Agilent Technologies 08112-90004 Water Heater User Manual
Contents
1. 12 digit hexadecimal number Stack MAC Address 0030C1C49982 located on the back of the HP JetDirect network card Stack IP Address 172 16 0 102 Sub mask 255 255 25 0 Bootp Server 172 16 0 101 Cancel Help 7 Click Done to exit the Xcalibur Instrument Configuration program 8 Open the Xcalibur data system before you turn on the devices of your Agilent1100 Series LC stack 12 Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition Thermo Scientific Triggering Data Acquisition with the Autosampler If you want the Agilent 1100 series autosampler to trigger data acquisition you must make the appropriate selections in the Timed Events page for the autosampler for each instrument method you create Instrument methods contain the contact closure signals the chromatographic conditions and the MS detector settings for an LC MS application Note Configure the Agilent 1100 Series autosampler before performing the following procedure Refer to Chapter 3 Configuring the Autosampler for Contact Closure lt To trigger data acquisition with the Agilent 1100 Series autosampler 1 Choose Start gt All Programs gt Xcalibur gt Xcalibur The Home Page appears 2 Click the Instrument Setup button The Instrument Setup window appears 3 Click the Agilent 1100 AS button in the Instrument Setup viewbar located on the left side of the window The Instrument Set2. The stack MAC address is a unique identification for each network card The manufacturer usually stamps it on the network card Note The TCP IP settings are shared by all Agilent 100 LC modules in the stack Changing the value of a setting for one module in the Instrument Configuration dialog box changes the value of that setting for all modules in the stack Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition 1 3 Configuring the Autosampler for Contact Closure e In the Stack IP Address box type the IP address for your Agilent 1100 LC stack Leave the value set to the default or contact your network administrator for the IP address The default stack IP address is 172 16 0 102 In the Sub mask box type the subnet mask address mask Leave the subnet mask set to its default value or contact your network administrator for the subnet mask The default subnet mask value is 255 255 255 0 In the Bootp Server box type the IP address for the network card in your PC that is responsible for assigning the stack IP address for your Agilent 1100 LC system Leave the value set to the default or contact your network administrator for the BOOTP server IP address The default IP address for the network card is 172 16 0 101 6 Click OK to save the settings and close the dialog box Figure 6 Agilent1100 Autosampler dialog box Agilent1100 AutoSampler General Tray TCP IP shared per stack
3. lt To contact Customer Service for ordering information Phone 800 532 4752 Fax 561 688 8731 Web site www thermo com finnigan lt To suggest changes to documentation or to Help e Fill out a reader survey online at www thermo com Icms techpubs e Send an e mail message to the Technical Publications Editor at techpubs finnigan lcms thermofisher com Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition vii Agilent Modules Supported by LC Devices Versions 2 0 2 and 2 1 0 Thermo Scientific Table 1 lists the model number and firmware versions for the Agilent 1100 Series LC modules that are supported by the Xcalibur 2 0 and higher data system Table 1 Xcalibur 2 0 supported firmware versions for the Agilent 1100 Series LC Module Model Number Firmware Version Binary pump G1312A A 06 01 012 Quaternary pump G1311A A 06 01 012 Autosampler G1313A A 06 01 012 Thermostatted autosampler G1329A A 06 01 012 Well plate autosampler G1367A A 06 01 012 Thermostatted column compartment G1316A A 06 01 012 Variable wavelength detector G1314A A 06 01 012 Diode array detector G1315A A 06 01 012 Multiple wavelength detector G1365B A 06 01 012 Only works with version B of the Control Module gt eo 1 To check the firmware version of an Agilent 1100 module Make sure that the Agilent 1100 Series modules are connected by CAN communication cables that all th
4. 2007 Thermo Fisher Scientific Inc All rights reserved Agilent is a registered trademark of Agilent Technologies Inc Hewlett PackardO is a registered trademark of Hewlett Packard Company LCQ LTQ LXQ MSQ TSQ and Xcalibur are trademarks of Thermo Fisher Scientific Inc Thermo Fisher Scientific Inc provides this document to its customers with a product purchase to use in the product operation This document is copyright protected and any reproduction of the whole or any part of this document is strictly prohibited except with the written authorization of Thermo Fisher Scientific Inc The contents of this document are subject to change without notice All technical information in this document is for reference purposes only System configurations and specifications in this document supersede all previous information received by the purchaser Thermo Fisher Scientific Inc makes no representations that this document is complete accurate or error free and assumes no responsibility and will not be liable for any errors omissions damage or loss that might result from any use of this document even if the information in the document is followed properly This document is not part of any sales contract between Thermo Fisher Scientific Inc and a purchaser This document shall in no way govern or modify any Terms and Conditions of Sale which Terms and Conditions of Sale shall govern all conflicting information between the tw
5. About This Guide This guide describes how to hardwire an Agilent 1100 Series LC to a Thermo Scientific mass spectrometer and the data system computer configure an Agilent autosampler for contact closure from within the Xcalibur Instrument Configuration program and trigger data collection with an Agilent autosampler This guide also describes how to upgrade a Hewlett Packard 1100 Series LC to an Agilent 1100 Series LC with Ethernet communication Related Documentation In addition to this guide Thermo Fisher Scientific provides Help available from within the Xcalibur software Safety and Special Notices Make sure you follow the precautionary statements presented in this guide The safety and other special notices appear in boxes Safety and special notices include the following CAUTION Highlights hazards to humans property or the environment Each CAUTION notice is accompanied by an appropriate CAUTION symbol CAUTION Highlights electric shock related hazards to human beings Each electric shock notice is accompanied by the international High Voltage symbol IMPORTANT Highlights information necessary to prevent damage to software loss of data or invalid test results or might contain information that is critical for optimal performance of the system Thermo Scientific Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition v Preface Note Highlights information of general interest T
6. The MAC address of the HP JetDirect 400N network card is located on the back of the card Because you need the MAC address when you configure the Agilent stack record the network card MAC address before you install the card Agilent 1100 Series LC systems with JetDirect network cards must have revision 2 mainboards to function properly with LAN communications Table 3 shows the required revision level for each module The serial number listed in the table and all serial numbers after that number are supported Table 3 Supported serial number Module P N Mainboard Serial Numbers for Supported Version G1310A G1311 65520 DE64300355 made in Germany Isocratic pump US64400233 made in U S A G1311A G1311 65520 DE64301137 made in Germany Quaternary pump US64401134 made in U S A G1312A G1312 65520 DE64300703 made in Germany Binary pump US64400425 made in U S A G1313A G1313 65520 DE64302092 made in Germany ALS autosampler US64400886 made in U S A G1314A G1314 65520 JP64201926 made in Japan Variable wavelength detector G1315A G131 65520 DE64301532 made in Germany Diode array detector US64400333 made in U S A All serial numbers above the listed number in numeric order are supported 4 Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition Thermo Scientific 2 Connecting the Hardware Installing a Network Card in an Agilent Module lt To install t
7. 1 Order the appropriate upgrade parts from your local office for Thermo Electron San Jose products e Ifthe HP 1100 is not interfaced to an MS detector as an Xcalibur controlled GPIB inlet device order the JetDirect Ethernet Control kit which contains the parts listed in Table 4 If the HP 1100 is interfaced to an MS detector as an Xcalibur controlled GPIB inlet device order the parts listed in Table 5 Note An HP 1100 LC system that is currently interfaced to a MS detector as an Xcalibur controlled GPIB inlet device should have already installed the contact closure PCB and the external contact closure cable Therefore you need to order only the parts specified in Table 5 Table 4 JetDirect Ethernet Control Kit P N OPTON 30018 Part Number Description of Kit 00012 27714 Contact closure PCB 00012 27716 External contact closure cable 00012 70008 Ethernet 10 Base T cable 2 00825 01 00024 10 100 Autosensing 8 port Ethernet switch 00825 01140 HP JetDirect 400N PCB Thermo Scientific Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition 17 A Upgrading an HP 1100 Series LC Table 5 Parts required to upgrade an Xcalibur controlled HP 1100 Series LC Part Number Description of Part 00825 01140 HP JetDirect 400N PCB 00012 70008 Ethernet 10 Base T cable 2 00825 01 00024 Ethernet switch 2 Follow the instructions in Installing a Network Card in an Agilent Module on page 4
8. install one as described below lt To install the external contact interface board 1 If you have not already done so turn off the autosampler and unplug it from line power CAUTION To avoid electric shock unplug the power cable that connects the Agilent module to line power After you turn the power switch to the Off position the power supply continues to draw current 2 To prevent damage to the interface board ensure that you are using ESD protection For more information on preventing damage caused by an electric discharge refer to the Reference Manual for the Agilent module CAUTION To prevent damage to an instrument always use ESD protection when handling electronic boards and components 3 To remove the cover plate from the slot where you plan to install the external contact interface board loosen the two screws that fasten the plate to the chassis of the autosampler 4 Insert the external contact interface board see Table 2 for the part number into the slot and then tighten the two screws to fasten the board to the chassis of the autosampler See Figure 4 Figure 4 View of the external contact interface board installed in an Agilent 1100 Series autosampler Screws for fastening the external contact interface board 0000000 00000 D OR E VIAL OUTPUT RELAY CONTACTS oo ala m REMOTE RS232 CAN CAN CONFIG 8 Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition
9. to install the JetDirect 400N PCB Note After the communication interface in the HP 1100 LC system is upgraded to an Ethernet interface the system is the same as and will be referred to as an Agilent 1100 LC system 18 Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition Thermo Scientific Thermo Scientific Index A Agilent 1100 Series LC configuring autosampler for contact closure 11 external contact interface PCB installing 8 solvent tracking feature deactivating 15 supported mainboards for JetDirect cards 4 Agilent LAN interface board G1369A 5 C configuring the Agilent 1100 Series Autosampler 11 contact board 11 contact closure configuring the Agilent Autosampler for 11 Contacting vi data acquisition triggering 13 deactivating the solvent tracking feature for Agilent 1100 LC pumps 15 E Electric shock safety precaution 5 8 ESD precaution vi 6 8 Ethernet cable connections 7 Ethernet card for upgrading HP 1100 LC 17 F firmware for Agilent LC 1 H HP 1100 Series LC upgrading to Ethernet interface 17 instrument methods triggering data acquisition 13 J JetDirect boards supported 4 MAC address 4 mainboards supported for JetDirect Cards 4 S safety precautions vi slot cover removing from an Agilent module vi solvent tracking feature for Agilent pumps 15 stack IP address 12 stack MAC address 4 12 X Xcalibur data system Instrument Config
10. Thermo Scientific 2 Connecting the Hardware Connecting the Trigger Cable Connecting the Trigger Cable A trigger cable with a DB15 connector relays the start signal from the autosampler to the MS detector lt To connect the trigger cable to the Agilent autosampler and the MS detector 1 Ifyou have not already done so install the external contact interface board as described in Installing the External Contact Interface Board 2 Connect the 2 pin connector to the I O panel of the MS detector such that the white wire is connected to the Start In pin and the brown wire is connected to the Start In pin 3 Connect the DB15 connector to the RELAY CONTACTS receptacle located on the external contact interface board of the Agilent 1100 Series autosampler See Figure 5 Thermo Scientific Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition 9 2 Connecting the Hardware Connecting the Trigger Cable Figure 5 Connections for 2 wire DB15 trigger cable TSO Series MS detector Right side Rear panel panel START INT i l l l j I pana Connection to autosampler De ee RELAY CONTACTS Right side panel Whitewire Brown wire DDD LCO Series Rear panel Surveyor MSQ _ _ Rear panel Start In Start In No
11. e modules are turned on and that the Agilent 1100 Control Module is connected Refer to the Agilent 1100 Series LC reference manuals for instructions on how to connect the CAN cables the LCD display Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition Press the F4 key on the Control Module to access the Records LCD display Press the Esc key on the Control Module until System appears in the upper left corner of 1 1 Agilent Modules Supported by LC Devices Versions 2 0 2 and 2 1 0 Module Product Serial Version On time EMF 4 Check the firmware versions of the Agilent 1100 Series modules Refer to Table 1 for the firmware versions supported by the Xcalibur 2 0 and higher data system 2 Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition Thermo Scientific Connecting the Hardware This chapter describes how to install the interface boards connect the Ethernet cables and make the contact closure connections required to control an LC MS system Agilent LC Thermo scientific MS system from Xcalibur Contents e Ethernet Communication Kit e Installing a Network Card in an Agilent Module e Connecting the Ethernet Communication Cables e Installing the External Contact Interface Board e Connecting the Trigger Cable Ethernet Communication Kit To connect an Agilent 1100 series HPLC to your Thermo Scientific MS detector you must have the Ethern
12. et Communication kit P N OPTON 30012 which contains the parts listed in Table 2 In addition one of the modules of the Agilent 1100 Series LC must have a JetDirect 400N LAN card P N 00825 01140 or an Agilent LAN interface board model number G1369A Table 2 Ethernet Communication kit P N OPTON 30012 Description Part Number Ethernet switch 00825 01 00024 PCB contact closure external contact interface 00012 27714 Cable trigger external contact 2 wire DB15 00012 27716 Cable patch 3 m 10 ft CATS RJ45 straight shield 00012 70008 Thermo Scientific Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition 3 2 Connecting the Hardware Installing a Network Card in an Agilent Module Installing a Network Card in an Agilent Module For the Agilent LC system to communicate with the Xcalibur data system through an Ethernet connection one of the modules in the Agilent 1100 Series LC stack must have a network interface card If the stack has a detector the card is usually installed in the detector Tip Vendors label network cards with a unique MAC address which is a 12 digit hexadecimal number The first portion of the MAC address identifies the vendor The second portion of the MAC address is a unique serial number For example a typical mark on a network card is AD 0030C1C49982 in which 0030C1C49982 is the stack MAC address The first portion 0030C1 identifies the vendor as Hewlett Packard
13. he network interface card in an Agilent module 1 Make sure the module usually the detector is turned off and unplugged from line power Figure 1 shows the location of the power switches When the power switch of a module is in the On position the LED on the switch is green When you turn the power switch of a module to the Off position the LED turns off Ifyour LC stack contains a detector for example diode array detector variable wavelength detector multiple wavelength detector install the network interface card in the detector Ifyour LC stack does not contain a detector install the network card in any module with an open slot CAUTION To avoid electric shock unplug the power cable that connects the Agilent module to line power After you turn the power switch to the Off position the power supply continues to draw current Tip You can install an Agilent LAN interface board model G1369A instead of a JetDirect 400N network card Figure 1 Front panels of the Agilent 1100 Series modules t Solvent cabinet Binary pump Power switch Power switch Column compartment Power switch Detector Power switch Thermo Scientific Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition 5 2 Connecting the Hardware Installing a Network Card in an Agilent M
14. ip Helpful information that can make a task easier Safety Precautions To connect the Agilent 1100 Series LC stack to a Thermo Scientific mass spectrometer you must install an external contact board in one of the Agilent modules and a LAN interface board in a second Agilent module To install a board you must remove the cover from the optional board slot Figure 2 on page 6 shows the location of the slot on the back panel of the detector Before you remove the slot cover from an Agilent 1100 Series module do the following e Turn the power switch to the Off position and unplug the power cable CAUTION To avoid an electric shock always turn off an Agilent module and unplug it from line power before you remove its cover e Refer to the Reference Manual for the module for additional safety information and for information on preventing ESD damage caused by an electrical discharge CAUTION To prevent damage to an instrument always use ESD protection when handling electronic boards and components Contacting Us There are several ways to contact Thermo Fisher Scientific lt To contact Technical Support Phone 800 685 9535 Fax 561 688 8736 E mail TechSupport C MS thermofisher com Knowledge base www thermokb com Find software updates and utilities to download at www mssupport thermo com vi Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition Thermo Scientific Thermo Scientific Preface
15. isition Thermo Scientific 2 Connecting the Hardware Connecting the Ethernet Communication Cables Connecting the Ethernet Communication Cables lt To connect the Ethernet communication cable to an Agilent 1100 Series LC 1 Connect a category 5 shielded Ethernet cable from the JetDirect 400N network card to the Ethernet switch CAUTION To comply with safety and EMC regulations you must use category 5 shielded Ethernet cables to make the Ethernet connections for your instrument 2 Connect a category 5 shielded Ethernet cable from the Ethernet switch to the Ethernet card in the computer dedicated to the LC system typically network interface card number 3 Figure 3 Ethernet connections E28 a LU o 7s aot E o hed Sok Y Y o wey gt myt TL amp QT PRO s nee mae oT bed la 28 Y z 0 4 Computer JetDirect 400N card Optiplex GX520 installed in one of subject to change the Agilent modules Not drawn to scale Ethernet Switch GAR ALAR ALA Cat5 shielded Ethernet cables Thermo Scientific Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition 7 2 Connecting the Hardware Installing the External Contact Interface Board Installing the External Contact Interface Board If your Agilent 1100 Series Autosampler is not already equipped with an external contact interface board
16. ng feature on the Agilent 1100 pump 1 If Xcalibur is open close it 2 Open the Analysis screen on the Agilent 1100 handheld control module 3 Press the Settings button Fl Figure 8 Agilent 1100 handheld control module 09000 FRI 3 F4 5 O DO O 0000_D 09060 OOO 4 Press the number corresponding to the pump 5 Press the Bottle Fillings button F4 6 Set all of the solvent Total boxes to 0 The solvent Actual boxes are then automatically set to 0 7 Clear the Error If Empty check box by using the right arrow to move the focus to this setting and then pressing Enter Thermo Scientific Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition 15 5 Turning Off the Solvent Tracking Feature 8 Press the Done button F6 9 From the Windows XP start menu choose All Programs gt Xcalibur gt Xcalibur The Home Page appears The Agilent 1100 devices should reconnect and appropriately display their status 10 If the Info view is not displayed choose View gt Info View 16 Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition Thermo Scientific Upgrading an HP 1100 Series LC The Xcalibur 2 0 and higher data system supports control of the Hewlett Packard HP 1100 Series LC only if you upgrade the HP 1100 communication interface to an Ethernet interface lt To upgrade your HP 1100 Series LC
17. o documents Release history First release February 2007 second release July 2007 For Research Use Only Not regulated for medical or veterinary diagnostic use by U S Federal Drug Administration or other competent authorities Contents Thermo Scientific Chapter 1 Chapter 2 Chapter 3 Chapter 4 Chapter 5 Appendix A ic AAAMOOO N v About Tiida dad AAA e wees v Related Documentation n ssuu asasan unean v Safety and Special Notices erario a eras v Safety Precautions sesi e a eaaa aA A a vi Contacts US un nut an ti oie Suc vi Agilent Modules Supported by LC Devices Versions 2 0 2 and 2 1 0 1 Connecting the Hardware ccc cece eee cece e eee nennen 3 Ethernet Communication Kit 2 0 eee ene ees 3 Installing a Network Card in an Agilent Module 0 0005 4 Connecting the Ethernet Communication Cables 0000005 7 Installing the External Contact Interface Board ooooooooooommomo o roo 8 Connecting the Trigger Cable coco ii ao i 9 Configuring the Autosampler for Contact Closure 0 11 Triggering Data Acquisition with the Autosampler 13 Turning Off the Solvent Tracking Feature 0 0 cece eee rm 15 Upgrading an HP 1100 Series LC cee cece eee 17 MON anna a a eu a aa e au kan ge 19 Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition Preface
18. odule 2 To prevent damage to the interface board ensure that you are using ESD protection For more information on preventing damage caused by an electric discharge refer to the Reference Manual for the Agilent module CAUTION To prevent damage to an instrument always use ESD protection when handling electronic boards and components 3 To remove the cover plate from the slot where you plan to install the network interface card loosen the two screws that fasten the plate to the chassis of the module Figure 2 shows the location of the cover plate on the back panel of an Agilent 1100 Series detector Figure 2 Back panel of an Agilent 1100 Series detector Cover plate D D OO dz arto OE oo ANALOG ANALOG RS232 RS232 CAN CAN NS U 4 Record the MAC address 12 digit hexadecimal number located on the back of the HP JetDirect 400N network card You will need this number to complete the configuration of the Agilent stack See Figure 6 on page 12 5 Insert the HP JetDirect 400N network card into the slot and then tighten the two screws that fasten the PCB to the chassis of the module 6 Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acqu
19. t drawn to scale Trigger Cable 10 Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition Thermo Scientific Configuring the Autosampler for Contact Closure The Agilent 1100 Series devices query the PC for the stack IP address only during their start up procedure Therefore complete the following procedure and ensure that the Xcalibur Home Page window is open before you turn on the Agilent 1100 Series devices eo 1 Agilent1100 AS 2 Double click the Agilent 1100 AS button in the Configured Devices area Thermo Scientific To assign contact closure control to the Agilent 1100 Series autosampler Choose Start gt All Programs gt Xcalibur gt Instrument Configuration The Instrument Configuration dialog box appears Scroll through the Available Devices area and double click the Agilent 1100 AS button The Agilent 1100 AS button is copied to the Configured Devices area and is displayed as a Configured Devices button The Agilent 1100 Autosampler dialog box appears Click the General tab The General page appears See Figure 6 In the General page make the appropriate selections Select the Contact Board Installed check box Note If you do not select the Contact Board Installed check box the Timed Events page does not appear in the Instrument Setup view for the autosampler e In the Stack MAC address box type the media access control address for your Agilent LC stack
20. up view for the Agilent 1100 AS appears 4 Click the Timed Events tab The Timed Events page appears 5 In the Timed Events page select the appropriate contact closure signal settings as shown in Figure 7 a Click the Contact 1 box to display the list and select Closed b Make sure that all the other Contact boxes display Open Figure 7 Timed Events page for the Agilent 1100 Series autosampler Initial Conditions Timed Events Time min Contact 1 Contact 2 Contact 3 Contact 4 0 00 Closed Open Open Open 1 00 Closed Open Open Open Open Open Open Open N ma 6 Make the appropriate entries and selections for the rest of the instrument method Thermo Scientific Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition 13 4 Triggering Data Acquisition with the Autosampler 7 Save your method with an appropriate name 8 Choose File gt Exit to close the Instrument Setup window Xcalibur prompts you with the Save As dialog box the File Summary Information Dialog box and the File Save Audit Trail dialog box 14 Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition Thermo Scientific Turning Off the Solvent Tracking Feature The solvent tracking feature on the Agilent 1100 LC pumps is not supported by Xcalibur at this time You must turn off this feature to prevent error messages from terminating the data acquisition lt To turn off the solvent tracki
21. uration program configuring the Agilent 1100 series autosampler for contact closure 11 Instrument Setup view 13 Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition 19
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