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Guidance on the Safe Operation of Vacuum Insulated Storage

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1. A Member of The Linde Group General housekeeping issues 42722 For the continued safe operation of the tank it is imperative that the site operator tank user maintains a close watch on the installation to ensure that any incorrect conditions are acted upon and rectified as soon as possible It is recommended that a daily inspection is undertaken by a trained operative and a log of the conditions maintained This can be useful in any investigations in the future and enables trends to be highlighted in parameters such as pressure and usage As well as the physical condition of the tank the maintenance of the prescribed safety distances is a priority These vary with product and size of vessel and are detailed in the following technical data sheets As well as maintaining the separation distances it is imperative that access is maintained at all time to allow Delivery vehicle access Emergency Services vehicle access If access is restricted it may result in an aborted delivery and subsequent loss of supply 1 25 2010 Page 19 M s Nitrogen safety distances A Member of The Linde Group Liquid ts amp gl 9 h Buk Flannabk Continua Liquid Star Be 8 Pris Ducis Fama Wri hearts Stm hut 1e underground n le Smal stocks at pipalines Lend a has Safety distances for liquid nitrogen argon or carbon dioxide storage 1000 to 250 000 litres 1 25
2. Automatic Economisation 12 BOC A Member of The Linde Group Some vessels are designed with automatic economisation so that if the vessel pressure rises through low or intermittent use any potential boil off gas is fed into the process line in preference to liquid Typical economiser systems are shown on a following slide but in brief they use a regulator to sense the higher than normal pressure and allow this qas to be fed to the liquid outlet line until the gas pressure drops to normal Designs vary but in all cases this does result in some pipework being subjected to thermal expansion and contraction on each operation of the economiser e The high pressure gas can either be returned to the liquid line at ambient temperature hot piped or at low cryogenic temperatures cold piped depending on the design e Hot piped systems experience greater thermal expansion than cold piped systems e Large tanks have longer associated pipework which results in greater thermal expansion 1 25 2010 Page 13 Automatic Economisation 12 BOC A Member of The Linde Group The vast majority of BOC vessels do not have any automatic economiser systems and are not susceptible to fatique stresses from thermal cycling Within the BOC organisation of those vessels that do have the facility they are in the main small vessels in the cold piped configuration These have been confirmed as being acceptable for continued operation There are a small numbe
3. Vacuum insulated tanks are fitted with a device to prevent the outer jacket being pressurised 1n the event of a leak from the 1nner vessel or 1nterspace pipework The operation of this device may be visible and or audible as escaping gas from a port or connection on the outside of the tank and 1s an indication of a serious internal problem with the tank this must urgently be reported to the gas supplier Examples of vacuum protection devices This picture shows gas venting from a vacuum protection device General condition and security of the system is satisfactorv Check area 1s clear of debris general housekeeping and security is good and that delivery vehicle access is clear NB for liquid oxygen 1t 15 essential that the area around the 1nstallation 15 kept clear of all combustible material Vessel pressure and contents indication is functioning In case of doubt report to the operator s responsible person and gas supplier Safetv warning signs in place 7 Signage should be in good condition visible and kept up to date 1 25 2010 _ ii i Page 26
4. 2010 net liquid capacity Technical data Page 20 Oxygen safety distances 2977 A Member of The Linde Group lt E e laca won a m Pay Och Dui Safety distances for liquid oxygen storage 1000 to Safety distances far liquid oxygen storage 17 500 17 500 litres nett liquid capacity Technical data to 175 000 litres nett liquid capacity Technical data 1 25 2010 Page 21 Housekeeping daily checks 472 A Member of The Linde Group Visual inspection of the installation Confirm no mechanical damage is visible Noabnormal frosting ice patches on outer shell Novisual audible leaks from any part of the system Noobvious changes in the visual appearance such as excessive icing on the vaporiser If the system has a changeover facility between sets of vaporisers confirm this is operational Details on ice build up and operational mode are in the user manual for each system Pipework downstream of vaporisers should not be iced or frosted Fenced compound is free of any stored materials that are not part of the gas storage system especially flammable materials Adequate liquid level is available for the expected use Pressure is within normal operating tolerances check against vessel data plate value 1 25 2010 Page 22 Housekeeping daily checks Mi A Member of The L
5. 2010 Page 24 Summary HSE 111 leaflet 1 25 2010 Check system for damage Any sign of damage to the tank or installation shall be reported to the operators responsible person and gas supplier immediately Relief valves are not continually venting Relief valves may vent periodically under normal operating conditions However if they are venting continually this shall be reported to the operator s responsible person and gas supplier immediately Check for abnormal frosting on tank surface Under normal use frosting and ice will develop around pipes valves controls and vaporisers as shown 1n picture 1 opposite The operator should inspect the outer skin of the tank for any new or abnormal signs of frosting The frosting indicated 1n picture 2 opposite 15 an example of an aclvanced and serious interspace pipework failure Abnormal condensation that can t be ascribed to morning frost dew or weather conditions may appear at the first instance of a failure before heavy localised frosting develops If any abnormal frosting is found it shall immediately be reported to the gas supplier ME A Member of The Linde Group Typical tank relief valves Picture 1 Picture ee v x Examples of acceptable and abnormal icing Page 25 Summary HSE L11 leaflet 42722 A Member of The Linde Group Check gas is not venting from any part of the tank surface or connections to it
6. 27 A Member of The Linde Group oc Guidance on the Safe Operation of Vacuum Insulated Storage Tanks VIEs and VITs Applicable to the UK and Ireland April 2009 Contents BOC A Member of The Linde Group 1 Introduction and Background 2 Tank Design and Operation 3 Automatic Economisation 4 General Housekeeping Guidance 5 Daily Check Regime 1 25 2010 Page 2 2722 Introduction A Member of The Linde Group Following an incident in the UK where a cryogenic storage tank suffered a failure of the outer jacket it is imperative that users operators of Vacuum Insulated Storage tanks are fully briefed on indications of a potential problem so as to be able to take the appropriate action The failed component was part of the internal automatic economiser system Many users of such storage equipment lease their tanks from the gas supplier and the maintenance of the pressure system is managed by that gas company However for the gas company to respond efficiently it needs to be advised of any significant changes as soon as possible For users of BOC equipment the telephone number to report such incidents changes is 0800 222 888 This number is manned 24hrs day 365 days per year This presentation s aim is to provide a basic understanding of storage tank design clarification of the design feature economiser that caused the problem and a simple quide to allow end users to identify potential issu
7. es at an early stage 1 25 2010 Page3 Background ME A Member of The Linde Group The incident has been covered in a number of documents issued by the Enforcing Authority HSE the British Compressed Gases Association BCGA and the European Industrial Gases Association EIGA UK documentation can be found at e http www hse qov uk chemicals cryogenicalert htm e http www bcqa co uk publications L11 pdf Follow the links below to navigate this presentation Basic tank design Economiser circuitry Indications conditions that are evidence of an internal pipework leak General housekeeping issues 1 25 2010 Page 4 Basic vessel design MFZ A Member of The Linde Group Liquefied gases such as Nitrogen Argon and Oxygen are stored at temperatures down to 196 degrees Celsius Under normal ambient conditions of 15 degrees Celsius these products are gases but as part of the manufacturing and storage process they are cooled and liquefied To maintain the product at low temperatures the storage tanks are vacuum insulated An outer jacket is built around the inner pressure vessel The interspace is evacuated and is normally filled with perlite an inert mineral insulation material This gives a very efficient insulation barrier between the cold product and the outside environment The insulation is so efficient that whilst the inner vessel is at 190C the outer jacket should be at ambient temperature under normal operat
8. inde Group Check all valves are in the normal operating positions e This should include actuated valves if fitted f any electrical items form part of the system check e All panels on e There are alarms displaying on the panel interface units e The panels and wiring are in good condition Confirm the fencing and gates are in good condition and security levels are being maintained Confirm all the signs and warning notices are in place and clearly visible Confirm that any lighting to allow operation such as deliveries during hours of darkness is working and in good order Note After a delivery ensure that the blanking cap is in place on fill coupling and that there are no leaks This is best done approx one hour after delivery when any ice on valve seats will have thawed 1 25 2010 Page 23 Daily Checklist 272 BOC A Member of The Linde Group 4M Customer Engineering services Dailv Inspection Check List for Vacuum Insulated Storage Vessels Step Check 1 Check vessel outer shell for evidence of ice patches 2 Vessel contents are adequate for expected use 3 The vessel pressure gauge 1s indicating pressure and 1s within the normal operating range 4 If a Liquid Decant attachment is installed on the vessel e the filling hose coupling for wear and tear e the flash gas vent pipe for blockage or obstruction 5 The vaporisers for excessive ice build up Reference the Ice Build Up section of this manual for
9. ing conditions Pipework passes through this interspace to allow product to be filled and withdrawn and for pressure relief and instrumentation pipework to pass out This does allow some heat in leak Under normal operating conditions the tank pressure does not rise significantly This is due to Customer s demand lowering the liquid level which increases the gas space volume If the increase in volume is greater than the evaporation boil off rate then pressure does not rise At each fill any excess pressure can be reduced by the driver ensuring there is a sufficient flow of the new colder liquid through the top fill pipe 1 25 2010 5 Basic tank design 277 BOC A Member of The Linde Group INSULATION FILLER AND OVER PRESSURE VENT IN THE EVENT OF INTERNAL LEAK INSULATION FILLED VACUUM INTERSPACE OUTER p i JACKET TOP FILL VALVE FILLING POINT BOTTOM FILL VALVE VACUUM VALVE 1 25 2010 Page 6 Cut away photograph 42722 A Member of The Linde Group GM 32 113 e ko EUER VV deg Depending on the size of vessel this interspace is approx 150 300mm 1 25 2010 Page 7 27 A Member of The Linde Group Filling Introducing liquid into the top of the vessel condenses the gas in the top gas space and reduces the pressure E Les BOTTOM FILL VALVE TOP FILL VALVE 9 BOC Introducing liquid into the bottom of the
10. more information e For ambient vaporisers defrost as necessary 6 The pipework downstream of the vaporiser for signs of frosting 7 Control panels show Supply On 8 Actuated valve visual indicators white buttons show valves are in correct position 9 That there are no alarms conditions indicated on any control alarm panels 10 The complete system and all equipment items for general damage and deterioration 11 The complete system and all equipment items installation for leaks 12 The position of the vessel valves i e open or closed on the vessel are as per the P amp ID plate mounted on the vessel 13 maintenance isolation valves are open and all vent valves are closed 14 Any electrical water or steam supplies to the equipment are healthy 15 That all safety notices are in place legible and not obstructed from view 16 The vicinity of the installation for anything introduced since last inspection which could affect the safe operation of the system Consult BOC if doubt exists a 17 That the installation compound is kept clear at all times Make sure there is nothing Da ly Ch ec lc SL that will burn e g paper cardboard boxes rags weed growth 18 Ensure that the area adjacent to the vessel and the site access route for the BOC delivery tanker are kept clear 19 Ensure that any lighting provided 1s in good working order 20 The site security is suitable and sufficient Gates and fences in good order 1 25
11. r of vessels in operation in BOC that are large and hot piped The economiser circuits on these have already been isolated to prevent thermal stresses occurring 1 25 2010 Page 14 Piping arrangements for typical Hot and Cold arrangements 27222 BOC A Member of The Linde Group High thermal expansion in this leg Fanchon ecan Ru A i d th h ion ec ot piped gas passes through a pressure raising vaporiser before l going back into the interspace and so Is at ambient temperature Low thermal Expansion in this leg 224 gt lt 7 Nur iade ATE P m gt lt fe rT Regulator is 2 M after the vaporiser T Cold piped gas diverts back x to the interspace without passing ese through the vaporiser and so is cold a at Regulator is before 1 25 2010 the vaporiser ME A Member of The Linde Group Failure mode High stress here High thermal expansion in this PIPE can under certain design and operational conditions result in high stress on the WELD resulting in failure The leak that results if not attended to quickly can result in further pipework damage and significant leakage This in turn can embrittle the outer shell and cause premature failure as shown High thermal expansion 1 25 2010 Page 16 Indications conditions that would be visible in the event of an internal pipework leak A Member of The Linde G
12. rised and returned to the top gas space to maintain the vessel pressure 1 25 2010 Page 10 277 55 Vaporisation to convert the liquid to gas A Member of The Linde Group Liquid from the vessel is vaporised in the Process Vaporiser A pressure regulator downstream of the Process Vaporiser delivers the gas to customer requirements PROCESS REGULATION The type of process vaporiser is PROCESS dependent on VAPORISER the required flow rate the customer s site services the space available for installation 1 25 2010 Page 11 Over pressure protection i A Member of The Linde Group Under normal operation excess vessel pressure will not be an issue However if the product is not used for an extended period or there is an issue with the vacuum the heat in leak may cause the liquid to warm resulting in an increase in boil off and a pressure rise in the vessel The vessel is equipped with a duty and standby set of pressure relief devices The system has a pressure safety valve and a bursting disc on each side of the 3 way valve sized to cope with the boil off rates likely to be experienced under fault conditions The 3 way valve allows one set of devices to be on line and one set isolated This allows the relief devices to be maintained without interruption of supply The 3 way valve cannot be set to isolate both sides simultaneously PSVs 3 Way valve Bursting discs 1 25 2010 Page 12
13. roup Ice patches on the side of the outer Jacket If there is an internal leakage of liquid the ice patch will be significant in size There are occasions when ice patches are not indicative of a leak They may be due to voids in the perlite insulation or simple vacuum loss through poor seals However all ice patches should be reported to BOC or the tank owner for investigation and remedial action An ice patch combined with a plume of condensation from the tank interspace over the pressure relief port bursting disc is indicative of an internal leak Immediate action is required Contact BOC or the tank owner immediately the vessel will have to be depressurised and emptied 1 25 2010 Page 17 Comparison of visible conditions between internal MQ BOC leak and simple loss of vacuum A Member of The Linde Group Conditions that would indicate an internal leak Excessive icing over an extensive area of the outer Outer shell moist on dry days shell that appears suddenly and rapidly expands Continual problems with storage tank operating Venting of cold gas liquid from either the interspace pressure being high and pressure safety valves relief port or bursting disc lifting Small ice patches in localised area that do not spread quickly Algae growth on the outer shell on vessels in open areas algae may grow naturally on vessels in the shade under trees etc 1 25 2010 If in any doubt report it to BOC or the tank owner TE
14. vessel hydraulically increases the pressure By balancing the flow through the top and bottom fill valves a constant pressure can be maintained during filling and the B customer s process is not affected 1 25 2010 Page 8 Instrumentation 27 2 BOC A Member of The Linde Group When the level indicator approaches the full mark the driver opens the trycock valve Gas vents from the trycock until liquid reaches the spill level When liquid spills from the trycock the driver ceases the fill operation and closes the trycock Trycock Valve PRESSURE GAUGE Vents to low level TOP FILL VALVE Bypass LEVEL INDICATOR FILL VALVE The level indicator is of the differential pressure Type reading the difference in pressure between the top of the liquid and the bottom of the liquid A bypass valve is included to equalise the pressures and simulate a zero reading i 1 25 2010 Page 9 Pressure raising circuit 472 A Member of The Linde Group If the customer use is large the drop in liquid level may result in a fall in pressure in the vessel The pressure raising circuit is design to maintain the set operating pressure PRESSURE RAISING ie REGULATOR The pressure is controlled automatically by the Pressure Raising Regulator which can be pre set to the Customer s required pressure PRESSURE GAUGE PRESSURE RAISING VAPORISER 7 Liquid is taken from the vessel vapo

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