2 Mo PDF file - ARTEC
Contents
1. Number of points ignored E Total porosity T Water mass Number of exponential E Partial water quantity E Humidity Number of points used in exponential T Partial porosity Siccity nie Export EL All exports are made into a csv file List of measurement Pas Unique Measurements ID to export ex 11 15 17 20 Data to export rs i Number of points used E Ei Author for the deconvolution E F Smoothing deconvolution E Study F TMin deconvolution Curves E TMax deconvolution Sequence Delimiter 1 T1 Calibration sample E Delimiter 2 T2 a Date E Total water quantity E Water percent Address where you want to save csv file export Ke This function allows you to export to CSV of a part or all the information relating to a measure in the Show database Select the measurement to export using Select measurements Sort measurements Identifiant F Date 2000 01 01 e 2015 04 12 2013 03 27 16 2 898 83 Ajouter l ID Add the measurements displayed Measurements ID to export ex 11 13 15 20 Accept Select the measurement ID and click Ajouter ARTEC SYSTEM SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 It is possible to a2. On this result window it is possible to recalculate exponential and deconvolution processing on measurement Two display modes are available for each curve the time scale can be either linear or logarithmic It is possible to show or hide the information of the measure This panel contains information about the sequence and the calibration Measurements and exponential processing setting It is possible to display different curves from the measurement absolute value rephase or noise power factor correction following the imaginary This menu allows the deletion of point at beginning of the curve It is also possible to modify the multi exponential calculation parameters These parameters are the number of points to use these points are systematically taken early in the curve and the number of exponentials to calculate Deconvolution setting It is possible from this mode to verify the proper calculation of deconvolution with the result of the calibration If necessary it is possible to test a modification of start and end of the calculation the number of calculation time and the curve smoothing If the standard is correct Store it by clicking on save otherwise come back to the settings window by Back Calibration sample ARTEC SYSTEM SARL au cap de 75 000 euros Si ge social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay
3. There is by default an expert login implemented in the software identifier and password Exp It is possible for the administrator to create other users with Expert rights mi 1 da 1 gt 2 se gt 3 Welcome to expert mode w n ely gt 5 my gt 6 gt 7 gt 8 a gt 9 be gt 10 mim 11 mp gt 12 Depending on customer options some of these features may be inaccessible New measurement New calibration New sequence Expert options Summary Curve comparison Well comparison Auto calibration Ger ee oe En Opening measurement 10 Export 11 Disconnection 12 Closing the application ARTEC SYSTEM SARL au cap de 75 000 euros Si ge social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 New sequence This window allows editing of the NMR CPMG or FID sequences in order to perform measurements Expert panel B ex jem EJ B b j x ty P90 P180 Tacq180 Tacq90 Frequency Dead time Phase Sequence name Study Sequence commentary Create sequence Presentecion de uno scan 8 40 ps 16 70 ps 20 us 10 us 7 98600 MHz 100 us Phase 2 y Sequence type Scans number
4. Identifiant H Date 1752 09 14 2015 04 12 2013 03 27 15 4 Sort by author 2013 03 27 15 5 ESS Unique ID 2013 03 27 16 1 Refresh Show the sequence Select sequence To select the sequence click on the corresponding ID the integer highlighted on the image then click on select the sequence It is possible to use the filters on the right to simplify the search for the desired sequence Calibration sample This field contains the name of the calibration sample to use To change the calibration sample to use click selection window appears This lists all the calibration sample in the database Select a calibration sample Name Date 2000 01 01 2013 04 12 TEST42003 2013 03 27 16 2 3 fier Par Auteur Tier Par Etude Show calibration sample settings To select the calibration sample click on the corresponding ID the integer highlighted on the image then click on select calibration sample It is possible to use the filters on the right to simplify the search for the desired calibration sample Sample mass Fill in the precise weights of the standard This value will be used for calculation of moisture ARTEC SYSTEM SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 Liqui
5. DIASPEC 18 Low field NMR relaxometry equipment User manual Summary SVS COMENT ea a a et a a a le ne EELER eegene ed 2 FERCA OCI Lee EE SLAUE IMOMC HOM et eg E e Radiofrequency structure RF scwassdencncesaracsancdeenateandacieussdnninnsonatecinusaduannousndeslannbbowunsusadedwasaiencrdoasdarnanes Structure geometry DISCO eebe Measuring equipement Connection DIALOG SO MATE DS EC e a cn LS SCOR CNS SON de ae gen EE EE EEN KSE en e ea eee ne a a en ee a te ten IVE WE ee Lee PR E E E EE A E A E 11 NO AS EE 14 RI lge E 19 CRY COMPARER ae eee a er et me oies 20 ege CaO ALO EE 21 OCR NS ET FG a eo nn da a a nie 22 5 4 80 9 D ee ne ee ee arr ere Seer er ter 24 3 EECHER 26 EE 27 POO IE OS are Patra ise atts reuse ts ee ct ee srt carci das dni one 32 4 Administrator mode ccceescccccssssseccccseesseccccseussecccsseuseececsseuseesecsseuseeeesssuuseceeeseuuseseesseaaeeeeesias 35 B VY RO D a E 36 DO SR a 38 EI ege D EEE 39 ARTEC SYSTEM SARL au cap de 75 000 euros Si ge social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 I System overview ARTEC SYSTEM propose a non destructive measurement system based on low field magnetic resonance technology to measure quantity of water oil or grease establish quality criteria a
6. Echoes number Waiting time Tau Averaging Measure Save sequence Reset A sequence is composed of the following parameters P90 Duration of the P90 pulse P180 Duration of the P180 pulse P180 is close to 2 P90 TACQ180 Duration of the acquisition of a CPMG echo TACQ90 Duration of the acquisition of the decay of magnetization after a pulse P90 choice FID Frequency Working frequency of the instrument Dead time DT Dead time before and after each pulse Prevents the registration of erroneous data due to residues of pulses FID Phase Phase cycling Recommended value SEQ2 Default Sequence type choice of the type of the NMR sequence to launch CPMG or FID Number of scans nScan The number of repetitions scans of the sequence The measured values are accumulated and then divided by the number of scans To get a better signal to noise ratio Recommended value a multiple of 4 with the choice of phase phase 2 Number of echoes nEch The number of echoes defines the number of measured points of the signal For quantities of water measurements a small number is sufficient 50 For relaxation times of the sample increase the number of echoes in order to obtain the complete decay of the signal SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com
7. power factor correction following the imaginary This menu allows the deletion of points at beginning of the curve It is also possible to modify the multi exponential calculation parameters These parameters are the number of points to use these points are systematically taken early in the curve and the number of exponentials to calculate ARTEC SYSTEM SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 Deconvolution setting It is possible from this mode to verify the proper calculation of deconvolution with the result of the calibration If necessary it is possible to test a modification of start and end of the calculation the number of calculation time and the curve smoothing In addition it is possible to use the delimiter to know the partial porosity of the sample at an interval deconvolution part of the curve in dark green Information about these calculations are shown in the Information panel ARTEC SYSTEM SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 Export
8. Select a sequence Date 1752 09 14 2013 04 12 2013 03 27 15 4 2013 02 27 15 5 Unique ID Refresh 2013 03 27 16 1 Show the sequence Select sequence To select the sequence you want click on the corresponding ID the integer highlighted on the image then click on select the sequence It is possible to use the filters on the right to simplify the search for the desired sequence Validate by clicking Sslectsequence iii Accept Click on for validate the options En TA Calibration Fill the parameters related to the sample Measurement Name The name of the measurement will be automatically filled to the measurement Liquid density Density of the liquid having served for the saturation of the sample ARTEC SYSTEM SARL au cap de 75 000 euros Si ge social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 Sample particle Granularity of the sample in the case of measurements on cuttings approx 2 7 For measurements on other sample types this value has no importance but must be gt 0 Sample mass Total mass of the sample for the calculation of moisture Machine type Choose DIASPEC Cuttings for DIASPEC 18 Measure Start measurement Measure sw Porosity mode Porosity Zoom activ
9. 0 0000 MHz Action Launch automatic calibration a 600 400 200 0 200 400 600 P90 0 00 ps Sequence type Scans number Echoes number Waiting time Tau Averaging 800 1 000 1 000 800 600 400 200 200 1000 ms 100 ps Spts 400 P180 600 800 1 000 0 00 ps Reset Default The automatic calibration tool allows a search of the optimal parameters of the measurement The calibration is carried out in three phases searching for the resonant frequency of the device then search for P90 and P180 research To start a calibration enter the parameters of the sequence near optimal settings It is possible for simplicity choose a sequence database or use the default settings Default Caution is recommended for the successful completion of the calibration using a sufficient number of scans at least 20 a sample wet enough and low number of echoes one hundred Once the calibration is complete a window appears providing the backup settings as default settings found These settings can be changed later see Expert Options ARTEC SYSTEM SARL au cap de 75 000 euros Si ge social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 Open measurement Open measurement Open
10. 250 g Ai 3 0 00 Taui 3 0 00 g 200 150 Ai 4 0 00 Taui 4 0 00 100 Ai 5 0 00 Taui 5 0 00 50 Water percent 95 36 Water mass 0 95 mg Parameters Deconvolution Parameters Humidity 95 36 TMin 0 01 Smoothing 0 30 Partial water que 0 39 mg z Siccity 0 05 TMax 100 00 gt Number of poin 100 Percentage ofp 41 02 Signal to noise 220 59 Save Back to Measurement Informations On this result window it is possible to recalculate treatments and exponential deconvolution of the measurement Two display modes are available for each curve the time scale can be either linear or logarithmic It is possible to show or hide the information from the measurement This section contains information about the sequence and the standard achieved More he finds the results of calculations on the measurement Measurement and exponential processing setting It is possible to display different curves from the measurement absolute value rephase or noise angle correction following the imaginary This menu allows the deletion of point at beginning of the curve It is also possible to modify the multi exponential calculation parameters These parameters are the number of points to use these points are systematically taken early in the curve and the number of exponentials to calculate ARTEC SYSTEM SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France
11. 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 New measurement Expert panel B ex ee El B b j ty Measurement Select sequence and calibration sample The measurement name The measurement study Calibration sample name TEST42003 Unique calibration sample ID 1 Wi Sequence name 42003 Unique sequence ID 3 ii Additional parameters Sample mass 20000 00 mg Liquid density 1 00 Partide density 0 00 Type of machine DIAMAT 7 If DIASPEC carrot Volume 0 00 cm3 Commentary Actions Reset 2 This window allows to fill parameters for the creation of a new sequence The parameters are as follows Measurement name This field contains the name of the measurement This name must be unique Study Fill in the study name the measurement was created for Several measurement may belong to the same study Sequence selection This field contains the name of the sequence to use To change the sequence to use click LJ A selection window appears This lists all the sequences in the database SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 ARTEC SYSTEM Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com Select a sequence
12. Zoom activated Scale Linear Z Measurement Calibration sample Sequence A 3 500 e E quence name S 3 000 2 500 Autor s name Exp D 2 000 Date 2013 04 15 14 27 02 1 500 Study test Jy Commentary Measurement parameters Exponential fitting parameter parameters Signal to noise an d z ll ess ignal to noise ei Number of points ignored 0 Pe Number of poin 100 Calculate SE EE M td a Number of expe 1 ponential fittir 183 73 P90 8 40 P180 16 70 Deconvolution Tacq180 20 Zoom activated Scale Logarithmic Tacq90 10 200 Dead time 100 a Frequency 7 9860 es Phase Phase 2 Sequence type CPMG Scans number 16 Echoes number 1000 Waiting time 1000 Tau 100 Parameters Averaging 5 2 nt pce Ce 7 ax 100 00 of points 100 sl os ger Number of Deconvolution Fe Back to Sequence Informations On this result window it is possible to recalculate exponential and deconvolution processing on measurement Two display modes are available for each curve the time scale can be either linear or logarithmic It is possible to show or hide the information of the measure This panel contains information about the sequence This function not calling calibration the calculations are made for visual analysis of the good treatment The numerical results are not given Measurements and exponential processing setting It is possible to display different curves from the measureme
13. au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 Identifiant Select a sequence ARTEC SYSTEM Date 2013 03 27 15 4 2013 03 27 15 5 2013 03 27 16 1 By default 1752 09 14 Calibration name This field contains the name of the future standard This name must be Sequence selection This field contains the name of the sequence to use To change the sequence to use click on Window appears It list all the sequences in the database Refresh Show the sequence Select sequence Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com 2013 04 12 Sort by author M Sort by study M Unique ID To select the sequence you want click on the corresponding ID the integer highlighted on the image then click on select the sequence It is possible to use the filters on the right to simplify the search for the desired sequence Calibration study Fills in the study name for which the calibration was created Several calibration can belong to the same study Mass of the calibration sample Fill in the precise mass of the sample used for the calibration This value is used for calculation of humidity measurements using this calibration Density of the liquid s saturation Density of the liquid having served to saturate the sample Comment T
14. measurement Measurement name test42003 Measurement ID 1 Measurements and exponential fitting 2 500 2 000 1 500 Scale Linear Le Zoom activated 1 000 un 500 0 ts nr LR a 0 50 100 150 200 Time E Calibration sample curve W Measurement curve W Courbe Multi Exponentielle Exponential fitting parameters Number of points ignored Number of points used 100 Quantit d eau totale 20069 36 mg a Calculate Exponential fitting Curve type i Number of exponential terms 1 Total porosity 0 00 Deconvolution Scale Linear M Zoom activated 300 250 T 200 5150 o 100 50 0 0 20 40 60 80 100 Time Delimiters Parameters Deconvolution Parameters Partial water quantity 11575 60 mg eee Partial porosity 57 68 Informations This window allows the reopening of a measurement database To select the measurement click It is possible to recalculate exponential and deconvolution processing of the measurement Two display modes are available for each curve the time scale can be either linear or logarithmic It is possible to show or hide the information from the measurement This section contains information about the sequence and the standard achieved Moreover he finds the results of calculations on the measurement Measurment and exponential processing setting It is possible to display different curves from the measurement absolute value rephase or noise
15. 3 000 Measurement name 2 500 Liquid density 0 00 T 2 000 Sample partide 0 00 5 Sample mass 0 00 n 1 500 Engine type DIAMAT Cuttings z 1 000 i If DIASPEC Carrot 0 00 an3 500 0 0 50 100 150 Time Zoom activated Scale type Linear v 1 000 Sequence 1 800 e 600 S E param 1 Decimal number NC 200 0 Sa an PL al ee LS EL EE Fee Eesen 0 200 400 600 800 1 000 Time Actions Calibration Measure Options If the calibration is correct it is possible to make a measurement Fill the parameters related to the sample Measurement Name The name of the measurement will be automatically filled to each measurement Liquid density Density of the liquid having used for the saturation of the sample Sample particle Granularity of the sample in the case of measurements on cuttings approx 2 7 For measurements on other sample types this value has no importance but must be gt O Sample mass Total mass of the sample for the calculation of moisture Machine type Choose DIASPEC Cuttings for DIASPEC 18 Choose a sequence Lie Measure Launch measurement ARTEC SYSTEM SARL au cap de 75 000 euros Si ge social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 Operator mode Operator Zoom activated C
16. 7100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20
17. RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 The signal is recorded on a time interval 2 Tau nEch Waiting time RD Time between two scans This time must be at least equal to 5 times the system dominant relaxation time ARTEC SYSTEM Tau Time between pulses P90 and P180 The signal is recorded on a time interval 2 Tau nEch Averaging Number of points at the top of the echo used to filter the value of the maximum of the echo Sequence name Name of the sequence must be unique Comment This field can be left blank or contain the information that the user considers as useful Buttons at the bottom have the following actions Reset This button empty boxes in the window Default This button filled the box containing the parameters of the sequence by the saved default settings Save sequence Allows you to save the sequence in the database Measure This mode allows to test the sequence before saving it Pressing this button launches a measure from the filled sequence ARTEC SYSTEM SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 raie Results ate Measurements and exponential fitting Infos a iat
18. Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 Deconvolution setting It is possible from this mode to verify the proper calculation of deconvolution with the result of the calibration If necessary it is possible to test a modification of start and end of the calculation the number of calculation time and the curve smoothing Furthermore it is possible to use the delimiter function to know the partial porosity of the sample at an interval deconvolution part of the curve in dark green Measurement can be saved by clicking on save Back to Measurement To do another measurement use Warning if the previous measurement has not been saved it will be lost ARTEC SYSTEM SARL au cap de 75 000 euros Si ge social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 Options Default Measurement Parameters Default sequence 42003 Sequence s ID 3 Default Calibration Sample TEST 42003 Unique calibration sample ID 1 Number of points ignored 0 param 1 Decimal number number Default parameters of exponential and deconvolution computation Default number of points used Default smoothing Default number of expo
19. ated Cuve type Absolute 7 Scale type Linear z Parameters Results 3 500 Exponential results 3 000 Water quantity 100 02 2 500 Water mass 1 00 mg E 2 000 Humidity 100 02 5 Siccity 0 00 o 1 500 Porosity 1 00 1 000 Signal to noise 156 39 500 0 Deconvolution results 0 50 100 150 200 Partial water quantity 0 00 mg Time Percentage of water partial 0 01 Zoom activated Scale type 400 350 0 1072 311 7371 300 rh c 200 A i50 100 50 0 0 01 0 1 1 10 100 Time Actions Calibration Measure Options Save Percentage of water Water mass in the sample relative to the calibration Water mass Mass of water present in the sample Humidity Relative humidity of the sample Partial water quantity Water quantity shown between the delimiters deconvolution dark green Percentage of partial water Ratio of the amount of water between the delimiters relative to the total quantity of water Save The measure must be saved by pressing ARTEC SYSTEM SARL au cap de 75 000 euros Si ge social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 4 Administrator mode Administrator mode allows database and users managing A default identifier is available username and password Admin gt 1 tp gt 2 Welc
20. d density Density of liquid used in the saturation of the sample Particle density Granularity of the sample in the case of measurements on cuttings approx 2 7 For measurements on other sample types this value has no importance but must be gt 0 Comment This field may be left blank or contain information that the user considers useful To start the measurement click Po Messe ARTEC SYSTEM SARL au cap de 75 000 euros Si ge social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 Results Measurements and exponential fitting Infos Zoom activated Scale Linear x Measurement Calibration sample Sequence 3 500 Measurement name test Autor s name Exp Measurement date 2013 04 15 14 44 29 Measurement study test Sample mass 1 00 mg Liquid density 1 00 Particle density 1 00 Measurement parameters Exponential fitting parameter paramet Exponential fitting parameter paramet Type of machine DIASPEC Cuttings He 0 est 100 E Total water qu 0 95 mg Carrot Volume 1 00 cm3 Bes a E Calculate eessen UH lnential fi Curve type Magnitude Number of 1 1 Total porosity 0 95 Measurement commentary Deconvolution Zoom activated Scale Logarithmic z 400 Ai 1 3036 50 Taui 1 17 35 350 300 Ai 2 0 00 Taui 2 0 00 TW
21. dd multiple measures In addition the use of the filters allows the selection of a measurement assembly with the same properties After selecting the filter date author study click Add the measurements displayed When all measurements are selected click Accept O pt to validate the choice Select the area indicated by a red strap which attributes to export measures Choose a directory for the extraction Address where you want to save csv file export ge CSV files will be created in the desired destination by clicking on SES ARTEC SYSTEM SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 3 Operator mode There is one default operator identifier implemented in the software username and password Ope Administrator can create other operator mode access according the operator users O perator panel Welcome to operator mode 4 z m gt ma gt 5 Depending on customer options some of these features may be inaccessible Operator mode Porosity mode Summary Disconnection GE ae o Closing the application ARTEC SYSTEM SARL au cap de 75 000 euros Si ge social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec s
22. electing sequences thereby by pressing the button ARTEC SYSTEM SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 Select a sequence Identifiant Nan Date 1752 09 14 2013 04 12 2013 03 27 15 4 Sort by author 2013 03 27 15 5 aosblawistudy Unique ID 2013 03 27 16 1 Refresh Show the sequence Select sequence To select the sequence click on the corresponding ID the integer highlighted on the image corresponding then click on select the sequence It is possible to use the filters on the right to simplify the search for the desired sequence Accept When all parameters are filled one sequence is sufficient validate options VE were CR In the Parameters tab on the right choose asequence rrr WM Launch calibration ARTEC SYSTEM SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 Operator mode Operator Zoom activated Curve type Absolute Scale type Linear X Parameters Results 3 500 1 5915 3123 8318 Measurement parameters
23. his field can be left blank or contain the information that the user considers as useful To initiate the creation of the standard click on Calibration sample After the measurement is carried out the following window appears Results Measurements and exponential fitting Infos Zoom activated Scale Linear Measurement Calibration sample Sequence 3 500 geg SH 3 000 2 500 Author s name Exp 0 2 000 Date 2013 04 15 14 31 39 1 500 i 1 000 Study test 500 Mass 1 00 mg 0 Calibration sample density 1 00 Measurement parameters Exponential fitting parameter parameters Signal to noise Commentary E y z ini a ignal to noise Number of points ignored 0 n Number of poin 100 3 Calculate Sign Curve type Magnitude Number of expc 1 ponential fittir 188 01 Deconvolution Ai 1 3184 20 Taui 1 17 45 Zoom activated Scale Logarithmic nA Ai 2 0 00 Taui 2 0 00 Ai 3 0 00 Taui 3 0 00 200 Ai 4 0 00 Taui 4 0 00 E 150 Ai 5 0 00 Taui 5 0 00 n 100 Parameters TMin 1 01 Smoothing Calculate TMax 100 00 Number of points Been Save Back Calibration sample ARTEC SYSTEM SARL au cap de 75 000 euros Si ge social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20
24. mode Porosity mode allows quick and easy access to porosity measurements Porosity 3 500 3 000 2 500 TG 2 000 1 500 1 000 500 1 000 800 600 Signal 400 200 ti Fill options Open the settings panel by clicking Calibration sample parameters Porosity mode T Zoom activated Cuve type Absolute Scale type 0 50 100 150 200 Time E Zoom activated Scale type 0 200 400 600 800 1 000 Time Calibration Options sequence 42003 Partide Density Liquid density Parameters Results Measurement parameters Measurement name Liquid density 0 00 Sample partide 0 00 Sample mass 0 00 Engine type If DIASPEC Carrot Volume Commentary param 1 Decimal number NC Options Unique sequence ID ARTEC SYSTEM SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 Calibration settings To achieve a proper calibration it is important to fill the mass of the sample used for calibration and its density Sequence choice Operator mode provides quick access to three different sequences though it is possible to use only one Selecting sequences thereby by pressing the button
25. nd characterize porosity Materials covered by these analysis can take the form of solids liquids or pastes DIASPEC is a transportable measuring instrument ideal for rapid characterization of samples in the laboratory or quality control The measurement and results analysis software is easily handled by non expert operators in NMR 1 Diagram of the equipment The general structure of the equipment is represented in the figure below Power generator Duplexer PROBE Amplification et Demodulation C O N T R O L High power signals Low power signals ARTEC SYSTEM SARL au cap de 75 000 euros Si ge social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 2 Technical specifications Static induction of the sensor The material used for the generation of static and uniform magnetic field required to operate the sensor is neodymium iron boron It presents a good thermal stability up to 80 C In the configuration of Diaspec devices the volume of measurement corresponds to a cylinder with an axis perpendicular to the static field a diameter of 18 mm and a height of 20mm The value of the static induction BO is approximately 0 44 T varies around this value depending on the device The inhomogeneity of the magnetic field is le
26. nential terms Default minimum time Default maximum time Default number of points used Default T1 Delimiter Default T2 Delimiter P90 z Frequency P180 NbScans Tacg180 gt NbEchos Tacq90 Tau Dead Time Engine type DIASPEC Cuttings z Save parameters Reset Use this page to change the default settings There are three groups of settings Measurement settings Fill in this block the settings to used by default for measurement the sequence and the calibration Processing settings These are the parameters defined by the expert At the return of measurement multi exponential and deconvolution processing shall be performed with these settings These parameters will be used for the calculations of operator mode Sequence parameters These settings are loaded by default for creating sequence They correspond to the optimal sequence parameters for the machine These settings are saved by pressing Save parameters ARTEC SYSTEM SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 Curve compare Expert panel Compare er Curves selection Curve 1 test42003 Curve s ID 1 1 Curve selection a Curve 2 test42003 Cu
27. nstrumentation from the switch on the front panel of the instrumentation and one on the rear face Please wait 15 seconds before the first measurement CAUTION TO THE PRESENCE OF VOLTAGE IN THE CAPACITORS IN THE AMPLIFIER AFTER EXTINCTION OF THE DEVICE DO NOT OPEN THE BOX OF INSTRUMENTATION ARTEC SYSTEM SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 HI DIALOG software presentation 1 Starting the software Check the connections of the device power and signal Turn on the instrumentation rack Launch Dialog by double clicking on the shortcut icon PMJ Software open the login window ALOG Version 4 2 1 Database Version 2 exit login User login A login give a type of access privileges operator expert or administrator Password Captures the password Secure the identification Language Choice of language the software restarts with the chosen language Application exit button ARTEC SYSTEM SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 2 Expert mode
28. nt absolute value rephase or noise angle correction following the imaginary This menu allows the deletion of point at the beginning of the curve It is also possible to modify the multi exponential processing parameters These parameters are the number of points to use these points are systematically taken early in the curve and the number of exponentials to calculate Deconvolution setting It is possible from this mode to verify the proper calculation of deconvolution with the result of the test sequence If necessary it is possible to test a modification of start and end times of the calculation the number of calculated points and the curve smoothing ARTEC SYSTEM SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 New calibration Expert panel B c gt Create calibration sample Calibration name Calibration sample Sequence selection 42003 Sequence s ID 3 Calibration study Calibration mass 0 00 mg Liquid density 0 00 Remark gt Actions e Reset x Calibration sample This window allows to fill the parameters used for the creation of a new standard The parameters are the following unique Select a sequence SARL
29. ome to administrator mode A gt 3 mien gt 4 ete gt 5 The following functions are available User manager Database manager Change options Disconnection GE a o Closing the application ARTEC SYSTEM SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 User manager Users managements Add user usersist Three actions are possible from this panel Add user Adduser Admin panel Users managements amp Add user Users lst V w Add a new user to DIALOG User name Password Acces privileges Operator x add ty To add a user you must fill its name this will serve as an identifier a password to protect the user account and an access level Indeed an account gives access only to a single mode administrator operator or expert SESCH Add Validate account by clicking on ARTEC SYSTEM SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 Admin panel Users managements weg Lied rrr fe Users list ID Nom Passwo
30. rd Acces Etat Sort by ID 4 P 1 Admin Admin Administrateur Actif Sort by user name A Z v 2 Exp Exp Expert Actif 3 Ope Ope Operateur Actif gt v x Refresh From this list select a user by ID allows access to modify function ge ucr seting Admin panel Users managements E Add user Users list ser setting wei Users list ID Nom Password Acces Etat Sort by ID zj TEY HE 1 Admin Admin Administrateur Actif Sort by user name A Z 2 Exp Exp Expert Actif 3 Ope Ope Operateur Actif Refresh Change user settings User name Admin User password Admin Acces privileges Administrator NA nd Account state Enable account D Disabled account w n This function allows changing the selected user account Change the password type of access and the ability to disable the account The account will never be deleted but if given inactive the connection will be impossible Changes Confirm change are validated by clicking SI ARTEC SYSTEM SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 Database manager It is possible from this menu to display software database Admin panel Database management sa Show X w Database list U
31. rve s ID 2 1 Curve selection curve 3 cuvesID3 o Reset Hide the selection panel Pas Compare the curves Tr Measurements and exponential fitting ay Curves type Scale E Zoom activated 2 500 2 000 CG m q 21 000 n 0 0 50 100 150 200 Time E Curve 1 M Curve 2 P Deconvolutions Scale T Zoom activated 40 60 80 100 Time Deconvolution curve 1 Deconvolution curve 2 Ke This mode provides a graphical comparison of several curves To add a curve click Curve selection selection It Kee is then possible to remove the last added curve or all curves presents Button bitte the selection pane reduces the area occupied by selection to increase The area covered by the display of curves ARTEC SYSTEM SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 Automatic calibration Calibration Unique sequence ID 0 1 000 800 Expert panel is Automatic calibration SS Sequence name A P90 5 00 ps wie P180 10 00 ps Tacq180 50 us Tacq90 500 ps ay am Frequency 19 35260 MHz e Dead time 100 ps Se Phase Phase 2 X DI 1 000 ml 800 600 400 ha 200 EL Ey RE EL e Taian ae LE LE EL 0 200 400 600 800 1 000 Frequency
32. sers z P Identifiant Nam Passwor d Acces Stat A 1 Admin Adm Administrateur Actif 2 Exp Exp Expert Actif 3 Op Op Operat Actif gt For some base calibration measurement and sequence it is possible to delete the records one by one or emptying the entire database Careful records are permanently deleted ARTEC SYSTEM SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 Options Admin panel Options E Additional parameters a ek D 3 Accept number of Number of additional parameters 1 nldlenienanriess Integer Decimal number Word Parameter number New name Action La v Parameter 1 parami Modify gt es xX This function allows you to add additional parameters to the measurements The administrator informs the desired number of parameters and their types and names to display Accept number of additional parameters To add parameters increment the number and click After information on the type and name parameters validate its implementation by You need to fill the value of each parameter before launch a measurement The default value will be entered by the expert in the options menu ARTEC SYSTEM SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 0
33. ss than dBO BO 10 T in the measuring volume Radiofrequency structure RF The radiofrequency structure integrated inside the sensor includes an antenna and a transmission line coupling It generates an RF induction perpendicular to the static induction in the measuring volume Structure geometry Diaspec 18 e Measuring tube diameter 18mm external e Radial resolution 18mm diameter e Vertical resolution 20mm height The external metallic case of the measuring instrument is covered with an anti corrosion coating a b a overview of equipment with sensor and spectrometer b top view of the NMR diameter 18 mm sensor ARTEC SYSTEM SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 II System connection For a first powering of the equipment please follow the connection method 1 Connect the 50 ohm coaxial cable from the sensor to the back of the instrumentation 2 Connect the USB cable from the back of the instrumentation to one USB 2 0 socket on the computer Caution be sure to connect the instrumentation to a USB2 port of the computer Connection to a USB 3 port rated USB SS or blue plastic on some PC will result in the non recognition of the device 3 Turn onthe computer Turn on the i
34. urve type Absolute v Scale type Linear A Parameters Results 3 500 Exponential results 3 000 Percentage of water 99 88 2 500 Water mass 1 00 mg E Een Humidity 99 88 Ki Siccity 0 00 o 1 500 Porosity 1 00 1 000 Signal to noise 153 18 500 0 Deconvolution results RU CC EE EES LL 0 50 100 150 200 Partial water quantity 0 00 mg Time Percentage of partial water 0 00 Zoom activated Scale type Logarithmic X 400 350 300 SEA Z D 200 O i50 100 50 0 0 01 0 1 1 10 100 Time Actions Calibration Measure Options At the end of the measurement the calculations are done automatically according to the parameters specified in the expert options Calculation results are displayed in the right panel Percentage of water Water mass in the sample relative to the calibration Water mass Mass of water present in the sample Humidity Relative humidity of the sample Partial water quantity Water quantity shown between the delimiters deconvolution dark green Percentage of partial water Ratio of the amount of water between the delimiters relative to the total quantity of water The measure must be saved by pressing ARTEC SYSTEM SARL au cap de 75 000 euros Siege social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 Porosity
35. ystem com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 ARTEC Operator mode Operator mode allows quick and easy access to the NMR measurements Operator panel Operator mode RI E Zoom activated Curve type Scale type Parameters Results E 1 000 i i Measurement parameters Measurement name 800 Liquid density 0 00 ja SS se are e amp Sample mass 0 00 un 400 Engine type DIAMAT Cuttings If DIASPEC Carrot 200 W 0 00 cm3 0 0 200 400 600 800 omen Time F Zoom activated Scale type Linear v 1 000 800 T 600 E D W 400 200 344 4593 4 6948 0 200 400 600 800 1 000 Time Actions es Calibration Measure Options Opt Fill options Open the settings panel by clicking ARTEC SYSTEM SARL au cap de 75 000 euros Si ge social 45 Avenue Rhin Danube 07100 Annonay France Tel 33 0 4 75 69 22 21 Fax 33 0 4 75 69 22 19 Mail info artec system com RCS Annonay 505 395 293 Banque Soci t G n rale Annonay 30003 02161 00020419085 20 Options Calibration sample parameters Study Liquid density Mass Options Calibration settings To achieve a proper calibration it is important to fill the mass of the sample used for calibration and its density Sequence choice Operator mode provides quick access to three different sequences though it is possible to use only one S
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