- JADE USER`S MANUAL - David Von Rohr 8/12/02 1. Double
Contents
1. is Jade 6 dave Drexel University Materials En File Edit Filters Analyze identify Qj sie elele em ul RE 2T 62 825 0 Peaks Raw Pattern d 1 4779 ing Monday Aug 12 2002 MATECU LEL PDF nem TEES ar ll Save Erase Macro Axes Tm vem Zoom Bun Web lel a zi 848 2 Theta LOG OFF 11 To return to the normal view simply press the lt Space Bar gt on the keyboard 12 On the right hand side of the bottom window is a vertical series of 9 icons ui i F r Spruce p ee erie 1 rire rears noe m Bun weh Qj le slol elm all Ilo siters v 1 I gt el a ee ee arar rrara peria srnka rga E aaa apm a min y Y T Zoom and Pan Control Buttons These are the Zoom and Pan buttons they allow you to move around the spectrum and view your particular areas of interest on the pattern 13 Ka2 peak stripping requires that the background be removed first To remove the background and then do curve fitting Go to the ANALYZE FIT BACKGROUND menu dit Filt PDF B M dep 9 s gt imm Find Peaks Fe gt FI exol o r Fi TIRE E EE Wart 0 0 a Fit Peak Profile dd mense us SCAN 3 39 95 149 95 0 1 0 5 sec Cu l max 380 03 11 97 12 50 Theta Calibration Simulate Pattern Fi UR n TON em Sheers TUM en pP sene ffs a fn e2. Raw Counts C Peak Area Vertical Font 3 PAN Asterisk Marker Scaling al 0 0 2 Save Heset Apply Close By placing a check mark in the above boxes this information will be displayed on the pattern MIES File Edit Filters Analyze Identify PDF Options View Help Save Erase Macro Ages Hide Report Zoom Run Web Qi xele g lapse Fm exer XS IMATECU RAw MATECU U Gpun d 2 0839 2T243 385 B 0 218 Search Labeling Peak Labeling and Scaling V Line Marker v FWHM alles Angstrom C nm v d Spacing Peak ee aaa i rystallite Size Unit w 2 Theta w hkl Indices elec Intensity Peak Height RawCounts Peak Area Vertical Font 8 P N Asterisk Marker Scaling 0 0 0 2 E d1 8049 2T 50 526 8 0 239 BufietsutPesksencu E EE erat Apply i TEET haa 0 253 1 0894 2T 89 991 B 0 274 i d 0 8085 2T2144 536 B d 0 6296 2T 1 36 389 8 0 157 d 0 9559 2T 107 384 B 0 168 i Kathy sshd Mh At ds VM Pr A soles aint sud ri or 100 Derived Pattern 7 Peaks 2T272 131 d 1 3084 I 784 EE Theta LOG OFF FE Start Ux MADE USER Microsoft w S Jade 6 dave Drexel Uriv ea 1241 pm By clicking on the lt Report gt button The following information will also appear in the window la x File Edit Filters Analyze Identify PDF Options View Help Save Erase Macro Axes Hide Report Zoom Run Web 9j le lelo
3. Close Read Ada Flaca Erawse Refresh Find Filter Import Tritt jave Eapy Help I EE C mdi x MDI Asc Pattern Files mdi en EF amp MIT CPs o FileName SealD Cate C Multimedia Files J Program Files C TEMP _ WINNT 0 Files Sorted on File Name SA PES DSP POF PFT RPT Pio 52s KSI FIT 2TH SBC RIA 45 zz 6 Double Click the Folder you wish to use e g lt David gt Head Pattern Files T oday 1 Week 1 HMonth 1 Tear 14 Close Head Adad fear BIGWEE Refresh Find Filter Import Print SAVE EGm Help TEE csanatiesi m x MDI Ascu Pattern Files mdi All 3 0 Files Sorted on File Name 5 amp v PES DSP PDF PFT RPT PID S25 Ksi FIT 2TH ABC RIR JE 4 7 Change this setting to read as shown below Head Pattern Files Today 1 W eek 1 Month 1 Tear 1 sd Es Cerdhiles D avidi Sc al mM r cps r Ics 3 xrdfiles MATECR R AM 03710799 MATECU RA MATE 037 11 97 MATEW RAW 03 12797 SI z Faw 4 2133 Thumbnail Ore Thumbnail AI 4 Files Sorted on File Name 5 amp v PES DSP PDF PFT RPT PID S25 Ksi FIT 2TH ABC RIR JE 4 8 Now Double Click on the file you wish to open Head Pattern Files T oday 1 Week 1 Month 1 Tear 14 Close Read Add Maca Browse Refresh Find Filter Impor
4. JADE USER S MANUAL David Von Rohr 8 12 02 Double Click the MDI Jade nk Icon on the screen The Jade program should open into the following window Jade 6 dave Drexel University Materials Engineering Monday Aug 12 2002 DEMO06 MDI Red Paint Pigment Mixture File Edit Filters Analyze Identify PDF Options View Help Save Erase Macro Axes Hide Report Zoom Run Web Q l ee alm uu 24 5 e Aa ee S 7512 Press F1 for Help 3 IDEMOOE MDI Red Paint Pigment Mixture Efe BEER ERR NE EIE RUDI RENT gy Counts Intensity Counts A J3j on uM A Ae 2 50 i 6 0 RawPattem 0 Peaks 27 27 390 d 32535 552 2Theta sav PKS DSP PDF PFT APT PID szs KSI rir 2TH ABC RIR LOG OFF i 3 Select PATTERNS under the FILE menu Jade 6 dave Drexel University Materials Engineering Monday Aug 12 2002 DEMO06 MDI Red Paint Pigment Mixture Edit Filters Analyze Identify PDF Options View Help Save Erase Macro Axes Hide Report Zoom Run Web A iE EL Press F1 for Help Patterns Ctr O0 AM Thumbnail Ctrl T Recall File Ctrl F ed Paint Pigment Mixture SCA 20 0 Reload File Alt Bksp xplorer Ctrl Read Ctrl R Save E Lua AA toaa anA A C A A Nt ae Exit Chive Fee ay 1 O Quit Ctrl O sz Q da BE 25 Aa oa E 9 1 e9 1 11 10 EE ese UE AJ LM Raw P
5. Toggles Line markers OFF and ON V Changes text from vertical to horizontal You may now lt Print gt or lt Save gt your Pattern 1 Print Simply click on the Printer icon at the top of the screen and follow the directions 2 lt Save gt Click on the lt Save gt icon at the top
6. 143 35 0 1 0 5 sec Cu I max 830 03 11 97 12 50 A wA D Tnt en wi ENARE P ES EAN P ES E EEO IE aces ag I NIE IEE O OLE A A LL C TS eaa M uiri Peri ot bea Qo IF O a 0 08 El ke Q ha 85 5 Aa ea C E Q Search Labeling Report Filter Type Peak Location Threshold amp Range E Points 9 Summit Threshold Sigmas 3 00 a Parabolic Fiter C CentoidFt Intensity Cutot 2 010 3 Peak Editor Button C pes r M Quartic Filter Parabolic Fit Aane n APE ho 0 v Variable Filter Length Points Ponie lo Avera E ge BG 7 w Screen out K alpha2 Peaks a v Erase Existing Peak Listing Angular Range 40 0 fi 49 9 fy w hito hl loaa Me ende Pl P Mh Abo S NA vi dbi ay A A fd Phe in eg Mo fg ew M uy 40 i 50 l 60 70 80 g0 Derived Pattem 7 Peaks 27 108 125 d 0 95136 1 236 2 Theta LOG OFF AStart A e SX made USER Microsoft w S Jade 6 dave Drexel Univ GB 12 26 pm gt F e 9 13 4 16 LABELING By clicking on the tab marked lt Labeling gt you can now determine how you want your peaks to be Identified ci Peak Search Labeling amp Scaling sje mamuasauasasanamAmARA RARE Peak Labeling and Scaling Am d Spacing Unit W Line wis FWHM FETTE TS d Spacing Peak Sage Fae lin ee stalte Size Unit 2 Theta hkllIndices Anostoma C nm Intensity f Peak Height
7. and Point S ampling cC LO E NM EO Cubic Spline Automatic Threshold Sigmas 6 0 Strip K alpha2 K a1 a2 Ratio 2 0 Offset of BG Curve from BG Dots 0 0 Area above the Background Curve 40 0 137 0 2646 h 12 4 E Save Reset Strip K alpha2 Remove Apply Close D jl i i i im X h PAA Ne J n A v MOA MA ia AY y AP E uw 4 MM m MJ A 21 n y yj V viu T l y Lai y M MOUN J N 4 UJ 75 80 J B B 85 ia bi i 90 Raw Pattern 0 Peaks Tum 74 288 d 1 2757 1 63 2 Theta LOG OFF c When you are satisfied with you background corrections click on Strip Ka2 gt All the dots will go away and your pattern should now only contain the Kal peaks 15 PEAK FINDING You are now ready to have the computer identify all your peaks Go to the lt ANALYZE FIND PEAKS gt menu and the following screen should appear Jade 6 dave Drexel University Materials Engineering Monday Aug 12 2002 MATECU RAW MATECU File Edit Filters Analyze Identify PDF Options View Help Save Erase Macro Axes Hide Report Zoom Run Web 9l mee m ue e A ss se eS 731232 Press Ft for Help ies SS MATECU RAW w MATECU SCAN 39 95 149 95 0 1 0 5 sec Cu l max 830 03 11 97 12 50 ci Peak Search Labeling amp Scaling x Search Labeling Rea IL Hepar lihtesnold BAL m Filter Type m Peak Location Threshold amp Range Points 17 H Summit Threshold Sigma
8. the following window should appear FSICDDAICPDS PDF Retrievals Level 1 PDF Sets 1 51 12 30 99 xjuejmds elmie mlele e w elm e srrrr a ES T T Copper sin 4 LL D CFA Fm 3m 225 aber W atkinsonite ASS 12 1375 V mPF3l P 1 12 821 Wathersite HgSCr06 45 1381 Vv 33 mC48 Cc 15 117 250 Wi athevilleite Maz2La su4 214H20 41 1360 F 38 W avellite A P 4 2 OHj3IS 25 0020 x 69 aF84 Pemn B2 9 624 W awavandaite LalzMn4B Bel85 46 1357 7 Wo qe mF138 P c 13 15 58E W aylandite B CajMI3IPU4 SiO 39 0367 F hRS H 3m 155 6 974 Af ehente M ah oh lF F nA 44 Ww nl AA From 4341 T 3T At this point if you know your pattern number you may type it in the second block If you want the computer software to identify the pattern for you click on the lt S M gt button If this 1s the first time the pattern has been viewed the following window should appear Search Match Display Subfiles to Search Inorganics Minerals Default Search_Match Ew ese 5 P I w Quartz sun Sil 46 1045 y ll Wesselsite CusrSi4010 43 1813 C w aedrulfite znMn3D t2 H2 33 9 47 1825 1 widgiemaalthalite NiS COM DOH gA 333 46 1398 T y CT Willemite Ca rich f4n Col25i04 99 9 46 1316 v IL Wustite Fel 33 3 45 1312 5 3 Quartz syn 5102 2T 19 798 d 44807 1 6733 E H HU SID2 AAW SID2 PDF CSD m OFF 4 IEC TTTT Il When this window appears simply clic
9. 0000 o nj Willemite Co rich zn Ca 25i04 999 V 46 1376 3 1 0000 x w ustite Fel 33 3 Wo 45 1312 2 lt 1 nun lt 1 Press F1 for Help 2T 25 885 d 3 3135 B412 IH SID2 RA amp w S102 POF C5B LOG O0FF After selecting the correct pattern click on the lt Exit gt button which will return you to the main menu with all of the information on the screen Hopefully it will look like the screen below ig Jade 6 dave Drexel University Materials Engineering Monday Aug 12 2002 SI02 RAW S102 8 x File Edit Filters Analyze Identity PDF Options View Help n eem emm Macro Ew His pem Zoom Run Web Q se alo I ele alko 73 1232 zem Press F1 for Help EI cu v SIOZ AAW m 02 naxl 1 20f gt 04 27i i m A NU d Ew Se ie Es 27T 45 352 d 1 9980 I 7011 Ves 1 i ji yi i ZEN VT Mann ui IET SED EDS i aO b ES SR ROE j s Derived Pattern 7 Peaks 27 45 352 d 1 9980 l 7011 2 Theta LOG OFF distat A e SI mJDEUSER Microsoft w Jade 6 dave Drexel eB 222 Pm n i The Buttons on the bottom right hand of the screen are used to label your pattern with the information you would like to see on the printout The button labels are as follows N Toggles the name from which the peak came S102 Gives you the peak height percentage H Displays the hkl Sequence number of the iteration used for the peak find I
10. Background Function and Point S ampling v Automatic Threshold Sigmas 6 0 v Strip K alpha2 K a1 a2 Ratio 2 0 Offset of BG Curve from BG Dots 0 0 Area above the Background Curve Strip K alpha2 Remove Apply Close Inte i 9 E ao ne lec dy safi Aes peque F Ah hu ae I asd Ae ES NEWS i yv bibet Ave Pa dnd m ijo f li ath NX Nps ly T7 f Hh hs shell v hs we rhe eth Ah Bey Aon Ms av Apod TNR SU Mt iy i esi ot 1 iC NOR 110 40o 50 60 ce t nk o a Raw Pattern 0 Peaks 2T 106709 d 096004 le1178 2 Theta PDF ir 2 LOG OFF AStart A E SI amp MADE USER Microsoft w E Jade 6 dave Drexel c3 C eB 11 56 4m b The mouse will now turn into a small Crosshair type pointer This pointer is used to move the Background DOTS to the position which you feel is more appropriate for your pattern To move a DOT place the crosshair over it and click and hold down the left mouse button You may now move it UP DOWN LEFT or RIGHT depending on your needs File Edit Filte v PDF ERIT EE Nem m Ec TEA TEES TER TEE Zoom Bun Web QI el gt un 4 7 t 8 Se eS Fe le MAT ECU SCAN 39 95 149 95 0 1 0 5 sec Cu I max 980 03 11 97 12 50 E 270 Li A m eeu dn P a Pri E T MEME M er egt ra AT rele A AA Ne m fca ne Int ie PT qn Pi Pm aen nme e me e Pj Pre P ga artes rod y d Background Function
11. atter OPeaks 21242822 d 21101 1 5173 2 Thetal LOG OFF 2 men ae V E AStart A 5 Document Microsoft wordl Jade 6 dave Drexel eB 11 15AM 4 The following screen should then appear ia Read Pattern Files Today 1 Week 1 Month 1 Year 14 1J Read Add Hacia Browse Refresh Find Filter Import Frint Save Copy Help s C Pragram Files MID Jade 6 0 demofile mdi x x MDI Ascii Pattern Files mdi All EE z E HM E Red Paint Pigment Mixture lo E File Mame Scan ID Eragon Files DEMOOT MCI Demoli 37 1487 4 733 9 169 18 303 9 77 01 01 NE c3 MDI Jade 6 0 DEMOO2 MDI Demols 36 1451 25 1135 4 471 27 1402 0101 99 gt dermotile DEMOOS MDI Demola 24 1035 36 1451 0101 99 DEMOO4 MEI Demol 33 1151 41 1485 21 1152 19 629 0101 99 DEMOO5S MDI DemoQ5 5 566 41 1475 33 1151 34 183 11 467 0101 99 DEMOOB MDI Hed Paint Pigment Misture 01701499 DEMOO MCEI Demol 19 1130 10 173 31 5647 0101 99 DEMO08 MDI Demola Corundum 01701799 PeYN 34 4 OEMO0OS MCI Quartz Calcite Dolomite Corundum 05731701 QEMO10 MOI Quartz Calcite Dolomite Corundum 05731701 DENUT 1 MDI Quartz Calcite Dolomite Lorundum 05731701 DEMOS MDI Quartz Calcite Dolomite Corundum 05731701 DEMO13 MDI o1 01 99 3 M 23 Files Sorted on File Name 5 Demola 10 423 5 Go to lt C xrdfiles gt Head Pattern Files Today 1 Week 1 Month 1 Year 14
12. e PT nj EN n by ate Abt tet SARA ry ye rcs mne denne ee f Lr m UIDES az 8 st le 9 en Al Yy P ys y Intensity Counts j m Vergi fd heathy aba h poen if he Vis da y Abe qe uA ah T Mns nal Aet m ly PU pen y M ES vw WM elu A n d y Jat AN HL v Ais m Wn Ney EEEN ERE JE m pvr Neat sae aa i EE IT Z ENSE 80 a Se bran a E m Jn 1 1 12 OPeaks 2T 56321 d 1 6321 1 377 2 Theta v PKS DSP PDF PFT RPT PID szs KSI FIT 2TH ABC E Jade 6 dave Drexel c3 C Ba 11 47 AM hs m i Eis meg Lou oat 40 Raw Pattern AStart um eate M JADE USER Microsoft w 30 ill LOG OFF The following dialog box will appear di Fit Hemove Background Strip K alp Background Function and Point 5 ampling c COCHE Cubic Spline Wo Automatic Threshold Sigmas 6 0 W Strip K alpha2 K al a2 Ratio 2 U Offset of BG Curve from BG Dots 0 0 lt Area above the Background Curve 40 0 137 0 E 7 Default BG Fitting Save Reset Apply f Smp kapha Bemare File Edit Filters Analyze Identify PDF Options View Help Save Erase Macro Axes Hide Report Zoom Run Web 9 rhs lel a sb lt GA KALA Bs 94 73 1232 A Press F1 for Help C SCAN 39 95 149 95 0 1 0 5 sec Cu l max 380 03 11 97 12 50 RAIURO 0 a frere Letina tic let le Nie I nun vani nih tue IN Wd MAPS m Background Function and Point Sampl
13. eport gt window when finished Also click close on the peak search and labeling window when finished with that 17 Comparing your Peaks to the PDF Database In the Menu at the top of the screen find the menu item PDF and then click on lt Retrieval gt as shown below ig Jade 6 dave Drexel University Materials Engineering Monday Aug 12 2002 MATECU RAW MATECU File Edit Filters Analyze Identify Options View Help Save Erase Macro Axes Hide Report Zoom Run Web 9l E 2d ui Retrieval Shift F6 D m Jo Press F1 for Help c SI MATECU RAW w Me Chemistry Shift F A 1 0 5 sec Cu I max 769 03 11 97 12 50 g270 m 3 Stoichiometry Shift F8 Miscellaneous Shift F9 Unit Cell Data Shift F 11 Color Information Shift F12 Literature Ref Ctrl L Setup Shift F5 FIZ ICSD Access dF1 6049 2T 50 526 8 0 239 Intensity e ve 1 2773 21 74 178 B 0 253 d 1 2TTSI2T T4 1 T8 B 0 282 0894 2T 89 991 B 0 274 A A d 0 8085 2T2144 636 5 t d 0 8296 2T 136 389 8 0 157 d 0 9561 2T 107 340 8 0 168 ad WW n M ld eode x ere NAW AM er aedis lt Miele wA AM My Moin AM Sl Ad S Dis ius l vli Nall dil M un w Mh hia 40 50 50 7 8t jo 100 110 120 eT E prm Pattem ET Peaks JE 52 284 dal 7483 HE 746 EE Theta m LOG OFF AStart A ux BADE USER Microsoft w Je Jade 6 dave Drexel H 1 25PM After lt Retrieval gt is clicked
14. ing l v Automatic Threshold Sigmas e0 v Strip K alpha2 K al a2 Ratio 2 0 H Offset of BG Curve from BG Dots 0 0 r Area above the Background Curve ano 137 0 9647 12 4 4 1 Save zl Reset Strip K alpha2 zT Remove E F ji Intensity Counts Pt fv DB ORE Raw Pattern 0 Peaks 2T 79 906 d 1 1995 1 526 2Theta SAV T PID szs KSI FIT 2TH ABC RIA LOGsOFF start 7 ESI DY WADE USER Microsoft w E Jade 6 dave Drexel Univ C GB 11 494m If you are satisfied with the fit of this Background click on the button marked lt Strip Ka2 gt If you are not satisfied with the way the background has been automatically fitted to your pattern follow the next series of steps 14 BACKGROUND CORRECTIONS a Click on the pe editing button BE as shown below ig Jade 6 dave Drexel University Materials Engineering Monday Aug 12 2002 MATECU RAW MATECU BEES File Ee a POF Drum View Help I Save Ee Meee Axes Hide rg Zo mm eb 9 mele m 2 ui ela e22 9 c SI MATECU RAW w MArEcu SCAR 4 E Iranana Panay arainn dan eae ee nde Pen pine Thr twm HAAN A nnde fms PES Ae tere aho gto rfe cn lets P hr iSo men nr e PA nA jean im enne ee a inv en A Pr ei rodea tem vs yh L Click to Add ux Move Ctrl ovs Adjacent Dots as well R Click to Erase E Rs QI da 8 WE m kag C m Dy Background Curve Editing Cursor
15. j elm aule Ie A siio IMarEcURAw w MarTECU D 5 sec Cu I max 769 03 11 97 12 8 gw 20 wj Report Button mo j NNNM Aer d UE SEEE boss Qo 7 E L Click to Move or Add Ctrl Add Exactly R Click to Erase d 2 0839 2T243 385 B 0 218 dA x Search Labeling Report Peak Labeling and Scaling v Line Marker M FWHM J d Spacing Peak w 2 Theta w hkl Indices Intensity Peak Height RawCounts 7 Peak Ares 13 366 67 763 1000 1957 P N Asterisk Marker Scaling 50 526 1 8049 63 233 392 841 74178 1 2773 65 142 18 6 422 oe 4 088381 10894 64 127 166 409 Seve Reset 107384 0 9559 63 35 46 6 136389 082986 83 46 60 85 1 14 536 0 8085 84 58 S 19 d Spacing Unit E A eaeckreral 1 C femi P Close Print di 6049 2T 50 526 8 0 239 12773 2T 74 178 B 0 253 del 2773 2 1 74178 8 0 253 4 08941 89 U DUO32 imi VUY USU p UL 1 1 1 1 vu vn hda aaan an eta Mati Maa a kynda ak lu A rli dis TT iita ida NM m Derived Pattern E Peaks OTs 98 034 FE 0204 1 837 2 Theat LOG OFF Large etre oM Lh Ple SN mu vm Pa rr deut s I a AMA oo ANS re fit VEM APR remi oret A Start A S MADE USER Microsoft W Jade 6 dave Drexel Univ eB 12 43PM This is all of the information about your peaks this information can be printed or saved by using the menus at the top of the lt Peak Search Report gt window Click lt Close gt on the lt Peak Search R
16. k on the S M button once more and the computer will do a fresh search and match for your material Once the computer has finished the search and match it will display another window ICDDAICPDS PDF Retnevals Level 1 PDF Sets 1 51 127307353 x eod EE n Fe e ve eo m 8 se r r n 7 j a 154523 eos m A cu o 4 ssWTESeier e o Hee mese Sae a e a D s Copper gun 04 0836 Fm 3m 225 3 615 Quartz syn TE 46 1045 i P3221 154 4 91 W atkinsanite LuzPbBid 528 5 8 42 1375 P a 10 12 321 W attersite HgSCrb 45 1381 Lec 15 17 250 Wattevilleite Navla S04 el4H20 41 1360 W avellite AIS PO4 2 OHJs 5 25 0020 Femn B2 3 524 W awayandaite LalzMn4BzBelSS 46 1357 5 P c 13 15 58E Ww aulandite Ri CaA APAA Si 39 0367 A 2 EEI F i d This window will allow you to test the match file on the smaller window behind it After you have found the item you think is the best match for your material you can close that window and select it in the window beneath it fal Search Match L Display Subfiles to Search Inorganics Minerals Default Sea arch_ Match M x a o gu E nope ele elie alee TT El 10 0 WE xb LES 2 Exit PE A Ae A artz syn 502 l a a a sf mj l pod ae ee mi Wesselsite Cusrsida u 33 3 M 49 1813 0 18 1 0 000 n w aadruffite znln30 7 2H 20 33 3 V 47 1825 14 1 Widgiemoalthalite NISCO3IHOH 4 99 9 Y 12 1
17. s 3 00 Parabolic Filter Centroid Fit Intensity Cutoff 0 10 2 Quartic Filter Parabolic Fit l E E o 0 v Variable Filter Length Points Points to Average BG 7 4 v Screen out K alpha2 Peaks v Erase Existing Peak Listing Angular Range 40 0 fi 43 3 Intensity Counts j ad Aw Pea velie Mor deveol tnl APP s ANNA hind wey AVIRA Mattel fede ptis Mn Py Mh w Mw 40 50 60 70 80 g0 100 i 110 120 130 140 DerivedPattem 0 Peaks 2T 65740 d 14193 l 1 2 Theta SAV PKS DSP PDF PFT RPT PID szs KSI FIT 2TH ABC RIR LOG OFF dst A Xxx mp user Microsoft W 5 Jade 6 dave Drexel Univ GB 1218PM Click on the Apply button and the automatic peak search should begin The peaks located will be marked with dotted vertical lines in both the top and bottom windows as shown below Marked by RED arrows If the peaks are not where you feel they should be you can move them using the Peak Editing button as shown below The peaks can be moved using the left mouse button and by clicking and dragging the peaks to where you want them To remove a peak click on it using the right hand mouse button ral lal x File Edit Filters Analyze Identify PDF Options View Help Save Erase Macro Axes Hide Report Zoom Run Web 9l tz lel Au amp 2 gt Ai Bs 9 73 1282 9 Press F1 for Help is IMATECU RAW MATECU SCAN 33 35
18. t Pririt Save Copy Help Es C erdfilessD avid x no Pattern Files i Sc Al MI CPS MATE la EC C3 rdfiles MATECR ARAM 03 10 99 MATECU AAW MATE 037 11 97 MAT EW Raw 3 12 87 SIOZ Hwy 04721799 Thumbnail Ore Thumbnail AI 4 Files Sorted on File Name 5 amp v PES DSP PDF PFT RPT PID S25 Ksi FIT 2TH ABC RIA JE 4 9 After double clicking the pattern you want the software will open your pattern which should look like the following Materials Engin a lada C daon Annal iinn rsity Materi SEC gei EET e b dave Drexel University terials Ent File Edit Filters Analyze em OL a au 4 C s E i hs Mp e o ui veras Ve A rhet Phe Vigo s sering Monday Auc 12 2002 n neeri ng l jond av Aug 20602 PDF Options View Help ll Save Eiats HS pa Hide TU Zoom Run Web E TECU RAW MATECU BS Ha amp 731 232 9 Press F1 for Help h T alba ejl My j TO A owed us m T TT f Vitia nn M ET AMA v Np Nye Fh NM Mi IH i wou LN NEN 40 50 60 f 70 80 i 90 100 110 120 140 i Raw Pattem DPeaks 2T 70 001 d 1 3429 l 667 2 Theta LOG OFF AStart A tus MADE USER Microsoft w S Jade 6 dave Drexel 3 C eB 11 324 10 To Zoom into a specific region of your pattern simply place the mouse pointer in the top window Click and hold the left mouse button and drag a box over the area you want
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