTM Lv0 V1 10 ASTM E1421 94 Level Zero Ver 1 10 Vahdation JP EP TIRsolution 1 30 JP EP JP JP TRsolution 1 40 JP EP EP IRsolution 1 40 EP
8. 3 1 2 4 1 2 ON Windows 15 4 1 3 IRsolution IRsolution 1 IRsolution
9. 5 2 6 1 2 7 1 2
10. 13 14 Correctness of the resolution and wavenumber by polystyrene film Test2 Earrectness of the resolution and wavenumber bu polystyrene film 14 lt OK gt E 2 IRsalutinn Basic 15
11. 2 JP JP ASTM 4 1 4 1 1 FTIR ON IRsolution FTIR
12. 20 5 37 PASS IRsalutinn Basic Overall Judgement PASS 37 1 38 FAIL IRsalutinn Basic Overall Judgement FAIL 38 lt OK gt 4 6 ASTM 29 Selection lt Load gt
13. 4 4 27 Measurel 32 mstrument Serial No Temperature Sample name Relative Humidity Inspected by 18 Parameter Setting Instrument lp Prestige Serial No 2345B Temperalure I25 Sample name Foystyene Rielative Humidity Ro Inspected by E himadzu Cancel 32 lt OK gt 33 Remove Sample from Sample Chamber
14. 4 3 12
15. 4 2 IRsolution ASTM E1421 94 Level Zero Validation Select Languagg Language Enalish bd 27 16 Language lt gt English Japanese lt OK gt
16. ASTM VahdASTM ptm IRsolutton Data ASTM JP ValidJP ptm IRsolution Data JP EP ValidEP ptm IRsolution Data EP IRsolution 4 3 MD AIM 52 77 1 7 B EE top 0 5 6 gt ASTM LevelD Validatio JP Validation EF Validation EasyScan ReportWiewer 3
17. 0207200151 smf 10 1 12 Open Power Snectrum _ a zee 0 0207200151 SMF lt 0207200215_ 1 SMF D207200215_2 SMF I EE CD GetFiePahesmD lt 22 23 Correctness of the resolution and wavenumber by polystyrene film 23
18. lt OK gt LahCnntral Macra Llaneglaees Remaye Sample from Sample Chamber 33 2 34 Set Polystyrene Film into Sample Chamber lt OK gt IRsalutinn Basic 34
19. o Parameter Setting Instrument lfPresigg Serial No 123456 Temperature 25 Sampl name Faystyrene Fielative Humidity 30 Inspected by Shimadzd cea 11 lt OK gt 12 Form of a power spectrum TesH1 Farm of a power speclrum 12 lt OK gt Remove Sample from Sample Chamber 13 lt OK gt
20. 2 lt PASS gt E 5 0 Absorption Spectrophotometry Infrared Control of resolution performance scale 5 Verification of the wave number EP4 0 2 3 3 m3 1 FTIR 8300 8400 8400S IRPrestige 21 IRAffinity 1
21. 0 5 3 lt PASS gt 4 15 28 H lt PASS gt 3000 1000cm 3000cm Scm WM 1cm 3000 1000cm 2 2 2
22. IRsolution IRsolution Basic Warning 2 The Spectrum window currently npened if a program is started is closed Cantinue 1 lk 28 lt OK gt Selection x Select method 1 Measuremert Settings Cancel 29 Selection 29 Load 4 6 MASUR Settings Reference ao
23. 1 Farm of a nawer spectrum PASS 2 Correctness of the resolution and wayenumber by nalsturehe film PASS 18 19 FAIL E 1 1 Form of a power spectrum FAIL Correctness of the resolution and wayenumber by polystyrene film FAIL 19 lt OK gt ns 3 6 JP EP 8 Selecttion lt Load gt Selection Select method 1 Measuremert Settings Cancel 8 Loadd
24. 2 10 2 3 3 5 Open Power Spectrum zo02 020720151 SMF 0207200215_1 SMF D207200215_2 SMF EztFisPFahesD S swt 24 13 3 7 SHIMADZU ITRPrestige IRAffinity FTIR 8000 Series Validation Report FTIR 8400S 25C NIST 25 T 3 Shimadzu 2002 10 29 11 20 _ 1 4600 0 28 1 12 14 4000 0 60 6 30 35 3000 0 91 2 60 71 at Maximum 121 4 50 00
25. 15 2 15 2 15 2 R UE E 8 100 E ASTM ASTM Level Zero
26. 3 3 2 IRsolution JP Validation EP Validation IIRPrestigeIRAffinity FTIR 8400S FTIR 8000 JI EFTIR 88200PC 8600PCJ FTIR 8000 351cm Select Imstrument Type 1 x linstrument IRPrestige IRAf lt 5 4 1 FTIR 8300 8400 8400S IRPrestige 21 IRAffinity 1 5 0
27. Instrument Serial No Temperature Sample name Relative Humidity tnspected by q Faramieter Setting Instrument fPresigg Serial No 123456 Temperalure Il25 Sample name Pasrene Rielative Humidit ln Inspected by 5 himadzu el 38 lt OK gt 39 2 lt gt 10 1 1 2 2
28. Spectrum1l Reference1 Spectrum1 Referencel 100 100 10 Spectrum1 Referencel 4000cm 400072000 5 gt RN 0 3 2000cm 2000cm 200071000 gt gt 0 3 1000cm _ 150cm non physical ey 100 4000cm 30 2000 cm 30 1000 cm 30 500 cm 30 si3HSs 8 2 One Hundred Percent Line Test 100 One Hundred Percent Line Test 100 T Spectrum2 Spectrum1 Spectrum1 Spectrum2 100 Spectrum2 Spectrum1
29. 2870cm 2830cm 18 1589cm 1583cm 12 lt PASS gt T 6 4 3060 0 1 5 em 2849 S 1 5 em 1942 9 1 5 em 1601 2 1 0 ecm 1S83 0 1 0 cm 11S4 S 1 0 cm 1028 3 1 0 cm i 3 6 5 1
30. 3 JP EP JP EP 15 5 0 FTIR NIST P N 206 70123 91 92 FTIR 2 1
31. NIST 2 FTIR 8300 8400 8400S IRPrestige 21 IRAffinity 1 5 0 FTIR 8000 15 3 2 2 1 IRsolution IRsolution 2 1 1
32. FTIR 8000 15 Instrument lt gt lt OK gt Select Language Language Enalsh lt 6 Languagel lt gt English Japanese
33. 2cm_ 45 2 8 low mm sec HAPP GENZEL Auto Files Shimadzu IRsolution Data JP FT P Validation EP Validation c WProgram Set Polystyrene Film into Sample Chamber gt lt OK gt c Program Files Shimadzu IRsolution Data EP Windows
34. 1 2 c Program Files Shimadzu IRsolution Data ASTM 0207180743 1 2 NIST c Program Files Shimadzu IRsolution Data ASTM REF Rl smf 1 R2 smf 2 R3 smf
35. lt PASS gt 0 5 5 10 25 50 0 0 10 2 1 400cm 403cm 2 331cm 6 2 F 6 3 1 FTIR 8000 15 0 01
36. 29 7 3 1 3060 0 1 0 cm 2849 5 1 0 cm 1942 9 1 0 cm 1601 2 1 0 ecm 1S83 0 1 0 em 11S4 S 1 0 em 1028 3 1 0 em lt PASS gt 7 4 5 0 3 lt PASS gt 7 5 5 0
37. 2D Graphic Preferences General 5 Character Format Size 10 6 Style 7 Show peak borders Peaklabel on top of peak 2D Granhic Freferences General Coloring Style Advanced WU r Data Style Style ntions ctive spectrum pen width g 1 3 a I Line at 2000 1 cm Fil peaks lp IY Show peak barders Ta dq 6 IY Peaklabel on top of peak Set default yalues sbr 26 8 lt OK gt 2 2 3
38. _ SHIMADZU IR Prestige ASTM Level 0 Rieport Instrument Dverall Judgement FAIL Serial No Temperature Sample name Relative Humidity Inspected by Date Time 2002 05 09 16 27 27 Approved by Date 1 45STM Level Test Enerq Spectrum Test ltem Today Prev Error Standard Judqe E 4000 E 2000 037 037 HOO DOS5 PASS E 2000 E 1OOH 1 75 1 76 OO OOS PASS E 150 E mas OO O00 O00 O05 PASS En rror Standard Judge 4000 93 62 E 38 5 OO FAIL 2000 9363 637 200 FAL 1000 9363 637 200 FAL 500 365 535 500 FAL Ignore following bands due to water vapor Peaks at 2200 1300cm 1 4000 3300cm 1 and CH2 Peaks at 2400 2250cm 1 05409 15 27 05 09 16 11 05 03 16 21 05 09 16 22 2A5TM Level Test 100 T Line PHP Noise Valuse N PPI T Standard Judae 4000 32 1 00 PASS 2000 O20 O10 FAL 1000 0 32 1 00 PASS 500 33 18 8 00 FAIL RMS Noise Valuse WN RMS T Standard Judge 4000 O07 030 PASS 2000 O03 O05 PASS 1000 008 030 PASS 500 545 200 FAL Average of SHS0o8 rage 2000 99 78 1000 33 32 42 2 5 2 42
39. mstrument Serial No Temperature Sample name Relative Humidity inspected by Parameter Setting x Instrument fPresigg Serial No ki23456 Temperature Il25 Sample name Pasbrene Helatiye Humidity ln Inspected by E himadzu Cancel 20 ml lt OK gt 21 Form of a power spectrum 21 lt OK gt OK 22
40. Abort Cancel E lt Abort gt lt Stop gt x Stopped measurement in macro Stop macro too LA 17 gt lt No gt lt Yes gt 3 5 5 18 PASS
41. kk 2 kk 2 JP EP 5 60 Ua 5 a a 7 5 i 5 IRsoluti6m SS 5 NN 6 7 8 SEe220 8 WM NIESNRSSRRNNRURNRIDMSOedEDRROGMA0RSSEROIR 11 JP EP kk 12 14 ASTM i 15 0 15 15 Rn Ni 15 IRsolution kk 16 A 16 NS NN 17 2 18 Rk 1 lt 20 ASTM i 21 22MBeR3 23 24 ASTM kk 24 ii 24 kk 25 EAI 25 NSP0223200S238 889430888833883380883 8883 26 27
42. uriy 19429 19434 05 15 Search 1601 2 1601 0 02 10 1 a 15830 15827 08 10 NE 11545 1154 4 01 10 KYO Attributes 1028 3 10281 02 10 4 No1 No 2 0 0 50 Administrator Nu GLP 1 5 RTF File Options Text File Print tx lt OK gt 0 EpJp Print txt OK NJ 2 Report txt 6 print txt
43. 0207180743 1 IRsolution 1 30 c Program Files Shimadzu IRsolution Data EPJP Stop Scanning Scanned 14 of j5 16 10 lt STOP gt Stop
44. 4 1 IRsolution IRsolution 2 1 2 1 1 2 1 2 3 1 3 1 1 3 1 2 3 1 3 3 3 3 4 3 6 3 7 4 1 4 1 1 4 1 2 4 1 3 4 2 4 4 4 5 4 7 4 8 4 8 1 4 8 2 2 B AA 1 RN EEE 2 kk 2
45. IRsolution OEMMacros lcm c Program Files Shimadzu IRsolution ValidASTM ptm ASTM ce Program Files Shimadzu IRsolution PrintTemplates ValhdEPJP ptm JP EP c Program Hiles Shimadzu IRsolution PrintTemplates ValidJP ptm JP c Program Files Shimadzu 1Rsolution PrimntTemplates ValidEP ptm EP c Program Hiles Shimadzu IRsolution PrintTemplates 2 1 2
46. 5 0 FTIR 8000 13 7 1 FTIR lt PASS gt IRPrestige 21 IRAffinity 1 FTIR 8300 8400 FTIR 8400S 10 25
47. 27 RS 27 27 NNN 28 kk 28 7 1 A 29 7 2 DA POR ROO NOOR OT RTT TOTP I OP OR RAPT OD OPP RMIT PO 29 7 3 Na 30 7 4 a NS 30 7 5 SS SNE EEEl kk 30 ASTM 31 8 1 Energy spectrum test 31 8 2 One Hundred Percent Line Test 100 i 32 8 3 Polystyrene Test 32 1 IRPrestige 21 IRAffinity 1 FTIR 8000 FTIR IRsolution 2 13 QP15 5 0 EPS 0 Absorption Spectrophotometry Infrared Control of resolution performance Verification of t
48. 4 3 os E 29 Settings 30 17 Selection x Select i ChangeBean Helference Cancel 30 lt Language gt 27 lt OK gt lt Change Beam gt 31 Select Change Beam hanqe
49. 50 50 0 10 2 0 3 0 01 1 400cm 403cm 10 30 60 60 0 10 2 0 3 2 331cm FTIR 8000 7 2 0 04mm 2870cmr 2851cm 0 33 1589cm 1583cm 0 08
50. ASTM ASTM E1421 94 Level Zero E o Referencel Reference2 Spectrum1 1 Spectrum2 Spectrum1 2 Spectrum3 Spectruml BKG 8 1 Energy spectrum test Energy Spectrum Test
51. 1 2 1 2 1 3 1 2 3
52. 10 60 0 10 2 0 5 IRPrestige 21 IRAffinity 1 FTIR 8000 FTIR 8200PC 8600PC FTIR 8400S 30 60 3 14 30 40 40 8 3 0 4 27 1 cm 0 04mm
53. 2002 10 29 08 47 50 2002 10 28 08 42 41 Shimadzu 4 8 4 8 1 ASTM JP JP ASTM 4 8 2 4 7 40 4 3 lt Reference gt 2 100 T 3
54. lt OK gt IRsolution LabControl Macro Languagg x Warning 3 5 2 The Spectrum windaw currently opened if a nrogram is started is closed Cantinue 7 lt gt 8 Select melhad 1 Measuemert Settings Can
55. 2 8 low mmsec 19 c Program Files Shimadzu IRsolution Data ASTM 0207180743_1 Windows lt STOP gt Le Stop Scanning Scanne
56. NIST 2 FTIR 8300 8400 8400S IRPrestige 21 IRAffinity 1 5 0 FTIR 8000 15 3 3 1 3 1 1 FTIR ON IRsolution FTIR P N 206 70123 91 92
57. 100 10 100 4000 2000 1000 500cm 100cm RMS P P 100 P P 4000cm 1 00 2000 cm 0 10 1000 cm 1 00 500 cm 8 00 100 RMS 4000cm 2000 cm 1000 cm 500 cm 4 00 8 3 Polystyrene Test Spectrum3 Reference2 Spectrum3 Reference3 Spectrum3 Reference2 100 10 2 4000cm 10 2000 cm 10 1000 cm 10 500 cm 10 ASTM E1421 94 7 3 1 1 T 1
58. 100 T 4 100 T 24 ASTM EP JP A ON DS DI 5 1 IRsolution Report Viewer 7T Control hlacro Language Report file not exist 41
59. 3 lx 0207200151 SMF 0207200215_1 SMF 0207200215_ 2 SMF OO lt Get File Patht smf 39 4 5 22 4 7 206 94979 SHIMADZU IRPrestige IRAffinity FTIR 8000 Series ASTM Level 0 Report 1 Test Energy Spectrum Test FTIR 84008 Shimadzu 25 NIST 25 G S 2002 10 28 14 43 56 E 4000 E 2000 0 49 0 49 E 2000 E 1000 1 98 1 98 E 150 E max 0 00 0 00 1 ASTM Level 0 0 25 5 00 2000 100 05 0 05 2 00 1000 100 00 0 00 2 00 500 99 98 0 02 5 00 4 Peaks at 2200 1300cm 1 4000 3300cm 1 Peaks at 2400 2250cm 1 4000 100 25 ASTM Level 0 PP PP T 4000
60. AIM 2 0 X 1 2G G 2nC 5 3 W 2 po gt TE 8 x 6 Object Position p 1 4600 0 1060 595 40000 2057 1486 3000 0 35 71 2973 at Maximum 5946 50 00 7000 1224 595 CPPWhFMRY9 5000 274 119 LID Rt if 4030 041 0380 Data Source Active Tab Index Macro Data Source SNGSRNea TNI J Macro Index 2870 0 28702 35 12 2850 0 28499 8 82 y 0 Width 1850 2550 RTF File Options Text File Object by Index 1 3 lt A 2 a BE PO YY Peak depth T 26 30 18 00 1589 0 1588 4 51 51 0682 15830 15827 31 98 IRsolution 9 Template Measure o o x View Manipulation 3060 0 3060 2 0 2 1 5 Thickness 2849 5 28499 04 15
61. 700 0 24 7 12 14 500 0 8 7 2 43 403 0 2 1 0 2870 0 2868 9 34 4 2851 0 2848 7 9 4 Peak depth T 1589 0 1583 0 Peak depth 3060 0 3058 9 3058 9 0 5 0 1601 4 1600 8 1600 8 1028 3 1028 0 1028 0 3060 0 M 0 5 1601 4 4 N 0 5 1028 3 12 8 6 0 5 3s00 Power Spectrum Polystyrene Spectrum 25 H 14 ASTM ASTM E1421 94 Level Zero FTIR NIST
62. Beam Un using lt 31 FTIR P N 206 70123 91 92 Use lt OK gt Un using lt OK gt lt Reference gt
63. 0 10 T Fs 2002 7 B JPEP2000 2002 10 D ASTM 2003 03 E 4 8 2004 02 F IVDD 2004 03 22 G ASTM 2005 10 25 H FTIR 8200PC 8600PC 2005 11 18 J EP5 0 I a 14 1 FTIR 8300 8400 2007 08 20 L IRAffinity 1 93
64. 0 04 1 00 2000 0 03 0 10 1000 0 03 1 00 500 0 40 8 00 RMS RMS T 4000 0 01 0 30 2000 0 00 0 05 1000 0 01 0 30 500 0 08 2 00 4000 2000 1000 T 100 11 100 00 99 95 500 99 66 ASTM Level 0 4000 0 09 2000 0 1000 0 500 0 07 5 00 03 2 00 01 2 00 75 00 at 3050 2850cm 1 1550 1400cm 1 800 650cm 1 600 500cm 1 2 Test 100 Line Test Hile Name No of Scans Resolution Apodization Apodization 1029084545_1 Date Timei 1029084655_2 20 User 20 4 lem 4 lem HapprGenzel HapprGenzel 2002 10 29 08 45 45 2002 10 29 08 46 55 Shimadzu 40 H 2 File Name No of Scans Resolution Apodization Apodization 1029084555_1 Date Time 1028084040_1 20 User 20 4 h cml 4 h cml Happ Genzel Happ Genzel 3 Polustyrene Test 2002 10 29 08 45 55 2002 10 28 08 40 40 Shimadzu File Name No of Scans Resolution Apodization Apodization 1029084750_3 Date Time 1028084241_3 20 User 20 4 h cml 4 h cml Happ Genzel Happ Genzel
65. 206 94978L Nov 2007 IRsolution No Text
66. OK gt 3 4 8 Measure 11 mstument Serial No Temperature Sample name Relative Humidity Inspected by
67. cel 8 Selection Load 3 5 MKSA Settings Caneel 3 3 IRPrestige IRAffinity 1 FTIR 8400S FTIR 8000 8 lt Settings gt 9 Selectian Select 9 lt Instr
68. d 14 of 45 35 StOD Abort Cancel lt Stop gt lt Abort gt IRsolution Stopped measurement in macro Stop macro too 7 36 lt Yes gt lt No gt 4 5
69. he wave number scale ASTM American Society for Testing and Materials E1421 94 Level Zero FTIR NIST IRsolution all Ge 1
70. n 3 4 2D Graphic Preferences General Character Format Size 10 6 Style 7 Show peak borders Peaklabel on top of peak 2D Graphic Preferences JP General Coloring Style adyanced Dala Stle Shule plions Active spectrum pen width k 4 a ho Line at 2000 1 cm peaks a IY Show peak borders pa Feaklabel an top of peak Set default yalues sy 4 8 lt OK gt 2 1 2
71. ument gt 5 lt OK gt lt Language gt 6 lt OK gt lt Change Beam gt Select Change Beam x Change Beam Un using lt 10 FTIR P N 206 70123 91 92 Use lt OK gt Un using lt
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