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User Manual - Liu Research Group

1. FAN 24V RED DYMAXION TURBO PUMP POWER CABLE 1 GROUND GREEN YELLOW l 24V BROWN P 24V BROWN P 24V RETURN BLUE 3 24V RETURN BLUE 31 NC 4 NC GROUND GREEN YELLO 24V RETURN BLACK TURBO FAN TURBO PUMP DISPLAY UNIT TURBO RS485 21 4 CHASSIS CONN 5i RS 4y 485 61 24V RETURN RS 485 N ProLine power supply 1 DC wiring diagram Figure 7 2a 7 2 AMETEK ProLine Mass Spectrometer HEATER JACKET POWER CONNECTOR 24V RED 24V RED 24V RETURN BLACK 24V RETURN BLACK GROUND GRN YELLOW POWER SUPPLY DC2 CNe 1 6 24V RED CN3 1 7 24V RETURN BLACK TEMPERATURE CONTROLLER INLET HEATER 8 24V RED 7 24V RETURN BLACK THERMOCOUPLE 21 THERMOCOUPLE YELLOW 1 THERMOCOUPLE RED Figure 7 2a ProLine power supply 2 DC wiring diagram HEATER JACKET l 24V RED 4 24V RETURN BLACK AIN WIRE INLET VALVE HEATER 24V RETURN BLACK 24V RED SOLID STATE RELAY 2 OUTPUT RED fi DUTPUT RED 3 INPUT RED 4 INPUT BLACK 4 OUTPUT 1 RED 31 OUTPUT 1 BLACK Wiring Diagrams 7 3 DYMAXION I O MODULE DIGITAL OUT DIGITAL IN ANALOG 1 0 1 0 MODULE TO CHASSIS CABLE 15 PIN D CONNECTOR 9 PIN D CONNECTOR 1 DOO BLACK 1 2 DOL WHITE 2 3 DO2 BROWN 3 4 DO3 WIE 4 6 D5 RE S 14 DO COMMON WHITE 6 NX 7 5
2. eC 1 Orange GROUND a e Green Pressure Control EE l Valve Circuit Board Black H To I O Board Brown Digital In Figure A 2 11a i Wiring diagram extended pressure range option without I O data acquisition E White VSO Valve Signal Analog I O White Inlet Pressure Signal Jo OONDOABRWNH option VSO Valve Inlet Pressure Control Board TB5 1 VSO Control Voltage Red 2 Ground Black External Digital In Cable Flow Switch 9 Pin D Conn 9 Pin D Conn TB2 1 Flow Switch Black 1 1 Flow Switch Orange 6 Flow Switch White 2 Flow Switch Green TB3 1 Inlet Pressure Orange Inlet Pressure Controller 2 Ground Brown Internal Cable 4 Inlet Pressure Orange 3 420 mA Orange 9 Pin D Connector 9 Pin D Conn 9 Pin D Conn PA pus L 4 Ground Brown J1 1 Flow Switch Black 1 ye 5 24V Red Flow Switch Whit 6 14 Gone 6 O 24V Return Black gt VSO a Signal Bien 2 T A E T N ee 7 Ground White 7 Digital Out B AV Retur TB4 3 Inlet Pressure Red 1 Digital In MEL eRe 8 Ground White 6 Analog I O 2 Inlet Pressure Orange 3 Chassis Ground Green Yellow Pressure Transducer 4 24V Return Black 1 24V Red 2 Inlet Pressure Orange TB1 3 Oo Chassis Ground Green Yellow 1 24V Red External Analog I O Cable 4 24V Return Black 2 24V R
3. WsiS uvME ZZ ioe t EN 4 omm cmm 11 opm OO on NN iio d CT 22 UN S1 SNAP BRAIN m m DISTRIBUTED O PROCESSOR Note Base Address set by jumpers on brain board SX Se DIGITAL ADDRESS 83000 BASE ADDRESS 0 434 ANALOG ADDRESS BASE 2 DIGITAL ADDRESS BASE 1 Leo Le 6 ANALOG ADDRESS BASE 3 Lat uw ss Power can be applied once the I O system is connected properly NOTE Appendix A 10 AMETEK ProLine Mass Spectrometer EXAMPLE This example shows a setup with three devices e 2digital Address 64 and 65 e analog Address 66 Digital Input Address 64 Modules 0 1 2 3 Digital Output Address 65 Modules 12 13 14 15 Analog Input Address 66 Modules 2 3 4 5 6 7 Analog Output Address 66 Modules 8 9 10 11 12 13 B3000 BRAIN Base Address 64 Optomux Digital 4 Channel Address 64 Digital Input Modules 0 1 2 3 2 Channel Analog Input 2 Channel Analog Input 2 Channel Analog Input 2 Channel Analog Output 2 Channel Analog Output 2 Channel Analog Output Optomux lem 4 Channel Address 65 I Modules 12 13 14 15 Digital Output Optomux Analog Input Address 66 Modules 2 3 Optomux Analog Input Address 66 Modules 4 5 Optomux Analog Input Address 66 Modules 6 7 Optomux Analog Output Address 66 Modules 8 9 Optomux Analog Output Address 66 Modules 10 11 Optomux Analog Output Address
4. m 1 7 AMIBIBKCIOSGODOULOS ene anin daki d dend karine salla k pe PR PEMPREE PED UE 1 9 ProLine Multi Port Samipl n 015 Y S N ccsecccsascssxserpeatsceveeciosmassss sosuseaueestzere 1 9 VALVE coniro 5 6 o NAR ME A RR 1 9 a aa ak E A eee 1 10 Temperature Control for Heater aye elan a lll ln e bem 1 10 8 OAC DK A AE MAY NN NY A 1 11 PONET UPP O sten tent IERI UERSUM DUI IRIURE SUM Te SUE 1 11 sa e A TOURS 1 11 e NN A TE E 1 11 RON A EA A YA 1 12 Extended Pressure Range ODEHOB acie sc stol mii elli 1 12 I O Data Acquisition Option NN 1 14 On Board Computer RR ERER PARAYA EE ERAY 00500 DORT ESO 1 14 TecHinical SUDDOED EE A RNA NAM 1 15 Specifications Installation Operation Jag el ila ee in Ag arg A A mR A me eee 3 2 P mping Systemi Ey MR A A YEPREM SEM 3 3 Installing che Turbo pp A NK A TE 3 3 Turbo Pump Cable OLE CHONG sapar ke elman sis dalla klein 3 5 CHAPTER 4 Backing Pump ODBe e ME OR EE O AMAN ERE 3 5 Electronics Package iis ta MA OM geye e al ai a ai lela 3 6 Connecting the Electronicsto OuadrupoleHead 3 6 Connecting Electronics to DC Line POW EE eiecerunt prt ttp n irati 3 7 Electronics Package Connections Lusiocxmriste sis iot ut eia sieso laci uinci stro E PARU 3 7 RS 485 Switch Termination Settings 1 elicere 3 7 Mp sn 3 8 0
5. 3 8 Gendm T 3 9 jd 3 9 DIDI e a a ay a a E SUMI A See alak 3 9 a MIA EE EN A EEE ME AMY NE PA MA MART EE UMEN 3 10 Heating Jacket VIamte idle P ORMANA E RAMA PE APO EE MMA 3 10 YE I MI 3 11 Attaching the Sample Calibration Lines eene 3 12 Purging the pressure regulator and calibration gas line 3 13 BS OPE e Instat ON esprai a 09920099003 909800 00 090 02000007 3 14 Prokne NE E EEE DN MUI DIE 3 15 FPowenne Up be PrOLIDE A MENA EEUE 3 15 Pump Controller Mieri amman ema eer tie Haste etam e ER 3 15 Electronics Package Warm Up Time uoce eot tnra eiut Pun pita Vid adadan 3 16 IgM HHR N 3 16 Shutting Down the PEGDIDOS A AA MR 3 17 Maintenance and Troubleshooting Pornic EIS IESUS SNNT TTE 4 Inlet Heater OU Fa sari iin ek nedim imi ekek l 4 1 Adjusting the inlet heater temperature esses 4 Pumping System Maintenance sadisamlaasad kamdakse la knn oni MISSAE RM E ERE RS M PEPERIT UMS 4 5 I 707 7 J 4 5 Diaphragm roughing backinepump 4 5 Rotary vane roughing backingepump 4 5 Extended Range PumpingOptilonMamtanance 4 5 Electronics Package MaintenanceandTroubleshooting 4 6 Quadrupole Head Maintenance NY A
6. JY Ye AKA Y YY CAAA A Lie TA BOY Heat Sink DA Gi 2 Li Rear Panel settings before returning board to factory to facilitate setting up the new board I O Option Board Removing the I O Option Board l Disconnect the cables from the three connectors 15 pin and two 9 pin at the back of the I O Option board Figure 5 2b Remove the screws from the top and bottom of the I O Option board that hold the case to the electronics unit See Figure 5 2a Gently slide out the board disengaging the inside connectors It may be nec essary to slightly wiggle the board so that it comes loose You do not need to remove the cover from the board 5 2 AMETEK ProLine Mass Spectrometer Replacing the I O Option Board 1 Gently slide the I O Option board into the slot in the back of the electronics unit making sure that you engage the connector on the board with the elec tronics unit itself 2 Insert the screws at the top and bottom of the I O Option board cover secur ing it to the electronics unit 3 Attach the cables to the appropriate connectors on the I O Option card See Figure 5 2b V0 7 MM oY N GG VY A A Z h lo A lo 8 an x GA d T Fi VA A E G Us espe Me X 5 4 Y Digital Out Top Conn
7. 1 Attach the pressure regulator to your calibration gas cylinder 2 Attach one end of the 1 8 stainless steel tubing to the pressure regulator at the calibration gas cylinder Attach the other end to the calibration Gas In port bulkhead fitting making sure it is installed as far into the fitting as pos sible 3 Ensure that the Gas Out port for the calibration gas 1s open and not capped 4 Open the calibration gas cylinder to allow the gas to flow through the pres sure regulator 5 Open the pressure regulator to allow the calibration gas to flow through the calibration gas line making sure the pressure is between 2 and 10 PSIG A The pressure must not exceed 20 PSIG CAUTION 6 Allow the calibration gas to flow through the gas inlet outlet for about 60 seconds to purge any stale air gas that may be in the line A longer purge time may be required depending on the length of your plumbing lines 7 Once the line is purged with gas still flowing place a 1 8 Swagelok cap on the Gas Out port for the calibration gas The calibration gas line does not need to be purged again unless you change the calibration gas for that port Installation Operation 3 13 Software Installation 1 Insert System 2000 software CD into CD ROM drive 2 The installation program should begin to run immediately If it does not start automatically click RUN from the Windows Start menu Type the drive letter follo
8. AlddnS 33 Ud Ny MOTTA n Brka ae annoa t JNO I MITTA N3389 GNOUMD T x bici n MOLOANNOD 33 Dd 30d y AlddN Yad 3LIH WALNAN NO d ONIdWNd XA 3NTI Z ADTA N334 NNO JNO JIS SHdSOWLY 8NS AUTAANTRD CNOIRD 7 JUHA WALAN N INO YOLISNNOD 33ADd Fd y X ANIMI JNO AlddN N3ADd ALIHA WALNAN y If X9V18 I T Ir MOTTA N334 INADA LIMA TALAN N dina YOLISNNOI S3ADd did DNDIOVG ATddNS 33A Id LIHA IVSLON Xov 18 GNTI 590718 WNIWS3L 310d 2 LIHA Ind WALNAN 2 ILIHA WaLnaNn ILIHA Wann WWE INI UN MAITTA N3389 ANNADA MOVE NIT yya NTI 3LIH TWALNAN H i X4 3NTI 9 MOWTA YO ILIHA Ca LN yya ANT dnd y Yma ILIHA NI gs if ond X78 NI N WNIWH3L Fd 2 NIHIL ld 2 ACOH ASNA AILT HOLIAS FINGOW ANINI XIADA c gt O TE eb o G 2 c 5 o DOG La 5 Wiring Diagrams 7 1 POWER SUPPLY DC CNe 1 6 24V RED CN3 1 71 24V RETURN BLACK DYMAXION POWER CONNECTOR l 24V RED P 24V RED 31 24V RETURN BLACK 31 24V RETURN BLACK GROUND GREEN YELLOW DYMAXION POWER CABLE l 24V RED P 24V BLACK 31 24V RETURN WHITE 4 24V RETURN GREEN GROUND DRAIN WIRE TURBO PUMP POWER CONNECTOR l GROUND GREEN YELLOW 2 24V RED 31 24V RETURN BLACK 4 NC 2 POLE POWER CONNECTOR l 24V RED P 24V RETURN BLACK VALVE CONTROL BOARD TB fi 24V RED TB 2 24V RETURN BLACK
9. Logic Output Voltage for SNAP IDC5 SW normally open 0 5 V max switch closed LED on Q 2 mA sinking 2 7 V min switch open LED off Q 0 4 mA sourcing 0 5 V max switch open LED on Q 2 mA sinking 2 7 V min switch closed LED off Q 0 4 mA sourcing 250V c Output Voltage for SNAP IDC5 SW NC normally closed Maximum Operating Common Mode Voltage Field Term to Logic Connector Power Requirements 5 VDC 0 25 200 mA Module Ratings Number of Channels Per 4 Module Turn on Time 5 msec Turn off Time 25 msec Channel to channel Isolation None Input to output Isolation 1500 V AC DC Temperature 0 C to 70 C operating 30 C to 85 C storage Typical switches for use with these modules are switched status sensors level sensors pressure indicators etc magnetic reed switches used on doors or windows for burglar alarms snap action micro switches the auxilliary switches on motor Starters and most relay contacts CAUTION The SNAP IDC5 SW and SNAP IDC5 SW NC inputs are not intended to be used with contacts that are connected to any external user supplied voltage or currents SNAP IDC5 SW and SNAP IDC5 SW NC Wiring Diagram DRY CONTACT SWITCHES SNAP MODULE F ELD CONNECTOR OPTO 22 PART SNAP FIELDCON POWER TO SENSE CONTACTS 5 SUPPLIED BY MODULE SNAP MODULE RELEASE LATCH OPTO 22 PART SNAP
10. ALM Ftr E Display Default DISP Ac ot r Input Failure Mode FAIL bPLS Ftb1 Setpoint Lockout SLOC no PL 1 Lockout Tag TAg none PSL1 Proportional Band Pb 6 ipi Integral Function It 99 99 Ot 2 Cycle Time CT 5 0 hyS2 Derivative Function dE 5 11 y Alarm Type ALty dEnc Alarm Hysteresis AhyS Z dSP2 Alarm Latch LAt no Unit Alarm Silence SIL no d Alarm Lo ALO 5 dSP Alarm Hi Ahl 5 rP l LOC Figure 4 2a Series 935A Watlow Controller Inlet OPERATIONS heater factory set parameters A M Auto Aut OFF CAL 0 ht M Pid Pb ht 6 It ht 99 99 Figure 4 2b dE ht 5 11 Series SD31 Watlow Controller A2 hi Inlet heater factory set A2 Lo E parameters 4 2 AMETEK ProLine Mass Spectrometer Figure 4 3 Watlow EZ Zone PM Controller Inlet heater factory set parameters Maintenance amp Troubleshooting 4 3 Ad S MAP nuS OPERATIONS Al READ ONLY READ ONLY 0 READ ONLY READ ONLY READ ONLY READ ONLY 4 4 AMETEK ProLine Mass Spectrometer Pumping System Maintenance Turbopump Change the oil cartridge in the turbopump annually following the turbopump manufacturer s instructions Remove power to the ProLine before performing this maintenance CAUTION Diaphragm roughing backing pump When the ProLine is in continuous use you must change the diaphragms in the diaphragm pump every six to nine months In some cases diaphragm life may be considerably longer depending on the composi
11. Closed Source The AMETEK conductance limited enclosed source contains a dual wire fila ment so the analyzer can continue to function if one side of the filament burns out The replacement filament comes in a protective container and can easily be replaced n the field e The filament should be replaced soon after its resistance exceeds 1 3 ohms thoriated iridium filament or 2 5 ohms tungsten filament or when it 1s determined to be half open filament LED is yellow Maintenance amp Troubleshooting 4 7 Equipment required to replace a filament e needle nose pliers e 5 64 hex wrench supplied by AMETEK e filament assembly kit supplied by AMETEK e latex gloves powder free optional Handling the filament by the shorting tabs Figure 4 5 on the fila n ment plate will ensure against contamination through handling since NOTE these tabs will eventually be discarded Before changing the filament you must remove the electronics from the quadrupole head and remove the quadrupole head from the 4 ION vacuum system The electronics power must be turned off before servicing Removing the electronics from the quadrupole head e After powering down the electronics carefully use the tightening knobs on the sides of the electronics to unlock the electronics from the quadrupole head e Once loosened gently pull straight back on the electronics without twisting until it is free of the head Do not remove the cab
12. ple molecules are turned into ions which are then focused towards the quadrupole to be detected The process occurs in the ionizer which consists of a filament filament electron repeller ionizer body ion volume and two focusing lenses See Figure 1 1 The filament produces electrons As current flows through the filament it 1s electrically heated to incandescence and emits free electrons Once the electrons are free they are accelerated towards the ionizer body by the potential difference between the filament and the ionizer body As a cloud of electrons accelerates 1 2 AMETEK ProLine Mass Spectrometer Filament Ceramic Insulator Electron Repeller lon Volume pe ee ee m nga en an en a a eg a Ta Rota a lonizer Body dedi Mass Filter lonizer components x towards the ionizer body the electrons collide with the sample in the center of the ion volume and create ions Once the positive ions are formed they are extracted from the ion region and focused towards the quadrupole mass filter by a difference in potential Lens 1 has an applied negative voltage that due to a difference in electrostatic potential attracts the newly formed positive ions passing them through Lens 2 Lens 2 in turn focuses the electrons into the quadrupole El lonization When a single electron is removed during ionization a positive 10n 1s created this 1s referred to as a molecular ion When the bombarding electrons cause the
13. tion connection to the computer 5 hard drive and a LAN connection ZA If you have the computer option on your analyzer the top board that 5 Ifyou do not have the computer option you will see two power supplies at tached to either side of the U bracket 6 Remove the four screws on the back cover of the electronics box to remove the cover and access the valve control board This also makes it easier to replace other components in the box The fan is attached to the back cover of the electronics box Make sure to detach the connector from the fan or power supply if you are NOTE removing the back cover 6 2 AMETEK ProLine Mass Spectrometer Electronics Box Parts Replacement Computer Board Replacement If you have this option refer to the appropriate appendix in this manual Power Supply Boards If you have the computer option on your analyzer first remove the computer board as described in the appendix You can now easily see both power supply boards attached to either side of the U bracket in the box Removing the power supply boards Looking at the analyzer from the back there are two power supply boards at tached to the U bracket Figure 6 1 e Left side Power supply for the turbo pump electronics package and fan e Right side Power supply for the heater 1 Using a Philips screwdriver remove the five screws on the standoffs that hold the power supply board to the U bracket Watlow Controller
14. 66 Modules 12 13 Opto 22 Option Appendix A 11 Setting the Device Properties for Digital Input Modules e On 2000 software click the Edit menu and select Device Properties Select your Opto 22 SNAP device from Select a device to edit Click OK The Device Properties dialog box appears If a digital device is not listed click Cancel On the main screen click the Edit menu and Add Device Click Optomux Digital Once the Opto 22 SNAP System has been added you can proceed with setting the parameters e Configure the General tab as follows Device Properties ES Select a device to ecit Bits per Second 9600 Address 64 Type Optomux Digital Make sure Device Enabled and Live Data boxes are checked a uk Device Properties General 1 0 Setup Scripts Communications Port RS 2 2 Pol R5 B5 Pot Bits per second Address 600 T g os Deuce Name p gbi Descnplion opto 22 Digital Appendix A 12 AMETEK ProLine Mass Spectrometer e Click the I O Setup tab for each module position enter the Type and Name see example below The SNAP I O system combines four inputs or outputs into one NOTE module For the SNAP I O system the System 2000 module number refers to a particular digital I O channel not the physical module For example if a single digital output module is installed in the first SNAP rack position the System 2000 will refer to it as Modules 0 1 2 and
15. BLACK LINE FROM POWER CABLE TERMINAL BLOCK DETAIL 4 25679JE Power Supply WHITE FROM POWER SUPPLY POWER CABLE WHITE FROM PUMP 8 POSITION MANIFOLD 9 339022JE Elbow 10 75155KE 8 Position Manifold 11 33541JE Male Adapter 12 33540JE Male Connector 4 POSITION MANIFOLD 9 33022JE Elbow 11 33541JE Male Adapter 13 75152KE 4 Position Manifold The ProLine equipped with the extended pressure range option re quires a different fuse than the ProLine operating without this option NOTE See Chapter 6 in this manual for information on replacing the power switch fuses 100 120V System 25779JE 10 Amp slow blow 5x20mm 200 230V System 25702JE 5 Amp slow blow 5x20mm Extended Pressure Range Option Appendix B 19 This page intentionally left blank Appendix B 20 AMETEK ProLine Mass Spectrometer
16. CE e i hap e o gd 612 02 6 a O Ogg ag OQ o o o0 N 00000000 7 Lie O o o oo ll oo M o 24 ard gt m um il o 0 o 5 ol le ol lo of lo cg gtd oooo jo ool 9 a oS vue o o o o o o 20 7 w 0000000 o 02 0 2 0 900000006 0 o o 2 m T 0 2 m 0000090000 0000090090 I KN gt 800000000 o o o o o o 2 e Oz P S 2 9g 9 00000000 090000000 Ce lo o oo l oo M o x pulgz 9 CL 400000000 ofl o 4 a o E s o ON MALS yi o o O o o oW o o o o o o m E ro Es 00000000 N y ps N m a O wl AJo A L hi x x x x x N a o o So Eg Oo o a n amt 9 me uc o no o Oo o 20000000020 lo0 o o o o o o o o O i gt E ice o o o o o o ouigz g a e 5 ole wml S o o o o o o o o O ex Q 6020 0 00 0 0 o i i Ero s Olde ma o S oll o N N N N N N N nd N faa m zs Yi oS ee ii gt gt Y N 9j 9 g O O o Lo o o 5 o o o o o o O o T O LZ ol o o o o o Q Q Js PIZ P18 L JP19 E P20 ea P21 EM ef of o ll O Oo LO K2 O Za she RS Z1 R6 pugc Q o ONI MALS l O E
17. molecular bonds to break fragment ions form This ionization process is known as electron impact ionization EI Operation of the mass spectrometer depends on maintaining low vacuum pres sures These pressures take into account not only the operational pressures of the mass spectrometer but also the pressures of the sampling system environments Overview 1 3 Separation Once the ions reach the quadrupole mass filter they are filtered according to their mass to charge m z ratio Each ion has an identifiable mass The quadrupole mass filter is constructed of four electrically conducting parallel cylindrical rods A constant direct current DC voltage and an alternating radio frequency RF voltage 1s applied along the length of the rods Through proper electronic tuning these voltages set the criteria for the ions that pass through the quadrupole As an ion enters the quadrupole mass filter the RF and DC fields cause it to undergo oscillations Depending upon the criteria set for motion through the quadrupole an ion either strikes a rod or passes through the quadrupole Ions meeting the m z criteria have stable trajectories and emerge from the mass filter assembly Figure 1 2 Ions with other m z values have unstable trajectories and are neutralized as they strike one of the rods Ions that successfully pass through the quadrupole are again focused towards the detector using an exit aperture which has an applied negative voltag
18. they generate secondary electrons Data System Overall control of the system acquisition of data and access to collected data is accomplished through the AMETEK Process 2000 software Adjustment of all instrument parameters that affect sampling ionization separation and detection are software controlled All data acquisition parameters are also set using the software Overview 1 5 ProLine Overview The ProLine consists of the following subsystems Figure 1 3a and b e Closed Source Mass Spectrometer Package e Multiple Valve Inlet System e Electrical and Controls System e Vacuum Pumping System e Options 24 5 62 cm Front View Figure 1 3a ProLine dimensions Front top height 1 6 AMETEK ProLine Mass Spectrometer Backing Pump Exhaust Fitting G 1 8 14 4 26 5 cm Top View sample Inlets and Outlets 1 8 Compression Fittings 86660000 60000000 60000000 000000000 Common Sample Bypass 1 4 Compression Fittings Sampling System Overview 1 7 Backing Pump Sensor Manifold Sample Inlet Box O Option Card Temperature Controller Turbo Pump Electronics Box Pump Veni Value Pump Controller Controller Connector to Interface Backing Pump Figure 1 3b ProLine systems labeled 1 8 AMETEK ProLine Mass Spectrometer AMETEK Closed Source The AMETEK smart sensor offers the latest quadrupole technology using a closed enclosed source The electron
19. 3 See Figure 2 B3000 I O Mapping and Example E23 Older I O systems had a single digital input or output per module Add Display for Digital Module Device Properties Digital IN 0 Isolation Valve Status e Tocreate displays so that you can view the data being monitored go to the mode display where you want your information viewed Right click on one of the screens e Click Scan e Click Device and select your digital device Mass 28 Properties Isolation Valve Status Opto 22 Option Appendix A 13 Click the Display tab to configure the parameters for the display Dui Detal IM 1 Praeses Scan Catcutetion Dol Alarm Analog Tite Dig Digital IN O F Aule p unix I Logairic Upper leet 1 00E 07 bw E 1 00E 11 Click OK for it to become part of the mode display you have chosen Does Sorte F000 Dae a i mee ams Ost olson jj ale uah Thay Digital IN 0 eed 10E 7 1808 DE ve aE 28 ee 3 Soran 106 10 7 0608 10E 11 1 0E 07 10E 06 TES 1 0E 10 1 0E 11 Appendix A 14 AMETEK ProLine Mass Spectrometer Setting Device Properties for Analog Input Modules e On the 2000 software click on the Edit menu and select Device Properties Select your SNAP I O System device under Select a device to edit Click OK The Device Properties dialog box appears If an analog device 1s not list
20. B 2 AMETEK ProLine Mass Spectrometer ooo 9 OO O 0 O QO Capillary Restrictor The sample gas then flows past the end of a capillary restrictor A small amount of the gas passes through the restrictor and into the mass spectrom eter head The remainder of the gas flows on to the extended pressure range option From Common Exhaust Port This is the port through which the gas that does not pass through the capil lary restrictor but exits the ProLine through the common exhaust enters the extended pressure range module From Exhaust Manifold Port This is the port where all the gases exhausting from streams that are not being sampled leave the exhaust manifold and enter the extended pressure range module Flow Switch Optional The sample gas flows through the flow switch which is monitored by the Pro cess software Chapter 19 Process Software Manual The software monitors whether or not the flow is adequate A no flow reading usually indicates that the selected sample line is clogged Pressure Transducer The pressure transducer measures the pressure in the sample line and sends a signal to the pressure control circuitry and to the software Electronic Pressure Control Valve The electronic pressure control valve controlled by the pressure control circuitry admits air into the sample plumbing The air flow is automatically adjusted to maintain a constant sample line pressure Manual Regulatin
21. Card The RF card is located directly behind the rear heat sink and separated from it by the conductor guide See Figure 5 5 Follow these steps to remove the RF card for replacement 1 There are eight screws holding the RF assembly in the unit casing Remove the 2 top 1 4 and 2 bottom 1 4 screws 2 Remove the 2 3 16 screws from each side 3 Grab hold of the rear heat sink and pull hard to remove the assembly from the casing 4 You now have the complete RF assembly in your hand Refer to Figure 5 5 5 Remove the Amp cover by removing the two 1 4 self tapping sheet metal screws The Amp card is underneath 6 Remove the 4 1 4 screws holding the Amp Card to the Amp card shield 7 Using the 1 4 nut driver remove the 4 3 8 standoffs from the Amp card shield You can now see the RF card Al Oxide Insulator Amp Card Shield Amp Cover RF Card Conductor Guide SS Amp Card Shield Amp Card T 2 Ww RF Card gt ZN 3 yf gt A Amp Card 1 p 4 JAM Ni Amp Cover Front Heat Sink Figure 5 5 Amp card and RF board replacement Electronics Boards Parts 5 11 8 Using the 1 4 nut driver remove the 4 5 8 standoffs holding the RF card to the connector guide 9 Remove the 1 2 screw on the top right of the RF card This holds the card to the aluminum oxide insulator on the rear of the heat sink It is very important to remember to replace this screw and insulat
22. E REFERER Au X docu MEnTs Join Ts Achtung Beachten s ie beiliegende d okumente cAuTion Hot surface ATTEn Tion su RFAc E c HAud E Achtung Hei e Oberfl che gt gt eip Environmental Information WEEE This AMETEK product contains materials that can be reclaimed and recycled In some cases the product may contain materials known to be hazardous to the environment or human health In order to prevent the release of harmful substances into the environment and to conserve our natural resources AMETEK recommends that you arrange to recycle this product when it reaches its end of life Waste Electrical and Electronic Equipment WEEE should never be disposed of in a municipal waste system residential trash The Wheelie Bin marking on this product is a reminder to dispose of the prod uct properly after it has completed its useful life and been removed from service Metals plastics and other components are recyclable and you can do your part by one of the following these steps e When the equipment is ready to be disposed of take it to your local or re gional waste collection administration for recycling e n some cases your end of life product may be traded in for credit towards the purchase of new AMETEK instruments Contact your dealer to see if this program 1s available in your area e Ifyou need further assistance in recycling your AMETEK product contact our office listed in the front of the instruction ma
23. Electronic Pressure Control Valve gt c Air From Sample Point 9 From Sample Point 10 From Sample Point 11 From Sample Point 12 11 Sample 12 Pump Exhaust 1 4 compression CALIBRATION GASES nit F 1 0 tting P 800 Torr Abs approx Supply Pressure 35 kPa Manual Q 6 L M approx Flow 0 1 L M Regulating Consumption 0 5 L Day Valve z kE Extended Pressure Range Option Figure A 2 2 Extended pressure range option sample The extended pressure range option allows sampling of gases at or slightly flow below atmospheric pressure and creates a stable sampling pressure for the mass spectrometer inlet Refer to Figure A2 2 to follow the sample flow The numbers in the circles on the diagram refer to the number sequence in the steps below 1 Sample Entry The sample gas enters the sample selection valves These valves are 3 way manifold mount electric solenoid valves They are housed in the heated inlet enclosure The user s sample gas connections are 1 8 compression fittings Common Exhaust When valves are not selected not energized the sample path 1s connected to a common exhaust that allows the sample gas to flow through all the sample lines continuously This ensures that fresh sample 1s available to the mass spectrometer G Sample Loop When a valve is selected sample gas flow is diverted from the exhaust 2 to plumbing leading to the vacuum chamber inlet flange Appendix
24. I O system interfaces with devices connected to SNAP input and output I O modules A device connected to an input module is read by the SNAP I O Brain The SNAP Brain processes the information and sends it to the host PC running the System 2000 software In the reverse direction the System 2000 PC sends an instruction to the SNAP Brain and the Brain processes the request and sends it to the appropriate output module to turn a device on or off or to set it to a value Communications with a host computer is via an RS 485 serial link that connects to the SNAP I O Brain N Disconnect all power from the SNAP I O system before starting these procedures WARNING Components of the SNAP I O System The components used in the Opto 22 SNAP I O System consist of e SNAP Brain e SNAP input output modules e SNAP rack power supply The SNAP Brain is the core of the I O system Using the SNAP I O modules it monitors and controls all connected I O points and provides communication functions OPTO Brain B3000 B The B3000 B is a mistic serial brain designed as a modern drop in replacement for the serial B3000 brain which 1s obsolete as of October 2009 The B3000 B has the same functionality as the B3000 except that it does not support the Optomux protocol Customers replacing the B3000 with the B3000 B are required to update to the Process 2000 software AMETEK part number 88175P Process 2000 Like the older B3000 the B3000 B 1s a h
25. T DYMAXION RS 232 9 PIN D CONN 2 TRANSMIT 3 RECEIVE 5 GROUND DYMAXION RS 485 9 PIN D CONN 4 TRANSMIT 5 TRANSMIT 8 RECEIVE 9 RECEIVE Figure 7 4 Dymaxion to computer wiring RS 232 and RS 485 1 0 OPTION MODULE 9 PIN D CONN A TRANSMIT TRANSMIT RECEIVE RECEIVE Figure 7 5 Opto 22 I O option module to computer RS 485 wiring COMPUTER MN DYMAXION TO COMPUTER 2 RECEIVE RS 23p WIRING 3 TRANSMIT 5 GROUND RS 232 TO RS 485 CONVERTER FULL DUPLEX 4 WIRE AMETEK 73858SE COMPUTER RS 232 PIN D CONN 9 PIN D CONN t TRANSMIT 9 PIN D CONN 9 4 RECEIVE 2 5 RECEIVE 3 8 TRANSMIT DTR 7 RECEIVE GROUND 9 TRANSMIT RIS DYMAXION TU COMPUTER m RS 485 WIRING FOR RS 485 COMMUNICATIONS SET SWITCH ON BACK OF DYMAXION AS SHOWN ABOVE RS 232 TO RS 485 CONVERTER FULL DUPLEX 4 WIRE AMETEK 73858SE COMPUTER RS 232 9 PIN D CONN 9 PIN D CONN PIN D CONN 4 RECEIVE 2 TRANSMIT RECEIVE 5 RECEIVE 3 RECEIVE TRANSMIT 8 TRANSMIT M DTR 9 t TRANSMIT t GROUND 7 RIS I O OPTION MODULE TO COMPUTER RS 485 WIRING Wiring Diagrams 7 5 SNAP ODC5SRC 1 Positive Common 2 I O 1 DB9 MALE 4 4 Channel 1 6 Channel 2 8 Channel 3 ON e O 2 e 2 Channel 0 Figure 7 6 O 1 DB9 connector pinout for SNAP ODC5SRC digital output module 4 channel 5 60 Volt DC 7 6 AMETEK ProLine Mas
26. all the sample line Once all of the valves have been opened and the pressure response is verified sample analysis can begin Extended Pressure Range Option Appendix B 11 Inlet Pressure Controller Settings These parameters are set at the factory and should not require any adjustment For a complete description of each parameter refer to the controller manufac turer s documentation which is included with your unit Figure A 2 10 For Watlow Series 96 Inlet Pressure controller settings Appendix B 12 AMETEK ProLine Mass Spectrometer OPEr USEr A M Auto Aut OFF AtSP 90 CAL1 0 OPEr Pid Pb 1 160 IT 120 02 DE 1 0 01 Set InP1 Sen1 Proc In 10 10 rL 10 rH 1 776 dEC1 0 Ftr1 0 0 Set Out1 Ot 1 hEAt Prc1 0 20 Set GLbL Unit SI Err nLAt FAIL bPLS PLSP 999 PL A 100 0 PL b 100 0 rP OFF ORLP OFF Figure A 2 10b For Watlow EZ Zone PM controller Inlet Pressure controller settings Extended Pressure Range Option Appendix B 13 Ad S MAP n s OPERATTONS READ ONLY READ ONLY 0 READ ONLY READ ONLY READ ONLY READ ONLY Appendix B 14 AMETEK ProLine Mass Spectrometer Black Flow Switch Optional Orange Green LINE Black Black 5 ange l Bown amp i Pressure Brown A Red Controller 5 Be d 6 Black NEUTRAL White 1or2 Red 1 3or4 Black 2
27. four pump mounting nuts Remove the packing material and discard it Next adjust the mounting nuts so that they are close to but do not touch the washers beneath them This allows the pump to float on the spring mounts reducing vibration to the unit See Figure A2 4 Manual Regulator Attach the power cable white connector on the extended pressure range module to one of the three line voltage outlets on power distribution box on the underside of the ProLine Figure A2 5 The signal cable is hardwired to either the opposite end of the inside of the base enclosure or if you also have the OPTO 22 option to the back of that option Reach into the base enclosure and find the signal cable Attach it to the signal plug on the electronics box of the extended pressure range option See Figure A2 4 Extended Pressure Range Option Appendix B 5 9 Once the pump mounting springs have been adjusted the power cable con nected and the signal cable connected you can slide the tray holding the ex tended pressure range option back into the base enclosure and secure it using the four mounting screws 10 Reattach all tubing Figure A2 6 Valve manifold tube Common exhaust tube ProLine Unit Valve Manifold i B Figure A 2 6 Tube mE en Location of valve EN manifold and exhaust tubing and exhaust Common ort Exhaust dide Tube Exhaust Extended Pressure Range Option Port Exhaust port m
28. in a corrosive explosive or combustible me dium unless the equipment is specifically designed for such service or exposure to any other service or environment of greater severity than that for which the equipment was designed The warranty does not apply to used or secondhand equipment nor extend to anyone other than the original pur chaser from us THIS WARRANTY IS GIVEN AND ACCEPTED IN LIEU OF ALL OTHER WARRANTIES WHETHER EXPRESS OR IMPLIED INCLUDING WITHOUT LIMITATION AND WARRANTIES OF FITNESS OR OF MERCHANTABILITY OTHER THAN AS EXPRESSLY SET FORTH HEREIN AND OF ALL OTHER OBLIGA TIONS OR LIABILITIES ON OUR PART IN NO EVENT SHALL WE BE LIABLE UNDER THIS WARRANTY OR ANY OTHER PROVISION OF THIS AGREEMENT FOR ANY ANTICIPATED OR LOST PROFITS INCI DENTAL DAMAGES CONSEQUENTIAL DAMAGES TIME CHANGES OR ANY OTHER LOSSES IN CURRED BY THE ORIGINAL PURCHASER OR ANY THIRD PARTY IN CONNECTION WITH THE PUR CHASE INSTALLATION REPAIR OR OPERATION OF EQUIPMENT OR ANY PART THEREOF COVERED BY THIS WARRANTY OR OTHERWISE WE MAKE NO WARRANTY EXPRESS OR IMPLIED INCLUD ING WITHOUT LIMITATION ANY WARRANTIES OF FITNESS OR OF MERCHANTABILITY AS TO ANY OTHER MANUFACTURER S EQUIPMENT WHETHER SOLD SEPARATELY OR IN CONJUNCTION WITH EQUIPMENT OF OUR MANUFACTURE WE DO NOT AUTHORIZE ANY REPRESENTATIVE OR OTHER PERSON TO ASSUME FOR US ANY LIABILITY IN CONNECTION WITH EQUIPMENT OR ANY PART THEREOF COVERED BY THIS WARRANTY XI This page intentionally
29. is fully pushed onto the feedthrough contacts Reset the electronics by unplugging the power cable from the unit and plug ging it back in Check the continuity between the filament feedthroughs Although protected the thoriated iridium filament will eventually wear out The best way to determine if this is the case 1s to check the filament continu ity The check should be performed on the pins on the atmosphere side of the unit Figure 4 9 The pins should be electrically isolated from each other and from ground There should be approximately one ohm continuous circuit between the filament Pins 3 and 8 They should be isolated from ground Maintenance amp Troubleshooting 4 19 A AMENT 6 Sa AMENI C DE r x Figure 4 9 Quadrupole head pinout view of flange atmosphere side Ifno continuity exists between Pins 3 and 8 remove the quadrupole head from the vacuum system and replace the filament assembly with a replacement filament assembly If the problem persists after going through these steps you will have to localize the problem area These potential problem areas are e Electronics Communications and LEDs e Filament LED 4 20 AMETEK ProLine Mass Spectrometer Electronics Communications and LEDs 1 Make sure the power su
30. operating pressure and temperature Open the Process 2000 software to the Process Status screen and open a sample valve by clicking on the red OFF indicator under the State column changing it to green ON Figure A2 9 RUN Sampling stream cal blend ECC NL e e TE Process Status Scan Data Status Inputs Digtal Dutputs Valves Name Value Unit Alarm Message a Main Box Temp o 0 Main Box Temp LOW Valve Box Temp o o Valve Box Temp LOW Turbo Pump Speed o 1 Turbo Pump Status o o Turbo Pump FAULT Flow Switch 1 o 0 Flow 1 LOW Flow Switch 2 o o Flow 82 LOW Moisture Detector o 0 Dymax Inlet Pressure o 0 ton Inlet Prop Valve o WI ENERO iil Sample Temp OK 1 o 0 Sample Temp 1 LOW Sample Temp OK 2 o 0 Sample Temp 2 LOW oI s To check the flow on the valve that you just opened on the Process Status screen click Status Inputs The Status Inputs screen displays Figure A2 10 Locate Flow Switch 1 in the left hand column If the sample flow is ad justed correctly the indicator beside the flow switch will be green If it 1s not flowing properly the indicator will be red Green Indicator on Flow Switch If the Flow Switch indicator 1s green you can continue checking all of the other valves by turning them on one at a time and checking the flow following the same procedure as for the first valve If all of the valves show proper flow test the operation of the switch itself by blocking one of the lines and then turning
31. percentage reading is below 20 lower the controller setting Repeat the setpoint adjustment until the percentage is within the 20 to 50 range 2 Open each of the sample and calibration valves manually using the Process 2000 software Note the Inlet Pressure on the Status Input screen before continuing NOTE On the Process Status screen click Valves A listing of all of the valves appears with an indication as to whether the valve 1s open green or closed red Figure A2 9 Open each valve by clicking on the red indicator under the State column Appendix B 8 AMETEK ProLine Mass Spectrometer Figure A 2 9 Valve status screen WMEKNNM eee to change the valve from closed to open green All valves should have a green indicator showing they are all open The pressure should stabilize at the setpoint in less than 15 seconds You may need to adjust the regulators on the calibration gas tanks to keep the inlet pressure in range Extended Pressure Range Option Appendix B 9 Adjusting the Flow Switch E Flow Switch is an option NOTE There is a flow switch inside the extended pressure range module that senses flow through the sample inlet valve currently selected Figure A2 2 point 7 The flow switch 1s set and tested at the factory but may need to be adjusted once all the sample lines are connected Figure A 2 10 Status input screen Make sure that the power is on and all sample lines are at
32. possible Always remove 24 VDC power from the Dymaxion electronics before removing the electronics from the sensor CAUTION Installation Operation 3 1 ProLine System Overview Inlet Valve Backing Pump I O Option Card Controller Inlet Heater Pump Controller Controller Interface Turbo Pump Figure 3 1 ProLine front view 3 2 AMETEK ProLine Mass Spectrometer Pumping System Installation The ProLine pumping system consists of the following e Turbo Pump turbo pump power cable RS 485 to pump controller cable flexible hose that connects the backing pump to the turbo pump e Backing Pump backing pump power cable Installing the Turbo Pump The sensor head and manifold are already attached to the turbo pump at the fac tory Remove any packing from the turbo pump The turbo pump will be mounted using the guides on the ProLine between the sample inlet box and the electronics box 1 Remove the top cover from the sample inlet box by removing the four screws holding the cover to the box 2 There is a U shaped cutout on the back wall of the sample box through which the sensor head and manifold will be positioned to provide access to the inlets There is also a piece of black metal with a U shaped cutout that is used to secure the sensor manifold in place 3 Set the turbo pump between the guides and rotate until you have positioned the sensor manifold correctly in the U shaped slot on the sam
33. that valve on When you check the Appendix B 10 AMETEK ProLine Mass Spectrometer Status Input screen for the status of the Flow Switch the indicator should turn red flow blocked after 5 or 10 seconds to show that the flow switch is working properly Red Indicator on Flow Switch Adjust Flow If the Flow Switch indicator remains red once the valve is opened and proper flow is expected you will need to adjust the flow switch e Locate the flow switch adjust access hole on the front of the extended pres sure range module Figure A2 11 Using a flat blade screwdriver insert it into the access hole and turn the adjusting screw inside clockwise until the indicator on the Status Input screen just turns green Turn 1 4 turn more Figure A 2 11 Location of flow switch adjust access hole Flow Switch Adjust Access Hole Exhaust _7 rr C ontroller Inlet e Test the flow by blocking the sample line The Flow Switch indicator should turn red to show that the sample gas is not flowing through the switch e Ifthe Flow Switch indicator remains green after the sample line has been blocked turn the adjusting screw counterclockwise until the Flow Switch in dicator just turns red Turn 1 4 turn more Unblock the sample line The Flow Switch indicator should turn green to indicate that gas 1s flowing through the switch After making these adjustments cycle through all of the valves to ensure cor rect operation of
34. the unit casing remove the upper left and bottom right 3 8 screws with internal tooth lock washer from the heat sink See Figure 5 4 Gently pull on the front heat sink to remove it The LED panel is now visible Scan Board LEDs Board Figure 5 4 Control and Scan boards Screw for Scan Board Front Heat Sink Control Board S SS N SS Screws for Heat Sink 5 6 AMETEK ProLine Mass Spectrometer 7 Remove the 1 4 screw from the bottom left of the LED panel 8 Gently pull the Control board away from the adhesive gap pad on the back of the LED panel Replacing the Control Board 1 Attach the LED panel at the bottom left using the 1 4 screw 2 Replace the front heat sink using the 3 8 screws and lock washers on upper left and bottom right 3 Insert the board into the unit making sure the four connectors 2 on each side are plugged in 4 Replace or retighten the screws for the option plate to put it back in place 5 Replace the 1 4 screws on the top and bottom and the 3 16 screw on the right side of the unit casing 6 Replace the I O Option board There are adhesive gap pads on the back side of the front heat sink and the LED panel to ensure that all fixtures are secure and in place NOTE Electronics Boards Parts 5 7 Scan Board Removing the Scan Board The Scan board is located across from the Control board and to its right behind the LED panel and the f
35. turbo pump controller interface Electronics all models Specify AMU range and whether the unit is Faraday or Multiplier Fan electronics cooling Fan turbo pump Ferrule 0 4mm ID 1 16 fitting Filament iridium Filament tungsten Fuse 120V 6 3Amp slow blow Fuse 120V 8 Amp Fuse 230V 3 15 Amp slow blow Fuse 120V Extended Range ProLine 10 Amp slow blow Fuse 230V Extended Range ProLine Gasket 2 3 4 copper Gasket 4 1 2 copper Heater finned strip 24V 100W Heater jacket Inlet assembly 8 valve Inlet manifold Ion volume Power supply 24 VDC out 150W 80545SE 09073JE 25654JE 12087JE 90519VE 75013SE 25584JE 33477JE 95499VE 74654SE 2092 JE 2099 JE 25693JE 25779JE Consult Factory GAS0001 GAS0002 25656JE 75018SE 74936SE 7493 1SE 74844KE 25648JE Service and Parts Replacement 6 9 Pump dry diaphragm voltage slectable Pump rotary vane 110V Pump rotary vane 230V Pump turbo Relay solid state Sensor 100 AMU Shield turbo pump protection Valve solenoid 3 way manifold mount 24 VDC Valve vent turbo pump 6 10 AMETEK ProLine Mass Spectrometer 38032JE 38033JE 38035JE 38031JE 25650JE 75028SE 42343JE 36075JE 36066JE WIRING DIAGRAMS p SNOILd0 INDHITA SLINN No cartaans UN SNULLO3NNUO X3M0d SNULLdD ALIHM TWALAGN XW 3ND Z AUTIA N33889 an ALIHA WLAN y IP Moya INIT 7 Fr
36. x 5 DC Connectors POWER SUPPLY AC id component side Pump Controller Connector m AC Box Power Switch Valve Control 2 Board 4 ad i Power Supply Figure 6 1 E CE BOE Inside of electronics EJ box back view Service and Parts Replacement 6 3 gt Each power supply has three connectors attached to the board a single AC connector and two DC connectors Remove these connectors from the board Replacing the power supply boards l The power supplies have three connectors that must be attached before mounting the board to the bracket Replace the one AC connector and the two DC connectors on the board Using a Philips screwdriver attach the board using the five screws to the standoffs that hold the power supply board to the U bracket Replace the covers of the electronics box Valve Control Board In order to access the valve control board you must remove the U bracket from the electronics box Removing the valve control board l 2 Remove the top and rear covers of the electronics box If your analyzer has the computer option remove the computer assembly as described in the appendix of this manual There are three optionally four connectors on the valve control board that must be removed If your analyzer uses the 8 valve system there is one valve control connector J4 on the top of the board
37. 4 Pull out the front panel and Master board Replacing the Master Board 1 Place the new board with attached front panel into the slot from which you removed the old board There is one connector into which to plug the re placement board 2 Replace or retighten the screws for the option plate to put it back in place 3 Secure the board and front panel in place using the 1 4 screws for the top and bottom of the unit and the 3 16 screw for the left side 4 Using the information that you recorded from your old board set the RS 485 and RS 232 RS 485 dipswitch settings Plug in the cables as required 5 Replace the I O Option board Electronics Boards Parts 5 5 Control Board Removing the Control Board The Control Board is located behind the front heat sink and the LED panel on the left hand side see Figure 5 1 It is the shorter of the two boards attached to the LED panel To remove the Control board follow these steps l A Control Remove the I O Option board Remove the 1 4 screws from the front top and bottom casing of the unit and the 3 16 screw from the right side See Figure 5 1 Loosen or remove the screws at the top and bottom of the option plate to al low easier access to the removal of the Control board Grab the heat sink and pull on it to remove the assembly with the Control and Scan boards It is connected to the unit by four connectors Once the assembly has been removed from
38. 8 152 156 10 a as 152 156 160 16s 6 172 176 180 184 188 spsps s 9 A A A A SJ S 5 5 e falelelelalelelelalelelelale fe Fisz 396 200 204 208 212 216 226 204 25 2 36 29 2s 226 252 e c e e t t F TF F7 re ps etol4 51e 9o 15151619 151516 ASCII Mode with CRC16 supported by Opto Control and PAC Control Upper address 9 51 8 32 15 20 e e elele lele switch ESXEZEJIECIEIEBESEIEIEAEZNEIEZETESETI Lower address lap ee ep lp e switch ea 68 72 76 a0 84 Te sz 96 100 108 108 12 116 12 124 4 4 4 4 5 5 5 5 6 6 6 6 7 7 7 7 1 5 9 D 1 5 9 D 1 5 9 D 1 5 9 D Fas 152 13 9 aa a8 152 156 16 16s 166 172 76 380 38 388 s s s s s A j AOJA 8 8 9 9 pt 9 95 ee ree e b pe 9 5 Fisz 6 09 204 298 212 246 226 204 2 2 36 49 2s 226 257 e c e e t F F F r Peepers 15 131519 po Appendix A 8 AMETEK ProLine Mass Spectrometer Binary Mode with Checksum not supported by Opto Control and PAC Control WY vn wv ES O oO i wv e c D 2C W n Lower address switch ASCII Mode with Checksum not supported by Opto Control and PAC Control WY vn w ES lt 5 ge w qD c e D 2C W ad E n Lower address switch Opto 22 Option Appendix A 9 RS 232 to RS 485 Converter Cable Figure 1 RS 232 to RS 485 V Jj converter cable f eai
39. AMETEK ProLine Mass Spectrometer User Manual AMETEK o Process Instruments 149001 150 Freeport Road 90516VE REV ZB Pittsburgh PA 15238 Offices USA HEADQUARTERS AMETEK Process Instruments 150 Freeport Road Pittsburgh PA 15238 USA Phone 412 828 9040 Fax 412 826 0399 USA Delaware AMETEK Process Instruments 455 Corporate Boulevard Newark Delaware 19702 USA Phone 302 456 4400 Main 800 537 6044 Service 800 222 6789 Ordering Fax 302 456 4444 USA Texas AMETEK Process Instruments 4903 W Sam Houston Pkwy North Suite A 400 Houston Texas 77041 USA Phone 713 466 4900 Fax 713 849 1924 CANADA AMETEK Process Instruments 2876 Sunridge Way N E Calgary Alberta Canada TIY 7H9 Phone 403 235 8400 Fax 403 248 3550 2007 AMETEK GERMANY AMETEK GmbH Postfach 2165 D 40644 Meerbusch OR Rudolf Diesel Strasse 16 D 40670 Meerbusch Germany Phone 49 21 59 9136 0 Fax 49 21 59 9136 39 SINGAPORE AMETEK Singapore PVT Ltd 10 Ang Mo Kio Street 65 705 12 Techpoint Singapore 569059 Republic of Singapore Phone 65 484 2388 Fax 065 481 6588 FRANCE AMETEK SAS Rond Point de l pine des champs Buroplus Bat D 78990 Elancourt France Phone 33 1 30 68 89 20 Fax 33 13038 89 29 CHINA AMETEK Process Instruments Room 408 Metro Tower No 30 Tian Yao Qiao Road Shanghai 200030 Phone 8621 6426 8111 Fax 8621 6426 7818 This manual is a guide for the use o
40. DI WHITE 8 1 0 MODULE TO TURBO CABLE 9 PIN D CONNECTOR 15 PIN D CONNECTOR g Die REB 8 8 DI BLACK 10 4 DI3 WHITE 9 9i DI3 GREEN 10 1 TURBO PUMP 1 0 MODULE INTERFACE CABLE 9 PIN D CONNECTOR f1 DOO BLACK 2 DO BROWN 3 DOP RED 4 DO3 ORANGE 5 DOS YELLOW 6 DO COMMON BLUE 7 D GRAY 8 DIL WHITE INTERNAL 1 0 MODULE INTERFACE CABLE 9 PIN D CONNECTOR 1 DOO BLACK 2 DO BROWN 3 DU RED 4 DO3 ORANGE 5 DOS YELLOW 6 DO COMMON BLUE 7 DI GRAY 8 DI WHITE VALVE CONTROL BOARD A BLACK va 1 LVES 1 8 B BROWN V i C RED D ORANGE Gt YELLOW J3 GND BLUE VALVES 9 16 TEMPERATURE CONTROLLER INLET HEATER MODEL 935 DUTPUT 2 WHITE OUTPUT 2 GRAY MODEL SD3f DUTPUT 2 WHITE DUTPUT 2 GRAY VALVE 1 8 CABLE 25 PIN D CONNECTOR 1 VALVE BLACK e VALVE 2 WHITE 3 VALVE 3 BROWN 4 VALVE 4 WHITE 5 VALVE 5 RED 6 VALVE 6 WHITE 7 ORANGE 8 2 9 VALVE 9 16 CABLE 25 PIN D CONNECTOR VALVE 9 BLACK VALVE 10 WHITE VALVE 11 BROWN VALVE 12 WHITE VALVE 13 RED VALVE 14 WHITE VALVE 15 ORANGE VALVE16 WHITE 24V YELLOW ON O OI 4 O amp M ul Figure 7 3 VALVES 1 8 VALVES 9 16 p QD mum WwW O I Ce DD e WN WN WN O gt WW 1 o Od Ww LLI a z L c gt gt o m o0 AUR 85 do 9 c aA
41. Geld l a Power Supply len Heat Power Supply iiid Turbo Pump Dymaxion Fan Service and Parts Replacement 6 5 Power Switch The power switch is located on the rear side on the outside of the electronics box The only replaceable parts on the switch are the fuses If you need to replace the power switch you must call the factory for assistance Do not attempt to replace the switch or any items in the AC power box yourself CAUTION Replacing the power switch fuses Make sure that you have removed power to the analyzer by switching off the power CAUTION 1 There is a small tab at the top of the outside of the power switch Using your fingernail or a small screwdriver pull down the tab to open the door exposing the fuse holders 2 There are two fuses that power the switch which are located in fuse holders that slide out from the switch box There are directional arrows at the bottom of the switch door and on each of the fuse holders to indicate correct orienta tion upon replacement 3 Slide out the fuse holders and remove the fuses Replace the burned out fuses with new fuses If you have a 120V system use an 8 Amp fuse if you have a 230V system use a 3 15 Amp fuse Units with the sub atmospheric pump option will have an 10 Amp slow blow fuse 110V or a5 Amp slow blow fuse 230V Check the fuse you are replacing to determine the correct one to use the standard fuses with an 10 Amp slow blo
42. I2 SPARE DI3 Position 2 through 6 Available Device Address 130 Factory Configured Position 7 Inlet Pressure All4 Inlet Proportional Valve ATIS I O 1 DB 9 Connector Pinouts for SNAP ODC5SRC Digital Output Module 4 ch 5 60 VDC I O 1 DB9 SNAP ODC5SRC 2 Channel 0 4 Channel 1 6 Channel 2 8 Channel 3 CEO BN e NOTE Baud Rate Baud Rate is 38 4 1 Positive Common See included module specification sheets for more information Jumper Position 3 2 1 0 Appendix A 2 AMETEK ProLine Mass Spectrometer I O MODULES SNAP D T gt gt DIGITAL INPUT MODULES DATA SHEET page 6 13 Form 773 030529 SNAP IDC5 SW and SNAP IDC5 SW NC Modules Description The SNAP IDC5 SW and SNAP IDC5 SW NC modules provide four channels of contact status input Each module supplies 15 volts of power to an external dry contact switch The SNAP IDC5 SW senses switch closure the SNAP IDC5 SW NC senses switch opening Each user supplied switch is connected with two wires Because these modules include power for the switch they are particularly cost effective when labor costs for wiring external power are high Specifications Field Side Ratings each channel 15 VDC typical Open Circuit Voltage Switch Open Short Circuit Current 7 milliamps nominal Switch Closed Minimum Off Resistance gt 20 K ohms Maximum Allowable On 500 ohms Resistance Wire Contact Resistance Logic Side Ratings
43. MODLATCH 16 14 12 10 8 6 4 2 D3 D2 D1 DO SNAP D GITAL MODULE BASE CONTROL CONNECTOR BOTTOM V EW Opto 22 Option Appendix A 3 I O MODULES SNAP l y P T gt 2 DIGITAL OUTPUT MODULES DATA SHEET page 11 21 TOU baza Part Number Description z 4 channel DC output 5 60 VDC logic Schematics ANE DOC Te oires j SNAP ODC5SRC 4 channel DC output 5 60 VDC logic Output Module Sourcing e source Factory Mutual approved NOTE See page 16 for FM modification FIELD WIRING DC SOURCING OUTPUT FIELD TERMINAL POSITIONS 1 3 5 AND 7 ARE INTERNAL BUSSED CONNECTIONS COMMUTATING DIODE MUST BE USED ON INDUCTIVE LOADS TYPICAL 1N4005 SNAP MODULE FIELD CONNECTOR a a ae ee VVJ ee E I SNAP DC OUTPUT SOURCING I PLUG GABLE ON BOARD FUSE ON BOARD FUSE AND m E mE FUSE HOLDER e SV POSITIVE z COMMON CHO I I I I I I iL I I ETE E E dit fogon E 5 I I iL I I WR a i J 4 cH2 PIN 1 E SNAP MODULE RELEASE LATCH ae 7 L_ OPTO 22 PART SNAP MODLATCH FORWARD PIN TH a I l CH3 A J CONTROL SIDE 8 6 4 2 D3 D2 DI DO SNAP DIGITAL MODULE BASE CONTROL CONNECTOR BOTTOM VIEW Appendix A 4 AMETEK ProLine Mass Spectrometer Installation The Opto 22 SNAP
44. NN RK MANA 4 7 CTS 6S OUI era rem ed nl akid lak al dial ei 4 7 Eguipmentreguiredtoreplaceafilament 4 8 Removing the electronics from the quadrupole head 4 8 POD DICIT nii 4 8 Disassembling TEC SO eke a a is a el E Ihm mM MM UM 4 11 IGS Be lt P PAP FE YE SEE UU DINI EEE EEE MA YA A N PM ONDE 4 11 Disassembly of conductance limited enclosed source 4 11 Cleaning the conductance limited enclosedsource 4 12 Assembling the conductance limited enclosedsource 4 15 Capillary Sa AH tcc TT OR 4 16 Elector MUIGPH OT e ee e a e a mais FUP PRETI HINT lm lala nal 4 18 iv AMETEK ProLine Mass Spectrometer Tro blesh ootna The JIC ROMICS A RR RANN NER 4 19 Ehime so ee SE yea lay yene elem alam amaaa amd 4 19 Occ and Easy SoOIUTOS MA REN ee EN GR YARAM EMEN 4 19 Electronics Communications and LES eee pietre ra rii Sen ERR S sb 4 2 Filament ngog LEDS L 4 22 CHAPTER 5 Board Replacement arde soci METRE T MC E 5 2 Masir BO ENE ARM E RR 5 5 TN D OT MNT 5 6 ICH OB PRI T RR 5 8 ZUBDDE did PE RR PE ENE E E mde tmi Ii iM MN one IP 5 10 RFC a EYE EE a TT 5 11 CHAPTER 6 Service and Parts Replacement Components in the Electronics BOX oes i e apseli vin at tds es anre pd unte 6 1 Accessing the Electronics Box Contents x csscesveneereevazerienseetevestelar
45. O O BE O m o oL SR 3 9 RE O O O O reg gt OUZ E ole o O do O mi D o B o AgL g8 amp o O EE B nr N Z ny a0 oOo o pi gt 06 De O J P13 JPI2 JPM JPL lt C15 C13 10 S o JP 10 ie ogo oo 6 6 6 Oldar zap S gt o gt gt ei O Figure 5 2c I O Option board show ing jumpers C16 C14 5 4 AMETEK ProLine Mass Spectrometer Master Board The Master board is found behind the front panel of the electronics unit to the left of the heat sink see Figure 5 1 The entire front panel is part of the Master board and is returned to the factory when a replacement board is ordered Make sure that the RS 485 and RS 232 RS 485 dipswitch settings are fy recorded before shipping the board to the factory to facilitate setting NOTE up the new replacement board Also note the outlets to which your cables are connected on the panel See Figure 5 2 Removing the Master Board To remove the Master board follow these steps 1 Remove the I O Option board for easier access 2 Remove the 1 4 screws from the top and bottom of the unit and the 3 16 screw from the left side of the unit see Figure 5 1 These three screws hold the board in place 3 Loosen or remove the screws at the top and bottom of the option plate to al low easier access to the removal of the Master board
46. P AOA 23 Dual channel analog output 4 20 mA current loop Output 4 20 mA Description The SNAP AOA 23 module provides a nominal output range of 4 mA to 20 mA An external loop power source is EXTERNAL LOOP required for the current loops POWER SUPPLY NOTE Both channels share a common reference terminal NOTE THIS MODULE MUST BE USED WITH AN EXTERNAL LOOP POWER SUPPLY Specifications Input 12 bit serial data each channel Outputs 4to 20 mA each channel 3 Response Time 96 of span delta 99 9 15 98 mA 3 mS delta time DC Common Mode 120 dB Rejection lt lt AC Common Mode Maximum Operating Common Mode Voltage SNAP MODULE FIELD CONNECTOR OPTO 22 PART SNAP FIELDCON Resistance Accuracy 0 196 of Span ca Gain Temperature PIN 1 Coefficient FIRST FORWARD PIN 50 PPM C SNAP MODULE RELEASE LATCH OPTO 22 PART SNAP MODLATCH 5V RTN 5V e u on co Loop Power 8 Volts DC min to 32 Volts DC max 18 16 14 12 10 8 6 4 2 a 5 LU LL in Max Loop m Resistance Ohms 250 450 650 1050 1450 Loop Supply 8V 12V 15V 24V 32V SNAP ANALOG MODULE BASE CONTROL CONNECTOR BOTTOM VIEW Max Loop Loop Loop Voltage 3 Resistance formula Resistance 0 02 77 MO Ambient Temperature A2 2 ProMaxion Process Mass Spectrometer EXTENDED PRESSURE RANGE OPTION Description The extended pressure range option is
47. ample calibration lines to the Sample Gas In port bulkhead fittings using 1 8 stainless steel tubing and 1 8 Swagelok nuts and fer rules Make sure that the tubing is installed as far into the fitting as possible 2 Hnecessary vent the Sample Gas Out lines from the process streams to a safe area e g a fume hood To conserve calibration gas cap the calibration gas line with a 1 8 Swagelok cap to ensure that calibration gas will not flow when another valve is selected 3 The sample gas exhaust is the last of the Gas Out fittings on the right front of the sample inlet box Figure 3 9 Use appropriate caution when venting the gas and vent at atmospheric pressure Gas Inlet Tubing Figure 3 9 Sample Gas In and Sample Gas Out ports 3 12 AMETEK ProLine Mass Spectrometer Purging the pressure regulator and calibration gas line Since the calibration gas line outlet is capped to ensure that the calibration gas will not flow when another valve is selected there is the possibility that gas may be residing in the dead space between the cap and the cal gas flow To ensure that the gas available for calibration is pure you will need to purge the calibration gas line as well as the pressure regulator on the calibration gas cylinder If the calibration gas is hazardous before proceeding make sure that you are able to vent the calibration gas to a safe location and with CAUTION appropriate caution
48. and two connectors I O Option and power on the side of the board closest to the front of the unit If you have a 16 valve unit there will be two valve control connectors J4 and J3 on the top See Figure 6 2 Once the connectors have been removed you will be able to tilt the entire U bracket and lay it on its right side so that the valve control board 1s facing up and you can access the screws to remove it Remove the valve control board by loosening the four screws holding the board to the standoffs 6 4 AMETEK ProLine Mass Spectrometer Replacing the valve control board To replace the valve control board follow these instructions l DySignal Valve Connector er Attach the board to the four standoffs on the U bracket using the screws you removed Attach either one 8 valve unit at position J4 or two 16 valve unit valve control connectors positions J4 and J3 to the top of the board Attach the I O Option and power connectors to the side of the valve control board Tilt the U bracket back to its original position so that it 1s seated on the floor of the electronics box Reattach the U bracket to the floor of the box using the four screws Replace the covers of the electronics box Power NOT USED Connectors to valves Valve Connector Figure 6 2 Valve Control board Component Side N mm Connectors lt 13 J4 I O Option gt Valve Conero B Power gt
49. ange option system and slides out for easy access The unit provides four 4 I O connectors and one RS 485 connector Figure 1 8 More information on configuring your I O system can be found in the Appendix of this manual Figure 1 8 Opto l O option for the ProLine Figure 1 9 On Board PC located in electronics box 1 14 AMETEK ProLine Mass Spectrometer On Board PC CE Pending This option includes an on board PC located in the electronics box Figure 1 9 The on board PC communicates with a remote PC using an Ethernet crossover CAT 5 cable plugged into an Ethernet port The on board PC can also communicate through a network LAN using a standard Ethernet cable The remote computer computer uses Mi crosoft s Remote Desktop Communication soft ware over the 10 100 Base T interface to establish communications Instructions for connection and operation are included in the Process 2000 software manual Technical Support AMETEK is committed to providing you with the best technical support in the industry If you need service or application assistance please call AMETEK at 412 828 9040 or call your local AMETEK representative If you need to return equipment you will be asked to provide the following infor mation before obtaining a Return Material Authorization RMA number e Billing and shipping address e Model number Serial number Purchase order number e Telephone number Overview 1 15 Th
50. ary replacement dimensions 7 The drawing in Figure 4 8 is a representation of the capillary con Tr figuration and does not depict the capillary when in use Tolerance on the capillary dimensions is 06 1 5mm NOTE ION Use safety glasses when uncoiling and cutting the capillary 1 Uncoil the capillary carefully and cut to a length of 7 5 inches 190mm us ing a capillary precision cutting tool SGE 0625010 or comparable tool 2 Mark insertion dimensions on each end using tape or permanent marker Mark the end that you insert into the ferrule on the inlet flange 2 2 inches 57mm from the end Mark the end you insert into the ferrule on the flowby tee 0 9 inches 22mm from that end 3 Loosen the nut holding the ferrule on the inlet flange to release the ferrule Figure 4 8 Thread the capillary through the ferrule 4 16 AMETEK ProLine Mass Spectrometer Insert the ferrule and capillary onto the inlet flange and secure with the nut just to keep in place Adjust the capillary to the insertion point you marked by loosening the nut to allow the capillary to move in and out easily Once the capillary is in the correct position at the insertion point you marked tighten the nut until the capillary is grasped and then tighten 1 4 turn more Do not overtighten Repeat the insertion process for the ferrule on the flowby tee Once the capillary is secure in both ferrules and at the correct insertion poin
51. d only with the same type and ratings as described on the power label Fuse must be certified listed BURN HAZARD The spectrometer heater jacket normally operates at 60 C 140 F on the surface and 110 C 230 F inside The inlet heater can reach 180 C 356 F AVOID CON TACT Grounding Instrument grounding is mandatory Performance specifications and safety protection are void if instru ment is operated from an improperly grounded power source Verify ground continuity of all equipment before applying power WARNING Chemical Safety This instrument may be used to measure process gases and vapors that may be hazardous The user must check the Material Safety Data Sheet MSDS as well as local and national regulations before dispensing and disposing any hazardous material Route exhaust lines ap propriately WARNING All process tubing and connectors are required to be suitable for the maximum pressure involved On oil vane pumps maintain proper oil level DO NOT OVERFILL CAUTION vill AMETEK ProLine Mass Spectrometer Warning Labels These symbols may appear on the instrument in order to alert you of existing conditions PRo TEc TiVE conduc ToR TERMIn AI Bo Rni ER dE EcRAn d E PRo TEc Tion s chutzerde CA u Tion Risk of electric shock ATTEn Tion Ris Qu E d E d Ec HARg E EI Ec TRiQu E Achtung Hochspannung ebensgefahr CA u Tion Refer to accompanying documents ATTEn Tion s
52. e you will have to loosen the springs on the sub at ProLine mospheric pump to free it for use The springs were tightened down at the factory to prevent damage during shipping and help reduce vibration when the analyzer is operating To release the springs on the sub stmospheric pump follow these steps 1 Loosen the four captured screws on the face of the tray that holds the sub atmospheric pump 2 Detach the inlet tubing from the inlet ports using a 9 16 wrench 3 Gently slide the tray towards you to allow access to the nuts that hold the springs down under the pump 4 Loosen the nuts on the springs with a 7 16 wrench until the nuts no longer touch the washers and the pump floats on the springs 5 Gently slide the tray back into the base replace the inlet tubing and secure the door with the four screws For more information on replacing the sub atmospheric pump refer to the manufacturer 5 instruction manual included with your unit NOTE Detailed information on the extended pressure range option can be x found in the Appendix 2 of this manual NOTE Overview 1 13 I O Data Acquisition Option This option is used when your application requires additional information that can only be obtained through analog digital input or output The Opto I O system consists of a series of I O modules a brain module and a power supply It 1s housed in the opposite end of the unit from the extended pressure r
53. e conductance limited enclosed source Assemble the source in reverse order of the disassembly taking care to center each ceramic washer in its seat to prevent cracking it Do NOTE not crush the ceramic washer or strip the threaded parts by over tightening the source hardware tighten to snug only 1 Install the source so that Lens 2 is seated against the ceramic quadrupole collar The hardware binding the source together may need to be loosened temporarily so that all the rods can fit through the ceramic quadrupole collar holes and so that Lens 2 can sit against the collar Carefully insert the rods through the holes in the ceramic collar and into the barrel connectors and the detector flange assembly according the pinout in Figure 4 6 Be sure that the screws are tightened snugly to the hardware once the source is in place 2 Install the filament as described in Replacing the Filament in this chapter 3 Once the quadrupole head has been checked replace the ion volume by set ting it back on the head Figure 4 5 and secure it with the lock screw Insert the head into the vacuum chamber and secure using the six bolts originally removed Maintenance amp Troubleshooting 4 15 Capillary Replacement 7 5 190 mm gt 2 2 57 mm 9 22 mm lt Connection to Inlet Valve Manifold Sr to oe ee oe 5 RS I ong e e EE WY A Flowby Tee Inlet Flange ZA Figure 4 8 Vacuum Manifold Capill
54. e electron ics package 1s inactive A red light indicates a communications error RF Shows the status of the RF circuit The LED is green if the RF amplifier is oper ating properly and turns red if you have an RF failure The LED is yellow during automatic RF tune Filament This LED indicates the status of the filament The LED is green if the filament is on and is working properly The LED appears red if the filament 1s off due to an overpressure open or short condition The LED appears yellow if half of the filament has failed Installation Operation 3 9 Heating Jacket The installation of the heating jacket requires no tools 1 There are three grounding strips on the heater jacket Figure 3 7 Before fitting the jacket to the manifold you must bend these strips around the edge of the jacket to the inside so the ground strip contacts the metal manifold surface to ground it 2 Once you have grounded the jacket position the jacket on the vacuum cham ber so that the snaps are on the back side of the manifold Once in position attach the snaps so the jacket fits snugly around the chamber Make sure the heater doesn t make contact with any other equipment or wiring that can be damaged from high temperatures 3 Plug the power cord on the jacket into the heater controller connection la beled Heater Jacket in Figure 3 2 When operating the heating jacket with the electronics package the mounting flange tempera
55. e that attracts the positively charged ions Exit Lens Quadrupole Detector lonization Chamber O Figure 1 2 Mass Filter 1 4 AMETEK ProLine Mass Spectrometer Detection The simplest detection setup consists of a Faraday cup detector An electron mul tiplier is used for amplified sensitivity A Faraday cup detector is a closed structure except for an opening that allows the ions to enter As the positive ions exit the quadrupole mass filter they strike the detector creating a current This current is then sent to the preamplifier for ampli fication and then to the data system for display When an electron multiplier is used the ions are attracted to the multiplier be cause of its negative charge As the ions strike the multiplier secondary electrons are emitted This creates a cascading effect as each secondary electron generates more secondary electrons as they move down the multiplier wall amplifying the signal by approximately one thousand The system uses a microchannel plate MCP electron multiplier It consists of an array of millions of small glass capillaries fused together in the shape of a disk The inside wall of each channel has a resistive electrically semi conductive layer forming independent electron multipliers As the ions are approaching the MCP a positive electrical gradient pulls the electrons into the MCP As they cas cade down and strike the channel walls
56. ector 15 pin Digital in Middle Connector 9 pin AnalogVO Bottom Connector 9 pin Figure 5 2b O Option board showing connectors Electronics Boards Parts 5 3 oOo 0000000 6 o o ooooo0o ae ONY gt 0000 00000 P 0000000000 Lu oooooooooo 4 N N 2 0 o6 69 59 u z vZO 000 000 000 00000000 o doe A d d mm i63 t Wy Pa ie oT oOooooooco o 2m Oo O 90 OO 9265 0 00 TN 00000000 OF a Cu o j lil o o an N n Lg 7 E B O O O O O O O O fg 2 O gt 5 20000000 o 9 Oe Oc ROK I Szo 2t 00000000 000000000000 00000200020 ee o0 009000000 OP P LNY S ae o OO0000000 9600000020709002000200202020 7 I e e al ae E Sooo OO Oo gry Spee oD a e SC CN R
57. ectors RS 485 Addressable Communications Interface Isolated baud rate selection of 1200 to 38400 programmable addresses 2 pin female D connectors Ethernet Connectivity 10 100BASE T Ethernet Auto Sensing RJ 45 connector Always use a shielded Category 5 cable for Ethernet connections This is required to minimize electromagnetic interference NOTE Dymaxion Physical Dimensions Weight 4 6 lb 2 1 kg without quad head 7 4 Ib 3 4 kg with quad head Width 4 5 11 4 cm Length 9 22 9 cm Height 5 25 13 3 cm ProLine Physical Dimensions Width 14 3 8 36 5 cm Length 24 60 96 cm Height 15 1 2 39 37 cm Software The Process 2000 software Minimum PC Requirements Pentium 233 MHz microprocessor 64 MB RAM with Windows 95 98 or NT XP Specifications 2 3 This page intentionally left blank 2 4 AMETEK ProLine Mass Spectrometer INSTALLATION OPERATION This chapter contains information of the installation and initial setup and opera tion of the ProLine including the following e ProLine System Overview e Pumping System Connections Electronics Package Installation and Connections e Sampling Setup e Software Installation e Turning the Filament On e Shutdown Procedure Electronics and Sensor ION Before connecting the 24 VDC power to the electronics ensure that the electronics are connected to the sensor Otherwise damage to the electronics is
58. ed go back to the main screen and click on the Edit menu and click Add Device Click Optomux Analog Once the analog module has been added you can proceed with setting the parameters e Configure the General tab as follows Bits per Second 9600 Device Properties xj General Tune Parameters 1 0 Setup Scripts Communications Dycor ProMaxion 2 15 Port C RS 232 Port 200 AMU Multiplier 1 0 Option com RS 485 Port Address Bits per second 9600 v 66 Quad Description Opto 22 Analog Type Optomux Analog v Live data OK Cancel Apply Help e Address 66 Type Optomux Analog Make sure that the Live Data box is checked e Click on the I O Setup tab and enter the Type and Name for the input and output channels see the example on next page Older I O systems had a single analog input or output per mod ule The SNAP I O system combines two inputs or outputs into one NOTE module For the SNAP I O system the System 2000 module number refers to a particular analog I O channel not the physical module For example if a single analog output module is installed in the first SNAP rack position the System 2000 will refer to it as Modules 0 and 1 See Figure 2 B3000 I O Mapping and Example Opto 22 Option Appendix A 15 Device Properties Modden 07 odas 15 Mete Emy Sf SS Mele Analgin z AnalogiNS Modded AnalogIN Analog IN 4 Modda Anal
59. enin salam sma esme R rede tne A 5 OPTO Brain 30009 ceder da cares cede AE NE MA AN AMA A 5 Opto Power SUPPLY EN ENE EE SERRA EN RA A 6 Opto Brain TE SOG Ee A 6 Oplo TO Modulos AN MN ME MRNA A 6 Input OUI VIOUS a akel sect e Satan eke a laa idm bl A 6 DUO FAUT A A A A AM PEN A 6 ODIO TRAC Wi OVO NR NN E PRE A 6 configuring the B3000 B OPTO Brain sakalar seksene sase sansin seninde A 7 R5 232 to RS 485 Converter Cable iiie s nen eiasisdankaiyeiebisink kadissikedi A 10 Setting the Device Properties for Digital Input Modules A 12 Add Display tor Digital Module saree emen an aR Cen MARS n SER RER E URRO RAE TE A 13 Setting Device Properties for Analog Input Modules A 15 Add Display tor Analog Module tero ett e erattu A 16 Digital and Analog OUIPUtS oe NR ECA ARANMAZ YAA A 17 APPENDIX A2 OPTO 22 User Setup APPENDIX B Extended Pressure Range Option TSUN es A A KE MN A B 1 vong gene mma ee eee A EE lr Oe eer nee eee ee a B 2 FAS L EE E kl hg ls all hs Sanil B 4 NO e a NN T A ANAK MKE NN E AN B 7 Turning On the Extended Pressure Range Module B 7 Tert A EE E p REM n DUUM B 7 Adjusting ihe e Kg Vy NN A YE A A AN O a B 10 Green Indicator om e FN A B 10 Red Indicator on Flow Switch AdjustFlow B 11 Inlet Pressure Controller Sell BS ein ERDMNIEMEPDIA ERU POEPEM PER aa B 12 Ex
60. ents Dymaxion Electronics and Sensor Before connecting the 24 VDC power to the electronics ensure that L A the electronics are connected to the sensor Otherwise damage to the electronics is possible Always remove 24 VDC power from the Dymaxion electronics before CAUTION removing the electronics from the sensor 4 6 AMETEK ProLine Mass Spectrometer Quadrupole Head Maintenance e The quadrupole head requires periodic maintenance When handling the quadrupole head follow standard vacuum practices including Do not touch any parts that resides within the vacuum system with bare hands Wear lint and powder free gloves Make sure that the area in which you are performing the maintenance 1s clean Do not blow off or dry any parts using compressed air unless you know that it is moisture and oil free After cleaning dry the parts in an oven or use a heat gun e o The entire head can be disassembled with the exception of the mass filter subassembly Most parts can be replaced if necessary e As the analyzer head is used deposits will form on the source parts and on the mass filter The lifetime of the source parts varies with application expo sure time and vacuum pressure Do not place the mass filter in an ultrasonic cleaner The filter parts can become loose during ultrasonic cleaning This will significantly degrade analyzer performance A loosened mass filter must be re placed CAUTION
61. ess photometric analyzers process moisture analyzers and sampling systems are warranted to perform the intended measurement only in the event that the customer has supplied and AMETEK has accepted valid sample stream composition data process conditions and electrical area classification prior to order acknowledgment The photometric light sources are warranted for ninety 90 days from date of shipment Resale items warranty is limited to the transferable portion of the original equipment manufacturer s warranty to AMETEK If you are returning equipment from outside the United States a statement should appear on the documentation accompanying the equip ment being returned declaring that the goods being returned for repair are American goods the name of the firm who purchased the goods and the shipment date The warranty shall not apply to any equipment or part thereof which has been tampered with or altered after leav ing our control or which has been replaced by anyone except us or which has been subject to misuse neglect abuse or improper use Misuse or abuse of the equipment or any part thereof shall be construed to include but shall not be limited to damage by negligence accident fire or force of the elements Improper use or misapplications shall be construed to include improper or inadequate protection against shock vibration high or low temperature overpres sure excess voltage and the like or operating the equipment with or
62. etesieisaetereta 6 2 Electronics Box Patts Replacement EN A O 6 3 Computer Board Replacement sisciccssasdecencazasessaseccdnarsesineiesscsasedetsncateeeeaienaeas 6 3 Power 5uppiy TOES EE REI EMEN EET 6 3 Removing the power supply DOGOFUS s s mme deye eres tv irem DESoeU eis 6 3 Replacing the power supply boards eese 6 4 Vive r Board conscia RA DEUS 6 4 REMOVING the valve control board siis eet rtt ra bre pasa ERE dESSSGS 6 4 Replacing the valve control DOQV esini seske zoe uva wu rtis Else ie qns 6 5 POW WUD rai y alli eMe UNI aliil lme al EUM yanam 6 6 Replacing the power switch fuses 6 6 Inlet Heater C OBEPOL E Eoo secede cron E E ae A YMM AE 6 7 Removing the inlet heater controller iiic bti itti akisi deese ibas 6 7 Replacing the inlet heater controller sueco eot verto e Ert mss 6 7 Turbo Pump Controller Ipnt f 306 29 0595099153990919105533390 98 5 MPRR EREEPuPESPUPS 6 8 Removing the pump controllerinterf ce 6 8 Replacingthepumpcontrollerinterface 6 8 e IPOs RE YY CE YO SPAM YAA EE CAY 6 9 CHAPTER 7 Wiring Diagrams APPENDIX A OPTO 22 SNAP Data Acquisition System Opto I O Rack 8 PositionModuleConfiguratlon A 2 DBA Connector FiOS aecuseedusdsdum aduer aIetiaiutenesem mimus eiue Eee A 2 Pud Bie ae Kek a b bm rei med Ree an ia kn A 2 m A e A 5 Components of the SNAP I O System eks
63. eturn Black 9 Pin D Conn 9 Pin D Conn 2 VSO Valve Signal White 2 7 Ground Green 7 1 Inlet Pressure Red 1 Power Supply 6 Ground Black 6 J2 10r 2 24V Red J2 3or 4 24V Return Black Figure A 2 11b Signal wiring diagram extended pressure range option without O data acquisition option Extended Pressure Range Option Appendix B 15 Black Flow Switch Optional Orange Green LINE Black Black O 533 G Pressure NEUTRAL White PRed g Controller 1 1or2 Red 7 s Ba TB1 Red 3or4 Black 1 5 Pressure Green Yellow o GROUND reaS eme 3 Transducer Green Pressure z Control Black 5 Valve Circuit Board Black 1 OPTO MODULE Fi A 2 12 2 SNAP IDC5 SW igure A 2 12a Wiring diagram extended pressure range option with O data acquisition option J1 OPTO MODULE SNAP AIV VSO Valve BN Inlet Pressure Control Board TB5 1 VSO Control Voltage Red 2 Ground Black O Data Acauisit ata Acquisition Flow Switch TB2 Option 1 Flow Switch Orange 2 Flow Switch Green SNAP IDC5 SW Module 1 CHO Black TB3 2 CHO White 1 Inlet Pressure Orange Inlet Pressure Controller 5 Ground Brown internal Cable 4 Inlet Pressure Orange 3 4 20 mA Orange Pin D Connector 6 Ground Brown lt lt 4 Ground Brown J1 1 Flow Switch B
64. f the AMETEK ProLine Mass Spectrometer Data herein has been verified and validated and is believed adequate for the intended use of this instrument If the instrument or procedures are used for purposes over and above the capabilities specified herein confir mation of their validity and suitability should be obtained otherwise AMETEK does not guarantee results and assumes no obligation or liability This publication is not a license to operate under or a recommendation to infringe upon any process patents ii AMETEK ProLine Mass Spectrometer CHAPTER 1 CHAPTER 2 CHAPTER 3 Table of Contents A a cee enn etn ne E ee ne nee NE ME IM ee ANE ll ae NO te M vil FTG CU IG AN ale BEAR RA APRE RR PE PEDER EXE AD EUN IUUENIS RUND DEEP vili 50 01 116 m Vill TAG ACA TS AR AA MS AN RAMA AR EN AA M Vill Ny a De UG esac NE YE E DR Ix EC Declaration ol Coni orni y ee en UM erdt lam a pimi X Overview Mass Spectrometer T MEYE sss diis 20100022334003543299 048994 158 1009885 IRNED 1 2 b D VSICT EE ZN n MEUM DNE 1 2 Mass Spectrometer HardWare EN MAN A AMA YAY 1 2 TOTO SK AY MN A A RO KA YE ME ONAN 1 2 LLON FAO C 1 3 1 21 UM EEN E ANAYA SANEM ER EKM 1 4 DOI OCT OI 1 5 e SUCTIN eene n a EEA EE EE E AE E AE SEEE E EEE 1 5 FO VO E E E 1 6 ProLine OVENI i aa imp E E N EEA AE tela anes 1 6 SE Si S e ol gala km EE N 1 7 iB
65. f the unit casing 5 8 AMETEK ProLine Mass Spectrometer 6 Replace the I O Option board A There are adhesive gap pads on the back side of the front heat sink ge and the LED panel to ensure that all fixtures are secure and in place NOTE Electronics Boards Parts 5 9 Amp Card Removing the Amp Card The Amp Card is part of the RF assembly at the rear of the unit It is located under the Amp cover See Figure 5 5 To remove the Amp card follow these steps 1 There are eight screws holding the RF assembly in the unit casing Remove the 2 top 1 4 and 2 bottom 1 4 screws 2 Remove the 2 3 16 screws from each side 3 Grab hold of the rear heat sink and pull hard to remove the assembly from the casing 4 You now have the complete RF assembly in your hand Refer to Figure 5 5 5 Remove the Amp cover by removing the two 1 4 self tapping sheet metal screws The Amp card is underneath 6 Remove the Amp card by removing the 4 1 4 screws holding it to the Amp card shield Replacing the Amp Card 1 Secure the Amp card onto the Amp card shield using the 4 1 4 screws 2 Attach the Amp card cover to the Amp card using the two 1 4 self tapping sheet metal screws 3 Insert the RF assembly into the unit casing and secure using the 4 1 4 screws for the top and bottom of the unit and the 4 3 16 screws for the sides 5 10 AMETEK ProLine Mass Spectrometer RF Card Removing the RF
66. filament is off due to an open or short condition The LED appears yellow if half of the filament has failed Maintenance amp Troubleshooting 4 21 Filament Trip and LEDs 1 Check the LEDs on the back of the electronics package You can determine filament status by the color of the lights Refer to the previous section for LED details 2 Make sure the filament is turned on by clicking the Light Bulb icon on the toolbar in the AMETEK System 2000 software to make sure it is yellow ON Check the filament status and emission current by accessing the Edit menu on the toolbar and clicking Add Display Click Head Status 3 Restart the entire system and recheck the filament status and emission cur rent 4 If there is no filament current turn off the instrument pull the electronics from the analyzer head and check the continuity between Pins 3 and 8 5 Ifthe filament is burned out LED is red open the vacuum system and re place the filament assembly If the filament checks out OK do the following e Check the LEDs on the back of the electronics e Ifthe LEDs are green and the filament has not tripped call the factory for assistance 4 22 AMETEK ProLine Mass Spectrometer BOARD REPLACEMENT The electronics unit contains six boards Figure 5 1 that can be replaced in the field 1f damaged or found to be not working properly These boards can be re placed using only a 1 Phillips screwdriver and a 1 4 nut driver T
67. g Valve All the gas exhausting from streams that are not being sampled passes through the regulating valve This valve is set at the factory and generally needs no adjustment Sample Pump Inlet Gas from both selected and unselected gas streams enters the sample pump at the inlet Sample Pump Exhaust Sample gases are exhausted from the sample pump at this point Calibration Gases The exhaust out ports for calibration gases are plugged to prevent calibra tion gas from flowing continuously The calibration gas IN connection is a 1 8 compression fitting Extended Pressure Range Option Appendix B 3 Installation Figure A 2 3 Clamps and clamp screws on base module shown without options inserted NOTE NOTE Remove the packaging materials that protect the unit during ship ment If the ProLine is not mounted on the base enclosure follow all of the steps below to mount the Proline If the ProLine has already been mounted to the base unit skip to Step 3 If the ProLine was attached to your extended pressure range option at the factory the fuses were replaced to accommodate this option If you are attaching the extended range option to the Proline yourself you must replace the power switch fuses A 100 120V system requires an 10 Amp slow blow fuse AMETEK 25779JE and a 200 230V system requires a 5 Amp slow blow fuse AMETEK 25702JE See Chapter 6 in this manual for instructions on replacing the fuses E
68. he back of the 0 y c Figure 3 5 to x pA Electronics Connections electronics and the connector labeled Dymax I O in Figure 3 5 RS 485 Switch Termination Settings stum When using RS 485 communications you must terminate us m ing the dipswitch settings on the back of the electronics unit as shown in the diagram on the right em Installation Operation 3 7 Figure 3 6 Communication port and LEDs LEDs The electronics LEDs are located on the back of the electronics as shown in Figure 3 6 When first started the electronics package cycles through the LEDs turning them green red and yellow This allows you to check that each LED is working properly When the unit is through cycling the top LED turns green and then the third LED RF turns green as well The LEDs are listed below in the order in which they appear top to bottom on the back of the electronics unit Hetwork Setting Switch R5 485 Connect 2 pin DBS male conector end of DCE converter to this port Switch between RS 237 and R 5 185 CPU Indicates CPU and system status OFF Electronics power is off RED CPU has stopped FLASHING RED Battery backed RAM has been cleared Check battery GREEN Normal operation 3 8 AMETEK ProLine Mass Spectrometer Comm Shows the status of communications between the electronics and the PC It flashes green when receiving data from the PC It remains off when th
69. he boards are e VO Option Board Located between the Front Panel and the LED Heat Sink e Master Board Located behind the left front panel on the front of the unit e Control Board Located behind the front heat sink and LED panel on the left side Scan Board Located behind the front heat sink and LED panel on the right side e Amp Card Located behind the rear heat sink and under the Amp cover e RF Board Located behind the rear heat sink and separated from it by the conductor guide Option Plate RF Card Control Card Master Amp Card Board 4 40 x 1 4 x screws y P di lt lt Control Small pattern kep nut Scan Card D must be used Scan Board Board 4 40 x 3 16 iy DU N TENE screws oo e se LRN gl h SON t RN SSS Front Heat Sink Figure 5 1 TUS 7 Dymaxion board Master Board locations Option Plate Front Panel Electronics Boards Parts 5 1 I O Option Board Figure 5 2a I O Option board replacement slot Front Panel is part of the Master Board and returned to the fac tory when sending in the board for replacement Replacement board includes the front panel Record NOTE The I O Option board must be removed to facilitate replacement of the Master Control and Scan boards The I O Option Board slot is located between the Front Panel and the LED Heat Sink see Figure 5 2a I O Option Board Screws Top and Bottom LED Panel 9 A
70. ics package operates at 100 AMU range us ing a Faraday cup electron multiplier detector ProLine Multi Port Sampling System The ProLine multi port sampling system Figure 1 4 comprises e an inlet system consisting of one or two sets of eight three way electric solenoid valves configurations of 8 or 16 and a valve control board Figure Lo aheatertoreducetherisk of condensation or other interference in the sample lines and a heating jacket for the sensor manifold avacuum system consisting of a turbopump and controller backing pump and associated tubing A constant pressure is maintained at the analyzer inlet using a fixed capillary in the sampling system Sample and calibration gas streams can range from 0 to 20 PSIG Gas Inlet Tubing Figure 1 4 Sampling system Overview 1 9 Valve control board The valve control board monitors valve activity If your analyzer uses the 8 valve system you will only be using one valve control connector J4 on the top of the board and the two connectors I O Option and power on the side of the board closest to the front of the unit If you have a 16 valve unit you will be using both valve control connectors J4 and J3 Connectors to valves J 3 r E Connectors E JA Bp lu I O Option T Valve Control B Power sarg d o L Power Supply Heater Power Supply Turbo Pump Dymaxion Fan Figure 1 5 Location of ProLine power supplies and valve c
71. igh performance processor used to remotely control a mix of SNAP analog and digital I O modules on a B series rack The brain connects to an Opto 22 controller or a host computer over an RS 485 serial link Opto 22 Option Appendix A 5 TX RX LED Serial l connector Reset switch MODULE MODULE MODULE lus MODULE MODULE wenn MODULE 0 1 2 3 4 5 6 7 Termination switches Address upper Address lower OPTO 22 83000 8 IRQ LED DIGITAL ANALOG STAT LED Opto Rack with I O Modules Opto Brain B3000 B Opto I O Modules d T m i m E m mir m om az ES E E IL B md ht amp a ami emi us FT TF eae SOD ob i Ma E Sy 1 fy Opto Power Supply M M al A Y 4 Input Output Modules Appendix A 6 AMETEK ProLine Mass Spectrometer Configuring the B3000 B OPTO Brain Using the B3000 B The B3000 B mistic serial brain is a drop in replacement for the obsolete B3000 serial brain The B3000 B can be used with FactoryFloor controllers running OptoControl strategies SNAP PAC S series controllers along with other mistic I O units migrated to PAC Project A PC equipped with an Opto 22 PCI AC48 adapter card which provides an RS 485 port NOTE The B3000 B has the same functionality as the B3000 except that it does not support the Optomux protocol For Optomux use an ET
72. is assisted by a backing pump Communication The ProLine uses a cable from the electronics package to the host PC for commu nication The cable is attached to the RS 232 communications port on the elec tronics package and is plugged into the RS 232 port of the host PC Overview 1 11 Options The Proline offers two options to the standard system an auxiliary pump for ex tended pressure range sampling and an I O data system Opto 22 Both of these options are housed in a base enclosure that is located underneath and attached to the base plate of the standard ProLine A Flow Switch can be added as an option to either system Flow Switch Adjust Access Hole Figure 1 6 Extended pressure range option Extended Pressure Range Option This option is used when your application requires an auxiliary pump to draw the sample into the inlet system The pump and associated electronics are easily accessed by sliding the optional extended pressure range unit out from the valve end of the ProLine after removing the inlet tubing and the four panel screws The extended pressure range option consists of the following Figure 1 7 e Auxiliary Pump e Pressure Controller e VSO Valve Flow Switch Optional e Power Supply e PCB Board 1 12 AMETEK ProLine Mass Spectrometer VSO Flow Valve Switch Pressure Controller Power Supply Figure 1 7 Extended pressure anos ii eds e Before operating the ProLin
73. is page intentionally left blank 1 16 AMETEK ProLine Mass Spectrometer ProLine SPECIFICATIONS Sensor Enclosed source Options electron multiplier 100 AMU Performance Mass Position 0 1 AMU Peak Height 2 per 12 hours Sensitivity PPM Specifications are valid after a 60 minute warm up Mass Range 1 100 AMU Resolution Adjustable to constant peak width 0 5 AMU at 10 height Emission Current 0 1 to 10 mA Electron Energy 30 to 150 volts to operate Specifications 2 1 lon Energy 1 10 volts Source Sensitivity Faraday Cup 2 x 10 amps per Torr at detector measured with nitrogen at mass 28 with peak width 0 5 at 10 height and 1 x 10 amps emission cur rent Pumping System Turbomolecular pump Backing pump Multi Stream Variable Pressure Inlet System Inlet with electronically controlled sample and calibration valves Valve position is controlled by the host PC Sample Pressure Range All Ports 0 20 PSIG Fittings 1 8 stainless steel compression fittings Utilities Electrical 100 to 230 VAC 50 60 Hz 500 VA Environment Ambient Temperature 53 F to 104 F 12 C TO 40 C IEC Installation Category II IEC Pollution Degree 2 Max Altitude 2000 meters Relative Humidity 10 to 90 non condensing 2 2 AMETEK ProLine Mass Spectrometer RS 232 Serial Communications Interface Isolated baud rate selection of 1200 to 38400 9 pin female D conn
74. lack 13 4 20 mA Orange 5 24V Red 6 Flow Switch White 14 Ground 6 24V Return Black 2 VSO Valve Signal Brown you f Ground White TB4 3 Inlet Pressure Red 1 24V Red 8 o Ground White 2 Inlet Pressure Orange 3 Chassis Ground Green Yellow SNAP AIV Module Pressure Transducer 4 24V Return Black 1 CHO Red 1 24V Red 2 CHO White 2 Inlet Pressure Orange TB1 3 CHO Brown 3 Chassis Ground Green Yellow 1 24V Red 4 CHO White 4 24V Return Black 2 24V Return Black Power Supply J2 1 0r2 24V Red J2 3or4 24V Return Black Figure A 2 12b Signal wiring diagram extended pressure range option with O data acquisition option Appendix B 16 AMETEK ProLine Mass Spectrometer Extended Pressure Range Option Parts e e 3 HH d EVE ETE A EE E mA a 1 25621JE 2 36083JE 3 38000JE 38002JE 4 25679JE 5 37055JE 6 36073JE Controller Regulating Valve Sample Pump 120V Sample Pump 230V Power Supply Flow Switch Optional Solenoid Valve Extended Pressure Range Option Appendix B 17 Te 25621JE Controller 1 4 Power Supply 25679JE Optional Solenoid Valve Flow Switch 3 055JE 5 6 7 8 36073JE Inlet Pressure Control Bd Pressure Transducer 80553SE 25681JE Appendix B 18 AMETEK ProLine Mass Spectrometer 5 37055JE Flow Switch 8 25681JE Pressure Transducer WHITE NEUTRALS FROM POWER CABLE
75. lange source side Make a paste by mixing aluminum oxide powder Lapmaster 1300 or equiva lent with tap water Using a small nylon bristle brush wet the parts and apply the paste A small round brush is required to clean the interior of the ion volume and the holes in the lenses Scrub only enough to remove any deposits or discolorations Scrubbing too long can damage the finish on the source parts Rinse parts thoroughly in tap water Sonicate the parts in a mixture of de ionized water and cleaner Alconox Powdered Precision Cleaner or equivalent for approximately one hour Re move from the sonicator Rinse the parts thoroughly in de ionized water Replace in the sonicator Sonicate the parts in de ionized water for approximately one hour Remove parts from the water and dry the parts by baking in an oven at 100 C for 30 minutes Alternatively dry the parts with a heat gun until the water has evaporated Reassemble the source Figure 4 7 1 Focus Lens 1 Source ON Multiplier 9 GET 2 Repeller CIS Lens Filament 8 gt O O 3 Filament Dco 7 Exit Lens 6 4 DC 4 5 Spare Maintenance amp Troubleshooting 4 13 Filament Hold Down Screws Filament Plate lon Volume Lock Screw Lens Rod 1 Lens Rod 2 Ceramic Washer Figure 4 7 Breakdown of conductance limited enclosed ion source 4 14 AMETEK ProLine Mass Spectrometer Assembling th
76. leaning the source follow in this chapter However it is often more advantageous to replace the source with a new one Contact AMETEK to order a new source Be prepared to install a new filament if you disassemble the source NOTE for cleaning or any other purpose E The source cannot be disassembled without damaging the filament Mass filter Deposits can form at the entrance to the mass filter rods when they are operated at high pressures or over a long period of time e Deposits can sometimes be seen as discolorations on the metal In some atmospheres the rods might be coated with an invisible layer that will keep the mass filter from operating properly This will result in a loss of sensitiv ity over the full range of the spectrum If the peaks disappear at high scan speeds an insulating layer may have developed on the surface of the rods e Unless the nature of these discolorations can be identified exactly the only sure way of removing them 1s with a fine abrasive e o The entire quadrupole head assembly must be disassembled to clean the rods We recommend that the assembly be returned to the factory where the rods can be cleaned properly NOTE 4 12 AMETEK ProLine Mass Spectrometer Cleaning the Source The ion volume and the source can be cleaned gently using a soft brush such as a toothbrush and a small round brush to access the interior of the ion volume l Figure 4 6 Quadrupole head pinout view of f
77. left blank xii AMETEK ProLine Mass Spectrometer OVERVIEW The AMETEK ProLine is a process quadrupole mass spectrometer that provides continuous multi point monitoring This overview of the ProLine provides information on the following e Theory of Mass Spectrometry e ProLine Subsystems e Technical Support Overview 1 1 Mass Spectrometer Theory The mass spectrometer allows you to identify the masses of individual atoms and molecules that have been converted to ions from a given sample This technique is unique in that it provides a fingerprint identification for the structural and chemical properties of these molecules A mass spectrometer consists of the following components e Sampling System e Mass Spectrometer Hardware e Data System Sampling System The Sampling System serves as a connection between the outside sample envi ronment and the vacuum environment that the mass spectrometer requires The AMETEK ProLine can be equipped with a variety of inlet systems All of these systems are configured to bring the required number of sample streams into the ProLine at the specified pressure while maintaining the high vacuum necessary for proper mass spectrometry operation Mass Spectrometer Hardware Once the sample reaches the mass spectrometer hardware three processes take place e onization e Separation e Detection lonization The AMETEK ProLine incorporates a closed ion source During ionization sam
78. ling from the electronics Replacing the filament 1 Remove the six 6 14 28 bolts that fasten the quadrupole head 10 pin feedthrough to the vacuum system and remove the quadrupole head 2 Remove and discard the copper gasket DO NOT TRY TO REUSE THE GASKET 3 Position the quadrupole head so that it is pointing up and is secure 4 8 AMETEK ProLine Mass Spectrometer Removing the ion volume The ion volume on the enclosed source must be removed to replace the filament Using a hex wrench remove the lock screw holding the ion volume and lock ring to the source Figure 4 3 Carefully remove the screw lock ring and ion volume and set them aside lon Volume lon Volume Lock Screw Filament Hold Down Lock Ring Gergin Filament Hold Down Screw Filament Plate Tab lon Volume Lock Screw Figure 4 3 Ison volume Removing the old filament The filament plate is held in place by two 2 socket head cap screws threaded into a filament base on each side Using the hex wrench provided loosen these two screws enough to rotate the filament plate counterclockwise and remove it by sliding the plate over the screw heads see Figure 4 3 Be sure to remove all residual pieces of the old filament 1 Install the new filament being careful not to bend or break the delicate fila ment wires Handle only the shorting tabs on the filament plate 2 Tighten the set screws that hold the new filament in place 3 Replace the ion v
79. llow the procedure below Turn off the filaments and scanning using the Process 2000 software Turn off the AC power by pressing the ON OFF switch After the power has been removed from the system the electronics A package and the filaments will still be hot CAUTION Installation Operation 3 17 This page intentionally left blank 3 18 AMETEK ProLine Mass Spectrometer MAINTENANCE AND TROUBLESHOOTING ProLine Maintenance Figure 4 1 Inlet Heater controller display Inlet Heater Controller The ProLine uses a Watlow electronic controller to regulate the inlet tempera ture This controller Figure 4 1 is mounted on the front panel The controller is user adjustable from room temperature to 80 C 176 F INLET HEATER RDY ST iS SA Adjusting the inlet heater temperature To adjust the temperature on the inlet heater do the following 1 Hold down the blue Set button The display changes to 0 2 Use the arrow up and arrow down keys to select the temperature you want to maintain 3 Release the Set button once you have reached the desired temperature The factory set parameters for the controller are listed in Figures 4 2a and 4 2b Maintenance amp Troubleshooting 4 1 Inlet Heater SETUP Setpoint SP 0 80 SEn Input Type In H Lin Celsius Fahrenheit CF C C F Range Low rL 0 ae Range High rH 80 A i Output 1 Function Ot1 heat SP hi Output 2 Function Ot2
80. n The backing pump was mounted on the ProLine at the factory There 1s only one connection that must be made to the backing pump Connect the power cable from the backing pump to the outlet labeled Backing Pump in Figure 3 2b There is a switch on the backing pump which is set to ON at the factory Once you apply power to the pumps the switch will turn CAUTION Oo green to indicate that the pump is on Do not turn the switch off Installation Operation 3 5 Electronics Package Installation The electronics package is shipped in a separate package along with the ProLine The electronics will be factory configured with the I O Option card installed and the appropriate cables ready to be installed in the ProLine Before installing the Electronics package on the sensor head do the following e Attach the communications cable to the RS 232 port on the back of the elec tronics package The other end of the cable is plugged into the RS 232 port on the back of the computer e Set the RS 232 RS 485 switch on the back of the electronics to RS 232 Figure 3 6 Connecting the Electronics to Quadrupole Head Power must be off WARNING di Before connecting the 24 VDC power to the electronics ensure that the electronics are connected to the sensor Otherwise damage to the CAUTION electronics is possible 1 Align the key on the electronics unit to the notch on the collar end of the quadrupole head assembly 2 I
81. nsertthe electronics onto the quadrupole head until firmly seated do not twist 3 Lock the electronics unit to the quadrupole head using the tightening knobs Tes HTB Tes HEHH G EPEA Ei EPEA 1 FOCUSILENS fj amp EXITLENS Figure 3 3 2 REPELLER CIS LENS 21 7 DEK 3 FILAMENT 8 FILAMENT Electronics Pinouts 4 Dot ii 5 HEAD ID 10 SOURCE 3 6 AMETEK ProLine Mass Spectrometer Figure 3 3 on the side of the electronics until it is SECURELY hand tightened NEVER TWIST THE ELECTRONICS Always insert it straight in and pull it straight back Connecting Electronics to DC Line Power POWER INPUT l The electronics package requires 24 volts DC 1 volt and 3 3 amps KEY 1 Ifnot already connected connect the DIN connector from E the DC power panel inside the enclosure to the power input R connection on the back of the electronics PIN 1 24VD PIN 2 24VDC 2 Align the key and push in the connector PIN 3 24V RETURN PIN 4 24V RETURN 3 Push the outer ring over the connector and rotate clock wise until the ring locks in place Figure 3 4 Figure 3 4 Power Input Pinouts Electronics Package Connections l Connect the communications cable from the back of the electronics to the RS 232 port on the back of your PC 2 Plug the power cable on the back of the electronics into the outlet labeled Dymax Power in Figure 3 5 3 Make the connection between the I O Option card cable on t
82. nstruments X AMETEK ProLine Mass Spectrometer WARRANTY AND CLAIMS We warrant that any equipment of our own manufacture or manufactured for us pursuant to our specifications which shall not be at the time of shipment thereof by or for us free from defects in material or workmanship under normal use and service will be repaired or replaced at our option by us free of charge provided that written notice of such defect is received by us within twelve 12 months from date of shipment of portable analyzers or within eighteen 18 months from date of shipment or twelve 12 months from date of installation of permanent equipment which ever period is shorter All equipment requiring repair or replacement under the warranty shall be returned to us at our factory or at such other location as we may designate transportation prepaid Such returned equipment shall be ex amined by us and if it is found to be defective as a result of defective materials or workmanship it shall be repaired or replaced as aforesaid Our obligation does not include the cost of furnishing any labor in connection with the installation of such repaired or replaced equipment or parts thereof nor does it include the responsibility or cost of transportation In addition instead of repairing or replacing the equipment returned to us as aforesaid we may at our option take back the defective equipment and refund in full settlement the purchase price thereof paid by Buyer Proc
83. nsure that the mounting clamps on the top side of the base enclosure are fully retracted by turning the clamp screws counterclockwise and pushing the clamps towards the center of the module as far as they will go See Figure A2 3 Attach the ProLine unit to the top of the base enclosure by positioning the rubber feet on the bottom of the ProLine unit over the four holes near the corners on the top of the enclosure Once you have inserted the rubber feet within the holes on the enclosure they fit loosely and are not tightened in any way the clamps will be positioned to grasp the railings on the bottom of the ProLine Fasten the ProLine to the enclosure by tightening the clamps using the clamp screws Do not overtighten clamp screws Appendix B 4 AMETEK ProLine Mass Spectrometer To remove packing materials from the option modules gt 4 gt 6 Figure A 2 4 Extended pressure range option module line voltage and signal connectors on electronics box Js Figure A 2 5 Three voltage outlets on underside of ProLine accessed through base enclosure 8 Loosen the four screws used to attach the option module to the base enclo sure Detach any tubing connected to the exterior of the module Slide the tray out until it is clear of the base enclosure Once the tray is clear of the base enclosure you will see packaging material beneath the sample pump To remove the packing material use a 7 16 nut driver to loosen the
84. nual EC Declaration of Conformity Manufacturer s Name AMETEK Inc Process Instruments ISO 9001 Registered 1995 Manufacturer s Address Process amp Analytical Instruments Division 150 Freeport Road Pittsburgh PA 15238 USA Phone 412 828 9040 Fax 412 826 0686 declares that the product Product Name AMETEK ProLine Mass Spectrometer Model Number s Faraday Cup Faraday Cup Electron Multiplier DP100 DPI00M DP200 DP200M DP300 DP300M complies with the requirements of EMC Directive 2004 108 EC EN 61326 1 Radio Frequency Emissions EN50011 CISPR 11 Radiated and Conducted Class A Group 2 ISM Device EN61000 3 2 Harmonic Current EN61000 3 3 Voltage Fluctuation Flicker EN61326 1 EN50082 1 Immunity EN61000 4 2 Electrostatic Discharge 4k V 8kV contact air EN61000 4 3 ENV50204 Radiated Radio Frequencies 3V m EN61000 4 4 Electrical Fast Transient Burst 5kV 1kV EN61000 4 5 Surge 1kV to Shields 1kV 2kV AC Differential Common EN61000 4 6 Conducted Radio Frequencies 3 V m EN61000 4 11 Voltage Dips and Variations 100 95 60 and 30 EN61000 4 8 Magnetic Immunity and with the low voltage directive 2006 95 EC EN 61010 1 Safety Requirement for Electrical Equipment Manufacturer s Address in Europe AMETEK Precision Instruments Europe GmbH Rudolf Diesel Strasse 16 7 D 40670 Meerbusch Germany Aa f Gop es Contact Dr Jurgen Gassen Mark Coppler Sr Compliance Engineer AMETEK Process I
85. ogIN Z Analog IN 5 Modde AnalogIN analog IN 6 Add Display for Analog Module e To create displays so that you can view the data being monitored go to the mode display where you want your information viewed Right click on one of the screens e Click Scan e Click Device and select your analog input device e Click on the Display tab to configure the parameters for the display Mass 28 Properties Mass 28 Properties X Main Box Temperature z Ex Iv oed 7 gl passe f a Appendix A 16 AMETEK ProLine Mass Spectrometer Digital and Analog Outputs 1 Refer to Chapter 8 in the 2000 software manual for setting up the Digital Outputs 2 Refer to Chapter 9 in the 2000 software manual for setting up the Analog Outputs Opto 22 Option Appendix A 17 This page intentionally left blank Appendix A 18 AMETEK ProLine Mass Spectrometer OPTO 22 USER SETUP The following OPTO 22 I O user modules are available with your ProLine mass spectrometer system Specifications for the modules are included in this chapter Analog Ouid ADAZI SNAP AOA 23 9 Pin Male D Sub O S WEJ GI BEN gt O COND GCI BEN SNAP AOA 23 NC NC NC Yellow NC NC Blue coo Ojo NN gt Figure A2 1 Pin out for AOA 23 modules Opto 22 User Setup A2 1 10O MODULES SNAP ay D P T P gt ANALOG OUTPUT MODULES DATA SHEET page 5 12 Form 1066 011022 Dual Ghannel Gurrent SNA
86. olume by setting it back on the head and secure it with the set screw 4 Remove the shorting tabs on the filament by gently bending them back and forth with needle nose pliers until the tabs break at the notches at their bases Maintenance amp Troubleshooting 4 9 A Be sure the filament coils are aligned with the slots in the ion volume CMT andionizer Make sure the filament coils do not touch the base plate ionizer or ion volume in any manner other than at welds 5 Install a new copper gasket on the quadrupole feedthrough flange Be sure it remains centered on the flange as the head assembly is installed into the vacuum system using the six bolts 6 Tighten the bolts using a cross pattern to ensure proper tightening and a leak tight connection The maximum torque required is 110 in lb 9 ft Ib 7 Check for electrical isolation between the feedthrough pins e The check should be performed on the pins on the atmosphere side of the unit Figure 4 4 e The pins should be electrically isolated from each other and from ground e There should be approximately one ohm continuous circuit between the filament Pins 3 and 8 They should be isolated from ground HTCH E S E Y 7 L L _TIPI a A AMENT 5 AMENI DETECT d x px Figure 4 4 4 V Quadrupole head pinout
87. ontrol board Electrical and Controls Electrical power is delivered to the unit through an AC power line All power and electrical signals must be delivered to the unit per the National Electric Code and local requirements Temperature Control for Heater The ProLine unit uses an electronic controller to regulate the sample inlet heater This controller is user adjustable for optimum performance and should require no subsequent maintenance See Chapter 6 for more information on factory set parameters and adjusting the temperature 1 10 AMETEK ProLine Mass Spectrometer O Option Board The I O Option board monitors the following parameters e Heater inlet temperature e Turbo pump status Power Supplies There are two power supplies located in the U shaped bracket in the electroncs box When viewed from the back of the analyzer the left hand power supply is used to power the turbo pump electronics package and the fan The right hand power supply is used to power the heaters Figure 1 5 Pumps The turbopump and backing pump start automatically upon application of power using the power button Both pumps will turn off if they are overheated because of leaks system failure or mechanical failure With the capillary inlet arrangement pressure inside the chamber is approximate ly 5 x 10 Torr The ProLine uses a turbomolecular pump with drag stages that 1s connected directly to the inlet manifold The turbomolecular pump
88. op and bottom of the unit and the 4 3 16 screws for the sides Electronics Boards Parts 5 13 This page intentionally left blank 5 14 AMETEK ProLine Mass Spectrometer SERVICE AND PARTS REPLACEMENT Components in the Electronics Box The electronics box houses the following components that can be replaced by the user e Power supplies e Valve control board e Power switch fuses e Heater inlet controller e Pump controller interface e Quadrupole head maintenance filament replacement Use caution when accessing any of the components in the electronics CAUTION box Service and Parts Replacement 6 1 Accessing the Electronics Box Contents Follow the instructions below to access components in the electronics box for service or replacement 1 After powering down the electronics carefully use the tightening knobs on the sides of the Dymaxion to unlock the electronics from the quadrupole head 2 Once loosened gently pull straight back on the Dymaxion without twisting until it is free of the head Do not remove the cabling from the electronics 3 Detach the tubing from the backing pump that is connected to the turbo pump You will not detach the backing pump from the top of the electronics box 4 Remove the six screws that hold the top cover on the electronics box you will view is the computer board It will have a plug in flash card OS and four connectors a power connection communication connec
89. or when reassembling the unit after replacing the board The insula tor is coated with thermally conductive joint compound If it is not replaced the unit will not work ION 10 Separate the RF card from the conductor guide It is very important to remember to retain the conductor guide as it is not part of the replacement board NOTE Replacing the RF Card 1 Using the 1 4 nut driver loosely attach the conductor guide to the RF card using the 5 8 standoffs 2 Plug the analyzer head onto the loosely assembled guide conductor and RF card Tighten the standoffs using the 1 4 nut driver Failure to secure the assembly to the analyzer head at this point can result in failure of the unit through cracking of the feedthrough If the CAUTION feedthrough is cracked a leak will develop 3 Screw in the 1 2 screw in the upper right corner of the RF card to connect to the aluminum oxide insulator Failure to install this screw and aluminum oxide insulator will cause the unit not to operate ION 4 Using the 1 4 nut driver attach the Amp card shield to the RF card using the 3 8 standoffs 5 Attach the Amp Card to the amp card shield using the 4 1 4 screws 6 Attach the amp card cover to the Amp card using the 2 1 4 self tapping sheet metal screws 5 12 AMETEK ProLine Mass Spectrometer 7 Insert the RF assembly into the unit casing and secure using the 4 1 4 screws for the t
90. or E2 brain Ifyou are not migrating to the SNAP PAC System but building a new system use SNAP PAC SB serial brains instead For Help This technical note covers basic configuration only See form 1781 the B3000 B User Guide for complete details If you cannot find the answer you need in the user s guide please contact Product Support Phone 800 TEK OPTO 835 6786 951 695 3080 Monday through Friday 7 a m to 5 p m Pacific Time Fax 951 695 3017 E mail support opto22 com Website www opto22 com B3000 B Top View Baud rate switch Pin 1 TX RX LED Serial connector Reset switch Termination Switches Address upper Address lower pu e o n eo N e ja e IRQ LED STAT LED 2 Rotate the baud rate switch to set the 4 Use the two rotary address switches to Setting Up Serial Networking 1 Attach an RS 485 serial cable to the serial port If you are using mistic interrupts wire IRQ and IRQ pins 6 and 7 See the B3000 8 User Guide for details on network wiring desired baud rate as shown in the table below NOTE Due to timing tolerances some baud rates may not work with some compatible devices Baud Rate Switch Reserved 3 Use the three termination switches to O End of cable set termination as follows A For the B3000 B at the physical end of the cable set all three of the termina tion switches to the ON position e For all B3000 B units
91. ple inlet wall Once it is in the correct position slide the clip onto the pump to lock it into position C 4 Slide the U shaped piece of metal over the top of the sensor manifold on the inside of the sample box wall Use the screws provided to attach it to Position Sensor Manifold the wall from the outside of the box The sensor in U Shape manifold should now be secure locking the head sensor in position Sample Inlet Box Back Wall 5 Attach the flexible roughing hose from the turbo pump to the backing pump by connecting each end of the hose Installation Operation 3 3 El E m d dp i runi vhi EATER DYSIGNALIO TummBO TURBO PELi POWER JACKET REMOTE Agii Lr P siri di BCKIN 1 ui i ii Lt n m B ME M nt DE TI Figure 3 2a Electronics box connections Remote E Heat TMS gt Turbo Pump Power Connector b Vent FV Pump E Figure 3 2b ran gt ProLine connections and turbo pump controller box 3 4 AMETEK ProLine Mass Spectrometer Turbo Pump Cable Connections 1 Attach one end of the turbo pump power cable to the connector labeled Turbo Power in Figure 3 2b Attach the other end to the power connector on the side of the pump controller This supplies power to the turbo pump 2 Attach the RS 485 turbo cable from the connector labeled Turbo RS485 in Figure 3 2b to the connector labeled RS 485 on the turbo pump controller Backing Pump Connectio
92. pply cable between the electronics and the power supply is plugged in at both ends 2 Make sure the electronics RS 232 RS 485 switch 1s in the correct position for the communications port that you are using 3 Check the LEDs on the back of the electronics to make sure that all lights are green The second light should be blinking green Refer to LED section below for LED details 4 Inthe software make sure that Device Enabled and Live Data boxes are both checked on the General tab The LEDs are listed below in the order in which they appear top to bottom on the back of the electronics unit CPU Indicates CPU and system status e OFF Electronics power 1s off e RED CPU has stopped e FLASHING RED Battery backed RAM has been cleared Check battery GREEN Normal operation Comm Shows the status of communications between the electronics and the PC It flashes green when receiving data from the PC It remains off when the elec tronics package is inactive A red light indicates a communications error RF Shows the status of the RF circuit The LED is green if the RF amplifier is operating properly and turns red if you have an RF failure The LED is yel low during automatic RF tune If you are having a problem in this area please contact your service engineer NOTE Filament This LED indicates the status of the filament The LED is green if the fila ment is on and is working properly The LED appears red if the
93. ront heat sink It is the longer of the two boards attached to the LED panel See Figure 5 1 Follow these steps to remove the Scan board 1 Remove the I O Option board 2 Remove the 1 4 screws from the front top and bottom casing of the unit and the 3 16 screw from the right side See Figure 5 1 3 Loosen or remove the screws at the top and bottom of the option plate to al low easier access to the removal of the Control board 4 Grab the heat sink and pull on it to remove the assembly with the Control and Scan boards It is connected to the unit by four connectors 5 Once the assembly has been removed from the unit casing remove the upper left and bottom right 3 8 screws with internal tooth lock washer from the front heat sink 6 Gently pull on the heat sink to remove it The LED panel is now visible 7 Remove the 1 4 screw from the top right of the LED panel 8 Gently pull the Scan board away from the adhesive gap pad on the back of the LED panel Replacing the Scan Board 1 Attach the LED panel at the upper right using the 1 4 screw 2 Replace the front heat sink using the 3 8 screws and lock washers on upper left and bottom right 2 Insert the board into the unit making sure the four connectors 2 on each board are engaged 4 Replace or retighten the screws for the option plate to put it back in place 5 Replace the 1 4 screws on the top and bottom and the 3 16 screw on the right side o
94. ror Status 8 Green Diode for Operating Status Installation Operation 3 15 Figure 3 11a Click filament on Figure 3 11b Use Control menu to turn filament on Electronics Package Warm Up Time As with all complex electronic systems the electronics package reaches thermal equilibrium only after a certain amount of time has passed once power has been applied and the unit is running We recommend that the electronics run for a minimum of one hour prior to its use in situations where the most stable readings are required Turning on the filament On the Process 2000 software desktop click the yellow light bulb icon on the toolbar Figure 3 1 1a Or on the Control menu click Filament The yellow light bulb icon on the toolbar will become indented Figure 3 11b Once the filament has been on for an hour you can begin to set parameters for your application NOTE Refer to the AMETEK Process 2000 Software manual for information on how to add a device set device settings and select display modes and preferences Dycor Process 2000 Dycorl File Edt View Control Mode Script Window Help Difco lta ej s rs ae alo e mesi o sole o s Ei a ilanla a sea v A slels 2 7l Click Here Tie Eat Ve Coma bonos lv NOE EEE Mens 4 E 2M IES 3 16 AMETEK ProLine Mass Spectrometer Shutting Down the ProLine To perform an orderly shutdown of the ProLine fo
95. s Spectrometer PROLINE ON BOARD COMPUTER c p du Oo gt Qv 2 U oL CN a w E e UE mm an YN ea c Ul gt t gt O Q uo O oc WU o U gt O O La U O e 99 lt Q LL oo oo nDoogaooaooo o R n n n ZAABdccoa A S j r jejej E 8888888888 Baa e uu D LLI i 3 T Z L YO 8B O gt cea acc Wa 2 O H Q O e Ig ZA Ce o On Lp LIEEXJEJEJETEJEITCETE Y foe oe fo fe oe 5 noooooooog S L JEXETEIJEJEIEJYEXSEJES Ez Er fa cf a g E Y a Ym a a U Cc EXISHETICHESESJESETETES lt a Pat gt C Lu e Figure 7 7 On board PC connections Wiring Diagrams 7 7 This page intentionally left blank 7 8 AMETEK ProLine Mass Spectrometer OPTO 22 SNAP DATA ACQUISITION SYSTEM These instructions describe the steps necessary to set up the SNAP I O Data Acquisition System to work with your analyzer Complete information on how to use the modules is provided in the Opto 22 SNAP user manual that you received with the product These instructions are divided into the following sections e Analyzer and SNAP I O System connections Required settings for SNAP modules e Setting module parameters using System 2000 software Opto 22 Option Appendix A 1 Opto I O Rack 8 Position Module Configuration Device Address 128 Position 0 Alarm DOO Alarm 2 DOT Alarm 3 DO2 Alarm 4 DO3 Device Address 128 Position Flow Switch Optional DIO SPARE DII SPARE D
96. sample line will vary with sample pressure tube diameter and line length Consult the factory if you have specific flow requirements NOTE 1 Open the Process 2000 software The Process Status screen Figure A2 7 will open Click on Status Inputs Find the Inlet Pressure and Inlet Prop Valve locations in the left hand column Figure A 2 7 Process Status screen with Status Inputs displayed The Inlet Pressure value should be between 400 and 760 initially The Inlet Prop Valve percentage reading should be in the range of 20 to 50 Extended Pressure Range Option Appendix B 7 Ifthe Inlet Prop Valve percentage reading is not between 20 and 50 change the setpoint on the pump controller to a number several digits lower or higher The controller is located on the extended pressure range module front panel near the lower right hand corner Figure A2 8 Figure A 2 8 Flow Switch Location of valve Adjust Access Hole manifold and exhaust tubing and exhaust port Exhaust _7 Inlet 7 te e ontroller The setpoint is shown at the bottom of the display It is changed using the up and down arrow keys on the right side of the face panel Pressure reading 1s shown at the top of the display Allow 10 to 15 seconds for stabilization after changing the setpoint and then read the Inlet Prop Valve percentage again Ifthe percentage reading is above 50 raise the controller setting If the
97. tended Pressure Range Option Parts 14 2 e eerte Ep pna HRR FUHR CIERRE SUE B 17 APPENDIX C HIPACE 80 with TC110 APPENDIX D TC110 APPENDIX E DCUOO02 vi AMETEK ProLine Mass Spectrometer Safety Notes wARnings c AuTions andno TEs contained in this manual emphasize critical instructions as fol lows ronmental contamination WARNING An operating procedure which if not strictly observed may result in damage to the equip ment Important information that should not be overlooked NOTE CAUTION Dymaxion Electronics and Sensor Before connecting the 24 VDC power to the electronics ensure that the electronics are con C nected to the sensor Otherwise damage to the electronics is possible Always remove 24 VDC power from the Dymaxion electronics before removing the electron EXUTIOM ics from the sensor An operating procedure which if not strictly observed may result in personal injury or envi Vii Electrical Safety Up to 2 kV may be present in the analyzer housings Always shut down power source s before perform ing maintenance or troubleshooting Only a qualified electrician should make electrical connections and ground checks Any use of the equipment in a manner not specified by the manufacturer may impair the safety protection originally provided by the equipment Do not operate this instrument outside of the temperature and humidity specifications stated in Chapter 2 Fuse must be replace
98. that are not at the physical end of the cable set all three of the termination switches to the OFF position M nj a RO gt I RX on ie X RX All other positions A Yd T Gal RO mc qp eu imd X RX NOTE Since biasing is normally done at the controller or computer the B3000 B does not include biasing switches set the unit s address as shown on the following page Baud rate switch set to A for 38400 bps baud rate Termination switches set to ON position for 4 wire end of link termination NOTE Upper address set to 8 and lower address set to 3 for a base address of 128 Opto 22 Option Appendix A 7 Each B3000 B contains four addresses the base address base 1 Upper base 2 and base 3 The base address is an even multiple of 4 address Normal communications are Binary with CRC16 Both Binary and ASCII with CRC16 are supported by OptoControl and PAC Control Switch settings for each address are shown in the tables below Lower address For Binary or ASCII with Checksum see tables on the following page Binary Mode with CRC16 supported by Opto Control and PAC Control Upper address KENERESEXEGENEJETEIEJEGEXESE3EJXEN switch KEKWEIELSESEWRETETSIRIEXEJEIEUIMTES Lower address ej4 sjcj oj4 8jc oj 4 8 C 0 4 8 C switch e 8 72 76 so s ee 92 96 100 104 1 12 116 20 124 4 4 4 4 5 5 5 5 6 6 6 6 7 7 7 7 oj4j 8 cjoj4 8 c jojJ4 8 c 0oj4 8 C 12
99. tion of the gases being pumped Diaphragm identification and replacement instructions can be found in the pump manufacturer s documentation supplied with your analyzer Rotary vane roughing backing pump When the ProLine is in continuous use the oil in the rotary vane pump should be changed at least once a year In some cases depending on the compounds being pumped oil must be changed more frequently If when viewing the oil through the sight glass it looks dark or discolored it needs to be changed Oil change instructions can be found in the pump manufacturer s documentation supplied with your analyzer Extended Range Pumping Option Maintanance The extended range pumpin option requires no regular maintenance Maintenance amp Troubleshooting 4 5 Electronics Package Maintenance and Troubleshooting This section includes information on e maintaining the quadrupole head changing the filament e disassembling the source e cleaning the source e reassembling the source e replacing the electron detector troubleshooting the electronics The rest of the electronics system should require no routine maintenance during normal use Disconnect all power from the analyzer before starting these proce dures Touching any part of the quadrupole head source or mass filter with your fingers will leave dirt and oil on the parts resulting in contami nation of the quadrupole head Use clean plastic latex gloves when handling compon
100. top side of the controller to release their grip on the controller Gently pull the controller out through the front of the electronics box Replacing the inlet heater controller l Slide the new controller through the front of the electronics box to the rear It will pass through the grip fingers to hold it in place on the top and bottom Replace the terminal block on the end of the controller by snapping it into place Replace the covers of the electronic box Service and Parts Replacement 6 7 Turbo Pump Controller Interface If the turbo pump controller interface needs to be replaced follow these instruc tions Removing the pump controller interface 1 Remove the top cover of the electronics box 2 Remove the four black screws holding the pump controller interface on the front of the electronics box 3 Gently push the controller interface from the rear through the front of the box to remove it 4 Remove the flat wire phone like connector from the controller interface Replacing the pump controller interface l Attach the flat wire connector to the controller interface 2 Position the new controller interface 1n the slot and secure to the front of the electronics box using the four black screws 3 Replace the top cover of the electronics box 6 8 AMETEK ProLine Mass Spectrometer Spare Parts Board valve control Capillary 30u ID 360u OD Controller temperature inlet heater Display unit
101. ts remove any temporary markers or tape Maintenance amp Troubleshooting 4 17 Electron Multiplier The multiplier is immune to up to air cycling and routine low level ion bombard ment However over time the system will begin to lose gain When this becomes unacceptable a new multiplier will restore the original gain of the system Call AMETEK Process Instruments or your local representative to fy arrange for factory service to replace the multiplier Because of the NOTE complexity of the detector flange assembly we recommend that the multiplier be replaced at the factory 4 18 AMETEK ProLine Mass Spectrometer Troubleshooting the Electronics Things to Check First In many cases a system failure is not due to a problem with an electronic compo nent but rather to one of the following Operation at too high pressure greater than 1 x 10 Torr Improper setting of parameters on a source or calibrate button Incorrect or improper cable connection Burned out filament Shorted out ion source parts usually resulting from an incorrect filament or source replacement Failure to establish proper communications Quick and Easy Solutions The first step in providing a solution to the problem is performing the following checks l Make sure the quadrupole rod assembly is properly supported within the vacuum housing Make sure all cables are connected properly to the electronics unit Make sure that the electronics
102. ture must not exceed 80 C WARNING Heating jacket operation produces high temperatures Avoid touch ing the jacket surfaces or equipment that is being heated CAUTION Heating Jacket Maintenance Analyzer J e 0 o 0 Connect to Grounding Strip Grounding Strip Figure 3 7 E Heating jacket ground strip locations PN The heating jacket doesn t require regularly scheduled maintenance However regular inspection is recommended and damaged units should be removed from service immediately Jackets should be protected from chemical spillage me chanical damage and corrosive atmospheres 3 10 AMETEK ProLine Mass Spectrometer Sample Gas Flow Figure 3 8 Sample gas flows from the inlet ports Figure 3 8 through the three way electric solenoid valves and manifold The selected sample gas then flows to the analyzer The vacuum pumps work together to maintain a constant pressure in the ionizer The vacuum system consists of a turbo drag pump a backing pump and associated plumbing The inlet system is configured so that all ports operate at a sample pressure of between 0 to 20 PSIG Dycor Head inside vacuum chamber Backing Pump Dymaxion Electronics Vacuum Chamber molecular Pump Sample Box DA l ProLine sample flow Installation Operation 3 11 Attaching the Sample Calibration Lines 1 Attach the s
103. used when the application requires sam pling of gases with pressures below atmospheric pressure down to approximately 650 Torr absolute This optional module draws sample into the inlet system while actively controlling the sample gas pressure at the entrance of the mass spectrom eter The pump associated hardware and electronics are mounted in an enclo sure beneath the inlet valve end of the ProLine Figure A2 1 The extended pressure range option consists of the following e Auxiliary dry rotary vane sample pump e Pressure controller e VSO valve e Flow switch Optional e Pressure control circuit board e Pressure transducer e Manual regulating valve e Power supply Figure A 2 1 ProLine with extended pressure range option ProLine Unit Valve 5 Manifold ai 8 A mar mm DE Tube z Line base outlets U Common Exhaust Tube Exhaust Port Extended Pressure Range Option Extended Pressure Range Option Appendix B 1 Sample Flow Sample Selection Valves 16 shown Heated Inlet Enclosure gt a Capillary Restrictor ER Exhaust DX 1 Mass Toon Back x aus R o Spectrometer 7 Pumpf Pumpf 1 4 compression fitting Q 0 0002 atm cc s From Sample Point 1 From Sample Point 2 From Sample Point 3 From Sample Point 4 From Sample Point 5 From Sample Point 6 From Sample Point 7 From Sample Point 8 Flow Switch Optional LT Pressure Transducer m
104. ust be plumbed to a safe area and exhausted at atmo spheric pressure I PSIA This 1 4 O D tube exhausts all of the gas that enters the inlet CAUTION 11 Attach the sample and calibration tubing to the ProLine Sample tubes can connect to any port that is connected to the exhaust manifolds On a 16 valve ProLine the sample gas tubes can connect to ports 1 through 4 and ports 9 through 16 On an 8 valve ProLine the sample gas tubes can connect to ports I through 4 Calibration gas tubes connect to the in port numbers 5 through 8 on both the 16 valve and 8 valve ProLine The out ports that correspond to the in ports chosen for calibration gas must be plugged with a 1 8 cap to prevent the continuous flow of gas Once you have completed the plumbing you can turn on the power Appendix B 6 AMETEK ProLine Mass Spectrometer Operation Turning On the Extended Pressure Range Module The extended pressure range module receives power as soon as the main power switch on the ProLine is turned on Allow the vacuum pumps time to reach oper ating pressure and then start the Process 2000 software and turn on the filaments as described in the Installation section of Chapter 3 in this manual Allow the unit to warm up Initial Adjustments Make sure that all sample and calibration tubes are connected and A operating at normal pressure and temperature before performing e these adjustments Flow and transit times from each
105. view of flange atmosphere side 4 10 AMETEK ProLine Mass Spectrometer Disassembling the Source Closed Source Disassembly of conductance limited enclosed source e Remove the filament see instructions in this chapter e Loosen the set screws on the barrel connectors that hold the three leads com ing down from the source elements The filament bases can be left intact Remove the source assembly from the mass filter 1 Loosen and remove the three 3 locknuts that hold the source connection rods in place on the lenses Refer to Figure 4 5 and Figure 4 7 2 Loosen and remove the three 3 screws that hold the lens together in sand wich form Be careful not to lose the small ceramic or metal washers from the source each serves to hold the source in precise alignment See Figure 4 7 Filament Base lon Volume Lock Screw lon Volume lon Volume lon Volume Lock Screw Lock Ring Source Lens 1 Lock Ring Detector Flange Assembly Figure 4 5 Closed enclosed quadrupole head Maintenance amp Troubleshooting 4 11 Cleaning the conductance limited enclosed source The conductance limited enclosed source can be fully disassembled and cleansed of deposits However only the removable ion volume will usually need cleaning since this is where most sample ionization occurs If the entire source assembly is covered with deposits it must be disassembled and thoroughly cleaned Instruc tions for c
106. w fuse for 120V system NOTE AMETEK 25779JE or a 5 Amp slow blow fuse for 230V system AMETEK 25702JE E If your system includes the Extended Pressure Range option replace 4 Replace the fuse holders in the switch box making sure to align them in the correct orientation as described by the arrows on the sliders and on the bot tom of the switch box door Close the switch box door and make sure it snaps shut 6 6 AMETEK ProLine Mass Spectrometer Inlet Heater Controller The heater inlet controller is located on the front of the electronics box Removing the inlet heater controller l 2 Remove the top and the back covers of the electronics box Remove the back terminal block from the inlet heater controller by hold ing the terminal block on either side placing your fingers on the ridges and squeezing the sides of the terminal block to release it from the controller The controller has hard plastic fingers both above and below where it en ters the electronics box that hold the controller in place It is easier to remove the controller if you release the plastic fingers on the underside of the con troller first Using a stiff piece of card stock or some other thin firm material slide it between the fingers of the holder and the controller on the underside of the controller This releases the grip of the fingers on the underside Using your fingers or another piece of card stock lift up the fingers on the
107. wed by a colon and a backslash and the word setup exe d setup exe and click OK to start the installation program 3 The Dycor Process 2000 setup begins and the Welcome screen opens Click Next to continue the installation or Cancel to abort the installation 4 Follow the instructions on the subsequent screens to complete the installa tion When you get to the Setup Complete screen click Finish to complete the installation The default location for the System 2000 software is in the Dycor System 2000 folder 3 14 AMETEK ProLine Mass Spectrometer ProLine Operation Figure 3 10 Pump controller display Powering Up the ProLine When you are ready to power up the ProLine plug the AC power cord into the connector labeled Power Figure 3 2 on the side of the electronics box Next press the switch above the cord to the on position to apply power to the unit The backing pump and turbo pump will be powered up upon application of power to the unit Pump Controller Interface After switching on the pump control unit performs a self test and also a test on the connected turbo electronics which can be seen on the pump controller inter face Figure 3 10 Providing there are no errors the control unit is now ready to operate DCU ee PFEIFFER VACUUM 4 LCD Display s 9 2 Status Display C 3 Error Acknowledgment Key 4 Key Left 5 Key Right 6 Pumping Station ON OFF Key 7 Red Diode for Er

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