User Manual - BioChromato
Contents
1. See P 8 for the reference of the part number in the description above 73 BioChromato Chapter 4 Before use P 9 10 4 1 To confirm accessories Confirm all accessories below Don t lose any accessories Aluminum beads Spiral Plug units Instruction Manual Qty 1 Qty 4 e Hose splices 1 Qty 2 E L 1 Please select a moderate a hose splice with outer diameter of 9mm or 12mm for the vacuum pump 2 On the shipment the port A D and the orifice inside are connected 4 2 To prepare items Please notice that these items below are not included in the product Tools e Vacuum hose Vacuum pump Container for concentration e Cold trap Refrigerant 73 BioChromato 4 3 Preparing before use 1 Prepare aluminum beads 3 Connect the hose splice Please put aluminum beads in temperature Please choose a hose splice with the outer control block diameter of 9mm or 12mm Then connect the hose splice and the port C Aluminum beads Temperature control block Don t use other aluminum beads to avoid troubles 2 Connect the Spiral Plug unit and the joint Port C Please connect the Spiral Plug unit and the joint until it clicks Joint Spiral Plug unit Outer diameters 9mm or 12mm Please connect them firmly In case of taking out the Spiral Plug unit push the If you need to choose other size please ask your metal point local distributor 4 Remove the plug Pl2. 17 5 2 4 Replacing gas 1 To open a valve of a gas supply 2 To flow the gas Please open a valve of a gas supply Please start flowing gas about 2 min Ex Gas line at 10 L min 1 Must have gas overflow 1 Gas replacement with the system is not 100 When replacing gas only use the containers that fit Spiral Plug P1 or P2 some work with P3 5 2 5 Start concentration 1 To turn on the vacuum pump 2 To adjust gas influx Please turn on the vacuum pump Please adjust gas influx with the vacuum Close the valve tightly before you begin control valve OD concentration If you use your pump please confirm a manual provided by a manufacturer Vacuum control valve ID To avoid sample loss and damages to machine and pump due to sudden suction adjust gas influx with the valve gradually 5 2 6 After finishing concentration 1 Close the vacuum control valve 41 tightly Then turn off the machine and vacuum pump 2 Then close the valve ofthe gas supply 3 Take out the container after cooling down the heated container 73 BioChromato 18 5 3 C Type Closed circulation system P 19 23 The Smart Evaporator can be used for the concentration within the closed circulation system Ex Included items Not included items Machine Circulation system Power cord Refrigerant Container 5 3 1 To confirm accessories To confirm all accessories below Don t lose any accessories Vacuum pump Ho
3. accumulation Don t place objects on the Smart Evaporator Power source You can use the machine in countries regions where the power supply is on 120V AC 2 3 Before use Must confirm a normal running for electric switch and temperature control before use Must connect with the power cord to the outlet properly If you find out any trouble or damage don t use the Smart Evaporator Example The power cord and outlet have damages The Smart Evaporator has damages The temperature control panel has damages Avoid tilt vibration and shock during running Avoid sucking solvents and trashes directly Don t put solvents trash water etc into ports of the Smart Evaporator 4 BioChromato 2 5 Storage Keep temperature from 10 to 40 C Avoid direct sunlight Keep humidity from 20 to 70 Not condensation Avoid conditions below Explosive gas flammable gas and Corrosive gas Chemical and Water Tilt Vibration and Shock Dust Iron powder and Oily smoke Environment may cause adverse effect for the electric circuit Severe temperature changes 2 6 Maintenance Don t expose the unit to avoid shock hazard Don t do anything to the unit for the maintenance except the description in this manual If the Smart Evaporator need repair please ask your distributor immediately In case of spilling water or solvents please clean it off after turning off the power im
4. cold trap gt Connect the exhaust port of vacuum pump and cold trap Under with vacuum hose lt Step3 Connect the machine and cold trap gt Connect the port B and the cold trap upper with vacuum hose lt Step4 Connect the power connection gt Connect the outlet with the power cord 5 4 2 5 Connection the gas tank 1 To take out plugs 2 To connect the gas tube Please take out plugs by pushing the root of Connect the port A D and the gas tank with the plug from the port A and Orifice the gas tube Gas tube Orifice 73 BioChromato 8 26 5 4 3 Set target temperature Keep the max temperature below 100 C to avoid damages to the machine Set the target temperature above room temperature 1 Turn on the Power for temperature control Current temperature Target temperature GA Wkey for setting temperature Select temperature from room temperature to 100 C 1 2 1 Please use this device after reaching target temperature 2 Please do not touch the key except for A Wkey It may cause a malfunction 5 4 4 Starting concentration i Preparing refrigerant 1 Put the refrigerant in the cold trap Don t use cold trap with liquid nitrogen because it could cause an explosion due to the liquefaction of oxygen in air ii To place the container 1 To open the cover 2 To place the container Please open the cover with snap locks Please set up the container on a
5. the valve tightly before you begin concentration To avoid sample loss and damages to machine and pump due to sudden suction adjust gas influx with the valve gradually If the machine sucks up samples directly please close the valve immediately Don t suck up dusts and foreign matters 1 To turn on the vacuum pump Please turn on the vacuum pump Close the valve tightly before you begin concentration If you use your pump please confirm a manual provided by thw manufacturer 2 To adjust gas influx Please adjust gas influx with the vacuum control valve AD Vacuum control valve MW To avoid sample loss and damages to machine and pump due to sudden suction adjust gas influx with the valve gradually 73 BioChromato 14 5 1 5 After finishing concentration 1 Close the vacuum control valve OD tightly Then turn off the machine and vacuum pump 2 Take out the container after cooling down the heated container 73 BioChromato 15 5 2 B Type Simple system connection Replacing gas P 16 18 The Smart Evaporator can replace the air inside with gas such as Nitrogen or Argon Included items Not included items Machine Vacuum pump Power cord Vacuum hose Container e Gas tank Gas line and etc Gas tube pressure tightness 5 2 1 Connecting method Please connect the vacuum tube completely Please take out plugs before replacing gas In case of replacin
6. Smart Evaporator Cl Instruction Manual Please read this instruction Manual before use Follow the basic procedure as shown Xd BioChromato lt 151014 US gt Chapter 1 Introduction P 2 Smart Evaporator has two features below Can be used for evaporating volatile solvents Can be used for keeping a temperature This instruction manual explains product summary operation trouble processing maintenance and storage below Must read this instruction manual before use Must understand the Warning and the Caution in this manual before use Adhere to the instruction manual Keep the machine out of the reach of children All rights are reserved If the instruction manual has mistakes or anything unpleasant please ask local distributors Please note that the product specification is subjected to the alternation without any notice The instruction manual has some pictures which are pumps containers and traps However please notice that these systems are not included in the product Don t use cold trap with liquid nitrogen because it could cause explosion due to the liquefaction of oxygen in air Please notice that a vacuum pump is not included in the product 4 BioChromato Chapters Chapter 1 Introduction P 2 Chapter 2 To use safely P 4 6 Chapter 3 Part names P 7 8 3 1 Front side P 7 3 2 Back side P 8 Chapter 4 Before use P 9 10 Chapter 5 How to use P 11 29 5 1 Simp
7. ce to organic solvents Q 3 Which containers are recommended Answer The Smart Evaporator can be used with various types of containers We recommend using flat bottom containers for efficient concentration Q 4 Do you have a recommended pump Answer Yes we have a recommended pump Please ask our local distributor Q 5 How do wash the plug unit Answer Please wash with moderate solvent or pure water according to your sample Please use it after the complete In addition it can be put in autoclaves or ultrasonic washing machines 4 BioChromato 31 Chapter 8 Limited Warranty P 32 We are willing to repair the machine in the case of troubles caused by normal use abided by quality assurance provisions below Please contact the local distributor from which you purchased it then provide it with product code and details such as the date of purchase and troubles 8 1 Parts for Quality Assurance Machine 8 2 Term of Guarantee 1 year after the purchase Please notice that the fees for repairing are charged after the period which includes costs for parts transportation and repairing work 8 3 Exception for Quality Assurance Please note that you are liable for the cost of repairs in the case below Troubles and damages caused by careless use Troubles and damages caused by accidents such as falling and shock during transportation after the purchase Troubles and damages because of using non desig
8. ease remove the plug from inside Port A and Orifice Then please put on plugs outside them 73 BioChromato 10 8 Chapter 5 How to use P 11 30 Selecting concentration method 1 Want to recover solvent yet e s NO y 2 Want to use inert gas 2 Want to use inert gas such as Nitrogen or Argon such as Nitrogen or Argon Atype Btype Dtype Simple system connection Simple system connection Closed circulation system Closed circulation system Just connect to vacuum pump Replace gas Replace gas Eech P 16 18 P 1923 H 24 29 73 BioChromato SE 5 1 A_Type Simple system connection P 12 15 Ex Included items Not included items Machine Vacuum pump e Power cord Vacuum hose Container 5 1 1 Connecting method Turn off machine and pump power before connecting them with a vacuum hose Confirm specifications for power supply before use Please confirm the vacuum pump works properly before use Please use an adequate and moderate vacuum hose Please avoid tension and bending of the vacuum hose and the power cord Please connect the power cord correctly nn er 1 Connect the power connection 45 and the outlet with the power cord 2 Connect the port C and the suction port of the vacuum pump with the vacuum hose 73 BioChromato 12 5 1 2 Set target temperature Keep the max temperature below 100 C to avoid damages to the machine Set the target temperat
9. g gas please leak the gas always Er 1 Connect the power connection 45 and the outlet with the power cord 2 Connect the port C and the suction port of vacuum pump with the vacuum hose 3 To take out plugs 4 To connect the gas tube Please take out plugs by pushing the root of Connect the port A D and the gas tank with the plug from the port A and Orifice the gas tube Gas tube Orifice 73 BioChromato z 16 5 2 2 Set target temperature Keep the max temperature below 100 C to avoid damages to the machine Set the target temperature above room temperature 1 Turn on the Power for temperature control GA Wkey for setting temperature Current temperature Target temperature Select temperature from room temperature to 100 C 1 2 1 Please use this device after reaching target temperature 2 Please do not touch the key except for A Wkey It may cause a malfunction 5 2 3 To place the container 1 To open the cover Please open the cover with snap locks Snap lock D Cover 6 3 To connect the Spiral Plug unit with the container Please adjust a height according to your container the dial 2 To place the container Please set up the container in aluminum beads Container Aluminum beads Put samples in a container from quarter to half container volume 4 To close the cover Please close the cover with snap locks 73 BioChromato
10. ghtly Then turn off the machine and vacuum pump 2 Then close the valve of the gas supply 3 Take out the container after cooling down the heated container 73 BioChromato 99 Chapter 6 Troubleshooting P 30 Error type Inspection Treatment Can t use and set Check the power cord Please connect the power connection and Se nn If the temperature control Check the duration of the use Please turn off the power e ee Ler Sucking and splash Check the gas influx Please adjust gas influx gradually after segs emer nn Can t generate the Check the connection between Please connect the vacuum pump Spiral air flow vacuum pump and vacuum hose and vacuum hose firmly Check the connecting condition Please connect the joint between the Spiral Plug unit and and Spiral Plug unit firmly the container Check the flow rate of the Please confirm the flow rate vacuum pump of the vacuum pump by referring to the manufacturer s instruction If you can t resolve any problems please feel free to ask our local distributor La BioChromato 30 z Chapter 7 Question and Answer P 31 Q 1 How long can use the Spiral Plug unit Answer It depends on the frequency of use However we recommend to replace the old Spiral Plug unit with a new one periodically Q 2 I m worried about the contamination from the Spiral Plug unit Answer It depends on the solvent However materials PTFE PFA and THV are resistan
11. h the vacuum hose lt Step2 Connect the vacuum pump and cold trap gt Connect the exhaust port of vacuum pump and cold trap under with vacuum hose lt Step3 Connect the machine and cold trap gt Connect the port B and the cold trap upper with vacuum hose lt Step4 Connect the power connection gt Connect the outlet with the power cord 5 3 3 Set target temperature Keep the max temperature below 100 C to avoid damages to the machine Set the target temperature above room temperature 1 Turn on the Power for temperature control DCurrent temperature Target temperature GA Wkey for setting temperature Select temperature from room temperature to 100 C 1 2 73 BioChromato 8 21 1 Please use this device after reaching target temperature 2 Please do not touch the key except for A Wkey It may cause a malfunction 5 3 4 Starting concentration i Preparing refrigerant 1 Put the refrigerant in the cold trap Don t use cold trap with liquid nitrogen because it could cause an explosion due to the liquefaction of oxygen in air ii To place the container 1 To open the cover 2 To place the container Please open the cover with snap locks Please set up the container on aluminum beads Snap lock D Container Cover 6 Aluminum beads Put samples in a container from quarter to half container volume 3 To connect the Spiral Plug unit with 4 To clo
12. le system connection P12 15 5 2 Simple system connection Replacing gas P 16 18 5 3 Closed circulation system P 19 23 5 4 Closed circulation system Replacing gas P 24 29 Chapter 6 Troubleshooting P 30 Chapter 7 Question and Answer P 31 Chapter 8 Limited Warranty P 32 Chapter 9 Product Specifications P 33 4 BioChromato Chapter 2 To use safely P 4 6 2 1 Important safety instructions There are two messages below May result in death and serious injury May result in minor injury and property damage Use for volatile solvents only Please protect the machine from water inflammable gas and explosive gas Insufficient protection may result in a fire malfunctioning or break down Don t expose the unit to avoid shock hazard Please follow safety instructions during use If you use the Smart Evaporator for in different ways other than instruction in this manual we are not liable for any damages arising 4 BioChromato 2 2 Setting up the machine Don t use the Smart Evaporator outside laboratory Avoid watery area or water splash Avoid tilt vibration and shock A Warning Keep the machine and the power cord away from heat Connect the power cord properly Don t place something on power cord to avoid accidents Don t use multiple tap electricity with the Smart Evaporator Place the machine horizontally Keep enough space around the Smart Evaporator to avoid heat
13. luminum Snap lock D Container Cover 6 Aluminum beads Put samples in a container from quarter to half container volume 73 BioChromato 27 3 To connect the Spiral Plug unit with the container Please adjust a height according to your container the dial 5 4 5 Replacing gas 1 To open a valve of a gas supply Please open a valve of a gas supply Ex Gas line Must have gas overflow 3 Put on a plug to the Orifice Please put on a plug to the Orifice 5 4 6 Start concentration 1 To turn on the vacuum pump Please turn on the vacuum pump Close the valve tightly before you begin concentration If you use your pump please confirm a manual provided by a manufacturer 4 To close the cover Please close the cover with snap locks 2 To flow the gas Please start flowing gas about 2 min at 10 L min 1 1 Gas replacement with the system is not 100 When replacing gas only use the containers that fit Spiral Plug P1 or P2 some work with P3 4 Remove the gas tube Please remove the gas tube Then put ona plug to the Port A 2 To adjust gas influx Please adjust gas influx with the vacuum control valve AD Vacuum control valve MW To avoid sample loss and damages to machine and pump due to sudden suction adjust gas influx with the valve gradually 73 BioChromato 28 5 4 7 After finishing concentration 1 Close the vacuum control valve OD ti
14. mediately 2 Disclaimer The company is not liable for any damages arising from earthquakes lightning storms floods or other natural disasters as well as fires actions by third parties other accidents intentional or mistaken operation by the customer or use under other unusual conditions outside the responsibility of the company The company is not liable for any damages loss of business income disruption of business and etc arising from use of or inability to use the product The company is not liable for any damages from using in different ways other than instruction in this manual 4 BioChromato Chapter 3 Part names P 7 8 3 1 Front side Port A Cover Orifice DSnap locks Joint Plate Temperature Dial control block Handle A E Vacuum control valve Power for temperature control Temperature control panel Part name Function Port A In case of the replacing gas connect the gas tube Orifice In case of the replacing gas leak gas Temperature control block To regulate the temperature Please put aluminum beads in before use Power for temperature control To supply electricity to temperature control block To turn the temperature unit on off lt 4 BioChromato 3 2 Back side A3Port B d Port C d5Power connection Part name Function Port B To connect the circulation hose Port C To connect the vacuum hose D Power connection To connect the power cord
15. nated voltage and frequency in this manual Troubles and damages because of unsuitable repairs Troubles and damages because of the alternation to machine and disassembling Unrelated alternations to the function and performance such as color change noise and vibration Reaching part life due to the frequent use of the machine Consumable parts Troubles and damages due to natural disaster fire and other external causes Troubles and damages caused by storing the machine under harsh conditions such as exposure to high temperature high humidity harmful chemicals corrosive gas Troubles and damages caused by contaminants with sand mud water and reagents Troubles and damages caused by using the machine for other applications that are not described in this manual 4 BioChromato z 32 8 Chapter 9 Product Specifications P 33 Product name Smart Evaporator C1 Product code C1 Color 120 A Outer size mm W 220 D 270 H 389 Net 5 3kg Weight kg Gross 8 5kg Body PTFE SUS304 C3604 THV PBT NBR Wetted materials Denatured PTFE Spiral Plug Unit PTFE PFA POM FKM Number of sample One Heating control temperature From room temperature to 100 C Operating temperature limits From 10 C to 40 C Operating humidity limits From 20 to 70 No condensation If some parts of this explanation may not be applied to your machine please ask your local distributor 4 BioChromato 33 Dist
16. port Thick For the suction port d Fine Thick Cold trap Erlenmeyer flask Qty 1 Qty 1 Holder Cut ring Qty 2 Qty 1 I 73 BioChromato 24 8 Hose splice For port of circulation Qty 1 5 4 2 Connecting method Don t use cold trap with liquid nitrogen because it could cause A Warning explosion due to the liquefaction of oxygen in air Must confirm all connecting method before use As much as possible use the Smart Evaporator with our IN Caution recommendation items such as pump cold trap and etc 5 4 2 1 Preparing the vacuum pump 1 Connect the thick hose splice to the suction port of vacuum pump 2 Connect the fine hose splices to the exhaust port of vacuum pump Inlet Exhaust port 5 4 2 2 Preparing the cold trap Connect the cold trap and the stand with the clamp 5 4 2 3 Preparing Smart Evaporator 1 Connect the hose splice to port B 13 2 Connect the hose splice to port C 9 3 Connect the power connection 5 and the power cord Two hose splices are the same ones See P 8 9 for the reference of the part number in the description above 73 BioChromato 25 5 4 2 4 Connection all accessories lt Step1 Connect the machine and the vacuum pump gt 1 Connect the power connection 5 and the outlet with the power cord 2 Connect the port C and the suction port of the vacuum pump with the vacuum hose lt Step2 Connect the vacuum pump and
17. ributor Manufacturer BioChromato USA BioChromato Inc http biochromato com http www bicr biz E mail info biochromato com E mail info bicr co jp 7098 Miratech Drive 1 12 19 Honcho Ste 100 Fujisawa shi Kanagawa Ken San Diego CA 92121 2510053 Japan TEL 858 385 2006 TEL 0081 466 23 8382 lt 4 BioChromato 34
18. se splices Vacuum hose Qty 1 Qty 2 Qty 1 Fine For the exhaust port Thick For the suction port B Fine Thick Cold trap Erlenmeyer flask Qty 1 Qty 1 Holder Cut ring Qty 2 Qty 1 e 73 BioChromato 19 Hose splice For port of circulation Qty 1 5 3 2 Connecting method Don t use cold trap with liquid nitrogen because it could cause A Warning explosion due to the liquefaction of oxygen in air Must confirm all connecting method before use As much as possible use the Smart Evaporator with our IN Caution recommendation items such as pump cold trap and etc 5 3 2 1 Preparing the vacuum pump 1 Connect the thick hose splice to the suction port of vacuum pump 2 Connect the fine hose splices to the exhaust port of vacuum pump Inlet Exhaust port 5 3 2 2 Preparing the cold trap Connect the cold trap and the stand with the clamp 5 3 2 3 Preparing Smart Evaporator 1 Connect the hose splice to port B 13 2 Connect the hose splice to port C 9 3 Connect the power connection 5 and the power cord Two hose splices are the same ones See P 8 9 for the reference of the part number in the description above 73 BioChromato 20 8 5 3 2 4 Connection all accessories lt Step1 Connect the machine and the vacuum pump gt Connect the power connection 5 and the outlet with the power cord Connect the port C and the suction port of the vacuum pump wit
19. se the cover the Please close the cover with snap locks container Please adjust a height according to your container the dial 73 BioChromato 292 z 5 3 5 Start concentration 1 To turn on the vacuum pump 2 To adjust gas influx Please turn on the vacuum pump Please adjust gas influx with the vacuum Close the valve tightly before you begin control valve AD concentration If you use your pump please confirm a manual provided by a manufacturer Vacuum control valve MW To avoid sample loss and damages to machine and pump due to sudden suction adjust gas influx with the valve gradually 5 3 6 After finishing concentration 1 Close the vacuum control valve OD tightly Then turn off the machine and vacuum pump 2 Take out the container after cooling down the heated container 4 BioChromato 5 4 D Type Closed circulation system Replacing gas P 24 29 The Smart Evaporator can be used for the concentration within the closed circulation system In addition it can replace the air within the system with gas such as Nitrogen or Argon Included items Not included items Machine Circulation system Power cord Refrigerant Container Gas tank Gas line and etc Gas tube pressure tightness 5 4 1 To confirm accessories To confirm all accessories below Don t lose any accessories Vacuum pump Hose splices Vacuum hose Qty 1 Qty 2 Qty 1 Fine For the exhaust
20. ure above room temperature 1 Turn on the Power for temperature control Current temperature Target temperature GA Wkey for setting temperature Select temperature from room temperature to 100 C 1 2 1 Please use this device after reaching target temperature 2 Please do not touch the key except for A Wkey It may cause a malfunction 5 1 3 To place the container Don t touch the temperature control block aluminum beads and the container immediately after using There is a danger of burns fire and or an accident If you put samples in a container more than half container volume the machine will suck up samples directly This will damage the machine and pump Please place machine and container horizontally Please confirm the size of Spiral Plug unit size before use 1 To open the cover 2 To place the container Please open the cover with snap locks CO Please set up the container in aluminum Snap lock Container Cover 6 Aluminum beads Put samples in a container from quarter to half container volume 73 BioChromato 13 3 To connect the Spiral Plug unit with the container Please adjust a height according to your container the dial 5 1 4 Starting concentration 4 To close the cover Please close the cover with snap locks 7 In case of using temperature control start concentration after reaching the target temperature Please confirm to close
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