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FZP 5G2s User's Manual - John Morris Scientific

1. Detection V5 3 Cd 47 3 C Co 53 5 C Do 50 8 C 1 1 50907 Signal de d tection Signal d opacit Do y Freezing Pt 10 10 30 50 50 40 30 Zo 10 o X XE HRecfiocid Chauffage Diagram 5 Result curve of a contaminated sample DOCV226A01 1 C FZP 5G2s User s Manual Page 3 39 on DL Information printed with the result curve In the top left eThe analyzer type its serial number the N of the software version installed the date of the current day eThe date at which the test has been performed the hour of the test end and the name of the operator eThe product name and the sample identifying name In the top right eThe result message Freezing point temperature at which the crystals disappear in the sample elf this result is rounded at 0 5 C F the indication Rounded appears under the result parameter of the product refer to the section 5 1 page 3 44 In the middle right eThe value of parameters Cd Co and Do eThe indication 1 1 Number of cooling cycle performed N of the cycle having allowed to detect the Freezing point up to 2 cycles 3 2 Result printing The FZP 5G2s can print results in different ways with or without details values with or without product parameters in ticket or in curve form The data printed depend on the analyzer setup and as required the results of the last test or of any tes
2. Displays Meaning of different menus Field values Power on parameters menu of the Setup menu Going from left to right and from top to bottom Run parameters Permanent field Default Product choice of the product profile 1240 1 By default selected by default to carry out a test when device is switched on applied to a product type Run parameters Default Product Run menu display Press the Default Product key this calls up the product list Select the product profile desired then press the OK key to validate Table 5 Run parameters menu displays 7 3 Configuring alarms the Alarm menu The Alarms menu allows thresholds of different alarms triggered in case of failure to be configured This menu also allows alarm buzzer modulation to be setup Activation of this menu calls up the following displays Displays Meaning of different menus Field values Alarms menu ofthe Setup menu Going from left to right and from top to bottom Buzzer permanent field Alarms setup Modulation to adjust the intermittence of discontinuous O gt 100 Buzzer Abn 30 OFF Test to test the buzzer ON OFF L Test Alarms menu display 1 Press the Modulation button to enter the new value 100 continuous alarm 0 alarm mute Use the Test button to test the buzzer after modifying its modulation DOCV226A011 C FZP 5G2s User s Manual Page 3 51 iSL Sample temperature
3. Diagram 11 The Quality menu The FZP 5G2s measurement instrumentation sometimes requires calibration How often depends on the user but it is recommended that all the measurement instruments be adjusted at least once a year The Quality menu has a series of menus dealing with the following adjustments these are grouped in the display below Quality Cd EUR Calib ticket L3 Table Calib Printino Figure 23 Quality menu display amp The Correct Table menu sample temperature measurement probe correction table V The Samp T Calib menu calibration of sample temperature measurement probe Adjustments carried out in this way can be printed out using the Calib ticket Printing menu 2 1 Sample probe correction table the Correct Table menu The Correct Table menu makes it possible to enter a correction table for the sample temperature measurement probe The sample temperature displayed takes this table into account during tests only On activating the Correct Table menu the following display appears Va Sample probe correction table Correction Probe value reference B mmm Unit Figure 24 Correct Table menu Display 1 This display allows the name of the correction table to be entered and the table s unit of temperature to be selected DOCV226A011 C FZP 5G2s User s Manual Page 4 61 On a series of displays similar to the display below the correction values can be entered correction value value
4. Instrumentation Scientifique de Laboratoire FZP 5G2s ee ena LEE User s Manual Instrumentation Scientifique de Laboratoire BP 70285 14653 CARPIQUET CEDEX FRANCE Phone 33 2 31 26 43 00 Fax 33 2 31 26 62 93 Web site http www isl france com Page 2 FZP 5G2s User s Manual DOCV226A011 C Historical Review Revision Modification descriptive index Pp origina issue 815 03 Part 1 4 3 3 1 ISL Alan manager software available on the FZP 5G2s analyzers Part 1 2 4 Cleaning recommendations of the detection cell 01 26 04 Part 2 2 3 3 Update of the end of test messages Appendix B Detailed characteristics of the RS 232C link communication protocol Part 1 8 2 1 Updating and adding of the eec methods ASTM D7153 and ED UR 18 Adding of an advertising on Class IIIA laser detection cell hazards 09 21109 Part 2 2 1 Modification of explanations concerning the Other menu DOCV226A011 C FZP 5G2s User s Manual Page 3 ou DL ISL c copyright The FZP 5G2s Analyzer and this manual are protected by copyright Reproduction of the unit will result in prosecution All rights to the manual are reserved Reproduction in any form including in the form of excerpts shall require written permission from the copyright holder ISL FZP 5G2s Software c 2003 ISL This present software is owned by ISL and is registered with the Agence pour la Protection des Programmes 249 rue de Crim e 7501
5. Printer Select 18 248 Line feeds Form Feed Setup menu display 2 Printer select printer selection compatible with the Analyzer using PCL3 or ESC P language Red code code for printing in red see printer doc Degree code ASCII code designating degree code see printer doc Line feeds number of line feeds after printing Epson compatible ESC P 40 columns DeskJet Black White DeskJet Color See printer doc See printer doc 0to5 4 printer types can be selected Eg Configuration of a 40 column CITIZEN printer 40 18 91 2 Configuration of an ESC P 80 column printer ESC P 248 2 Configuration of a DeskJet Color printer DeskJet 18 248 Form Feed Color For the exact configuration however reference must be made to the manual supplied by the printer manufacturer Table 1 Print Setup menu display FZP 5G2s User s Manual DOCV226A011 C ou Test setting and printing the Run Environment menu DL 5 Test setting and printing the Run Environment menu o e e Main level screens FZP 5G2s S N 214 FZP 5G2s S N 214 FZP 5G2s S N 214 Software V w x Detection Vy z Software V w x Detection Vy z J lt gt Software V w x Detection Vy z PT RUN Start Display C2 Print JRun env Service J quality Run environment programming Diagram 7 The Run Environment menu All run parameters of a product profile are visible but a product can onl
6. S232 menu ofthe Set p menu Going from left to right and from top to bottom RS232 Link setup permanent field RS232 Link setup lt not detected Link on line link established Yes No KG OFF Check send a link control raster lt ISL FZP 5G2s ES gt ON OFF Re E RS232 menu display 1 Press the Link on line or Check key to scroll through the various possibilities Flip flop selection Next display RS232 Link setup permanent field RS232 Link setup rot detected Data sent with the result ransmitted data with the result Condition of run context of the test e g operator name YES NO product profile NO NO Condition of run e Product Product run parameters of the product selected to carry YES NO out the test RS232 menu display 2 Next display RS232 Link setup permanent field RS232 Link setup lt not detected gt Analyzer ID Analyzer identification Automatic validation automatic transmission of the YES NO 1 NON 0 results at the end ofthe test uu ES EOT char end of transmission character ASCII code String RS232 menu display 3 Press the Analyzer ID or End Character key then enter a value with the NUMERIC KEYPAD Press the ENTER key to confirm Press the Automatic Validation key to scroll through the various possibilities Flip flop selection Next display RS232 Link setup permanent field RS232 Link setup lt not
7. 2 28 Start Now 2 28 C Calibration 4 61 Sample probe 4 62 Care Cleaning products 1 18 Unpacking 1 18 Connecting Mains 1 19 Connection RS 232C link 1 20 Correction table Sample probe 4 61 E ENQ ACK protocol RS 232 81 Entry Access code 3 56 Calibration values 4 65 4 66 DOCV226A011 C Internal parameters printing 4 64 ISL 4 1 15 1 23 df JET 3 44 K Keys ALARWSTOP 1 23 CANCEL 1 23 Control 1 23 DIRECTION 1 23 ENTER 1 23 LED 1 23 Reset 1 23 Stop Test 1 23 L Language choice Locking 3 51 M Mains menu screens 87 Menu Access 3 56 Clock 3 54 Correct Table 4 61 Diagnostics 4 60 FREEZE Start 2 31 FZP Pt Run Start 2 28 General 3 51 Labo 3 52 Measures 4 59 Quality 4 61 Run parameters 3 51 Samp T Calib 4 62 Service 4 59 4 65 Service printing 4 64 N NCK2 5G Dimensions 1 17 Features Technical specifications 1 17 Power supply 1 17 Weight 1 17 O Operator Identification s lection 2 29 Operator name list FZP 5G2s User s Manual Page Index 91 ou DL Setup 3 45 P PC link RS 232C 1 20 Printer Setup 3 41 Printing Calibration ticket 4 61 Examples 71 Internal parameters 4 64 Operator name list 3 45 Product parameters 3 44 Printing content setup 3 40 Probe Sample calibration 4 61 4 62 Sample correction table 4 61 Product 1 16 3 36 3 44 3 50 Identific
8. NVRAM has a service life of 7 to 8 years This alarm may therefore be due to a faulty battery The content of the saved RAM memory where the Analyzer parameters are stored is checked by the microprocessor If there is an error the Analyzer goes automatically into download mode so that the contents of the RAM memory saved can be restored by loading a backup file from a PC For this purpose a diskette containing the internal parameter factory settings necessary if memory has not been recently uploaded and a PC up download program are shipped with the standard version of the Analyzer Refer to the section 4 4 File download command the ISL UDS menu page 4 66 on how to load the Analyzer parameters Ee Note So as to have an up to date copy of the Analyzer s internal parameters always to hand it is advised to upload the internal parameters to the PC during routine maintenance operations Use a new file name each time this operation is performed Do not use the internal parameter file name on the original diskette supplied with the Analyzer 6 4 2 Low battery The system keeps a permanent check on this failure If the failure is reported V Do not switch off the analyzer as this will delete any stored data V Print or upload to a PC file the Analyzer parameters contained in the non volatile back up memory NVRAM gt Uploading refer to the section 4 4 page 4 66 on how to load the back up memory internal parameters setting v
9. The unit driver card version the CPU EPLD version eThe date at which the analyzer has been put back into circulation eE The total number of test the analyzer performed The hardware and software version numbers are always indicated on the bottom line of the list of internal parameters supplied with the analyzer DOCV226A011 C FZP 5G2s User s Manual Page 3 55 on DL 8 Access levels and password the Access menu Main level screens FZP 5G2s S N 214 FZP 5G2s S N 214 FZP 5G2s E a 214 Software V w x Detection vy z Software V w x Detection vy z Software V w x BERONETET a vy z FREEZE Pt RUN Sites PIELES 0 Print JRun env Serviceff quality Current Access Level 2 Lab Service Level Tgtevel 7 Level 0 Diagram 9 The Access menu If entry to a protected level is attempted the following message is displayed indicating the current level and the access level requested The access codes previously defined can be entered by means of two buttons Level 1 and Level 2 see the Lab setup menu for configuring the access code for level 1 laboratory Also see the Service setup menu for the definition of the access code for level 2 service refer to the Part 3 section 4 The Service menu of the Setup main menu page 4 65 Access Denied Current Access Level 0 Required 1 Lab Service o pev ums eA J Figure 20 Access to level refused message indicati
10. amp A labcdefghi jkImnopgrstuvwxyz_ lt gt Select an operator name gt FZP Pt Run Display screen Prod 1 By default ID Status Cooling 26 0 C 24 01 2003 14 12 a DOCV226A011 C FZP 5G2s User s Manual Page Appendix C 87 2 Action chart dmes peojdn peojumop Aowa e dnjes suajawesed uog2ajep jeandoe Aqua enjeA uonesqyege Ayua s4ojoure4ed uoneinay e isn pe euim ejeq e dnjes cgpSM ull 2d dnjes yull ZEZ Sue 29 Mag uoneoyipouir SS999E Z Jo 0 40j amp 10qe 1 uoneoyipour SSo22e JoA0 uoneziwmojsng dnjes sunejy e dnjes s4ejeurejed jso dnjes ssajawiesed Jesauab snje eddy e Bunuud 39491 UOHEIGIED e uone4qijeo bugeouy jueureJnseeur Jun Buioo2 jo4u02 enje1eduie ejduieg e syed 1 z jeuy ujen e fue Buguiuud e qe UONDIAUOI aqolde Buifejdsip sainseaye dnjes jnojuug dnjes 1ejuug s4ojoureed uonemgies ssajauresed uone nBe1 sainseaul Bunuud ears e 49491 UOHEIGIED e dnjas bBuguud SI eureu 10724840 jueuiuo4IJAuo uny e uolajap J2npoJg 90325 40 dnjes jonpolde eAno Buguud sjjnsaye 0 Janay 0 yorge Agua sso22e Z Jo o e Agua ssoa2e Jo o e EMA Z uol3281eQ X M A aseMayos Ovz N S SZ9S dz4 Z AA 01329384 X M A JEMJJOS Opz N S S796 dz4 uoneinBiuoo Bunuide uoissiusueg JJnso4 404 uoneplye bBuguud jyjnsay Burhe
11. s 1 23 6 3 The Welcome displays ee d ete eb iem eene cep S ne bete epe i teret idee ere 1 23 PART 2 USE OF THE FZP 5G2S WITH PRE INSTALLED PRODUCTS sense 2 25 1 INTRODUCTION 2 27 2 THE FIRST TEST 2 27 2 1 Selection of a pre installed product ore or re e ente i e Db edet ec epe aedi 2 29 2 2 Characterization of the test ss nen nennen nenennetnennetn enne innen enn eene senes 2 29 2 21 Sample identifying erii epp eo RR REIR Ur UR Re i veis b 2 29 2 2 2 Operator ID e 2 2 3 Textentry display ien svencacteedh iriser n E ede cag eh go E E AEE EER ces E Giani 2 30 2 3 Initiating the test iecit b e Rm e e ten i Ee o D HE HF PENNE 2 31 2 3 1 Procedure E 2 3 2 Test IN prOgTesS s eee RERO D etie deti e OUI IRE IE GERI EE 2 31 253735 End oftest Mean O O te 2 32 2 4 Cleaning the detection c l saana MR A tree ler nee der dead lve one tree 2 32 PART 3 ADVANCED USE OF THE FZP 5G2S scssscssssscscccssseeesscesesseesscesesseesscesesseesccesesseeseseescereoese 3 33 1 INTRODUCTION 3 35 2 THE MAIN LEVEL SCREENS 3 35 3 RESULTS DISPLAYING AND PRINTING THE RESULTS MENU 3 37 3 1 Result displaying from result memory ses 3 37 3 2 Result printing ete ette rhin ep dta eei ede d Pere ip ce ep tbe tan 3 40 4 PRINTING AND PRINTER SETUP THE PRINT MENU 3 41 4T SERVICE printing degere e ep reete in ut eta ee Tele e de etre eg ERR EENE
12. ANALYZER HOST COMPUTER Result sent faulty reception ENQ 1 result message XXXXX gt not properly received NAK 4 ENQ Same message XXXXXX gt not properly received 4 NAK 4 ENQ Same message XXXXXX gt not properly received Host ends the communication EOT Abort DOCV226A011 C FZP 5G2s User s Manual Page appendix B 81 ou DL 5 Transmitted data Example 1 R JetA 2 51 GI G4 IS 07 N3 1 99 0 9999 9 44 0 9999 9 9999 9 9999 9 1 8E 1 C HC 99 99 9 999 9 99 9 999 9 15 07 1999 4 16 43 5F 1 T Jet C 0 0 99 999 999 9999 9 120 0 999 999 1 09 The data that can be transmitted are divided in 3 groups Result See messages R below Always Run context See messages C below If defined in the RS232 link setup Test product See message T below If defined in the RS232 link setup To be transmitted a result must be validated V Manual validation must be performed at the analyzer level refer to the section 3 1 page 3 37 The transmission is only possible after the validation V Automatic validation can be set in the RS232 link setup refer to the section 7 6 1 page 3 53 screen 2 of the RS 232 menu 5 1 Message format Messages are in ASCII code Character strings are enclosed within double quotes They start with an opening bracket They finish witha closing bracket 2 characters CK and the characters C
13. Analyzer or the whole content of the non volatile back up memory NVRAM and for uploading internal parameters of the Analyzer non volatile back up memory Downloading Uploading is made via the Analyzer SERVICE port It is also possible to update the Analyzer software using an update diskette An external connection cable is standard equipment for data flow between PC and Analyzer Downloading Uploading is a function special to this Analyzer The Analyzer is in this mode either by automatic detection of a download request or by an explicit request made via the Analyzer s keyboard In the first case once the Analyzer is in this mode it can only quit when a connection has been made to the computer In the second case it is preferable not to try to quit download mode Downloading causes memory loss If an error is made it is better to let the downloading continue and then download again If the operator stops the Analyzer during downloading the next time the Analyzer is powered up it will automatically detect that a transfer is necessary 4 4 1 Transfer procedure The Analyzer goes into download mode either automatically or requested by the user It waits for a PC transmission When the downloading software is run on the PC it sends a specific message to the Analyzer In replying to this message the Analyzer indicates the type of downloading required followed by a safety sequence The PC then sends data which is processed by the Anal
14. Link on line state of link between FZP 5G2s and the PC Yes No eer nee Analyzer newt Address FZP 5G2s address on a rene Pee id PC Link menu display 1 PC Link setup Next display PC Link setup permanent field PC Link setup Interface status possible error code linked to the FZP Interface status 10 0 Correct 5G2s PC interface Interface initialization initialization of FZP 5G2s PC Interface interface initialisation PC Link menu display 2 Table 9 PC Link menu displays 7 7 Date Time setting the Clock menu The date and time are set by means of Clock menu It is possible to change the date format according to the country in which the FZP 5G2s is being used When the Clock menu is activated the following display appears Displays Meaning of different menus Field values Clock menu Going from left to right and from top to bottom Adjust Date Time permanent field JJ MM AA Adjust Date Time Date format to select the format of the date A MER Date date in the format selected AA JJ MM JJ MM AAAA 01 01 1999 JJ MM AAAA END NN MM IFAARA AAAA MM JJ Clock menu display 1 AAAA JJ MM Next display F Adjust Date Time permanent field Adjust Date Time Time format to select the format of the hour 12 24 h Hours to enter the hour hh mn 24 hours 15 45 AM PM In the case of a 12 hour clock format select AM AM PM _ time format Hours SPM Clock menu displ
15. S L Zi Verson www isl france com 14790 VERSON Tel 02 31 26 43 00 FRANCE Fax 02 31 26 62 93 English Frangais Figure 2 Welcome display This display remains active until the key corresponding to the language of your choice is pressed Doing this activates the display 1 of the FZP Pt Run Start menu see Diagram 1 page 2 27 ePress the key corresponding to the language of your choice to continue Note You can disable the language choice as part of the startup parameters refer to the Part 3 section 7 1 page 3 51 If the choice is locked press any key on the front panel DOCV226A011 C FZP 5G2s User s Manual Page 1 23 Page intentionally blank Page 1 24 FZP 5G2s User s Manual DOCV226A011 C Part 2 Use of the FZP 5G2s with pre installed products Page intentionally blank Page 2 26 FZP 5G2s User s Manual DOCV226A011 C Introduction 1 Introduction ou DL This part will be concerned with all aspects relating to the test for determining the freezing point of hydrocarbons using pre installed products They are stored in a memory that can be saved or updated very easily e g when a standard is changed by downloading from a PC via the SERVICE port refer to the chapter 0 page 4 66 2 The first test In this chapter we will deal with a Freezing point test carried out with the FZP 5G2s stage by stage We will however only describe the menus that are strictly necessary for the successful operation of th
16. calibration When the display becomes almost stable with the first three Resistor 80 312 Q A D 35052 characters of the A D conversion stable validate with OK Press OK when the reading is stable LS Ok Samp T Calib menu Display 5 Proceed similarly with the Simulator knob set on 50 C 122 F At the end of operation display 1 of the Quality is displayed Table 14 Samp T Calib menu displays At the end of the calibration procedure 1 Power off the Analyzer 2 Disconnect carefully probe simulator connector from the J10 port and then reconnect the sampling temperature sensor 3 Replace the protective cover and fix with the four screws DOCV226A011 C FZP 5G2s User s Manual Page 4 63 on DL 3 The Service menu of the main printing menu Main level screens FZP 5G2s S N 214 FZP 5G2s S N 214 FZP 5G2s Eee edens 14 Software V w x Detection Vy z Software V w x Detection vy z Software V w x Detection Vy ee edens FREEZE Pt Run Start PARTIES a Printing Loy Diagram 12 The Print menu The Service menu of the main printing menu is dedicated to Analyzer maintenance and it requires a Level 2 access authorization Actually collect the regulation data linked to the device functions and print them enables a diagnostic to be made easier Data can also be stored in a PC fill Activate the Service menu of the Print menu the following screen is displayed
17. contrast and low DIRECTION key for more contrast refer to the next section CS Note The intensity of the backlight can change according to the ambient temperature Page 1 22 FZP 5G2s User s Manual DOCV226A011 C er The user interface DL 6 2 The control keys Three keys take up the lower left hand side of the front panel namely STOP TEST To stop a test or any other operation STOP If the LED is lit up this means that a test is in progress RESET To cancel and go up through the display menu hierarchy Interrupts the audible alarm signal ALARM STOP If the LED is lit up this means that a problem has arisen Pressing on this button will give the error message content Iel The rest of the front panel is occupied by a numeric keypad equipped with a CANCEL KEY and an ENTER key ENTER key validate an input of variables TO CANCEL characters Finally in the lower left hand section there are four direction keys used to move around a text field and select characters to enter variables e g name of sample DIRECTION keys 6 3 The Welcome display When the analyzer is switched on the welcome screen is displayed If it does not first check the backlight settings see section 6 1 2 on the previous page This screen provides information about ISL and two menus offering the choice of language when this choice has not been set as one of the Analyzer s internal parameters I
18. dimension in 1993 by obtaining ISO 9002 certification from the BVQI Working hard to extend our quality assurance program we received ISO 9001 certification in 1995 Though best known for distillation viscosity testing cold behavior instrumentation flash point evaporation loss oxidation and asphalt testing equipment ISL s contributions to automated petroleum testing continue to grow With more than 10 patents to date ISL s constant research into new technologies buttresses our precedent for ultimate precision performance and safety The company now offers over 20 Automatic Analyzers for different applications giving incontestable benefits to its users in increasing of test precision by elimination of operator subjectivity and human errors while increasing productivity and reduce operator time with highest level of safety A worldwide distribution network supports our customers with quick efficient service and our highly knowledgeable service staff buttresses this relationship providing solutions to product or application challenges Please visit our web site for more information http www isl france com DOCV226A01 1 C FZP 5G2s User s Manual Page 1 15 ae DL 1 2 About this manual This manual is made up of four main parts entitled gt Part General gt Part Il Using the FZP 5G2s with pre installed products gt Part IIl Advanced use of the FZP 5G2s Part IV FZP 5G2s Maintenance The first part presents
19. env to upload the prestored products and the operator names list All to upload the whole content of the NVRAM memory regulation and calibration parameters run environments and results Table 16 ISL UDS menu of the Service setup menu screens eSelect the required functions the uploading will be to the PC The Analyzer screen will display the type of transfer PC Start the transfer on the PC as explained in the ISL UDS software Read me file Enter the number 1 or 2 of the serial communications port used COM Downloading Analyzer software Key in the data file name key in the name and the extension of the file ISIFZP5G2s Vxx xx software version Validate with ENTER Downloading internal parameters Enter the required file name and then validate with ENTER Key in the name and the extension of the file A display on the PC informs the operator of the type of operation running For internal parameters upload to a PC use a new file name for each download for example use the Ee date as a name IPDDMMYY NVM Moreover it will be interesting for the user to identify the type of the file uploaded with its extension name Upload to PC run environment file1 env ball file2 nvmAnalyzer End of transfer If the transfer was OK eThe Analyzer is automatically reinitialized DOCV226A011 C FZP 5G2s User s Manual Page 4 67 iSL 4 4 4 Transfer fails or screen not lit If the transfer fail
20. handling these materials while operating the Analyzer Please gt read the manual gt wear proper protective clothing perform all suggested service procedures use care to prevent accidents The manufacturer accepts no responsibility for any damage or liability arising from the use of Analyzers Use of Non ISL Products and Accessories Defects or damage that result from the use of Non ISL branded or certified Products Accessories Software or other peripheral equipment are excluded from warranty CAUTION Laser radiation when open the detection cell Disconnect the analyzer from the mains nex Cupar iw sim DO NOT STARE INTO BEAM CONSEQUENCES COULD BE This label is located on the detection cell DOCV226A011 C IRREVERSIBLE The use of optical instruments with this product will increase eye hazard The FZP 5G2s is equipped with a Class IIIA laser detection cell As the laser beam used is harmful to eyes do not attempt to disassemble the cell Refer servicing to qualified personnel only FZP 5G2s User s Manual Page 7 Page intentionally blank Page 8 FZP 5G2s User s Manual DOCV226A011 C Contents PARTI GENERAL nn epe ea rt tte eh EEE EE Her eS SET OEKE oo SOES ETEN ES ETE EnS 1 INTRODUCTION INOI ISE compatyiprolle s 4b EE cn NN SP EE OEE A EE AAAA A a eta A Ata 1 2 About this manual iiie ini Er A E E p OT UR d e eE AE a een 1 3 Typographical conventions S 1 4 Meaning
21. of symbols ener ere ee eret idees n D REPAS ER acd ened e TI EHE GR IHR OR PE ae 2 TYPE OF ANALYZER 2 T EZP 5G28 pr duct Oye VIEW ederet tete epe e D ROTG i taret ete vete D nt ttes 2 25 Technical specifications iei Oe d DR e n B DIES 2 2 1 Operation in ambient conditions lt PO ALI EE EA EEE E E EA OE E E I EE EE TE 2 23 POWET SUPP rhin e re OE PRIORE RD UO Ce Hae FO Hp a 2 24 DIM NSIONS SR e IM ed D MM de Ate ndi c 3 CARE IN USE 3 1 Care in the use of testing and cleaning equipment 1 18 3 2 Precautions to take when using built in cooling Analyzers 1 18 4 UNPACKING AND INSTALLATION 1 18 LM GC SRBRIIDEIU SHIRE 1 18 4 2 Installing the FZP 5G2s unlocking the shock absorber sss eee 1 18 4 3 Connections 4 3 1 Connection to the Tmalns iei e He cere eed ee e ORE ee Ue D E eee eere e adde die dapes 1 19 4 3 2 Connecting the printer se eee eee reete tn cesses eheu ee eda dra oat int eee eo aede ena ena eic eus aeo ea den se eben en eg 1 19 43 3 FZP 5G2s 7 PE Ink sere eere nieder e enit der aene a SRI HD ER NOR I ORA RA 1 19 5 DESCRIPTION OF THE DEVICE 1 21 6 THE USER INTERFACE 1 22 Gil Eront patios 4 carta a eere e er UH NI tn er E EIE less dal trs tee A cubed dns an nd 6 1 1 The LCD X 6 12 Backlight settitg retener ee ee RE rre dee e med 1 22 0 2 The contol ATE
22. safety permanent field Alarms setup Thresh to enter the lower sample temperature the 150 C gt 55 C Sample temperature safety system accepts alarm triggered after a recognition time 125 C 45 C 10s Thresh to enter the upper temperature safety the 150 C gt 55 C Thresh Thresh rafter system accepts alarm triggered after a recognition time After setting of the recognition time before upper 0 gt 120s Alarms menu display 2 threshold to be taken account If the sample temperature exceeds limits values in the recognition time here 10s the system stops the test immediately and the alarm message Sample temperature safety is displayed Next Disnlav Cooling circuit permanent field Al oT ms setup Thresh 1 minimal cooling rate in opacity searching T Clmin gt Cooling circuit phase A Cmin 1 C min 120s 3 C min After setting of the recognition time before the threshold 0 120s ium iym ETE ra m 5559 taken account Thresh 2 minimal cooling rate 45s after test starting 2 Cimin gt Alarms menu display 3 5 C min Net Disnlav Table 6 Alarm menu screens 7 4 Personalization and access authorization to level 1 the Lab menu The FZP 5G2s can be personalized and so bear the name of the laboratory that acquires it together with the name of the head of the laboratory He or she can restrict access to write protect certain parameters The following displays can be called up
23. supplied with the analyzer to form an RS 232C serial link enabling results to be collected on a PC and for transmission to a LIMS see Appendix B RS232 link features on FZP 5G2s page Appendix 77 for the meaning of the messages Use the adapter supplied with the analyzer see the Packing List it has two RS 485 connectors on one side which have to be connected simultaneously to the Analyzer s Alan input and output and on the other side an RS 232C connector to be connected to the PC The ISL analyzers allow transmitting data according to specific customized criteria and a user defined E protocol Note The RS 232C communication mode has to be parameterized Refer to the section 7 6 1 RS232C link setup the RS232 menu page 3 53 4 3 3 3 The SERVICE port The FZP 5G2s has a serial SERVICE port as a standard fitting with which with the help of the ISL UDS service software supplied software updates can be downloaded via a PC and the contents of the memory such as the internal parameters and results can be saved for subsequent reloading refer to the section 4 4 page 4 66 for transfer commands Alan network inlet and outlet RS485 link RS 232C link with adapter Logic card Ms ventilator EHE Parallel port Printer Main switch and Sockel Cooling unit ventilator Shock absorber fixing panel with two blocking bolts in place Picture 3 Rear panels and connections
24. the Setup menu 7 1 Power on parameters the General menu The General menu allows choosing the access level and the language if you would like to lock it in place when the device is switched on It also allows configuring or deactivating the assisted edition the FZP 5G2s can proposes a suite to the characters entered based on prior enters refer to the section 2 2 3 2 page 2 30 Displays Meaning of different menus Field values Aa L Going from left to right and from top to bottom General setup General setup permanent field Power on parameters p EE ceci on 2 Access level choice of default access level 0 3 ints when the device is switched on kd Country It should be noted that only the current access level or lower access level could be General menu display chosen Country language choice of language selected Selection Engli by default locked Selection allows the sh operator to choose the language Frangais Auto Edition characters number needed to 029 activate the auto edition 0 inhibits the function Press the ACCESS LEVEL key or the AUTO EDITION key then enter a value with the NUMERIC KEYPAD Press the ENTER key to confirm Press the LANGUAGE key to scroll through the various possibilities flip flop selection Table 4 General menu displays 7 2 Run parameters the Run menu The Run menu allows choosing the product profile in place when the device is switched on
25. the Analyzer and this manual content The second part allows the operator to carry out an initial test to determine the hydrocarbon freezing point with the FZP 5G2s in a few steps confidently and with no particular prior knowledge The third part on the other hand makes it possible to use the FZP 5G2s potential to the full It is therefore intended rather for the knowledgeable user who is familiar with tests for determining hydrocarbon freezing points In any case the sensitive parts of the FZP 5G2s software those linked to the test parameters can be read and write protected by a system of passwords chosen by the user The fourth part intended for service staff explains in detail maintenance and upgrade operations of the Analyzer 1 3 Typographical conventions Convention Meaning Bold Important words or phrases Bold Italics Menus or buttons on the LCD Bold SMALL CAPITALS Keys on the front panel of the device 1 4 Meaning of symbols CS Note Important comment A CAUTION Call for particular care LI Referral Referral to a particular document Standards or to another manual Page 1 16 FZP 5G2s User s Manual DOCV226A011 C F3 Type of Analyzer 2 Type of Analyzer 2 1 FZP 5G2s product overview ISL s FZP 5G2s has been designed to provide highly accurate freezing point determinations down to 100 C 184 F of aviation fuel It combines a patented built in cooling system and highly precise detec
26. the ISL authorization This could question the good working order of the unit This menu also group together commands for software update commands for file transfer to a PC and saved memory deletion and backup Activating the Service menu of the Configuration menu gives access to two displays Displays Meaning of different menus Field values Service menu Going from left to right and from top to bottom Service setup permanent field ee 5G2S UNE AccCode access code to level 2 maintenance 32768 gt Service setup 32767 Regul regulation parameters entry L1 mant Regu Calib entry of setting values e g sample Service menu display 1 temperature probe ISL UDS software downloading commands and command for data transfer to PC Next display Service setup permanent field id ashe EE Detect entry of optical detection parameters Service setup Memory init to access to the deleting menu or Memory initialization menu for backup Ram memory Init storage areas gt RESULTS deleting of the results stored gt PRODUCT deleting of the product lists gt OPER deleting of the operator names lists gt ALARMS amp REVIEW alarms initialization with default values and deleting of the alarms memorized gt SAMPLE PROBE deleting of the correction table value of the sample temperature measurement probe Service menu display 2 Table 15 Service menu displays DOCV226A011 C FZP 5G2s User s Ma
27. y z gt Software V w x Detection y z FREEZE Pt Run Stee DEN RES EOSSIIH O Print MEM Service f quality Dj Res 26 52 29 12 2003 15 26 Prod 1JET C ID 257321H4 Freeze point 34 2 C Diagram 3 The Results menu Test results are stored in a dedicated memory The FZP 5G2s can store between 45 and 50 test results When the memory is full the FZP 5G2s automatically overwrites the first results recorded Results can be displayed printed and sent to a PC by the RS232C link refer to the Part 1 section 4 3 3 FZP 5G2s PC link page 1 19 3 1 Result displaying from result memory From the Freeze Pt Run Start menu the user must go up one level in the display hierarchy press the arrow key on the left bottom of the display the PREVIOUS DISPLAY key see in Part 1 section 6 1 1 page 1 22 to return on the main screens level see Diagram 2 then 1 Press the button for the Results menu of the main level screen 1 this calls up the display allowing access to all the results saved which are shown as the display below Figure 10 2 To access the desired result press the DIRECTION KEvs as many times as needed Note The black arrow at the left bottom of the screen indicates the presence of a registered result after the result displayed Res 36 52 05 01 2004 10 11 Prod 1 Jet A1 ID Jet A1 Freezing point 50 5 C Figure 10 Display of the Results menu This screen contains the following indication
28. 011 C ou Interface features DL In this document analyzer is used for the ISL FZP 5G2s while host computer designates the computer to which the ISL FZP 5G2s is connected 1 Interface features EIA RS 232C serial link Rate 300 to 19200 BPS Data bits 7 8 Stop bits 1 2 Parity none odd even Switchable on line off line state Pre defined message transmission available for test Possibility to define an identifier number for the analyzer Possibility to activate result auto validation Automatic detection of the RS232 interface cable adapter 2 Outlet connector broaching The RS 232C connector of the adapter is a 9 pin connector The pin configuration is as shown below TxD e RXD SIGNAL e 4 GND N 5 s i 9 H 7 6 RTS E CTS EIA RS 232C interface Line status in standby 12 V MARK Input signals used CTS RTS DOCV226A011 C FZP 5G2s User s Manual Page appendix B 79 ou DL 3 Communication protocols Flow control Protocol can be None RTS CTS Xon Xoff gt ENQ ACK Flowcontro Type Comments i Xon Xoff E Transmitted messages are sent without any way to stop them from the host computer However a special parameter Time between two messages in the ISL analyzers allows to define a pause between to successive message from 0 0 s to 10 0 s by step of 0 1 s Note This time is applied bet
29. 9 Paris It is protected in France by the Code de Propri t Intellectuelle laws and internationally by international treaty provisions and all other applicable national laws It must not be copied reproduced adapted translated rented or disassembled This also applies to the accompanying manuals INFORMATION Information in this document is subject to change without notice and does not represent a commitment on the part of ISL ISL provides this document as is without warranty of any kind either expressed or implied including but not limited to the particular purpose ISL may make improvements and or changes in this manual or in the product s and or the program s described in this manual at any time This product could include technical inaccuracies or typographical errors Changes are periodically made to the information herein these changes may be incorporated in new editions of the publication Reproduction of any part of this manual without express written permission is forbidden Translation in foreign local language other than French or English Translation in other language than French and English have no contractual value and have been performed under responsibility of the local distributor In any case the reference of the present literature will be the French and or English release provided under ISL copyright Page 4 FZP 5G2s User s Manual DOCV226A011 C CUSTOMER Reserved for public relations department e
30. C ou The first test 2 3 Initiating the test 2 3 1 Procedure After having prepared the analyzer carry out the following operations to initiate a freezing point test Do not forget to put the beaker under the drain tube in order to recover the used sample see Picture 5 Se page 1 21 1 Withdraw by means of the syringe provided a 10 ml volume of the sample for a justification of this choice of volume refer to the chapter 5 Description of the device page 1 21 2 Insert syringe gently into the orifice designed for this purpose on the test bench see Picture 4 on page 1 21 and inject the contents of the syringe CE After the sample is injected it is essential that the syringe remains inserted in the sample injection orifice 3 Activate the Start now menu of the FZP Pt Run Start menu see Figure 3 page 2 28 if all the stages have been carried out correctly the test starts and the following display will appear Prod 1 By default ID Status Cooling 26 0 24 10 2002 14 12 Figure 7 Start now display in cooling phase The display contains the following information eProd product type selected to carry out the test eID identifying name of sample eStatus indicates the operation in progress in the case of the above figure this is the cooling phase for the sample The indication gt Freeze in the status field characterizes the hydrocarbon freezing point search phase eThe current date and time eT
31. E RENTUR ER 3 41 AD Printer setup 25a cree x e EHE EN Cae AER ESETA EENE ESEA ORI nas ve EE sexe see es Sen Sn Ree ERE 3 41 DOCV226A01 1 C FZP 5G2s User s Manual Page 9 ou DL 5 TEST SETTING AND PRINTING THE RUN ENVIRONMENT MENU 3 43 5 1 Run parameters of a product 502 List OF operator Dames vier eee I oe et ph ep E EEE EEE O E E 6 ALARM TREATMENT 6 1 Types Of alarm 671 ls Farlur alarms zi eaten ce See elie a be aes 6 1 2 Wartung A latins scie ceca reet ain dud daa esee eter da less tr E AE en Peine ronds ed re 6 2 Displaying alarms stopping the buzzer 6 3 Alarm processing 6 4 Failure alarms 6 4 1 Memory tallufe 5 5e plecti ta ee te RE De Mee e RO ore oer e derat de eri dolente dessen 0 4 2 Low battery sn nt es eene tege Re Ua tee he Me ge e da Ur eO press Eten are beer el sen etre ren 6 4 3 Signal conditioning A D Cnv 6 4 4 Cooling circuit 6 4 5 Heating circuit 6 4 6 Sample temperature safety issues 6 4 7 Cooling unit temperature safety ss 6 4 8 Cooling unit stroke control safety 6 4 9 Cooling unit board link safety 6 5 Warning alarms sse 6 5 1 End of test Freeze point detected een nennen enne eterne netter eren 6 5 2 End of test Freeze Pt not detected xe ree Deere ote Real tete ERES ERE e Nee EROR 6 5 3 End of test Crystall not detected 0 3 4 Buz
32. ERATOR NAME LIST PRINTING 73 4 CALIBRATION TICKET PRINTING 73 5 ANALYZER MEASURE PRINTING 73 6 INTERNAL PARAMETER PRINTING 74 APPENDIX B RS232 LINK FEATURES ON FZP 5G25 ssscccesssscecssssececsscccessssccecssscccecssccessscceessneees 77 1 INTERFACE FEATURES 79 2 OUTLET CONNECTOR BROACHING 79 3 COMMUNICATION PROTOCOLS 80 4 ENQ ACK PROTOCOL DETAILS 81 5 TRANSMITTED DATA 5 1 Message fotM t SERE 5 2 The r sult message ii ene ete ne ete ame deti inde qe been ite heal adie 5 3 The run context message 5 4 The test product message 5 5 RS232 link test me88886 ardent Mens Ait eed doe ed dee TR Pr EORR ERR 6 RS232 COST APPENDIX C SEQUENCE CHARTS teer ees ba rent b neuen bebe eU eee seek PE res enne E epe ovk Pee e vae v Pe be evo e teese 85 TEST LAUNCH DIAGRAM 87 2 ACTION CHART 88 INDEX T 89 INDEX 9 FZP 5G2S SPARE PART GIST sise sas aassas cues sex Yn PER ea b re Eee EXER MINER ERE baseanseduncveaseneeesss DOCV226X200 UNLOCKING THE SCHOCK ABSORBER eee ee ee eene eene tne te tone tone eoa e ense ene s ense en seen eta DOCV226X001 DOCV226A011 C FZP 5G2s User s Manual Page 11 Page intentionally blank Page 12 FZP 5G2s User s Manual DOCV226A011 C Part1 General Page intentionally blank Page 1 14 FZP 5G2s User s Manual DOCV226A011 C er Introduction DL 1 Introduction 1 1 ISL company profile We would like to take this opp
33. ISL This software is a multitasking software running under Windows allowing up to 31 ISL Analyzers to be connected to the same PC computer see the illustration below It allows data coming from different ISL analyzers to be collected and stored Besides multi analyzers results database management and control according analyzer type run control alarms displaying internal parameters management the ISL Alan software allows transmitting results directly to a LIMS or ever information system LL CE Note The RS485 communication mode has to be parameterized Refer to the section 7 6 2 Alan link setup the PC link menu page 3 54 Note The Alan Kit is optional hardware and software package Refer to the Alan Installation and Getting Started Manual Each analyzer connects to the Alan network via the RS485 serial interface through two ports input output located on the rear panel see Picture 3 on the next page for more explanations Example of an ISL Analyzers network Converter CPP 97 2 NCK2 5G FP92 5G 5G2 and Le GER FP93 5G 5G2 J m N AM 19 x P Y AD86 5G and M AD86 5G2 FP56 5G 5G2 and FP170 5G 5G2 FZP 5G 5Gs and FZP 5G2s FPP 5G 5Gs DOCV226A01 1 C FZP 5G2s User s Manual Page 1 19 ae DL 4 3 3 2 RS 232 C serial link The network input output ports of the analyzer link interface with the Alan network may be connected via a special adapter
34. Page 1 20 FZP 5G2s User s Manual DOCV226A011 C Description of the device ISL 5 Description of the device The FZP 5G2s consists broadly speaking of two major parts eA user interface eA test bench The user interface will be the subject of the next section The extremely simplified test bench features an orifice through which by means of a syringe supplied a 10 ml sample is injected for test purposes This volume is calculated precisely to allow in one single operation eThe old sample to be removed and replaced by the new one eThe cell to be cleaned by dilution of the old sample by the new Caution Cell cleaning is normally done with the next sample and a chase n flush technique Do not use acetone Note If the cell is accidentally cleaned with a solvent this will be rapidly rinsed with an injection from 10 to 20 ml of heptane or kerosene All solvents are prohibited they may cause deterioration of the cell Use only heptane CAUTION Laser radiation when open the detection cell Disconnect the analyzer from the mains DO NOT STARE INTO BEAM CONSEQUENCES COULD BE IRREVERSIBLE The use of optical instruments with this product will increase eye hazard The FZP 5G2s is equipped with Class IIIA laser detection cell As the laser beam used is harmful to eyes do not attempt to disassemble the cell Refer servicing to qualified personnel only By means of an appended tube on the right side of the FZP 5G2s the
35. Q ACK protocol details DL 4 ENQ ACK protocol details The host computer must acknowledge all messages from the analyzer Should communication fail only the host computer can decide whether or not to abort transmission Analyzer response time on receiving ENQ lt 100 ms Waiting time for message acknowledgment 2 sec Results transfer delay after end of test delay for ENQ not limited Number of transmission of the same result message on not limited end with ACK or EOT reception receiving NAK Request reception and acknowledgement of results The host computer uses the ENQ code 05H to ask the analyzer if any results are ready to be sent If the analyzer has no results to send it replies ACK 06H The host computer does not have to reply to this ACK ANALYZER HOST COMPUTER No result available 4 ENQ No result ACK gt If the analyzer has results it starts their transmission On receiving the message the host computer must check it checksum and must reply ACK 06H or NAK 15H depending on whether the message was correct or not If there are several fruitless communications the host computer may decide to abort transmission by sending an EOT 04H character ANALYZER HOST COMPUTER Successfull transmissions 4 ENQ 1 result message XXXXX gt 4 ACK 4 ENQ Next result YYYYY ELLO 4 ACK 4 ENQ No more result ACK p gt
36. R LF and EOT CK 2 characters checksum the 2 least significant digits expressed in ASCII of the result of the hexadecimal sum of all the preceding characters including the brackets CR 1 non printable character Carriage Return ODh LF 1 non printable character Line Feed OAh EOT 1 non printable character End Of Transmission character programmable in the RS232 setup menu If 0 there is no end of transmission character The value 999 indicates that the field is not being used reserved for a future use er 5 2 The result message As indicated above if the transmission of data on the RS 232C link has been validated automatic or manual validation the result message is systematically transmitted Temperatures expressed in C or F corrected or not by barometric correction depending on the product programmed Example 1 R JetA 2 51 GI G4 IS 07 N3 1 99 0 9999 9 44 0 9999 9 9999 9 9999 9 1 8E Page Appendix B 82 FZP 5G2s User s Manual DOCV226A011 C Transmitted data ou Meaning of result message fields under ticket form from left to right Message R Fields Format Number of Characters Analyzer no from 00 to 99 2 Type of message string 2 ID sample string 12 Sample number string 12 Product number from 00 to 99 2 Reserve 99 2 Temperature unit 00 to 01 2 Reserve 999 9 to 9999 9 6 FREEZE result 999 9 to 9999 9 6 Reserve 9999 9 6 Reserve 9999 9 6 Reserve 9999 9 6
37. Service Printing Measuresi Regul Figure 26 Service menu of the main printing menu The Service menu of the main printing menu contains following buttons V Measures to print values measured by the different FZP 5G2s sensors refer to the section 1 1 Measurement displaying on the FZP 5Gs Analyzer the Measures menu page 4 59 See Appendix A chapter 5 page A 73 for a printing example V Regulation regulation monitoring feature Analyzer internal measures printing each seconds Internal parameters Analyzer internal parameters printing setup parameters run parameters and setting values 40 80 key this feature enable the internal parameters to be printed out according to the printer setup 40 or 80 columns 80 key this feature enables the internal parameters to be printed out in 80 columns whatever the printer setup may be 3 1 Regulation monitoring The Regul menu enables all regulation data linked to the Analyzer devices to be collected and transmitted to a printer or other peripheral PC or LIMS These data are read each seconds during the entire test To do so enables a diagnosis to be made easier 3 2 Internal parameters A number of internal parameters are stored in the non volatile memory They are controlled by the microprocessor with a code checksum stored in the memory These internal parameters relate to V Setting values amp Setup values V The Analyzer identifying One of the first operat
38. Software V w x Detection Vy z FREEZE Pt Run 3 C FZP 5G2s S N 214 Software V w x Detection Vy z e p S FZP 5G2s S N 214 Software V w x Detection Vy z e O ESTE j Figure 9 The three displays of the main menu The main display level includes the following components respectively from top to bottom and from left to right eThe name of the device eThe serial number of the device eThe version of the control software and the version of the detection cell The menus of the main level are FZP Pt Run Start FZP Pt Run Display Results Access Print Run Environment Service Quality and Setup These menus will be dealt with in detail in the paragraphs following It should be noted however that the FZP Pt Run Start and Display menu was covered almost in its entirety in Part 2 In the following we shall assume that the access level is level 1 Laboratory This level allows access to the settings associated with tests making it possible to modify them and thus design personalized products that respond to specific needs The access levels will be dealt with through the Setup menu Page 3 36 FZP 5G2s User s Manual DOCV226A011 C ou Results displaying and printing The Results menu DL 3 Results displaying and printing The Results menu 6 Main level screens FZP 5G2s S N 214 FZP 5G2s Hum 214 FZP 5G2s S N 214 Software V w x Detection y z Software V w x Hum
39. Type of test end 00 a 05 2 Adjustments to be made string 1 indicator Type of test end 1 Freezing point detected 2 Freezing point not detected 3 Not used 4 Crystallization not detected Contents of Freeze Result field according to type of test end Field value R result Reserved for number of cut 0 C 1 F Reserved for the presumed number OK to be made 1 Freezing point temperature rounded if requested in the product 2 No temperature recorded 3 Not used 4 test stop temperature set in the run product see message T below 5 3 The run context message Example 1 C HC 99 99 9 999 9 99 9 999 9 15 07 1999 4 16 43 5F Meaning of run context message fields under curve form from left to right Message C Field Format Analyzer no from 00 to 99 Type de message string Operator name string Reserve 99 Reserve 99 Reserve 9 Reserve 999 9 Reserve 99 Reserve 9 Reserve 999 9 Date string Date format from 00 to 07 Time string DOCV226A011 C Numbers of Characters 2 D IN O1 2 m Oo 2 IN N EN DIS FZP 5G2s User s Manual Comments C Context 0 JJ MM AA 1 MM JJ AA 2 AA MM JJ 43 AA JJ MM 4 JJ MM AAAA 5 MM JJ AAAA 6 AAAA MM JJ 7 AAAA JJ MM Page appendix B 83 ou DL 5 4 The test product message Example 1 T Jet C 0 0 99 999 999 9999 9 120 0 25 999 1 09 Meaning of product message fields under c
40. ZP 5G2s User s Manual DOCV226A011 C ou Adjustment the Quality menu ISL Displays Meaning of different menus Field values Samp T Calib menu Going from left to right and from top to bottom Frequency frequency of calibration 0 gt 365 days Sample temp measurement calibration 0 days indicates that there is no check for the Performed 01 01 2003 Next 01 01 2004 passing of the calibration date 365 days NO Test refusal initiation of test denied when date Yes No O NUNN Dj or calibration passed Samp T Calib menu Display 1 Next display Operator name of calibration operator String ANS END Measurements calibration Calib Reference calibration reference String lt Name gt Ref operator Samp T Calib menu Display 2 Next display Cancel cancel calibration Return to display 1 of Samp T Sample temp measurement calibration Calib menu een be sure the Pt100 simulator Continue once calibration has been initiated it is no longer is connected then press continue possible to cancel it The keys on the front panel are disabled Samp T Calib menu Display 3 Next display Position the Simulator knob at Sample temp measurement calibration 50 C 58 F Position simulator on 50 C 58 F Resistor value enter if necessary the resistance value Ohm 80 3120 Samp T Calib menu Display 4 Next display Sample temp measurement
41. aboratory name Title Auto Yes Format Ticket Content Detail Line feeds 2 lines Conditions of run NO Product YES Automatic result validation NO Stop bits 1 Parity None Flow control None if no flow control used 0 1s Analyzer PC ID ISL FZP 5G2 Time 24 hours Kp2 5 0 Ki2 0 50 Kd2 0 0 Next calibration date 27 03 2004 Start test refused NO 50 C 122 F 119 4110hms A D 52118 80 C 0 0 70 C 0 0 40 C 0 0 30 C 0 0 0 C 0 0 10 C 0 0 40 C 0 0 50 C 0 0 80 C 0 0 90 C 0 0 CDd 5 ZmDd 10 ZcDd 5 0 4 08 03 2003 496 FZP 5G2s User s Manual DOCV226A011 C Internal parameter printing Cooling unit parameters S N M100B3L161 9 22 01 2003 83 03 0 00 05 02 2003 17 0 9 17 34 51 68 87 100 110 27 03 2003 17 0 9 17 34 51 68 87 100 110 DOCV226A011 C 0 26 0 00 10 1min25 2min18 2min50 3min20 4min35 6min02 7min51 10min26 12min41 14min56 1min20 2min10 2min41 3min10 4min20 5min44 7min27 9min56 12min23 14min58 241 239 238 237 236 233 231 231 230 230 251 248 247 246 244 240 236 230 227 216 Runs 35 28 03 2003 0 26 0 40 10096 10096 FZP 5G2s User s Manual ou Page Appendix A 75 Page intentionally blank Page Appendix A 76 FZP 5G2s User s Manual DOCV226A011 C Appendix B RS232 link features on FZP 5G2s Page intentionally blank Page Appendix B 78 FZP 5G2s User s Manual DOCV226A
42. alues run environments and results gt Printing the run environments product run parameters operator names list see chapter 5 page 3 43 and the internal parameters refer to the chapter 3 page 4 64 V Switch off the Analyzer and call an ISL approved technician to replace the battery refer to the Service Manual V Download Analyzer internal parameters or enter it refer to the chapter 3 The Service menu of the main printing menu page 4 64 Note Regular uploading of the intemal parameters must be programmed as part of the analyzer CS maintenance procedure Use a new filename e g with the current date in the name PIDDMMY Y NVM This way the latest version of the internal parameters will be saved to a file 6 4 3 Signal conditioning A D Cnv This failure is reported upon detection of no dialogue between the CPU and the A D converter Switch the analyzer off then on again If the failure persists contact the ISL Customer Service 6 4 4 Cooling circuit The system checks the cooling circuit 5 min after test starting by verifying the cooling rate The alarm is triggered if gt 1 min after the test is started the rate is higher than threshold 2 by default 3 C min programmable from 2 to 5 C min On cooling during opacity search if the rate is higher than threshold 1 by default 1 C min programmable from 1 to 10 C min during a recognition time programmable from 0 to 120 s A test currently running
43. an store up to 40 prestored products the black arrow in the top right hand corner of the screen indicates the presence of more lists following on Use the RIGHT and LEFT DIRECTION KEvs to move from table to table and scroll through the different pages of products Select a prestored product if you wish to modify its associated run parameters or select an empty field if you wish to create a new product see in Part 2 section 2 1 Selection of a pre installed product page 2 29 for precise explanations on how to select a field Press the Details key screen 1 of the product Details menu is displayed as shown in the table below Display Meaning of different menus Field values Product details menu Going from left to right and from top to bottom Current product is N 1 Name product name entry button String The product name in this case is JET Product No 1 JET CO Unit selection of temperature CPF a GNSURGN measurement unit The temperature Product details menu display 1 is here measured in C Next display Results Rounded the results can be YES NO Product No 1 rounded to the nearest 0 5 C NO 100 c Stop Tmp temperature of the end of the cooling phase Min 1200 C Results 2 Rounded D 184 F Product details menu display 2 Max rose UE Table 2 Product details menu displays Ee Without the necessary authorizations passwords it is not possible to change the field values of the Product menu d
44. asily 2 Keep the ventilation holes in the side of the unit clear They must be regularly blown clear of dust to avoid clogging and possible blocking 4 Unpacking and installation 4 1 Care in unpacking After unpacking check the device and its accessories as well as any possible damage sustained in transit which must immediately brought to the attention of the carrier so that a statement of damage can be made The various parts of the FZP 5G2s are carefully checked and tested before shipping Nevertheless it is worth checking that the equipment received corresponds to the packing list enclosed On taking delivery of the FZP 5G2s unpack all these parts Put the Analyzer on a workbench near electrical sockets and connections to cold sources Allow enough space for access to the rear connectors Leave sufficient space behind the Analyzer for cabling access and for clear ventilation 4 2 Installing the FZP 5G2s unlocking the shock absorbers The FZP 5G2s cooling compressor is mounted on shock absorbers that must be locked during transportation The shock absorbers is locked by bolts that screw in underneath the unit please refer to the document DOCV226X001 To ensure that the bolts are removed after transportation the unit will not sit flat on its base until they are removed When unwrapping the unit 1 Remove the shock absorber locking bolts from underneath the unit 2 Screw them into the special storage panel at the back of the un
45. ation s lection 2 29 Setup 3 44 Product name 3 44 R Regulation monitoring 4 64 Request and reception of results RS 232 81 Resetting Result memory reset 4 65 Results Printing 3 40 Send to a PC or a LIMS 1 20 Storage 3 37 RS 232C link 1 20 Page Index 92 RS 232C Interface 79 Run environment Operator name list setup 3 45 Product setup 3 44 S Sample Identification 2 29 Screen LCD 1 22 Next 1 22 Previous 1 22 Selection Operator 2 29 Service printing menu 4 64 Setup General 3 51 Operator name list 3 45 Printer printing 3 41 Printing content 3 40 Product list 3 44 Run 3 51 Stop printing 3 40 T Technical specifications 1 17 Test Launch 2 27 W Welcome screen 1 23 FZP 5G2s User s Manual DOCV226A011 C
46. ay 2 Table 10 Clock menu displays Page 3 54 FZP 5G2s User s Manual DOCV226A011 C ou DL Configuration the Setup menu 7 8 The Service menu The Service menu of the main Setup menu is used for analyzer service and it requires a level 2 access authorization It includes sub menus from which you can enter or modify the analyzer s internal parameters This menu also comprises commands for software updating and memory content resetting downloading uploading data transfer from or to a PC The Service menu of the main Setup menu is explained in section 4 The Service menu of the Setup main menu page 4 65 7 9 The SL menu Level 3 access is required to access this menu It is for use by ISL only 7 10 The About FZP 5G2s menu The Station Version menu lets you access various items of information about your FZP 5G2s analyzer FZP 5G2s c ISL 2002 S N 214 Boot 400 DFFF 1 FFFF Software w x AAAA Txt y z BBBB Hardware C D 08 03 2003 E Figure 19 About NCK2 5G screen This menu supplies the following information from left to right and from top to bottom eThe name of the unit the creation year of this analyzer type and the serial number of this unit eThe bootstrap software version and checksum value the optional bootstrap software version and checksum value ew X y z The program software version and checksum value then the text software version and checksum value eC D
47. boratory Manager name Title Comments Date Signature 5 Analyzer measure printing 12 01 2004 16 05 ISL FZP 5G2s Software V 5 4 S N 214 Measures Sample temperature 21 1 C R 108 22 ohms A D 6821 Cooling 0 0 O Flags 00000011 Heating 0 0 0 Detection 9 pts Opacity 9 pts DOCV226A011 C FZP 5G2s User s Manual Page Appendix A 73 iSL 6 Internal parameter printing 12 01 2004 16 05 Internal parameters General setup Run setup Alarms setup Sample T t 125 C t 45 C 10s Laboratory setup Laboratory Manager name Printer setup Result printing Printer Deskjet color RS232 setup Transmitted data with the result On line NO Analyzer ID 1 Rate 9600 Data bits 8 End of transmission character 0 Time between two messages PC link setup On line NO Address 0 Date Time Setup Date DD MM YYYY Regulation parameters of the pump Kp1 2 5 Ki1 0 10 Kd1 0 0 Km 10 0 Sample Temp measurement calibration Calibration frequency 365 days 50 C 58 F 80 3120hms A D 35052 Sample probe correction table 100 C 0 0 90 C 0 0 60 C 0 0 50 C 0 0 20 C 0 0 10 C 0 0 20 C 0 0 30 C 0 0 60 C 0 0 70 C 0 0 Detection parameters SBd 25 CCd 10 CdmCo 40 SC2 3 Ofz 0 09 Abf 0 9 ISL 400 DFFF 1 FFFF 5 4 27F 5 4 57F5 Page Appendix A 74 ISL FZP 5G2s Software V 5 4 S N 214 Access level O Auto edition 2 Product 1 Buzzer modulation 3096 Cooling t1 1C m 120s t2 3 C m L
48. by activating the Lab menu Displays Meaning of different menus Field values Cab imonmprihassetup menu Going from left to right and from top to bottom Laboratory setup permanent field Access Code access code to level 1 Up to 6 characters Lab Name name of laboratory using FZP 5G2s String Laboratory setup D Access Code EA Lab menu display 1 Next display Laboratory setup permanent field Laboratory setup Manager name of laboratory manager String Title title of laboratory manager String Manager __ E Title Lab menu display 2 Table 7 Lab menu displays 7 5 Printer configuration the Printer menu Printer configuration has been dealt with in chapter 4 Printing and printer setup The Print menu page 3 41 of the current part 7 6 FZP 5G2s amp PC communication the PC Link and RS232 menus The FZP 5G2s is an open device in more than one respect Not only it is fully user definable but it can also communicate with a PC through the following facilities The RS 232C link connection of the Alan amp Input Output ports through a special adapter supplied refer to the section 4 3 3 2 page 1 20 The RS485 link connection to the Alan network refer to the section 4 3 3 1 page 1 19 The Service port rear panel of the analyzer see Picture 3 page 1 20 Each of these communication modes is specialized as follows The RS 232C link enables the FZP 5G2s to s
49. ct list to be displayed in order to select a product other than one selected by default at switching on Different parameters defined in the Run Environment menu refer to the Part 3 chapter 5 page 3 43 are associated with each of these products Activating the Product menu displays the screen below Select a product Figure 4 Product list display of the FZP pt Run Start menu The FZP 5G2s Analyzer can store up to 40 prestored products the black arrow in the top right hand corner of the screen indicates the presence of more lists following on Use the RIGHT and LEFT DIRECTION KEvs to move from table to table and scroll through the different pages of products To select a prestored product enable the corresponding field with the DiRECTION KEvs When the desired field has been enabled press the OK key to confirm the selection and return automatically to the FZP Pt Run Start menu The Other menu lets you create a new product to configure a test without using a prestored product but this new product will not be stored in the list of prestored products this operation requires level 1 Laboratory level authorized access This method is therefore recommended for one off tests only Press the OrHER key The screen 1 of the product Environment menu is displayed allowing configuring all parameters of a product Refer to the Part 3 chapter 5 Test setting and printing the Run Environment menu page 3 43 for the procedure to follow 2 2 Cha
50. detected Rate transfer rate in baud 9600 bd 9600 bds None Data bits data bits 7 8 Data Stop bits stop bits 1 2 a Bd E T Mill nov None RS232 menu display 4 Next display RS232 Link setup permanent field RS232 Link setup lt not detected gt Flow control flow control None None 0 1s RTS CTS 1me between Xon xoff Ra Bu ENQIACK Time between two messages when there is no transfer 0 10s RS232 menu display 5 protocol Table 8 RS 232 menu displays The results messages including the product if it is selected move on to screen 2 of the RS232 menu in the table above are transmitted in the form of a character string in ASCII code See Appendix B page 77 for the meaning of the content of the messages DOCV226A01 1 C FZP 5G2s User s Manual Page 3 53 7 6 2 Alan link setup the PC link menu When the input output ports of the Alan network link interface are connected the unit automatically detects the presence of the local network link cge Note The FZP 5G2s has been designed to run under ALAN management software developed by ISL refer to the section 4 3 3 FZP 5G2s PC link page 1 19 The parameters of this link are presented and fixed in the table opposite Displays Meaning of different menus Field values PE Fink mont onto Setup menu Going from left to right and from top to bottom PC Link setup permanent field Analyzer PC ID identifying name of PC on network Anal ias ea SERNER i
51. diagnostic sus 2 ADJUSTMENT THE QUALITY MENU 2 1 Sample probe correction table the Correct Table menu ss 2 2 Calibration of sample temperature measurement the Samp T Calib menu 2 2 1 Tools required uere tetro een enano cas isi eei erae 2 22 Procedure ces eee deett eb apte teer EO I Pe cei edebat terere eb eta edd 3 THE SERVICE MENU OF THE MAIN PRINTING MENU 3 1 Regulation monitoring ses 3 2 Ant rnal parameters ins eese Re eden Id d eleva EO Re er E 4 THE SERVICE MENU OF THE SETUP MAIN MENU 4 1 Entering regulation values the Regul menu sen 4 2 Entering calibration values the Calib menu ss 4 3 Entering detection values the Detect Menu sen 4 4 File download command the SL UDS menu 4 41 Transfer procedure nsi soisi teh et re tr ner E ERES RE ERR OO ORE ire o E P se ee ele 4 4 2 Installation and start up of the downloading program 4 4 3 User requested transfer 4 4 4 Transfer fails or screen not lit 5 MAINTENANCE 5 1 Control Unit housing cover disassembling 5 2 Location of the Acquisition Board sense Page 10 FZP 5G2s User s Manual DOCV226A011 C APPENDIX A PRINTING TYPE EXAMPLE SG ssccccssssscssssscccessssccecssssccesssccecssssccsessceccecsaceesssscceessneees 71 1 RESULT TICKET PRINTING DETAILED FORMAT WITH PRODUCT 73 2 PRODUCT PARAMETER PRINTING 73 3 OP
52. e printing The Service menu of the Print menu is designed for Analyzer maintenance and requires Level 2 access It contains submenus from which internal Analyzer measurements can be printed either instantly or during a full test run monitoring regulation or also the internal Analyzer parameters Refer to the Part 4 chapter 3 The Service menu of the main printing menu page 4 64 4 2 Printer setup The printer is configured by means of the Setup button of the Printer menu see Diagram 6 above Configuration can also be carried out by means of the Printer menu of the Setup menu screen 3 of the main screens level The following screens appear DOCV226A01 1 C FZP 5G2s User s Manual Page 3 41 Page 3 42 Display Meaning of different menus Field values Print menu of the Setup menu Going from left to right and from top to bottom Next display Auto automatic printing at the end of test Yes No Printer setup a Format printing format Curve Ticket Results printing configuration Complet Yes curee A Printer check Setup menu display 1 Content printing content Printer check starting of the printer test Detailed Light When the content is detailed the detailed values Cd Co and Do refer to the section 3 1 page 3 37 are printed with the result ticket or curve and parameters of the product profile used to carry out the test are printed on the result ticket Printer setup Deskjet color
53. e test the main screen level being explained in Part 3 We will further assume that the operator has taken due note of the care that needs to be taken with the substances tested ze IrIsE ZI Verson www isl france com 14790 VERSON Tel 33 2 31 26 43 00 FRANCE Fax 33 2 31 26 62 93 Francais FZP Pt Run Start menu Prod 1 By default ID Op Select a product 1 By default 6 j 7 3 5 8 4 9 5 10 Sample ID n INBCDEFGHIJKLMNOPQRSTUVWXYZ amp A bt abcdefghijkimnopqrstuvwxyz lt gt gt Select an operator name 1 21 3i 5 6 Ls 8 A 9 10 Diagram 1 Starting a test DOCV226A011 C FZP 5G2s User s Manual FZP Pt Run Display screen Prod 1 By default ID Status Cooling 26 0 C 24 01 2003 14 12 a Page 2 27 When the device is switched on the welcome display see Figure 2 page 1 23 appears After the language has been selected or any key pressed if the language has been locked the FZP Pt Run Start menu display directly appears thus refer to the Diagram 1 on the previous page Prod 1 By default ID Start Smpl ID now i Figure 3 Screen of the FZP pt Run Start menu There are two points to be made in this respect After switching on the device the display of the FZP pt Run Start menu above is obtained after the language has been chosen
54. earance are frank Freezing point is the temperature at which last crystals disappear during the reheating stage this value is determined by the detection signal gt Cd is the temperature at which the first crystal appears This value is determined by the detection signal gt Co is the temperature at which the sample becomes dark In Neat Fuels crystals apparition is very frank and the sample becomes nearly immediately dark Cd is almost the same as Co In Contaminated Samples Cd is detected much earlier as typically crystals of contaminant appear first At low levels of contamination concentration of such crystals is not sufficient for generation enough light for reliable Co determination Co will be detected when crystalline structure starts to be formed which correspond to beginning of aviation fuel crystallization the sample becomes dark gt Do is the temperature at which dark almost completely disappears detected by the Opacity signal In Neat Fuels Do is almost the same as Freezing point In Contaminated Samples Do responds only when the general mass of crystals has disappeared Due to still retained crystals of contaminant the real Freezing point according to method is significantly warmer than the less sensitive Do reading Nevertheless at low levels of contamination Do value can give obvious idea what might be the Freezing point of aviation fuel if it were not contaminated Printout of this additional information on t
55. earch The result is stored in the memory device Stop on stop temperature xx x The indication appears at the end of the test i e when the sample has reached the final temperature The alarm is stopped each time a test is run Page 3 48 FZP 5G2s User s Manual DOCV226A011 C ou DL Alarm treatment 6 5 4 Buzzer modulation setup Alarm displayed during the audio alarm test after modulation setting refer to the section 7 3 Configuring alarms the Alarm menu page 3 51 of the current part 6 6 Alarms historical The FZP 5G2s can register up to 16 alarm messages Activate the Review menu from the alarm displaying screen see Figure 17 page 3 46 the following screens appear Displays Meaning of different menus Field values Reviewsnenu Alarm displaying screen Going from left to right and from top to bottom Faults review Faults review permanent field Date Time Message registered Exit To go back to the alarms displaying screen Print To print the complete alarms review Details To display the detailed alarm message Display 1 of the Review menu Press the DETAILS key to access to the detail displaying screen of the alarm selected Date date at which the failure occurs Src state of the analyzer when the failure occurred idle Date Src run diagnostic Def Def alarm message displayed Exit to go back to the alarm displaying screen Details display the R
56. ee eee eee REPORT De ss PURPOSE wish to Report an error Submit a suggestion a comment Get more information In the area of Hardware Software Manual ANALYZER ENVIRONMENT please be complete e HARDWARE Type of Analyzer FZP 5G2s Senol N sans use ailes Options Parallel printer Graphic printer Plotter RS232C interface Current loop interface e SOFTWARE MISERE ATTACHED SHEETS Listing Diskette Drawing Text Other PROBLEM DESCRIPTION COMMENTS SUBMITTED BY Name Company Address Phone Fax Date Send this report to your local Sales office or to Groupe ISL Service Clients BP 70285 14653 CARPIQUET CEDEX FRANCE Phone 33 2 31 26 43 00 Monday through Friday from 9 00 a m to 5 00 p m French Time Fax 33 2 31 26 62 93 Web site www isl france com DOCV226A01 1 C FZP 5G2s User s Manual Page 5 Page intentionally blank Page 6 FZP 5G2s User s Manual DOCV226A011 C AVOM EXPOSURE laser radiation its emitted from the APERTURE Te DANGER LASER RADIATION AVDID INRECT EYE EXPOSURE LASER DIODE Wavelength 430 840 ni This ISL Analyzer has been carefully designed manufactured and inspected for quality It has been equipped with a number of safety features However the use of this Analyzer may involve the handling of solvents chemicals and other potentially dangerous flammable toxic etc materials Please exercise caution when
57. end among others test results in ASCII code to a PC or any other computer system LIMS for example The RS485 link enable the FZP 5G2s to be connected to the Alan network The Alan network enables if necessary several analyzers to be linked between us FZP 5G2s and others They are controlled from the host computer Page 3 52 FZP 5G2s User s Manual DOCV226A011 C ou DL The Service port enables the control software or the memory content to be updated by downloading and the memory content to be saved by uploading refer to the section 4 4 page 4 66 Parameters relating to each of these communication modes are explained below Configuration the Setup menu 7 6 1 RS232C link setup the RS232 menu If the RS 232C link is selected as means of communication mode you will first need the appropriate adapter see packing list shipped with the analyzer This adapter has two RS485 connectors on one side which must both be connected to the Input Output ports of the Analyzer s Alan network and an RS 232C connector on the other side which is connected to the PC refer to the section 4 3 3 2 page 1 20 for more explanations When the adapter has been connected the analyzer automatically detects the presence of an RS 232C link Then The RS 232C link is declared in service The RS485 link is declared out of service Parameters of this link are presented in the table below Displays Meaning of different menus Field values
58. er bit 7 6 5 4 3 2 1 and O Bit Significance Bit 0 1 Adjustment of the temperature measurement circuit have to be done Not used Not used Not used 4 1 Test performed with two cooling cycles Not used Not used Not used lOO Go Nh Oo Note When only the condition 2 cooling cycles occurs the warning binary message is not indicated on the curve because the message As dual cooling cycle was done Opacity signal is not available is clearly printed in the bottom right of the curve Page 3 40 FZP 5G2s User s Manual DOCV226A011 C ou Printing and printer setup The Print menu DL 4 Printing and printer setup The Print menu Main level screens FZP 5G2s S N 214 FZP 5G2s FZP 5G2s a a 214 Software V w x Detection Vy z Software V w x Detection oe Software V w x Detection vy d FREEZE Pt RUN Start LELEN eB Print Run envi Service J quality a Printing Diagram 6 The Print menu To access to the printing menu activate the main level Print menu the following display will appear as the Diagram 6 above describes it Printing Figure 13 Print menu screen The Print menu screen contains the following menus and commands eService To print the values of measurements and internal parameters level 2 access required eSetup To setup printing parameters eStop To stop the current printing job 4 1 Servic
59. esults displaying and printing The Results menu page 3 37 for the description of information supplied 2 3 3 End of test The end of the test will be indicated by a warning alarm when the sample temperature has attained about 12 C 1 The message End of test Freeze point detected indicates the Freeze point of the sample tested is obtained The result is displayed and stored in the analyzer memory device 2 The message End of test Freeze Pt not detected indicates the point at which the crystals disappear has not been found The FZP does not store any temperature the result display will not be displayed but the result is nevertheless registered 3 The message End of test Crystall not detected indicates that no crystallization had been detected Cd see Diagram 4 page 3 39 before the lower temperature set in the product run parameters is reached Then the Analyzer can not search the point of crystals disappearance but the result is nevertheless registered Press the ALARM Stop key on the keypad to display the alarm message and to acquit it These messages will be stored with the results in the memory device In few rare cases the FZP 5G2s can start a confirmation cycle so as to improve the result accuracy The indication Second cycle then appears on the Start now display replacing the sample temperature field see Figure 7 page 2 31 Then the test can last up to 30 min This will be signaled by a message on the re
60. eview menu Table 3 Screens of Review menu of the alarms displaying screen DOCV226A011 C FZP 5G2s User s Manual Page 3 49 au DL 7 Configuration the Setup menu Main level screens FZP 5G2s S N 214 FZP 5G2s S N 214 FZP 5G2s S N 214 Software V w x Detection Vy z Software V w x Detection Vy z Software V w x Detection Vy z R PT RUN Start MIELE FZP 5G2s S N 214 FZP 5G2s S N 214 FZP 5G2s S N 214 gt Analyzer setup Analyzer setup Analyzer setup Run Diagram 8 Setup menu The FZP 5G2s working environment can be completely configured Thus the testing product in place when the device is switched on can be re set The triggering or stopping of an alarm can also be set for when a given error occurs and in other conditions set out below as RS 232C PC link and Alan local network The configuration of the FZP 5G2s is carried out by means of the Setup main menu at the main display level see Diagram 8 above After the Setup menu is activated the following displays appear S FZP 5G2s S N 214 Analyzer setup General Run Alarms FZP 5G2s S N 214 Analyzer setup Cl DSC Se ES MAT LI FZP 5G2s S N 214 Analyzer setup C2 Service About FZP J Figure 18 Displays of the Setup menu The above displays allow access to the configuration parameters set out below Page 3 50 FZP 5G2s User s Manual DOCV226A011 C ou DL Configuration
61. formation organized into two displays Displays Measures menu Meaning of different menus Going from left to right and from top to bottom Measures Smp 20 0 C 0 1 c min 107 810 47084 Opt OFF Detection 7 Opacity 64 Cooling unit Heat 0 00000000 0 0 0 096 Measures menu screen Smp sample temperature C variation rate in temperature reheating or cooling resistance of sample probe Q analog digital conversion value Opt ON OFF functioning state of the optical emitter Detection Number of points received on the detection signal Opacity Number of points received on the opacity signal refer tot he section 3 13 37 for the optical detector functioning Cooling unit 0 Effective number of points applied to the cooling unit information given back by the compressor control board State indicators order D 76543210 DO reserved for ISL use D1 reserved for ISL use D2 reserved for ISL use D3 ventilation 12 ON 0 OFF D4 temperature alarm D5 optical stroke D6 maximum current D7 optical stroke fault 0 0 Power requested in percentage sent to the cooling compressor control board Heat 0 Effective number of points applied to the heating information given back by the control board 0 0 Power requested in percentage sent to the heating control board Print printing of two displays Table 11 Measures menu displays DOCV226A011 C Next dis
62. g to 110 C During this phase the values of temperatures to be noted are taken time required to fall to each notable temperature and effective number of points at this same temperature 3 Reheating return to ambient temperature The Print button allows a printout to be made of the cooling compressor parameters plus the values noted during phase two see above which can if necessary be sent to ISL s Customer Service for the compressor s condition to be checked The following table explains the cooling unit diagnostic procedure to follow Displays Meaning of different menus C Unit menu Going from left to right and from top to bottom Cooling unit diagnostic Empty the cell then press start Duration 80min max 10096 L3 Cool C Unit menu display Cool button for entering percentage cooling required 100 by default Start menu for running the diagnostic procedure Print printing cooling compressor parameters stored during the last diagnostic Table13 C Unit menu display of the Diagnostic menu Page 4 60 FZP 5G2s User s Manual DOCV226A011 C ou Adjustment the Quality menu ISL 2 Adjustment the Quality menu Main level screens FZP 5G2s S N 214 FZP 5G2s Software V w x Detection vy z FREEZE Pt Run er ae 214 FZP 5G2s S N 214 Software V w x er ae vy z Software V w x Detection Vy z Quality orrec amp alib ticKe D BEJG calib Printing
63. he current sample temperature given by the sensor in bold characters 2 3 2 Test in progress The FZP 5G2s will cool the sample down until hydrocarbon crystals appear When the optical detection cell detects the sample is dark the cooling phase stops The FZP 5G2s then starts to search for crystals disappearance point by heating the sample at a low rate When the point at which the crystals disappear has been found the message FREEZE Pt appears and the result is displayed Then the final phase of sample reheating starts the analyzer begins a faster warming up of the sample to reach the ambient temperature thus allowing a new test to be begun rapidly O 1 Samp Tmp 18 C FREEZE Pt 24 10 2002 14 12 Figure 8 End of test display in reheating phase To achieve a greater reliability in the result the FZP 5G2s continues for a moment to heat the sample at a cge low rate after finding the point at which the crystals disappear to satisfy itself that the point of disappearance of the crystals is indeed that found previously This being so the sample temperature display Figure 7 jumps to the End of test display Figure 8 DOCV226A01 1 C FZP 5G2s User s Manual Page 2 31 iSL The rapid warming up phase is indicated by the flashing of the green LED of the Stop Test key please refer to the section 6 2 page 1 23 The result is displayed in reverse video It is stored in the memory refer to the chapter 3 R
64. he result ticket or on the result curve is disabled in factory delivered FZP 5G2s units however an experienced user can enable these functions in the field refer to the section 4 2 Printer setup page 3 41 It s important to note that this additional information Cd Co Do is exclusive to ISL s FZP 5G2s design and detection technique and should be interpreted and applied by users at their own discretion These values are derived from a physical property of tested fuel and are therefore repeatable and reproducible however repeatability and reproducibility have not been defined ISL does not warranty correlation of these additional values to any known test method ISL however does guarantee reliable Freezing point value from the FZP 5G2s Page 3 38 FZP 5G2s User s Manual DOCV226A011 C ae Results displaying and printing The Results menu DL ISL FZP 5G2s S N 214 V5 4 12 01 2004 Date 05 01 2004 10 11 Op HC Product 1 Jet Al ID Jet A1 Freezing point 50 5 C Detection V5 3 Cd 54 1 C Co 55 6 C Do 50 6 C 1 1 sox Signal de d tection Signal d opacit A Do Freezing Pt d oM 10 10 30 50 50 46 30 Zo 10 o T c lt Re froid gt lt Chauf fage gt Diagram 4 Result curve of a neat sample ISL FZP 5G2s S N 214 V5 4 12 01 2004 Date 05 01 2003 10 37 Op HC Product 1 Jet A1 ID 2 Go Freezing point 37 0 C
65. ilures set off a continuous audio alarm and the red LED of the ALARM STOP key lights up on the keypad see in section 6 2 page 1 23 Press the ALARM STOP key to display the alarm message and acknowledge it or not The red LED stays on for as long as the failure persists even if the alarm has been acknowledged 6 1 2 Warning alarms The warning alarms warn the operator of an expected event End of test Freezing point detected for example They are accompanied as for them by a discontinuous audio alarm the signal modulation width is adjustable refer to the section 7 3 page 3 51 of this part The red LED on the ALARM SroP key lights up on the keypad It goes off when the alarm is acknowledged 6 2 Displaying alarms stopping the buzzer When an alarm is triggered press the ALARM Stop key to display the cause The following screen is displayed No alarm to signal Figure 17 Alarms displaying screen The alarms screen display contains the following menus and buttons V Exit to go back to the previous screen without acquitting the alarm Acquit to acquit the alarm and to go back to the previous screen Press the Acquit key to stop the buzzer and return to the previous screen Note that the red LED on the ALARM Stop key stays on for as long as the default persists even if the alarm has been acknowledged V Review to display the alarm historical 6 3 Alarm processing Certain alarm cases present a danger This is why most defaul
66. indicated by the probe reference value for temperatures from 100 C 148 F to 90 C 194 F with an increment of 10 C Sample probe correction table Correction Probe value reference 0 0 0 0 0 0 0 0 Cl eel mxfum mefurm AA Figure 25 Correct Table menu Display 2 2 2 Calibration of sample temperature measurement the Samp T Calib menu Calibration of the sample temperature measurement is done through the Samp T Calib menu of the Quality menu 2 2 1 Tools required Flat screwdriver 1 small 1 large A temperature check box PS100 2 2 2 Procedure 1 Switch off the Analyzer 2 Remove the Analyzer s cover refer to the section 5 1 Control Unit housing cover page 4 69 3 On the Acquisition board see Picture 7 page 4 69 disconnect the sample temperature sensor from the connection port J10 Use a small flat tipped screwdriver to move the small locking pin refer to the section 5 page 4 69 for electronic boards and port J10 location A 4 Connect the probe simulator connector to the free connection on port J10 5 Power on the Analyzer The connector and the wires of the sensor are extremely fragile Connection and disconnection must be made with extreme care CS Tum instrument on for at least 30 minutes to allow the electronics to warm up and stabilize 6 Activate the Samp T Calib menu of the Quality menu then follow the indications on the displays set out below Page 4 62 F
67. ions we recommend on receiving your Analyzer or before any modification is to print out all service parameters Keep this list to resort to it in case of problem Refer to Appendix A section 6 page appendix 74 for a printing out example of the Analyzer internal parameters A copy of the service parameters is also delivered with the Analyzer FZP 5G2s but it should be kept safe by the person in charge of the laboratory Page 4 64 FZP 5G2s User s Manual DOCV226A011 C ou DL The Service menu of the Setup main menu 4 The Service menu of the Setup main menu The Service menu is mainly dedicated to the Analyzer service and it requires having level 2 access authorization the Setup menu is explained in Part 3 o L2 e FZP 5G2s S N 214 FZP 5G2s S N 214 Software V w x Detection Vy z Software V w x Detection Vy z Main level screens FZP 5G2s S N 214 Software V w x Detection Vy z Pt RUN Start_JgDisplay FZP 5G2s S N 214 FZP 5G2s S N 214 FZP 5G2s S N 214 X Analyzer setup Analyzer setup Analyzer setup tabo RS2352 tobe Diagram 13 Setup menu This menu contains menus with which regulation parameters can be entered and setting values and optical detection instrument parameters be modified Regulation parameters and setting values are part of internal parameters They can be directly entered in this menu but it should be avoided modifying them without
68. is stopped Alarm is stopped each time a test is run DOCV226A011 C FZP 5G2s User s Manual Page 3 47 iSL 6 4 5 Heating circuit The system checks for this failure from the start of the test by verifying the heating rate The alarm is triggered if it is not sufficient The system cuts the heating command and stops a test being run The alarm is stopped each time a test is run 6 4 6 Sample temperature safety The system checks for this failure during the entire test The alarm is triggered if gt The sample temperature is higher than threshold by default 45 C programmable from 120 to 55 C during the recognition time programmable from 0 to 120s gt The sample temperature is lower than threshold by default 120 C programmable from 120 to 55 C during the recognition time programmable from 0 to 120s A test currently running is stopped Alarm is stopped each time a test is run 6 4 7 Cooling unit temperature safety This alarm is triggered if the cooling unit is above 48 C A test currently running is stopped In this case it is advised to gt Turn off the Analyzer gt Clean the ventilation filters Turn on the Analyzer If the problem continues contact ISL Customer Service 6 4 8 Cooling unit stroke control safety Contact ISL Customer Service 6 4 9 Cooling unit board link safety This alarm is triggered if no dialogue is detected with cooling unit co
69. isplays This requires authorization at Access 1 level Page 3 44 FZP 5G2s User s Manual DOCV226A011 C ou Test setting and printing the Run Environment menu DL 5 2 List of operator names Press the Operators key in the Run Environment menu to display the prestored list of operator names up to 10 the following screen is displayed Select an operator name Figure 16 List of operator names The Product menu screen contains the following menus V Print to print the list of operator names V Details to enter a new name or modify the name selected The Print menu lets you print out the complete list of operator names Press the Print key to start printing immediately See the sample printout in Appendix A section 3 Operator name list page appendix 73 Select a prestored operator name if you wish to modify it or select an empty field if you wish to create a new operator name Press the Details key the Operator text entry screen is displayed Enter the name see in section 2 2 3 page 2 30 for further details on using the text entry screen then press OK to confirm DOCV226A011 C FZP 5G2s User s Manual Page 3 45 ae DL 6 Alarm treatment 6 1 Types of alarm 6 1 1 Failure alarms The failure alarms warn the operator in the event of a malfunction Failure alarm detection has at least one of the following consequences eA test cannot be started eA test in progress is stopped These fa
70. it as shown below Shock absorber locking bolt Special storage panel for shock absorbers locking bolts Picture 1and 2 Locking unlocking the shock absorbers Page 1 18 FZP 5G2s User s Manual DOCV226A011 C er Unpacking and installation DL 4 3 Connections 4 3 1 Connection to the mains After unpacking the FZP 5G2s the different extensions need to be connected and it should be plugged into different networks and circuits see Picture 3 next page Regarding the connection of the FZP 5G2s to the mains it should be noted that the device is built to operate from 90 to 130 and from 100 to 240 Volts at 50 or 60 Hz in accordance with the majority of countries where the device is marketed The power cable corresponding to the country of sale is supplied with the device 4 3 2 Connecting the printer A parallel port is provided at the back of the analyzer for connecting a printer compatible with the Analyzer using PCL 3 or ESC P language with which to print out test results among other things A 4 3 3 FZP 5G2s PC link Caution The Analyzer and peripherals must be switched off before connecting any new peripherals The FZP 5G2s Analyzer is fitted as standard with an RS 232C interface and an RS485 interface 4 3 3 1 RS 485 serial link Connection to the ALAN Network The FZP 5G2s analyzers can be connected to the ISL Alan network Automatic Laboratory Analyzer Network with the ISL Alan software developed by
71. jdsip S Iejop HNS Y bBuifejdsip jjnsaye uolj2a as Jjnsay Burfejdsip S21NSE9UI uni ui JSOJ e uonoejos Aus aureu 40je10dQ uogoejes jonpo4g GI 4equinu ajdures Aus qi ejduies Burplejs jso ES SE Su93919S nu9ul UIEN Z A u0132838Q X M A JEMJJOS Ovz N S S29S dZ4 DOCV226A011 C FZP 5G2s User s Manual Page Appendix C 88 INDEX Page intentionally blank Page Index 90 FZP 5G2s User s Manual DOCV226A011 C ou Index Index Optical detection parameters 4 65 A Regulation parameters 4 65 4 66 Access code Text Numerical values 2 30 Level 2 4 65 Action chart 88 F Adjust Format Time Date 3 54 Date Time 3 54 ALAN 1 19 4 67 Alarm I Acknowledgement 3 46 Identification Default alarm 3 46 Operator 2 29 Modulation 3 51 Sample 2 29 Safe memory NVM 3 47 Warning alarm 3 46 Alarms Buzzer modulation setup 3 49 Cooling circuit 3 47 Cooling unit board link safety 3 48 Cooling unit temperature safety 3 48 Data memory Ram 3 47 End of test Crystall not detected 3 48 Freeze point detected 3 48 Heating circuit 3 48 Historical 3 49 Low battery 3 47 Processing 3 46 Sample temperature safety 3 48 Signal conditionning 3 47 Software memory PROM 3 47 Analyzer Address 3 54 Asterisk 3 37 B Button Delete 2 30 Insert 2 30 Level 1 Level 2 3 56 Oper 2 28 Product 2 28 Setup 3 41 Smpl ID
72. key to display the Operator name text entry screen Enter the operator name according to the procedure described below see section 2 2 3 on the next page After confirming the operator ID by pressing the OK key the initial screen returns automatically to the FZP Pt Run Start menu DOCV226A011 C FZP 5G2s User s Manual Page 2 29 iSL 2 2 3 Text entry display 2 2 3 1 Text entry On this screen the sample identifying name for example can be entered Values for the fields offered can be entered by means of the corresponding buttons Thus to enter the sample identifying name the Smpl ID button of the FZP Pt Run Start display is pressed The following display then appears Sample ID ABCDE FGHIJKLMNOPQRSTUVWXYZ 8 amp A abcdefghi jklmnopqrstuvwxyz lt gt Figure 6 Text entry screen The field concerned is the sample identifying name sample ID This display is typical of text entry displays It is found at all points and is essentially made up of two parts A variable part on the upper part of the display which is the name of the field A recurrent part whatever the field is consisting of an alphabetic table from which the characters to be entered are selected and three buttons OK DELETE and INSERT The characters are entered in the following way 1 On the entry display a black rectangle flashes on the first letter of the table A To select a letter use the direction keys on
73. ng that the level is written protected The main display of the Access menu shown below enables access to a given level or if necessary to zero level Current Access Level 0 Lab Service o T N CA BA Figure 21 Access menu display The digital access code is entered through the numeric segment If the code is correct access is achieved validation with the ENTRY key Page 3 56 FZP 5G2s User s Manual DOCV226A011 C Part 4 Maintenance of the FZP 5G2s Page intentionally blank Page 4 58 FZP 5G2s User s Manual DOCV226A011 C Measurement and diagnostic the Service menu ou DL 1 Measurement and uae the Service menu Main level screens FZP 5G2s Software V w x Detection Vy z FZP 5G2s FREEZE Pt Run SES LATE C Print_ Software V w x Detection Vy z UTEM ESS S N 214 FZP 5G2s ER awit 214 Software V w x eee awit vy z Setup _ Diagram 10 The Service menu Service Service Measures RETSTISERSTSE The Service menu is in great part dedicated to maintenance With this menu it is possible to Display measures amp Slave the main parts of the device Activating the Service menu calls up the following display Ya Service LS Measures Diagnostics Jj Figure 22 Service menu displays 1 1 Measurement displaying on the FZP 5Gs Analyzer the Measures menu The Measures menu in the Service menu gives access to the following in
74. ntrol board A test currently running is stopped gt Turn off the Analyzer gt Open the Analyzer and check the electronic boards connection refer to the section 5 2 page 4 69 Turn on the Analyzer If the problem continues contact ISL Customer Service 6 5 Warning alarms 6 5 1 End of test Freeze point detected The normal Freezing point is obtained The result is displayed and stored in the memory device The indication is displayed at the end of the test i e when the sample has reached the ambient temperature The alarm is stopped each time a test is run 6 52 End of test Freeze Pt not detected Detection temperature range was exceeded temperature of the end of the cooling phase set in the product profile without the Freezing point being detected the opacity temperature has been detected The FZP does not store any temperature the result display will not be displayed see section 2 3 2 page 2 31 but the result is stored in the memory device The alarm is triggered at the end of the test i e when the sample has reached the final temperature The alarm is stopped each time a test is run 6 5 3 End of test Crystall not detected The message Crystallization not detected indicates the sample temperature has exceeded the stop temperature set in the test product and the opacity temperature has not been detected Then the Analyzer could not search crystals disappearance point Check on cooling during opacity s
75. nual Page 4 65 on DL 4 1 Entering regulation values the Regul menu The regulation parameters can be entered directly in the screens of the Regul menu refer to the internal parameters list supplied with the analyzer S Note These parameters are factory set and they normally must not be modified 4 2 Entering calibration values the Calib menu If data are lost the calibration values can be entered directly on to the display below without prior adjustment Sample temperature calibration 50 C 58 F 50 C 122 F 80 3129 35052 119 411 52118 T rdum HOE HHS eo Figure 27 Calib menu display Modifying sample temperature adjustment values High and low reference resistance values are related to the adjustment of the sample temperature They are calculated by automatic adjustment and do not normally need modifying If these values are modified manually this is indicated by an asterisk on the display and on the results printout 4 3 Entering detection values the Detect Menu The detection parameters can be directly entered in the screens of the Detect menu refer to the internal parameters list supplied with the analyzer CE Note These parameters are factory set and they normally must not be modified 4 4 File download command the SL UDS menu The basic Analyzer is delivered with the ISL UDS PC program for downloading internal parameters from a PC file to the
76. old sample can be drained into a beaker Picture 4 Injecting the sample Picture 5 Recovering the used sample Refer to the section 2 3 page 2 31 for the complete initiating test procedure DOCV226A011 C FZP 5G2s User s Manual Page 1 21 di DL 6 The user interface 6 1 Front panel The front panel of the device appears thus S Activation keys for ine LC menus or buttons displayed on LCD LCD navigation key Keys Stop Reset and Alarm stop Numeric keypad and CANCEL and ENTER keys Direction keys FZP 5G2s Picture 6 Front panel 6 1 1 The LCD The front panel of the device therefore includes an 8 line LCD which may be represented thus Returns one level Button calling for in the display entry of a numeric hierarchy or alphanumeric value Previous display Next display Menu activated by key immediately below see Picture 6 Figure 1 General operation of display and menus On either side of this display two buttons make it possible to travel up and down the hierarchy of menus press the navigation keys see Picture 6 above corresponding to the NExT SCREEN and PREVIOUS SCREEN buttons see Figure 1 above to activate them In the lower part of the display there are four keys by means of which the menus displayed on the display can be activated 6 1 2 Backlight setting The LCD screen backlight is set by a combination of the ENTER key and the high Direction Key for less
77. or by pressing any key on the front panel if the language has been locked ce gt This screen is not placed hierarchically after the Welcome display The arrow on the left bottom of the display the PREVIOUS DISPLAY key see in section 6 1 1 page 1 22 allows backing up on the main screens level refer to the Part 3 chapter 2 The main level screens page 3 35 These measures have been taken to accelerate access to test related menus The FZP Pt Run Start menu display contains the following information eProd type of product tested selected by default at switching on eID identifying name of the sample eOp identifying name of the operator The FZP Pt Run Start menu display contains the following menus and buttons V Product selection of the product type and its associated run parameters used to carry out the test amp Smpl ID sample identifying name entry button V Oper operator name entry button amp Start now Start test button GE Note All these information are optional to start a Freezing point determination test Actually if the product selected by default at switching on is suitable for the specimen to be tested just start the test by pressing the Start now button Page 2 28 FZP 5G2s User s Manual DOCV226A011 C ou The first test DL 2 1 Selection of a pre installed product The Product menu of the FZP Pt Run Start display see Figure 3 on the previous page enables the factory pre installed produ
78. ortunity to thank you for choosing ISL product We are confident that you will be completely satisfied with your new Analyzer and we hope that you continue to call on us for all of your laboratory s petroleum testing needs Before you begin we ask you to take a few minutes to become acquainted with ISL and its history ISL s beginnings go back to 1975 when a group of engineers and scientists from the heart of the Northern France s petrochemical industry began seeking ways to automate petroleum testing The neighboring industry served as an excellent research and development proving ground for their new equipment By the end of 70 s several quality instruments had been developed and were being marketed in Europe under ATPEM Trademark The most famous of these new instruments was the CPP 97 Automatic Cloud and Pour Point Analyzer Introduced in the early 1980 s its successor the CPP97 6 revolutionized cold flow testing enabling up to six tests automatically and simultaneously Adding new automatic instruments each year ATPEM soon became a worldwide leader in automatic petroleum test instrumentation In 1986 they expanded operations reorganizing into the company now knows as ISL Striving to maintain close contact with customers in over 75 countries ISL has since grown founded Sales amp Service branches on each continent With design marketing service and support operating together under the ISL roof the company reached a new
79. photograph to locate the various components Acquisition Board Connector J10 adjustment of sample temperature Control Unit Board measurement circuit Picture 7 Internal topview of the FZP 5G2s Analyzer DOCV226A01 1 C FZP 5G2s User s Manual Page 4 69 Page intentionally blank Page 4 70 FZP 5G2s User s Manual DOCV226A011 C Appendix A Printing type examples Page intentionally blank Page Appendix A 72 FZP 5G2s User s Manual DOCV226A011 C ou Result ticket printing detailed format with product DL 1 Result ticket printing detailed format with product 12 01 2004 16 05 ISL FZP5G2s Software V 5 4 S N 214 10 04 2003 10 43 Op ML Prod 1 ID Freezing point 35 5 C Cd 45 6 C Co 74 2 C Do 68 7 C Detection V5 3 Product 1 Rounded Yes Stop 120 C 2 Product parameter printing 12 01 2004 16 05 ISL FZP 5G2s Software V 5 4 S N 214 Product 1 Rounded YES Stop 120 C 3 Operator name list printing 12 01 2004 16 05 ISL FZP 5G2s Software V 5 4 S N 214 Operators list 1 ML 2 GL 3 SL 4 LL 5 39XNO 0 4 Calibration ticket printing 12 01 2004 16 05 ISL FZP 5G2s Software V 5 4 S N 214 Calibration ticket Sample Temp measurement calibration Operator LL Calibration reference Calibration performed 07 01 2003 Next calibration 07 01 2004 50 C 58 F 80 3120hms A D 35052 50 C 122 F 119 4110hms A D 52118 Sample probe corr table Laboratory name La
80. play FZP 5G2s User s Manual Page 4 59 iSL 1 2 Diagnostic aid The Diagnostics menu of the Service menu can only be accessed by users with the level 2 access authorization service This menu allows the various FZP 5G2s power consuming devices to be slaved such as the cooling compressor the cell or the heating for the good operation to be verified Activate the Diagnostic key of the Service menu gives access to the screens below Displays Diagnostics menu Meaning of different menus Going from left to right and from top to bottom Measures Smp 20 0 C 0 1 c min 107 810 47084 Opt OFF Detection 7 Opacity 64 Cooling unit Heat 0 0 00000001 0 0 096 mifm BAe Diagnostic menu display Refer to the previous section 1 1 page 4 59 for explanations on the various information fields C Unit to access to the cooling unit diagnostic menu refer to the next section Cool to enter the power requested to the cooling compressor control board in percentage Emit to power on the optical emitter Heat to enter the power requested to the heating control board in percentage Activate the C Unit menu gives access to the cooling compressor diagnostic menu refer to the next section Table 12 Diagnostics menu displays of the Service menu 1 3 Cooling compressor diagnostic Diagnostics has three phases 1 Initialization heating to 40 C and regulation for 3 min 2 Cooling coolin
81. racterization of the test 2 2 1 Sample identifying Press the Sampl ID key of the FZP Pt Run Start menu see Figure 3 page 2 28 to complete the information regarding the sample identifying the Sample ID entry screen is displayed Enter the sample identification name according to the procedure explained in the section below see section 2 2 3 on the next page After confirming the sample ID by pressing the OK key the initial screen returns automatically to the FZP Pt Run Start menu 2 2 2 Operator ID Press the Operator key of the FZP Pt Run Start menu see Figure 3 page 2 28 to complete the information regarding the operator identifying A list of operator names is displayed Select an operator name Figure 5 List of operator names The FZP 5G2s can store up to 10 operator names If the desired name has already been saved enable the corresponding field with the DiRECTION Keys on the front panel and then press OK the initial screen returns automatically to the FZP Pt Run Start menu The Other menu lets you identify a new operator but not record the new identifying name in the list of prestored names this operation requires level 1 Laboratory level authorized access This method is therefore recommended for one off tests only To create a new name and save it to memory see Part 3 chapter 5 Test setting and printing the Run Environment menu page 3 43 Select a name or select an empty field then press the OTHER
82. s eRes Number of the result displayed over the number of results stored in memory an asterisk appears in front of the result number if the test was run although a default had been notified or if a default occurred during the test These defaults are not displayed but they are printed out with the result in the form of a binary message refer to the next section eDate and time of the end of the test eProd name of the product profile use to test the sample eID Identifying name of the sample eFreezing point Temperature of the point at which crystals in the sample disappear and the cause for test termination 2 other possible causes for termination can be displayed Freezing point not detected Crystal Not detected till _ The different types of test have been dealt in the section 2 3 3 End of test page 2 32 The end of a test triggers a warning alarm peculiar to each type of end of test Refer to the section 6 5 page 3 48 for more precise details about these alarm messages DOCV226A011 C FZP 5G2s User s Manual Page 3 37 The result display contains the following menus and button Print To print the result selected displayed and to access to the printer setup menu see next section V Transm Press the Transmit button to validate the result displayed and send it through the serial RS 232C link Parameters linked to this communication mode have to be set refer to the section 7 6 1 page 3 53 Messages are transmit
83. s the Analyzer will automatically detect a download request Also on powering up if the Analyzer screen does not light up the Analyzer will similarly detect a download request Power down the PC and the Analyzer Power up the PC and the Analyzer Run the downloading program as explained above section 4 4 3 page 4 67 If downloading is necessary the Analyzer will detect this automatically When the Analyzer is waiting for a download the red LED will flash every second A download in progress is indicated by rapid flashing which is related to the rate of data transfer Page 4 68 FZP 5G2s User s Manual DOCV226A011 C an Maintenance DL 5 Maintenance 5 1 Control Unit housing cover disassembling ADVERTISEMENT CAUTION Switch off the Analyzer and disconnect it from the mains before removing the housing If the service operations require you to switch on the Analyzer switch it off again before disconnecting or removing any electrically powered components e Switch off the Analyzer and disconnect it from the mains e Using an Allen key remove the 2 screws in low corners each side of the Analyzer and the screw above the screen e Grip the housing near the top between your two hands and pull towards the top to remove it CAUTION Replace the housing cover before switching on the Analyzer eProceed in the reverse order to reassemble the housing cover 5 2 Location of the Acquisition Board Use the relevant
84. sult curve and by a binary message on the result ticket refer to the section 3 2 page 3 40 The personalization of the parameters together with the display and printing out of test results will be dealt with in the second part of this manual 2 4 Cleaning the detection cell Cell cleaning is normally done with the next sample and a chase n flush technique It will be recalled however that the sample volume has been so calculated that the cell is cleaned by it But the detection cell will have to be cleaned from time to time or after running dirty samples or heavily contaminated jet fuel samples For this inject 10 ml of heptane do not forget to put a beaker at the appended tube end A CS Al solvents are prohibited they may cause deterioration of the cell Use only heptane Caution Do not use acetone Note If the cell is accidentally cleaned with a solvent this will be rapidly rinsed with an injection from 10 to 20 ml of heptane or kerosene Page 2 32 FZP 5G2s User s Manual DOCV226A011 C Part 3 Advanced use of the FZP 5G2s Page intentionally blank Page 3 34 FZP 5G2s User s Manual DOCV226A011 C ou DL Introduction 1 Introduction This part deals with the advanced use of the FZP 5G2s i e the setting of the device according to the needs of the user As previously indicated this presupposes that the user is familiar with the techniques of plugging tests The FZP 5G2s settings are accessible from
85. t refer to Appendix A page 71 for printing type examples It is also possible to print test results automatically after the end of the test refer to the section 4 2 Printer setup page 3 41 To be able to do this make sure that the unit is linked up to a printer compatible with the analyzer using PCL 3 or ESP P language and set on line From the display of the Results menu Figure 10 page 3 37 press the Print key the following display appears Results printing Start printing Print Printe Now Content Stop Figure 12 Print menu display of the Results menu This display contains the following menus and buttons eStart printing Now To start the printing of the selected result according to the printer setup ePrint content To define the data to be printed and to set the printer Pressing the Print Content button calls up the Setup menu of the Print menu Refer to the section 4 2 Printer setup page 3 41 Modify the printer setup requires having level 1 access authorization ePrinter Stop To stop the current printing Information like warnings occurred during a test just appears at result ticket printing These failures indicated at result displaying by an asterisk in front of the result number see the Figure 11 page 3 38 are identified by a binary message printed with the result at the bottom of the ticket or on the curve in the top left following the information Warning during test Displaying of bits in the following ord
86. t settings switch the Analyzer into idle status thus the cooling unit is cut out and the heating is stopped However this is not to say that this type of analyzer is hazard free or that if the Analyzer fails to go into idle status the operator and or Analyzer are not in danger It is important always to check what is going on whenever an alarm is triggered A For example owing to a faulty component an alarm that normally should place the analyzer in idle mode fails to do so In that case the operator must intervene by switching off the Analyzer Attention Generally when the alarm buzzer is triggered the operator must display the cause and ensure that everything is working correctly Page 3 46 FZP 5G2s User s Manual DOCV226A011 C ou Alarm treatment DL 6 4 Failure alarms 6 4 1 Memory failure When the analyzer is switched on the microprocessor checks the content of the different memories If there is an error it will be detected by calculation and comparison with the checksum 6 4 1 1 Software memory PROM failure If this failure is reported switch the analyzer off then on again If the failure persists contact the ISL Customer Service 6 4 1 2 Data memory Ram failure If this failure is reported switch the analyzer off then on again If the failure persists contact the ISL Customer Service 6 4 1 3 Safe memory NVM failure The battery for backing up the non volatile back up memory
87. ted in the form of character string in ASCII code refer to the Appendix B for the meaning of the content of the messages Details To display the result detail display Res 36 52 05 01 2004 10 11 Prod 1 Jet Al ID JET Al Freezing point 50 5 C Cd 54 1 C Co 55 6 C Do 50 6 C Figure 11 The Result Details display This screen contains in the upper part the same indications as the display of the Results menu and in the lower part 3 additional values that characterize the tested fuels cooling behavior Cd Co and Do resulting from the two signals supplied by the optical detection cell see the following diagrams ethe Detection signal allowing to determine crystals presence ethe Opacity signal allowing to indicate the sample opacity Therefore crystal appearance and disappearance in fuel sample causes typically two peaks in the FZP 5G2s Detection Signal its amplitude and width depend on size and shape of crystals as well as freezing rate of a particular jet fuel Neat jet fuels typically show narrow sharp curves see Diagram 4 below while contaminated fuels curve shape can vary widely as their inherent multi stage crystallization process generates a complex response curve formation see Diagram 5 below Like Detection Signal the form and amplitude of the Opacity Signal curve depend on crystal size and shape as well as the freezing rate of a particular jet fuel But generally speaking crystals appearance and disapp
88. the front panel Press the key as often as necessary or keep the finger pressed on it to indicate the direction of the character sought 2 When the flashing rectangle is positioned on the character sought press the ENTER key on the NUMERIC KEYPAD If the character is incorrect cancel it with the CANCEL key 3 If there is a mistake in the string of characters entered use the DIRECTION Keys and the Insert and Delete buttons to remedy it 4 Finally validate with the OK button of the text entry display Proceed in similar fashion for the operator name Ee Note To speed up the test run procedure the text entry screen has a semi automatic input feature After validating the initial display returns automatically in this case to the FZP Pt Run Start menu The same is true at each entry of text variables by means of the text entry display 2 2 3 2 Assisted edition To speed up test starting the text entry screen enjoys a semi automatic input feature the latest text inputs are stored in memory so that the operator only needs to enter the first two or three characters for the whole to be displayed If the function Auto Edition is activated the Analyzer proposes a suite when characters are entered according to prior enters This function is intended for accelerate test initiating and it can be configured or deactivated refer to the section 7 1 Power on parameters the General menu page 3 51 Page 2 30 FZP 5G2s User s Manual DOCV226A011
89. the main screens level see the Diagram 2 bellow 2 The main level screens Ise Zi Verson www isl france com 14790 VERSON Tel 02 31 26 43 00 FRANCE Fax 02 31 26 62 93 Fran ais FZP 5G2s S N 214 FZP 5G2s S N 214 FZP 5G2s S N 214 Software V w x Detection y z Software V w x Detection y z Software V w x Detection y z FREEZE Pt Run Site MOuESE XS a OT EX RUES C Setup _ Main screens level CS FZP Pt Run Start menu Prod 1 By default ID Op Start smpi ID now Diagram 2 Access to the main display level The main level display is the highest hierarchically speaking It is not directly accessible when the unit is switched on To access it after switching on the unit and selecting a language or pressing any key if the language has been locked it is necessary to go up one display level press the RETURN ONE LEVEL UP button see in Part 1 section 6 1 1 page 1 22 The Diagram 2 above shows how access to this level operates refer to the Appendix C page 85 for a complete view of menus functionality elf the user has operator level access access 0 a simple menu is available gt A test can be started and followed gt A result and result details can be displayed and printed Users with laboratory access 1 or service access 2 level access have a complete menu 0 0 0 DOCV226A011 C FZP 5G2s User s Manual Page 3 35 FZP 5G2s S N 214
90. tion mechanism into an ultra compact easy to use instrument that s ready to work whenever and wherever you are The unit automatically controls cooling and heating of specimen and uses optical detectors to monitor appearance and disappearance of hydrocarbon crystals Selfcleaning operation speeds and simplifies testing while novel detection cell based on patented laser beam technology assure testing of difficult and contaminated samples and assure low temperature flow performance of aviation fuels The ISL FZP 5G2s analyzer complies with ASTM D7153 and IP 529 standard methods now included in MOD Def Stan 91 91 issue 5 Jet Fuel specification and test data obtained are in correlation with ASTM D2386 IP 16 ISO 3013 and JIS K2276 standard methods ISL has taken great care with the design and manufacture of this device and hopes it will give you every satisfaction 2 2 Technical specifications 2 2 1 Operation in ambient conditions Operating temperatures 15 C to 35 C Storage 20 C 4 F to 40 C 104 F 2 2 2 Features Patented built in cooling system Self contained operation no external connection necessary Temperatures range down to 120 C 184 F Temperature measurement Direct specimen temperature control Measuring instrument Pt 100 IEC 751 probe class A Resolution 0 1 C 0 1 F Stability 0 5 C Detection ISL c patented optical detection cell CAUTION Laser radiation
91. urve form from left to right Message T Field Format Numbers of Comments Characters Analyzer no de 00 a 99 2 Message type string 2 T test product Product name string 12 Temperature unit 00 or 01 2 0 C1 F Type of analysis 00 2 Reserve 99 2 Reserve 999 3 Reserve 999 3 Reserve 9999 9 6 STOP temperature 999 9a 6 9999 9 Reserved 99 a 999 3 Reserve 999 Rounding of result 00 or 01 2 0 No 1 Yes 5 5 RS232 link test message ISL FZP 5G E5 6 RS232 cost There is neither option nor extra fee for RS232 software and hardware including the RS485 RS232 cable adapter which is provided as standard Page Appendix B 84 FZP 5G2s User s Manual DOCV226A011 C Appendix C Sequence charts Page intentionally blank Page Appendix C 86 FZP 5G2s User s Manual DOCV226A011 C Test launch diagram DL 1 Test launch diagram I S L zi verson ww isl france com 14790 VERSON Tel 33 2 31 26 43 00 FRANCE Fax 33 2 31 26 62 93 FZP 5G2s S N 240 E FZP 5G2s S N 240 FZP 5G2s S N 240 oftware V w x Detection Vy z A Software v w x Detection vy z Software v w x Detection vy z FREEZE Pt Run start CEE Print Run env Service RUES Main screens level FZP Pt Run Start menu Prod 1 By default ID Op XK A I By default 6 Zi 8 9 10 Select a product Sample ID CDEFGHIJKLMNOPQRSTUVWXYZ
92. ween 2 entire messages not between characters Existing signals defined in the RS232C interface standard are used to control the transmission Connect the host computer serial RTS signal to the analyzer CTS signal When the input buffer of the host computer is full the RTS signal changes its state Seeing its CTS signal changing the analyzer stops transmission until CTS changes again Note This hardware handshake is controlled by the communication hardware devices and can stop restart transmission between any characters This well known handshake is qualified as software protocol because it is controlled by the host computer reception software to control the data flow If the software needs time to process the last incoming message it can send the Xoff character to the analyzer which immediately stops the transmission until it receives from the host computer the Xon character This is a full protocol It allows flow control and data acknowledgment The transmission is fully controlled by the host computer which must send an ENQ enquiry character Any message must be acknowledged by the host computer by sending a ACK character Note There is no need to define a time between messages because the message sequencing keeps pace with the ENQs sent by the host computer Xon 11H Xoff 13H Developed by ISL this protocol is detailed below FZP 5G2s User s Manual Page Appendix B 80 DOCV226A011 C ou EN
93. when open the detection cell Disconnect the analyzer from the mains DO NOT STARE INTO BEAM CONSEQUENCES COULD BE IRREVERSIBLE The use of optical instruments with this product will increase eye hazard The FZP 5G2s is equipped with Class IIIA laser detection cell As the laser beam used is harmful to eyes do not attempt to disassemble the cell Refer servicing to qualified personnel only 2 2 3 Power supply Mains power supply 100 240 VAC 50 60 Hz Wattage 150 W 2 2 4 Dimensions Dimensions 250 mm I x 620 mm L x 390 mm H 18 W x 25 D x 18 H Weight 26 Kg DOCV226A011 C FZP 5G2s User s Manual Page 1 17 ae DL 3 Care in use 3 1 Care in the use of testing and cleaning equipment It is supposed that operators are familiar with the handling of hydrocarbon products and that they are thus aware of the dangers and risks that attach to them 3 2 Precautions to take when using built in cooling Analyzers Built in cooling Analyzers comprise a cooling compressor that necessitates several special precautions to be respected for the long life of the Analyzer and its optimum performance eAvoid using the Analyzer on a vibrating surface Surface vibrations can enter into resonance with those of the compressor and cause damage to the Analyzer eThe optimal operating temperature for the Analyzer is around 20 C To avoid harmful overheating of the unit 1 Keep the rear of the unit clear to allow heat to escape e
94. y be created or modified if one has the level 1 access authorization Laboratory Access to the run parameters of a product profile as follows 1 Enable the Run Environment menu on screen 2 of the main level screens see Diagram 7 above The following screen is displayed Run environment programming L3 Product oper Figure 14 Run Environment menu screen The Run Environment menu screen contains the following menus V Product to display the prestored products list to print modify or create of a new product profile Oper to display the operator names list to print modify or create a new operator ID cge Values in the fields of the Run Environ menu screen cannot be changed without level 1 access password Laboratory DOCV226A011 C FZP 5G2s User s Manual Page 3 43 5 1 Run parameters of a product Press the Product key in the Run Environment menu to display the list of prestored products the following screen is displayed Select a product Figure 15 Product menu screen The Product menu screen contains the following menus V Print to print run parameters of the product selected The Print menu lets you print out the run parameters for the product selected Press the Print key to start printing immediately See the printout example in Appendix A section 2 Product parameter print page appendix 73 V Details to access to the product setup menu see table below The FZP 5G2s Analyzer c
95. yzer When the PC software considers the downloading is finished it validates this with a signal to the Analyzer 4 4 2 Installation and start up of the downloading program See instructions in the ISL UDS software Read me file Page 4 66 FZP 5G2s User s Manual DOCV226A011 C F3 DL The Service menu of the Setup main menu 4 4 3 User requested transfer Preparation Power down the PC and the Analyzer and plug the cable into the SERVICE port connector at the back of the Analyzer and the serial port of the PC ePower up the PC and the Analyzer Analyzer eSelect the ISL UDS menu from the Service setup menu refer to the Table 15 page 4 65 Data uploading and downloading commands are accessible from the following screens Screen Meaning of the different menus ISL UDS menu of the Service Setup menu from left to right and from top to bottom Upload Download FZP 5G2 Analyzer software upload download FZP 5G2 Analyzer software FZP 5G2 software download control software download code and text FZP software Download ISL UDS menu screen 1 Next screen Internal parameters upload download Upload Download Download from to download a PC file Internal parameters PC to download the whole content of the Analyzer non volatile back Download from Upload to P up memory the content depends on the command used during the Run env All upload see below ISL UDS menu screen 2 Upload to PC Run
96. zer modulation setup eder ere te eter eaten ed or epe open in eee eqs ies 6 62 Alarms historical oe teer eer dee EO e pv rare DR Eee e ee p nd e e easier 7 CONFIGURATION THE SETUP MENU 7 1 Power on parameters the General menu ss 3 51 7 2 Run parameters the Run meri cte eant eroe ree B D EE RES PRSE ER Lee DIE E EEEE E 3 51 7 3 Configuring alarms the Alarm menu ss 3 51 7 4 Personalization and access authorization to level 1 the Lab menu 3 52 7 5 Printer configuration the Printer menu E UE 3 52 7 6 FZP 5G2s amp PC communication the PC Link and RS232 menus essssseeseeeeeeenen nennen 3 52 7 6 1 RS232C link setup the RS232 menu ses 3 53 7 6 2 Alan link setup the PC link menu ss 3 54 7 7 Date Time setting the Clock menu TER INEM Servicer Menu sos oo Mesa src Mecum d eL Oo LN T d tt 7 97 The JS E menu eterne ere de RBS HE P ur Marne etes Ramadan ares EE TAOS The About EZP 5 G2s nent repetere eee eee gene en ere ser ene get ee dere e pe ea Pepe E pee nt dee ta pred na Dade 8 ACCESS LEVELS AND PASSWORD THE ACCESS MENU PART 4 MAINTENANCE OF THE FZP 5G2S eee eee esee ee seen eene nennen natuss ta sets seasons sensns sense enne 1 MEASUREMENT AND DIAGNOSTIC THE SERVICE MENU 1 1 Measurement displaying on the FZP 5Gs Analyzer the Measures menu 1 2 Diagnostic adress nent eae tle he e e e esten orbit endet 1 3 Cooling compressor

FZP 5G2s User's Manual - John Morris Scientific

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