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        Kodak D-31 User's Manual
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1.          Ls  16  Table 3  Storage Temperature and Relative Humidity            17  Summary of Requirements for Storage and  Preservation of Records on Kodak Microfilm              Lun  17  Storage Facilities ie reder ah ad aac Rd Po e BARCA UR ede deg 17  References and Bibliography                  00  cece ee eee 18       D 31 June 2002    Introduction    Photographic film remains an important  documentary material  The increasing quantity  and value of microfilm records used in financial  institutions  libraries  government offices  and  industrial firms have focused attention on the  care of such records to make certain that they  last as long as possible     The distinction between photographic film records  intended for storage and those intended for use  has not always been clear  Use or work copies  are the predominant photographic records found  in libraries or record centers and are subject   to much handling due to their value as quick  references  However  because of this handling   they are subject to dirt  abrasion  fingerprints   contamination with foreign materials  and  exposure to excessive light  temperatures  and  harmful atmospheric pollutants  As a result  these  copies in daily use cannot be considered suitable  for long term preservation  For long term storage   itis imperative to prepare duplicate copies that  meet certain criteria  such as proper filming   duplicating  processing  minimum handling   controlled environment  and storage     In general 
2.        on Acetate Base    Methylene Blue Method      IT9 17   ISO 18917   Specifications for Thermally IT9 19   Processed Silver Microfilms  ISO 18919   Specifications for Stability of IT9 5   Diazo Films      ISO 18905   Specifications for Stability of IT9 12   Vesicular Films    ISO 18912     Practice for Storage of IT9 11  IT9 11  IT9 11  IT9 11   Photographic Film  ISO 18911 ISO 18911 ISO 18911 ISO 18911                D 31 June 2002    15       Table 2  Storage Life of Microfilms       Film Type Parameter    Anticipated Storage Life       Medium Term   Minimum of 10 Years     Extended Term   Minimum of 100 Years     Long Term   Indefinitely        Silver Gelatin Films  Residual Hypo    Residual Silver Salts     1    2     Not above 0 030 grams  per square meter  1        Not above 0 014 grams  per square meter  1        No more than perceptible tint by spot stain test           All Films     Storage Conditions  Temperature and   Relative Humidity    See Table 3       Air Conditioning    Not necessary  unless film records  are subjected to  frequent or sustained  high humidity  3     Essential   including slightly positive air pressure        Air Purification    Normal    and other contaminants     Must be free from airborne gases  dirt particles                    Enclosures Not necessary with If proper humidity control is provided  plastic or  moisture control metal  unsealed  can be used   and or air conditioning      If adequate humidity control is not available  only
3.       Thermally Processed Silver Microfilm   Specifications  for Stability     ANSI NAPM IT9 19 1994 or ISO DIS  14806 1996     26     The Effects and Prevention of the Vinegar  Syndrome     A  Tulsi Ram  David F  Koperl   Richard C  Sehlin  Stephanie Masaryk Morris   James L  Vincent  and Paige Miller  Journal of  Imaging Science and Technology  Vol  38  No  3   249 261  May June 1994     27     Use of Kodak Brown Toner to Extend the Life of  Microfilm     Eastman Kodak Company  Kodak  Publication No  A 1671     T Available from the American Society of Heating   Refrigerating and Air Conditioning Engineers   1791 Tullie Circle NE  Atlanta  GA 30329 2305     All ANSI Specifications are available from American  National Standards Institute  Inc   11 W  42nd St    New York  NY 10036 or http   www ansi org     All AIIM Standards are available from Association for  Information and Image Management  1100 Wayne  Avenue  Suite 1100  Silver Spring  MD 20910 or  http   www aiim org     Kodak Publications are available by calling  1 888 247 1234        D 31 June 2002    EASTMAN KODAK COMPANY  Document Imaging  Rochester  New York 14650    www kodak com go docimaging    Kodak  Eastman  Estar  and Prostar are  trademarks of Eastman Kodak Company     KODAK Publication No  D 31   CAT No  811 6386 6 2002   OEastman Kodak Company  2002   Printed in U S A   DOCUMENT  IMAGING       
4.   inert desiccates should be used  and  itis essential that the system be designed so  that particulate material cannot enter the storage  area  The use of molecular sieve packets is  recommended  as this is an efficient desiccant   Chemically pure silica gel may also be used as  a desiccant  provided that filtration is used to  remove particle layers larger than 0 3 micron   See ANSI PIMA IT9 11 1998 and ISO 18911   1998  or their latest revisions     Moisture Tight Containers   If humidity control of the storage area is not  possible  the storage of film in moisture tight  containers is required to maintain the film s  humidity limits  The film must be conditioned to  the required humidity before being sealed in the  container  This requires the temporary use of an  air conditioned cabinet or room  or an electrical  dehumidifier  Smaller quantities of film can be  conditioned for two or three weeks in a desiccator  containing activated silica gel  and then removed  and quickly sealed     Only properly sealed metal or glass containers  are considered moisture  and gas proof  They  are preferred when long term air conditioning is  not practical  when gaseous impurities may  regularly be present  or when low temperature  storage is used     Plastic boxes  such as Kodak Microfilm Plastic  Storage Cartons  CAT No  108 6867   16 mm   CAT No  841 8741   35 mm   can be used as  protective containers in controlled areas  They  provide satisfactory protection against short term  prob
5.   metal or glass sealed containers are acceptable   NOTES      1  Expressed as thiosulfate ion      2  Specific limits have not been set   the recommended washing should be satisfactory      3  Dehumidification may be necessary even though automatic air conditioning is not practical        D 31 June 2002    Summary of Requirements for  Storage and Preservation of  Records on Kodak Microfilm    Storage Facilities    The type of storage vault  safe  cabinet  or area  selected must be based on the value of the film  records and their intended storage life  In general   one roll per container is recommended   Containers should be stored in metal cabinets   Cabinets should be spaced in the room so there  are no stagnant air pockets or localized areas  where temperature and humidity may reach  higher levels than the general condition  If  humidity is not controlled  sealed metal or glass  containers are required     Although the same general storage principles  apply to medium term and long term storage  records  much greater care must be taken to  obtain maximum protection for long term storage  records  makeshift or temporary arrangements  should not be considered     In summary  Table 3 indicates the conditions that  are considered suitable for black and white silver   gelatin  thermally processed silver  diazo  and  vesicular Kodak Microfilms     Table 3  Storage Temperature and Relative Humidity                                                    Extended and Long Term Medium T
6.  18911  and ANSI PIMA   T9 2 19919  ISO 18903      Theft Protection    Safes provide good protection against the theft of  valuable records  Where such records are large in  number  vaults of burglar proof construction may  be required  Theft of important records involves  double peril   that of classified films falling into  unauthorized hands and the complete loss of  valuable information  Protection against the latter  can  of course  be provided by storing duplicate  records in another location        D 31 June 2002    Processing for Permanence    Silver Gelatin Films    Processing is one of the most important  factors affecting the potential permanence of  photographic records  The removal of residual  processing chemicals  the exclusion of dirt  contamination  and uniform drying are factors  normally controlled by proper processing     Processed film  for long term storage or  permanent records  must meet the requirements  of ANSI PIMA IT9 1 1992  R1996  or ISO 18901    The ability to meet most of these requirements is  controlled in film manufacture  but films must be  fixed and washed adequately  whether given  conventional or full reversal processing  to meet  residual thiosulfate requirements  Films  processed without fixation  such as in halide   reversal processes and certain reversal  processes with only redevelopment  may give a   visible  usable image   but do not come under the  scope of the long term storage standards     If fixing and washing are inadequate 
7.  Bie Fe RU Re eg dre e 10  Metall iiu ere grex PRI REND Een ERO NP Ae 10  Adhesive         e ees 10  Printing  INKS  eos md xe n pet oot Be ew ere E DOE eus Bee Ri 10  Theft Protection ice rero exe hte RIT ene 10  Processing for Permanence                00 cee eee eee eee 11  Silver Gelatin IIMS  54 42 52 aen wee  trae inei eR e ER ren bcne 11  FIXING Baths 5 danses a e ito UR Sab Oe rice MEALS DA Au 11  WASH  suite oRA ERA e bore eis dux edes s A ERN MM 11  SGUBegBBS  63 ecc Exo b pa a hd Se a acea Pad S guter ita es 12  DIVING  cuc ri eer I nce an Rr RU eo ek SERT tet 12  Washing AIdS oues uot Soie quU eoo Dose A Ud aU ra ded 12  Residual Hypo Tests eire aee OP PE Loe epee ES 12  Residual Silver Compound Test                00000 eee 12  Protective Coatings wor woe EE ux REY RA cee hee EE 12       Processing of Other Film Types               slsleeleseeeess 13    Thermally Processed Silver  TPS                  Llsusus  13  Diaza  FUIMS a yesi sn asi aye Ur RSS ad Mea ae a es 13  Vesicular Films                lulii  13  Special Storage and Hazards              0 0  c eee eee ee 13  Underground Storage 4L asana aane 13  Effects of Nuclear Explosions               00000 13  Time Capsule Storage        ee anaana 14  Handling and Filing Film Records                sselllssssse 14  BITTEN  yh CHE EI PC  rM 14  Ir SDOGOFT  rues dee x b pea ie I aque xb Ea RR S 15  Table 1  Applicable Standards for Microfilm                   15  Table 2  Storage Life of Microfilms              
8.  Standard     Imaging Materials     Ammonia Processed Diazo Photographic Film     Specifications for Stability     ANSI PIMAIT9 5 1996 or  ISO 18905     5  American National Standard     Imaging Media     Processed Safety Photographic Film   Storage      ANSI PIMA IT9 11 1998 or ISO 18911     6  American National Standard     Imaging Media     Photographic Processed Films  Plates  and Papers     Filing Enclosures and Storage Containers       ANSI IT9 2 1991     7  American National Standard     Protection of Records      ANSI NFPA 232 1995     8  American National Standard   Installation of Air  Conditioning and Ventilating Systems   ANSI NFPA  90A 1996     9  American National Standard   Tests for Fire  Resistance of Record Protection Equipment    ANSI UL 72 1990     10     Prevention and Removal of Fungus on Prints and  Films   Eastman Kodak Company  Kodak Pamphlet  No  AE 22     11     Inspection of Processed Photographic Record Films  for Aging Blemishes   C  S  McCamy  National Bureau  of Standards Handbook 96  January 24  1964     12     Microscopic Spots   A Progress Report   D  G  Wiest  and R  W  Henn  National Micro News  70  249257   June 1964    13     Microscopic Spots in Processed Microfilm   Their  Nature and Prevention     D  G Wiest and R  W  Henn   Photographic Science and Engineering  7  5    253 261  1963     14     Microscopic Spots in Processed Microfilm  The Effect  of lodide     R  W  Henn  D  G  Wiest  and B  D  Mack   Photographic Science and Enginee
9.  The life expectancy of your microfilm  processed  to established quality control standards and stored  under ideal environmental conditions  can be  many years  However  we do not have control of  environmental surroundings at all times     Therefore  you should consider taking the extra  precaution of toning your films against oxidative  attack  Toning can be accomplished by use of  sulfide toning agents such as Kodak Brown Toner   Other types of toners  such as selenium or gold   are also accepted but not commonly used   ANSI PIMA IT 9 1 1998  ISO 18901  now  recognizes that films toned with toners like   this can still be considered to meet the standards  for records of permanent or long term value   Brown toning is a service offered by the   Kodak Disaster Recovery Laboratory    The lab can be reached at 1 800 EKC TEST   1 800 352 8378  or 1 585 253 3907        D 31 June 2002    Chemical Contamination    Air contaminants may add an oxidizing or  reducing effect to the atmosphere  This in turn  may cause deterioration of the film base and a  gradual fading of the photographic image  as  well as the formation of the microscopic blemishes  mentioned above  Typical contaminants are   paint fumes  peroxides  nitrogen oxides   hydrogen sulfide  sulfur dioxide  and similar  gases  If an area is to be painted  any films stored  there should be removed beforehand and should  not be returned to the area for three months    The removal of contaminating gases from the   air requires
10.  air should be filtered to remove dust   cleansed of gaseous contaminants  if present   and controlled to the desired relative humidity and  temperature  Slightly positive air pressure should  be maintained within the storage room or vault   Film should be conditioned to this environment  and then placed in containers     Where air conditioning is not available and high  humidities are likely to be present  the humidity  of the storage area can be lowered by electrical  refrigeration type dehumidifiers  These are readily  available and inexpensive  The storage space  should first be vapor sealed by covering the walls  with asphalt or aluminum paint or  better yet   paper laminated aluminum foil or other water   vapor barriers  Painting the storage area is  suggested  but follow the painting precautions    A humidistat set at the desired level of humidity  should be used to control the dehumidifier  The  humidity level should be checked frequently with a  reliable hygrometer  such as a sling psychrometer   For added protection against short term moisture  effects  such as dehumidifier failure  tape the  containers as described in the following section    Moisture Tight Containers      Dehumidifiers using desiccants should be used  with caution  They may create a danger of fine  dust particles getting on the film and causing  abrasion when the film is used  Also  when some  chemical desiccant particles are trapped in rolls  of microfilm  they may form bleached spots   Therefore
11.  not be markedly different  from that of the storage area  Very large humidity  differences may lead to some physical distortion   The best relative humidity for storage is the  lowest that can be achieved practically and  controlled reliably  within the limits specified   in ANSI PIMA IT9 11 1998 and ISO 18911  or  their latest revisions        D 31 June 2002    High Humidity   Storage in moist air  such as that frequently found  in basement rooms  and storage humidities above  5096 should be avoided  relative humidities of  4096 or less are recommended for minimizing the  possibility of growth of microscopic blemishes    At humidities above 60   there is the additional  danger of fungus growth           Moisture  percent dry base     Estar Base             Relative Humidity  percent     These curves show the relationship between relative  humidity and the moisture content of a typical emulsion   triacetate film base  Estar Base  and a complete film at  equilibrium of various relative humidities at 21  C  70  F      Low Humidity   At low humidities  problems of brittleness or  static might arise if the films are to be handled  frequently  However  in the case of inactive  films  regardless of their intended permanence    the increased protection that low humidity gives  against microscopic blemishes might be  desirable  The recommended humidity is   30  for silver gelatin polyester base film and  15  for silver gelatin acetate base film and all  other silver and non silver f
12.  peroxides  ozone   nitrogen oxides  oil based paint fumes  organic  solvents  floor cleaning agents  cardboard  cartons  excessive temperature and humidity    or a variety of other materials that generate  peroxides which attack silver microfilms     The use of low concentrations of potassium  iodide in the fixing bath  0 2 g L  has been  recommended and has been found to provide   a good degree of protection against these  blemishes    Kodak Microfilm and Prostar Fix  Solutions contain this stability enhancing iodide     Once the deterioration of the microfilm occurs   it cannot be reversed  Silver film duplication   Kodak Brown Toner  and the use of molecular  sieves can be used to stabilize the reaction        D 31 June 2002    The conditions under which microfilm is stored  have been found to play an important role in  the development of microscopic blemishes   Storage in cool  dry air that is free of oxidizing  gases or vapors is an effective means for  arresting their formation and growth  Storage  in sealed  metal cans is a sound preventive  measure  if this is practical and consistent with  the humidity requirements     Additional protection can be obtained by adding  molecular sieves to the storage containers   or toning the film with toners such as Kodak  Brown Toner  CAT No  146 4452   8 oz     CAT No  140 0928   1 gal    For information  about the use of brown toner as a treatment   to extend the life of microfilm  order Kodak  Publication A 1671        Toning   
13.  special consideration 5 1 1516 17    Contaminants can come from illuminating gas   coal gas  automobile exhaust  and certain  chemical plants  They are present in harmful  concentrations in most industrial and urban areas   Other contamination can come from ozone and  ammonia produced by certain photocopying  devices  For this reason  a long term storage vault  should be located as far as possible from such  areas  When a contaminated atmosphere cannot  be avoided  steps should be taken either to  eliminate the fumes by air conditioning the  storage area or to protect the film from contact  with the atmosphere by sealing it in containers     In addition to atmospheric contaminants  care  should be taken about other materials kept or  used in the storage area  It has already been  mentioned that nitrate base films should never be  used for permanent record films  Furthermore   such films should never be stored with safety film  records  either in the same room or in rooms  connected by ventilating ducts in the same  building  because the gases given off by  decomposing nitrate film will damage or destroy  images on safety film records     Films not of the silver gelatin type  e g   diazo and  vesicular  should not be wound on the same rolls   stored in the same containers  or be in physical  contact with silver gelatin films  In addition  some  older vesicular films have been known to give off  acidic fumes and require a separate storage  housing with a separate circulating a
14.  the care needed for storing  photographic records is similar to that for  storing written paper records  although there  are some requirements peculiar to the storage  of photographic film     The permanence of photographic records  depends on the chemical stability of the film    how the film is processed  and the conditions  under which the processed film records are  stored  The stability of the film layers is  determined in manufacture and processing  while  storage is controlled by the user  This pamphlet  discusses the composition and properties of  black and white silver gelatin  thermally  processed silver  TPS   diazo  and vesicular films  as they relate to film permanence  It also  describes the essential requirements of good  processing and storage practices     NOTE  Refer to the latest revision of each ANSI or  ISO Standard specified     Definitions   To help understand storage requirements    the composition and structure of microfilm are  described and definitions of commonly used  terms are given      Overcoat              Emulsion               Substratum     7    GEN A a GU Un  Jm Jmm            Polyester Support    Antistat  amp  Matte    Structure of a typical black and white negative film        Acetate film    acetate base  safety film with a  base composed principally of cellulose acetate  or triacetate     Antihalation undercoat   separate layer of  light absorbing dye located between the film  emulsion and the base to suppress light reflection   Duri
15.  the other processing  solutions  In some cases  extremely soft water  can also cause reticulation  In the case of  contained chemical kits such as the Kodak  Miniprocessor  the manufacturer s recommended  film processing capacity should not be exceeded        D 31 June 2002    11    Squeegees    It is important to use an adequate squeegee  where the film leaves the water wash and enters  the drying section  Otherwise  residual water  droplets will dry and form visible surface defects  and  in some cases  cause physical sticking of the  film laps  In wound up rolls  these spots may  provide places where microscopic blemishes can  form  Inspect squeegees regularly  particularly  blade and roller types  to make sure that they do  not cause film scratches     Drying   Drying should be uniform  The drying air should  be filtered so that airborne particles of dirt or  potentially harmful chemical dusts  often present  in processing laboratories  will not become  imbedded in the emulsion while it is tacky     In machine processing  the recommendations of  both the equipment and film manufacturer for  operating conditions and processing chemicals  should be followed     In other modes of processing  the following factors  are involved     Washing Aids   Using a washing aid  such as Kodak Hypo  Clearing Agent  CAT No  146 4254   5 gal   or  Kodak Microfilm Clearing Bath and Replenisher   greatly increases both the rate and thoroughness  of hypo removal during the washing step     Aft
16.  thiosulfates  or silver salts  or both  will be retained by the film   These can break down  especially under poor  storage conditions  to produce yellow stain in  clear areas and fading in areas containing   image silver     Fixing Baths    In the fixing step  undeveloped silver halide  crystals in the emulsion are converted to soluble  silver compounds which can be washed away with  water  The chemicals most commonly used for  fixing are sodium or ammonium thiosulfate   commonly called    hypo      The fixing bath may  also contain other chemicals to maintain a  desirable pH  provide hardening  stabilize the  solution  protect the image from microscopic  blemishes  etc     For maximum washing efficiency  a non hardening  fixer followed by a non oxidizing washing aid   such as Microfilm Clearing Bath and Replenisher  should be used   Call Solutek at 1 617 445 5335  to order CAT No  414 24   Hypo eliminators  containing oxidizing agents  such as peroxide   should be avoided  Oxidizing agents may promote  image deterioration     To make sure that there is enough time for the  fixing reaction to be completed  specific  recommendations for each type of film should   be followed  Undeveloped silver halides are  dissolved by the fixer as complex ions of silver  and thiosulfate  As the silver content of the fixer  increases with processing  the silver thiosulfate  complex becomes increasingly difficult to wash  from the film  This can be avoided by frequent  replacement or proper 
17. ANSI PIMA IT9 11   1998 and ISO 18911 1999       During conditioning  the film should be in the form  intended for final storage  wound on itself or a  glass rod  not on a conventional core or reel   because the possibility of rapid moisture change  makes it inadvisable to rewind the film after  conditioning  The capsule should be loaded in the  conditioning chamber  if possible  if not  the film  should be transferred immediately to the capsule  and sealed tightly     The capsule should be a stainless steel cylinder  gasketed cover  When there is more than one roll  of film  it is a good idea to separate rolls with  stainless steel disks of the same inside diameter  as that of the capsule  Cores  reels  or wrapping of  any kind should not be included  only the film itself  should be put into the capsule     Handling and Filing  Film Records    Well planned filing systems and proper handling  of film records are important in the storage of  records  The custodian should set up safeguards  against loss or misplacement of valuable records  and also make sure that the methods of filing and  handling do not add unnecessary wear to the  records  When films must be used  duplicates  should be made and originals retained in storage     Interfiling    Microfilm may be subject to interactions when  stored with films of different generic types   e g   diazo and silver gelatin   Do not wind  different generic film types on the same roll or  store them in the same container  Diazo and  s
18. Company    at 1 323 468 5774 or contact your local   Kodak Representative     Cleanliness of the work space is essential to  success in these operations  Static discharge  devices are available for use when handling film  which has been in dry storage  Alternatively  film  can be conditioned to a higher relative humidity  before cleaning and then reconditioned to the  original low relative humidity  Other suggestions  for improving handling operations can be found in  Eastman Professional Motion Picture Films  and  The Book of Film Care          D 31 June 2002    Inspection    The potential life of photographic records depends  largely on atmospheric conditions   temperature   humidity  cleanliness   and the manner in which  the film is used  If storage conditions are kept  within the limits suggested in Table 3  inspection  of an adequate number of properly selected lot  samples should be made at two year intervals       While extended term records should definitely be  kept under the recommended storage conditions   film records of medium term value may have  more leeway in terms of storage humidity and  temperature  Where humidity is not controlled  closely  film should be inspected more frequently  than at two year intervals  the intervals between  inspection should not initially exceed six months  and then  if no deterioration is noted  can be  extended but should not exceed one year     Sometimes film inspection is considered too  laborious and costly and is neglected f
19. Kodak Micrographic Quality  D 31    Storage and  Preservation  of Microfilms    Contents    D 31    June 2002    Introduction     tierce Rand nre RAG ERA Aah SRL aye exo oa o Rs 1  DGTININONS     cS oet or on D A e Ho Nea ONE ED e e e Tee a 1  Electronic Imaging sss uae tick ique xg Se Bose RUN RR E Pao  2  Record Classification   424056 d e stu RR ERO E EUER pes pdt 3  Storage Hazards and Protection             lilii e eee 3  Fire Protection        llle 3  SIOr ade Valli   15 2  9 BASH EUR ee Pos BA ae 4  Cabinets and Safes    ovde REDE ieee dew wee REF EX 4  Effects of High Temperatures                 2 00  4  Water Protection   iua emo RUE ach lantsiavagyias pEEsEREE 5  Effects of High and Low Relative Humidities                   5  High Humidity   s  2 ardore E Rae  doth tete S a aci Se uad 5   Low  Humidity csar tober dae r                        m 5  Molecular Sieves ecu va Mee p RO RR IR Pee Na 6  Humidity Control eee s Rena xag Set TER RS 7  Air Conditioning a ooh   m od bd Ga debet Qe Barbee dee    Eus deles Sos i 7  Moisture Tight Containers           liliis liess 7  Humidification             iaai aa D ees 8  PURnOUS  Growth 2 45 3 3 cai PE OE Sek A SS dor Rois be mea 8  Microscopic Blemishes 2224  evi ctu twee DER RS Y Res 8  TOWING  take modera eL ER uL EUM n EU DM EN Pete 9  Chemical Contamination               llle 9  Composition of Enclosure Materials                llllssn  10  Papel sched 2 Se eed RR RR RA M lua e ras ud 10  PlaStl6  3 4 4 0222 4 dct Seren
20. and burning    time test as specified in ANSI and ISO Standards     Safety poly ethylene terephthalate  base     a polyester film base for recording materials  composed mainly of a polymer of ethylene  glycol and terephthalic acid  All safety films   both acetate and polyester  manufactured  by Eastman Kodak Company meet these  requirements  This means that they are  difficult to ignite and are slow burning     All silver gelatin Kodak Microfilms on Estar Base   when processed as recommended by Kodak   meet the current specifications established by the  American National Standards Institute  Inc     ANSI  for films intended for use as LE 500     Substratum  subbing or precoat    the layer  that bonds the emulsion to the base     Electronic Imaging    With the coming of electronic digital imaging  systems  the need for continuing the quality  concepts already established in the micrographics  arena has evolved  Following are a few   key concepts     Digitization   use of a scanner to convert  documents  on paper or microforms  to  digitally coded electronic images suitable  for electronic storage     Digital   the use of binary code to record  information   Information  can be text in a binary  code  e g   ASCII   images in bitmapped form   or sound in a sampled digital form or video     NOTE  Information is recorded digitally for  accuracy in storage and transmission   Some types of data manipulation are  easier in digital form     Scanning   1   In electronic imaging  scanni
21. ar film  Although Kodak Thermal Print  Films can withstand 71  C  160  F  for several  hours  high temperatures can cause a complete  loss of images if care is not taken with regard to  temperature control        D 31 June 2002    Water Protection    Film records should be protected from possible  water damage  such as from leaks  fire sprinkler  discharge  and flooding  If possible  storage  facilities should be located above basement  levels  Storage cabinets should be raised so that  the lowest shelf or drawer is at least 15 2 cm    6 in   off the floor and should be constructed so  that water cannot splash through ventilating  louvers onto the records  Drains provided should  have adequate capacity to keep water from a  sprinkler discharge from reaching a depth of   7 6 cm  3 in       If the record storage area should become flooded   prompt steps should be taken to reclaim any  immersed records  Allowing microfilm records   to dry  even partially  will cause the layers to   stick together  If there are no local facilities for  rewashing and drying the films immediately   promptly place the films in a water filled container  and send them to a laboratory where they can be  washed and dried properly        Effects of High and Low  Relative Humidities    The choice of humidity level for storage depends  on the type of photographic film and the humidity  of the work area  In order to minimize subsequent  moisture conditioning in storage  the humidity of  the work area should
22. at  least four hours     Many fire resistant safes and cabinets use a type  of insulation that when heated releases moisture  and thus fills the interior of the safe with steam  during a fire  This can cause melting or stripping  of the film emulsion layer and loss of the image   For protection  films stored in such a safe should  be placed in moisture tight cans  as described  under    Humidity Control    in this publication     It is preferable to use fire resistant safes that are  available with an inner chamber sealed against  moisture  These are classified by Underwriters     Laboratories  Inc   as Class 150 Record  Containers   Film damage caused by steam   is not a problem with these safes     The question is sometimes raised as to whether  microfilm stored in drawers or cabinets designed  to resist fire for several hours might  in case of a  fire  generate enough pressure to damage or  explode the cabinet  There is practically no  danger of an explosion from the storage of either  Estar Base or acetate base safety film under  these conditions  There are small amounts of  organic materials in acetate film base  as well as    moisture  which will expand under heat and  under  some conditions  might generate slight pressure   However  such intense heat would be required on  the outside of the fire resistant cabinet that the  cabinet would be seriously damaged from the fire  before appreciable pressure developed     Effects of High Temperatures    In addition to complete 
23. d into the  existing flip top boxes containing microfilm will  last for five to seven years  under recommended  storage conditions  Microfilm should be inspected  periodically to offer an opportunity to replace   the molecular sieves     The sieves must be replaced at some interval   depending on storage conditions  The use of  molecular sieves is cited by the American National  Standards Institute  ANSI  as another procedure  to reduce redox blemishes caused by high  humidity conditions and oxidants in the air  For  more information or to obtain molecular sieves   listed below   call Multisorb at 1 800 445 9890                    Molecular Sieves  Part No  Film Format Content  41 ag 43 16mm 3 5 grams 400  41 ag 47 35 mm 7 0 grams 200  41 ag 51 105 mm 12 5 grams 125                      With or without molecular sieves  it is very  important to follow current industry recommended  practices for film storage  such as keeping film  under proper temperature and relative humidity  conditions  However  placing recommended  amounts of molecular sieves inside flip top  boxes will extend the life of the films significantly   This adds additional protection by slowing the  deterioration process     D 31 June 2002    Humidity Control    Control of relative humidity is required for  preservation of permanent records     Air Conditioning   Properly controlled air conditioning of the storage  area is definitely recommended for the optimum  long term preservation of permanent records   The
24. e  provided  that the surface is well protected by lacquer   enamel  tinning  plating  or some other corrosion   resistant finish  Lacquer  which might give off  reactive fumes  peroxides  or exudations during  storage should not be used     Adhesive   Some photographic images can be damaged   by adhesives incorporating impurities such as  sulfur  iron  copper  or other ingredients that  might react with image silver or gelatin  Pressure   sensitive adhesives and ether linked products  should be avoided     Rubber based products such as rubber cement  should not be used  Not only might they contain  harmful solvents or plasticizers  but they might be  compounded with photographically damaging  sulfur  usually as a vulcanizer  accelerator  or  stabilizer  Even some    low desensitizing    or   sulfur free  rubbers contain sulfur     Photographic quality gelatin and many polyvinyl  acetate and cellulose ester adhesives are  suitable for use with paper enclosures  Heat  sealing and mechanical sealing should be used  when possible     Printing Inks   Printing inks are known to cause microscopic  spots in fine grain silver microfilm  consequently   there should be no printed matter on the inside of  the filing enclosure  The ink used for imprinting  the outside of filing enclosures should not bleed   spread  or transfer  and it should not be a source  of products that attack the photograph or the  enclosure itself     For additional specifications  see ANSI PIMA   T9 11 1998   ISO
25. er fixing  the film is first rinsed to remove the  major portion of hypo  next  the film is treated in a  Kodak Microfilm Clearing Bath and Replenisher   then it is given a final wash     NOTE The use of hypo eliminators  such as  Kodak Hypo Eliminator HE 1  is not  recommended for microfilm because  some hypo eliminators contain oxidizing  agents that can contribute to the  formation of emulsion blisters and  microscopic blemishes     Residual Hypo Test    The accepted criterion for adequate washing is  the methylene blue method described in ANSI   PIMA IT9 17 1998    IT9 17 1998 also describes  the silver densitometric method  which has been  suggested by the Association for Information and  Image Management  AIIM  as a simpler and less  expensive alternative  If the silver densitometric  density difference is 0 02 or less  AIIM considers  that the methylene blue requirements for  extended term storage record films have been  met  In both methods  a clear area of the film is  tested and residual hypo tests may be run up to  two weeks after processing  A simpler  but less  sensitive  method is the use of the Kodak Hypo  Test Kit  CAT No  196 5847   This test gives an  indication of residual hypo  but it should not be  used as a measurement for meeting the  requirements of the ANSI specification     NOTE For satisfactory residual hypo levels in  films  both fixing and washing must be  acceptable   inadequacies in one cannot  be compensated by the other     Residual Silver Com
26. erm  Film Type Bude  Magana Oe Lee  e  Humidity C F Humidity    F  Silver Gelatin Cellulose ester   20 50  2 35 6   20 60  25 77   Acetate  20   40  5 41 0  20 30     44 6  Silver Gelatin Polyester 30 40  21 69 8   20 60  25 77  Thermally Processed Silver Polyester 15 30  21 69 8   20 60  25 77  Diazo Polyester 20 50   10 14 20 60  25 77  20 50   8 26 6  20 50  2 35 6  Vesicular Polyester 15 50  20 70 20 60  25 77  Electro Photographic Polyester 15 50  20 70 20 60  25 77  Photo Plastic Polyester 15 50  20 70 20 60  25 77  Color Cellulose ester   20 30   10 14 20 60  25 77   Acetate  20 40   3 26 6 20   60  25 77  Color Polyester 25 30  2 35 6   20 60  25 77                         NOTE  If the storage temperature is sufficiently low or if the air where the film is to be handled is quite  moist  leave the film in its closed container until it warms up to approximate room temperature   Otherwise  condensation of moisture will occur on the cold film surfaces        D 31 June 2002    17    References and Bibliography    1  American National Standard   Technical Report     Glossary of Document Technologies   ANSI AIIM  TR2 1998     2  American National Standard   Imaging Materials     Processed Silver Gelatin Type Black and White  Film   Specifications for Stability     ANSI PIMAITO9 1   1996 or ISO 18901     3  American National Standard     Imaging Materials     Photographic Films   Specifications for Safety Film      ANSI IT9 6 1991  R1996  or ISO 18906     4  American National
27. ey germinate and grow under favorable  conditions  When silver gelatin films are stored for  any length of time in an atmosphere having a  relative humidity of above 60   fungus  often  called mold or mildew  has a tendency to grow on  the emulsion surface  the back of the film  or on  the film reel  The higher the relative humidity  the  greater the chance of fungus attack and the more  abundant its growth  The only real protection  against fungus growth is to make certain that  conditions are unfavorable for its growth     If fungus growth progresses far enough  it can  cause serious and permanent damage to film   This takes the form of distortion of the emulsion  and eventually causes chemical breakdown so  that the gelatin becomes sticky and readily soluble  in water  Water or water solutions should not be  used for the removal of fungus growth because  either may lead to disintegration of the image   Clean affected film by wiping it with a soft plush  or cotton pad moistened with an approved  film cleaning liquid  such as isopropyl alcohol   This procedure is described in detail in a separate  Kodak Pamphlet        Fungus can grow on most surfaces  including  diazo and vesicular films  however  these films are  more resistant to fungus growth than silver gelatin  films  If necessary  clean these film types by  wiping with a soft  plush or cotton pad  moistened  with water  Do not use solvents on diazo   vesicular  or thermally processed silver films     The Kodak Disaste
28. hieved by simply  heating the cool  moist air that is present    For example  conditions in a typical mine may be  10  C  50  F  and 85  relative humidity  by heating  the storage area to 21  C  70 F   the relative  humidity is reduced to 4096  Where it is not  practical to lower the relative humidity adequately  by this means  supplementary dehumidification  may be required     Effects of Nuclear Explosions    The protection of vital microfilm records against  the effects of nuclear explosions is mostly a  matter of providing sufficient blast and fire  protection  Processed microfilm is essentially  unaffected by radiation  even of the intensity  encountered in the vicinity of a nuclear explosion   Best protection from blast and fire is afforded  by removing security files from potential target  areas  Storage in underground vaults  with  duplicate copies in different locations  provides  the greatest security        D 31 June 2002    13    Time Capsule Storage    Only silver gelatin films conforming to ANSI PIMA   T9 1 1998  or ISO 18901 1999 should be used  for time capsules or sealed in cornerstones of  buildings  Film intended for this kind of storage  should be conditioned to a low relative humidity   20 3095 is recommended for acetate base films   in a conditioning room or chamber  During  conditioning  air should be circulated against   both roll surfaces  Conditioning times should be at  least two weeks for 16 mm film and four weeks for  35 mm film  This conforms to 
29. ilms        Very low humidities have  in the past  caused film  to be brittle  However  film of current manufacture  has not been found to exhibit brittleness or  breaking tendencies under normal handling    even at relative humidities as low as 1596  Old film  that is found to be brittle at low humidity should  be reconditioned to a higher humidity before   use  One day s storage is usually sufficient for  conditioning a dry 16 mm roll halfway to a higher  ambient relative humidity  to bring it to full  equilibrium requires about a week  In each case     both sides of the roll should be exposed to the air     TET  WERT  JEN    ji    Single Strip  AIL LU             Percent of Equilibrium                      1 23456810 2030501 2 345681015 1 2 34561 2 3456  Minutes jours Days Weeks    x    Time  Rate of conditioning a typical safety film from 20  to 50   relative humidity at 21  C  70  F      Low humidity affects the curl of silver gelatin film   causing a slight contraction of the emulsion layer  and resulting in a slight curl toward that side   This is generally believed to be an advantage  because the concave emulsion surface is better  protected against abrasion  However  excessive  curl may cause difficulty in focusing images in  some microfilm readers  This can be avoided   by conditioning the film to a relative humidity of  30 50  before use  The curl of diazo  TPS  and  vesicular films is virtually unaffected by humidity     Film handled at very low humidities may als
30. ilver  TPS  have an LE of 100 years        D 31 June 2002    Extended term storage conditions   storage  conditions suitable for the preservation of  recorded information on the majority of freshly  processed photographic films for 500 years     Medium term storage conditions   storage  conditions suitable for the preservation of  recorded information for a minimum of 10 years     Methylene blue   a chemical dye formed  during the testing of permanence of processed  microimages using the methylene blue  method  Also called residual thiosulfate ion  and silver densitometric method     Storage Hazards and Protection    There are a number of hazards to the satisfactory  storage of photographic film that apply to records  intended for medium term  long term  or  extended term storage  In fact  it is not always  possible to predict the desired life of records at the  time they are made     While films of medium term  long term  or  extended term interest are subject to the same  hazards  the storage protection provided for  them will differ in degree because of a number  of factors  These include the cost of providing  storage facilities  desired record life  frequency  of record use  value of the records  etc  See  ANSI PIMA IT9 11 1993   and ANSI IT9 2 1991 9    Fire Protection    All Kodak Microfilms are slow burning films as  defined by the American National Standards  Institute  Inc   Even though photographic records  will burn considerably slower than paper  the  same precau
31. ilver gelatin microfilms should be stored  separately before and after processing   Diazonium salt gases emitted from Diazo  microfilm  pre  and post process  can be  detrimental to silver gelatin microfilm     Continual handling of film  even under favorable  conditions  causes some wear  but wear can be  accelerated greatly by certain factors which can  be controlled  Scratching occurs when film is dirty  or equipment is poorly maintained or wrongly  used   Cinching  causes scratches and occurs  when film is made to slide layer on layer    e g   when the end of a loose roll of film is pulled    Tearing and fingerprinting occur when equipment  and handling methods are not suitable     Remove dirt from film by wiping with a lintless  fabric pad moistened with film cleaner or its  equivalent  Carry out cleaning operations in an  atmosphere of about 50  relative humidity to  minimize the possibility that the film will become  electrostatically charged and attract dust particles     Another proven method for removing foreign  matter from film is the use of Particle Transfer  Roller  PTR  technology  These rollers are a  polyurethane material whose tackiness and  cushiness pick up dust  hair  and other unwanted  material from a continuous moving film surface   These rollers can be mounted in line with most  film operations  They can be cleaned easily with  warm water and mild soap  For more information  about Particle Transfer Roller technology call  FPC  Inc    an Eastman Kodak 
32. ir system      Avoid using rubber bands around rolls of film   since residual sulfur from rubber vulcanization  promotes the growth of microscopic blemishes   Adhesive tapes  tape splices  bleached papers   and printing inks also cause undesirable effects     Composition of Enclosure Materials    Paper   Paper should be made from rag  bleached sulfite  or bleached kraft pulp with an alpha cellulose  content greater than 8796  It should be free from  highly lignified fibres  such as ground wood  as  determined by the phloroglucinol spot test     For paper in direct contact with black and white  photographic material  the pH should be between  7 5 and 9 5  The pH should be close to 7 0 when  in direct contact with color or diazo material  There  should be an alkali reserve of at least 296  m m    The alkali reserve should be obtained by the  incorporation of an alkaline earth carbonate   Neutral or alkaline sizing chemicals should be  employed and the material should be essentially  free from particles of metal  Glassine envelopes  should not be used     Plastic    Suitable plastic enclosure materials are  photographic film support materials such as  uncoated polyester  polyethylene terephthalate   polypropylene and polyethylene  Chlorinated   or nitrated sheeting should not be used and  cellulose nitrate  in particular  should be avoided     Metal    Metal enclosures should be noncorrosive  materials such as anodized aluminum or stainless  steel  The use of steel is permissibl
33. lems of moisture or gaseous impurities   such as might occur with floods  dehumidifier  failures  smoke from a fire  or moisture released  by insulation  upon exposure to heat  in certain  fire resistant safes and cabinets     With both metal and plastic containers  all  materials  including any gaskets and protective  paints or lacquers  must be non corroding and  free of peroxides  reactive fumes  and exudations  during storage  Closed containers with friction   type or threaded twist on lids may require no other  seal  but should be tested for imperviousness     If the container is in an area having the prescribed  humidity and known to be free of harmful gases   taping is not required  If these conditions are not  met  taping will provide satisfactory protection     Plastic boxes or cans are preferable  as they  provide more insulation in case of fire        D 31 June 2002    Humidification   Humidification is not necessary or desirable  unless the prevailing relative humidity is under  15    under 30  for polyester base films   for  long periods of time and unless the film is used  frequently and physical troubles are encountered   Neither water trays nor saturated chemical  solutions should be used for humidification of  storage cabinets because of the more serious  danger of overhumidification  Even humidification  controlled by instrumentation is risky unless     fail safe    devices are installed     Fungus Growth    Fungus spores are found in the air everywhere   Th
34. loss by fire  damage to film  records can also occur if they are exposed to very  high temperatures  Excessive heat causes film to  buckle because of shrinkage at the edges  When  severe  this distortion affects the ease with which  the information can be taken from microfilms   either by projection  for reading  or by printing  onto another film     Silver gelatin films that have been conditioned at  a relative humidity of 50  or lower will withstand  121  C  250  F  for 24 hours without significant  loss in readability or printability  At 149  C  300  F    severe distortion can occur in a few hours     Films that have been conditioned at a relative  humidity above 50  may show objectionable  distortion in somewhat shorter times or at lower  temperatures  Higher humidities  however  are  undesirable for other reasons  as explained later     Thermally processed silver films will build   up background densities fairly rapidly at  temperatures of 93  C  200  F  and above    At these temperatures  even a few hours will  produce significant loss in readability or  printability  At 149  C  300   F  or above  severe  distortion can occur in a few hours     Diazo films  while quite stable  contain dye images  that can fade and or discolor as a result of high  temperatures  Kodak Diazo Microfilms can  withstand a week at 93  C  200   F  without image  loss  At 149  C  300   F  or above  severe distortion  can occur in a few hours     High temperature is the greatest enemy of  vesicul
35. ng is  the operation which precedes digitization  where  the surface of a document is divided into pixels  and analog values are collected representing the  optical density  brightness and possibly color    of each pixel     2   In electronic imaging  OCR scanning is the  conversion of marks that represent symbols into  symbols for use in a data processing system   The paper or microfilm with the human readable  marks is first scanned as an image  then is  analyzed to recognize the intended symbol   The result is the set of symbolic information    in a machine readable code such as ASCII   also known as handprint character recognition   intelligent character recognition  and optical  character recognition      3   In micrographics  scanning is the movement of  an image on a reader screen in a direction  perpendicular to the direction of roll film transport     4   Scanning is the systematic examination of  data  ISO         D 31 June 2002    Scanner   a device that electro optically converts  a document into a series of pixels by detecting  and measuring the intensity of light reflected or  transmitted  When initially captured  each pixel is  a level of brightness  gray or color   initially an  analog quantity  but potentially digitized     NOTE For many applications  total information  about each pixel is not needed and would  represent a burdensome amount of output  from the scanner  Therefore  most  scanners digitize the value of each pixel  and reduce the amount of data o
36. ng processing of this film  the dye layer  becomes transparent     Base or support   a flexible plastic material that  is coated with a thin  light sensitive  image   forming layer  The thickness of the base varies  with different film types     Dimensional stability   ability of photographic  materials to maintain their original size and shape  during and after processing and also under  various conditions of temperature and humidity     Emulsion   the image forming layer  For  unprocessed black and white silver gelatin films   itis composed primarily of minute silver halide  crystals suspended in gelatin  Exposure to   light in a camera or printer causes no visible  effect  but there is an invisible change which  produces a  latent image   To obtain a visible   usable image  the exposed material must be  chemically processed     For diazo and vesicular films  the sensitized layers  are composed of light sensitive diazonium salts   To obtain a visible  usable image with these films   the exposed material is heat processed  Diazo  films are typically heat processed in the presence  of ammonia     For TPS films  the image forming layer is typically  silver halide and silver salts suspended in a  polymeric binding        D 31 June 2002    Emulsion layer s    image or image forming  layer s  of photographic films  papers  and plates     Film base   the plastic support for the emulsion  and backing layers     Halation   halo or ghost around the desired  image on a photographic em
37. o  develop a static charge as it passes through a  reader or rewinder  This static charge will attract  dust particles that can damage the emulsion by  chemical action or physical abrasion  Therefore   it is important that any film handling area be kept  clean  If film is kept in a dry storage area  it may  be necessary to use the film in an office area of  higher humidity to minimize static problems   However  as previously noted  large humidity  differences may lead to conditioning problems        Molecular Sieves    Molecular sieves are capable of absorbing most  of the potential film degradation agents such as  moisture  oxidants  solvents  and others when  kept in close proximity with the films under  confined storage    Therefore  Eastman Kodak  Company recommends the use of molecular  sieves with triacetate and polyester based films to  reduce the physical aging of films and increase  the longevity of black and white images under  confined storage  It also prevents ferrotyping   mold fungal growth on films   as it reduces the  moisture content of film     Tests have shown that molecular sieves prevent  vinegar syndrome associated with acetate based  films and micro blemishes  and arrests the  oxidation of silver images due to peroxides and  ozone in the atmosphere  Using molecular sieves  slows the rate of these degradation reactions  under confined storage and thus extends the  keeping and longevity of older film collections     A single molecular sieve packet inserte
38. of fading in the heat of the reader  and potentially shorten keeping life  Processing  within manufacturers  recommendations should  maximize keeping qualities  In addition to  monitoring process temperature and time    regular checks should be made to make   sure that scratch free film is being produced   ANSI PIMA IT9 12 1995 and ISO 18912 1999      Specifications for Stability of Processed Vesicular  Film   discuss the criteria for proper development     Special Storage and Hazards    Underground Storage    Most large industrial organizations and  government agencies have developed methods  for safeguarding vital records in the event of a war  or a natural catastrophe  Many keep their vital  records in underground repositories located many  miles from large metropolitan areas  When  microfilm is kept underground in caves  mines   tunnels  subbasements  or similar locations   special care should be taken to make certain that  there is adequate control of the relative humidity     Film should not be stored where the relative  humidity exceeds the limits recommended for  storage  See Table 1 of ANSI PIMA IT9 11 1998  or ISO 18911 1999  If humidity cannot be  controlled satisfactorily  film must be dried  as  described under  Air Conditioning    then placed  in a moisture proof container  The film must also  be protected  as in other types of storage  against  airborne dirt or chemical contamination     In underground situations  proper film storage  conditions can often be ac
39. or many  years   occasionally with unfortunate results    If itis not always possible to open every film   can or rewind every roll at the recommended  frequency  select a few rolls at random from   the film collection each month for examination   This approach provides some protection at a  relatively small cost  If there is any indication  that film records are not keeping properly   storage conditions should be improved and other  protective treatments given the film  Make copies  of films that show signs of deterioration because  deterioration  once initiated  is an irreversible  process that may be restrained  but not  terminated  by improving storage conditions   Therefore  extensive and frequent inspections  should be made     ANSI AIIM standards and technical reports are  available related to the inspection of silver gelatin  microforms  An example can be found in  American National Standard   Imaging Materials     Processed Silver Gelatin Type Black and White  Film   Specifications for Stability        Table 1  Applicable Standards for Microfilm                                            LE is for polyester based Thermally    LE is for acetate based Silver Gelatin   Processed Silver Diazo Vesicular   TPS   Long Term Long Term Medium  Long Medium  Long  LE 500  LE 100  LE 100  LE 100   LE 100       Safety Film Specifications    IT9 6  IT9 6  IT9 6  IT9 6   ISO 18906 ISO 18906 ISO 18906 ISO 18906   Specifications for Microfilms on IT9 1   Polyester Base  ISO 18901  and
40. pound Test    ANSI PIMA IT 9 17 1998 9 and ISO 18917 1999  contain a test designed to indicate residual silver  salts in the film  Such salts are an important cause  of image layer degradation in aged processed  photographic films     Protective Coatings    It should be recognized that while lacquers and  other coatings have advantages for working prints  receiving hard use  they are not within the scope  of the ANSI long term storage specifications        D 31 June 2002    Processing of Other Film Types    Thermally Processed Silver  TPS     This film should be processed in accordance  with the manufacturers  recommendations for  optimum image stability  ANSI PIMA IT9 19 1994  and ISO 18919 1999  give specifications for  stability of TPS films     Diazo Films    The proper processing of diazo films can also  affect keeping qualities  In the diazo process   the film should be processed to completion for  maximum storage stability  ANSI PIMA IT9 5   1992  and ISO 18905 1999 give specific details  for methods and measurements for proper  development for image stability     Also  as with conventional silver films  if  processing equipment utilizes squeegees and  dryer chambers  regular inspections should be  made to make sure that the process is scratch   free and free from airborne dirt and chemicals     Vesicular Films    The only variables in processing thermal or  vesicular films are the processing temperature  and time  Insufficient processing can increase  the possibility 
41. r Recovery Laboratory  offers no charge evaluation of suspect microfilm  and can be reached at 1 800 EKC TEST   1 800 352 8378  or 1 585 253 3907     Microscopic Blemishes    Some processed silver gelatin microfilms in  storage for two to twenty years have developed  microscopically small colored spots or blemishes   The fogged leader at the outside of the roll is most  frequently affected by the blemishes  which are  generally red or yellow in color and smaller in size  than the image characters  e g   a typewritten  letter reduced 20X  on the microfilm  On occasion   these spots progress further into the roll and  appear in image areas  A more detailed  description of the blemishes and of the techniques  used in inspecting microfilm is given in National  Bureau of Standards Handbook 96      The spots are caused by local oxidation of image  silver  resulting in the formation of minute deposits  of yellow  or red colored colloidal silver        Possible oxidizing agents entering from outside  the roll of microfilm are aerial oxygen  whose  action on the film is strongly accelerated by  moisture  and atmospheric contaminants such   as peroxides  ozone  sulfur dioxide  hydrogen  sulfide  and nitrogen oxides  which all occur in  industrial atmospheres     Assuming that your microfilm was processed to  established quality control standards  microscopic  blemishes  redox  may occur due to the oxidation  of the metallic silver image by the presence of  oxidants in the storage area 
42. replenishment of the fixing  bath or by in line recirculating electrolytic recovery  of silver from the fixer     Recovery of silver from fixer is advisable for  reasons of economics  conservation and ecology   There are three principal methods of silver  recovery     metallic replacement  electrolytic   and sulfide precipitation  For additional  information  refer to Kodak Publication J 212 2     Washing    Adequate washing is essential to the permanence  of silver gelatin microfilm  After all undeveloped  silver halide is converted  the emulsion is still  saturated with fixing bath and some dissolved  silver compounds  If these are not removed by  washing  they will slowly decompose and attack  the image  causing discoloration and fading    The effect is accelerated greatly by high humidity  and temperature  The smaller the grain size of  the image  the greater this reaction is  Microfilms   being very fine grained  are very sensitive to   this effect     For good washing  a rapid flow of fresh water  should be used  The water should be filtered to  remove dirt particles  To improve washing   countercurrent and spray systems are frequently  used in processing machine construction   Washing efficiency decreases rapidly with  decreased temperature and is very low   at temperatures below 16  C  60  F   High  wash water temperatures produce the most  efficient washing  but emulsion reticulation can  result if the wash water temperature is too high  and not kept close to that of
43. ring  9  3    167 173  1965     15  Fundamentals  ASHRAE Handbook  New York   American Society of Heating  Refrigerating and Air   Conditioning Engineers  1993    16  HVAC Systems and Equipment  ASHRAE Handbook   New York  American Society of Heating  Refrigerating  and Air Conditioning Engineers  1992      17  HVAC Applications  ASHRAE Handbook  New York   American Society of Heating  Refrigerating and Air   Conditioning Engineers  1991      18  Refrigeration  ASHRAE Handbook  New York   American Society of Heating  Refrigerating and  Air Conditioning Engineers  1994      19   Recovering Silver from Photographic Materials    Eastman Kodak Company  Kodak Publication  No  J 10A     20  American National Standard   Photography     Determination of Residual Thiosulfate and Other  Related Chemicals in Processed Photographic  Materials   Methods Using lodine Amylose   Methylene Blue and Silver Sulfide     ANSI PIMA   T9 17 1993 or ISO 18918     21     Eastman Professional Motion Picture Films    Eastman Kodak Company  Kodak Publication  No  H 1     22  American National Standard   Imaging Material     Processed Vesicular Photographic Film     Specifications for Stability   ANSI PIMA IT9 12 1995  or ISO 18912     23   The Book of Film Care   Eastman Kodak Company   Kodak Publication No  H 23     24   The Technology of Silver Recovery for Photographic  Processing Facilities   Eastman Kodak Company   Kodak Publication No  J 212     25  American National Standard   Imaging Media  Film
44. tions against damage by fire   should be taken for them as for paper records   of comparable value     Depending on the importance of the records   fire protection provided can vary from the full  protection described on the following pages for  valuable records to that provided by ordinary  office storage     Storage Vaults    The highest degree of protection for a large  number of records is afforded by a fireproof  storage vault or record room  It should be located  and constructed in accordance with the local  building code  Fire Underwriters    Regulations  and  the requirements of the National Fire Protection  Association  NFPA     for a valuable record   room  except that an approved  controlled   air conditioning unit should be installed  While  NFPA discourages air conditioning such an  installation  the fire hazard introduced by  openings for air conditioning ducts can be  overcome by the use of automatic  fire control  dampers approved by Underwriters  Laboratories   Inc  These can be installed in the ducts in  accordance with recommendations of NFPA     Sufficient insulation should be provided in the  vault to permit satisfactory temperature control at  all seasons of the year and to prevent moisture  condensation from forming on the walls     Cabinets and Safes   For smaller quantities of records  a fire resistant  cabinet or safe of the type described by NFPA     will provide considerable protection  Such a safe  should protect records against a severe fire for 
45. ulsion   This is  caused by the reflection of rays of light from the  base to the emulsion or by internal scattering of  light within the film      Nitrate film   a photographic film with a base  consisting of cellulose nitrate  Nitrate base films  decompose with age and are not suitable for  permanent records  The manufacture of nitrate  film by Eastman Kodak Company in the United  States of America was discontinued in 1951  but  older nitrate motion picture films are often found in  storage  It is not always possible to determine by  visual examination if a film has a nitrate base   However  neither KODAK nor RECORDAK  Microfilms in any width were ever made on  nitrate base     Non curl backing layer   a layer  usually made  of gelatin  applied to the side of the film base  opposite to that of the emulsion layer  for the  purpose of preventing curl     NOTE  It is comparable to the emulsion layer  in thickness and is not removed in  processing   Antihalation or other  layers removed in processing are  excluded from this definition      Polyester film   a photographic film having a  polyester base  This type of base manufactured  by Eastman Kodak Company is called Estar Base   It is exceptionally tough and strong and has  excellent dimensional stability  Microfilm  emulsions on Estar Base are currently supplied  for many purposes  Kodak currently manufactures  only microfilms on Estar Base     Safety photographic film   photographic film  which passes the ignition time test 
46. utput to  only that which is required  For example   output might be limited to one bit per pixel  for  black and white  scanning     Scanner threshold   the brightness level above  which a pixel is considered pure white and  below which the pixel is considered pure black   sometimes set manually  lighter darker   setting   or set automatically based on the  average brightness of the document      Record Classification    On the basis of required retention  photographic  records can be classified broadly as requiring  medium term storage and long term storage     Archival medium   recording material that can  be expected to retain information forever  so   that such information can be retrieved without  significant loss when properly stored  However   there is no such material and it is not a term to be  used in American National Standard material or  system specifications     Life expectancy  LE    the length of time that  information is predicted to be retrievable in a  system at 21  C and 50  RH     LE designation   the rating for the  life  expectancy  of recording materials and  associated retrieval systems     NOTE The number following the LE symbol is a  prediction of the minimum life expectancy   in years  for which information can be  retrieved without significant loss when  stored at 21 C and 5096 RH     For example  LE 100 indicates that  information can be retrieved for at least  100 years of storage  Silver gelatin films  have an LE of 500  thermally processed  s
    
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Garland RADIANT CHAR-BROILER 4522970 REV 1 User's Manual  Sun Fire X4100, X4100 M2, X4200, and X4200 M2 Servers Linux  CD Radio Cassette    Copyright © All rights reserved. 
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