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1414 WinSpectral Manual - Faculté de médecine de l`université d

1. CERTIFICATE This is to certify that this instrument and its components and subunits have been tested according to the Wallac Instrument Quality Control plan and that it fulfils the specified quality and performance values Details ofthis plan can be obtained from your local Wallac representative Date MAL bh APES 7 Pa P eem Signature k 2 On behalf of fie Quality Control Department 1 1 al nn m m le pum ie ees TA ils U TL n Te a Me EI Y R i a AA nn AA a r en A 1086 1430 September 1995 Warning This equipment must be installed and used in accordance with the manufacturer s recommendations Installation must be performed by properly trained and authorised personnel Failure to follow these instructions may invalidate your warranty and or impair the safe functioning of your equipment Please contact your local Wallac representative for installation Zk EG2G WALLAC Installation Environment Normal clean laboratory conditions usually provide a satistactory operational environment but the following points should be taken into consideration Ideally a separate room should be provided for your Wallac 1414 WinSpectral counter as this allows the best control over the immediate environment Ventila tion should be adequate for all conditions of use the temperature should be reasonably constant at about 22 C relative humidity should not be excessive and direct sunlight should
2. n Fig 1409 1410 1411 13 ID Unit 10855818 96 10 10 FOR PART NUMBER 10855818 ID UNIT 10355819 950110 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 10555375 LABEL SET CONNECTOR LABEL FAPER CAL 177 i 1 10855668 P C ASSEMBLY RAMCODE READER RAM 10355667 10 1 10355734 ID BODY FE PLATE S 1 5 NTL 5 20 3 1 10455732 FIECE AL PLATE S 5 NTL 5 30 4 10455733 SUPPORT PIECE AL 15 20 NTL 5 40 5 1 10455725 LOWERPIECE AL NTL 5 50 5 1 10455724 UFFERFIECE AL NTL 5 60 7 4 11290024 BUSHING D3 4 6 7 5 843 070 70 E 2 15455731 GUIDE AL NTL 5 80 9 4 11252033 RIVET 3 12 AZ 90 10 1 19455726 SLEDGE POM BLACK NTL 5 100 11 1 10455728 PLATE AL NTL 5 116 12 1 10455750 FILL PIECE 2 5 950 NTL 5 120 13 1 10354288 GOGGED BELT WHEEL GRILON W 5239 1297 130 14 2 10455727 AXLE D3 NTL 5 140 15 1 10553597 P C BOARD 1 6MM 2 P EP LK RRA 1205 1470 150 16 3 11290019 BUSHING D3i 4 6 5 5 83 050 160 18 0 015 111560065 SHRINKABLE TUBING 1 4 CLEAR 201 150 19 1 11350048 COGGED BELT SYNCHROFLEX 6 T2 5 200 1520 20 1 11250008 WASHER 3 2 7 0 5 FE YELLOWPASS 200 21 4 11250008 WASHER 4 3 9 0 8 FE YELLOWPASS 210 33 1 10455899 BASEPIECE FE PLATE S 3 NTLS 175 23 1 11271016 SCREW M 3 4 FE YELLOWPASS 230 24 3 11271018 SCREW M 3 6 FE YELLOWPASS 240 25 1 11271023 SCREW K 3 14 FE YELLOWPASS 250 26 1 11271026 SCREW M 3 18 FE YELLOWPASS 260 27 2 11271034 SCREW M 435 FE YELLOWPASS 270 28 4 11271036 SCREW M 4 10 FE YELLOWPASS 280 29 4 11271075 SCREW M 3 6
3. MS Dz20 SOLUPOLYETHEN AL PLATE S 2 FE PLATE D 2 AL FLATE 5 2 3 5 2 P 00 P500 250KB AL SQUARE BAR 5 2x8 2 AL 99 5 S l AL PLATE S 0 5 O SMM AL PLATE 8 2 FE PLATE S 1 POM ROD 40 MU 8 0 1 4 3 9 0 8 FE YELLOWPASS 5 3 10 1 FE YELLOWPASS 6 4 18 1 6 FE ZINKED 3 20 ST 1 1 2 M 3 4 FE YELLOWPASS M 4 5 FE YELLOWPASS M M M 5 12 FE YELLOWPASS 5 20 FE YELLOWPASS 6 30 FE YELLOWPASS M6 12 FE YELLOWPASS M6 25 YELLOWPASS M4 8 FE BLACKFASS 10260207 DCD 10355455 DIC 10354883 DIE 10354603 DPA 10353503 HPS 10354022 1414 l414 1414 1414 1414 NTLS 1415 NTL5 1470 NTLS 1415 1415 1415 1415 NTLS NTLS NTL 5 NTL 5 NTL 5 NTLS 1414 FD1137H 1414 NTL5 NTL5 NTL5 NTL5 NTL5 EDS 0 3 TAP D BS 33 5 3 15 1 6 FE YELLOWPASS AL PLATE S 3 M 4 10 FE YELLOWPASS M4 FE YELLOWPASS FE PLATE 5 1 Mo 12 FE YELLOWPASS HV ALO 08 AL 5 0 08 FE PLATE T 1 M 3 10 FE YELLOWPASS SOLUPOLYETHEN S 20 WHITE SELF ADHESIVE L FE PLATE T 1 FE PLATE T 1 C 2 9 6 5 FE YELLOWPASS FE S 1 FE 5 1 FE PLATE 31 LEAD CAST CAST LEAD CAST LEAD LEAD 4 1 12 1 FE ZINKED M 4 8 FE YELLOWPASS C 4 2 9 5 FE YELLOWPASS NTL5 NTLS 1410 WARNING 1410 CR 1410 PROGRAM CR L35C 5 NTL 5 NOTE LSC LEC 10255679 1409 11 15 1409 11 15 1415 1415 1415 1415 1282 1480 45 55 55 75 85 95 146 130 135 145 147 175 205 195 135 210 230 240 250
4. How does PSA work The PSA integrates the delayed tail and the prompt peak light pulse from a sample producing both types of radiation If the ratio of the delayed to prompt com ponent exceeds the preset ratio the pulse is directed into the long pulse or alpha spectrum If the ratio does not exceed the preset ratio the pulse is directed into the short pulse or beta spectrum Very low background count rates are achieved for alpha particles since most of the LS background is composed of short pulses The above mentioned preset ratio is controlled by the user with the PSA level whose range is from 0 to 255 in steps of 1 The higher the PSA level is set the more counts will be directed into the long pulse spectrum At PSA level 255 all counts are directed into the long pulse spectrum and at 0 all counts go Into the short pulse spectrum An optimum value for the best alpha beta separation can be found somewhere be tween these two extremes as explained tn the next paragraph PSA levels higher than the optimum reduce beta counting efficiency and and background leading often to better figures merit Lower PSA leveis than optimum do same for alpha counts Determining the PSA level Cocktails produce different pulse lengths HiSafe cocktails show relatively slow pulses while xylene and toluene based cocktails are fast The PSA option al lows the optimum PSA level to be found to match the cocktatl speed This is done by stepping over
5. mill of proteculed E TENE ar AAA OB EFE DE e FR S pe AO DO PA E um arua Haye k k 7 n F gt r a r a o x zd az ERE N O hot he compents dr ere amp gi vu 5l esessto wiTH THE ALO OF A TOOL When this instrument is no longer in use the Eu 152 standard capsule must be removed and sem to the appropriate radiation safety authorities or to the Insitument manufacturer for safe digosal III ME m EMEN ny EEE FE TL n n 5 T c D oO E e 2 c NN O This docuamer Miisu and 822182 RADIOACTIVE MATERIAL Des que cet instrument n est plus employ la source standard de Eu 152 doit tre enlev e et envoyee aux autorit s de radioprotection ou au Fabricant de l instrument pour limination ait M LEAD SHIELD Kun tama latte poistetaan lopuilisests kayt sta on u 152 standardi kapseli irroctettava ja towmitettava satenlyturvadlisuusviranomaisille tai laitteen valmistajalle SENSOR AAA Y VA A CAUTION RADIOACTIVE MATERIAL Pras 39 ee en iacit O SATEILYVAARA prul fue win T THE ABOVE LABELS ARE PERMANENTLY ATTACHED TO LEAD SHIELD THE EXTERIOR REAR PLATE OF THE INSTRUMENT THICKNESS 40mm TUBE PA N nee Taygigr See WIRE HR ow dL lt A er dnt
6. 1 10561514 LABEL 11570078 BRADY CE LABEL 429 1 11310040 CLAMP ACCOZ A gt 46 gt 11310037 CLAMP FCC A CS 387 1 1215 111 UNO STANDARDS SET 20ML VIALS 3H 14C BACK 1215 111 1000 1 1224 513 SOFTWARE PACKAGE 1414 WINSPECTRAL 1224 513 1010 1 1414 931 INSTRUMENT MANUAL FOR 1414 001 1414 931 1020 1 10990045 OC CERTIFICATE 10930045 10350 1 l 10560804 BODY ASSEMBLY 1414 10160805 10 2 1 10855818 ID UNIT 1410 10355853 11 3 1 10255338 SAMPLE CHANGER 1410 10255339 15 1 10854849 MEASURING UNIT 1410 10354850 ao 5 1 10859369 P C ASSEMBLY HV DIVIDER UNIT RFA19359368 10355373 35 6 i 10860806 TOP COVER ASSEMBLY 1414 10260807 45 n 1 10856466 F C ASSEMBLY MICRO COMPUTER DCD 10356465 55 1 10854884 F C ASSEMBLY L O BOARD DIC 103543853 65 8 1 10854606 P C ASSEMBLY MCA DIE 10354603 75 10 1 10853316 F C ASSEMBLY POWER SUPPLY DPA 10353503 85 11 10854021 P C ABSEMBLY MOTOR CONTROL BOARD HPS 10354072 35 12 1 10360743 FRONT PANEL RIGHT 1414 146 13 1 10361369 BOX ASSEMBLY 1414 130 14 1 10360774 SIDE BOX RIGHT FE PLATE 5 1 0 1414 135 15 1 10360773 SIDE BOX LEFT FE PLATE S 1 0 1414 145 16 1 L03650752 FRONT PLATE LEFT 1414 147 17 2 10455328 CAM D25 NTL5 175 18 2 10458890 GUIDE PLATE FE PLATE 2 3 1415 205 19 1 10455330 BUSHING D12 NTL5 1470 195 20 3 10455329 PLATE FE PLATE 5 3 NTL5 185 21 22 23 24 25 26 27 28 29 30 32 33 33 35 36 37 38 49 40 41 42 43 44 45 46 47 48 49 30 51 52 53 5d 55 56 57 55 60 61 62 63
7. 1409 1410 1411 19 Support 2 Assembly 10455079 O E m y E b 2 o o D OAS x RE ie i DO 0 e co 0 er er co eo lt z m N Oo Tr 5 M 29 Fig 1409 1410 1411 20 Plate Assembly R 10855051 96 10 10 FOR PART NUMBER 10855051 PLATE ASSEMBLY R 10455052 940929 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 2 10855235 P C ASSEMBLY SENSOR BOARD RSV 10455234 10 2 1 10355053 GUIDE PLATE RIGHT AL PLATE S 2 NTLS 20 3 2 10455054 COVER PLATE FE PLATE 5 2 NTLS 30 4 3 10455055 PLATE FE PLATE 551 5 NTLS 40 5 3 11250002 WASHER A4 3 YELLOWPASS 50 6 4 11274002 SCREW M3 6 FE YELLOWPASS 60 3 11274006 SCREW M4 10 FE YELLOWPASS 70 56 Fig 1409 1410 1411 20 Plate Assembly R 10455052 10 45 5052 Piir 880915 745 Tark 880915 Hyv 88095 g 57 Fig 1409 1410 1411 21 Plate Assembly L 10855056 96 10 10 FOR PART NUMBER 10855056 PLATE ASSEMBLY L 10455057 940929 ITEM NO QTY ORDER NO NAME TYPE MANUF iNF LINE 1 2 10855235 P C ASSEMBLY SENSOR BOARD RSV 10455234 10 2 i 10355058 GUIDE PLATE LEFT AL PLATE 5 2 NTL5 20 3 1 10455054 COVER PLATE FE PLATE 8 2 NTLS 30 d 3 10455055 PLATE FE PLATE S 1 5 NTLS 40 5 3 11250002 WASHER A4 3 YELLOWPASS 50 6 4 11274002 SCREW M3 6 FE YELLOWPASS 60 7 3 11274006 SCREW M4 10 FE YELLOWPASS 70 8 1 10455888 HOLDER FE PLATE 2 NTLS 31 98 10455057 Fig 1409 1410 1411 21 Plate Assembly L 222 16088 MAH El6088 H
8. 5 1 10356031 SHELF 2 FE PLATE S 0 5 BLACK NTL5 30 5 2 10456032 SHELF 3 FE PLATE S 2 5 NTLS 50 7 1 10456033 HANDLE 1 FE PLATE 5 0 5 NTL gt 70 8 1 10456034 HANDLE 2 FE PLATE 5 0 5 NTLS 80 3 4 10456035 BRACKET FE FLATE 5 2 NTL5 20 10 10456036 SUFPORTING RAIL FE PLATE 3 2 NTLS 100 11 4 10456037 SUPPORT PLATE STAINLESS PLATE 5 0 8 NTLS 110 12 d 10456038 FIN STATHLES ROUND BAR D5 NTL5 120 13 1 10355039 END FLATE RIGHT 12MM NTLS 130 l4 1 10356040 END PLATE LEFT 12MM NTLS 140 15 1 10356041 SEPARATION WALL 12MM NTL5 150 16 1 10456042 DECK 18 MM NTL5 160 17 1 10456043 BOTTOM PLATE 15MM NTL5 170 18 1 10356044 CHEST OF DRAWERS NTL5 180 19 1 10356045 VERTICAL ROD NTL gt 190 20 1 10456047 SWINGING ARM NTLS 200 21 2 10456048 BUSHING FE AUTOM STEEL D22 NTLS 210 22 1 10456049 PLATE ASSEMBLY NTLS 220 23 1 10356052 BOTTOM PLATE AL PLATE 5 3 NTLS 230 24 3 10456023 PLATE FE PLATE 3 3 NTLS 240 25 3 10456054 NUT 6K19 NTL5 250 26 4 11350085 WHEEL ESL J 75ND K 260 27 2 113100431 SLIDE BS 230E6500 270 28 12 11271093 SCREW M4 6 FE YELLOWFASS 280 29 2 11274034 SCREW M6 30 FE YELLOWPASS 290 30 12 11274038 SCREW MS 16 FE YELLOWPASS 300 il 4 11274023 SCREW M8 30 FE YELLOWPASS 310 32 4 11274024 SCREW MB 40 FE YELLOWFASS 320 33 3 11277010 SCREW M8 35 FE YELLOWPASS SFS 2458 iil i4 56 11276031 SCREW 3 5 12 YELLOWPASS HECO FIX 340 i5 B 11278003 NUT M FE YELLOWNPASS 350 38 4 11278011 NUT MB FE YELLOWPASS 360 37 11260017 RIVETED NUT M5 1 0 2 0 MS 338581RIV
9. Bench top model 1 6 Bi directional conveyor 1 2 C Cables 6 5 Printer to PC 5 4 Types 5 3 Calculation methods 3 1 Chemiluminescence Calculation 3 4 Chemistrip 1 12 Problem of chemiluminescence 1 12 Random comcidences 1 12 Single photon event 1 12 Solution to chemiluminescence 1 12 Chemistrip 1 12 Chi square for repeat replicates 3 5 Cleaning 6 5 Coincidence resolution time 6 1 Colour index 3 3 Error 3 3 Colour quench index 3 2 Connections 6 1 Count rate 3 Error 3 1 Counterweight See Elevator Counting efficiency 3 3 Counting time See Background CPM Counting 1 7 Monitor 1 7 D Dead time correction 6 2 Decay See Radioactive decay Detector stabilization ACSS 1 4 Digital Overlay Technique See DOT DPM Dimensions 6 1 Disk drives Internal 1 6 Program disk drive 1 6 DOT DPM 8 E Efficiency 6 2 Electronics 1 6 Elevator 1 4 Endpoint of spectrum See External standard Enhancement accuracy 1 9 Error in Activity 3 1 Colour index 3 3 Count rate 3 1 Spectrum quench index 3 4 Total quench index 3 3 Eu 152 See External standard Europium See External standard External standard 1 5 F Fine tun ng Lock I 14 FIP See Fractite Integral Presentation Floor Stand 1 6 Floor standing model 1 6 Fractile Integral presentation 3 2 8 Index 8 Index Frequency distribution See Statistical analys s G Guard detector H Half life Correction 1 12 Half life correction 3 4 Hardware 6 2 Humi
10. OR k 8 bo Bo o S o b 8 8 zu 5 4 nO 1 amp 9 Serialno sseessaeosvstesvetoesetesvesosesseoceveceseseveteecooceeoevesoos Sample capacity PHOTOMULTIPLIER TUBE INFORMATION position size type serial no Ao ENCIH R331 L23 CIC3 4 d 6 3 bot oh bot k b dy d d b FF Zu o Wow S 5 F F 9 b bo b F 9 9 boh 9 Fx ICH Ca u d B5B T d 4 Zu FE TT o ROW RO 42 9 Bo ea 4 5 amp c Cala ir A SAA e RI L 10 BASSO de dy oh bb f 8 o 5 B hb 5B P ou 4 Pod Bbo o k 8 8 8 8 amp od amp k amp ob k PE 9 o4 Ca ER 5 LINCS 110 EO INIA Sts 3 3 od k o o b amp PE A f o o EE SE SE SE T Gu ob w FF s bod k 4 oh b b k tv b F 8 ORB 8 h SE SE EE DO ws d ob boh 5 5 G t titt 4 y amp k amp eE o o5 9 YT 9 8 5 OP ok F 4 Boh amp 4 W
11. tails of parameter setting Sample quality monitor Sample inhomogeneity One problem in liquid scintillation counting is inho mogeneity of the mixture composed of the sample be ing analysed and the liquid scintillation cocktail If sample and cocktail are not adequately mixed some of the beta particles will be absorbed 1n the sample phase and thus not reach the scintillation liquid phase This will appear as a reduced counting efficiency for the sample This happens because the external standard spectrum which is produced by the Compton electrons resulting from the gamma radiation from the external standard is not affected by the inhomogeneity of the sample and cocktail mixture This is because the Compton elec trons are generated throughout the whole volume and thus will produce scintillations effectively The count ing efficiency might even be improved for the external standard as the quenching agents are in the sample phase Thus the counting efficiency obtained from the meas urement of the external standard is not correct if the sample and cocktail mixture is two phased The sample and liquid scintillator mixture can be ho mogeneous when the counting Starts but as time goes the last samples can be inhomogeneous if the samples are close to the sample holding capacity of the cock tail When using an emulsifying cocktail the sample is suspended in drops micelles in the cocktail The micelles are small compared to the ra
12. 1 X an array or row vector comprising the count rates x y number of counts z fractite for total quench index p G standard error at 68 3 confidence limit stand ard deviation X z reduced chi square 4 Quality control information Qc Contents QC Contents Quality Control Certificate nennen enssnnsseneneinnenennn 1099 0045 Final Test Data Sheet RE 1096 0594 Electrical Safety routine test report n nsnsi 1096 1059 Safety evaluation of the Eu 152 source and ext std transport system 1099 0196 Quality control report 1096 1060 External standard transport system l u n sun 1036 1092 Certificate for Eu 152 source AAA 1095 7794 Certificate for unquenched LSC standards nsn E390 0171 PROTOCOL 1 MAPPING DATE 2 1998 02 11 TIME 15 26 ID POLSSOS0 Quench Standardization Waliac 1400 DSA Counting mode Quernch index Isotope s HS Frotocol name Counting time Activity DFM 2 sigma Minimum cpm Vial type Liquid system Advanced modes Halflife zerotime Zerotime of Ha Output to Frinter ver 2 50 B W 41401859 ak eH AH DEM SF Hs ghee 45 y MAFFING G00 194500 O 01 Checking time Clear 10 ah ww Eh EX sit on Au xm ME En LOPS SOT POT Xylene Halflife 10200500 CTIME CPI CPMer 1 EFF 1 SPE SOFE E Additions to Frint
13. 11252007 RIVET 3 2 6 1 MONELL TLF D BS424 135 951121 56 0 105 11240174 RF GASKET SPRING BeCu 28MM 6MM 97 438 02 196 951121 Fig 1409 1410 1411 02 Body Assembly 10154917 18 tob tTa na um Herz 10 15 4917 D Piirt 881201 Ws Tork B amp 1201 Hyu 581201 ze Fig 1409 1410 1411 03 Sample Conveyor 10855197 96 10 10 FOR PART NUMBER 10855197 SAMPLE CONVEYOR 10155198 960610 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 10555603 LABEL SET CONNECTOR LABEL CATO 520 1 i 10855064 MOTOR UNIT 1 10355065 10 z 1 10855070 MOTOR UNIT 2 10355071 O 3 1 10855074 SUPPORT i ASSEMBLY 10455075 30 d 1 10855078 SUPPORT 2 ASSEMBLY 10455079 40 5 1 1085505 PLATE ASSEMBLY E 10455052 5D amp 1 10855056 PLATE ASSEMBLY L 10455057 50 7 1 10255199 CONVEYOR PLATE AL PLATE S 5 NTLS 8 4 10455200 PLATE 1 AL PLATE 0 5 NTLS 50 Q 1 10455201 PLATE 2 AL PLATE S 0 5 NTLS su 10 1 10455202 PLATE 3 AL PLATE 520 5 NTLS 100 11 10 10455203 WASHER AL PLATE 5 4 NTLS 110 12 1 10355204 SUPPORT ASSEMBLY NTLS bed 13 1 10357958 SUPPORT ASSEMBLY S 6 8 NTLS 230 14 2 10358091 SUPPORT BAR AL 3115 1410 140 i5 2 103580827 PLATE Sol 1410 150 16 4 10455209 BUSHING 6K10 NTLS 150 17 1 10355210 FLATE AL EM NTL5 i70 18 2 10355211 GUIDE 1 POM PLATE BLACK 8225 NTL5 180 19 2 10355212 GUIDE 2 POM PLATE BLACK 5 3 NTLS 190 20 2 10455213 BRACKET ASSEMBLY NTLS 200 21 2 10455316 BUSHING MS 6K10 NTLS 210 22 2 10447733 SPRING Dir 75 1266 1250 148
14. 11276032 11550112 WASHER LOCKRING SCREW SCREW SCREW SCREW SCREW LABEL SCREW INSULATING TAPE 12 5 3 10 1 FE YELLOWPASS 16 1 M 3 4 FE YELLOWPASS M 5 12 FE YELLOWPASS M6 12 FE YELLOWPASS M6 16 ST YELLOWPASS M4 8 FE BLACKPASS WARNING STICK PVC ALUM EURGPIUM 152 C 3 5 6 5 YELLOWPASS S 1 2 1 4 CE 015 425 465 495 515 545 546 565 595 650 660 960115 950324 960115 960115 950324 960115 950115 950216 960311 960311 10155600 Fig 1409 1410 1411 01 LSC Assembly 14 S695 213 AMI THA 263 Braten Sa ter 247 310605 Tsa for 264 docala Ta Kor Tas aes as 85 ES iere dg SupD21344 215 AR Ra M inr PR Mk ZA vr 566521 AL NOTE U5ED ONLY 141 KAYTOSSA VAIN 14tS X 4 amp LFAD OPTION 10 15 5600 B LSC 1410 Pirt 881220 Gas Tark 881720 Ma Hyw 881220 4 Fig 1409 1410 1411 02 Body Assembly 10854916 85 10 10 FOR PART NUMBER 10854916 BODY ASSEMBLY 10154917 960503 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 12 11310037 CLAMP FOC A CB 320 7 11310038 CLAMP ACCHB A 330 8 11310046 CLAMP ACCE2Z A 340 1 10555601 LABEL SET F31 370 1 10555430 LABEL SET CA24 380 1 1 10254913 BODY NTL5 19 2 1 15160738 BOTTOM PLATE ASS 1414 2G 3 1 10354921 COVER FLATE RIGHT AL PLATE S 2 5 NTLS ac 4 i 10354222 COVER PLATE LEFT Ab PLATE 5 2 5 NILO 40 2 1 10354923 BOX AL PLATE 5 1 5 NTL5 50 6 1 103545
15. 140 B 11252019 RIVET 2 475 1 AL TAP D BS 33 150 10155600 3d 1 10555665 LABEL AL 820 5 NTLS 30 10155600 75 1 11570061 LABEL WALLAC 52422 165TICKER 35 10255462 23 1 10355660 COVER PLATE POLYCARB 0 375 20 PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 10857646 LSC 1410 001 920502 ITEM NO QTY ORDER NO HAME TYPE MANUF INF LINE DATE 2 10855393 PREAMPLIFIER UNIT 1410 10455334 0 9410396 1 10854735 F C ASSEMBLY COINCIDENCE BOARD LAC 10354734 90 911030 1 10855551 P C ASSEMBLY SAMPLE amp HOLD lCH LAD 10354773 100 911030 LSC Model 1411 001 10857648 96 10 10 FOR PART NUMBER 10857649 LSG 1441 091 931203 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 10446545 FOOT PAG BLACK 30 GLAS 1215 1470 10 1 10857646 LSC ASS 1409 1410 1411 10155600 40 1 10861091 STD CAPSULE 10361101 50 1 10855272 EXTERNAL STANDARD 10255273 60 1 10856730 BCH EXPANSION KIT DCD 10356465 10 1 10857653 P C ASSEMBLY SW KEY MODULE BOARD RJG 10457652 310 1 10857618 PROGRAM PACKAGE MAIN PR 1409 31 LSC WALLAC 1400 DSA 122 i 10857810 PROGRAM PACKAGE COMM PROTOCOLS 4409 44 1403 11 15 i30 i 1411 932 INSTRUMENT MANUAL FOR 14089 1411 1411 932 148 i 10990045 OC CERTIFICATE 10990045 145 1 10555672 LABEL AL 99 5 5 1 NTLS 150 1 10494512 WARNING PLATE AL PLATE 160 8 11252019 RIVET 2 475 1 AL TAP D BS 33 i70 10155600 34 1 10557602 LABEL AL 5 0 5 NTLS 30 10255462 23 1 10357616 COVER PLATE POLYCARB O 375 1411 20 10255462 37 i 11570063 LABEL
16. 188 308 446 SBE 668 9808 SHH 08 INTEGRC 584 657 9484 063 CPM Bi 4 195 CPM BUNCH 4 FM 3894 68 DPM FM tin3 Bl 46385 E 95 84 x 1096 0594 AN SU EGG COMPANY FINAL TEST DATA SHEET FTDS INSTRUMENT SIN 740181 HV GENERATOR PMT VOLTAGE EPM A OUTPUT calculated DVM input impedance 10 MQ PERFORMANCE WITH SUPPLIED STANDARDS HARTA LRC VALUE A CONV STEPS ua Product Description The 1215 111 Liquid Scintillation Standards set consists of two activity standards and one blank standard The activity standards are precisely calibrated sealed unquenched samples of carbon 14 labelled 1 14C stearic acid and tritium labelled 7 n 3H cholesterol in 10 ml of xylene based scintillation solution The labelled compounds are produced by DuPont NEN Belgium and Amersham International UK The unquenched blank standard is a sample of 10 ml of xylene based scintillation solution The standards are supplied in 20 ml capacity low potassium content Wheaton vials These are flame sealed and secured with white silicon mastic and an aluminum cap Standards are deoxygenated with pure nitrogen before ling Activity Calibration The tritium standards are calibrated against reference standards of tritium labelled toluene by the National Institute of Standards and Technology NIST Standard Reference Material SRM No 4947C the estimated accuracy of which was 1 2 The Carbon 14
17. 265 275 285 295 305 306 148 425 143 415 423 421 375 385 395 403 430 431 435 445 455 465 475 485 495 905 915 525 535 545 555 565 434 326 510 585 327 511 417 418 419 404 514 409 413 i28 329 276 119 400 401 254 253 251 252 255 440 513 570 104 2 11274010 SCREW M 4 25 FE YELLOWPASS 512 105 2 11310047 MUT M4 1 7 2 7 590 106 4 11290015 BOD D4 8 4 4 14 08 040 426 115 1 10860713 DUMMY PLUG 1414 1414 10460712 126 116 1 10460762 PLATE RIGHT FE PLATE S 2 0 1414 150 117 i 10460761 PLATE LEFT FE PLATE 5 2 0 1414 151 118 2 11250006 WASHER 3 2 7 0 5 FE YELLOWPASS 432 119 6 11274002 SCREW M 3 6 FE YELLOWPASS 566 122 1 10460964 SHELTER POM PLATE 5 8 BLACK NTL 5 402 123 2 11271053 SCREW M4 8 FE YELLOWPASS 490 124 2 11274156 SCREW M6 16 ST YELLOWPASS 530 126 2 10561339 LABEL ST POLYESTER 11570076 MACH LABEL 1414 002 411 127 2 10461378 LEAD SHIELD LEAD 99 9 1414 002 256 128 2 10361379 SUPPORT FE PLATE 2 1414 002 257 141 1 10861410 P C ASSEMBLY CONNECTION BOARD RGE 10461408 114 142 2 10461276 HOLDER FE PLATE S l NICKELIZED 350 143 1 10461414 SUPPORT 1 FE PLATE S 1 0 1414 340 144 2 11240173 RF GASKET 6 35x6 35 MONEL GLUE 01 0901 6603 600 145 2 300 11240162 RF GASKET 3 2X4 8 MONEL 01 0901 6601 610 146 2 10461480 PLATE 1414 360 147 6 11276022 SCREW C 2 9 9 5 FE YELLOWPASS 580 148 1 10557386 LABEL PVC FASKAL 400 T 0 1 1410 RESET 428 149 1 10461613 HOLDER FE PLATE T 1 1409
18. 355 10260807 43 1 10358879 SHIELD ASSEMBLY FE PLATE LEAD CAST 1415 270 10260807 23 1 10361030 COVER PLATE 2 POLYCARB 0 375 1414 410 10260807 37 1 11570061 LABEL WALLAC 52X22 16STICKER 424 10260807 42 4 11250039 WASHER 4 3 12 1 FE ZINKED 441 10260807 41 2 11274006 SCREW M 4 10 FE YELLOWPASS 486 10250807 48 2 11276025 SCREW C 3 9 9 5 FE 567 10355819 17 1 10355762 ED SHIELD FE PLATE S 1 NTL 5 405 10355818 43 1 10457903 PLATE ST PLATE T 1 5 1410 406 10355819 44 1 10357902 SUPPORT RST T 0 8 1410 407 w24 1 10861346 FLAT CABLE 405 405 FC207 10461300 117 W32 1 10861411 WIRING ASS CA210 115 PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 10861383 ALPHA BETA 1414 001 10160809 960404 ITEM NO ary ORDERNO NAME TYPE MANUF INF LINE DATE W26 1 10855592 FLAT CABLE 508 508 FC35 10455666 118 951128 147 11276022 SCREW C 2 9 9 5 FE YELLOWPASS 580 960403 1 1414 102 PC PROGRAM PACKAGE PSA SPECT ANALYS PRG 1414 102 1015 960402 i 1414 931 INSTRUMENT MANUAL FOR 1414 001 1414 931 1020 951201 101 1414 Guardian 1414 003 96 10 10 FOR PART NUMBER 1414 03 GUARDIAN 1474 003 960620 QTY ORDER NO NAME TYPE MANUF INF LINE l 10861384 GUARDIAN 1414 003 10160809 10 1 1410 405 SAMPLE TRAY FOR SAMPLE RACKS 1410 405 110 1 1410 401 RACKS 20 ML PACKASE OF 10 RACKS 1410 401 120 1 1409 411 ID KIT 1409 411 130 0 500 1200 437 OPTIPHASE HISAFE 3 2X5 L 1200 437 140 1 1414 160 MONITOR STAND 600 MM 230 MM 150 1 10859610 PACKAGE 1415 104596
19. 5 11271045 SCREW M3 5 FE YELLOWPASS 110 li 11271021 SCREW M3710 FE YELLOWPASS 120 12 3 11278002 NUT M3 FE YELLOWPASS 130 13 1 11310006 CLAMP MS 1 25 MEL A 3024 ASA 140 14 2 11251614 PIM 1 5 ST 154 15 0 400 11241061 GROUNDING BRAID D2 4 MONEL MR111 160 16 2 11250001 WASHER A3 2 YELLOWPASS 170 237 1 11620027 CAPACITOR ELECTR INF 20 50 500 221265703102 27 R77 83 7 11603501 RESISTOR MF 14 1 0 25W SOPPM 411 2 VITROHM 23 B a a Fig 1409 1411 11 Preamplifier Unit 10860160 96 10 10 FOR PART NUMBER 10860160 PREAMPLIFIER UNIT 12 DYNODE 10455394 960103 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 10860159 P C ASSEMBLY PREAMPLIFIER BOARD RAS 10360158 10 2 1 10355395 BOX ASSEMBLY NTL 5 30 3 1 15355397 COVER FE PLATE 5 1 NTL 5 40 4 4 10455398 NUT MS 6K6 NTL 5 50 5 1 10455399 INSULATION PRESPAN 0 5 NTL 5 0 6 2 10455400 SPRINGTION S 0 15 NTL 5 70 7 i 10455401 BASE E678 21A NTLS BO 8 1 10544576 LABEL DANGER H V SERIVA 90 9 4 11271044 SCREW M i 4 FE YELLOWPASS 100 10 5 11271645 SCREW M 3 5 FE YELLOWPASS 110 11 2 11271019 SCREW M 3 8 FE YELLOWPASS 120 12 1 11278002 NUT FE YELL WPASS 130 i3 2 11310006 CLAMP MS 1 25 MKL A 3024 ASA 140 14 2 11251014 PIN 1 5 ST 150 15 0 400 11241001 GROUNDIMG BRAID D2 4 MONEL MR111 160 16 4 11250001 WASHER A3 2 170 17 2 11271017 SCREW M 3 5 MS KTS 11271079 180 18 2 11260035 RISE FIN M3 10 MS 5 03 103 190 C37 41 2 11620027 CAPACITOR ELECTR INF 20 50 500V 221265703102 27 R7 7 86 10 11603501 R
20. 530 K S88 76 1 104588982 BRACKET RIGHT FE 5 1 1409711715 400 77 1 1045889 BRACKET LEFT FE 5 1 1409 11 15 Ach 75 G 10G 10458891 BRACKET FE PLATE 5 1 1415 240 79 D 100 10458887 LEAD SHIELD LEAD CAST 1415 239 81 0 100 103558585 LEAD CAST LEAD 1415 237 Ba 0 100 10355888 LEAD CAST LEAD 1415 236 104 11250039 WASHER 4 3 12 1 FE ZINKED 440 102 11274004 SCREW M 476 FE YELLOWNPASS 513 105 z 11310047 NUT M4 PLATE 1 7 2 7 2 54 32 590 112 0 100 11550112 INSULATING TAPE S 1 2 1 6 CE 016 660 113 1 10460803 COVER PLATE ST PLATE T 1 5 NTL 5 640 114 2 11276032 SCREW C 3 5 65 5 FE YELLOWPASS 650 115 1 10460954 SHELTER POM PLATE S 8 BLACK NTL 5 545 116 2 11271053 SCREW M YELLOWPASS 548 117 D 100 16361270 PB PLATE PB 99 6 NICKELIZED 1400 SERIE 241 118 1 10861410 P C ASSEMBLY CONNECTION BOARD RGE 10461408 40 118 2 11274155 SCREW M 6 16 ST YELLOWPASE 546 126 1 10460762 PLATE RIGHT FE PLATE 5 2 0 1414 680 124 1 10460761 PLATE LEFT FE PLATE S 2 0 1414 690 122 4 11274002 SCHEW M 376 FE YELLOWPASS 700 i23 2 10461276 HOLDER FE PLATE Sz1 NICKELIZED 710 124 1 10461414 SUPPORT 1 FE PLATE 5 1 1414 720 125 2 700 311240172 GASKET 6 35x6 45 MONEL GLUE O1 0901 6603 730 Lab 1 BO0 112740162 RF GASKET 4 244 8 MONEL 03 0901 6601 74a 127 1 10461613 HOLDER FE FLATE T 1 1409 725 10355319 43 1 104572303 PLATE ST PLATE T 1 5 1410 12 l0255218 44 1 10357902 SUPPORT RST T 0 8 1410 13 10355819 17 1 10355782 ID ZHiELD PE PLATE 5 1 NTL gt 635 wid 1 1066
21. 690 00 710 720 730 740 750 760 770 780 790 BQO 810 820 830 840 850 860 870 80 890 900 910 920 930 940 550 960 970 950 990 1600 1010 1020 1030 1040 1050 1060 1080 1090 1116 1120 1130 1135 1136 1140 1160 1170 1180 1130 1200 1210 1220 1230 1250 PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 1410 201 SPARE PART KIT 1410 1410 201 980731 ITEM NO QTY ORDERNO NAME TYPE MANUF INF LINE DATE i 10854755 P C ASSEMBLY COINCIDENCE BOARD LAC 10354734 100 920120 1 10855551 ASSEMBLY SAMPLE amp HOLD 1 DAD 10354773 120 920120 1 10553313 P C ASSEMBLY SAMPLE AND HOLD EBC 10353702 170 440117 1 115200489 STEPPING MOTOR 12V 0 4A 1 5AST 0 2 6NM 6500 15 4 13 5 211 320327 l 40555353 PREAMPLIFEER UNIT 1410 10455394 350 3920120 1 1410 5231 JUMPER SETTINGS 1410 SERVICE BAG 1110 921 14220 930527 7 1410 921 JUMPER SETTINGS 1410 SERVICE BAG 410 921 1220 940425 1 10854744 PLC ASSEMBLY GAIN STABILIZER 10354783 130 911026 1 10854242 P C ASSEMBLY 4 D CONVERTER EEP 103523905 166 931011 1 1221 243 PROGRAM PACKAGE GEN TERM 1221 243 1100 931129 1 115500623 DISK CARD BOX 9 174 02177 1070 960731 3 10857820 PROGRAM PACKAGE 1409 FIXED PROTOCOLS 1136 960730 LSC Model 1409 001 10857647 96 10 10 FOR PART NUMBER 10857647 LSC 1409 001 930316 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 10857646 LSC ASS 1409 1410 1411 10155600 40 1 108557
22. 7 i 10856464 P C ASSEMBLY MICRO COMPUTER DCD 10356465 55 B 1 10854284 P C ASSEMBLY 1 0 BOARD DIC 10354883 65 9 1 10854506 P C ASSEMBLY MCA DIE 10354603 75 10 I 10853316 P C ASSEMBLY POWER SUPPLY DPA 10353503 85 11 2 10854021 P C ASSEMBLY MOTOR CONTROL BOARD HPS 10354622 95 12 1 10859287 DISPLAY UNIT 1400 SERIES 10355598 115 13 1 16361369 BOX ASSEMBLY 1414 125 14 1 10300774 SIDE BOX RIGHT FE PLATE 1 0 1414 135 15 1 10360773 SIDE BOX LEFT FE PLATE 5 1 0 1414 145 16 1 10455523 BOTT M ASSEMBLY NTLS 155 17 2 10455328 CAM D25 NTLS 175 18 2 10458830 GUIDE PLATE FE PLATE S 1 1415 205 13 1 10455330 BUSHING D12 NTL5 1470 195 20 2 10455329 PLATE FE PLATE S 3 NTL5 185 Al i 10355332 LEAD LEAD 99 95 NTL 5 215 22 2 10455333 LEAD LEAD 99 9 NTL 5 225 23 2 10455334 LEAD LEAD 99 9 NTL 5 235 24 1 10355335 HANDLE 1 FE PLATE S 2 NTL5 245 25 1 10255612 BACK PLATE FE PLATE S 1 NTLS 265 26 4 10455616 BUSHING MS D 20 NTLS 275 27 1 10355817 INSULATION SOLUPOLYETHEN 285 28 1 103554618 COVER 1 AL FLATE 5 2 NTL 5 295 29 1 10455632 COVER 2 FE PLATE 5 2 NTL 5 305 30 1 10355742 COVER 3 AL PLATE 5 2 NTL5 306 32 0 200 10461480 FLATE 1414 325 33 1 11710021 FLOPPY DISK DRIVE 3 5 2 F B8OU D5007250KB FDl137H 335 37 1 10548122 LABEL 0 366 38 1 10355677 SUPPORT AL PLATE 5 2 NTL5 375 23 1 10355686 COVER FE PLATE 5 1 NTL5 385 40 1 10455723 BUSHING POM ROD D 40 NTL5 495 41 2 10455797 SHIELD MU s 0 1 NTL5 405 42 15 11250008 WASHER 4 3 5 0 8 FE YELLOWPASS 415 43 12 1125001
23. 91 09 25 TO 96 10 10 FOR PART NUMBER 10854789 COUNT WEIGHT 10454790 960620 ITEM NO QTY ORDERNO NAME TYPE MANUF INF LINE DATE 1 10454793 AXLE DEHE NTL5 10 931115 1 10454794 BUSHING MS ROD D30 NTL5 15 931115 1 19454795 TUBE D10H8 NTLS 20 931115 l 10454796 BUSHING MS ROD D36 HTLS 30 931115 4 11350073 JOURNAL BEARING GLYCODUR PG 060810 F 40 931115 3 11350675 JOURNAL BEARING GLYCODUR PG 101210 F 50 931115 1 11251070 LOCK WIRE FOR D 10 AXLE FW 10 60 931115 1 11251053 LOCK WIRE FOR D 6 AXLE EW 70 931115 i 11251055 PIN 2 10 RUSTPROOF 80 931115 50 Fig 1409 1410 1411 17 Count Weight 10454790 ME 2073 331221 AS 1045 4790 Piirt 870826 745 Tark 870827 Ma Hyv 870827 Fig 1409 1410 1411 18 Support 1 Assembly 10855074 96 10 10 FOR PART NUMBER 10855074 SUPPORT ASSEMBLY 10455075 951006 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 1 10355076 SUPPORT ASSEMBLY NTL5 10 2 1 10455077 AXLE D6H8 NTL5 20 3 1 10353761 COGGED BELT WHEEL PA6 30 MINERAL 1297 30 4 l 11350098 COG WHEEL 10 56 10 40 5 1 10455068 AXLE D6H8 NTLS 50 6 1 10455669 BEARING HOUSE 6Kl4 NTL5 60 7 1 11350073 JOURNAL BEARING GLYCODUR PG 060810 F 70 8 3 11350072 JOURNAL BEARING GLYCODUR PBG 060804 F 80 9 1 11251037 GRIP RING FOR D6 AKLE G6 90 10 1 11278015 NUT M12 FE YELLOWPASS 100 11 1 11275007 SCREW M4 5 110 12 2 11275008 SCREW M4 6 120 13 1 10456254 COGGED BELT WHEEL BLANK 10353761 31 14 1 11250019 WASHER 6 4 18 1 6 FE YELLOWP
24. HAN 37 SHORE A 130 14 2 10455281 AXLE 2 D6HS 140 15 2 10455282 BEARING POM NTL 5 150 16 1 10455283 GUIDE 1 AL 1025 NTL 5 150 17 1 10455284 GUIDE 2 AL 10325 NTL 5 170 18 L 10455285 LATH FE S 1 NTL 5 180 1 1 16452652 SPRING D 1 5 1220 130 2G i 10455286 TUBE ACID PROOF TUBE D 4 200 21 2 10455287 BUSHING MS FOD D20 NTL 5 210 22 1 10455288 SPRING SPRINGERONZE S 0 NTL 5 220 23 2 10455289 BRACKET FE S 1 5 NTL 5 230 24 1 10355290 LEAD SHIELD LEAD 99 9 NTL 5 240 26 10455292 FLATE AL 10X20 NTL 5 240 27 1 10461099 LABEL AL Sz 1400 SERIES 270 AB 1 10553597 P C BOARD 1 5MM z P EP LK RRA 1205 l470 280 29 0 950 11183031 TUBE D 6 4 POLYAMID amp 1 PA il 230 31 4 11250006 WASHER 3 2 7 0 5 FE YELLOWPASS 310 32 3 11250008 WASHER 4 3 9 0 8 FE YELLOWPASS 420 33 2 11250019 WASRER 6 4 18 1 6 FE ZINKED 330 34 3 11250039 WASHER 1 3 12 1 FE ZINKED 440 45 4 11251031 FASTENING RING FOR 5 7 MM AXLE 350 36 2 11252003 RIVET 1 9 3 ST KDS O 43 460 37 2 11260021 PLUG NUT M6 11 ST SINE LAS 370 38 4 11271016 SCREW M 3 4 FE YELLOWPASS 390 39 16 11274004 SCREW M FE YELLOWPASS 390 40 6 11274007 SCREW M 4 12 FE YELLOWPASS 400 di 4 11274015 SCREW M 5 16 FE YELLOWPASS 410 42 1 11274072 SCREW M4 16 FE YELLOWPASS 420 43 4 11275008 SCREW M4 6 AISI316 430 44 2 11274095 SCREW ME 25 YELLOWPASS 240 45 2 11350027 BEARING D 6 10 9 HE0609 450 46 2 11350080 JOURNAL BEART GLYCODUR PBG O081005 5F 460 47 1 10556158 LABEL WHITE SELF FASTENING 1410 271 48 2 1125000
25. M5 i6 ST YELLOWPASS oT POLYESTER 11570075 NTLS NTL5 1410 WARNING 1410 CR 1410 PROGRAM CR LSC 5 NTL gt NOTE LSC LEC 10255679 1409 11 15 1405 11 15 1415 1415 1415 1315 1415 1282 14850 2 54 329 14 068 040 sac 10358303 1166 10 1415 1414 10460712 1414 1414 NTL 5 MACH LABEL 1414 003 275 285 295 405 306 148 425 148 415 423 421 375 385 395 403 450 431 435 445 455 465 475 485 435 205 215 S25 535 545 555 565 454 326 510 585 427 511 417 415 41 404 514 409 413 328 329 576 119 400 401 254 253 5 251 252 255 440 513 570 512 590 426 51 427 330 580 120 150 151 432 556 402 490 530 411 14 1 10861410 P C ASSEMBLY CONNECTION BOARD RGE 10461408 114 142 2 10461276 HOLDER FE FLATE 5 1 NICKELIZED 350 143 1 10461414 SUPPORT 1 FE PLATE 551 0 1414 340 144 2 11240173 RF GASKET 6 35x6 35 MONEL GLUE 01 0901 5603 60D 145 2 306 11240162 RF GASKET 3 2X4 8 MONEL 01 0901 6601 610 146 2 10461480 PLATE 1414 360 147 6 11276022 SCREW C 2 9 9 5 FE YELLOWPASS 577 145 1 10461613 HOLDER FE PLATE T l 1403 355 10260807 43 1 10358873 SHIELD ASSEMBLY FE PLATE LEAD CAST 1415 270 10260807 23 1 10361031 COVER PLATE 3 POLYCARB 0 375 1414 410 10260807 37 1 11570061 LABEL WALLAC 52X22 165TICKER 424 10260807 42 4 11250033 WASHER 4 3 12 1 FE ZINKED 441 10260807 41 2 11274006 SCREW M 4 10 FE YELLOWPASS 466 10260807 48 2 11276026
26. PART NUMBER 10854822 LIGHT SHUTTER UNIT 10354823 930518 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 10553597 P C BOARD 1 5MM 2 P EP LK RRA 1205 1470 200 1 11863089 P C CONNECTOR 5 P STRAIGHT LOCKABLE MLSS100 5E 210 1 1 10454824 BODY PLATE FE PLATE S 2 NTL5 20 2 1 10354825 SHAFT COVER DSO NTL5 30 3 1 10354826 BODY 10x40 NTLS 20 4 1 10457757 COUPLING 1 POM D 30 BLACK NTL5 S 5 2 11251095 PIN 1 18 60 6 1 10454830 PLATE 1 SPRINGSTEEL S 0 2 NTLS TO 7 1 10454831 PLATE 2 SPRINGSTEEL 0 2 NTL5 BO 8 1 10454832 PLATE 3 SPRINGSTEEL S 0 2 NTLE 90 9 1 10454833 PLATE 4 SPRINGSTEEL 5 0 2 NTLS 100 10 1 10454834 COVER PLATE FE PLATE S 1 NTES 110 11 1 10455111 COVER 1 10x40 NTL5 120 12 2 10454837 BUSHING n3 NTL5 130 13 1 10454838 COUPLING POM D 30 BLACK NTL5 140 14 4 11251071 LOCK WIRE FOR Dz28 AXLE FW 28 145 15 1 11271045 SCREW Ma 5 FE YELLOWPASS 150 16 1 11271045 SCREW M3 5 FE YELLOWPASS 160 13 2 11271051 SCREW M3 16 FE YELLOWPASS 170 18 4 11271035 SCREW M3 8 FE YELLOWPASS 180 19 1 10455112 COVER 2 1040 NTL5 125 20 2 10458293 WASHER SPRINGPRONZE Tz0 5 NTL5 142 M 1 11690050 STEPPING MOTOR 1 5IN 0 7A STEP ANG1 amp 6500 R564 150 we 1 10855405 WIRING ASS CAZ 10 PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 10854822 LIGHT SHUTTER UNIT 10354823 920625 TEM NO QTY ORDER NO NAME TYPE MANUF INF LINE DATE 2 1 10454327 FLANGE D30 NTL5 50 9201232 5 2 10454829 PIN D1 NTL5 60 930517 2 10458293 WASHER SPRINGPRONZE T 0 5 NTL5 142 921215 14 2 11
27. Results are printed out shown in the example on the next page The plot has the reference counter channel number on the x axis and the measured real channel number on the y axis Two lines are drawn one is a solid dine and the other rs dashed on the raw data printer it is marked with crosses The solid line represents the reference counter MCA channels and the dashed crossed line the measured channels On the display the reference line is tn blue and the actual in red This ine may reside slightly above and below the ideal line There should be no straight horizontal or vertical section which would indicate missing MCA channels The mapping information is also saved in numerical form in the printer and instrument history file When the Ready message is displayed on the Status bar after mapping has been done it shows that the mapping information has been saved in the EEPROM memory Then switch the instrument off and on again to reboot it 6 3 Routine maintenance PROTOCOL 1 MAPPING DATE 1994 08 11 TIME 10 25 TD P01A5002 Quench standardization Wallac 1414 WinSpwetral DSA version Counting mode Quench index Isotopets Frotocol name Counting time Activity DEM 2 sigma Minimum cpm Vial type Liquid system Advanced modes Halrlife zerotime Zerotime of H3 Qutput to printer POS CTIME CPM1 CPMerl EFFI Additions to printer Spectrum Quench standard samples Pos CTime H3_CPM H3_CFMe
28. SCREW NUT PLATE SCREW LABEL LABEL LABEL PLATE SCREW INSULATION LABEL BRACKET GUIDE SCREW RESET UNIT BRACKET RIGHT BRACKET LEFT WASHER SCREW NUT BOD DUMMY PLUG PLATE RIGHT PLATE LEFT WASHER SCREW SHELTER SCREW SCREW LABEL P C ASSEMBLY HOLDER SUPPORT 1 RF GASKET RP GASKET PLATE SCREW LABEL HOLDER 98 LEAD 99 9 LEAD 99 9 LEAD 99 9 FE PLATE 5 2 FE FLATE 5 1 MS D 20 SOLUPOLYETHEN AL PLATE S 2 FE PLATE S 2 AL PLATE S 2 3 5 2 P BUU P560 250KB AL SQUARE BAR 8 2x8 2 AL 99 5 Sel AL PLATE 5 0 5 D SMM AL PLATE 3 2 FE PLATE 5 1 POM ROD D 40 MU S 0 1 4 3 9 0 8 FE YELLOWPASS 5 3 10 1 FE YELLOWPASS 6 4 18 1 6 FE ZINKED 3 20 ST 13 1 1671 1 953 ST 2 4 5 1 AL M 3 4 FE YELLOWPASS M 4 5 FE YELLOWPASS M 5 12 FE YELLOWPASS M 5 20 FE YELLOWPASS M 6 30 FE YELLOWPASS M6 12 FE YELLOWPASS M6 25 YELLOWPASS M4 8 FE BLACKPASS NTL 5 NTL 5 NTL 5 NTLS NTLS NTL5 NTL 5 NTL 5 NTLS 1414 FD1137H 1414 NTL5 NTL5 NTLS NTL5 NTLS KDS 0 3 TAP D B5 33 5 3 15 1 5 FE YELLOWPASS AL PLATE 5 3 M 4 10 FE YELLOWPASS M4 FE YELLOWPASS FE PLATE 5 1 M6 12 FE YELLOWPASS HV ALO Q08 AL S 0 08 FE PLATE T 1 M 3 10 FE YELLOWPASS S 20 WHITE SELF ADHESIVE L SOLUPOLYETHEN FE PLATE T 1 FE PLATE T 1 C 2 9 6 5 FE YELLOWPASS FE 5 1 FE 551 4 3 12 1 FE ZINKED M 4 6 FE YELLOWPASS M 1 7 2 7 D4 8 4 4 1414 FE PLATE S
29. SCREW C 3 9 9 5 FE 567 10355813 17 1 10355762 ID SHIELD FE PLATE 5 1 NTL 5 405 10355819 43 1 10457903 FLATE ST PLATE T 1 5 1410 406 10355819 44 1 10357902 SUPPORT RST T 0 1410 407 Wag 1 10861346 FLAT CABLE 405 405 FC207 19461300 117 w32 1 10851411 WIRING ASS CA210 115 PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 10861384 GUARDIAN 1414 603 10160809 960404 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE DATE W26 1 10855592 FLAT CABLE 205 508 FC35 10455666 118 951128 147 4 11276022 SCREW C 2 9 9 5 FE YELLOWPASS 577 960403 1 1414 102 PC PROGRAM PACKAGE PSA SPECT ANALYS PRG 1414 102 1015 966402 1 1414 931 INSTRUMENT MANUAL FOR 1414 001 1414 931 1920 951201 104 10160809 Fig 1414 34 LSC Assembly 105 106 941116 AKO 950405 AKO 950502 AKO 3950626 AKO 950829 AKO 951 Ar 10160809 I 1414 001 WINSPECTRAL 10860678 1414 002 ALFABETA 10861383 1414 003 GUARDIAN 1414 103 GUARD OPTION 1414 103 1414 104 GUARD OPTION 1414 1 1474 111 GERMANY OPTION 1414 111 1414 112 GERMANY OPTION 1414 112 PIIRT 941007 AKO TARK 941007 VS HYV 941619 KLOU Fig 1414 35 Body Assembly 10860804 66 10 10 FOR PART NUMBER 10860904 BODY ASSEMBLY 1414 10160805 960509 ITEM NO QTY ORDER NO MAME TYPE MANUF INF LINE 12 11310037 CLAMP FCC A CH 330 7 11310038 CLAMP ACC3H A 40 E 11310040 CLAMP ACC 2 A 350 1 10555601 LABEL SET FC31 380 1 10555430 LABEL SET CALA 396 1 1 10254918 BODY NTLS 29 2 1 10150788 BOTTOM PLATE
30. SCREW M 3 10 FE YELLOWPASS 580 20 2 11271026 SCREW M 3 18 PE YELLOWPASS 690 2l E 11250044 WASHER 3 2 0 0 8 FE YELLOWPASE 700 22 1 11271013 SCHET M 3 6 FE YELLOWPASS 710 23 2 11250006 WASHER 1 2 7 0 5 FE YELLOWPASS 720 24 1 10861635 F C ASSEMBLY FILTER BOARD EYP 10461634 525 20 1 10861638 P C ASSEMBLY FILTER BOARD RYO 10461637 535 26 0 050 11180017 PE STRING 5 5 BLACK PZ 940 SJH 730 27 1 10453697 INSULATOR PLATE PRES PAN 5 0 5 1205 740 28 0 850 11220014 TAFE 12MM CLEAR TESA4971 750 W25 1 10851794 FLAT CABLE 268 268 10451787 530 W25 1 10855592 FLAT CABLE 505 505 FC35 10455666 933 W33 1 10861704 FLAT CABLE 345 345 FC220 10461702 537 PART HISTORY FROM 93 11 11 TO 96 10 10 FOR PART NUMBER 10859287 DISPLAY UNIT 1400 SERIES 10359598 960612 GTY ORDERNO NAME TYPE MANUF INF LINE DATE 1 10355623 PROGRAM PACKAGE DISPLAY PRG HCB BOARD 521 930825 7 5 11271030 SCREW M3 35 FE YELLOWPASS 580 40405 W 1 10851794 FLAT CABLE 265 265 10451797 530 960213 5 5 10455619 BUSHING MS D6 4 NTL5 560 960115 7 4 11271030 SCREW 3 35 FE YELLOWPASS 580 560115 11 1 11211029 SCREW M 3 30 FE YELLOWPASS 585 960115 8 12 11278002 NUT Mi FE YELLOWPASS 590 960112 68 10355598 MM LOOSE A AH Marl SHL 04088 LBCOSuUl J 86SSSE0L 69 j 655c3H ar COLOSE D 256 34 VSESIEC9S 3 1 SZ 3l YSL 412096 S 69 c 39 Sv L26055 Sv 919055 S slot 6 YSL 200005 Fig 1409 1410 1411 24 Display U
31. TES 196 38 2230 30 1 11274001 SCHEN M 3 5 FE YELLOWPASS 300 31 1 11274015 SCREW M 5 16 FE YELLOWPASS 310 32 7 11275003 SCREW M3 4 AISI3168 320 33 1 11310031 CLAMP AIO31ASA 230 34 2 11390034 O RING OR 3 10 1 60 00044 2d 360 35 1 10456132 ADJUST PART NTIL 5 176 36 2 11250019 WASHER 5 4 18 1 6 FE ZINKED 211 38 3 11278002 NUT M3 FE YELLOWPASS 312 39 2 11278004 NUT M5 FE YELLOWPASS 313 40 1 11275025 SCREW MI 16 AISI316 314 41 1 10457147 FIN POM BLACK 1410 178 42 1 10449428 SPRING D 0 5 1291 1235 179 K 1 11863089 P C CONNECTOR 5 F STRAIGHT LOCKABLE HLSS1I00 5B 350 M 1 11690044 STEPPING MOTOR 12V 0 44 1 3AST 0 26NM 6500 15 4 13 5 R455 340 PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 10855618 D UNIT 10355819 850110 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE DATE 20 4 11250005 WASHER 3 2 7 0 5 FE YELLOWPASS 200 950199 23 3 11271015 SCREW M 3 4 FE YELLOWPASS 230 950109 24 2 112371018 SCREW M 3 6 YELLOWPASS 240 9501092 29 6 11271075 SCREW M 3 6 MS TES 196 38 290 950109 32 6 11275003 SCHEW M3 4 320 950109 42 10355819 Fig 1409 1410 1411 13 ID Unit BE gogg MAH Xe 90198 AUDI 90089 V 6185 SE OL NDO T3I 1350 NOSVi NYH WJU ISSO LAGMa3W YTISOHVE s LOSE Y TE IW SOSE 3H vci 8 IRE hoy OSL vocobg eg 1103 SHL 20219438 99 loa 43 a Fig 1409 1410 1411 14 Light Shutter Unit 10854822 96 t0 10 FOR
32. WALLAC 52 22 16 STICKER 35 PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 10857649 ESC 1411 001 931203 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE DATE 2 10857681 PREAMPLIFIER UNIT 1411 10455394 80 911030 1 10857670 P C ASSEMBLY COINCIDENCE BOARD LAC A 10357727 90 911030 1 10857671 P C ASSEMBLY SAMPLE amp HOLD 1CH LAD A 10357728 100 911030 10155600 75 1 11570061 LABEL WALLAC 52xX22 16 STICKER 35 931202 i 10855268 STD CAPSULE 10455269 560 950216 Fig 1409 1410 1411 01 LSC Assembly 10857646 96 10 10 FOR PART NUMBER 10857646 LSC ASS 10155600 960321 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE n 1215 111 UNO STANDARDS SET 20ML VIALS 3H 14C BACK 1215 111 110 l 10551111 LABEL CSA APPROVED ALO 08 LR52500 BRADY 404 1 10560490 LABEL SET CA22 12 DYN 409 1 10555509 LABEL SET FC33 FC207 412 1 10556126 LABEL VME RACK 1410 Ald 1 10561614 LABEL 11570078 BRADY CE LABEL 416 1 11310040 CLAMP ACCBZ A 586 5 11310037 CLAMP FCC A C8 587 0 300 10561102 LABEL WARNING STICK BRADY EU 152 10561102 LAB 595 6 300 10856077 TNSTALL KIT 115 FOR 1410 605 0 700 105856078 INSTALL KIT 250V FOR 1410 615 1 11560029 MOUSE MAT 194344 670 1 1 108549165 BODY ASSEMBLY 1410 10154917 10 2 1 10855413 ID UNIT 1410 10355859 11 3 1 10855334 SAMPLE CHANGER 1410 10255333 15 4 1 10854849 MEASURING UNIT 1410 10354850 25 5 1 10859369 P C ASSEMBLY HV DIVIDER UNIT RFA10359368 10355373 35 6 1 10861711 TOP COVER ASSEMBLY 1409 1411 10255462 45
33. and vial A protocol can be created which scans the PAC levels over a range which s appropriate for the cocktail see the User manual for more details Both the active sam ple and the background are measured The count rates in the windows of the beta emitter are printed There are two extra windows both wider than the whole spectrum but the first one is for the beta spec trum while the second one Is for the PAC rejected beta spectrum The results are printed each line contains the CPM value in each window the PAC level used and a calculated field RATIO which ts the CPM value in the beta window the pulses with less ampli tude disparity than defined by the PAC level divided by the total CPM value The higher the PAC level the closer to each other must the amplitudes be for the pulse pair to be accepted A greater number of pulses will be rejected at high PAC values than at low ones Software features and benefits A printout and a plot of RATIO ys repeat number is generated in the run and spectra saved The optimum PAC level is the one at which E E B beta counting efficiency squared over background or figure of merit in the beta window is at a maximum PAC does not reject alpha pulses as much as beta pulses since the number of photons from an alpha de cay is very much greater than that from a beta decay The variation of the left and right pulse amplitudes 15 thus less for an alpha decay event than for a beta de
34. correcton in LS counting Digital Overlay Technique DOT DOT is used to reconstruct a standard spectrum at the same quench level and intensity as the unknown sam ple When the standard spectrum has been fitted the DPMs are calculated The procedure is the same for dual or triple label counting except that when the standard spectrum for each isotope has been reconstructed these spectra are combined and fitted to the composite spectrum of the unknown sample After a successful fit the isotope ra tios and intensities are established and the DPM values calculated Spectrum library A Wallac WinSpectral with DOT DPM has a library of spectrum data comprising information about iso tope cocktail vial type combinations for about 00 quench levels 10 chemical x 10 colour This library is built in to the counter during its production Along with each combination the SQP E and colour index are determined and saved WinSpectral then works not with quench curves but with quench surfaces which represent both chemical and colour quenching In sample counting the SQP E and colour index are measured and the corresponding point on the quench surface is determined This is then combined with the the counting mode isotope and vial type specified In parameter setting to get a specification for the spec trum data to be selected from the library Advantages of DOT DPM the Wallac library provides Easy Count DPM results without quench curve me
35. elevator driven by electric motor single dual plate light shut ter system sample change time 5 s Rack and sample position movements controlled by electro optical sen SOFS Optional external standard Eu 152 450 kBg 12 Ci enclosed tn a stainless steel capsule Optional temperature control unit Controls sample and instrument 5 C of ambient Detector assembly Two PM tubes in coincidence Assembly includes also light emitting diodes for the automatic spectrum stabi lizer Coincidence resolution time is 15 ns Racks and modification kits Sample racks 1410 401 for 20 ml vials max vtal diameter 28 4 mm 12 sample positions per rack 1410 402 for 6 mi vials max vial diameter 18 4 mm 18 sample positions per rack 1410 403 for 4 ml vials Skatron or Biovial max vial diameter 13 4 mm 24 sample positions per rack Max acceptable vial height is 68 mm Rack modification kits 1410 408 for Eppendorf tubes to be used in 1410 402 racks 1410 409 for microfuge tubes to be used in 1410 403 racks Posiden sample identification system Each rack can be provided with a 1410 407 ID clip for 1450 452 ID labels The ID clip has two marked areas 6 1 Specifications the upper for the protocol number and the Jower for rack number or special code This provides the infor mation needed for Good Laboratory Practice Electronic hardware A 16 bit microprocessor controls counting and data re duction Memory co
36. extent to which the observed error de viates from the theoretical X2 multiplied by the de grees of freedom n can be used to determine a probability that random sample from a normal distri bution would have a larger or smaller value of X than the observed value List of symbois used a activity DPM b FIP channel c measured total count rate CPM cj measured channel count rate CPM C an array or column vector comprising the meas ured count rates cj d error in function or parameter e counting efficiency f fractile value gi diagonal element of matrix G G the matrix SW esy h surface function parameter i Index to isotope j index to channel k index to surface function parameter number of parameters defining the surface m maximum number of isotopes n maximum number of channels or number of re peats replicates p total quench index SOP E g number of fractiles f r colour quench index Colour sj reference spectrum a column in sj channel value in reference spectrum an element in the matrix a matrix containing the reference spectra si counting time or elapsed time tio half life u index to fractile fand FIP channel b wj weight value for channel j a diagonal element in the matrix W W the weight matrix xj unknown total count rate for isotope 7 an element in the array X LA Calculation methods xij unknown channel count rate for isotope
37. the 36 from the expression 30 3 SORT BGD t where BGD is the measured mean background rate in the window and t is the counting time in minutes Note a typical change in efficiency of 2 for H over a period of a year may be expected Serial port settings The factory settings of the printer serial port on Win Spectral are as follows Baudrate 4800 PC Parity No Data bits 8 Stop bits 2 Handshake DTR i e ESN These settings may be changed by selecting System parameters in the System menu See the User manual on page 71 5 6 MultiCalc installation Introduction If you are planning to use MultiCalc to handle results from Wallac WinSpectral please follow the installa tion instructions below in addition to the normal Mui tiCalc installation procedure do normal the MultiCalc installation see the Multi Calc Installation module in the Supervisor s manual start up Windows with File Manager copy the file c 400w mnc win beta cOl to the directory c wiacalc Ocom create the directory c wiacalc Ocom winbeta create a new program In the Windows StartUp group click Browse to select c 1400 wimc WTA PIF start MultiCale by double clicking that icon select Level 5 if your starting level is 3 or less then press F7 LEVELS then F4 Level 4 and then again LEVELS F7 and Level 5 F5 select the System properties to be AOSPMTIV fol low the sequence F7 SYSTEM F8 ETC F3 COMM PROT F4 PROP
38. the sam pie Chamber and thus offers true background event de tection dt does not cause observable counting effi ciency losses In iow level counting A sample event iat is simultaneous with the guard event is rejected by Ihe ciectronics since the event 15 then most probabiy as Hardware features and benefits caused by a particle or photon from the environment No limitation in sample fluor selection ts introduced by this background subtraction method The guard is switched on automatically and remains on except when the extemal standard is being used Usage of Wallac Guardian is thus tdentical to that of Wallac 1414 WinSpectral but the performance is improved due to the lower background rate Temperature control for sample homogeneity When dealing with the maximum sample holding ca pacity of scintillators t becomes very essential that the temperature remains practically constant through the whole sample batch Proper temperature control guar antees that all samples are counted at the same tem perature in spite of variation of ambient conditions if for instance the am conditioning is turned off during the mght time Thus the risk of phase separation in samples due to for example a temperature drop dur ing overnight counting is elinunated The conveyor can be temperature stabilized This is achieved by installing the optional Temperature Con trol unit which can be set to maintain the temperature at a sele
39. using conventional toluene xylene and cu mene based cocktails The solution Wallac WinSpectral has a built in ionizer unit which removes static charges by sending positive and nega tive ions towards the vial Since the vials in the Flexi Rack system ate raised directly into the measuring chamber wethout making further contact with other materials the ionizer is very effective The rack design also reduces static charge build up because the sam ples are located in round holes in the rack without any sharp edges which tend to collect static charges more easilv In addition to the ionizer there is the Statistics Moni tor The purpose of this monitor is to warn of unac ceptable count rate variation in a sample The sample count rate in different periods of the sample counting time is measured to determine the sample count rate variation A Y test is used to see if the count rate 1 13 Software features and benefits variation for each sample hes within the range ex pected from the statistical nature of radioactive decay Sometimes it may not lie within this range due to for example chemiluminescence radio frequency signals static or extreme cases of normal statistical variation In such cases of unexpectedly high sample count rate vartation the sample ts recounted The test is applied to both the sample alone and the sample with the external standard in position A maxi mum of two recounts are made for each of these c
40. 0 16 1 11278015 NUT M12 FE YELLOWPASS 180 17 2 10553597 F C BOARD l 6HMM 2 P EP LK RRA 1205 1470 130 18 4 11320106 LOCK CARD SPACER NYLON KGLS 38 200 20 1 11350077 COGGED BELT SYNCHROPLEX 10 T2 5 160 130 21 2 11251037 GRIP RING FOR D AXLE G6 45 K 2 11863089 P C CONNECTOR 5 P STRAIGHT LOCKABLE MLSS100 5E 230 HL M2 11620042 STEPPING MOTOR 5V 1A 1 8AST 0 4NM 6500 20 4 4 5 R416 215 PART HISTORY FROM 91 09 25 TO 95 10 10 FOR PART NUMBER 10855070 MOTOR UNIT 2 10355071 941026 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE DATE M4 1 11690042 STEPPING MOTOR lA 1 5AST 0 4NH FH265 04 215 920211 M3 1 11590043 STEFFING MOTOR 5V 1 54 1 8AST 0 835NM PH268 21 220 920212 Fig 1409 1410 1411 16 Motor Unit 2 10355071 SJ y v iN on E Ez p o O 885 if q 7 e 1 tis Ga E y ul ci a Y 49 Fig 1409 1410 1411 17_ Count Weight 10854789 96 10 10 FOR PART NUMBER 10854789 COUNT WEIGHT 10454790 960620 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE i 1 10454794 BUSHING MS ROD Bag NTLS 15 1 10454795 TUBE D10H8 NTL5 20 3 1 10454796 BUSHING MS ROD D46 NTL5 30 4 3 11350073 JOURNAL BEARING GLYCODUR PG 060810 F 40 5 3 11350075 JOURNAL BEARING GLYCODUR PG 101210 F S 6 1 11251070 LOCK WIRE FOR D 10 AXLE RW 10 p 7 1 11251058 LOCK WIRE FOR D 6 AXLE FW TO 8 1 10454793 AXLE D6HE NTL5 10 9 1 11251055 PIN 2 10 RUSTPROOF ag PART HISTORY FROM
41. 0 220 23 4 104552717 BALE MS 6K NTL5 30 24 1 10455218 PLATE WTES 240 25 2 10454558 COGGED BELT WHEEL NTL5 250 38 2 10455220 HOLDER FE PLATE 5 2 NILS 260 27 2 10455221 SUPPORT NTLS 270 28 2 10455222 HOLDERT FE PLATE Sz1 5 NTLS 280 2 1 10355223 FLATE FE PLATE S 1 5 NTL 5 290 30 1 10355368 SUPPORT FE PLATE S 1 NTL 5 300 41 o 10258236 TOOTH POM BLACK 1410 310 32 2 400 113500285 CHAIN HMM 445 320 35 2 11350025 LINK SMM 330 3d ae 11250002 WASHER 44 3 340 15 4 112510223 FASTENING RING 4 5 MM 350 36 z 11250019 WASHER 6 418 1 6 FE ZINKED 360 1 2 11251006 LOCE RING o D 7 370 48 2 11251037 GRIP RING FOR D amp AXLE 380 39 5 11252007 RIVET 3 2 6 1 MONELL TLP D BS424 390 AG 14 11274006 SCREW M 4 10 FE YELLOWPASS 400 41 2 11274007 SCREW M 4 12 FE YELLOWPASS 410 12 e 1132741072 SCREW M4 16 FE YELLOWPASS 470 43 10 11274072 SCREW M4 16 FE YELLOWPASS 430 44 4 11274132 SCREW M3 8 FE BLACEPASS 440 45 10 11271034 SCREW M 4 5 FE YELLOWPASS 450 46 4 11350072 JOURNAL BEARING GLYCODUR PREG 050804 476 47 4 11278002 NUT M3 FE YELLOWPAZZ 470 4 8 5 11350078 COGGED BELT SYNCHROFLEX 10 T2 5 1300 480 43 1 10855243 PF C ASSEMBLY POSITION SENSOR RSU A 10355242 SG 2 11320106 LOCK CARD SPACER NYLON EGLS 35 490 51 4 11310038 CLAMP ACCIS9 A 510 52 2 11276005 SCREW C 4 2 9 5 FE YELLOWPASS 460 53 E 11250008 WASHER 4 3 9 0 8 FE YELL WPASS 341 55 2 11274005 SCREW M 4 8 FE YELLOWFASS 345 58 4 11278003 HUT M4 FE YELLOWPASS 475 59 1 10455263 BRACKET FE P
42. 0 WASHER 5 3 10 1 FE YELLOWPASS 425 44 1 11250019 WASHER 6 4 18 1 6 FE ZINKED 435 45 18 11251018 PIN 3 20 ST 445 46 4 11251045 LOCKRING 13 1 455 47 4 200 11251077 LOCEKRING 1631 465 AB 2 11252008 RIVET 1 9 3 ST KDS 0 3 475 45 10 11252019 RIVET 2 4 5 1 AL TAP D BS 33 485 56 6 11271016 SCREW M 3 4 FE YELLOWPASS 495 51 4 11271034 SCREW M 4 5 FE YELLOWPASS 505 52 12 11274013 SCREW M 5 12 FE YELLOWPASS 515 53 2 11274016 SCREW M 5 20 FE YELLOWPASS 525 54 2 11274034 SCREW M 6 30 FE YELLOWPASS 535 55 6 11274145 SCREW M6 12 FE YELLOWPASS 545 56 1 11274095 SCREW Me 25 YELLOWPASS 555 57 10 11274139 SCREW M4 FE BLACKPASS 565 58 2 11276022 SCREW C 2 9 9 5 FE YELLOWPASS 575 59 2 11250018 WASHER 5 3 15 1 6 FE YELLOWPASS 434 60 d 104551331 COOLING PLATE DL PEATE 223 NTLS 3426 57 E 11271035 SCREW Mario FE YELLOWPASS 510 62 5 11278003 NUT M FE YELLOWPASS 85 63 1 10455897 PLATE FE PLATE S 1 NTLS 327 6d 2 11271095 SCREW M6 12 FE YELLOWPASS 511 65 1 10555070 LABEL HV 1410 WARNING 406 56 1 195560935 LABEL ALO 06 1416 CR 407 47 i 1055607i LABEL AL 0 2 143 PROGRAM CR 408 55 1 10456182 PLATE FE FLATE T 1 LSC 5 410 59 2 11274003 SCREW M 310 FE YELLOWPASS 514 76 1 10456382 INSULATION SOLUPOLYETHEN Sz20 NTL 5 411 73 H 10556507 LABEL WHITE SELF ADHESIVE L MOTE 413 72 2 10457299 BRACKET FE PLATE T i ESC 325 73 i 10457300 GUIDE FE PLATE T 1 LEC 329 4 2 11276015 SCREW C 2 9 6 5 FE YELLOWPASS S76 75 6 400 11140018 SEALING TAPE 11512 SM
43. 024 EDGE STRIP FE PLATE T 1 NTL5 741 38 6 11250041 WASHER 4 3 9 0 8 FE BLACK 850 39 2 11290013 FOOT D12 3 RUBBER WHITE iM SJ 5012 870 40 4 10456181 WASHER FE PLATE T 2 LSC5 742 4 4 11274031 SCREW M5 12 YELLOWPASS 850 42 2 11250039 WASHER 4 3 12 1 FE YELLOWPASS 750 43 1 10358873 SHIELD ASSEMBLY FE PLATE LEAD CAST 1415 655 44 1 10459978 EXTENSION ARM MS D 8 1409 510 45 1 10458578 MOUNTING PIN MS ROD Did 1409 515 46 2 11274004 SCREW FE YELLOWPASS 205 PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 10859279 TOP COVER ASSEMBLY 1415 10255462 940623 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE DATE 1 1 10855445 SPRING ASSEMBLY 10455446 NTL5 510 930812 7 1 10255475 SUPPORT AL PLATE 10425 NTL5 590 940607 40 2 10456181 WASHER FE PLATE T 2 L5c5 742 940607 29 id 11274012 SCREW M5 10 FE YELLOWPASS 790 940607 41 2 11274004 SCREW M4 6 FE YELLOWPASS BOS 940622 86 10255462 Fig 1415 30 Top Cover Assembly K YT SS VAIN 1415 sta 10 25 5462 USED ONLY 1415 HUGH NOTE zor 32 Aiao Tus ary 6 Bode x Piirt 881109 87 Fig 1415 31 Guard 10858914 96 10 10 FOR PART NUMBER 10858914 GUARD 1415 10458913 930915 ITEM NO QTY ORDERNO NAME TYPE MANUF INF LINE 1 1 10358909 LID CU Sz0 5 1415 10 2 1 10258902 GUARD TANK ASSEMBLY 1415 20 3 0 550 11090011 SOLVENT DOBANE 103 DOBANE 103 70 3 0 125 11091022 SILICONE RUBBER 2 KOMP CLEAR RTV 615 80 3 11120019 SECONDARY SCINTILL Q
44. 044 to which this declaration relates is in conformity with the following standard s or other normative document s Title and or number and date of issue of the standard s ar other normative document s EN 50082 1 71992 EN 50081 1 1992 EN 61010 1 1993 if applicable following the provisions of the following directives Electromagnetic compatibility EMC 89 336 EEC Low voitage LV 73 23 EEC Place and date of issua 12 Nov 1997 Turku Finland Name and signature or equivalent marking of authorized person Zu Heikki Kouru Quality Assurance Manager AN JL EGG COMPANY 1096 1060 Quality Control Report Name of Product 1400 Series Liquid Scintillation Counters Manufacturer Wallac Oy Turku Finland Function Tested Classification of External Standard Capsule Eu 152 according to ISO 2919 Activity of the capsule 440 kBq CERTIFICATION Eu 152 External standard source has been tested according to ISO 2919 Sealed Radioactive Sources Classification The tests are Test Class Short definition Temperature 4 40 C 20 min 400 C 1 h and thermal shock to 20 C Ext pressure 3 25 kPa abs to 2 MPa abs Impact 4 2000 g from Im Vibration 3 2 times 10 min two axes 25 Hz to 50 Hz 5G 50 Hz to 90 Hz 0 635 mm amplitude 90 Hz to 400 Hz 10G Puncture 4 50 g from 1 m Leakage tests according to ISO TR 4826 have been performed after the classification tests The tests show no sig
45. 0RZ2 1460 D1 1 11721006 DIODE SRIDGE 2Q00V 25A BYV25 200 160 F1 2 2 11830006 FUSE 2 08 250V SLOW 6 3 32 19343 200 F3 1 11830020 FUSE 154 32V FAST 6 3X232 AGC 15 210 Kl KZ 2 11662133 CONNECTOR 6 N FEMALE 15AWG CT156Fl18 5B 570 Li l 11650063 MATHS FILTER CONN 250W AA 3 N FN321 6 01 190 Ri 1 11501173 RESISTOR IM 2 0 5W B 1 2 BEYSCHLAG 150 51 1 11845021 ROCKER SWITCH eae 10A 250V AlL4ASOVA 170 52 11845027 VOLTAGE SELECTOR iX6 S TENSION 10A 250V SWPO33 1109 180 TR 11650066 TRANS PORMER BBVA 125 29 PART HISTORY FROM 93 09 22 TO 96 10 10 FOR PART NUMBER 10855115 POWER UNIT 10255116 960112 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE DATE 11 2 10455124 SLIDE PVC PLATE S 8 NTL5 110 950920 48 8 11274012 SCREW M 5 10 FE YELLOWPASS 441 950920 40 7 11278004 NUT M5 FE YELLOWPASS 490 950920 52 0 105 11240174 RF GASKET SPRING BeCu 28MM 6MM 97 438 02 620 960111 51 11 11252007 RIVET 3 2 6 1 MONELL TLP D BS424 630 960111 30 Fig 1409 1410 1411 07_ Power Unit 10255116 10 25 5116 D 31 a Fig 1409 1410 1411 08 Elevator Assembly 10854857 96 10 10 FOR PART NUMBER 10854857 ELEVATOR ASSEMBLY 10254858 951025 ITEM NO QTY ORDER NG NAME TYPE MANUF INF LINE 1 1 10254859 BODY AL 3 NTLS 10 2 3 10454860 GUIDE PIECE AL 1025 NTLS 20 4 1 10454862 GUIDE POM BLACK 5 220 NTLS 40 5 l 10454864 HRACKET FE 2 1 5 NTLS 60 7 1 10454465 SPRING SPRINGBRONZE S 0 5 NTLS 70 B i 10454866 BRACKET 2 2 5 NTES BD 9 1 10454667 PLAT
46. 1 10454824 BODY PLATE FE PLATE S 2 NTLS 230 2 1 10354825 SHAFT COVER MS DSO WTLS 240 j 1 10354826 BODY AL 10x40 NTLS 250 4 1 10457757 COUPLING 1 POM D 30 BLACK NTLS 250 5 2 1125195 PIN 1 18 357 6 1 10454830 PLATE 1 SPRINGBRONGE z 0 2 WTL 5 240 7 1 10454831 PLATE 2 SEFRINGPR NZE So0 2 WEL 5 790 B 1 10454332 PLATE 3 SPRINGBRONZE 6 0 2 NTL 5 300 9 1 10454833 FLATE 4 SPRINGBRONZE 0 2 NTL 5 310 10 1 10454834 COVER PLATE FE PLATE S 1 NTLS 320 11 1 10458894 SHIELD 1 MS 10 46 1415 330 12 2 10454837 BUSHING NTES 440 13 1 10454538 COUPLING FOH D 30 BLACE NTLS 350 14 4 11251071 LOCK WIRE 2 355 15 1 11271045 SCREW 3 5 FE YELLOWPASS 460 16 1 11271045 SCREW M 3 5 FE YELLOWPASS 370 17 2 11271051 SCREW M 3 15 FE YELLOWPASS 330 18 4 11271035 SCREW M4 8 FE YELLOWFASS 390 19 1 10458895 SHIELD 2 l0 40 1115 335 20 2 10458293 WASHER SPRINGPRONZR T 0 5 NTL5 352 M 1 11690050 STEPPING MOTOR 1 5IN 0 74 STEP AHGl 8 6500 R568 400 Wwe 1 10855405 WIRING A455 CA21 220 PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 10859276 LIGHT SHUTTER UNIT 1415 10354823 950814 ITEM NO QTY ORDER NO HAME TYPE MANUF INF LINE DATE 2 10454829 PIN DI NTL5 270 930518 2 10458293 WASHER SPRINGPRONZE T 0 5 NTL5 352 950811 Fig 1415 29 Light Shutter Unit 10354823 He 161 pbi AS HE 1 510515 M Ad E 191 HE 195 HE 2113 SUHI A 10 35 4823 Pirt 881108 FMS Tark 881108 Ma Hyv 881108 Z 85 a Fig 1415 30 Top Cover
47. 1086 1430 September 1995 Warning This equipment must be installed and used in accordance with the manufacturer s recommendations Installation must be performed by properly trained and authorised personnel Failure to follow these instructions may invalidate your warranty and or impair the safe functioning of your equipment Please contact your local Wallac representative for installation Y EGzG WALLAC 1414 932 02 March 1995 INSTRUMENT MANUAL 1414 WinSpectral Digital Spectrum Analysis DSA based liquid scintillation counter For instruments with software version 1 3 including WinSpectral o B and Guardian d COMPANY Wallac Oy P O Box 10 FIN 20101 Turku Finland Tel 358 21 2078111 Telex 62333 wac fin Telefax 358 21 2678 357 Contents 1 Introduction Introduction Hardware features and benefits Software features and benefits 2 User manual 3 Calculation methods 4 Quality control information Warning regarding 1nstallation and warranty OC contents 5 Installation Information Installation MultiCalc installation Installation report for Wallac 1414 WinSpectral Installation report appendix 6 Specifications Safety and Routine maintenance 6 1 Specifications 6 2 Safety and radioacti ve materials 6 3 Routine maintenance 7 Spare parts information 8 Index Contents M 80 o 6 1 6 3 6 5 Trademarks WinSpectral FlexiRack DOT
48. 11 170 1 1411 3402 P FROGRAM PACKAGE SPECTRUM ANALYSIS PRG 180 1 1224 533 PC PROGRAM EASY SCAN 1224 533 180 L0160809 120 1 10860862 KEYBANK ASSEMBLY 1414 10260855 160 Fig 1414 34 Guardian 10861384 96 10 10 FOR PART NUMBER 10861384 GUARDIAN 1414 003 10160809 960404 QTY ORDER NO NAME TYPE MANUF INF LINE 1 10857653 B C ASSEMBLY SW KEY MODULE BOARD RIG 10457652 110 1 10856730 DCD EXPANSION KIT DCD 103564465 121 1 10855272 EXTERNAL STANDARD 10255273 122 1 10861091 STD CAPSULE 10361101 1400 SERIES 123 0 300 10856077 INSTALL KIT 115V FOR 1410 124 0 700 10856078 INSTALL KIT 250V FOR 1410 125 1 10446545 FOOT PAG BLACK 30 GLAS 1215 1470 408 1 10555509 LABEL SET FCi3 FC207 412 1 10556126 LABEL VME RACK 1410 414 1 10551111 LABEL CSA APPROVED ALO 08 LR52500 BRADY 416 1 10560490 LABEL SET 12 DYN 420 0 300 10561102 LABEL WARNING STICK BRADY EU 152 10561102 LAB 422 1 10561348 LABEL PATENTS BRADY LABEL STD B PLATE 428 1 10561614 LABEL 11570078 BRADY CE LABEL 433 1 11310040 CLAMP ACC62 A 586 5 11310037 CLAMP FCC A C8 587 1 1215 111 UND STANDARDS SET 20ML VIALS 3H l C BACK 1215 111 1000 1 1224 513 SOFTWARE PACKAGE 1414 WINSPECTRAL 1224 513 1010 1 1414 932 INSTRUMENT MANUAL FOR 1414 00271414 003 1414 532 1020 1 10990045 QU CERTIFICATE 19390045 1030 1 i 10850804 BODY ASSEMBLY 1414 10160805 10 2 1 10855818 ID UNIT 1410 10355859 11 3 1 10855335 SAMPLE CHANGER L410 10255339 15 4 1 108
49. 11251018 11251045 11251077 11252008 11252019 11271016 11271034 11274013 11274016 11274034 11274145 11274095 11274139 11276022 11250018 10455131 11271036 11278003 10455897 11271095 10556070 10556095 10556071 10456182 11274003 10456382 10556607 10457293 10457300 11276015 11140018 10458898 10458899 16458891 10458887 10358514 10358585 10358888 10448323 10460785 11250039 11274004 11276005 11274010 11310047 11290015 11250936 10858304 11760040 10358501 11278002 11550112 10450803 11276032 10460964 HANDLE 2 BACK PLATE BUSHING INSULATION COVER 1 COVER 2 COVER 3 PLATE FLOPPY DISK DRIVE LABEL LABEL WARNING PLATE LABEL SUPPORT COVER BUSHING SHIELD WASHER WASHER WASHER PIN LOCKRING LOCKE ING RIVET RIVET SCREW SCREW SCREW SCREW SCREW SCREW SCREW SCREW SCREW WASHER COOLING PLATE SCREW NUT PLATE SCREW LABEL LABEL LABEL PLATE SCREW INSULATION LABEL BRACKET GUIDE SCREW SEALING TAPE BRACKET RIGHT BRACKET LEFT BRACKET LEAD SHIELD GUARD LEAD LEAD LEAD SHIELD LEG WASHER SCREW SCREW SCREW MUT BOD WASHER P C ASSEMBLY PHOTOMULTIPLIER LIGHT SEAL NUT INSULATING TAPE COVER PLATE SCREW SHELTER 76 FE PLATE 5 2 1415 FE PLATE 5 1 NTL MS D 20 NTLS SOLUPOLYETHEN AL PLATE 5 2 NTL 5 FE PLATE 5 2 NTL 5 AL PLATE S 2 NFLS 1414 3 5 2 P 80U P500 250KB FD1137H BRADY 1415 AL 99 5 S 1 NTL5 AL PLAT
50. 11800007 11802007 11802009 11802010 11801014 11800009 11830006 11830017 11330009 11845027 11313618 11814011 11784015 10442965 11863069 11782023 11780015 11781006 10953597 11350044 10451435 11350065 113500768 11350077 11350048 11350087 11350683 11350097 11350078 10354388 11862143 11862144 11862132 11862133 11862137 11862130 11562135 11862131 10855315 10555603 11550073 1221 244 10857062 10856281 10856289 10857813 10857820 10856296 10855628 10854502 10855262 11510021 11510022 11550108 1410 921 10857679 10457685 TRANSIS TRANSIS TRANSIS TRANSIS TRANSIS TRANSIS FUSE FUSE FUSE VOLTAGE MICROCIRCUIT LIN OPTICAL DIODE L SERIAL NUMBER TOR PNP TOR FET TOR FET TOR FET TOR NPN TOR PNP SELECTOR SENSOR IGHT EMITT PLAT F C CONNECTOR ZENER DIODE DIODE DIODE B RD BELT P C BOA COGGED COGGED COGGED COGGED COGGED COGGED COGGED COGGED COGGED COGGED GOGGED CONNECT COVER CONNECT CONNECT COVER CONNECT COVER CONNECT RIDGE BELT BELT BELT BELT BELT BELT BELT BELT BELT BELT WHEEL OR OR OR DR OR WIRING ASS LABEL 5 DISK STORAGE BOX PROGRAM SERVICE PROGRAM PROGRAM PROGRAM PROGRAM PROGRAM ET PACKAGE PROGRAM PACKAGE PACKAGE PACKAGE PACKAGE PACKAGE PROGRAM PACKAGE SERVICE PC BOARD EXTRACTOR HEXAGON HEXAGON PLASTIC JUMPER RAM EXTENSION KIT LOCKRIN CONNECTOR
51. 1346 FLAT CABLE 405 405 FC207 10461300 117 wie 1 1085651311 WIRING ASS CA210 120 PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 10857646 LSC ASSEMBLY 10155600 960321 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE DATE 5 1 10854024 HV DIVIDER UNIT HV DIVIBER UNIT 10355373 35 930812 2 10857681 PREAMPLIFIER UNIT 1411 10455334 36 920625 1 10857670 P C ASSEMBLY COINCIDENCE BOARD LAC A 10357727 37 920625 1 10857671 P C ASSEMBLY SAMPLE amp HOLD iCH LAD A 10357728 38 20625 1 10356263 PROGRAM PACKAGE 3410 80186 BIOS ROM 106 911007 35 1 10555672 LABEL AL 99 5 5 1 NTL5 355 911002 36 1 10494512 WARNING PLATE AL PLATE 365 911002 12 1 10855537 DISPLAY UNIT 1410 103555598 115 9403513 18 2 10455331 PLATE FE PLATE 5 3 NTLS 205 940325 1 10555406 LABEL SET Che 409 940525 1 10551111 LABEL AL PLATE 0 2 LRS2506 404 9412143 1 10855451 TOP COVER ASSEMBLY 1410 10255462 45 960122 w24 1 10855508 FLAT CABLE 405 405 FC33 117 951128 Wed 1 10855522 FLAT CABLE 505 505 FCS5 10455666 118 960321 13 1 103555464 FRONT BOX ASSEMBLY NTLS 125 960115 14 1 10355567 SIDE BOX RIGHT FE PLATE S 1 NTL5 135 960115 15 1 10355568 SIDE BOX LEFT FE PLATE S 1 NTL5 145 960115 32 0 500 10455572 PLATE 2 NTLS 325 960313 1 11570078 LABEL THERMAL TRANSFER PRINT THT 5 438 10 404 950508 42 10 11250008 WASHER 4 3 9 0 8 FE YELLOWPASS 415 960115 43 47 50 52 FE 116 57 112 114 300 100 11250010 11251077 11271016 11274013 11274145 11274156 11274133 10556201
52. 160805 960509 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE DATE W11 19 W27 1 10861450 1414 FRAME WIREING 35 960126 59 11 11252007 RIVET 3 2 6 1 MONELL TLP D BS424 195 951128 55 11 11240174 RF GASKET SPRING BeCu 28MM 6MM 97 438 02 320 951128 108 10160805 Fig 1414 35 Body Assembly 109 Fig 1414 36 Top Cover Assembly 10860806 96 10 10 FOR PART NUMBER 10360806 TOP COVER ASS 1414 10260807 960321 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 1 113810265 GAS SPRING 16 1 168 135 60 245 2 1 10350767 PLATE RIGHT ASS 1414 30 3 1 10360763 PLATE LEFT Ass 1414 40 4 1 10260754 SUPPORT PLATE ASS 1414 S 5 2 10455474 FLATE FE S 3 NTL 5 70 7 2 10255475 SUPPORT BL 10x25 NTL 5 80 8 1 10355476 HINGE BODY RIGHT FE PLATE 5 1 5 NTL 5 90 E 1 10355477 HINGE BODY LEFT FE PLATE 5 1 5 NTL 5 100 10 2 10455000 SPRING D NTL 5 110 11 2 10455478 GUIDE D6H8 NTL 5 120 12 2 10455479 FIN POM BLACK D 12 NTL 5 130 13 2 10455480 BRACKET NTL 5 149 14 1 10255481 TOP COVER NTL 5 150 15 1 10254553 COVER 5 NTL 5 160 16 1 10355484 HINGE RIGHT FE FLATE 21 5 NTL 5 170 17 1 10355489 HINGE LEFT FE PLrw a 1 5 NTL 5 180 18 10455490 NUT MS D18 NTL 5 190 19 2 10455491 FIN d2 5 NTL 5 200 20 1 10455492 SUPPORT AL 2X8 2 NTL 5 210 21 1 10460827 FLATE POM BLACK 10455493 1414 220 22 1 10360742 HANDLE FE PLATE 5 1 0 1414 230 24 1 10861714 INSULATION SET 7 CODES 9 PARTS 1400 20 25 2 11250008 WASHER 4 3 9 0 8 FE YELLOWPASS 250 26 12 11250010
53. 2 0 FE PLATE 2 0 3 2 7 0 5 FE YELLOWPASS M 3 6 FE VELLOWPASS POM PLATE 5 8 BLACK M4 8 FE YELLOWPASS M6 16 ST YELLOWPASS ST POLYESTER 11570076 CONNECTION BOARD FE S 1 NICKELIZED FE PLATE S 1 60 6 35x6 35 MONEL GLUE 3 2X4 8 MONEL C 2 9 9 5 FE YELLOWPASS PVC FASKAL 400 T 0 1 FE PLATE T 1 NTLS NTL5 1410 WARNING 1410 CR 1410 PROGRAM CR LSC 5 NTL 5 NOTE LSC LST 10255679 1409 11 15 1409 11 15 14 08 6040 1414 10460712 1414 1414 NTL 5 MACH LABEL 1414 001 RGE 10461408 1414 01 0901 6603 01 0901 6601 1414 1410 RESET 1409 210 230 240 250 265 275 285 295 305 306 148 425 149 415 423 421 375 355 395 403 430 431 435 445 455 465 475 485 495 565 515 525 535 545 555 565 434 325 510 585 327 511 417 418 413 404 514 403 413 328 329 575 119 400 401 440 513 590 426 120 159 151 432 966 402 490 530 411 114 350 340 600 610 360 570 428 355 102560807 23 l 105600657 COVER PLATE POLYCARB 0 375 1414 410 10260807 37 1 11570061 LABEL WALLAC 52X22 16STICKER 424 10355819 17 1 10355762 ID EHIELD FE PLATE Sct NTL 5 495 10355815 43 1 10457903 PLATE ST PLATE T 1 5 1410 495 10355819 44 1 10357902 SUPPORT RST T 0 8 1419 407 Wi 4 1 10861346 FLAT CABLE dos dos FC207 10461300 LL Wiz 1 10561411 WIRING ASS CA210 115 PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 10
54. 20 SUPPORT NTLS 171 36 l 10355112 LEAD LEAD 99 9 NTL 5 172 37 4 11251818 FIN 3 20 ST All 38 4 11250015 WASHER 8 4 17 1 6 FE YELLOWPASS 181 39 4 11274126 SCREW FE YELLONPASS 251 do 3 11271016 SCHEW HM 3 4 FE YELLOWPASS 229 di 1 10855115 POWER UNIT 10255116 42 1 10855133 POWER RACK 27 44 1 10855187 VME RACE el 44 1 11590045 FAN Z2AVDC SW 800FPM 4314 360 45 1 11690040 FINGER GUARD 105x105 MM 9 601 43 370 46 12 11274015 SCREW M 5 15 FE YELLOWPASS 251 47 d 11250001 WASHER Ai 2 t76 de 4 11271025 SCREW M 3 16 YELLOWPASZ 228 49 4 11278002 NUT M3 FE YELLOWPASE 289 zT 4 10455327 BUSHIMG POM ROD D10 BLACK NTL5 166 51 2 10455338 BRACKET FE PLATE 5 1 NTL 5 151 5d 1 11274030 SCREW M FE YELLOWPASS 286 1 11480047 FERRITE CLAMP D 6 6 MM 28B2025 0OAQ 410 57 1 1148380048 FERRITE CLAME D 1i MM 2 8B2024 0A0 420 R 2 11480052 FERRITE CLAMP A0 WIRE FLAT CABLE 2SB2001 000 59 z 11480043 FERRITE CLAMP A6 WNIFE FLAT CABLE 28B2022 000 405 5 U 4 11480050 CLAMP FOR 246 W FLAT C CLAPM M CLIP 430 51 1 10452059 INSULATOR TEFL N PLATE T 1 173 TR 1 11650053 TRANSFORMER fa SKU 0 45VA 310 WL1 1 1 10858057 1410 FRAME WIREING CA 23 30 SYT 35 wed W21 We 3 10855441 FLAT CABLE 265 2 265 19 N23 1 10853250 FLATCABLE d0s 2x343 10453252 O MAT 1 10861347 WIRING ASS CAZUS 15 930 1 105856412 WIRING ASS CAST 26 107 PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 10860804 BODY ASSEMBLY 1414 10
55. 251071 LOCK WIRE FOR D 28 AXLE RW 28 145 920207 M 1 11690049 STEPPING MOTOR 12V 0 44 1 8AST 0 26NM 5500 15 4 13 5 190 911213 Fig 1409 1410 1411 14 Light Shutter Unit 10354823 10 35 4823 Pirt 68108 TMS Tark 881108 Ma Hyv 881108 Z 45 a Fig 1409 1410 1411 15 Motor Unit 1 10855064 96 10 10 FOR PART NUMBER 10855064 MOTOR UNIT 1 10355065 941026 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 1 10255066 MOUNTING BRACKET FE PLATE 522 5 NTL5 10 l 10455067 AXLE D6HB NTL5 20 3 1 10353799 COGGED BELT WHEEL PA6 30 MINERAL 1237 30 2 10353761 COGGED BELT WHEEL PA6 30 MINERAL 1297 40 5 1 10357482 COGGED BELT WHEEL z 28 NTL gt 50 amp 2 10354388 GOGGED BELT WHEEL GRILON W 5239 1297 60 7 2 104548357 PLATE FE PLATE 5 2 1409 1235 1297 70 8 1 11350098 COG WHEEL 710 565 10 a0 9 1 10455068 AXLE 6 HTL5 90 10 1 10455069 BEARING HOUSE 6K14 NTLS 100 il l 11350073 JOURNAL BEARING GLYCODUR PG 060810 F 110 12 3 11350072 JOURNAL BEARING GLYCODUR PBG 060804 F 120 13 11250008 WASHER 4 379 0 8 FE YELLOWPASS 150 14 8 11274007 SCREW M4712 FE YELLOWPASS 160 15 1 11275008 SCREW M4 6 AISI316 170 i 1 11275007 SCREW M d 4 180 17 1 11278015 NUT M12 FE YELLOWPASS 190 18 2 10553537 P C BOAED 1 6MM 2 P EP LK RRA 1205 1470 220 19 4 11320106 LOCK CARD SPACER NYLON EGLS 35 230 20 1 11350078 COGGED BELT SYNCHROFLEX 6 T2 5 120 130 31 1 11350077 COGGED BELT SYNCHROPLEX 10 T2 5 160 140 22 2 11251037 GRIP RING FOR D6 AXLE G
56. 30 DCD EXPANSION KIT DCD 10356455 50 1 10857553 P C ASSEMBLY SW KEY MODULE BOARD EJG 10457852 60 1 10855233 P C ASSEMBLY SENSOR BOARD EXC 10455232 100 1 10857618 PROGRAM PACKAGE MAIN FR 1409 11 LSC WALLAC 1400 DSA 110 1 1411 932 INSTRUMENT MANUAL FOR 1409 1411 1411 932 120 1 10990045 CERTIFICATE 10990045 130 10155600 34 1 l0557601 LABEL 1409 AL 5 0 5 30 10255462 23 1 10457957 SUPPORT ST D 16 1408 10 102554152 231 1 10357612 COVER PLATE POLYCARBLO 375 140 20 10255452 37 1 11570061 LABEL WAnLAC 52X22 16 STICKER 35 PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 10857647 LSC 1409 001 930813 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE DATE 10155600 75 1 11570061 LABEL WALLAC 52X22 16 STICKER 35 330315 d 10855393 FREAMFLIFIER UNIT 1410 10455394 60 911030 1 108547345 P C AS5EMBLY COINCIDENCE BOARD LAC 10354734 70 911030 1 10855551 F C ASSEMELYT SAMPLE k HOLD 10H LAD 10354773 BO 911030 LSC Model 1410 001 10857648 96 10 10 FOR PART NUMBER 10857648 LSC 1410 001 920602 ITEM NO GTY ORDER NO NAME TYPE MANUF INF LINE 1 10446545 FOOT PAG BLACK 30 GLAS 1215 1470 10 1 10857679 RAM EXTENSION KIT DIE RAM 10354603 40 1 10857646 LSC ASS 14097141071411 10155600 50 1 10855272 EXTERNAL STANDARD 1025527 60 1 10855258 STD CAPSULE 10455269 NTL5 70 1 10855620 PROGRAM PACKAGE 1410 LEC INSTRUMENT PROGRAM 110 1 1410 931 INSTRUMENT MANUAL FOR 1410 1410 431 120 1 10555672 LABEL AL 99 5 5 1 NTLS 130 1 10434512 WARMING PLATE AL PLATE
57. 4 ASA 130 7 2 11320106 LOCKE CARD SPACER NYLON EGLS 35 120 B 3 11271018 SCREW HM 3 6 FE YELLOWPASS 1760 3 5 11271019 SCREW M 3 8 FE YELLOWPASS 150 19 3 11271023 SCREW M 3 14 FE YELLOWPASE 150 11 B 11278002 NUT M3 FE YELLOWPASS 140 12 1 10556568 LABEL WHITE Z5ELF ADHESIVE L HV OUTPUT INPUT 220 13 2 11480047 FERRITE CLAMP D 6 6 MM 28B82025 0A0 115 14 4 11273013 SCREW M2 5 4 FE BLACK 135 15 l 10461951 INSULATOR PLATE PRESPAN S 0 5 280 ci 1 11626002 CAPACITOR H Y 2 5NF 3KV DD30 252 50 Ca 5 4 11626008 CAPACITOR H Y 150PF 3 0KV 20 50 9 0130 6 D FERROP AQ R1 1 11601149 RESISTOR 10K 2 0 5W B 1 2 BEYSCHLAG 166 R2 1 11604045 RESISTOR MF SM 100 1 0 125W 100PPM CRCW1205 90 R3 7 10 14 20 11664241 RESISTOR MF SM 1 00M 1 0 125W 100PPM CRCW1206 60 17 21 24 28 RB 15 22 29 4 11604225 RESISTOR MF SM 464K 1 0 125W 100PEM CRCW12 06 70 R9 16 23 30 4 11603858 HY RESISTOR 24Mohm 5 0 5 3 5kKVDC 232224213225 95 R31 34 4 11604208 RESISTOR MF SH 215K 1 0 125W 100PPM CRCW12068 BO 51 8 1 111 11863070 P C CONNECTOR 40 PIN STRAIGHT 11 25 36G 20 64 69 IB 154 10 35 5373 B Piirt 881107 GUS Tark 881107 Hyv 881107 Ze HUN 1SPIAIG AH EZ LEvE OLbL 60r1 big ELESSEOL 66 Fig 1410 24 Display Unit 10855597 96 10 10 FOR PART NUMBER 10855597 DISPLAY UNIT 10355598 940516 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 1 10854665 P c ASSEMBLY DISPLAY HDG 10254761 10 2 i 10854760 P C ASSEM
58. 4 WASHER A6 4 ZN 309 49 1 10457125 BUSHING POM 1410 201 50 1 10460571 SPRING SPRINGBRONZE S 0 NTL 5 225 K 1 11863089 P C CONNECTOR 5 P STRAIGHT LOCKABLE MLSS100 5B 490 M 1 11590042 STEPPING MOTOR BV 1A 1 8AST 0 4NM PH265 04 480 PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 10855272 EXTERNAL STANDARD 10255273 041216 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE DATE 6 1 10455275 FLATE FE PLATE 2 0 NTL5 60 930115 22 1 10455288 SPRING SPRING PRONZE 220 5 NTLS 420 940510 27 1 10455310 LABEL AL FLATE 5 1 NTLS 270 941215 34 Fig 1409 1410 1411 09 External Standard 10255273 x E Ti o e 338 o Fr a a Fig 1409 1410 1411 10 Measuring Unit 10854849 96 10 10 FOR PART NUMBER 10854849 MEASURING UNIT 10354850 950522 ITEM NO QTY ORDER N NAME TYPE MANUF INF LINE 1 10855189 ANALOG RACK 1410 4 1 10854767 P ASSEMBLY MCA INTERFACE 1CH LER 10354766 45 1 10854652 P C ASSEMBLY HV SUPPLY EPM A 10354653 47 0 150 11240068 CONNECTING WIRE 1 0 20 MM2 GREEN TPF 61507 150 0 150 11240071 CONNECTING WIRE 1 0 20 MM BLACK TPF 01507 160 0 150 11240067 CONNECTING WIRE 1 0 20 MM2 YELLOW TFF 01507 170 0 150 11240072 CONNECTING WIRE 1 0 20 WHITE TPF 01507 180 1 10560490 LABEL SET CA22 12 DYN 200 1 1 10859277 OPTECS 1415 10356123 20 2 1 10854789 COUNT WEIGHT 10454790 30 3 2 10860160 PREAMPLIFIER UNIT 1409 11 15 12 DYNGDE 10455394 40 4 2 10454039 LIGHT SEAL SILICON BLACK NTLS 90 6 1 10357670 P C ASSEMB
59. 4 kg Guardian Power Mains voltage selectable 100 115 120 220 and 240 V 10 50 60 Hz Power consumption is 200 VA without the temperature control umt and 300 VA with it Standby power supply Power failure recovery and protection by back up standby power supply provided with NiCd accumula tors In the case of power failure the status of the counting process will be stored on diskette thus pro viding effectively an unlimited standby time for recov ery from power failure Input output connections Serial ASCII interface RS 232C Two output termi nals port 1 for printer port 2 for laboratory PC Radiation shield Low specific activity lead around detector assembly and external standard rest position Weight 103 kg WinSpectral 135 kg WinSpectral B 128 kg Guardian thickness at least 48 mm around the meas uring chamber Operating conditions Temperature 415 to 435 C Humidity max 75 FlexiRack sample changer and conveyor Sample capacity varies from 336 to 1248 vials de pending on the used rack combination When using only standard vial racks 336 samples in 28 racks of 12 samples each With minivial racks 720 samples in 40 6 1 Specifications racks of 18 samples each With small mini microvial racks 1248 samples in 52 racks of 24 samples each Rack transport by friction belt drive system transverse movement by toothed chain driven by electric motors Sample lifted up to measuring chamber by
60. 4314 230 24 1 11690040 FINGER GUARD 105x105MM 9 601 43 240 25 1 11690046 FAN 24VDC 2 2W 3300RPM 8314 250 26 26 11250008 WASHER 4 3 9 0 8 FE YELLOWPASS 250 27 3 11250021 SERRAT LOCK WASHER 3 0 ANNEALED YELLOWPASS 3 2 5 5 0 45 270 28 3 11271019 SCREW M3 8 FE YELLOWPASS 280 29 4 11271053 SCREW H4 E FE YELLOWPASS 290 30 2 11271057 SCREW M4 16 FE YELLOWPASS 300 31 14 11274006 SCREW M4 10 FE YELLOWPASS 410 32 11274072 SCREW M4 16 FE YELLOWPASS 320 33 8 11274009 SCREW M4 20 FE YELLOWPASS 330 34 4 11274142 SCREW M4 40 AISI 316 ACID PROOF 340 35 10 11276015 SCREW B2 9 6 5 FE YELLOWPASS 350 36 14 11278003 NUT Md FE YELLOWPASS 360 37 2 11814502 PTC SENSOR 1000R 25AST C 2 ETY8R1 120 191 38 2 11605034 RESISTOR Ww 10R 5 50W HSA50 1 2 39 1 11310031 CLAMP A3031ASA 380 Weg 1 10856411 WIRING ASS CA50 06 70 10156322 Fig 1409 1410 1411 25 Thermostat Unit 71 72 10 15 6322 Tark 891010 MYa Hyu 891010 A Ho 1415 Supplement 73 74 96 10 10 FOR PART NUMBER 1415 001 LSC 1415 001 951004 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 10858924 LSC 1415 001 10155600 10 1 1410 405 SAMPLE TRAY FOR SAMPLE RACKS 1410 405 20 1 1409 411 ID KIT 1409 411 30 0 500 1200 437 OPTIPHASE 3 2X5 L 1200 437 40 1 1224 313 MULTICALC EDITOR 1224 313 SO 1 1224 512 PC PROGRAM 1400 DSA WIW 1224 512 60 1 10859610 PACKAGE 1415 10459611 100 Fig 1415 26 LSC Assembly 10858924 96 10 10 FOR PART NUMBER 10
61. 455723 16455797 11256008 11250010 11350019 11251018 11251045 11251077 11252008 11252019 11271016 11271034 11274013 11274016 11274034 11274145 11274095 11274139 11250018 30455131 11271036 11278003 10455897 11271055 10556070 10556055 10556071 10456182 11274003 19456382 10556607 10457299 10457300 11276015 10866710 10458898 10458839 10458891 10458567 10358359 10353388 10448323 11250039 11274004 11276005 TOP COVER ASSEMBLY P C ASSEMBLY P C ASSEMBLY F C ASSEMBLY P C ASSEMBLY P C ASSEMBLY FRONT PANEL RIGHT BOX ASSEMBLY SIDE BOX RIGHT SIDE BOX LEFT FRONT PLATE LEFT CAM GUIDE PLATE BUSHING PLATE LEAD LEAD LEAD HANDLE 2 BACK PLATE BUSHING INSULAT TON COVER 1 COVER 2 COVER 3 LID ASSEMBLY FLOPPY DISK DRIVE HANDLE LABEL WARNING PLATE LABEL SUPPORT COVER BUSHING SHIELD WASHER WASHER WASHER PIN LOCKRING LOCKRING RIVET RIVET SUREW SCREW SCREW SCREW SCREW SCREW SCREW SCREW WASHER COOLING PLATE SCREW NUT PLATE SCREW LABEL LABEL LABEL PLATE SCREW INSULATION LABEL BRACKET GUIDE SCREW RESET UNIT BRACKET RIGHT BRACKET LEFT RRACKET LEAD SHIELD LEAD LEAD LEAD SHIELD WASHER SCREW SCREW 100 l l4 MICRO COMPUTER I O BOARD MCA POWER SUPPLY MOTOR CONTROL BOARD FE PLATE FE PLATE sel S 1 B25 FE PLATE 5 3 D12 FE PLATE 5 3 CAST LEAD CAST LEAD CAST LEAD FE PLATE 2 FE FLATE S 1
62. 495 305 515 525 535 245 555 565 575 585 444 336 520 595 337 531 416 417 418 420 524 421 423 338 339 586 598 400 401 411 246 40 247 248 250 412 587 588 589 590 500 601 602 110 115 117 594 635 630 640 033 116 2 11271053 SCREW FE YELLOWPASS 648 117 0 100 10361270 PB PLATE PB 99 6 NICKELIZED 1400 SERIE 252 118 1 10861410 PLC ASSEMBLY CONNECTION BOARD EGE 10461408 i12 115 2 11274156 SCREW Mo6 I6 ST YELLOWPASS 556 120 1 10460762 PLATE RIGHT FE PLATE 5 2 0 1414 680 121 1 10460761 PLATE LEFT FE PLATE S 2 0 1414 690 122 4 11274002 SCREW M 3 5 FE YELLOWPASS 123 2 10461276 HOLDER FE PLATE 52 NICKELIZED 710 124 1 15461414 SUPPORT 1 FE PLATE S 1 0 1414 720 125 2 700 11240173 RF GASKET 6 35x6 35 MONEL GLUE 01 0901 6603 730 126 1 800 11240162 RF GASKET 3 2X4 8 MONEL 01 0901 6601 740 127 1 10461613 HOLDER FE PLATE P 1 1409 725 10255462 37 1 11570061 LABEL WALLAC 52X22 165TICKER 350 LO255462 23 1 10358600 COVER PLATE POLYCARBON S 0 375 1415 352 10355819 43 1 10457903 PLATE ST PLATE T 1 5 1410 22 10355819 44 L 10357902 SUPPORT RST T 0 8 1410 23 1035581 17 1 10355762 ID SHIELD FE PLATE 2 2 NTL 5 645 W24 1 10861346 FLAT CABLE 409 405 FC207 10461700 127 Wa 6 1 10855592 FLAT CABLE 505 505 FC35 10455666 128 932 1 10861411 WIRING ASS CA210 130 PART HISTORY FHOM 91 09 25 TO 96 10 10 FOR PART NUMBER 10858924 LSC 1415 001 10155600 960314 ITEM NO QTY ORDER N NAME TYPE
63. 59278 MEASURING UNIT 1415 19354850 25 1 10859369 P C ASSEMBLY HV DIVIDER UNIT RFA1O399368 10355373 35 6 1 10860806 TOP COVER ASSEMBLY 1414 10250807 45 7 1 10856466 P C ASSEMBLY MICRO COMPUTER DCD 10356465 55 1 10854884 P C ASSEMBLY I O BOARD DIC 10354883 65 El 1 10854606 P C ASSEMBLY MCA DIE 10354603 75 10 1 10853316 P C ASSEMBLY POWER SUPPLY DPA 10353503 85 11 2 10854021 P C ASEEMBLY MOTOR CONTROL BOARD HPS 10354022 95 12 1 10360749 FRONT PANEL RIGHT 1414 146 13 1 10361369 BOX ASSEMBLY 1414 130 14 1 10360774 SIDE BOX RIGHT FE PLATE S 1 9 1414 135 15 1 10360773 SIDE BOX LEFT FE PLATE S 1 0 1414 145 16 1 10360752 FRONT FLATE LEFT 1414 147 17 2 10455328 CAM O25 NTLS 175 18 2 104588906 GUIDE PLATE FE PLATE 5 1415 205 19 1 10455330 BUSHING D12 NTL5 1470 195 20 2 10455329 PLATE FE PLATE 5 3 NTLS 185 21 1 10358884 LEAD CAST LEAD 1415 214 22 2 10358885 LEAD CAST LEAD 1415 230 23 2 10358886 LEAD CAST LEAD 1415 240 24 1 1045889 HANDLE 2 FE PLATE 5 2 1415 250 25 1 10255612 BACK PLATE FE PLATE 5 1 NTLS 265 102 28 27 28 29 30 32 33 34 35 36 47 38 39 40 41 42 43 44 45 46 47 48 49 50 51 53 54 55 25 E 59 60 61 62 53 64 65 67 65 H0 Yi 72 73 74 75 TB FA 78 73 50 el B2 83 101 102 103 104 105 106 108 103 110 111 115 116 117 118 113 122 123 124 i25 H P P W a E EJ p i Lr vu be bi um b BEDS lt FE m
64. 6 45 K 2 118963089 P C CONNECTOR 5 P STRAIGHT LOCKABLE MLS5S100 5B 240 MI M2 2 11690042 STEPPING MOTOR 5V 1A 1 8AST 0 6500 20 4 4 8 R416 215 PART HISTORY FROM 91 09 25 96 10 10 FOR PART NUMBER 10855064 MOTOR UNIT 1 10355065 941026 ITEM NO Ory ORDER NO NAME TYPE MANUF INF LINE DATE M1 1 11690043 STEPPING MOTOR SY 1 54 1 8AST 0 835NM PH268 21 210 920212 M2 1 11690042 STEPPING MOTOR 5V 14 1 8AST 0 4NM PH265 04 215 920211 Fig 1409 1410 1411 15 Motor Unit 1 Tsa 224 8408 52 e e 1885 9006914 E 1890 901104 AG 47 10355065 Q x S EN a 88 2 ES o rer a Fig 1409 1410 1411 16 Motor Unit 2 10855070 96 10 10 FOR PART NUMBER 10855070 MOTOR UNIT 2 10355071 941026 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 1 10255066 MOUNTING BRACKET FE PLATE 2 5 NTLS 10 2 1 10455087 AXLE D6H8 NTL5 20 3 1 10353799 COGGED BELT WHEEL PA6 30 MINERAL 1297 30 4 z 10353761 COGGED BELT WHEEL PAG 30 MINERAL 1297 40 5 2 10354188 GOGGED BELT WHEEL GRILON W 5239 1297 5n 6 2 10454867 PLATE FE PLATE 5 2 1409 1235 1297 60 7 1 11350098 COG WHEEL 210 S6 10 70 B 1 10455068 AXLE DEHE NTL5 80 g 1 19455069 HEARING HOUSE 6K14 NTLS 90 10 1 11350073 JOURNAL BEARING GLYCODUR PG 060810 F 100 il 3 11350072 JOURNAL BEARING GLYCODUR PBG 060804 F 110 12 8 11250008 WASHER 4 3 9 0 8 FE YELLOWPASS 140 13 B 11274007 SCREW M4 12 FE YELLOWPASS 150 14 1 11275007 SCREW M4 5 160 15 1 11251037 GRIF RING FOR D6 AXLE G6 17
65. 61102 LAB 422 1 10561348 LABEL PATENTS ERADY LABEL STD B PLATE 427 1 10561614 LABEL 11570078 BRADY CE LABEL 429 1 11310040 CLAMP ACCH2 A 586 5 11310037 CLAMP FOC A C8 587 1 1215 111 ONO STANDARDS SET 20ML VIALS 3H l4C BACK 1215 111 1000 1 1224 513 SOFTWARE PACKAGE 1414 WINSPECTRAL 1224 513 1010 1 1414 932 INSTRUMENT MANUAL FOR 1414 002 1414 003 1414 932 1020 1 10990045 CERTIFICATE 10990045 1050 1 1 10860804 BODY ASSEMBLY 1414 10160605 10 2 1 10855818 ID UNIT 1410 10355859 11 3 1 10855338 SAMPLE CHANGER 1410 10255339 15 1 10859278 MEASURING UNIT 1415 10354850 25 D 1 10859369 P C ASSEMBLY HV DIVIDER UNIT RFA1O359368 10355373 35 99 6 1 7 1 8 i 9 1 10 1 11 2 12 1 13 1 14 1 15 1 16 1 17 2 18 2 19 H 20 2 21 1 22 2 23 2 24 1 25 1 26 4 27 1 28 1 29 1 30 1 32 1 33 1 34 i 35 1 36 1 37 1 38 1 39 1 40 1 41 2 42 15 43 10 44 1 45 26 46 4 47 4 48 2 49 8 50 6 51 4 52 10 53 2 54 2 55 6 56 1 27 10 59 3 60 a 61 8 62 8 63 1 64 2 65 1 55 1 67 1 68 1 69 2 1 71 1 72 2 73 1 74 2 75 1 76 1 77 1 78 1 79 1 81 1 82 1 83 1 101 4 102 12 103 10860806 10856466 10854884 10854606 10853318 10854021 10360749 103613649 10360774 10360773 10360752 10455328 10458599 10455330 10455329 10358884 10358885 10358886 10458893 10255612 10455616 10355617 10355618 10455632 10355742 10360744 11710021 104652743 10555672 10494512 10548122 10355677 10355686 15
66. 64 65 66 67 68 70 71 72 73 74 75 76 77 161 102 105 106 115 116 117 118 115 122 123 124 126 141 142 143 144 145 146 147 148 149 Meeme ee ee a ro xn Ha co O bJ am E y t C PANE Hat blto iS tor biti FPREENHE m po st O HI t3 bd bg Fr CE EI DB 10355332 10455333 10455334 10355335 10255612 10455616 10355617 10355618 10455632 10355742 10360744 11710021 10460743 10555672 10494512 10548122 10355677 10355686 10455723 10455797 11250008 11250010 11250018 11251018 11251045 11251077 11252008 11252015 112710168 11271034 11274013 11274016 11274034 11274145 11274095 11274139 11250018 10455131 11271036 11278003 16455897 11271095 10556070 10556095 10556071 10456182 11274003 10456382 10556607 10457299 10457300 11276015 10860710 10458898 10458899 11250039 11274004 11310047 11290015 10660713 10460762 10460761 11250006 11274002 10460564 11271053 11274156 10560656 10861410 10461276 10461414 11240173 11240162 10461480 11276022 10557386 10461613 LEAD LEAD LEAD HANDLE 1 BACK PLATE BUSHING INSULATION COVER 1 COVER 2 COVER 3 LID ASSEMBLY FLOPPY DISK DRIVE HANDLE LABEL WARNING PLATE LABEL SUPPORT COVER BUSHING SHIELD WASHER WASHER WASHER PIN LOCKRING LOCKRING RIVET RIVET SCREW SCREW SCREW SCREW SCREW SCREW SCREW SCREW WASHER COOLING PLATE
67. 8 MONEL 01 0901 6601 630 15 1 10385162 LID ASSEMBLY TIN COVERED NTL 5 640 16 1 10361690 BOX ASSEMBLY TIN COVERED NTL 5 550 17 2 10461689 BUSHING MS NTL 5 660 18 S 11276015 SCREW C 2 9 6 5 FE YELLOWPASS 670 13 6 11271021 SCREW M 3 10 FE YELLOWPASS 680 20 E 11271026 SCREW M 3 18 FE YELLOWPASS 690 21 8 11250044 WASHER 3 2 9 0 8 FE YELLOWPASS 22 1 31271018 SCREW M 336 FE YELLOWPASS 710 23 2 11250006 WASHER 3 2 7 0 5 YELLOWPASS 720 24 1 10861635 P C ASSEMBLY FILTER BOARD RXP 10461634 525 25 1 10861638 P C ASSEMBLY FILTER BOARD RYO 10461637 535 26 0 050 11180017 PE STRING 5 5 BLACK P2 940 SJH 730 27 1 10453497 INSULATOR PLATE PRES PAN S 0 5 1205 740 28 0 850 1122001d TAPE 12MM CLEAR TESA4S S71 750 W25 1 10851794 FLAT CABLE 268 268 10451797 530 W26 1 10855592 FLAT CABLE 505 505 FOSS 10455666 533 W33 1 10861704 FLAT CABLE 345 345 FC220 10461703 537 PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 10859287 DISPLAY UNIT 1415 10355598 950612 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE DATE 1 10655628 PROGRAM PACKAGE DISPLAY PRG HCB BOARD 521 930825 7 5 11271030 SCREW M3 35 FE YELLOWPASS 580 940465 Wl 1 10851794 FLAT CABLE 265 265 10451797 530 960213 5 5 10455619 BUSHING MS D6 4 NTL5 60 960115 7 11271030 SCREW M 3 35 FE YELLOWPASS 580 960115 11 1 11271029 SCREW M 3 30 YELLOWPASS 585 960115 g 12 11278002 NUT M3 FE YELLOWPASS 590 960112 10355598 Fig 1415 33 Display Uni MH LOZDUB AAH DAW LOo2088 MV S
68. 858924 LSC 1415 001 10155600 960314 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 10855272 EXTERNAL STANDARD 10255273 15 1 10861091 STD CAPSULE 10361101 1400 SERIES 20 i 10857653 P C ASSEMBLY SW KEY MODULE BOARD RIG 10457652 90 1 10856730 DCD EXPANSION KIT DCD 10356465 100 1 1215 111 UNO STANDARDS SET Z0ML VIALS 3H l4C BACK 1215 111 120 1 10446545 FOOT PAG BLACK 30 GLAS 1215 1470 410 1 10551111 LABEL CSA APPROVED ALO 0B LR52500 BRADY 414 1 10560490 LABEL SET CA22 12 DYN 419 1 10555509 LABEL SET FC33 FC207 422 1 10556126 LABEL VME RACK 1410 424 1 10561348 LAPEL PATENTS BRADY LABEL STD B PLATE 128 1 10561614 LABEL 11570078 BRADY CE LABEL 429 1 11310040 CLAMP ACC6Z A 596 5 11310037 CLAMP POC A CB 597 0 300 10561102 LABEL WARNING STICK BRADY EU 152 10561102 LAB 605 0 300 10856077 INSTALL KIT 115 FOR 1410 B15 1 10857616 PROGRAM PACKAGE MAIN PR 1409 11 LSC WALLAC 1400 DSA 620 1 10857810 PROGRAM PACKAGE COMM PROTOCOLS 1409 11 1409 11715 622 0 760 10856076 INSTALL KIT 250 FOR 1410 625 1 1411 932 INSTRUMENT MANUAL FOR 14551311 1411 532 650 1 16930045 OC CERTIFICATE 10990045 660 1 11560029 MOUSE MAT 154 244 670 1 1 10854518 BODY ASSEMBLY 1410 10154917 10 2 1 10855813 ID UNIT 1410 10355559 2l j 1 10855334 SAMPLE CHANGER 1410 10255339 25 4 1 10859278 MEASURING UNIT 1415 10354820 35 5 1 10859369 P C ASSEMBLY HV DIVIDER UNIT RFAI103233525 103255273 45 6 i 10861712 TOP COVER ASSEMBLY 1415 10255462 55 7 1 10856466 P C ASSEMBLY MICRO COMP
69. 860578 WINSPECTRAL 1414 001 10160809 960404 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE DATE 147 4 11276022 SCREW C 2 89 9 5 FE YELLOWPASS 570 960403 6 10 10 FOR PART NUMBER 1414 002 ALPHA BETA 1414 002 960620 ITEM NO QTY ORDER NAME TYPE MANUF INF LINE 1 10851383 ALFABETA 1414 002 101608053 10 1 1410 405 SAMPLE TRAY FOR SAMPLE RACKS 1410 405 110 1 1410 461 RACKS 20 ML PACKAGE OF 10 RACKS 1410 40 120 1 1409 411 ID ELIT 1409 411 130 0 500 12400 437 OPTIPHASE HISAFE 3 4245 L 1200 437 140 1 1414 166 MONITOR STAND MM 230 MM 150 1 10859610 PACKAGE 1415 10459611 170 1 1411 302 PC PROGRAM PACKAGE SPECTROM ANALYSIS PRG 180 1 1224 533 PC PROGRAM EASY SCAN 1224 511 190 10160809 120 1 10860552 KEYEANK ASSEMBLY 1414 10250855 160 Fig 1414 34 Alpha Beta 10861383 96 10 10 FOR PART NUMBER 10861383 ALPHA BETA 1414 002 10160809 960404 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 10857653 P C ASSEMBLY SW KEY MODULE BOARD RJG 10457652 110 1 10856730 DCO EXPANSION KIT DCD 10356455 121 1 10855272 EXTERNAL STANDARD 10255273 132 1 10861091 STB CAPSULE 10361101 1400 SERIES 123 0 300 10855077 INSTALL KIT 115v FOR 1410 124 0 700 10856078 INSTALL KIT 250V FOR 1410 125 l 10446545 FOOT PAG ELACK 30 GLAS 1215 1470 408 1 10555509 LABEL SET FC207 412 1 10556126 LABEL VME RACK 1410 414 1 10551111 LABEL CSA APPROVED ALO 08 LR52500 BRADY 415 i 10560490 LABEL SET CAZ2 12 DYM 420 0 300 10561102 LABEL WARNING STICK BRADY EU 152 105
70. 924 LID NTL5 BL 7 4 10454925 GUIDE ASSEMBLY NTLS 1470 1460 70 8 4 10454928 TUBE ASSEMBLY NTL5 1470 14650 9 10354931 SUPPORT FE FLATE S 1 5 WTLS 20 lU 1 10454932 BOX ASSEMBLY NTL5 100 i 1 10354935 SUPFORT RIGHT NTL 110 12 1 10354940 SUPPORT LEFT NTL5 120 13 4 10454941 ADJUSTER NUT 614 NTL5 1470 130 14 11275024 SCREW HEYD 140 it 2 10454943 BRACKET ASSEMBLY NTLS L50 16 4 10446545 POT PAG BLACK 30 GLAS 1213 1470 150 AT A 11250010 WASHER 2 3 10 1 FE YELLOWPASS 170 1 14 11250018 WASHER 35 23 15 1 6 FE YELLOWPASS 180 13 14 11252012 RIVET gt 2 7 4 MONELL TLP D BS 429 190 at az 11252002 RIVET 2 2 3 1 MONELL TLP D BS435 200 21 20 11260010 RIVETED MUT MS 2 0 3 0 MS 3182582RIV T 210 22 4 11274004 SCREW M 4 6 FE YELLOWPASS 420 23 8 11274012 SCREW M 3 10 FE TELLOWPASS 230 2 4 11274013 SCREW M 5 12 FE YELLOWPASS 240 25 11274016 SCREW M 5 20 FE YELLOWPASS 250 2b 2 11274031 SCREW M 5 12 FE YELLOWPASS 260 27 1 11274136 SCREW M8 40 YELLOWPASS 270 28 3 11278011 NUT M FE YELLOWPASS 251 23 4 11278026 NOT M5 NYLOC 290 30 4 10455004 BUSHING POM BLACK LD l5 NTL5 155 il 8 11350004 WASHER A6 4 ZN 165 32 11274076 SCREW M6 16 FE YELLOWPASS 215 33 1 10854387 INSULATION SET 11 CODES 13 PARTS NTLS 18 34 L 10855506 P C ASSEMBLY ICNIZER RRI 11 35 1 10355320 SUPPORT NTLS 151i 36 1 10355113 LEAD LEAD 99 9 NTL 5 1852 37 4 11251018 PIN 3 20 ST 201 38 4 11250015 WASHER 8 4 17 1 6 FE YELLOWPASS 171 39 4 11274126 SCREW M5 35 FE YELLOWPAS
71. AG 430 12 11601177 RESISTOR 1 5M 2 0 5W B 1 2 BEYSCHLAG 440 12 11601178 RESISTOR 2 2M 2 D 5W B 1 2 BEYSCHLAG 450 12 11601179 RESISTOR 3 2M 2 D B5W B 1 2 BEYSCHLAG 460 12 11601180 RESISTOR 4 7M 2 0 Ov B l 2 BEYSCHLAG 470 1 11556051 SHIELDING BAG 125 200 MAPOSTAT 480 0 060 11550159 INSULATION MS PU JE 40110 490 2 11810160 MICROCIRCUIT TTL QUAD BUS LINE DRIVER N74F244N 500 2 11816131 MICROCIRCUIT TTL QUAD 2 INP MUX SN74155157N 510 2 11811048 MICROCIRCUIT C MOS OCTAL BUS TRANSCEIVER FC74HCT245P 520 2 11811047 MICROCIRCUIT C MOZ OCTAL D TYPE LATCH PCTJHCT3731P 530 2 11811050 MICROCIRCUIT C MOS OCTAL D TYFE FLIP FLOP PC74HCT374P 540 3 11811051 MICROCIRCUIT C MOS HEX INV SCHMITT TRIGG MC 4HCTL4AN n50 a 11512024 MICROCIRCUIT LIN QUAD OPER AMPL CA 324 E 560 2 11815038 MICROCIRCUIT LIN QUAD JFET INP OF AMPL TLOS4EN 570 11813033 MICROCIRCUIT LIN OPERATIONAL AMPL LF356N 580 2 11813025 MICROCIRCUIT LIN QUAD COMPAR LM 339 N 590 2 11513037 MICROCIRCUIT LIN PWM CONTROL TL4S4CN 600 2 11811032 MICROCIRCUITY C MOZ 5 INF ANALOG MUX HCF4051 BE 610 2 11814037 MICROCIRCUIT CMOS 1X262144 BIT DYN RAM HY51Cz565 12 620 2 11814039 MICROCIRCUIT HMOS SERIAL COMM CONTROLLER P82530 6 630 2 11813019 MICROCIRCUIT LIN QUAD LINE DRIVERS 121488 540 1 11814028 MICROCIRCUIT CMOS SXS1L92 BIT RAM HM6264P 12 650 2 11601012 TRANSISTOR NPN 40v LOMAQ 3iW 2N3904 660 Mh Le bd f ba PREER qp Nt b S BPRERPRPRP PREP Re Hero uui Behe
72. ASS 130 15 1 11251006 LOCK RING FOR 6 0 7 AXLE 140 16 1 11251037 GRIP RING FOR D6 AXLE 45 PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 10855074 SUPPORT 1 ASSEMBLY 10455075 941026 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE DATE 11 1 11275021 SCREW M4 4 110 941024 Fig 1409 1410 1411 18 Support 1 Assembly 10455075 10 45 5075 Piir 88098 445 Tark 88093 Hyv 880913 EK 93 a Fig 1409 1410 1411 19 Support2 Assembly 10855078 96 10 10 FOR PART NUMBER 10855078 SUPPORT 2 ASSEMBLY 10455079 951006 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 1 10355076 SUPPORT ASSEMBLY NTLS 10 2 1 10455077 AXLE D6H3 NTLS 20 3 1 10353761 COGGED BELT WHEEL PA6 30 MINERAL 1297 30 4 1 10357482 COGGED BELT WHEEL 228 NTL5 40 5 1 11350098 COG WHEEL Al 56 10 50 1 10455068 AXLE D6H8 NTL5 60 7 1 10455069 BEARING HOUSE 6EK14 NTL5 B8 1 11350073 JOURNAL BEARING GLYCODUR PG 060810 F B 9 3 11350072 JOURNAL BEARTNG GLYCODUR PRG 060804 F 90 10 1 11278015 NUT Miz FE YELLOWPASS 100 11 1 11275007 SCREW M4 5 110 12 2 11275008 SCREW M4 6 120 14 1 10456254 COGGED BELT WHEEL BLANK 10353761 il 14 1 11250019 WASHER 6 4 18 1 6 FE YELLOWPASS 130 15 1 11251006 LOCK RING FOR 6 0 7 AXLE 140 16 1 11251037 GRIP RING FOR D6 AXLE G6 45 PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 10855078 SUPPORT 2 ASSEMBLY 10455079 951006 ITEM NO GTY ORDER NAME TYPE MANUF iNF LINE DATE 11 1 11275021 SCREW M4 4 110 941024 Fig
73. ASS 1414 40 3 1 10354321 COVER FLATE RIGHT AL PLATE S 2 5 NTLS FEN A 1 10354922 COVER PLATE LEFT AL PLATE 5 2 5 NTLS g 1 10354923 BOX AL PLATE 5 1 5 TLO BO 6 1 10354924 LIE NTLS 7 7 4 10454925 GUIDE ASSEMBLY NTL5 14 70 14n0 30 8 4 10454928 TUBE ASSEMBLY NTLS 1470 1460 90 o 2 10354931 SITEPORT FE PLATE 5 1 5 NTLS 100 10 1 10454932 BOX ASSEMBLY NTLS 110 11 1 10354935 SUPPORT RIGHT NTLS 120 12 1 10354940 SUPPORT LEFT NTLS 130 13 4 10454941 ADJUSTER NUT 6E14 1470 140 14 4 11275024 SCREW Hat RST 150 15 2 10454943 BRACKET ASSEMBLY HTL5 150 15 4 10450785 LEG BRASS ROUND SECTION 1414 170 17 2 11250020 WASHER 3r 0 1l FE YELLOWPASS 150 18 14 11250018 WASHER 58 3 15 1 6 FE YELLOWPASS 190 19 l4 11252012 RIVET 3 2 7 4 MONELL TLP D BS 42 200 20 22 11252002 RIVET 3 2 8 9 MONELL TLP D BS435 210 21 20 11260010 RIVETED HUT 5 2 0 3 0 MS 338597RIV TI 220 a2 4 11274004 SCREW M 4 6 FE YELLOWPASS 230 24 B 11274012 SCREW M 5 10 FE YELLOWPASS 240 24 a 11274013 SCREW M 5 12 FE YELLOWPASS 250 25 2 11274016 SCREW M 5 20 FE YELLOWPASS 260 26 d 11274031 SCREW M 5 12 FE YELLOWPASS 270 27 1 11274136 SCREW M 3j0 YELLONPASE 280 ad a 11278011 NUT ME FE YELLOWPASS 230 29 4 11278026 NUT M5 NYLCOC 300 30 4 10455004 BUSHING POM BLACK D 15 NTLS 165 31 11250004 WASHER A6 4 ZN 175 32 11274076 SCREW M 15 FE YELLOWPBASS 285 33 1 10854987 INSULATION SET 11 CODES 13 PARTS HTLb5 2H 34 1 10855506 P C ASSEMBLY ICNIZSER FRI 21 35 1 103553
74. Assembly 10859279 96 10 10 FOR PART NUMBER 10859279 TOP COVER ASSEMBLY 1415 10255462 940623 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 1 11391026 GAS SPRING PJ DER 16 1 168 135 680 745 2 1 10355463 PLATE RIGHT ASS NTL5 530 3 l 10355467 PLATE LEFT ASS NTLS 540 4 1 10355470 SUPPORT BOX ASS NTL5 550 5 2 10455473 PLATE FE PLATE S 1 5 NTLS 560 6 2 10455474 PLATE FE PLATE 5 NTLS 570 7 2 10255475 SUPPORT AL FLATE 10x25 NTLS 580 B 1 10355476 HINGE BODY RIGHT FE PLATE S 1 5 NTLS 5390 9 1 10355477 HINGE BODY LEFT FE FLATE 5 1 5 NTLS 600 10 2 10455000 SPRING D2 NTLS 610 11 2 10455478 GUIDE D6H8 NTL5 520 Le z 10455473 FLATE POM BLACK D 12 NTL5 630 13 2 10455480 BRACKET NTL5 640 14 1 10255481 TOP COVER NTLS5 550 15 1 10254553 COVER PLATE 5 NTLS 660 16 1 10355488 HINGE RIGHT FE PLATE 5 1 5 NTL5 570 17 1 10355489 HINGE LEFT FE PLATE 521 5 NTL5 680 18 6 10455490 NUT MS Di NTLS 690 19 2 10455491 PIN D2 5 NTL gt 700 21 1 10455493 PLATE POM PLATE 5 8 NTL5 720 22 1 10355494 HANDLE POM PLATE 5 25 NTL gt 320 24 1 10855453 INSULATION SET NTLS 520 26 12 11250010 WASHER 5 3 10 1 FE YELLOWPASS 750 27 1 11251015 PIN 2 10 ST 770 29 12 11274012 SCREW M5 10 YELLOWPASS 790 30 1 11274088 SCREW H3 20 FE YELLOWPASS B00 41 6 11274133 SCREW M4 6 FE BLACKPASS 810 32 4 11274134 5CREW M5 10 FE BLACKPASS 520 33 z 11276030 SCREW B4 2 22 FE YELLOWPASS 830 34 1 10455763 COVER ASSEMBLY NTL5 731 35 11276015 SCREW B 2 9 6 5 FE YELLOWPASS 840 36 1 10456
75. BLY DISPLAY CPU HCB 10354759 20 3 i 10255574 BOX NTLS 40 4 1 11842036 TOUCH PANEL 1410 FRONT PLATE TOUCH KEY 010377 50 5 5 10455619 BUSHING MS D6 4 NTLS 60 6 2 11250001 WASHER A3 2 YELLOWPASS 70 7 5 11271030 SCREW M3 35 FE YELLOWPASS 80 8 12 11278002 NUT M3 FE YELLOWPASS 99 W H 10851794 FLAT CABLE 268 268 10451797 30 PART HISTORY FROM 93 10 11 TO 96 10 10 FOR PART NUMBER 10855597 DISPLAY UNIT 10355595 940516 ITEM NO QTY ORDER NAME TYPE MANUF INF LINE DATE 1 10855628 PROGRAM PACKAGE DISPLAY PRG HCB BOARD 2 921231 10 1 11842024 PUSH BUTTON SWITCH 1X2 28VDC 1A 8121Y7 110 911001 m E a Fig 1409 1411 24 Display Unit 10859287 36 10 10 FOR PART NUMBER 10959287 DISPLAY UNIT 1400 SERIES 10355598 960612 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 1 10854665 P C ASSEMBLY DISPLAY HDS 10254761 S10 2 1 10954760 P C ASSEMBLY DISPLAY CPU HCB 10354753 520 3 1 10259243 BOX ASSEMBLY 1415 540 4 1 11842036 TOUCH PANEL 010377 550 5 2 11250001 WASHER AG 2 57D 5 4 11278002 NUT M3 FE YELLOWPASS 590 9 1 10557386 LABEL PVC FASKAL 400 T 0 1 1410 RESET 600 12 2 11480049 FERRITE CLAM 25 WIRE FLAT CABLE 28B2022 000 610 13 2 11480050 LAMP FOR 26 W FLAT CLAPM M CLIP 620 14 1 11240152 RF GASKET 3 244 484 MONEL 01 0901 6602 630 15 1 10361691 LID ASSEMBLY TIN COVERED NTL 5 640 18 1 10361690 BOX ASSEMBLY TIN COVERED NTL 5 650 17 2 10461689 BUSHING MS NTL 5 660 15 9 11276015 SCREW C 2 9 5 5 FE YELLOWPASS 670 19 6 112716021
76. D SPACER WY DON KOLS 35 210 3 11271018 SCREW M3 6 FE YELLOWPASS 240 M 1127101 SCREW M378 FE YELLOWPASS 230 lc 3 11271023 SCREW Mi 14 FE YELLOWPASS 240 11 3 11278002 MUT M3 FE YELLOWPASS 136 12 1 10556568 LABEL WHITE SELF ADHESIVE L HV SUTPUT INPUT 18 Cl l 11526002 CAPACITOR H V 2 5NF 3EV DD30 252 10 Ca 2 11626008 CAPACITOR A V 150PF 3 0KV 20 50 970130 9 D FERROP 20 Rl 1 11601149 RESISTOR 10K 2 0 E 1 2 BEYSCHLAG 30 R2 1 11604049 RESISTOR MF SM 100 15 0 125W lO0PPM 40 RS 15 2 11604209 RESISTOR MF SM 218 1 0 325W 100PFM ab RlI7 2Z1 24 28 10 11604241 RESISTOR MF SM 1 00M 1 0 125w LOOPPM 45 n22 29 2 11504225 RESISTOR MF FM 464 13 0 125W 100PPM 43 Bl 4 0 5606 11863070 F c CONECTOR 40 PIN STRAIGHT 511 25 366 60 63 a n m Fig 1409 1410 1411 23 HV Divider Unit 10859369 96 10 10 FOR PART NUMBER 10859369 HV DIVIDER UNIT RF 10359369 10355373 960607 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 11860001 COAXIAL CONNECTOR 11H4 50 3 1 iQ 1 11460001 SOLDERING TAG D 5 5 3 A2021 ME 110 5 11250021 SERRAT LOCK WASHER 3 0 ANNEALED ZINKED i 2 5 5 0 45 190 4 11250001 WASHER Ai 42 200 1 090 11240035 COAXIAL CABLE RG 58 C U 210 1 10554024 P C BOARD 1 6MM 2 P EP LK RRH 1410 230 1 L 10358910 PLATE FE PLATE 5 1 1415 260 2 3 10454335 NUT MS 6K6 NTL5 240 3 2 11260035 RISE PIN M3 10 MS 5 093 103 150 4 1 10454401 BOX ABE S 2 1205 250 5 1 15544576 LABEL DANGER H Y SERIVA 270 5 1 11310006 CLAMP MS 1 25 MEL A 302
77. DPM Poslden ChemiStrip and MultiCalc are trademarks of Wallac Oy Lotus 123 and Symphony are registered trademarks of Lotus Development Corporation MS DOS Microsoft Windows and Excel are registered trademarks of Microsoft Corporation Pentium is a registered trademark of Intel Corporation 1 Introduction Introduction A new LS counter The Wallac 1414 range of DSA liquid scintillation counters WinSpectral WinSpectral e B and Guardian is created to bring the very latest in LSC and PC tech nology to your laboratory The combination of Digital Spectrum Analysis DSA with the Microsoft Win dows graphical user interface as well af separation WinSpectral o B and Guardian and sophisticated shielding Guardian makes an unbeatable combina tion PC display for WinSpectrai software and live results Instrument cover Keep closed when counting Disk drive for program disk behind cover Wallac 1414 WinSpectral and peripherals Introduction In this manual you will find a description of what you can do with your counter whichever model you have including the various options available an explanation of how to use the instrument as well as background information about how it works and how to install it Note m this manual the name WinSpectral is normally used and no distinction is made between the three dif ferent models except where they differ The figure below shows the instrument and identifies th
78. E FE 53 1409 1235 1297 90 10 1 10357482 COGGED BELT WHEEL z 26 NTL 5 100 11 1 10354388 GOGGED BELT WHEEL GRILON W 5232 1297 110 12 1 194548723 LIFT ARM NTLS 120 14 1 10454875 PLATE FE S 1 5 NTL5 140 18 1 10454876 AXLE D5H8 NTL5 155 18 4 11350098 COG WHEEL 210 s6 10 150 17 10454878 PLATE ROSTPROOF PLATE 0 8 NTL5 170 18 1 10454870 BUSHING MS DS 6 NTL5 150 13 2 10454580 PIN SPRINGBRONZE 1 716 NTLS 180 20 2 10454881 BUSHING POM BLACK D 8 NTLS 200 21 2 11250008 WASHER 4 3 9 0 8 FE YELLOWPASS 210 23 1 11252007 RIVET 3 2 6 1 MONELL TLPD ES424 230 a4 4 11274004 SCREW M 4 6 FE YELLOWPASS 240 25 11274005 SCREW M 4 8 FE YELLOWPASS 250 26 4 11274007 SCREW M 4 12 FE YELLOWPASS 260 27 6 1124012 SCREW M 5 10 YELLOWPASS 270 29 4 11275021 SCREW M4 4 AISI316 290 30 3 11276015 SCREW C 2 9 6 5 FE YELLOWPASS 300 31 0 600 11350025 CHAIN 5 MM 445 310 32 1 11350044 COGGED BELT SYNCHROFLES eT 2 5285 320 33 4 11350072 JOURNAL BEARING GLYCODUR PAG 060804 F 330 34 4 11350073 JOURNAL BEARING GLYCODUER PG 060810 F 340 35 2 10454882 AXLE DLD6H8 150 36 1 10553597 P C BOARBRD 1 6MM 2 P EP LE RRA 1205 1470 201 37 1 10855196 F C ASSEMBLY CONNECTION BOARD RSP 10455155 202 38 1 10456162 BUSHING BRASS ROUND BAR D30 NTLS 203 39 1 10456164 AXEL STAINLES BAR NTLS 204 40 1 10456163 PLATE FE FLATE 5 1 NTLS 205 41 1 10456161 BUSHING BRASS ROUND BAR DS NTL5 206 42 2 11251055 PIN 2 10 ROSTPROOF 238 43 2 11271035 SCREW HM 4 5 FE YELLOWPASS 239 44 1 11391012 B
79. E S 0 5 0 SMM AL PLATE S 2 NTLS FE PLATE S 1 NTLS5 POM ROD D 40 NTLS MU S 0 1 NTLS 4 3 9 0 8 FE YELLOWPASS F 3710 1 FE YELLOWPASS 6 4 18 1 6 ZINKED i 20 ST 13 1 16 1 1 9 3 ST EDS 0 3 2 4 5 1 AL TAP D BS 33 3 4 FE YELLOWPASS 4 5 FE YELLOWPASS 5 12 FE YELLOWPASS 5 20 FE YELLOWPASS 6 30 FE YELLOWFASS lt M6 12 FE YELLOWPASS M6 25 YELLOWPASS M4 8 FE BLACKPASS C 2 9 9 5 FE YELLOWPASS 5 3 15 1 5 FE YELLOWPASS AL PLATE 5 3 NTLS M 4 10 FE YELLOWPASS M4 FE YELLOWPASS FE PLATE 1 NTLS M6 12 FE YELLOWPASS HV 1410 WARNING ALO O8 1410 CR AL 5 0 08 1410 PROGRAM CR FE PLATE T 1 LSC 5 M 3 10 FE YELLOWPASS SOLUPOLYETHEN S 20 NTL 5 WHITE SELF ADHESIVE L NOTE FE PLATE T 1 Lot FE PLATE T 1 LSC C 2 9 6 5 FE YELLOWPASS 10 12 SM 530 K FE 551 1409 11 15 FE 5 1 1409 11 15 FE PLATE S 1 1415 LEAD CAST 1415 1415 1415 CAST LEAD 1415 CAST LEAD 1415 12852 1480 BRASS ROUND SECTION 1414 4 3 12 1 FE ZINKED M 4 6 FE YELLOWPASS C 4 2 9 5 FE YELLOWPASS M 4 25 FE YELLOWPASS M 1 7 2 7 2 954 329 D4 B 4 4 14 08 040 4 3 CLEAR NYLON GUARD PREAMPLIFIER SAC 10358303 D19MM 1ODYN 12PIN R1166 10 SILICONE D21 15 BLACK 1415 M3 FE YELLOWPASS 1 2 1 6 CE 016 ST FLATE Tz1 5 NTGS C 3 5 5 5 FE YELLOWPASS POM PLATE 5 8 BLACK NTL 5 255 275 285 295 305 315 318 335 345 413 360 455 i76 385 395 405 415 425 435 445 455 465 475 485
80. EAL NUT DUMMY PLUG FLATE RIGHT PLATE LEFT WASHER SCREW SHELTER SCREW SCREW LABEL 103 MS D 20 SOLUPOLYETHEN AL PLATE 5 2 FE PLATE 5 2 AL PLATE 5 2 3 5 2 F 600 PS00 250KB AL SQUARE BAR 8 2x8 2 AL 99 5 5 1 AL PLATE 5 0 5 SMM AL PLATE 5 2 FE PLATE 5 1 POM ROD D 40 MD S 0 1 4 3 9 0 8 FE YELLOWPASS gt 3 10 1 FE YELLOWPASS 6 4 18 1 6 FE ZINKED 3 20 ST 13 1 9 3 ST 475 1 AL 3 4 FE YELLOWPASS 4 5 FE YELLOWPASS p a 2 12 FE YELLOWPASS 3 20 FE YELLOWPASS 30 FE YELLOWPASS M6 12 FE YELLOWPASS M6 25 YELLOWPASS M4 8 FE BLACKPASS NTL5 NTL5 HTL 5 WTL 5 NTL5 1414 FD1137H 1414 NTLS NTL5 NTL5 NTL5 NFLS KDS TAP D BS 33 5 3 1571 6 FE YELLOWPASS AL PLATE 523 M 1210 FE YELLOWPASS M FE YELLOWPASS FE PLATE S 1 M 12 FE YELLOWPASS HV AL E AL 5 0 08 FE FLATE T M 3 1L0 FE YELLOWPASS SOLUPOLYETHEN S 20 WHITE SELF ADHESIWVE L FE PLATE T 1 FE PLATE T 1 C 2 9 6 5 FE YELLOWPASS fei FE S 1 FE S 1 PE PLATE 5 1 DEAD CAST idi CAST LEAD CAST LEAD LEAD 112371 FE ZINKED M 4 6 FE YELLOWPASS C 4 2 8 5 FE YELLOWPASS M 4 25 FE YELLOWPASS M4 1 7 2 7 D4 23 4 4 GUARD PREAMPLIFIER D19MM lODYM 12PIM SILICONE D21 15 BLACK Mi FE YELLOWPASS 1414 FE PLATE S 2 6 FE PLATE 5 2 0 4 2 7 0 5 FE YELLOWPASS M 3 6 FE YELLOWPASS POM PLATE S 8 BLACK Ma 8 FE YELLONPASS
81. EM PROTOCOL 5 SPECTRUM DATE 1778 02 16 TIME E TD PUBASOLO Unknown samples Pos Crime HS CPM 14 CrM SOF I SFE i 120 127326 4 127612 9 175 77 966 40 Spectrum Plot Yo EJ a E EL C5 z t ani A T I i T i 1 T L a ab Chanresl rumber Total count rate 127526 4 CRM G 144 127612 7 CPF POCO F 1 23 Soo reir ol PROTOCOL 8 SPECTROM ITE 1998 02 16 TIME 09 40 ID PORASOLT Unknown samples Fos CTime H3 CPM C14 CEM SEPT HAPE 2 120 Zu l0zZ9865 0 415 90 9743 06 Spectrum Flot Ari 1 ADU x j 5 e ES 128 uu 9 d TTTT TT PT Ut aAA 1 Channel mumtber Total count rate HZ 7725 97 CPM 14 io02955 0 CPM PROTOCOL 15 145 Benz protocol DATE 1990 02 17 TIME 16105 FILE r A41641401896P15SAS01l6 TAT ID F15SA SQ16 Wallac 1414 WinSpectral v1 30 Counting mode Isotope 5 C14 Protocol name Counting time Repeats Cycles eplicates 2 sigma A Minimum cpm Advanced modes PSA level PAC level Output to Printer S N 4140189 CPM C14 660 2730 00 y i4C Benz protocol 14400 1 1 1 0 50 0 00 Checking timet PSA PAL 85 163 3 F un mm 30 F hM Eh da POS CTIME SOPI CPMwi CPMw2 CPMw3 Additions to Printer Output to Display FOS RACKPOS CPM SOF T CPE Additions to Display Fath of File Qutp
82. ERTY select the protocol winbeta and then type in the properties go to the MultiCale main menu by pressing ESC ESC create a startup macro for MultiCalc as follows Press ctrl A Select MACROS Select CREATE Enter as the macro name Select level 2 Press Enter as the comment Press function key this is the body of the macro and it means that the program will go to COUNTER Now the macro is complete and should be ended by pressing the ESC key To save the macro on disk you now have to exit from MultiCalc To do so press ESC once and then press X 5 7 MultiCalc installation and select Fl Yes for the question Exit MultiCalc Yes No now use the Windows Program Manager and copy the icon WinSpectral to the StartUp group To do this drag it from the WinSpectral group to the StartUp group while you hold down the CTRL key Changes to Autoexec bat Edit the MS DOS Autoexec bat file Use Windows Notepad or a DOS editor to do thts Make sure that you have there the command COMRS and that it has the parameter 00000000 Le eight zeros This ts to force MultiCalc not to use serial ports at all Otherwise you will get the question about who should use the COMI or COM2 port the Windows applica tion or the DOS application when MultiCale 15 started While you are editing the Autoexec bat file add also there the command WIN to make Windows start auto matically after a bootup Setting up a protocol in Mul
83. ESISTOR MF 1M 1 0 25w SOPPM 411 2 VITROHM 23 PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 10860160 PREAMPLIFIER UNIT 12 DYNODE 10455394 960103 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE DATE 11 2 11271021 SCREW M 3 10 FE YELLOWPASS 120 960102 12 i 11278002 NUT M3 FE YELLOWPASS 130 960102 13 1 11310006 CLAMP MS 1 25 HKL A 3024 ASA 185 960102 16 2 11250001 WASHER A3 2 170 960102 38 Fig 1409 1410 1411 11 Preamplifier Unit 10455394 lt c o TEN e tO SES 3 25 lt eo co 90 O t lt z 39 Fig 1409 1410 1411 12 Optics 10856122 96 10 10 FOR PART NUMBER 10856122 OPTICS 10356123 930916 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 1 10854822 LIGHT SHUTTER UNIT 10354823 10 1 10354851 BODY NTLS 20 3 10256157 REFLECTOR ULTEM 1000 NTLS 30 5 2 10457768 RING POM BLACK 1410 50 s 2 10454853 TUBE CU TUBE D 57752 NTLS 60 7 1 10454854 BOX 1 AL FLATE 5 1 NTL5 70 B l 10454855 BOX 2 AL PLATE 3 1 NTL5 BO 2 6 11271045 SCREW M3 5 FE YELLOWPASS 30 10 2 10555418 P C BOARD l 5MM 1 P EP RXI i10 11 2 11271107 SCREW M2 5 6 M5 NICKEL 120 12 2 11278017 NOT M2 5 FE YELLOWPASS 130 13 2 11460001 SOLDERING TAG D 5 573 5 8 A2021 ME 140 14 d 11250042 WASHER 2 7 5 0 5 ACID PROOF 150 D1 D2 2 11784015 DIODE LIGHT EMITT D3X5 YELLOW 585NM lt 100NS MV5374C 100 Fig 1409 1410 1411 12 Optics 10356123 THS Wa Hyv 881115 10 35 6123 Piirt 881115 Tark 881115 41
84. ETED NUT M 4 1 0 2 0 MS 33649 3RTV TL 350 at 2 11260010 RIVETED NUT M 5 3 0 3 0 MS 338592RIW TI 360 aH H 11270001 SCREW M 5 25 CU 370 29 G 11862127 LOCKING MUT ASSY D CONN LY 1 4 40NC 2B 17D20415 2 350 30 2 11271021 SCREW M 3 10 YELLOWPASS 390 31 4 11271025 SCREW M 3 16 FE YELLOWPASS 400 32 2 11271048 SCREW M 3 10 FE YELLOWPASS 410 33 2 11271054 SCREW M 4 10 FE YELLOWPASS 420 34 2 11274009 SCREW M 4 20 FE YESLLOWPASS 430 35 2 11274015 SCREW M 5 16 FE YELLOWPASS 440 35 4 11274072 SCREW FE YELLOWPASS deb 37 2 11276010 SCREW C 2 9 13 FE YELLOWPASS 460 i8 B 11278002 MIT Mi FE YELLOWPASS 470 39 3 11278003 NUT Ml FE YELLOWPASS 480 4 9 11278004 NUT MS FE YELLOWPASS 430 di z 11278006 NUT M CU 500 42 2 31561035 CABLE LUG 0 75 1 SMM A 1543 R 5105 43 l 11861028 CABLE LUG M 0 75 1 5MM2 Ai156 5R 520 44 1 11310040 CLAMP ACCH2 A 550 45 4 11861003 FLAT CONNECTOR 6 380 8MM 0 75 1 5MM2 A 1507 FL 530 45 i 11250008 WASHER 4 3 970 8 FE YELLOWPASS 311 47 7 11460004 SOLDERING TAG Dio 6 10 A2004 ME 540 48 10 11274012 SCREW M 5 10 FE YELLOWPASS 441 49 1 16461424 SLIDE AL 8X30 1400 SERIE POWER U 610 50 9 260 11240173 RF GASKET 6 35x6 35 MONEL GLUE 01 0901 6603 600 51 10 11252007 RIVET 3 2 6 1 MONELL TLP Db BS424 630 SA 0 096 11240174 RF GASKET SPRING Be u Z8MM 5MM 7 438 02 620 cl 1 11626007 CAPACITOR H V ATNF 20 250VAC lKVDC PME275MESA470M RIFA 130 CS 3 2 11630036 CAPACITOR ELECTR 10000UF 10 30 amp AQ PEH179KD5100
85. K 360 0 150 11240067 CONNECTING WIRE 10 20 MM YELLOW 370 0 150 11240072 CONNECTING WERE 1 0 20 WHITE 480 1 10560490 LABEL SET CONNECTOR LABEL CAZ2 lz2 DYN 400 1 1 10853277 OPTICS 1415 10156123 220 2 1 108547459 COUNTER WEIGHT 10454790 2530 3 2 10860160 PREAMPLIFIER UNIT 1409 11 15 12 DYMODE 10455354 240 4 2 10454039 LIGHT SEAL SILICON BLACK NTLS 290 5 1 108551835 ANAL RACE 1410 241 1 10857570 P C ASSEMBLY COINCIDENCE BOARD LAC A 10357727 242 H 1 10857571 P C ASSEMBLY SAMPLE amp HOLD 1H LAD A 10357728 243 8 1 19859028 P C ASSEMBLY AE CONVERTER FB 10359027 z43 g 1 10854767 F C ASSEMBLY MCA INHTERFACE 1CH LBR 10354766 245 10 1 10860105 P C ASSEMBLY GAIN STABILIZER EBU A 10360197 246 li i 10854652 P C ASSEMBLY HV SUPPLY EPM A 10354653 247 FH 2 11860438 PHOTOMULTIPLIER D52MM 12DYM B21 R331 05 SLTD 330 Wo W10 2 10855406 WIRING ASS Car 210 PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 10359278 MEASURING UNIT 1415 10354850 931109 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE DATE 7 z 10857651 PREAMPLIFIER UNIT 1409 11 10 DYNODE 10455394 240 930327 4 1 10254242 P C ASSEMBLY A D CONVERTER EBP 10353905 244 930607 10 1 10854784 P C ASSEMBLY GAIN STABILIZER EBU 10354783 248 930927 EM 2 11760038 PHOTOMULTIPLIER L52MM l2DYN B21 R331 05 330 931106 EM 11750045 PHOTOMULTIPLIER D52HMM 12DYM B21 R331 05 SLTD 330 931217 L 10555408 LABEL SET Caz 10 DYM 400 940202 FAS 213 S90 NOTE Xx USEO ONLY fht HUCMi KAY
86. KEY KEY PEEL SETTINGS G KEY 40V 10MA 0 310 40V SOMA 0 37WP CH MOS 50V 12A 75W N CH MOS 1 184 75W N CH MOS 604 5A 65W DARLINGTON 50V SA 65W DARLINGTON 2 0A 250V SLOW 6 3 32 4 0A 250V SLOW 6 3 32 6 34 250V SLOW 5 20 1X6 10A 250W VOLTAGE REG 5V 1A D3X5 2585NM lt 100NS PIN JUMPER ZA 157 5 17MA lW 30V 124 DUAL SCHOTTKY 2004 255 1 6NM 2 P EP LE SYNCHROFLEZX BRECOFLEX BRECOFLEX SYNCHROFLEX SYNCHEOFLEX SYNCHROFLEX SYNCHROFLEX SYNCHROFLEX SYNCHROFLEX SYNCHROFLEX GRILON W 5239 5 N 24AWG 5 1 6 P FEMALE 24AWG amp N FEMALE 1BAWG FOR 3 P CONNECTOR g N 24 AWG 8 N 16 N d 3 5 ULTROTERM 1205 BETAPLATE 1410 SERVICE PROGRAM 1410 SERVICE PROGRAM 1409 SERVICE PROGRAM 1409 FIXED PROTOCOLS 1410 DO MAPPING PRG DISPLAY PRG HCB BOARD 1205 4MM Ad CLEAR DIE RAM GPRINGSTEEL T 0 7 2N3906 3N163 BUZ10 BUZ2 1 TIP120 TIP125 19343 19343 19195 SWPO33 1109 MC 7805 CP OPBEO4 MV5373C 59001 1N4744A VSEK1J BYV25 200 RRA 1205 1476 T 2 5285 1205 6 T2 5 120 10 T2 5 160 6 T2 5 200 T2 57380 6 T2 5 500 10 T2 5 650 10 T2 5 1300 1297 CT100F24 5B TCLOOF 5 CT156F24 6B CT156Fl18 6B TCl56F 5 CT100F24 8B TCLOOF 8 CT100F24 16B CAZU CA20 MICROBOX 5 TERMINAL EMULATOR WITH FIXED PROTOCOL FOR HARDWARE V1 4 V1 8 V2 0 SERVICE PROGRAM 10454503 10455261 NO 368 NO 368 T126 A4 0 08 1410 921 10354603 1410 670 630
87. LATE S 2 0 NTLS 313 60 4 11275014 SCREW 455 61 2 112374012 SCREW M 5 10 FE YELLOWPASS 435 BA 1 103557965 SUE DE FE PLATE S 2 HTLS 314 63 1 10455633 BRACKET FE PLATE 5 1 5 NTLS 315 6d 2 10355889 PLATE 1410 1470 1297 316 66 2 10456345 GLUE FILM i GLUE FILM T 0 16 FIXMATE 500 318 67 4 10456346 GLUE FILM 2 GLUE FILM T 0 16 FIXMATE 500 319 55 0 100 11140002 SEALING TAPE C 10 BLACK 73 63120 515 11290013 FOOT D12 3 RUBBER 3M SJ 5012 530 59 1 Wi 1 10855299 WIRING ASS CAl5 61 WZ 1 10855300 WIRING ASS CAL 52 Wa 1 10855313 WIRING ASS Cala 67 Wo W7 2 10855315 WIRING ASE CA20 59 PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 10855197 SAMPLE CONVEYOR 10155198 940203 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE DATE 14 2 10355207 SUPPORT BAR 9 3 15 1470 1257 146 911018 15 10355208 PLATE Sai 1470 1257 150 911018 31 40 10353703 TOOTH POM BLACK 1470 1297 310 920519 20 Fig 1409 1410 1411 03 Sample Conveyor 10155198 21 Fig 1409 1410 1411 04 Floor Stand 10856020 96 1D 10 FOR PART NUMBER 10856020 FLOOR STAND 10256021 890828 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 11550143 PACKING BOX 1050 780 860 VIEEX 400 n 11550069 L LIST 90 90 25 1000 6311 01 410 1 11550043 PACKING LISTBAG MERCAPOCKET 180X140 CA 420 l 10549484 LABEL WALLAC 430 l l 10256022 BOTTOM FRAME NTL5 10 2 1 10256025 TOP FRAME NTL5 20 3 E 10356027 VERTICAL TUBE NTL5 30 4 1 103560310 SHELF 1 FE PLATE 5 0 5 BLACK NTL5 40
88. LY COINCIDENCE BOARD LAC A 10357727 42 7 1 10657571 P C ASSEMBLY SAMPLE amp HOLD ICH LAD A 10357728 43 B 1 10859028 P C ASSEMBLY A D CONVERTER EBZ 10359027 44 10 1 10860105 P C ASSEMBLY GAIN STABILIZER EBU A 10360127 46 FM 2 11760038 PHOTOMULTIPLIER D52MM 12DYN Bel R331 13 130 Wwe W10 2 10855406 WIRING ASS CAZA iQ PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 10854849 MEASURING UNIT 10354850 950522 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE DATE 3 z 10857681 PREAMPLIFIER UNIT 1409 11 l0 DYNODE 10455394 40 931112 1 10854242 P C A SSEMBLY A D CONVERTER EBP 10353905 44 931011 1 10554784 P C ASSEMBLY GAIN STABILIZER EBU 10354783 46 931020 1 10555408 LABEL SET CA22 10 DYM 200 940524 1 1 10856122 OPTICS 1410 10356 20 950519 Fig 14 g 1409 1410 1411 10 Measuring Unit 10354850 10 35 4850 37 a m Fig 1410 11 Preamplifier Unit 10857681 96 10 10 FOR PART NUMBER 10857681 PREAMPLIFIER UNIT 10 DYNODE 10455394 940831 ITEM NO QTY ORDER NAME TYPE MANUF INF LINE 1 1 10857669 P C ASSEMBLY PREAMPLIFIER BOARD RAG A 10357726 10 2 1 10355395 BOX ASSEMBLY NTLS 30 3 1 10355397 COVER FE PLATE 821 NTL5 40 4 4 10455393 NUT GEB NTLS 50 5 1 10455399 INSULATION PRESPAN PLATE 5 0 5 NTL5 40 5 2 10455400 SPRINGT ION GERMAN SILVER 5 0 15 NTL 5 70 1 10455401 BASE BASE HAMAMATSU E678 21A NTL5 60 8 1 10544576 LABEL WARNING LABEL DANGER H V SERIVA 90 3 d 11271044 SCREW M3 4 FE YELLOWPASS 100 10
89. MANUF INF LINE DATE B7 1 11570061 LABEL WALLAC 52X22 16 STICKER 350 930315 1 10358600 COVER PLATE POLYCARBON 20 375 1415 352 930315 1 10555408 LABEL SET CA22 419 940202 1 10551111 LABEL AL PLATE S 0 8 LR52500 404 941214 1 10855268 STD CAPSULE 10455269 NTL 5 20 950216 6 i 10859279 TOP COVER ASSEMBLY 1415 10255462 55 960122 W24 1 10855508 FLAT CABLE 105 405 FC33 127 951128 13 l 10355564 FRONT BOX ASSEMBLY NTLS 135 960116 14 1 10355567 SIDE BOX RIGHT FE PLATE S 1 NTL5 145 960115 15 1 10355568 SIDE BOX LEFT FE PLATE 5 1 NTLS 155 960116 32 0 500 10455572 PLATE 2 NTLS 335 960313 85 4 10458900 FOOT 5 1 1415 412 950612 1 11570078 LABEL THERMAL TRANSFER PRINT THT 5 43 10 414 950508 dz 10 11250008 WASHER 4 3 9 0_8 FE YELLOWPAEZZ 425 960116 33 112580010 WASHER 5 3 10 1 FE YELLOWPASS 435 960115 47 4 11251077 LOCKRING 1631 475 950324 50 4 11271016 SCREW M 3 4 FE YELLOWPASS 505 960116 52 12 11274013 SCREW M 5 12 FE YELLOWPASS 525 960116 25 8 11274145 SCREW M6 FE YELLOWPASS 555 550324 115 z 11274156 SCREW M6 146 ST YELLOWPASS 556 960116 0 300 10556201 LABEL WARNING STICK PVC ALUM EUROPIUM 152 505 950216 77 78 10155600 Fig 1415 26 LSC Assembly Fig 1415 27 Measuring Unit 10859278 96 10 10 FOR PART NUMBER 10859278 MEASURING UNIT 1415 10354850 940203 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 0 150 11240062 CONNECTING WIRE 70 20 MM GREEN 350 0 150 11240071 CONNECTING WIRE 1 0 20 MMZ BLAC
90. OL cM 816099 3d ZSOS Sp OL 59 Fig 1409 1410 1411 22 Spring Assembly L 10855445 96 10 10 FOR PART NUMBER 10855445 SPRING ASSEMBLY 10455446 950207 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 1 10455447 TUBE 1 D12710 NTLS 10 2 0 390 11182011 FTFE TUBE 10 8 TEFLON 80 3 1 10455449 PIN 1 Diz NTLS 30 4 1 10455003 SPRING Di NTLS 40 2 l 10455450 PIN 2 DE NTL gt 5D 6 1 10455451 FIN 3 OSHE NTL5 60 7 1 10455452 FLANGE D12 NTLS 70 60 10455446 Fig 1409 1410 1411 22 Spring Assembly L AX 104088 N H Vy LOLOB8AJDL Sri 04088 Jud ObPS SP OL 61 62 m a Fig 1409 1410 1411 23 HV Divider Unit 10854023 25 10 10 FOR PART NUMBER 10854023 HV DIVIDER UNIT 10355373 10355106 920515 ITEM NO GTY ORDER NO NAME TYPE MANUF INF LINE 1 11860001 COAXIAL CONNECTOR 1iH4 50 3 1 Bo 1 11460001 SOLDERING TAG 5 5 3 5 8 A2021 ME cat 1 11250021 SERRAT LOCE WASHER 3 0 ANNEALED YELLOWPAS 3 27 5 5 0 45 140 2 11250001 WASHER A3 2 YELLOWPASS 135 1 100 11240035 COASTAL CABLE RG 58 C U BLACK 100 0 1006 11240008 WIRE LOGI PVC 105 0 400 11240101 COPPER WIRE D 0 8 110 l 10554024 P C BOARD 1 5MM 2 P EP LK EFH 1410 10 1 10355372 FLATE FE PLATE 3 1 FTLS 156 2 3 10454836 HUT 5K 160 3 e 11250035 EISE FIN M3 10 5 03 103 170 d 1 10454401 BOX ABS PLATE 2 1205 180 a 1 10544576 LABEL WARNING LABEL DANGER H V SEREVA 190 6 1 11310006 CLAMP MS 2 25 MEL A i024 ASA 200 7 2 11320105 DOCK CAR
91. Pintwbasibtely Cyber ai LL iin 94121 AS tex 961212 HKY P 941212 Fair alg Per Capo Pegs Pe Oe ee l ELLEt TOISIN MAARATA Lewyn zu Did MM RACAL Ine SOURCE al TALHED wallac oy Wi Eu 152 EXT STD TRANSPORT SYSTEM vu TURKU ANAND 10 36 1092 4 ad m T ar a 1095 7794 wallac CERTIFICATE for SEALED RADIOACTIVE SOURCE Manufacturer Wallac Oy Batch No 7C 10 uu 20101 TURKU 10 Serial No FINLAND Description of the Radionuclide EU 152 gamma source in stainless steel shield of thickness 0 35 mm Active length 1 3 mm Max activity 440 kBq 12 uCi ISO classification ISO 2919 C43434 Leakage test The sealed source is immersed in distilled water The water is heated to 323 5 K and held at this temperature for 4 h The sealed source is then removed and the activity of the water is measured with a liquid scintillation counter Activity levels exceeding 185 Bq will be cause for rejection Result of test Passed Date of test 15 09 97 Signature mo 5 Installation information 1099 0045 wal lac March 1991 Fa ar ee A AN EG26 COMPANY QUALITY CONTROL CERTIFICATE PRODUCT INFORMATION WATI E AG 12414 Tesch Name of product 9o ee 4 8 4 9 5 99 8 OR P b 4 k OB o t ROB 4 BOB Ao d Ao 00 7 Product type no amp o BOB OR Bod BOR BOB REOR OR Po Wo ob BOR k k
92. R PART NUMBER 10860862 KEYBANK ASS 1414 10260855 960205 ITEM NO QTY ORDEH NO NAME TYPE MANUF INF LINE l 11560029 MOUSE MAT 194 244 120 1 10961122 1414 KEYBANE ASS 130 1 1 10160796 KEYBOARD BOX ASS 1414 lo 1 10260790 COVER ASSEMBLY 1414 20 3 1 10360786 FASTENING PLATE 1 FE PLATE 5 1 5 1414 30 4 1 10360787 FASTENING PLATE 2 FE PLATE 5 1 5 1414 40 2 2 10460784 LATH FE PLATE 5 3 0 1414 50 6 2 10460795 FASTENING LATH FE PLATE 5 3 0 1414 60 7 2 11310057 SLIDE FOR BOX WHITE BS 220M 450 70 8 l 11450008 INLET INSULATOR 27 21 14 5 8 1 70 30017 BO 9 2 11290033 FOOT D12 3 GREY 3M SJ 5012 90 16 10 11271093 SCREW Md amp FE YELLOWPASS 100 10160809 121 11274004 SCREW M 4 6 FE YELLOWPASS 110 10160509 42 8 11250008 WASHER 4 3 9 0 8 FE YELLOWPASS 115 PART HISTORY FROM 95 01 10 TO 96 10 10 FOR PART NUMBER 10860362 KEYBANK ASS 1414 10260855 960205 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 7 1 11310097 SLIDE FOR BOA WHITE RS 220M 450 70 950907 112 10260855 Fig 1414 37 Keybank Assembly MOTH LEZOT AAH SA Mevi DHr DcOL 6 id 23809801 SS809201 4v GM EOLLYE 113 8 Index Index See Sample quality A Accuracy enhancement 1 9 ACSS l 4 Activity 3 1 Error 3 Alpha beta separation 1 10 Automatic continuous spectrum stabilization See ACSS Background Calculation 3 4 Correction 1 7 Counting time 1 8 Reduction 1 10 Sample positions 1 8 Backup 5 4 Barcode See Poslden ID reader
93. R cL Ei LS uug p Hp pp rR hI E oo bj lat oo Ch T J Z de m co F Px RI DI b 10455616 10355617 10355618 10455632 10355742 10360744 11710021 10450743 105359672 10494512 10548122 10355677 10355585 10455723 10455797 11250008 11250010 11250019 11251018 11251045 11251077 11252008 11252019 11271016 11271034 11274013 11274016 11274034 11274145 11274095 11274133 11250018 19455131 11271036 11278003 10455897 11271095 10556070 10556095 10556071 10456182 11274003 10456382 10556607 10457299 10457300 11276015 10860710 10458398 10458899 10458881 15458887 10858914 15358839 10358888 10448323 11250039 11274004 11276005 11274010 11310047 11290015 10558304 11760040 10358501 il278002 108560713 10460752 10460761 11250006 11274002 10460964 11271053 11274156 10561340 BUSHING INSULATION COVER 1 COVER 2 COVER 3 LID ASSEMBLY FLOPPY DISK DRIVE HANDLE LABEL WARNING PLATE LABEL SUPPORT COVER BUSHING SHIELD WASHER WASHER WASHER PIN LOCKRING LOCEKRING RIVET RIVET SCREW SCREW SCREW SCREW SCREW SCREW SCREW SCREW WASHER COOLING PLATE SCREW WUT PLATE SCRE LABEL LABEL LABEL FLATE SCREW INSULATION LABEL BRACKET GUIDE SCREW RESET UNIT BRACKET RIGHT BRACKET LEFT BRACKET LEAD SHIELE GUARD LEAD LEAD LEAD SHIELD WASHER SCREW SCREW SCREW NUT EOL F C ASSEMBLY PHOTOMULTIPLIER LIGHT S
94. REAK SPRING 0 5 5 30 ROSTPROOF 341 45 2 10461476 JOURNAL BEARING 6 9x10 208 45 1 11251042 PIN 2 B 235 K 1 11863089 P C CONNECTOR 5 P STRAIGHT LOCKABLE MLSS100 5B 350 M 1 11690042 STEPPING MOTOR V 1A 1 8AST 0 PH265 04 360 PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 10854857 ELEVATOR ASSEMBLY 10254858 951025 ITEM NO QTY ORDERNO NAME TYPE MANUF INF LINE DATE 5 1 10454863 PLATE FE FLATE 5 1 5 NTLS 50 820406 11 1 10357481 COGGED BELT WHEEL Z 28 NTLS 110 820403 16 4 10454877 COGWHEEL s6 10 NTL5 140 911212 13 1 10454874 LIFT ARM HEAD STAINLESS STEEL D6h3 NTL5 139 950608 34 11350073 JOURNAL BEARING GLYCODUR PG 060810 F 340 951024 10254858 Fig 1409 1410 1411 08 Elevator Assembly Ax igg AH HI gg HL She LLL Hd APDIOJSON 9 258p Sc OL 33 Fig 1409 1410 1411 09 External Standard 10855272 96 10 10 FOR PART NUMBER 10855272 EXTERNAL STANDARD 10256273 941216 QTY ORDER NO NAME TYPE MANUF LINE 2 2 10855233 P C ASSEMBLY SENSOR BOARD RAC 10455232 20 3 l 10355274 BODY AL PLATE 5 5 NTL 5 30 4 1 10454666 BRACKET FE PLATE S 2 5 NTLS 40 5 1 10454867 PLATE FE PLATE 22 143 1235 129 7 50 7 1 10455276 LOCKING RING MS 520 NTL 5 70 2 10455277 PLATE i FE PLATE 2 5 NTL 5 80 9 a 10455278 PLATE 2 FE PLATE 2 5 NTL 5 9 10 1 10455062 WHEEL 1 URETHAN 87 SHORE A 100 11 1 10455279 BUSHING MS ROD D18 NTL 5 110 12 1 10455280 AXLE 1 DSH NTL 5 120 13 1 10455063 WHEEL 2 URET
95. REW M2 5 4 FE BLACK 135 15 1 10461951 INSULATOR PLATE PRESPAN 5 0 5 280 Ci 1 11626002 CAPACITOR H V 2 5NF 3KV DD30 252 50 ca 5 4 11626008 CAPACITOR H V 150PF 3 0KV 20 505 9 0130 9 D FERROP 40 Ri 1 11601149 RESISTOR 10K 2 0 54 B 1 2 BEYSCHLAG 100 RZ 1 11604049 RESISTOR MF SM 100 1 0 125W 100PPM CROW1206 90 R3 7 10 14 1 20 11604241 RESISTOR MF 5M 1 00M 1 0 125W 100PPM CRCW1206 60 R8 15 22 29 4 11604225 RESISTOR MF SM 464K 1 0 125W 100PPM CRCW1206 70 R9 16 23 30 4 11603568 HY RESISTOR 22Mohm 5 0 5W 31 5kVDC 232224213226 95 R31 34 4 11604205 RESISTOR MF SM 215K 1 0 125W 100PPM CRCW1206 30 S1 8 1 111 11863070 P C CONNECTOR 40 PIN STRAIGHT SL1725 36G 20 90 Fig 1415 32 HV Divider Unit AS 340427 AS 1452 4 951130 AS Kor 276 640005 Tha HE 2510 6 30610 HE 2158 91 10355373 m 9g DEN O 855 o 383 a a Fig 1415 33 Display Unit 10859287 96 10 10 FOR PART NUMBER 10859287 DISPLAY UNIT 1415 10355598 960612 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 1 10854665 P C ASSEMBLY DISPLAY HDG 10254761 510 2 1 10854760 P C ASSEMBLY DISPLAY CPU HCE 10354758 520 3 1 10259283 BOX ASSEMBLY 1415 240 4 l 11842036 TOUCH PANEL 010377 550 5 2 11250001 WASHER A1 2 570 B 4 11278002 NUT M3 FE YELLOWPASS 90 9 1 10557386 LABEL PVC FASKAL 400 T 0 1 1410 RESET 600 12 2 11480049 FERRITE CLAMP 26 WIRE FLAT CABLE 28B2022 000 610 13 2 11480050 CLAMP FOR 26 W FLAT C CLAPM M CLIP 620 14 1 11240162 RF GASKET 3 2X4
96. REW M4 8 FE YELLOWPASS 260 29 12 11274012 SCREW M5 10 FE YELLOWPASS 290 30 1 11274088 SCREW M3 20 FE YELLOWPASS 300 31 6 11274133 SCREW M4 6 FE BLACKPASS 310 iz 4 11274134 SCREW M5 10 FE BLACKPASS 320 33 2 11276030 SCREW B4 2 22 FE YELLOWPASS 330 38 1 10455763 COVER ASSEMBLY NTL5 231 35 z 11276015 SCREW B2 9 6 5 FE YELLOWPASS 340 36 1 10456094 EDGE STRIP FE PLATE 5 1 NTLS 241 38 6 11250041 WASHER 4 3 9 0 B FE BLACK 360 39 2 11290013 FOOT D12 3 RUBBER WHITE 3M SJ 5012 370 40 4 10456131 WASHEH FE PLATE 5 2 LSC 5 242 44 1 10459978 EXTENSION ARM MS D 8 140 10 45 1 10459979 MOUNTING PIN MS ROD Di0 1409 15 46 11274031 SCREW M5 12 FE YELLOWPASS 295 PART HISTORY FROM 91 09 25 TO 88 10 10 FOR PART NUMBER 10855461 TOP COVER ASSEMBLY 10255462 940623 ITEM NO QTY ORDER NAME TYPE MANUF INF LINE DATE 1 1 10855445 SPRING ASSEMBLY 10455446 NTL5 10 930812 10255462 Fig 1409 1410 1411 05 Top Cover Assembly H a KAYTDSSA VAIN 1415 USED ONLY 1415 10 25 5462 Piirt 381109 us Tork 881109 Ma Hyv A109 Z 29 Fig 1409 1410 1411 06 Sample Changer 10855338 96 10 10 FOR PART NUMBER 10855338 SAMPLE CHANGER 10255338 910603 ITEM NO QTY ORDER NAME TYPE MANUF IMF LINE 1 1 10855197 SAMPLE CONVEYOR 1410 10155198 10 2 1 10854857 ELEVATOR ASSEMBLY 1410 10254858 20 4 2 11274031 SCREW M5 12 FE YELLOWPASS 40 26 Fig 1409 1410 1411 06 Sample Changer 10255339 10 25 5339 27 28 F
97. S 2171 40 3 11271016 SCREW M Jrd FE YELLOWPASS 219 4i 1 10855115 POWER UNIT 10255116 12 42 1 10855188 POWER RACK 13 45 i 10555187 VME RACK 14 44 1 11690045 FAN 24VDC 5W 2800RPHM 4314 350 45 1 11690040 FINGER GUARD 9 601 43 3850 46 13 11274015 SCREW M 5 16 FE YELLOWPASS 241 47 d 11250001 WASHER A1 2 166 n 4 11271025 SCREW 3716 FE YELLOWPASS 218 49 4 11278002 NUT M3 FE YELLOWPASS 279 4 10455327 BUSHING POM D30 BLACK NTLS 156 51 2 10455938 BRACKET FE PLATE 5 1 NTL 5 151 54 1 11274030 SCREW M FE YELLOWPASS s 255 55 1 11480047 FERRITE CLAMP D 6 6 MM aB8p2025 OAQ 400 56 1 11420048 FERRITE CLAMP D 13 MM 28B2024 0AO0 410 57 2 11480045 FERRITE CLAMP 26 WIRE FLAT CABLE 28B2022 D00 420 58 11480050 CLAMP FOR 26 W FLAT C CLAPM M CLIP 430 59 2 11480052 FERRITE CLAMF 40 WIRE FLAT CABLE 28B2001 000 440 au 1 10462059 INSULATOR TEFLON PLATE T 1 157 TR 1 11650053 TRANSFORMER 2774 SRV 0 45VA 300 w11 19 1 10858057 1410 FRAME WIREING CA 23 30 SYT 25 W20 W21 WZ 3 10855441 FLAT CABLE 268 2 268 FC31 09 w23 1 10855442 FLAT CABLE 345 2 345 405 FC32 10 W27 1 10855593 WIRING ASS CA36 17 W30 1 10856412 WIRING ASS CAS1 16 PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 10854916 BODY ASSEMBLY 10154917 960503 ITEM NO QTY ORDER NAME TYPE MANUF LINE DATE W27 1 10855593 WIRING ASS CA35 15 930512 2 1 10354920 BOTTOM PLATE FE PLATE S 1 5 20 941026 52 0 100 11550112 INSULATING TAPE S 1 2 1 6 FOR PLATE CE 016 310 941027 55 11
98. TEPPING MOTOR SV LA 1 8AST 0 4NM PH2652 04 QU 1 11690044 STEPPING MOTOR 12V 0 4A 1 8AST 0 28NM 6500 15 4 13 5 R455 210 1 11690050 STEPPING MOTOR 1 5IN 0 73 STEP ANCI 8 6500 R568 ill 1 10855233 P C ASSEMBLY SENSOR BOARD RAC 10455232 220 1 10855235 P C ASSEMBLY SENSOR BOARD HsV 104552314 230 1 10855231 P C ASSEMBLY SENSOR BOARD Ras 10455230 240 1 10356622 1410 OPTICS MODKIT 1410 250 1 10853686 ID UNIT 1205 RSJ 10354300 260 1 10855313 WIRING ASS CALS 270 1 10055668 P C ASSEMBLY RAMCODE READER RAM 10355667 250 1 10855385 P C ASSEMBLY RXA HOME SENSOR BOARD RXA 10455384 290 1 11760040 PHOTOMULTIPLIER D13MM 10DYN 12PIN R1166 10 300 1 10855243 P C ASSEMBLY POSITION SENSOR RSU A 10355242 316 1 10855186 P C ASSEMBLY CONNECTION BOARD RSP 10455185 320 1 10854760 P C ASSEMBLY DISPLAY CPU ACB 10354759 330 1 108531794 P C ASSEMELY PREAMPLIFIER BOARD RAE 10353795 340 1 10857681 PREAMPLIFIER UNIT 1409711 10 DYNODE 10455394 350 1 10860150 PREAMPLIFIER UNIT 1409 11 15 12 DYNODE 10455334 355 1 10856793 P C ASSEMBLY PREAMPLIFIER BOARD RAP 10353795 360 2 11611025 TRIMPOPENTIOMETER aK 10 0 56 CERMET TWERIK 370 2 11611024 TRIMPOTENTIOMETER ZK r 10 0 5W CERMET 67WR2K 380 2 11611032 TRIMPOTENTIGMETER 10K 10 0 5 CERMET 67XRIOK 490 2 11611033 TRIMPOTENTIGMETER 100K 10 0 5W CERMET 67XRIOQOE 400 2 11611026 TRIMPOTENTIOMETER BOOK 10 0 5W CERMET 67WRSGOK 410 12 11601165 RESISTOR 470K 2 0 5W E 1 2 BEYSCHLAG 420 12 11601173 RESISTOR IM 2 0 5W B 1 2 BEYSCHL
99. TI 361 22 Paw m A um Sr Me na E 7 Peo om Qu ER E e ud NA Y N N X 8 Tl m e 10 15 5198 A F g 1409 1410 1411 04 Floor Stand 10256021 10 25 6021 Fig 1409 1410 1411 05 Top Cover Assembly 10855461 96 10 10 FOR PART NUMBER 10855461 TOP COVER ASSEMBLY 10255462 940623 ITEM NO GTY ORDER NO NAME TYPE MANUF INF LINE 1 1 11391026 GAS SPRING 16 1 168 135 40 245 2 1 19355463 PLATE RIGHT ASS NTL5 30 3 1 10355467 PLATE LEFT ASS NTL5 40 4 1 10355470 SUPPORT BOX ASS NTL5 20 5 2 104155473 PLATE FE PLATE 5 1 5 NTLS 60 6 e 10455474 PLATE FE PLATE 1 NTL5 70 7 2 10255475 SUPPORT 10x25 NTL5 20 B 1 10355476 HINGE BODY RIGHT PE PLATE S 1 5 NTLS 90 n 1 10355477 HINGE BODY LEFT FE PLATE 5 1 5 MTLS 100 10 2 10455000 SPRING D2 NTL5 110 Il 2 10455478 GUIDE DEHE NTL5 120 12 2 10455473 FLATE POM BLACK D 12 NTLS 130 13 z 10455480 BRACKET NTL5 149 14 1 10255481 TOP COVER NTL5 150 15 1 10254553 COVER PLATE 5 5 NTLS 160 16 1 10355438 HINGE RIGHT FE PLATE 5 1 5 NTL5 170 17 1 10355489 HINGE LEFT FE PLATE 5 1 5 NTL5 189 13 6 10455490 NUT MS D18 NTL5 190 19 2 106455491 PIN DZ 5 NTL5 200 20 1 10455492 SUPPORT 8 2X8 2 NTLS 210 21 1 10455493 PLATE POM PLATE 5 3 NTL5 220 22 1 10355494 HANDLE POM PLATE 5 25 NTL5 230 24 1 10855453 INSULATION SET NTLS 20 25 2 11250008 WASHER 4 3 9 0 8 FE YELLOWPASS 250 26 12 11250010 WASHER 58 3 10 1 FE YELLOWFASS 260 27 1 11251015 PIN 2 10 ST ATO 2B 2 11274005 SC
100. TOCOL DATE 19787 02718 TIME 00 25 FILE E AFUSIASOISTGPITAGOOL TXT ID r F17AS001 Wallac i414 Wintpectrai v1 30 S N 4140187 Counting mode CPM isotope s HS H 3 q 350 12 43 y Frotocol name m amp Er amp Bg Ophss protocol Counting time i 14400 Repeats 1 Cycles a 1 Replicates z 7 sigma s 1 00 Minimum cpm E 9 00 Checking time 10 Advanced modes FSA PSA level zg Output to Printer POS CTIME SOFPI CPMNwl CFMwe CPMws FNCTS Additions to Frinter Listing Output to Display 5 FOS CTIME SPI PM w CPMw2 CEM FNET1 RACKFOS CRM CRM Additions to Display Spectrum Listing Path of File 3374140197 Output to File POS CTIME SQPI CPMwI CPFWwZ CFMwS FNCTI gi bh kh Additions to File t Spectrum Listing Spectrum Alpha Beta Window i s 370 670 Deta Window 2 S70 670 Alpha Window 3 1 1024 Beta Window 4 1 1024 Beta Window 3 1 1024 Beta Window 6 1 1024 Beta FNCTL FNETI 1O08CPMW2 CPMW1 CPMW2 3 FNCT2 FNCT2 FNCTS FNCTS FNCT4 FNCT4 Unknown samples Fos LTime SQFI CPMwi CPMw3 1 12542 3597 48 15 0 7881 6 199 1 79 9 2 72 946 63 1507 2 TaT 65359 2 o 14400 389 54 61 3 47 0 4 0 Total count rates H 1296 2 DPM A 249 999 CPM ch 289 91 min S414B189NP1 8S881SS804B181 8B1 SPH 4 Bi 0 868 CPM ch 231 83 min 54148109SNSP17 S801sS80830814101 98B81 SPH 4 L 1 i 1 i t t I L Aa s 1
101. TOSSA VAIN 1415 LESD OPTION 10 15 5600 5 LSC 1410 P rt 881220 YS Tark 881220 Ma Hyv 881220 e Fig 1415 27 Measuring Unit 10354850 10 35 4850 TM ark 881115 Ma Hyv 881115 ge 81 u Fig 1415 28 Optics 10859277 96 10 10 FOR PART NUMBER 10859277 OPTICS 10356123 930916 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 1 10559276 LIGHT SHUTTER UNIT 1415 10354823 160 2 1 10354851 BODY NTLS 170 3 2 10256157 REFLECTON ULTEM 1000 NTL5 180 5 2 10457768 RING POM ELACK 1410 200 6 2 10454853 TURE CU TUBE D 57 52 NTLS 210 7 l 10358896 SHIELD 1 FE PLATE S 1 1415 220 B 1 10358897 SHIELD 2 FE PLATE 5 1 1415 230 3 5 11271045 SCREW M 3 5 FE YELLOWPASS 240 10 2 10556418 P C BOARD 1 6MM 1 P EP RXI 260 11 2 11271107 SCREW M2 5 6 MS 270 12 11278017 NUT Mz 5 FE YELLOWPASS 280 13 2 11460001 SOLDERING TAG D 5 5 3 5 8 A3021 ME 290 14 4 11250042 WASHER 2 7 5 0 5 ina Dl D2 2 11784015 DIODE LIGHT EMITT D3X gt YELLOW MV5374C 250 82 Fig 1415 28 i t e 2 ou 5 Na 2 en 10 n Optics 10356123 e A N ER Y wee LO 555 r a 7 D o Es ir m m a Fig 1415 29 Light Shutter Unit 10859276 96 10 10 FOR PART NUMBER 10859276 LIGHT SHUTTER UNIT 1415 10354823 950814 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 10553597 P C BOARD 1 5MM 2 F EF LK RRA 1205 1470 410 1 11863089 Plt CONNECTOR 5 P STRAIGHT LOCKABLE MLSS100 5B 420 1
102. UALITY BIS MSB 90 3 0 007 11120018 PRIMARY SCINTILLAT QUALITY PPO 100 4 1 10460181 SEAL p50 3 POM 1415 110 PART HISTORY FROM 91 09 25 TO 96 10 16 FOR PART NUMBER 10858914 GUARD 1415 10458913 950424 ITEM NO QTY ORDER NAME TYPE MANUF INF LINE DATE 3 0 500 11091022 SILICONE RUBBER 2 KOMP CLEAR RTV 615 80 950421 Fig 1415 31 Guard 10458913 e 10458913 89 a m Fig 1415 32 HV Divider Unit 10859369 96 10 10 FOR PART NUMBER 10859369 HV DIVIDER UNIT RFA 10359368 10355373 960607 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 11860001 COAXIAL CONNECTOR 11H4 50 3i 1 30 1 11460001 SOLDERING TAG D 5 5 3 5 8 A2021 ME 110 5 11250021 SERRAT LOCK WASHER 3 0 ANNEALED ZINKED 1 2 5 5 0 45 190 4 11250001 WASHER A3 2 00 1 090 11240035 COAXIAL CABLE RG 58 C U 210 1 10554024 P C BOARD 1 5MM 2 P EP LK RRH 1410 230 1 1 10358910 PLATE FE PLATE S 1 1415 260 Z 3 10454836 NUT MS 6K6 NTLS 240 3 2 11250035 RISE PIN M3 10 MS 5 03 1603 180 4 1 10454461 BOX ABS S22 1205 250 5 1 10544576 LABEL DANGER SERIVA 270 5 1 11310006 CLAMP MS 1 25 MEL A 3024 ASA 130 7 2 11320106 LOCK CARD SPACER NYLON KGLS 35 120 8 3 11271018 SCREW M 3 6 FE YELLOWPASS 170 3 6 11271019 SCREW M 3 8 FE YELLOWPASS 160 10 3 11271023 SCREW M 3 14 FE YELLOWPASS 150 11 11278002 NUT M3 FE YELLOWPASS 140 12 1 10556568 LABEL WHITE SELF ADHESIVE L BV OUTPUT TNPU T 220 13 z 11480047 FERRITE CLAMP D 6 6 MM 285B2025 0AO 115 14 4 11273013 SC
103. UTER DCD 10356465 55 8 1 10854554 P C ASSEMBLY L O BOARD DIC 103545583 75 9 1 10354606 PC ASSEMBLY MCA DIE 10354603 85 18 1 10853316 P C ASSEMELY POWER SUPPLY DPA 10353503 a5 11 2 10854021 P C ASSEMELY MOTOR CONTROL BOARD HPS 10354022 105 12 1 10859287 DISFLAY UNIT 1400 SERIES 10355558 125 13 1 10361359 BOX ASSEMBLY 1414 135 14 1 10350774 SIDE BOX RIGHT FE PLATE 5 1 0 1414 145 15 1 10360773 SIDE BOX LEFT FE PLATE S 1 0 1414 155 16 1 10455523 BOTTOM ASSEMBLY NTLS 165 17 2 10455328 CAM Da5 NTLS 185 18 2 10458890 GUIDE PLATE FE PLATE 52 3 1415 215 19 1 10455330 BUSHING D12 NTLS 1470 205 20 2 10455329 FLATE FE PLATE S 3 NTL5 195 21 1 10358884 LEAD CAST LEAD 1415 225 22 2 10358885 LEAD CAST LEAD 1415 235 23 gt 10358886 LEAD CAST LEAD 1415 245 24 25 Ab 27 28 49 30 32 33 34 35 36 i7 38 33 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 63 65 66 57 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 85 101 102 103 104 105 105 107 108 109 110 111 112 113 114 115 pi p gt B rb B bi a Ne A A A mb Cn o 2 ho LA tJ m PRPS FRO eE pa RS m RA MM Mh NM Mo BPR eR PREP Oo br o b pu bo s aes 0n 200 400 200 10458893 10255612 10455616 10355617 10355618 10455632 10355742 10461480 11710021 10559262 10555672 10494512 10548122 10355677 10355686 10455723 10455797 11250008 11250010 11250019
104. Unscrew and remove the PC board fig 3 4 Pull the top cover forward and remove it fig 5 7 Fig 5 4 Remove the PC board Fig 5 7 Pull the tap cover forward Install the lead shielding for 1414 001 WinSpectral as Unscrew the top cover screws fig 5 5 shown fig 5 8 the lead sections are numbered 1 2 1 3 Y Y y gt Fig 5 8 Installing the shielding tor WinSpectral In the case of 1414 002 Win Spectral o B first place the two iden tical pieces of lead Mes 5 9 shielding with shielding for metal supports On WinSpectral Remove the additional screws securing the inner cover top of the PMTs xB fig 5 6 around the tube for he counterweight see fig 5 9 Fig 5 5 Releasing the top cover 5 2 Installation information When you have done this proceed with the following Installina th instructions which are the same for 1454 002 Win sta 9 e stand by power Spectral amp B and 1414 003 Guardian see the follow supply fuse ing three figures During transportation the stand by power supply 15 disconnected Install the fuse after the lead shield n The shielding should be installed in the order shown in Stallation fig 5 13 fig 5 10 Fig 5 10 Installing the shielding for Fuse WinSpectral o B and Guardian There 15 additional shielding to install around the vial sensor fig 5 11 and under the instrument on the Fig 5 13 Stand by power supply fuse bench centred on the el
105. WASHER 5 3 10 1 FE YELLOWPASS 260 27 1 11251015 PIN 2 10 ST 270 28 2 11274005 SCREW M 4 8 FE YELLOWPASS 280 29 12 11274012 SCREW M 5 10 FE YELLOWPASS 290 30 1 11274058 SCREW M3 20 FE YELLOWPASS 300 31 6 11274133 SCREW M4 6 FE BLACKPASS 310 32 4 11274134 SCREW MS 10 FE BLACKPASS 320 33 4 11278002 NUT M3 FE YELLOWPASS 330 34 1 10455763 COVER ASSEMBLY NTLS 231 35 2 11216015 SCREW C 2 9 6 5 FE YELLOWPASS 340 46 1 10456094 EDSE STRIF FE PLATE T 1 NTL 5 241 38 6 11250041 WASHER 4 3 9 0 8 FE BLACK 360 39 2 11230013 FOOT D12 3 RUBBER 3M SJ 5012 370 4g d 10456181 WASHER FE PLATE T 2 LSC 5 242 44 1 10459978 EXTENSION ARM MS D 8 1409 10 45 1 10459979 MOUNTING PIN MS ROD Di 1409 15 46 4 11274031 SCREW M 5 12 YELLOWPASS 295 47 4 11250096 WASHER 3 2 7 0 5 FE YELLOWPASS 365 PART HISTORY FROM 91 09 25 TO 96 10 10 FOR PART NUMBER 10860806 TOP COVER ASS 1414 10260807 960321 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE DATE 24 1 10855453 ENSULATION SET 7 CODES 9 PARTS NTL 5 20 960307 6 2 10460760 PLATE FE PLATE 5 3 0 1414 70 960320 110 941216 AKO 350922 AKO 951010 AKO 951020 AKO 951026 AKO 551123 AKO 960402 AKO 950508 AKO 10160805 G 10860304 PIHT 940919 AKO TARK 940919 VS HYV 3310410 KLOU 10260807 Fig 1414 36 Top Cover Assembly O rm KORJ N 10260807 A 10860806 PHAT 940921 AKO TARK 940921 VS HYY 29 00 D 111 Fig 1414 37 Keybank Assembly 10860862 38 10 10 FO
106. a range of PSA values Ascertaining the correct PSA level is ideally done with two reference samples one that emits alphas e g Am 241 and the other that emits betas in the alpha spec trum range e g Cl 36 Sr 90 P 32 Count rates should be kept below a reasonable limit by dilution if necessary less than 10 000 CPM is recommended The reference samples must be made in the same type of vial same cocktail and same mixing ratio as the actual unknown samples to be measured A protocol can be created which steps PSA levels over a range which is appropriate for the cocktail See the User manual for details There are two extra windows that can be set which in range are typical for the alpha region but the first one is for measuring the beta spec trum short pulses while the second one 15 for the alpha spectrum long pulses The results are printed each line contains the CPM value for both windows the PSA level used and a calculated field RATIO which s the CPM value in the alpha window divided by the total CPM value For example you can select the final PSA level to allow from 0 5 to 5 loss of alpha counting efficiency alphas spilling into the beta channel In this way an almost pure alpha spectrum is acquired with the minimum loss of counting effi ciency In the same way when you are only interested in beta counting in the presence of alphas or glass originated background you may allow some percent age loss of beta cou
107. am of the conveyor moved by friction contact with two rubber belts Movement along the transfer lanes is by precision made toothed belts The conveyor ts coated by an electrically conductive teflon layer to re duce friction to 4 minimum and to prevent the genera tion of static electricity on the sample racks The con veyor motors run very quietly to avoid disturbance to users and others in the laboratory All movement is controlled by stepper motors and di rectly triggered optical sensors This removes the dan ger of sensors jamming and increases the reliability of the whole conveyor system Sample change time is about 9 secs Conveyor movement is fully bi directional With the OneRack function counting Is interrupted the rack in the counting position is driven backwards so that you can load a single rack for stat counting After this rack has been counted counting of the other racks resumes automatically You do not have to remember to put the interrupted rack back at the head of the in stream later Coloured dot mc le 2 m lm N Empty stop rack on because it is already in the right position to resume counting Multi size racks and vials You are no longer limited to using only one size of rack on the conveyor if you have the appropriate op tions With FlexiRack I you can load racks of twelve 20 ml samples along with cacks of eighteen 6 ml samples With FlexiRack II you can not only load racks of the abo
108. an and free of dust This is most easily accom plished if al surfaces are as smooth as possible and tf the minimum number of extra surfaces is introduced into the room Lastly it is extremely important to store ail radioactive materials in a separate room to which access is restricted 6 3 6 2 Safety information 6 2 Safety information 6 4 6 3 Routine maintenance Keeping the instrument clean The conveyor cover should always be closed to pre vent dust from getting onto the conveyor and into the electronics below the conveyor If there is still dust and other dirt on the conveyor then remove the dirt by a dry clothing ID labels Check the labels on the ID clip Those in bad condi tion should be replaced by new ones to guarantee cor rect reading of the labels When frxing ID labels on the clip ensure that the area where the labe is to be fixed ts clean e g there 1s no perspiration from your fingers on it Power supply fan Check that the cooling fan in the power supply unit is working by listening for its sound Cables Check that the power cable and the cables to the pe ripherals are tightly connected and that the cables and connectors are not damaged Any damaged cable should immediately be replaced Response mapping MCA calibration What is response mapping The quench correction system and DOT DPM tech nique make use of built in libraries of information de rived from a reference counter Response mappin
109. ases The various flags that can appear are given in Output items in the User manual After a second recount if there is one the result of the second recount will be appear as output then counting of the next sample or repeat will begin The chemiluminescence monitor and correction fea ture as well as the special static eliminator allow the correction of chemiluminescence if tt persists and static is eliminated anyway However the Statistics Monitor gives you an independent check on sample count rate variation and avoids results based on unex pectedly high sample count rate variation being ac cepted undetected Advanced statistical result evaluation If you want to do statistical analysis on your results as many do especially in a research environment then your Wallac WinSpectral provides you the tools you need You can get quench monitoring errors DPM er rors theoretical errors observed errors chi squares to mention but a few In addition you can select trend plots and frequency distributions You do not need to go to an external statistics program to do the analysis The Spectrum Plot option allows the printout of the sample spectrum atter the numerical results The Spec trum Plot option also allows the sample spectra to be sent and stored on the datalogger PC or Mainframe if corresponding options are installed The Statistical Plot option allows a graphical presenta tion of the result to be added to the printout
110. asurements no quench curve measurements are needed for spe cific isotope combinations in dual or triple label count ing no window settings are needed result quality is not dependant on isotope ratios successful fit gives assurance of sample quality no systematic errors caused by colour quench no plastic vial effect no volume dependence DOT allows for analysis of the fine structure in the isotope spectrum which can be used to warn the user of phase separation contaminations or other phenom ena which will give erroneous values Accuracy Enhancement for even better re sults A typical DPM measurement includes determination of quench level with the help of the external standard calculation of the counting efficiency corresponding to the quench level with the help of a quench curve counting of the sample to obtain sample CPM and then the final DPM calculation The critical factor which determine the quality of the DPM results is how correctly the counting efficiency was determined The accuracy of the counting effi ciency value is totally depending on how accurate the External Standard Quench parameter ts and how ex actly the quench curve used represented the unknown samples The external standard values suffer from counting er ror due to the counting statistics The modern external standard quench parameters are usually calculated from the endpoint of the external standard spectrum and depend on the s
111. build up because the samples are located in round holes in the rack without any sharp edges which tend to collect static charges more easily The light shutter is in the form of two plates which close around the stem of the elevator af ter the vial is in position There 1s also a Statistic Monitor which flags any sam ples which show signs of static electricity discharges Automatic continuous spectrum stabilization ACSS LED Calibration pulse Sample spectrum NT ACSS system You need to be sure that your instrument is stable You do not want changes in high voltage temperature detectors or aging to affect the accuracy of your re sults The patented built in automatic continuous spectrum stabilization system ACSS offers gain sta bility for your Wallac WiaSpectral counter without the need to measure reference samples This system is completely automatic and requires no user interven tion The principle is to detect when a change that would affect the gain of the instrument occurs and by means of a feedback loop to correct for the change so that the gain remains stable Each photomultiplier has a tem perature compensated reference light emitting diode LED which is fixed close to each detector and is used to check the gain of the PMT see the figure above A reference pulse is produced in the photomul tiplier 10 times a second The ratio of the pulse pro duced at the first dynode to that produced at the an
112. cay Chemiluminescence Why is chemiluminescence a problem About two thirds of all samples in LSC are of biologi cal origin which means that they comprise long macro molecules In order to get them soluble in organic scintillator solution these macromolecules have to be hydrolysed to smaller fragments This process often results in the release of chemiluminescence in sam ples How is it solved There are two levels of solution to the chemilumines cence problem the first of which is common to most beta counters and the other is specific for Wallac Win Spectral DSA counters Chemiluminescence events are single photon ones Each time chemiluminescence occurs a single photon is emitted in one direction In contrast a normal radio active decay releases a burst of several photons in dif ferent directions a multiple photon event A beta counter has two detectors viewing the sample vial from opposite sides A chemiluminescence event or any other single photon background event or random noise event in a detector will trigger only one of the detectors whereas a radioactive decay will trigger both detectors almost simultaneously By requiring that a signal be received from both detectors within a few nanoseconds and by rejecting signals that only come from one detector or the other most of the chemilumi nescence and random background can be cut out However there are limits The period of a few nanoseconds referred to abo
113. cted value in the range 5 C below ambient to 10 C above The temperature control system is based on two thermoelectric Peltier modules which en ables users to adjust and control the temperature via software A more powerful external cooling system 10 C be low room temperature can be added later if needed A parameter called TEMP in the programmable output allows you to output the temperature at which sample measurements were made External standard for higher precision DPM The wide range of vial types accepted by Wallac Win Spectral counters puts greater demands on the external standard parameters than ever before If the count rate of the externa standard depends on the sample vol ume the few microlitres in a Microfuge tube will give a low count rate To avoid this the isotope of the exter nai standard is Eu which belongs to a lower toxic dy class than previously used external standard iso opes which means a higher activity can be used thus Hardware features and benefits allowing the external standard count ume to be re duced and the counting precision increased The external standard source is mounted on a wire which moves it from its rest position in its own shield ing to just beneath the sample vial This arrangement allows the external standard to be positioned very ac curately beneath the sample vial it actually moves through the sample elevator shaft to a position beneath the sample The exter
114. d in place by again pinching the shield ISO test The capsule has been tested by the Quality Assurance department of Wallac Oy according to the ISO 2919 standard The rating C43434 has been achieved External standard transport system The transport system is illustrated in document 1036 1092 The standard 15 mounted on a metal wire which is moved by two friction wheels controlled by a stepper motor and two sensors The capsule has two stable positions in the transport system one in the storage shielding and the other in the measuring chamber inside the lead shielding The storage shield is made of lead thickness 50 mm and is equipped with a radiation hazard warning label This includes a definition of the isotope and its activity The capsule is transported to the measuring chamber along PA polyamide tube and stainless steel elevator tube The transport time is less than 3 seconds Disposal of the capsule When the instrument is no longer in use the Eu 152 standard capsule must be removed and sent to the appropriate radiation safety authorities or to Wallac for safe disposal This procedure must be performed only by a qualified Wallac service engineer am pesi EE i i 79 941212 AS __ nn A WE STAINLESS STEEL AISI 303 WIRE STEEL STAINLESS STEEL ASI 303 Peel o be imparted to m LMAir para y Pr DE ita lor any uu PUDO TE
115. dity 6 1 ID clip See PosIden ID reader ID labels See PosIden ID reader Initial time See Radioactive decay Installation instructions 5 1 Ionizer 1 4 see Static electricity L Lead shielding installation 5 1 Locking fine tuning 1 14 Mapping response 6 5 MCA dual programmabie 1 6 MCA calibration See Response mapping Microprocessor 6 2 Monitor See CPM monitor See Sample count rate variation See Sample quality P PAC 1 11 PC Connection to counter 5 3 Plastic vial effect 1 9 Port serial parameters 5 5 PosIden ID reader 1 3 6 1 Printer 5 3 PSA 1 10 Pulse amplitude comparator 1 11 Pulse shape analysis 1 10 Q Quality See Sample quality Quench index 3 2 R Racks 6 1 Sizes 1 3 Radioactive decay Half life correction 1 12 Problem of decay 1 12 RAM 6 2 RATIO 1 11 Reference samples Positions 1 8 Reference spectra 3 2 Repeat counting statistics 3 4 Replicate counting statistics 3 4 Response mapping 6 5 ROM 6 2 Routine maintenance 6 5 S Safety 6 3 sample count rate variation Problem of 1 13 Sample quality See Monitor Serial port parameters 5 5 Shielding 6 1 Multi section passive shielding 1 5 Shielding installation 5 1 Specifications 6 1 spectrum Library use in DPM counting 1 8 spectrum analysis program 1 14 Spectrum quench index 3 3 Error 3 4 Spectrum stripping See Background correction SOPE See Total quench index SQP see Spectrum quench index SOP D DOT 1 9 Stability 6 2 Static el
116. e all make for ease and convenience in operating the system while keeping the footprint in the labora tory to a minimum Software features and benefits Windows graphical user interface Older types of LSC software still run under MS DOS a character based operating system Since MS DOS does not allow the possibility of mulutasking any ap plication program or commercial software must be run after the counting protocols Thus kind of sequential operation inhibits the effectivity of a busy research team The new generation WinSpectral software running un der Microsoft Windows offers dozens of features No longer are you limited to 640 kB of memory or charac ter based software packages You can exchange data between WinSpectral and any Windows compatible software The graphical user interface itself is intuitive and easy to use Operation involves clicking buttons or icons with a mouse pointer or selecting items from menus on the PC screen Hypertext help All steps of operation are guided by comprehensive context sensitive help screens conforming to the style you are used to with other Windows software pack ages Simply press the Fi key to get help for just the point of operation you are at You can use the help to search for information on any feature you like The hypertext links enable you to instantly jump in the help to other related pieces of information The hy pertext help is truly manual at your fingertips Easy Co
117. e different parts of the system Instrument on off switch and sockets for cables to PC and raw data printer Output printer Hardware features and benefits Hardware features and benefits Elegance The first things that comes to your attention when you look at a Wallac 1414 WinSpectral DSA liquid scintil lation counter are the elegant lines of the conveyor cover and the conveniently placed PC screen key board and mouse These impressions of elegance and convenience are not just superficial features of the counter they run through every aspect of the Win Spectral hardware and software These features and the benefits they bring you are described in the follow ing chapters FlexiRack sample changer The conveyor is designed to give the maximum visi bility to the user You can easily see the sample racks wherever they happen to be on the conveyor The cover of the conveyor is made of a plastic which both allows a clear view of the conveyor yet shields the samples from ultra violet fight and thus reduces the problem of chemiluminescence The cover is sup ported by a spring loaded lever so that it opens and closes smoothly Conveyor cover Disk drive cover Loading racks on Wallac WinSpectral The sample conveyor has two lanes for sample racks an in stream on the right and an out stream as well as two transfer lanes one of which is the counting lane Sample racks glide along the in stream and out stre
118. e reference time fo is the time elapsed at the end of the counting period since the reference time and 7 72 is the half life Chemiluminescence correction chemiluminescence spectrum is recorded at the same time as the normal uncorrected spectrum by using the delayed coincidence principle After meas urement the measured spectrum is corrected by sub tracting the delayed spectrum from the normal spec trum channel by channel The percentage of chemilu minescence CLM 15 computed by the formula CLM 100 lt where yge is the number of counts in the delayed spec trum and y is the number of counts in the normal spec trum Statistics of repeat replicate counting The mean value of n count values v is _ Y n 2 Yi i Note It is assumed that the counting times of all n repeats replicates are the same The theoretical standard error o or standard devia tion of each measurement is equal to Vy The stand ard error of the 4 measurements is equal to G N 2 TEDI l while the observed standard error G of the mean is equal to G The theoretical standard error oy of the mean 15 equal to Gy 1 H zo NE Fi Oy The theoretical standard error oy can be compared to the observed standard error Gy by using the reduced yr Chi square value BL 2 r gt Oy The degree to which ye deviates from unity is a direct measure of the
119. ectricity 1 4 Ionizer 1 13 Problem of static 1 13 Statistical analysis How to do it 1 14 8 2 Statistics monitor See Sample count rate variation Surface function 3 3 T Temperature Control 1 5 6 1 Environmental 6 1 Total quench index 3 3 Error 3 3 Trend plots See Statistical analysis V Volume dependence See DPM counting 8 Index
120. er Spectrum Auenen standard samples CTime H3 CEM Hz CPHMer 600 1945 0 0 00 EEPROM LISTING Reo TEMP CONV Listing 5 Beta HZ ERX CHF Ec 0 64 GORE 1 00 965 19 x 199 AQ 100 Al Q zw STEPS 112 Mapping a t a Channels ALTE TRUE TRUE WLIB 0 0 Oo 9 0 47 7 ad 10 7 gu Z uU 137 8 137 5 0 3 156 1 104 6 1 5 175 7 171 7 a O 1921 ni ij Ir x 210 6 203 6 1 9 3 At i LA i BI I x D Led te CH tn iz 3 ya 6 FOS 1 G d TTR 90 25 t IA a t J e brt C J al 912 mum LH pkeR doi RII RE d PR TER HI GUITL GELD TRIN FIRES Tram is as abend ana Happing lip ae 4 L i TRUE ch 5 188 aL it m T T TT T TU Tq T T U T 253 cac HL IE ch Total activity H3 194500 0 DPM 3 242 kBq PROTOCOL 5 SH 14C DATE 1998 02 13 TIME 16 33 ID POFASOLE Wallac 1414 WinSpectral Counting mode Isotope s Hs 14 Protocol name Counting time Repeats Cycles signa A Minimum cpm Output to Printer EG Wallac std v1 30 S N 4140189 2 CPM H3 014 Ee 350 12 47 y S 660 5730 00 y i H a SH 145 BG Wallac std 1200 4 5 1 a 1 E 0 30 4 00 Checking time 10 POS CTIME CPM1 CPM2 SOPI SQPE Additions to Frinter Dutpur to Display Listing z FUOS mRAaACEPOS GPM RFT SOPI CPMI CPMZ Additions to Di
121. es or cycles high resolution printout of measured spectra For the laboratory with recurring routines the Wallac Spectrum Analysis Macro Program allows macro pro gramming of often repeated analysis routines and sum ming subtraction of spectrum files Password protection Y ou can set a password to protect any protocol LSC fine tuning or Easy GLP This will mean that the pro tocol can be used by those not knowing the password but it cannot be changed To unlock a protocol so that you can change it you must give the password first H the password is forgotten your local service repre sentative can get access to the protocol How to proceed Part 2 is for the User manual which you will find in the package with the program disks This gives you all the information you need to operate Wallac WinSpec tral You can keep this manual in this Instrument man ual or use it separately with the instrument Part 3 describes the methods used for calculating re sults Part 4 contains the Quality control information that comes with the counter Part 5 gives you information on how to Install and start the instrument Part 6 presents the instrument specifications gives safety information and describes routine maintenance that can be performed by the user Part 7 contains spare parts information Part 8 is the alphabetical index for the Instrument manual excluding the User manual which has its own index We at Wallac trust that y
122. evator see fig 5 12 Replace the instrument covers Installing the PC keyboard shelf Assemble and ftx the PC keyboard and mouse shelf product number 10860862 and the monitor stand 1414 160 following the instructions supplied with them see fig 5 14 Monitor A Diskette drive stand SIME behind cover Fig 5 11 Extra shielding for WinSpectral dB and Guardian Fig 5 14 WinSpectral peripherals Checking the mains voltage setting Measure and note the mains voltage at the outlets to be used Locate the mains selector switch this 1s on the left Extra shielding i i side when looking at the rear of the instrument If nec ng 5 12 Extra shielding underneath WinSpectral o B and essary adjust the mains selector switch to correspond nardan with the measured supply For supplies with a nominal 5 3 Installation information WinSpectral Cables Options 1221 470 9 pin 1221 503 9 pin with shielding 1221 459 25 pin Fig 5 158 Cables when raw printer connected to PC WinSpectral Raw data printer Any Epson Fx compatible Fig 5 15b Cables when raw printer connected to WinSpectral voltage of 230 V it is recommended that the selector be set to 240 V Check that the fuses fitted in the fuse carriers on the back panel are of the correct rating for the local sup ply and according to the label Connecting the counter and peripherals Connect the counter to the PC and the pr
123. extras e g sample CPM as a function of sample number The Sta tistical Plot also include Levy Jennings type plot of repeat or replicate measurements Alternatively you can output results to MultiCalc or Excel for further evaluation Other computer interfaces Wallac WinSpectral can also save data in ASCII for mat files or binary WKS type files The WKS type files can be read directly into spread sheet programs such as LOTUS 123 Symphony or EXCEL Spectrum analysis option Note this feature is an option for 1414 WinSpectral and can be installed later for 1414 WinSpectral a B and 1414 Guardian it 15 built in Alpha counting and low level beta counting applica tions include spectrum analysis as a final step The counter saves the measured sample spectra in the connected PC The spectra can then be analyzed off line using the Wallac Spectrum Analysis program The Spectrum analysis program can be installed in the PC connected to the counter but also in a PC in the researcher s office The program offers Off Ime optimization of caunting windows display of up to three spectra simultaneously on screen smoothing and zoom function for analysis of details colour graphics calculations of Figure of Merit Counting Efficiency during on screen optimization calculation of radio carbon age calculation of tritium units litre for H in water statistical calculation and Levy Jennings plots of re peats replicat
124. f length x As the number of equations is much larger than the number of unknowns m this set must be solved by using the method of least squares In practice the method of weighted least squares is preferred in which the statistical accuracy of each count rate in C is taken into account The solution can be written as X Ss iS slew lac G where 5 represents the transpose of the model matrix and W represents the inverse of the weight matrix W The matrix W is an n by r matrix in which the diagonal elements are equal to the weight of each channel and all other elements are equal to zero A suitable weight value w is the inverse of the number of counts n channel 7 The errors m the vector X du due to the reference spectrum fitting are given by the equation Calculation methods dxj2 Nleid m in which denotes a diagonal element in the matrix G defined above Reference spectra The built in reference spectra sj are stored in the spec trum library by using Fractile Integral Presentation FIP The spectrum library data for an isotope is pro duced by measuring in the factory from 60 to 80 standards of the isotope In this standard set there is one subset with only chemical quench one subset with only colour quench and one subset with a mixture of both The spectra are stored 1n Integral form reduced to a limited number of channel values real numbers buy lt u q corre
125. g is the procedure by which a connection is established be tween the MCA channel values in your actual counter and the reference counter This allows the libraries in your counter to be customized to fit your counter in the case that there are small differences between it and the reference counter This is done in the factory before you receive your counter but mapping must be done again when the measurement electronics is adjusted or repaired or the PM tubes are replaced or the external standard capsule is changed Mapping can also be done at any time and it is recommended that it should be performed at least once 4 year as part of routine maintenance 6 5 6 3 Routine maintenance How to do response mapping Boot the instrument with the 1414 WinSpectral nstru ment program disk Create or edit a fine tuning protocol e g Finetuning 01 Set the protocol name to MAPPING Use the sealed H standard sample Set the DPM value accord ing to the value printed on top of the standard Set half life correction on and set the half life zero time according to the date printed on top of the standard set the counting time to 300 5 Save the protocol Load a rack with the sealed H standard sample onto ihe conveyor instream Other positions in the rack should be left empty start counting the protocol To stop the instrument after measurement of the map ping sample put an empty rack on the conveyor after the mapping sample rack
126. g the interrupt function The ID labels are supplied in a binder with 20 sheets of labels The ID Clips are supplied in a package of 100 The box on the PC keyboard shelf can be used to share the ID binder and clips Elevator reliability The elevator system is designed to handle a whole va riety of sample vials without the danger of the vials falling over or getting jammed The key to this is the small sized elevator head combined with the centraliz ing counterweight The counterweight meets samples before they are raised from the rack thus ensuring that they remain vertical all the time they are on the eleva tor Static elimination Plastic vials are widely used in liquid scintillation counting and manufacturers tend to use plastic also as a rack material Conditions are often optimum for the build up of static charge especially when relative hu midity is low central heating and lab technicians have to use plastic gloves during sample preparation as when using conventional toluene xylene and cu mene based cocktails Static build up on the sample vials 15 minimized both by the presence of ionizers around the sample elevator and by the fact that at no point does the vial come into contact with any material which might tend to deposit charge on it since a vial in the FlexiRack system is raised directly into the measuring chamber without making further contact with other materials The rack design also reduces static charge
127. hape of the spectrum With higher quench levels and smaller sample volumes the shape becomes more and more undefined and the counting error greater Consequently there will be bigger errors Software features and benefits in the external standard quench parameter and bigger DPM errors In the DOT method the SQP E value ts only the start ing point for an iterative procedure which searches the spectrum library for the spectrum which gives the best possible fit to the measured unknown spectrum The Accuracy Enhancement gives the following features Accuracy Enhancement minimizes the DPM errors caused by erroneous externa standard quench parame ter values Savings in time only a few seconds counting time is needed for the external standard even for samples with small volumes Normally the counting efficiency quench parameter relation s also dependent on the quenching agent and the cocktail used Thus if the samples are quenched by another quencher than the one used for the quench curve systematic errors will occur With Accuracy En hancement systematic errors due to Quenching agents or different cocktails are minimized thus the applicability of the Wallac libraries is increased When using Easy Count it is not necessary to specify spectrum library or vial type Accuracy Enhancement will search through all variations to find the best fit SQP I DOT Single Label DPM The SQP D DOT option offers you single label DPM res
128. hi 202088 Hild LEDD Sea J 86SS5 0l JESSE 3 SLzO96 YS 038 SY BLZ156 57126076 Sy SL 90476 93 94 1414 Supplement 1414 WinSpectral 1414 001 96 10 10 FOR PART NUMBER 1414 001 WIN SPECTRAL 1414 001 960505 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 10860678 WINSPECTRAL 1414 001 10160809 10 1 1410 405 SAMPLE TRAY FOR SAMPLE RACKS 1410 405 110 1 1440 401 RACKS 20 ML PACKAGE OF 10 RACKS 1410 401 120 1 1409 411 ID KIT 1408 411 130 0 500 1200 437 OPTIPHASE HISAFE 3 2X5 L 1200 437 140 1 1414 150 MONITOR STAND 600 MM 230 MM 150 1 10855584 PACKAGE 10455885 1410 170 10160309 120 1 10860852 KEYBAME ASSEMBLY 1414 10260855 160 a a Fig 1414 34 Win Spectral 10860678 96 10 10 FOR PART NUMBER 10860678 WIN SPECTRAL 1414 001 10160809 960404 ITEM NO QTY ORDER NO NAME TYPE MANUF INF LINE 1 10557653 F C ASSEMBLY SW KEY MODULE BOARD RIG 10457662 110 1 10556730 DCD EXPANSION KIT DCD 10356465 121 1 10855272 EXTERNAL STANDARD 10255273 122 1 10861091 STD CAPSULE 10361101 1400 SERIES 123 0 300 10856077 INSTALL KIT 115V FOR 1410 124 0 700 10856078 INSTALL KIT 250V FOR 1410 125 1 10446545 FOOT FAG BLACK 30 GLAS 1235 1470 408 1 10555509 LABEL SET FC33 FC207 412 1 10556126 LABEL VME RACK 1410 414 1 10551111 LABEL CSA APPROVED ALO 08 LRS2500 BRADY 416 1 16560490 LABEL SET CA22 12 DYN 420 0 300 10561102 LABEL WARNING STICK BRADY EU 152 10551102 LAB 422 1 10561342 LABEL PATENTS BRADY LABEL STD B PLATE 427
129. ibute to the delayed spec trum whereas the sample events will not Channel by channel stripping subtraction of chemilu minescence from the sample chemiluminescence spectrum is then done This maintains the exact shape of the sample spectrum by removing the exact chemi luminescence spectrum from the combined one The corrected CPMs are then used in further calculations The result is that you can cease to worry about chemi luminescence Just select chemiluminescence correc tton on and and your Wallac WinSpectral will took after the rest Isotope decay The problem of decay If you are counting samples labelled with an isotope such as phosphorus 32 with a half life of 14 2 days you are likely to face the situation where the count rate for samples drops over the course of an assay In this case there will be about a 1 change from the first to the last samples n three hours With longer counting runs or repeat runs over several days this could intro duce significant errors in your results 1 12 The solution When you are setting your LSC or measurement pa rameters protocol you select half life correction as part of the advanced mode parameter Since you will have already specified the isotope s used the counter will know exactly what correction to make In addition you can specify if you want the initial time for the correction to be the start of the counting of the assay or a date which you set See the User manual for de
130. ig 1409 1410 1411 07 Power Unit 10855115 96 10 10 FOR PART NUMBER 10855115 POWER UNIT 10255116 960112 ITEM NO QTY ORDERNO NAME TYPE MANUF INF LINE 1 10555703 LABEL SET 121 b 11310013 WIRE TIE 2 4 102 NYLON SSTIMPANDUIT 560 2 11862137 COVER FOR 3 F CONNECTOR TCLO6F 6 580 0 250 11450017 WRAPPINS SPIRAL 12 MM PLIOSPIRE 12MM 590 1 10850578 CONNECTION BOARD 1230 RPC 105505795 10 2 1 10850577 CONNECTION BOARD 1230 RPD 10650580 20 3 1 108583848 P O BOARD CONNECTION BOARD RPS a0 4 1 10255117 BODY PLATE AL PLATE 5 3 NTLS 40 5 1 10355115 COVER PLATE AL PLATE S 2 NTLS n0 5 1 10355119 BOX FE PLATE 521 NTL5 60 7 1 10455120 SEAL PRESPAN 5 0 5 NTLS TO B 1 16455121 SEAL paz 94u0 Sl 1 10355122 PLATE AL 5 4 NTLS 90 10 1 10355123 COVER FE PLATE 5 1 NTL5 100 11 1 16455124 SLIDE PVC LII NTL5 116 12 A 10454836 NUT MS GKG NTLS 120 13 1 11730016 ACCU PACK l2V 4AH NICD 10X NCLOVRA 220 14 1 11870048 CONNECTOR STRIP 3 P 2 5MMZ 32180503 230 15 3 11880025 FUSE HOLDER leA 250 FEU 031 1673 240 16 3 11880027 FUSE CAP FUSE 6 3X32MM FEK 031 1661 250 17 1 10555002 LABEL POLYETHEN 1205 ACCU 260 18 l 10548240 LABEL 1215 16 WALLAC 270 19 4 Ll250001 WASHER Ade 280 20 4 11250002 WASHER Ad 3 290 21 2 11250004 WASHER Ab 4 2M 300 32 4 11250006 WASHER 1 2 7 D0 5 FE YELLOWPASS 310 33 4 11250010 WASHER 3 3 10 1 FE YELLOWPASS 320 24 4 11250021 SERRAT LOCK WASHER 3 0 ANNEALED ZINKED i 2 5 5 0 45 330 25 1 11250012 WASHER M CU 340 6 5 11260015 RIV
131. imit and yp denotes the number of pulses below this limit Hence the error dr is given by dr r 1 None u Spectrum quench index The spectrum quench index SQP D can be used as an alternative to SQP E and Colour index for quench monitoring and activity calculations SQP is defined by the equation Calculation methods id iyi iH ul i SORT where H and ul are the lower and upper limits of the spectrum When using SQP 1 the Colour index is as sumed to be equal to the value for an uncoloured sam ple The error in SOP T is expressed as dSOP ei SOPA Cit Chat E i ci Crot SQP I i Lx i ci cro SQP D2 Chot where cy gt Cj i Background correction If a background sample is measured then the count rate cj is corrected by subtraction Cicorr Cj Cibko where Cicorr 1 the corrected count rate in channel and Cjbkg 1s the measured count rate in channel j In this case the correction is made before spectrum fitting If a background value is submitted then the count rate xj 15 corrected after spectrum fitting Half life correction Half life correction 1s performed on the count rate x and the activity a after spectrum fitting by using the equation 2 41 e Me n tha fa Auer in 2 yt 3 4 where In 2 is the natural logarithm of 2 t is the time elapsed at the beginning of the counting period since th
132. inter s using the cables shown in fig 5 15 above As well as the normal PC Windows printer e g a network laser printer you can also have a raw data printer Normally this will be connected to the PC fig 5 153 but you Windows printer LPT or An network printe Cable 1224 122 Raw data printer Any Epson Fx compatible Windows printer Note The factory settings of the printer may not correspond to those used in WinSpectral If printing does not function properly check the settings according to the information given in Serial port settings can have it connected to WinSpectral directly in port fig 5 15b The PC is connected to port 2 of the counter The third port is not used and should have a blanking connector 1086 0713 Further details of the settings for the printer are given in its own installation sheet which follows these instal lation instructions Plug in the power cables for each device Installing the PC software Install the WinSpectral following the instructions in the User manual After installation start the program by double clicking the 1414 WinSpectral icon in the WinSpectral win dow When the WinSpectral main window appears you will see at the bottom the status bar this is divided into four sections In the third and fourth there are the date and time respectively In the second there is a message about the communication status If the counter ts not
133. ional 69 others One error source in CPM counting 15 that of unex pected counting efficiency variations e g partial elu tion of the sample from the filter disk Your Wallac counter includes features to detect and inform the user of counting effictency variations as described below CPM monitor The CPM Monitor is another feature of your counter it allows you to be confident of the consistency of the quench level of your samples The CPM Monitor checks the SQP I value of each sample If this is within 10 of SOP D the first sam ple then there is no flag If the difference is larger it then calculates and outputs the percentage ratio of the sample SQP D to the first sample SQP 1 The accep tance limit default 10 is a system parameter and can be changed there see the User manual Spectrum stripping background correction The traditional methods for background correction are a typed in background CPM vaiue or a CPM value measured from a background sample in a counting window However the intensity of the background ra dation is different at different energy levels so these methods do not give the best result The new calcula tion methods in Wallac WinSpectrai DSA counters do Software features and benefits not utilize counting windows but use digital spectrum analysis DSA to calculate the CPM DPM values over the MCA area covered by the sample spectrum The background counting time is selected to be either the the same a
134. is not more than 5 years 1390 0171 AN di EGG COMPANY Doc no 10961059 M Ala Uotila Electrical safety routine test report 1400 DSA 1414 003 A140 i S lt wr rs m Dr Test description Test results rs Protective Earth Continuity Measured between the ground terminal of the mains connector and accessible metal parts max 0 10 ohm Dielectric Strength The leagake current Result of the test 1500 V AC is applied rejection limit is 12 5 between the mains input and mA including the the ground terminal for 1 current through EMI minute suppression capacitors Defined in the UL Client s Test Data Program passed S gnature A Earth Leakaze Current The current through the max current 0 50 mA ground lead is measured during normal operation The test is repeated with max current 0 50 mA mains polarity reversed The tests have been performed with the measuring equipment which belong to the regular Wallac calibration program Dave Tests performed by TEN Date 18 08 199 1390 3693 DECLARATION OF CONFORMITY FOR CE MARKING Address PL 10 20107 TURKU FINLAND Supplier s name WALLAC OY declare under our sole responsibility that the product Name type or model lat batch or serial number possibly sources and numbers of items 1414 Liquid Scintillation Counter Valid from serial number 4140
135. l FAC level Output to Printer POS CTIME SOFI CFMw1 CPMwe CPMws FNCT 4 Additions to Printer Listing Output to Display POS CTIME SOFT CRPMwi CPMwe CPHWwSENCTI RACKFOS CPFMH CPMHI RPT DPFHMi Additions to Display Spectrum Listing Path of File 3 G41401897 Output to File POS CTIME SQPT CPMi CRM2 CFMS FNCTL Additions to File Spectrum Listing 1993 04 01 00 00 00 205 120 ro au ma Bh nu Spectrum i Alpha Beta POCFe IG Window i 20 200 Beta dindow 2 20 200 PACKe 76 dindow 20 200 lpha Window 4 H 11 1024 Beta Window 5 E 1 1024 Beta Window amp i 1024 Beta FNCT 1 2075003 FNCTZ f FNET3 FNCTS FMCT4 FNCT4 d Unknown samples Fos CTime SAF 1 CP Mia 1 LEMIWZ CPMw3 1 742 112 01 wi oes 101 5 2229 9 2548 2 14400 376 976 4 1 OQ C 1 5 2 0 Total count rates HX ARIS sd CRM Al 558 888 CPM ch 11 82 min N4148189SP4A66SB17S8S0881B181 861 SEH 1 Bi B 168 CPM ch 231 06 min A amp 41481894P1600SH17SHH28181 001 SPH 1 m 1 14 200 308 494 GBA 600 68 WH 1BBHB IHTEGRC 58 143 A 31768 0085 CPM LB 2 4021 CPN BUNCH 4 FM 158828 97 DFHco FM EA B 199 E 28 06 Isotope Hez Half Life 12 42 Y STANDARD preparation date 01 04 93 12 00 207500 00 DPM messurement date 17 02 98 12300 159020 97 DPM decay corr decay ratio Aion 0 7612 H B 17 Am Sr amp Bg Ophss protocol PRO
136. n be initiated automatically Good laboratory practice requires that the results are identified in data files or on printouts with ID num bers The Wallac WinSpectral PosIden ID reader en ables all this PROTOCOL NO Rack number or standardization or INTERRUPT RACK Poslden system Posiden uses a barcode reader and ID labels These are self adhesive and attach to a strip of plastic the ID Clip which is then attached to the end of the sample rack The position of the clip is such that the coding can be easily read without moving the rack wherever the rack is on the conveyor The combination of ID labels and clips allow each laboratory to prepare the Hardware features and benefits needed combination of coded ID Clips to meet its nd vidual requirements The ready to use ID Clip can have labels on it as fol lows The clip for the first rack in the assay has up to two labels a label with the protocol number an optional label with the rack number for the first rack The clips for other racks in the assay need only to have the rack No label fixed them If the rack contains quenched standards the ID Chip is coded w th a label showing the quench protocol num ber 1 99 and instead of rack No a special label which identifies the samples in the rack as samples for spectrum library fine tuning For automatic interrupt counting the rack is coded with a clip with the protocol number and a special label indicatin
137. n the following information about the type of work the instrument is to be used for We would also be pleased to get some brief feedback about your opinions concerning Wallac as a company Service specialist fills in Instrument type Serial no Country Customer fills in Name amp Profession Fax no This instrument is used as described below x Main segment Data management Clinical Diagnostics Software Connections Academic Research None PC Industrial Research Ria MultiCaic Local network Environ Research Workstation Mainfame Other Rate the importance of the items below on a scale of 1 to 5 12 not important 5 very important In the column Wallac put a mark if you think the company does well for that item and a mark if you think it should do better Rating Wallac not very imp imp 1 2 3 4 5 PRODUCT PRICE OU po QUALITY amp RELIABILITY 1 I FL TECHNOLOGY FEATURES PERFORMANCE EASE OF USE DATA MANAGEMENT SUPPORT amp SERVICE SYSTEM SUPPLIER COMPANY IMAGE Other comments 6 Specifications Safety and Routine maintenance 6 1 Specifications Description Wallac 1414 001 WinSpectral 1414 002 WinSpectral oB and 1414 003 Guardian are general purpose liquid scintillation counters for counting sample vials from racks Physical dimensions Width 900 mm Height 700 mm Depth 600 mm Weight 218 kg WinSpectral 250kg WinSpectral a 6 24
138. nSpectral and can be installed later for 1414 WinSpectral ovp and 1414 Guardian it is built in Introduction Electrons from beta decays and electromagnetic gamma X ray interactions as well as Cerenkov phe nomena produce pulses consisting mainly of prompt or fast fluorescence On the other hand the heavily ioniz ing particles such as alpha particles or neutrons pro duce pulses with a more delaved slow component and are thus longer than those produced by beta parti cles WinSpectral with alpha beta separation option utilizes Pulse Shape Analysis PSA to separate be tween the long pulses typical for alpha decay and the shorter pulses typical for the gamma or beta back ground radiation The other function of this option 1s called PAC pulse amplitude comparison PAC rejects more background counts than sample counts because background pulses have greater amplitude disparity than do sample counts Adjustment of the PAC can lead to a better figure of merit Benefits The background of glass vials exhibits some slow fluorescence which is induced by cosmic and other en vironmental radiation and the inherent radioactivity of glass material Pulse shape analysis is therefore a use ful method of reducing this background in beta count ing The glass fluorescence appears mainly in the spec trum region of low energy beta particles such as those from trinum The simultaneous alpha beta separation allows you to measure alpha radia
139. nal standard quench parameter value SORE is the endpoint of the spectrum The use of Eu means that you get high precision for the SQP E due to the well defined end of the Compton spec trum and also high sensitivity for the colour correction feature due to the relatively high energy of the isotope All of these features contribute to high precision DPM results Electronic convenience So far we have been concentrating on the body of the instrument Now we turn our attention to the brains the electronics This is basically found in three racks and the detector unit The proven approach of mounting the electronics in racks allows easy upgrading and service thus reduc ing down time when any changes are made The cen tral processor unit uses a 16 bit microprocessor to en sure speedy response and data handling The electronics not only controls operation of the in strument but it communicates with PC to allow control of the counter from the PC running the Windows Win Spectral software Multiple programmable MCA Wallac WinSpectral DSA counters have a multiple programmable multichannel analyser MCA The iso tope spectrum is divided into 8 logarithmically set spectral ranges of 4096 discrete channels The tritium tange offers up to 0 0038 keV resolution this is equivalent to a 520 000 channel linear MCA The ap propriate number of linear channels are summed into 1024 logarithmic channels These retain the preci
140. nates each of the m pure isotope spectra In mathematical terms this can be expressed as a set of linear equations isotope i gt 1 2 m X24 Xm gt 1 channel Xp 2x22 d t Xn27602 channel 2 X1 T X2 F tan Cn channel n For each isotope i the individual count rate xij 15 product of the unknown activity of the isotope aj the counting efficiency e and a scaling factor 5j telling which proportion of the spectrum 1s ip each channel j While the activity and the efficiency are the same for 3 Calculation methods all channels each channel has its own scaling factor The array of scaling factors is in fact equal to the reference spectrum of the isotope i normalized so that the sum of all scaling factors equals 1 0 Thus Xij Sip di ei Sij Xi where x denotes the unknown count rate of Isotope i Using this relationship the above set of n linear equa trons can be written as SLIKIFSZIR2H SmlXm c 5 2X T dn l Am C S at S242 Sana A n En Introducing matrix notation this set of linear equa tions can be written as SX C where denotes an m by n matrix containing the m reference spectra sj C is an array or column vector comprising the measured count rates c and X is an array or row vector comprising the m unknown count rates xj to be determined In the case of single label counting the matrix is reduced to a column vector o
141. nfiguration is 64 kbyte ROM and 1 Mbyte RAM Logarithmic A D converter energy range 1 2000 keV Dual 1024 channel multichannel analyzer Built in dead time correction Performance Efficiency Counting efficiency typical 3H 68 min 64 60 HC 96 min 94 Stability Count variation less than 0 2 24 h not including random statistics 6 2 6 2 Safety and radioactive materials The following comments about precautions and safety measures in handling radioactive materials are in cluded as a guide and are not intended to be fully com prehensive More complete details may be found else where for example in the booklet SAFE HANDLING OF RADIONUCLIDES published by the International Atomic Energy Agency Vienna this may be recom mended as a useful code of practice appropriate to ra dio chemica laboratories Uniess a specially designed radioisotope laboratory is used limitations should be placed on the amount of active material in the laboratory area depending on toxicity and type of chemical operation For high tox icity material and wet chemical operations involving the risk of spillage the AEA recommend a maximum activity of about 10 CI Personne should be properly trained in the safe han dling of these materials maximum levels of stored ac tivities should be set proper records should be kept and a definite monitoring schedule maintained The areas where samples are handled should be kept cle
142. nge of the beta particle energy so that absorption in the micelles is minimized However if the sample amount ts big close to the sample holding capacity the micelle start to grow which will affect the counting efficiency Software features and benefits Sample Quality Monitor Wallac WinSpectral DSA counters include a Sample Quality Monitor which can be chosen in output selec tion see Output items in the User manual In the DPM case this monitor evaluates the amount the spectrum of the external standard and the unknown samples deviate from the library values you are using If the deviation is not significant then the monitor gives the output 100 If there is a significant deviation but one that might be accounted for by some fine tuning of the library then the sample quality monitor is below 95 You should check your sample and if it seems all right you should consider fine tuning the library you are using The Sample Quality Monitor warns you of problems with your sample as well as indicating when fine tun Ing 5 necessary Sample count rate variation monitor Statistics Monitor The problem Plastic vials are widely used in liquid scintillation counting and manufacturers tend to use plastic also as a rack material Conditions are often conducive for the build up of static charge especially when relative hu midity is low central heating and lab technicians have to use plastic gloves during sample preparation as when
143. ni E a Fig 1409 1410 1411 25 Thermostat Unit 10856321 96 10 10 FOR PART NUMBER 10856321 THERMOSTAT UNIT 10156322 930909 ITEM NO QTY ORDER NG NAME TYPE MANUF INF LINE 11310026 WIRE TIE 2 4 140 NYLON 66 370 0 080 11183018 PVUVC INSULAITING Di 5 BLACK 390 0 650 11193027 PVC INSULAITINC D4 0 BLACK 200 1 11310038 CLAMP ACC3B A 410 0 150 111341024 SILICONE TUBING 2 9 0 4 420 1 i 16858342 F C ASSEMBLY COOLING UNLT RRM 10456341 10 z 1 10255323 COOLING PROFIL ALUM PROFIL 5 5 120 NTLS 20 3 1 10256324 INSULATION BOX NTLS 40 4 1 10356325 INSULATION PE PLATE P2940 NTL5 40 5 z 10456326 FASTENING PIECE CU 10x100 NTLS 2 2 16356327 COGLING PLATE 1 CU PLATE amp 1 NTL5 6 7 4 10456328 COOLING FLATE 2 OU PLATE S 1 NTL5 70 8 4 10456329 COOLING PLATE 3 CU PLATE S 1 NTLS 80 Y 4 19456330 COOLING PLATE 4 CU PLATE 5 1 NTL5 90 10 4 10456331 COOLING PLATE 5 CU PLATE 5 1 NTL5 100 11 4 10456332 INSULATION BUSHING POM D10 NTLS 110 12 1 10256333 COVER FE PLATE S 1 NTLS 120 13 2 10456334 BUSHING POM NTLS 130 14 2 10456335 INSULATION PLATE POM NTLS 140 15 2 10456336 SCREW NTLS 150 16 2 10456337 BRACKET FE PLATE NTT 5 160 17 1 10356318 BOX ASSEMELY NTL5 170 18 4 30451961 BUSHING 6 4 1219 130 19 2 11691000 COLD ELEMENT 12V CP1 4 127 06L 190 20 2 11802009 TRANSISTOR FET SOV 124 75W N CH MOS BUZ1 200 21 2 11731007 INSULATOR TO 220 MICA MI6108 210 22 2 11450027 INSULATING BUSH TO 220 TO 3 CONNECTION 43 37 11 220 23 1 11690045 FAN 24VDC SW 800RPM
144. nificant leakage A A S o E L e e iE The source fulfils ISO 2919 requirements and is therefore classified as C43434 Date 25 Nov 1994 Signature of controller Rum Vii Raimo Kananen M Sc Physicist Quality Assurance Department Instruments T7871 yo 1099 0196 November 1995 Evaluation of the safety of the Eu 152 external standard source in Wallac 1400 series LS counters Isotope Europium 152 Maximum activity 12 microcuries half life 13 5 years Origin of radioactive material The Eu 152 radioactive matertal ts made by the Radiochemical Centre Amersham England Manufacturer of the standard capsules The Eu 152 standard capsules are manufactured by Wallac Oy Finland Manufacturing process The manufacturing process by which the radioactive standards are produced involves two steps the preparation of the radioactive material and the encapsulation of this material with a metal cover In the manufacturing process the active Eu 152 solution 1 mCi ml is absorbed homogeneously into crystalline synthetic zeollies in such a way that the activity of each active source is 12 Ci The active source ts enclosed in a stainless steel shield of thickness 0 35 mm The source is sealed first with silicon rubber and then the shield is closed by using a stainless steel pin which is held in place by pinching the shield with a special tool The wire that moves the capsule is then inserted into the shield and fixe
145. not be able to reach the instru iment It is also important that the various isotopes are stored well away from the instrument in another room Only those radioactive samples that are actually being measured should be in the laboratory at any time in order to keep the background at a low level Electric power Three electrical outlets should be available with if possible a separate power line for the instrument itself having an isolation switch and a fuse box If excessive fluctuations in the mains voltage are anticipated a mains stabilizer may be necessary Unpacking To unpack the instrument proceed as follows see fig 5 1 Cut off and remove the binding bands Open the clinching nails and hit off the cover Unpack the sepa tate packages Then open the lower clinching nails and remove the box Unscrew the fixing screws Lift the instrument up from the shipping package base and un screw the suspension bushes from the frame Check all units and accessories against the packing list Note any possible transport damage Move the instrument to its place of operation Installing the lead shielding Remove the screws holding the back panel fig 5 2 Installation information Fig 5 1 Unpacking the instrument and accessories Remove the screws Fig 5 2 Removing the screws Installation information Remove the back panel fig 5 3 Fig 5 3 Remove the back panel Fig 5 6 Releasing the inner cover
146. nting efficiency betas spilling into the alpha channel Note that the slower the cocktail the lower will be the optimum PSA level One may use a more limited win dow to include the main alpha emission range e g for Software features and benefits Ra 226 and Rn 222 Ch 600 800 is good with water miscible HiSafe cocktails A printout and a plot of RATIO vs repeat number is generated in the run and the spectra are saved The optimum PSA level for glass vial background re duction in beta counting is found in a similar way You prepare two samples one hot and one back sround sample You then step over the desired PSA levels and select the final level with e g 10 of hot counts spilling into the alpha category For rapid use without stepping you can select LOW as the default PSA level for slow cocktails and HIGH for fast cocktails How does PAC work The Pulse Amplitude Comparator PAC can be used for background reduction in uncoloured samples The sample pulse amplitudes from the left and right photo tubes differ less from each other than do the back ground pulse amplitudes since quite many of the latter ones are generated n the phototubes themselves by environmental and internal radiation Determining the PAC level To find the suitable PAC level for optimum back ground reduction an active beta sample and a blank sample are made matching the samples to be meas ured n the type of cocktail mixing ratio
147. ode is measured This ratio should be constant even if the LED output changes H the ratio changes then the gain has changed To compensate the high voltage is ad justed until the reference pulse ratio 1s back to what it was This takes care of changes to the high voltage and detectors A second feedback loop monitors the signal at the first dynode to ensure that the whole system is temperature stabilized ACSS also acts as a protection against any damage to detectors through light leaks H a leak occurs the volt age to the detectors is automatically reduced thus pro tecting them from overloading Multi section passive shielding The massive lead shielding combined with the coinct dence efectronics for the pairs of detectors reduces the background to a low level However this shielding does not make for an instrument too heavy to be con veniently handled because you can easily remove the lead shielding and then reassemble it when the instru ment has been moved to its new position The figure below shows the pieces and the order in which they should be removed from Winspectral Assembly is performed in the opposite order See the installation chapter for more information about shielding Order for removing shielding Guardian guard detector The Wallac 1414 Guardian tow level counter is equipped with an external guard detector around the sample chamber and phototubes The guard has its own phototubes and is optically isolated from
148. of the samples in a batch To do this several methods have been devel oped during the hfetime of LS counting Other methods Several methods are offered for DPM calculations in LSCs e g methods based on counting windows meth ods based on isotope spectrum quench parameters methods based on external standard quench parame ters methods based on extrapolation Efficiency 1 8 ing methods based on factory installed quench curves etc Common to these methods ts that they are not univer sal this means they are good for some applications but give bad results for others This requires a good knowledge to select the right method for any specific application Usually the methods require special calibrations quench curves to be measured which are dedicated to a specific experimental situation isotope pair cocktail colour or chemical quench etc Preparation of quenched standards checking of quench curves etc Is time consuming In dual label counting counting win dow settings are critical and different isotope ratios demand different window settings Separate stand ardizations must be done for different isotope combi nations Possible occurrence of colour quench will cause systematic errors The Wallac solution one universal method DPM counting in Wallac WinSpectral uses the DSA features the Digital Overlay Technique DOT and the use of spectrum libraries DOT is the most general method available today for quench
149. ou will find your Wallac WinSpectral counter to be a powerful and reliable aid to enable you to achieve the results you want in your work 1 15 Software features and benefits 2 User manual The User manual from the program package can be inserted in this section of the Instrument manual if desired 3 Calculation methods Calculation methods Introduction This chapter describes the path by which the Wallac 1414 WinSpectral DSA counter arrives at the final iso tope activity values using the Digital Spectrum Analy sis DSA features such as Digital Overlay Technique DOT Measured count values are combined with built in reference spectrum information which takes account of both chemical and colour quench as well as cocktail type in order to arrive at the final activity values Corrections such as those for chemilumines cence and half Ife etc are also included rf required Activity The DPM or activity a is defined as a x e y t e in which x is the count rate CPM e 1s the counting efficiency and y is the number of counts collected dur ing counting time The error in a da can be written as da 5 V dx a de Count rate For a mult label sample with rn isotopes the meas ured spectrum is the sum of m individual pure isotope spectra Hence for each channel ES j S m in the measured composite spectrum the total count rate c is equal to the sum of the individual count rates x where i IS ES m desig
150. ounting efficiency e s also a function of the two quench indices p and r The counting efficiency e is a surface function defined as I e p r hk N p p rer ho k 1 where Ax are parameters defining the shape of the surface Ap is a constant and px and rk are coordinate pairs defining a grid lattice on the surface The error in e de is a function of the errors in p and r dp and dr hk p pt p pi rn ho er i 9 y hic r rk Or O kal r rk ho and finally 3 de de e a dp ut dr dp Total quench index CHEMICAL QUENCH SERIES Al Mil The total quench index p is defined by the expression Lori fell Calculation methods in which j denotes the pulse height channel denotes the upper pulse height limit 2 denotes the lower limit and z is a constant 0 01 The external standard spec trum is here rather treated as a continuous distribution c j instead of a discrete distribution c m order to ta cilitate greater detail in determining p which is hence not an integer but a real number H e dj z cr P The error dp is given by the expression VOA ee Horie 5 1 27 Z car for j Colour index COLOR QUENCH SERIES a NN IA The colour index r is defined by the equation Ya Yb where ya denotes the number of counts above the left right or night left pulse height criterion l
151. r 1 50 2019 0 0 0 1000 800 600 400 20D 200 EEPROM LISTING LEC 200 AO 110 Al TEMP 25 0 CONV STEPS 114 1 0 Mapping data DEM SOPIE Channels WLIB TRUE TRUE WLIB H3 0 0 0 0 0 0 MAPPING 48 9 58 4 9 5 300 95 0 99 2 4 2 202400 140 4 142 5 2 1 6 01 159 3 150 6 1 3 0 06 Checking time i0 177 4 178 0 0 6 Clear 195 7 195 8 0 1 HiSafe 214 8 214 3 0 5 Halflife 682 9 695 2 12 3 745 1 768 1 22 1 1994 08 01 12 00 00 798 6 834 1 35 5 886 0 977 9 91 9 SOPE SOPer 94 7 993 6 98 5 Listing 1000 0 1000 0 0 0 Beta Total activity H3 201800 0 DPM 3 363kBq H3 Eff amp S PE SQPer 1 60 977 87 0 04 Mapping Reference counter B Actual counter 600 1000 200 400 7 Spare parts information 1410 951 05 November 1995 1409 1410 1411 1414 1415 Spare Parts Catalogue AN Z EGzG COMPANY Wallac Oy P O Box 10 FIN 20101 Turku Finland Tel 358 2 2678 111 Telex 62 333wac fin Telefax 358 2 2678357 Ordering Information f parts are being ordered from Wallac Oy give the following information on the order Purchase order number Type and serial number of the instrument for which the spare part Is intended Quantity of each item ordered Ordering number and description obtained from parts list Where the parts are to be sent When the order is to be dispatched Preferred mode of transport Note Subassemblies with an order number beginning 10 84xxxx 1085
152. s or five times the length of the sample counting time Background correction proceeds as follows Firstly one or more background samples are measured and a background spectrum accumulated Then using the spectrum stripping technique the background spectrum is subtracted channel by channel from the sample spectrum This gives you a reliable background correc tion Note If you use both background samples and refer ence samples then the positions of the background samples must be immediately before those of the refer ence samples and start from position 1 If there are only reference samples they must begin from position 1 No empty positions are allowed DPM counting DOT DPM Why the need for DPM correction A fact which makes LS counting unique among ana lytical methods is that each sample is also a unique detector Usually analytical methods are based on the principle that the sample emits radiation or some form which 1s measured in an external detector e g gamma counter or an external source sends radiation which is absorbed by the sample e g spectrophotometric meth ods In LS counting each sample consists of the actual sample mixed with the detector the scintillation cock tail Thus counting efficiency is dependent on sample type sample to cocktail ratio volume colour of the sample cocktail type etc The counting efficiency vari ation from sample to sample must be corrected for to allow comparisons and analysis
153. sion of the origmal analogue to digital conversion of 0 0038 keV per channel This feature makes possible the DSA features such as ChennStrip method of chemiluminescence correction 1 6 spectrum stripping background correction and DOT DPM calculation Internal disk drive The counter has an internal disk drive with a 3 5 mi crofloppy disk which contains the program The pro gram disk can easily be changed to accommodate pro gram changes and updates This is a much simpler pro cedure than changing chips on an electronic circuit board This drive is behind the cover at the front of the conveyor as shown on page 1 To access the drive you must slide the cover upwards to release it External personal computer The WinSpectral Windows software runs on any 386 SX 486 SX or PENTIUM computer Since our counters are designed to work within standard PC ar chitecture you can be assured that WinSpectral will serve you long beyond the 486 generation of com puter Bench top or floor standing A Wallac WinSpectral DSA LSC can be either bench top or floor standing You can select which ever ts most convenient for your working environment The Wallac Floor Stand allows the counter to become floor standing and easily movable without having to collect together lots of separate pieces of equipment The monitor arm and a pullout shelf for the PC key board and mouse are standard features whether or not you use the Floor Stand Thes
154. splay spectrum Window 1 Window 2 Window Window 4 Wi 5 Window FNCT1 FNCT2 FNOTZ FMCTS FNCTS FNCT4 FNCT4 Unknown samples Fos CTime HS_CPM i 222 127295 7 i 225 127472 4 1 223 127405 0 i 223 127462 2 muu muu mr m HE ee Hrb Hiriek brim irimi mm mikuni r r rr da wz Listing spectrum Beta 11 1074 Beta 1 10Z4 Beta 1 1024 Beta i1 i1024 Beta 1024 Beta 1 1024 BHeta Eu he En aH nh u gE Bil tn kit 514 CPM iF 1 SUFE 1278402 2 176 41 F66 42 127586 7 l 5 99 66 1 127207 1 176 00 9TRA535 14 127565 1 1768 01 9769 16 prr 1 17 dr S ir ri risa sn oram ani hr rrr Midi m EEE WLIALL DEE L L4 LLLE LELA Koi Link ee ee eee ee FEREF o 1 5 Pos fime H2 CRM 27 z263y0 0 2 pap 707 7 273 27140 1 2 27 eto FES a 5 O 263790 130 4 Pos CTime HS CPM A 1200 19 0 E O00 i7 1 E 1200 15 7 a 1 200 16 7 LADO l PES Total count rate REPEATS 127509 8 176 09 965 71 Mean 76 7 0 22 0 66 St Dev C14 CPM SPI SQPE 102616 2 419 99 963 68 102489 5 419 50 961 01 102521 8 419 29 961 53 102098 8 419 38 963 236 102431 6 419 52 9562 40 Mean 228 3 0 26 SZ St Dev C14 CPM Sar I SQPE weet ee Fah OS owe oP 9 9767 15 23 2 412 357 966 159 24 1 407 87 968 22 wen ae em emt at um nee a rf ae F REPEATS Z35366 I 966 97 Mean 0 5 12 270 1 07 St Dev 455 154415 7 CPM Ci4 229964 9 C
155. sponding to g predetermined percentage values fractiles of the total integral intensity Conversion of spectrum to FIP format Differential shape of standard spectrum counts per channel Fractile 95 3 2 210095 Thus each spectrum is reduced to g fractile channels with value b The b values depend on the quench level in a well behaved manner which can be described as a function of a suitable quench index In Wallac WinSpectral two quench indices are used the total quench level SQP E or p and the colour quench level Colour or r The variable p is equal to the overall quench level index determined from the end point of the external standard spectrum see be low while r is equal to the colour index determined from the left right dispersion of the external standard pulses see below Thus each fractile channel by can be described by surface function of the form balp 2 Y hux N pp er ho for 1 lt u lt g k 1 where Ay k are parameters defining the surface Ag is a constant and px and r are coordinate pairs defining a grid lattice on the surface The constant Ao and the grid points pk and rz are the same for all b parame ters A complete reference spectrum is arrived at by first computing the by parameters interpolating this array and differentiating the result Notice that errors in the reference spectra are considered to be unimportant Counting efficiency The c
156. srsoT ms a nir sTrs an M ar mr a Load some racks with ID labels then start countine and check that the instrument wil change the protocoi as required by the labels Performance test with Easy GLP To define the proper values for GLP you have to make an initial measurement of the local background Make sure that al stationary and moving gamma sources are removed from the neighbourhood of the instrument Use at least 300 s measurement time Start the editing of the Easy GLP protocol see page 52 in the User manual Type the values of the sup plied standards into the text box marked Reference samples The isotope windows are 5 350 for H and 5 650 for C The measurement time should be 300 s or fonger and the precision 0 5 Test values are as follows where FTDS means the Final Test Data Sheet included with the Instrument manual local backe ne ee from FTDS value from value local ase t nnd from FTDS value The minimum and maximum background warning limits for GLP are calculated from the value meas ured during installation 36 Some example back grounds and 3G limits are Observed background 36 o 46 50 95 36 40 31 35 26 30 21 25 16 20 1 15 s p Pa TOR D 150 e r3 feo fem ito C ta installation information E g if your background is 21 then 36 is 6 7 which means the minimum and manximum limits are 14 3 and 27 7 respectively You can calculate
157. standards are calibrated against reference standards of n hexadecane 1 14C supplied by the National Institute of Standards and Technology Standard Reference Material SRM No 4222C the estimated accuracy of which was 0 81 The absolute activity of the standards is within 0 5 of the reference standards of NIST SRM s f On behalf of ihe Quality Control Department V lac Oy P O Box 10 SF 20101 Turku Finland UNQUENCHED LSC STANDARD for Liquid Scintillation Counter Product No 1215 111 CERTIFICATE Hadioactive isotopes tritium carbon 14 and blank The absolute activities of standards and the reference dates for all standards are as follows 3 194500 _ dpm 1 Jul 1997 Ref Date 140 106000 dpm _ Nov 1997 Ref Date Blank _ Feb 1997 Ref Date The 1215 111 is from the production Lot No 9702 A Definition of Use The 1215 111 unquenched standards set is intended for use with LS counter Serial No 4707 to calibrate the instrument and measure day to day H and 1405 counting efficiencies and background for comparison with original factory specifications and for verifying stable system performances For specific instructions on the use of these standards with an LS counter the Instrument manual should be consulted Precautions on Storage and Use Fluors are susceptible to photo chemical degradation The standard set should be stored in a dark place at room temperature Recommended shelf life
158. switched on then there will be a message No response from counter Starting the counter Lift ehe instrument cover and then the diskette drive cover This latter should be lifted straight up first to release it Then insert the instrument program diskette into the diskette drive in the counter and replace the cover Do not remove the program diskette Switch on the counter The message on the status bar wil change to Counter online During the loading process the status bar will show the following mes sages Loading DOT Loading texts and Loading 1400 program When the program is completely loaded the message Counter idle will appear Load ing takes some 2 minutes Note The program diskette labelled BACKUP may also be used but be sure to always have program diskette in addition to the one in the instrument When needed make a backup copy using the Backup instru ment disk function in the System menu It is also rec ommended that from time to time you make a backup copy of your program diskette to save your own proto cols and spectrum libraries Note You should also make backup copies of the WinSpectral program diskettes before use Use e g the Copy disk function in your Windows File manager Carrying out a functional check of the instrument For checking the instrument mechanically and for checking the function of the ID reader proceed as fol lows 5 5 Installation information II ra
159. tiCalc In WinSpectral go to System Options Directories and give the MultiCalc assay path as CAWIACALCOCOMWINBETA From the MultiCale main menu select F4 PROTO COLS and create a new protocol The name should be a short one e g MCASS Select the protocol type e g RATIO and edit the the protocol or use the default settings Save the protocol After you exit from Protocol editing go to the main menu and select from there Fi COUNTER MultiCale is then ready to evaluate results from WinSpectral Switch now to the WinSpectral program Setting up a protocol in WinSpectral Creafe a protocol for any user group and give the pro tocol the same name as you gave for the assay proto col WinSpectral allows longer protocol names but use MultiCalc installation exactly the same name as for the assay protcol e g MCASS Set the counting time and the isotopes used Then go to Output devices and select Filing data Click the More button and select MultiCalc export Save these settings You are then ready to run the protocol WinSpectral will receive data and save it on the hard disk of the PC As the samples in the assay are being counted WinSpectral will create a file in the Multi Calc communication protocol directory MultiCale will find the file and start evaluating it in about 30 seconds depending on the speed of your PC and the amount of time you have given for DOS applications INSTALLATION REPORT APPENDIX Please fill i
160. tion with a back ground of less than CPM The sensitivity for alpha detection approaches the detection limit for semicon ductor alpha particle detectors but with considerably simpler sample preparation The ability to simultaneously measure gross alpha and gross beta activity reduces the workload in the fabora tory because the alpha detection level is sufficient to detect alpha activity at the picocurie activity levels which are the allowed activity limits Moreover simultaneously with the measurement of al pha radiation beta radiation from the decay chain can be detected and analyzed The beta spectrum may con tain also Cerenkov radiation conversion electrons Compton electrons X rays and Auger electrons if they are being produced tn the sample The PSA PAC features can also be used to discrimi nate a part of the background pulses from the sample pulses The best benefit of this is obtained when glass vials and a fast scintillator are used Especially in low energy beta counting considerable reduction of glass vial background can be achieved by using the PSA Due to this alpha beta separation feature Wallac Win Spectral with this option has a lower background than a standard LS counter Thus the improved sensitivity can be used to minimized sample volumes and specific activity with savings in consumables and waste as a result Note vial carriers as an guard for small vials can be used to further improve background values
161. ults without the use of the external standard The method is based on the Digital Overlay Technique This means that no counting window is required To use the SQPG DOT you need to make a quench standardization or fine tuning of one of the HiSafe or Xylene quench data sets in the Wallac library The standard spectra and the counting efficiency are stored as a function of the SQP I instead of the external standard quench parameter The fine tuned spectrum library can then be combined with counting protocols to obtain DPM results of un known samples Depending on the number of protocols 15 or 100 the SOP D DOT option allows you to make 14 or 99 quench standardizations Software features and benefits Dual DOT CPM DPM This offers you dual label counting without using the external standard You need to make two fine tunings one for each isotope to be used to label unknown sam ples For each fine tuning you must only use one standard and the chemical and colour quenching of these two standards must be the same Samples can have quench levels which differ to some extent from those of the standards because the Accuracy Enhance ment procedure takes account of this When you define the DPM counting protocol you specify the two isotopes to be used then the program prompts you to give the numbers of the two sets of fine tuned data Alpha beta separation and background reduction option Note this feature is an option for 1414 Wi
162. unt If you do not want to set parameters then you can use the Easy Count feature You simply toad the samples and click the Easy Count button The DSA feature al lows the counter to determine automatically which so H tope you are using from a selection of three CH or C are the defaults and then counts the samples An Easy Count protocol can also be initiated by using a special ID label on the racks Easy Count is described in detail in the User manual Easy GLP Compulsory daily calibration the so called GLP Good Laboratory Practice feature has proved inade Software features and benefits quate in older generation counters since minor tem peraiure fluctuations or voltage changes can affect the response at any time The basis for Wallac WinSpectral s superior perform ance is Wallac s patented ACSS feature see the pre vious chapter on Hardware features The GLP protocol allows you to quickly set parame ters for the monitoring of up to 8 performance parame ters for GLP and get a ready formatted report after the run CPM counting Introduction CPM counting s used when sample preparation is ex pected to yield samples with close to constant counting efficiency This means that the results of the sampies in an assay can be compared with each other and used in further data analysis A typical CPM application is filter counting Wallac WinSpectrai allows you to select from six common isotopes plus an addit
163. upplement Fig No Fig Name Page Win Spectral 1414 001 95 99 Alpha Beta 1414 002 99 101 Guardian 1414 003 102 104 Fig 34 LSC Assembly 105 Fig 35 Body Assembly 107 109 Fig 36 Top Cover Assembly 110 111 Fig 37 Keybank Assembly 112 113 1409 1410 1411 Spare part kit 1410 201 96 10 16 FOR PART NUMBER 1410 201 SPARE PART KIT 1410 1410 201 960731 ITEM NO GTY ORDER NO NAME TYPE MANUF INF LINE 1 11550141 SERVICE RIT 590 400 260 EIRI 10 1 10853316 P C ASSEMBLY POWER SUPPLY DPA 10353503 al 1 10856466 F C ASSEMBLY MICRO COMPUTER DCD 10356455 30 1 10956730 DCD EXPANSI N RIT DCD 10356465 40 1 10854654 P C ASSEMBLY 1 0 BOARD DIC 10354393 20 1 10853314 P C ASSEMPLY MCA DIA 10353517 60 1 10354606 P C ASSEMBLY MCA DIE 10354603 70 l 10854021 P C ASSEMBLY MOTOR CONTROL BOARD HPS 10354022 B l 1085486572 P C ASSEMBLY HV SUPPLY EPM A 10354653 90 1 10857670 P C ASSEMBLY COINCIDENCE BOARD LACH 10157727 100 1 10854767 P C ASSEMBLY MCA INTERFACE LCH LBR 10354766 118 1 10857571 P C ASSEMBLY SAMPLE amp HOLD ICH LAD A 10337728 120 l 10860105 P C ASSEMHBLY GAIN STABILIZER EBU A 10360197 130 1 10852642 P C ASSEMBLY POS HV SUPPLY EPE 10652641 140 1 10853857 P C ASSEMBLY PREAMP AND COINS BOARD LAB A 150 L 10859023 P C ASSEMBLY A D CONVERTER EBZ 10352027 140 1 10858037 P 2 ASSEMBLY SAMPLE AND HOLD EBC A 10358036 170 2 103546579 P C ASSEMBLY EXTENSI N BOARD LPA 180 H 10849795 P C ASSEMBLY POWER EXTENSI N BOARD 10649755 190 1 1185890042 S
164. ut to File Listing a E a Listing Spectrum a 4140189 xn wu ah POS CTIME SQPI CPML CPM2 CPM3 FNCT1 Additions to File Spectrum Window Window Window Window Window Window FNCT 1 FNCTZ FNCT S FNCT4 Oo Of b id EJ FNCT 1 FNETZ FNCTS FNC T4 H d od H Unknown samples Pos Clime SGP 1 CFIw 1 1 115 259 950 76617 2 2 44400 476 975 1 2 Total count rate Spectrum Listing s Beta 200 500 Beta 200 500 FACkRej z ZOO 500 Alpha 1 1924 Beta 1 1024 Beta i 1024 Heta 100XCPHW1 103600 En wk Wm CE Mw CPMws FNCTI 2381 97 1225 1 75 9 0 4 1 O O C14 89774 1 CFM ini 396 666 CPM ch 1 81 min 4 1414818MP1545816158818161 B81 SPH 1 BJ 8 052 CPM ch 231 14 min 6 4148189 XP15058156 380828181 081 SPH 1 TIN WE 1 igg 25 388 448 SHH 606 7660 BB 988 INTEGRC 268 4913 CA 77678 8865 CPM B 1 177 CPM BuNCH 4 FM 183600 640 DFM FM LAl iBl 4777 E 74 98 2 16 3h qs 8 12 PROTOCOL PROTOCOL DATE 1998 02 17 TIME 20507 FILE ff 42140109GF1509017 TXT ID P164s017 Waiiac 1414 WinSpectral v1 30 S N 4140189 Counting mode CRM Isotope is H3 H wo 550 12 45 y Frotocol name Sh qs 6 12 PROTOCOL Counting time 14400 Repeats Cycles 1 Replicates 1 sigma 4 50 dinimum cpm 9 00 Checking times 10 Advanced modes Halflife PSA PAC Halfiife zerotime Zeratime of HS PSA leve
165. ve is called the coinci dence resolving time of the detectors If two chemilu minescence or other random events occur within the coincidence resolving and so that each triggers one of the detectors then the result will look like a true multi ple photon event and will be counted If there is a high rate of chemiluminescence events many of these ran dom coincidences will occur resulting in false count results The DSA feature ChemiStrip a unique pat ented spectrum stripping chemiluminescence correc tion method solves this problem The counter has five 1024 channel MCAs ChemiStrip uses one MCA to store the combined sample and chemiluminescence spectrum and another the chemilu minescence alone This second spectrum is obtained by making use of the difference between the chemilu minescence and sample spectra The latter comes from discrete bursts of photons which occur within the cain cidence resolving time of the detectors If the signal from one detector is delayed relative to the other then no coincidence will occur and no count wil be re corded in the delayed spectrum MCA In the case of chemiluminescence the spectrum ts formed by an al most continuous flood of photons This means that there is Just as much chance of a random coincidence between two single photon events occurring at the same time as there 1s between one event and the de layed signal of a previous event The chemilumines cence events will thus contr
166. ve two types but also racks of twenty four 4 ml samples These can be in any order A 20 ml sample rack can hold twelve samples with a maximum vial diameter of 28 4 mm The conveyor will accept 28 racks making a full load of 336 sam ples The corresponding figures for 6 ml vials are 18 4 mm diameter 18 samples per rack and 40 racks on the conveyor making 720 samples in all For 4 ml vials the figures are 13 4 mm diameter 24 samples per rack 52 racks per conveyor load Le 1248 samples 20 mi sample rack Racks for different vial sizes accepted by the FlexiRack system The maximum height allowed for the top of a vial above the conveyor is 78 mm This means that for a Hardware features and benefits vial of the maximum diameter in any of the categories its length can be up to 68 mm Smaller vials in any category can be a few millimetres longer Not only flat bottomed vials can be accepted but also round bottomed and conical vials For example adapt ers allow Eppendorf tubes and Microfuge tubes to be counted directly without the need for carrier vials Users with different vial sizes can load their own batches of samples on the same conveyor at the same time Posiden ID reader The purpose of the ID system is to allow hands off performance of the instrument and to enable total re sults identification Hands off means that counting procedures such as changes of protocol quench fine tuning or stat counting ca
167. xxxx or 1086xxxx are kept as stock items It should be noted that these subassemblies consist of several smaller parts which can be ordered as separate items if necessary using the corresponding order numbers Index 1409 1410 1411 LSC Fig No Fig Name Spare Part Kit LSC Model 1409 001 LSC Model 1410 001 LSC Model 1411 001 Fig 01 LSC Assembly Fig 02 Body Assembly Fig 03 Sample Conveyor Fig 04 Floor Stand Fig 05 Top Cover Assembly Fig 06 Sample Changer Fig 07 Power Unit Fig 08 Elevator Assembly Fig 09 External Standard Fig 10 Measuring Unit Fig 11 Preamplifier Unit Fig 12 Optics Fig 13 ID Unit Fig 14 Light Shutter Unit Fig 15 Motor Unit 1 Fig 16 Motor Unit 2 Fig 17 Count Weight Fig 18 Support 1 Assembly Fig 19 Support 2 Assembly Fig 20 Plate Assembly R Fig 21 Plate Assembly L Fig 22 Spring Assembly L Fig 23 HV Divider Unit Fig 24 Display Unit Fig 25 Thermostat Unit Page 5 7 8 8 9 10 13 15 17 19 21 22 23 24 25 26 27 29 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 92 53 54 55 96 57 06 59 60 61 63 65 67 69 70 71 INDEX CONT 1415 Supplement Fig No Fig Name Page Fig 26 LSC Assembly 73 79 Fig 27 Measuring Unit 80 81 Fig 28 Optics 82 83 Fig 29 Light Shutter Unit 84 85 Fig 30 Top Cover Assembly 86 87 Fig 31 Guard 88 89 Fig 32 HV Divider Unit 90 91 Fig 33 Display Unit 92 93 1414 S

1414 WinSpectral Manual - Faculté de médecine de l`université d

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1414 WinSpectral Manual - Facult&eacute; de m&eacute;decine de l`universit&eacute; d

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1414 WinSpectral Manual - Faculté de médecine de l`université d